NCG550274_Lab Data_20240724

Ms. Bernard, sorry for the delay in getting this
to you.
Thank you so much for your guidance
throughout the process, it's much appreciated.
Bill Hirt
581 Hideaway Lane
Leasburg, NC 27291
248-494-2049
[e-mail]
NCG550274
1
JUL Z 4 2424

�cea
July 16, 2024
One Time Client
Private Small Jobs
Huntersville, NC 28078
RE: Project: Private Client Annual
Pace Project No.: 92738286
Dear One Client:
i� V ])C,-)! of Quality
JUL L 4 2024
Ralpig Rego-na Yzc�
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on June 25. 2024. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNIINELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Eden
• Pace Analytical Services - Raleigh
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
inj � )
,7 Jiv, 4, l J` w1--
Ashari Taylor -Watson
[e-mail]
704-977-0939
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
-I•is report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC,
Page 4 of 22

Protect: Private Client Annual
Pace Project No,: 92738286
Pace Analytical Services Raleigh
4915 Waters Edge Dr. #120, Raleigh, NC 27606
North Carolina Wastewater Certification #: 67
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
FloridalNELAP Certi ication #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
Pace Analytical Services Eden
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
CERTIFICATIONS
North Carolina Drinking Water Certificat on #: 37731
South Carolina Laboratory ID: 99030
South Carolina Certification # 99030001
VirginialVELAP Certification #: 460222
North Carolina Wastewater Certification #: 633
V rg'niaNELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 22

Pace Analytical Services, LLC
9800 Kincey Ave. Suite100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Private Client Annual
Pace Project No.: 92738286
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92738286001 OUTFALL-001 SM 254OD-2015
JMM2
1
PASI-E
SM 521OB-2016
VLG
1
PASI-E
SM 9222D-2015
MF
1
PASI-R
SM 4500-CI G-2011
JMH1
1
PASI-A
TKN+NO3+NO2 Calculation
MDW
1
PASI-A
EPA 350.1 Rev 2.0 1993
SSW
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
EGC
1
PASI-A
EPA 365.1 Rev 2.0 1993
NCF
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-E = Pace Analytical Services - Eden
PASI-R = Pace Analytical Services - Raleigh
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLf,. Page 3 of 22

(--Pace
ANALYTICAL RESULTS
Project: Private Client Annual
Pace Project No.: 92738286
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: OUTFALL-001
Lab ID: 92738286001 Collected: 06/25/24 10:45
Received: 06/25/24 1322 Matrix: Water
Parameters
Results Units Report Limit DF
Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 254OD-2015
Pace Analyt cal Services - Eden
Total Suspended Solids
46.4 mg1L 11.4 1
06/26/24 14A6
52108 SOD, 5 day EDN
Analytical Method: SM 521OB-2016 Preparation Method: SM 521OB-2016
Pace Analytical Services - Eden
BOD, 5 day
22.1 mg1L 2.0 1
06/26/24 16:10 07/01/24 15:59
MBIO 9222D Fecal Coliform RAL
Ana:ylical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytica Services - Raleigh
Fecal Cn;iforms
ND CFU1100 mL 1.0 1
06/25/24 15:10 06/26/24 14:25
4500CL G Chlorine, Residual
Analytical Method: SM 4500-CI G-2011
Pace Analytical Services - Asheville
Chlorine, Total Residual
8.4 mg1L 1.2 -M
07/03/24 13:33 7782-50-5 H3
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Pace Analytical Services -Asheville
Total Nitrogen
52.2 mg1L 0.040 1
07/10/24 14:00
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg1L 0.10 1
07/08/24 20:54 766441-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation
Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Kjeldahl, Total
3.2 mg1L 0.50 i
07/09/24 20:56 07/10/24 08:15 7727-37-9
353.2 Nitrogen, N021NO3 pres.
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analyt cal Services - Asheville
Nitrogen, NO2 plus NOS
49.0 mglL 0,40 10
07/10/24 13:02
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phcsphor.is
4.8 mg1L 0.050 1
07/03/2414:06 0710512417:48 7723-14-0
Date: 07/16/2024 10:03 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written co"seni cf Pace Analytical Services, LLC.
Page 4 of 22

�ce�
QUALITY CONTROL DATA
Project: Private Client Annual
Pace Project No.: 92738286
Pace Analytical Services, LLC
9800 Ki-cey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
QC Batch: 864312
Analysis Method:
SM 254OD-2015
QC Balch Method: SM 2540D-2015
Analysis Description
2540D Total Suspended Solids
Laboratory:
Pace Analytical Services - Eden
Associated Lab Samples: 92738286001
METHOD BLANK: 4455883
Matrix: Water
Associated Lab Samples: 92738286001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Suspended Solids
mg1L
ND
2.5 06/26/24 14:41
LABORATORY CONTROL SAMPLE: 4455884
Spike LCS
LCS % Rec
Parameter
Units
Cone. Result
% Rec Limits Qualifiers
Total Suspended Solids
mg1L
250 248
99 90-110
SAMPLE DUPLICATE: 4455885
92738522001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg/L
167
160 4
Results presented on this page are In the units Indicated by the "Units" column except where an aitemate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in lull.
Date: 07/16/2024 10:03 AM without the written consent of Pace Ana ytical Services, L L.0 Page 5 of 22

(--Facem
Project: Private Client Annual
Pace Project No.: 92738286
QC Batch: 864311
QC Batch Method: SM 521OB-2016
Associated Lab Samples: 92738286001
METHOD BLANK: 4455879
Associated Lab Samples: 92738286001
Parameter
BOD, 5 day
QUALITY CONTROL DATA
Analysis Method: SM 521OB-2016
Analysis Description 5210B BOD, 5 day Final EDN
Laboratory: Pace Analytical Services - Eden
Matrix; Water
Blank Reporting
Units Result Limit Analyzed Qualifiers
mg1L ND 2.0 07/01/2414:33
LABORATORY CONTROL SAMPLE: 4455880
Spike LCS
Parameter Units Conc. Result
BOD, 5 day mg/L 198 185
SAMPLE DUPLICATE: 4455882
92738341001 Dup
Parameter Units Result Result
SOD, 5 day mg/L 9.0 ND
Pace Analytical Services, LLC
99M Kincey Ave. Suite 10C
Huntersville, NC 26070
[phone]
LCS % Rec
% Rec Limits Qualifiers
93 84.6-115
RPD Qualifiers
B2
Results presented on this page are in the units I9dicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 07/16/2024 10:03 AM without the written consent of Pace Analytical Services, LLC
Page 6 of 22

ce°
QUALITY CONTROL DATA
Project: Private Client Annual
Pace Project No.- 92738286
QC Batch: 864549 Analysis Method: SM 9222D-2015
QC Batch Method: SM 92220-2015 Analysis Description: 9222D Fecal Coliforrn(MF) - RAL
Laboratory: Pace Analytical Services - Raleigh
Associated Lab Samples: 92738286001
METHOD BLANK: 4457168 Matrix: Water
Associated Lab Samples: 92738286001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms CFUI100 mL ND 1.0 06/26/24 14:25
SAMPLE DUPLICATE: 4457169
92738286001 Dup
Parameter Units Result Result RPD Qualifiers
Fecal Coliforms CFUI100 mL ND ND
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 07/16/2024 10:03 AM without the written consent of Pace Analytical Services, LLC.
Page 7 of 22

(--Pace"
QUALITY CONTROL DATA
Project: Private Client Annual
Pace Project No.: 92738286
QC Batch: 865968 Analysis Method: SM 4500-CI G-2011
QC Batch Method: SM 4500-CI G-2011 Analysis Description: 4500CL G Chlorine, Total Residual
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92738286001
METHOD BLANK: 4464003
Associated Lab Samples: 92738286001
Parameter Units
Chlorine, Total Residual mglL
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.024 0710312413:25
SAMPLE DUPLICATE: 4464004
92738286001 Dup
Parameter Units Result Result
Chlorine, Total Residual mg/L 8.4 8.4
RPD Qualifiers
1 H3
Pace Analytical Services, LLC
9804 Kincey Ave. Suite 100
Huntersvitle, NC 28078
[phone]
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right ofthe result.
REPORT OF LABORATORY ANALYSIS
Th!s report shall net be (eproduced, except in full,
Date: 07/16/2024 10:03 AM wit--)ul the written consent of Pace Analytical Services, LLC.
Page 8 of 22

(-) a' c e �
Project: Private Client Annual
Pace Project No.: 92738286
QC Batch: 866641
QC Batch Method: EPA 350.1 Rev 2.0 1993
Associated Lab Samples: 92738286001
METHOD BLANK: 4467058
Associated Lab Samples: 92738286001
Parameter Units
Nitrogen, Ammonia mg/L
QUALITY CONTROL DATA
Analysis Method: EPA 350.1 Rev 2.0 1993
Analysis Description- 350.1 Ammonia
Laboratory: Pace Analytical Services - Asheville
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.10 07/08/24 20:20
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28070t
[phone]
LABORATORY CONTROL SAMPLE: 4467059
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Ammonia mg1L 5 5.3 ` 107 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4467060 4467061
MS MSD
92738156001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg1L ND 5 5 5.7 5.7 113 113 90-110 0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4467062 4467063
MS MSD
92738209001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg1L ND 5 5 5.4 5.4 107 108 90-110 0
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except n fu 1,
Date: 07/16/2024 10:03 AM with:3Ut the written c� nsent of Pace Analytical Services, LLC,.
Page 9 of 22

(--FaCe�
Project: Private Cl ent Annual
Pace Project No.: 92738286
QC Batch: 866875
QC Batch Method: EPA 351.2 Rev 2.0 1993
Associated Lab Samples: 92738286001
METHOD BLANK: 4468014
Associated Lab Samples: 92738286001
Parameter Units
Nitrogen, Kjeldahl, Total mglL
QUALITY CONTROL DATA
Analysis Method: EPA 351.2 Rev 2.0 1993
Analysis Description: 351.2 TKN
Laboratory: Pace Analytical Services -Asheville
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.50 07/10/24 08:13
LABORATORY CONTROL SAMPLE: 4468015
Spike
Parameter Units Conc,
Nitrogen, Kjeldahl, Total mg/L 10
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LCS LCS % Rec
Result % Rec Limits Qualifiers
10.3 103 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4468967 4468968
MS MSD
92738929001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mg1L 13.9 10 10 19.9 24.7 60 108 90-110 22 M1,R1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4468969 4468970
MS MSD
92738929002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua]
Nitrogen, Kjeldahl, Total mg1L 3.3 10 10 13.7 13.3 104 100 90-110 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/16/2024 10.03 AM without the written consent of Pace Analytical Services, LLC.
Page 10 of 22

aceR
QUALITY CONTROL DATA
Project: Private Client Annual
Pace Project No.: 92738286
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 867021
Analysts Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993
Analysis Description: 353.2 Nitrate + Nitrite, preserved
Laboratory. Pace Analytical Services - Asheville
Associated Lab Samples: 92738286001
METHOD BLANK: 4469040
Matrix: Water
Associated Lab Samples: 92738286001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Nitrogen, NO2 plus NO3 mglL
ND 0,040
07/10/24 11:48
LABORATORY CONTROL SAMPLE: 4469041
Spike LCS.
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Nitrogen, NO2 plus NO3 mglL
2.5 2.5
99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4469042 4469043
MS MSD
92738151002
Spike Spike MS
MSD MS MSD
/. Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Nitrogen, NO2 plus NO3 mglL ND
2.5 2.5 1.9
1.9 77 78
90-110 1 M1
MATRIX SPIKE 8, MATRIX SPIKE DUPLICATE: 4469044 4469045
MS MSD
92738151003
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Nitrogen, NO2 plus NO3 mglL ND
2.5 2.5 2.0
2.0 82 81
90-110 1 M1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except to fu,,
Date: 07/16/2024 10:03 AM without the written consent of Pace Analytica Serviceu, t I C.
Page 11 of 22

(--Face"
Project: Private Client Annual
Pace Project No.: 92738286
QC Batch: 865763
QC Batch Method: EPA 365.1 Rev 2.0 1993
Associated Lab Samples: 92738286001
METHOD BLANK- 4463164
Associated Lab Samples: 92738286001
Parameter Units
Phosphorus mg1L
QUALITY CONTROL DATA
Analysis Method: EPA 365.1 Rev 2.0 1993
Analysis Description: 365.1 Phosphorus, Total
Laboratory: Pace Analytical Services - Asheville
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.050 07105/2417A0
Pace Analytical Services, LLC
9800Ki1ceyAve Suile100
Hwtersvilla, NC 28078
(71)4)875-9092
LABORATORY CONTROL SAMPLE: 4463165
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Phosphorus mg1L 2.5 2.5 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4463166 4463167
MS MSD
92738286001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mglL 4.8 2.5 2.5 7.4 7.4 101 102 90-110 0
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 4463168 4463169
MS MSD
92738325001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone, Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg1L 2.1 2.5 2.5 4.5 4.4 94 93 90-110 0
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date. 0716-2024 10:03 AM v*hni.t the written consent of Pace Analytical Services, LLC.
Page 12 of 22

(-�Face�
QUALIFIERS
Project: Private Client Annual
Pace Project No.: 92738286
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit,
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
OUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropr.'ate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4.5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylam.ne using Method 8270, The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN - The NE LAC Institute.
ANALYTE QUALIFIERS
82 Oxygen usage is less than 2.0 for al' dilutions set. The reported value is af� estimated less than value and is calculated
for the dilution using the most amount of sample.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
r h s report shall not be reproduced, except in full,
Date: 07/16/2024 10:03 AM wits -out the written consent of Pace Analytical Services, I.I.C. Page 13 of 22

(--Pace"
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project'
Pace Pro.ecl No..
Private Cl ent Annual
92738286
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92738286001
OUTFALL-001
SM 254OD-2015
864312
92738286001
OUTFALL-001
SM 521OB-2016
864311
SM 521OB-2016
864824
92738286001
OUTFALL-001
SM 922213-2015
864549
SM 9222D-2015
864551
92738286001
OUTFALL-001
SM 4500-CI G-2011
865968
92738286001
OUTFALL-001
TKN+NO3+NO2
867230
Calculation
92738286001
OUTFALL-001
EPA 350.1 Rev 2.0 1993
866641
92738286001
OUTFALL-001
EPA 351.2 Rev 2.0 1993
866875
EPA 351.2 Rev 2.0 1993
867049
92738286001
OUTFALL-001
EPA 353.2 Rev 2.0 1993
867021
92738286001
OUTFALL-001
EPA 365.1 Rev 2.0 1993
865763
EPA 365.1 Rev 2.0 1993
866067
Date: 07/16/2024 10:03 AM
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 14 of 22

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^' 2540D Totat Suspended 3olldo
350.1 Ammonia; 365.1 Phosphorus,
TOW
351.2 Total Njoldahl Nllrogen; 353.2
Wagon. NO2
4500CL O ChVine, Residual
52105 BOO, 5 day
MBIO 02UD Focal CWlform RAL
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OC#_Titie: M-FRM-HUN1-Q731 "lvrine Da Sheet
a11ce.
Effective Until. 02/2712fi23 -
��►,��fi- scyv��Q'f`I�: IFS 6�S/n� Date: 6r�Z5z
Client: 5 ! q aretplelt7:[j'_Uo _
Location:.- �l>N►'dfu L
Instrument modei ' ' Seri I Number A nuqJ Calibration verification Date
D•
t pN reacFby model l8 .SSj` �S' Serial Number � �4� 3
[Date:
eld Data sheet Review
MQ �
ChSckParameter Tested gy;
JOUitra-low chlorine (units itg/L) Reporting limit`'0 µ910-values louver would be <14 WJL
XLOW'(TRC) total residual chlorine (units. mg/L) Reporting limit �cu MSW �- values lower would be cn.1: mg/L
❑ Free available Chlorine (FAC) (units mg/L) j� (rtAM Reporting limit 10mg/L) - values lower would be <0.1 mg/L
of-'4*e Circleco"
sAnflding units below
Time Collected: b- 5$ Hrs. (1) with Interterence C orine result: • x3 WiL g/ /1#/S 3.911311
Initial PH: -�_S.t'.L. 22d aC (2) Interference: Dow-? 116140PI I
(Optional) Ice Bath: c 21 "C Nh sec
oa reading (1) minus reading (z) = actual _.Job itg/L ��°!l�d9
��� ((AnCorrected pH (betweerl6& 7 S.U.) �•8i S.U. Read Time; �� � �� Result. _3.� .., PIjL �
��I[LLI.GYV Htarfierence CC ettlnenroe+edum � � + * 7+�%�ry�fL� Vt� 1 \"iV i��%.J�
Manganese, oxldlzed lMn4+, Mn7+j or Chromium, oxidized (Cr6+)
1. Adjust sample pH to 6-7 with 1.00 N sulfuric Acid or Sodium Hydroxide, p�
[[�
2. Add 9 drops Potassium Iodide (30 g/Ll to an 80 mi. sample. V � N s1J ►�� ��
3. Mix and waft I rnlnute. ; � 3Q
4. Add 9 drops of Sodium Arsehite 15 g/U and mix,
S. Analyte the treated sample as described In the procedure. 5. Subtract the result of this test from the original analysis to obtain the correct c!n0entratlon, ��•�N ~ P b i'N� ,
Chlorine. fi d T aced h e ran as soneetinayarnr�e F1 �=1
Manganese, azidlled (MnO,Mtr7+) or Chromium, oxrdlrad lG6+j •
1. Adjust sample pllto 6-7 with 1.00 N Sulfuric Add or Sodium Hydroxide. i-
2. Add 9 drops potassium Iodide t30 gJQ to a 30 mL sample.
3• Mix and wait one minute,
4. Add 9 drops Sodium Arsenite (5 g/i.) and Wit. l
5. Analyze id rnL of treated sample es described in procedure. F&P 2►io> 5. Subtract the result from this test from the original analysis to obtain the cwrrec�C chlorine con ntratlon. "U
1I of vl
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Page 18 of 22

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2540D Total Suspended Solids
350.1 Ammonia; 365.1 Phosphorus,
Total
351.2 Total Kjeldahl Nitrogen; 353.2 n
Nitrogen, NO2 �'
4500CL G Chlorine, Residual
S
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Page 19 of 22
1-<11
—LL
Preservillan nen-confafmsnce Identified for = r
H-�+171-1-
I
I—
sample.

aCE` DC# Title: ENV-FRM-HUN1-D131_Chlorine Dam Sheet
Effeetive Date: 02/27/2023
Am pfh+ S"ti'•Y (Q&l u'- T-SSf1.S�DZI` Date: �45 zN
Client: = 5�i H(A0WAV . safriplElD C ti(�of - .— Location �lil�Eul!'c,{�rrallQ��QorS�c+�1 ..
Instrument raudei Serial Number Annual Calibration Verification Date
pig read by model ixr E+S Serial f�fumber r' �o� Field Data sheet Review
Crack Parameter Tested Date: By:
Ultra -low chlorine (units µg/L) Reporting limit (Io µg/L) - values lower would be <10 µg/L
XLow (TRC) total residual chlorine (units mg/L) Reporting limit (0.1 mg/L) --values lower would be 011 mg/L
❑Free available Chlorine (FAC) (units m'g/IL)f�,(lfilN, Reporting limit 10.1 mg/L)- values lower would be <0.1 mg/L
�i13+P Time Collected: Circle corresponding units below
(1) with n b� Ss Hrs. ` Interference Chlorine result: rR X3 µglq� I f; l5' 3c91jft
Initial pH: I� • 19 S.Lt.[a1 pl -C (2) Interference: aolX3 µg/L���•elbil9 A►3�'J/�
(Optional) Ice Bath: < 21 °C /M s/e�c. reading (1) minus reading (2) = actual �, µg/L Q> ll:fq
i(+ (( orrected pH (between 6 & 7 5.U.) b -9 S.U. Read Time; it ( AM RestJlt:
.51111 6y� �Ie Af d2 war Troia }� r � ono
�^'`�,LL_ � �ry�� � y l��i Js,
Manganese, oxidized (Mn4+. Mn7+j or chromium, oxidized (Cr6+)
1. Adjust sample pH to 6-7 with 1.00 N Sulfuric Acid or Sodium Hydroxide. Wv } t Aqsu (-�� 0
2. Add 9 drops Potassium Iodide (30 g/Q to an 80 mL sample. rrj 1Q �j /l
3. Mix and wait I minute.
4. Add 9 drops of Sodium Arsenite (S g/L) and mix.
S. Analyze the treated sample as described In the procedure.
6. Subtract the result of this test from the original analysis to obtain the correct concentration. LM�r{, j
Chlorine, free and Total low and high range correcting eroMdure F/b� ! /ooO ik �(.% 1 Y^' 15�.3+p���[�
Manganese, oxidized (Mn4+ Mn7+) or Chromium, oxldlzed (Cr6+) v 5 J
I. Adjust sample pH to 6-7 with i00 N Sulfurlc Acid or sodium Hydroxide. f7 �� �+��fx f aoz , ,,^
2. Add 9 drops Potassium Iodide 30 L to a 30 mL sample. / ``� t IU�f n
3. Mix and wait one minute. •
4. Add 9 drops Sodium Arsenite (5 g/L) and miF. /�-
S. Analyze 10 mL of treated sample as described In procedure. �t (�rdns//h)n�p
6. Subtract the result from this test from the originsl analysis to obtain the Correct chlorine con ntratlon. ' "U `
Res!nt Used Lot Number
DA��tuf�_lr�rn�� 02s ,-wS
Qua)trax ID: 133778 Page 1 of 'I
Page 20 of 22

DC# Title: ENV-FRM-HUN1-0083 �04 Sample Condltion Upon Receipt
ace
Effective Date: 04126/m2A
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood
Sample ❑ Huntersville ❑ Raleighf Mechanicsville❑ Atlanta
El Client Name:
Upon Receipt 0)_C_
❑ Kernersville❑
` � 7 Project #;
Courier: ❑�F d Ex
❑ Commercial Pace QUPS ❑LISPS ❑Gient
❑Other:
Custody Seal Present? Yes Na Seals Intact)
QYes QNa ❑N/A
Packing Material: ❑Bubble Wrap
❑Bubble Bags None
Thermometer:
❑ IR Gun ID: 6 (Tb6 5
Type of Ice: Q�Wet
Ub Correction Factor:
Gaoler Temp: Add/subtract('[) U
Cooler Temp Corrected ('Q: U
USDA Regulated Sail (N/A, water sample)
Did samples origfna )n a quarantine zone within the United States: CA, NY, or SC
(check maps)? I-)Yec I- im-
Oate/Initials Person Examining Contents:-S—A_
❑ Other Biological Tissue Frozen? Co�2s/ Zy
Oyes [IN, pJN/A
❑Blue ❑None
Temp should be above freezing to 6'C
[]Samples out of temp criteria. Samples on fee, cooling process
has begun
Chain of Custody Present?
Samples Arrived within Hold Time?
Yes
ONO
❑N/A
1.
Short Hold Time Analysis (<72 hr.)?
Yes
ONO
❑N/A
2
Rush Turn Around Time Requested?
Yes
❑No
❑N/A
3.
❑Yes
Na
❑N/A
4.
Sufficient Volume?
Carrel Containers Used?
es
ONO
❑ N/A
S.
-Pace Containers Used?
es
des
ON.
❑N/A
6.
Containers Intact?
❑No
❑N/A
Dissolved analysis: Samples Field Filtered?
QY es
ONO
❑N/A
7.
Sample Labels Match COC?
Dyes
lallo
❑N/A
a.
gles
❑No
❑N/A
9.
-Includes Date/rime/ID/Analysis Matrix:
(,l
Headspace in VOA Vials (>5-6mm)?
Trip Blank Present?
Dyes
[:]No
N/A
10.
❑Yes
❑No
N/A
11.
Trip 8iank Custody Seals Present?
COMMENTS/SAMPLE DISCREPANCY
Did samples originate from a foreign source (fnternationally,
including Hawaii and Puerto Rlco)? 11v- • n.,..
CLIENT iYOTIfiCAT1ON/RESOLUTION Lot ID of split conta iners:
-person contacted: - --
Date/Time:
Project Manager SCURF Review:
Project Manager SRF Review:
Date:
Date:
field Data Required?
haltrax ID: 69614 Page 21 of 22

DC# Title: ENV-FRM-HUN1-0083 v04 Sample
C6r
.- E'ffectjve Date: 04/26/2024
Condition
Upon Receipt
'Check mark top half of box If pH and/or dechlorrnatton Is vetmed and wMln the
acceptance range for preservation samples.
Project #
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom
F�
half of box is to Hst number of battles
"'Check all unpreserved Nitrates for chlorine
Laboratory Receiving Location: Asheville ❑ Eden[] Greenwood ❑ Huntersville ❑
Cllent T
Ralefg Mechanicsville❑ Atlanta❑
iiiiii
Nem
.5
� T rofife Number,` Notes
a
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6 m
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3 ,on
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E E 4g
E E
E
Fr --I
N
N
MKIPMEN
MEMEN
WOMEN
IMMMMI
MIL40001
MIC001
Mill
hIM
pH Adjustment Log for Preserved Samples
Sample ID Type of Preservative pH upon receipt Date preservation adjusted I Time reservat on
adjusted
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the
added
1
W( 6&trazl6.6 6614
Page 22 of 22
Paae 2 of 2 — -_t