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HomeMy WebLinkAboutWQ0035049_Monitoring - 09-2024_20241028Monitoring Report Submittal Permit Number#* WQ0035049 Name of Facility:* Maple Hill WWTF-Wastewater Irrigation System Month: * September Year: * 2024 Report Information Type* Upload Document* NDMR, NDAR-1, NDAR-2, NDMLR Maple Hill September 2024 NDMR, NDAR-1.pdf 1.27MB PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Confirmation Email Address: * acolon@pendercountync.gov Name of Submitter: * Anthony Colon Signature: Date of submittal: 10/28/2024 This will be filled in automatically Initial Review Reviewer: Wanda.Gerald Is the project number correct?* WQ0035049 Is the monitoring report accepted?* Yes No Regional Office* Wilmington Reviewer: _anonymous Review Date: 11/7/2024 FOR}: NDMR 10-13 NON -DISCHARGE MONITORING REPORT (NDMR) Page _1_ of J2_ Permit No.: W00035049 Facility Name: Maple Hill WWTF County: Pender Month: September Year: 2024 PPI: 001 Flow Measuring Point: 71 infiuent O Effluent El No flaw generated Parameter Monitoring Point: Lt influent 0 Effluent 3 Groundwater Lowering Surface Water Parameter Code -► 60050 00400 00310 00530 00610 00620 00626 31616 00600 00665 00940 70300 p f4 ;= w U h O c O E :� 1- y O 3 M = qQQ t$ m 7s e v h y N N 4 ca Z e v a� .5 o Z `0 0 0_ O U c CID 1- "�" Z `3 t CL h a •. O U a c„a v_ ~ N O n N 24-hr hrs GPD su mg/L mg/L mg/L mg/L mg/L #1100 mL mg/L mg/L mg/L mg/L 1 12,406 2 07:30 6 23,049 8.1 3 07:30 6 15,705 8.1 4 07:30 7 11,334 7.8 5 07:30 7 7,890 7.8 6 07:30 7 8,6 7.9 7 9,936 a 9,684 9 07:30 7 10,464 6.7 10 07:30 7 7,317 7.3 11 07:30 7 7,554 6.7 12 07:30 6 8,613 6.8 13 07:30 7 7,267 6.7 4 7.1 <0.2 20.4 <1 20.4 6.92 141 11,939 151 11,739 16 07:30 7 76,415 6.7 17 07:30 6 26,726 6.9 18 07:30 7 14,034 7.3 19 07:30 6 11,900 6.5 20 07:30 6 11,730 6.5 21 11,151 22 12,945 23 07:30 7 10,729 6.5 24 07:30 5 11,172 7.1 25 07:30 6 8,908 7.3 26 07:30 7 10,340 7.8 271 07:30 6 11,451 7.3 281 11,312 29 11,565 30 07:30 7 9,844 7.1 31 Average: 13,774 4.00 710 0.00 20.40 0.00 20.40 6.92 Daily Maximum: 76,415 8.10 4.00 7.10 0.20 20.40 1.00 20.40 6.92 Daily Minimum: 7,267 6.50 4.00 7 10 0.20 20.40 1.00 20.40 6.92 Sampling Type: Recorder Grab Composite Composite Composite Composite Ccmcasito Grab Composite Grab Composile Composite Monthly Avg. Limit: 42,000 n/a 30 30 15 n/a n/a 200 n/a n/a n/a n/a Daily Limit: rVa 6 to 9 n/a n/a n1a n/a n/a nla rif/a nr'a n/a n/a Sample Frequency: Continous 5XWK Weedy Weekly Wee My Weekly VJeek!y Weekly Monthly idlontly 3XYR 3XYR FORM: NDMR 10-13 NON -DISCHARGE MONITORING REPORT (NDMR) Page _2_of_2_ Sampling Person(s) Certified Laboratories Name: Samples were collected by the Certified Laboratory Name: Environmental Chemists, Inc. Name: 11 Name: Jay Baker -1 Compliant i , Nan -Col If the facility is non -compliant, please explain In the space below the reason(s) the facility was not in compliance. Provide in your explanation the dates) of the non-compliance and describe the corrective actions) fakan Attarh ariddinnal shepts If necessary. Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: Christopher Pickett Permittee: Pender County Utilities Certification No.: 995432 Signing Official: Anthony Colon Grade: WW2 Phone Number: 910-259-1570 Signing Official's Title: Director Has the ORC changed since the previous NDMR? ❑ yes I_' No Phone Number: 910-259-1570 Permit Expiration: 8/31/2026 I Signature Date Signature Date By this signature. I certify that this - accumate and complete to the best of my knowedge I cerbfy, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief. true, accurate, and rnmplete. I am aware that there are significant penalties for submet ..[: false information, including the posstolity, of fines and impneonment for knowing violations. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 FORM: NDAR-1 10-13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page _1_ of Permit No.: Facility Name: Maple Hill WWTF County: Pe der Month: September Year: 2024 Field Name: 1 Field Name: 2 Field Name: 3 Field Name: 4 Did irrigation occur Area (acres): 1.72 Area (acres): 1.72 Area (acres)': 1.72 Area (acres): 02 at this facility? Cover Crop: Bermuda Cover Crop: Bermuda Cover Crop: Bermuda Cover Crop: Bermuda E7 YES ❑ NO Hourly Rate (in): 0.41 Hourly Rate (in): 0.41 Hourly Rate (in); 0A1 Hourly Rate (in): 0.41 58 Annual Rate (in): 29.71 Annual Rate (in): 29.71 Annual Rate (in): 29.71 Annual Rate (in): 2971 Weather Freeboard Field Irrigated? 0 YES Cl ND Field Irrigated? O YES ❑ NO Field Irrigated? o YES ❑ NO Field Irrigated? 2 YES 0 NO '06 O O1 y (Q 7 Q E d O aR+ 'V d d m i a0+ N y °' Q. 16 U T .a c6 O, 0 16 vi 'i: ,m Q �* '! I 'p W �. IW hr Fr = `G O J >` 'tu o 'E in 7 �' C _ 7 'R p - A Gl -O d 7 C O '� a N y E ~ •� "O 00 J 0 E a of 3 L C E 3 0- W 2 00 y -O £ CL D IL �' Q V CF E 1- � 'rs E >, m O 7 L C J E 'i R 2 Y. � J 0 d V £ N = 4. o > Q V N ate+ E F' >= - T3 E T m p O% E J E a tii x O Z. � J 0 °r in ft ft gal min in In gal min in in gal min in in gal min in in 1 2 PC 73 0 3.3 3 C 66 2.6 3.3 4 C 65 0 3.3 15,080 40 0.32 0.32 14,960 40 0.32 0.32 13,960 40 0.30 0.30 14,800 40 0.32 0.32 5 C 67 0 3.3 6 CL 66 0 3.3 13,840 40 0.30 0.30 14,160 40 0.30 0.30 13,320 40 1 0.29 0.29 13,880 40 030 0.30 7 8 9 C 63 0.3 3.3 10 C 54 0 3.3 11 PC 60 0 3.4 14,560 40 0.31 0.31 14,560 40 0.31 0.31 13,560 40 0.29 0.29 14,640 40 0.31 0.31 121 PC 74 0 3.4 131 R 72 0.1 3.4 13,920 40 0.30 0.30 13,800 40 0.30 0.30 13,920 40 0.30 0.3.0 13,920 40 0.30 0.30 14 15 161 R 1 69 1.6 3.4 17 C I 68 3.5 3A 18 C 64 0 3.4 19 CL 70 0 3.4 20 CL 68 0.3 3.4 21 22 23 C 66 0.2 3.4 14,360 40 0.31 0 31 14,520 40 0.31 0.31 13,440 40 0.29 0.20 14,280 40 0.31 0.31 24 CL 69 0 3.4 25 PC 79 0.1 3.4 26 CL 73 0 3.4 1 13,640. 40 0.29 0.29 14,080 40 0.30 0.30 13,280 40 0.28 0.28 1 13,640 40 0.29 0.29 27 CL 77 0A 3.4 28 29 30 C 73 0.4 3.4 31 Monthly Loading: 85,40D 1.83 1 OA9 86.080 1.84 1049 81,480 1.74 9.76 85,160 1.82 10.43 12 Month Floating Total (in): FORM: NDAR-1 10-43 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page _2^ of _4_ Permit No.: WQ0035049 Facility Name: Maple Hill WWTF County: Pender Month: September Year: 2024 Field Name: 5 Field Name: 6 Field blame: 7 Field Name: 8 Did irrigation occur Area (acres): 1.72 Area (acres): 1.72 Area (acres): 1.74 Area (acres): 1.71 at this facility? Cover Crop: P Bermuda Cover P Bermuda Cover P Bermuda over P Bermuda ❑ YES ❑ NO Hourly Rate (in): 0.41 Hourly Rate (in): 0.41 Hourly Rate (in): 041 Hourly Rate (in): 0.41 Annual Rate (in): 20.71 Annual Rate (in): 29.71 Annual Rate (in): 29.71 Annual Rate (in): 29.71 Weather Freeboard Field Irrigated? 0 YES 0 NO Field Irrigated? [71 YES ❑ NO Fuld Irrigated? E YES 0 NO Field Irrigated? 0 YES ❑ NO ❑1>°, C vUta`, is m RCL n E w I—U) c 2 a` = ' 0 W >o a CO C. ❑ ca dd CL .Q a ud c p ❑ R a o�L Q "all 0 'ea ❑ E 3 >1 E M W i o. S E� i. VG p m ❑ E 'e •a' E -6 CL i= '0 a'C E°aJ y.s o J m ❑ 'F in ft ft gal min in in gal min in in gal min in in gal min in in 1 2 PC 73 0 3.3 3 C 66 2.6 3.3 4 C 65 0 3.3 13,960 40 0.30 0.30 15,040 40 0.32 0.32 15,160 40 0.32 0.32 14,800 40 0.32 0.32 5 C 67 0 3.3 6 CL 66 0 3.3 1 13,160 40 0.26 0.28 15,200 40 0.33 0.33 14,360 1 40 0.30 1 0.30 14,120 4C 0-30 0.30 7 8 9 C 63 0.3 3.3 10 C 54 0 3.3 11 PC 60 0 3.4 13,840 40 0.30 0.30 14,960 40 0,32 0.32 15,120 40 0.32 0.32 15,240 40 0.33 0.33 12 PC 74 0 3.4 13 R 72 0.1 3.4 13.840 40 0.30 0.30 14,480 40 0.31 0.31 14,200 40 0.30 0.30 13,880 40 0.30 0.30 14 15 16 R 69 1.6 3.4 17 C 68 3.5 3.4 18 C 64 0 3.4 19 CL 70 0 3.4 20 CL 68 0.3 3.4 21 22 23 C 66 0.2 3A 13,520 40 0.29 0,29 14,880 40 0.32 0.32 15,080 40 0,32 0.32 13,480 40 0.29 0.29 241 CL 69 0 3.4 25 PC 79 0.1 3.4 26 CL 73 0 3.4 11,560 40 0.25 0.25 14,040 40 0.30 0.30 14,640 40 0.31 0.31 13,760 40 0.30 0.30 27 CL 77 0.1 3.4 28 29 30 C 73 0.4 3.4 31 Monthly Loading: 79;880 1.71 :� 88,600 1.90 88,560 1.87 _ 85.280 1 84 12 Month Floating Total (in): =`.�:` ; =`� 9.48 ��.. 10 79 10.49 = = 10.721 FORM NDAR-1 10-13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page _3_ of _4_ Permit No.: WQ0035049 Facility Name: MAPLE HILLWWTF County: Pender Month: September Year: 2024 Field Name: 9 Field Name: 10 Field Name: 11 Field Name: Did irrigation occur Area (acres): 1,75 Area (acres): 1.77 Area (acres): 1.72 Area (acres): at this facility? Cover Crop:Bermuda Cover Crop; P� Bermuda Cover Crop: P� Bermuda Cover Crop: P: 0 YES ❑ No Hourly Rate (in): 0.41 Hourly Rate (in): 0.41 Hourly Rate (in). 041 Hourly Rate (in): 0 Annual Rate (in): 29.71 Annual Rate (in): 29.71 Annual Rate (in): 29.71 Annual Rate (in): Weather Freeboard Field Irrigated? ❑ YES L7 No Field Irrigated? o YES ❑ No Field Irrigated? El YES ❑ NO Field Irrigated? ❑ YES ❑ NO 1d d a U R ? 3 N C ;r D. N Gil 2 .VCL - ❑ l4 LO 'V 'U 3 b C V R J b 9 1 ,' W 'O d 3 ,Q. "O .�+ £ L R J ❑ E m 7 �' C E 3 V pi -O d ,� G d .4+ Ir C 'Q q J O E o 7 i= 0 tit d a i= � a 9 r �_ m a m O L J £ 7 O °F in ft ft gal thin in in gal min in in gal min in in gal min in in 1 2 PC 73 0 3.3 3 C 66 2.6 3.3 4 C 65 0 3.3 14.920 1 40 0.31 0.31 14,800 40 0.31 0.31 13,560 40 0.29 0.29 5 C 67 0 3.3 6 CL 66 0 3.3 14,120 40 0.30 0.30 14,080 40 0.29 0.29 13,120 40 0.28 0.28 7 8 9 C 63 0.3 3.3 10 C 54 0 3.3 11 PC 60 0 3.4 14.840 40 0.31 C 31 14,760 40 0.31 0.31 13,560 40 0.29 0,29 12 PC 74 0 3.4 13 R 72 0.1 3.4 14,240 40 0.30 0-30 13,640 4C 0.28 0,28 12,80.0 40 0.27 0.27 14 15 16 R 69 1.6 3.4 17 C 68 3.5 3.4 18 C 64 0 3.4 191 CL 70 0 3.4 201 CL 68 0.3 3.4 21 22 23 C 66 0.2 3.4 14,950 40 0.31 0.31 14,640 40 030 030 13,960 40 0.30 0.30 24 CL 69 0 3.4 25 PC 79 0.1 3.4 26 CL 73 0 3.4 14,240 40 0.3.0 0.30 13,960 40 0.29 029 12.760 40 0.27 0.27 27 CL 77 0.1 3.4 28 29 30 C 73 0.4 3.4 31 Monthly Loading: 12 Month Floating Total (in):I 87,320 -; 1.84 10.49 85,880 1.79 10.26 79.760 Unliff 1.71 9.63 0 000 FORM NDAR-1 10-13 NON -DISCHARGE APPLICATION REPORT(NDAR-1) Page _4_of_4_ Did the application rates exceed the limits in Attachment B of your permit? Were adequate measures taken to prevent effluent ponding in or runoff from the sites? Was a suitable vegetative cover maintained on all sites as specified in your permit? Were all setbacks listed in your permit maintained for every application to each permitted site? Were ail freeboards maintained in accordance with the specified freeboard heights in your permit? ca Compliant ❑ Non -Compliant O Compliant L7 Non -Compliant 17 Compliant ❑ Non-Complrant G1 Compliant ❑ Non-Comphart Q Compliant ❑ Non -Compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: Christopher Pickett Permittee: Pender County Utilities Certification No.: 1010919 Signing Official: Anthony Colon Grade: WW-SI Phone Number: 910-259-1570 Signing Official's Title: Director Has the ORC changed since the previous NDAR-1? 0 yes F v; Phone Number: 910-259-1570 Permit Exp.: 8/31/26 Signature Dale Signature Date By this signature, i certify that this report is accu rate and complete to the best or my knowledge I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel property gathered and evaluated the information submitted Based on my inquiry of the person or persons who manage the system. or those persons dn:ctly responsible for gathering the hnfomhation the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violators Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 [enviriocehem ANALYTICAL & CONSULTING CHEMISTS Pender County Utility Operations Post Office Box 995 Burgaw NC 28425 Attention; Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab , 910,392,4424 Fax 710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 t, 910.347.5843 Lab/Fax infotaenvironmentalchemistacom Date of Report: Oct 04, 2024 Customer PO #: Customer ID: 08100095 Report #: 2024-21546 Project ID: Maple Hill WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 24-53196 Site: Effluent 9/1312024 10:00 AM Water JCS/Envirochem Test Method Results Date Analyzed Ammonia Nitrogen EPA 350.1, Rev. 2.0, 1993 < 0.2 mg/L 09/1712024 Total Kjeldahl Nitrogen (TKN) EPA 351,2, Rev. 2.0, 1993 < 0.5 mg/L 09/23/2024 Residue Suspended (TSS) SM 2540 D-2015 7.1 mg/L 09/1612024 BOD SM 5210 B-2016 4 mg/L 09/13/2024 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353.2, Rev 2.0, 1993 < 0.02 mg1L 09/13/2024 Nitrate+ N itrite-N itrogen EPA 363.2,Rev 2.0 1D93 20.4mg/L 09/17/2024 Nitrate Nitrogen Sublract*n Method 20.4 mg/L 09/17/2024 Lab ID Sample ID: Collect Dateffime Matrix Sampled by 24-53197 Site: Effluent - Grab 9/13/2024 10:45 AM Water JCB/Envirochem Test Method Results Date Analyzed Fecal Coliform Idesa Col lect-18 <1 MPN/100ml 09/13/2024 Temperature SM 255013-2010 24.6 C 09/13/2024 pH SM 4500 H B-2011 8.1 units 09/13/2024 Total Phosphorus SM 4500 P (F-H)-2011 6.92 mg/L 09/23/2024 Comment: a Reviewed by: Report M: 2024-21546 Page 1 of 1 ,initial: Jat-' BaKer i.er tt airon � _ d Frcitit) Name: I- Permit th pH Reference Method SM45t;o H-A lwarit wnt It') RTARA2211 wili;, )c Calibration Time Cal Buffer d 0 s u Cat Buffer 10 0 s u Check Ciaffrr 7 0 s u Comments 02. � 0, 00 -7. 01 'pit check aurrer must read vnthm 2 u t pit units of the bullcr's true value 4 su buffer Lott//- Rim 1R061 ExROM 7 su buffer Lot# Ricca 22" 10Cr40 Exo. I nnA 10 su buffer Lott RICCA 1304P74Exa. 10Q4 Sample Location Sample Collection l.tn1e+ Sarnple Analysts Tuneo pH Result s u 10.Post anal sis Buffer Check Value s u 1„ Co mmcntslf)asa Qualifiers r (�i 1A,; b* Post analysis hufEer check is required when performing analyses at multiple sampling locations and nnim tit ;t ,hw - v 1 +Inns Of tide t otter's true V;tlue A I I pil values in pl I units if e , s u ) Record all data to the nearest 0 01 sm and report to the nearest 0 1 s u Total Residual Chlorine JRQ ltefcrence iictliori SM A500CI-G2011 INN 8167 14R t Picric cirt:te ap licable hlethoa/ Instrument 11) HACH Colorimeter 1512OE289091 Daily Cheri; Post•anal sits } Check Sid Time check "ample tiamPle Sample TRC Result tilanderd Result anal) zing Standard ocauou CollectionAna1^<s s pk' 't or ht,,lt Cotnmenis/Data Qualifiers 1k6/LOriTlPfj, allntJllit:l'S11eil Analyzed Analyzed ' Time Time ftmc �+• t KC Daily Check Standard true Value_. _ ttgni, or mg/l, acceptance range ,pg1l or mg/1 CEL SIDS HACH A0038 Cheek standards must recover si itlun 110% of the check standard's true value Annual Calibration Curvc Verification Date- _ 11/25/23 MXX Exp Date- E-ND, Daie Reagent plank Value: (When applicable Analyze- and document a rcagcnt blank) when standards, sample dilutions or PT Samples are prepared) Dissolved Oxygen (DO) RefircoccMetbud.Sb14W0G 2015 ingirunicnllr) VC1 PR(1209.211tillltil., Calibration/ Verification Time Caltbratioll sariable Meter reading or^aeliicieney after calittration ♦ Post -analysis calibration verification 6-hen necessary) C`r ttrra la:, Temp oC 134111ronttNnc pressure mmll Salinity, pPt Thearctical Value mgA. Calculated Value mgil tti ve this ro-A vihen perfurming a tcrificWtion instead 4, f calibration Sample Location Sample Collection Time 'Sample Anahsis Time DO reading —MeA. Comments/Data Qualifiers • » hen performing analyses at multiple locations. Inc mi.,tef must be recalibrateii at each site before analysis or a post.anal"is calibration venfcatuin must be perfinnine i ' It innipte Is measured dirceii} in the stream and or onsite, o!. c• time analy fed %ould be %carded with a rule that dies are measured tit stiff or 1- i it edialell. Temperature Releterice kleihml SAt IiSD R.1010 Inunim. m Ill ST A 92 A 7 71 • ven6'79C Samplo Location Sample Collection Time *Sample Analysis Time Temperature C Commtmts Data Qualifiers Orr ti4S D:45 24. D-- ' it sample is measured dnecuN nt the strenni anti or ,in :.m D;d•, tsen:7 an. P. :,i ssuuld •. t ca..la' is fill.-[ riot, 111.11 fh� i M: m--a.ut ill in fila Ur AttlnCdlltelt Annual Verification oate 11-25-23 Field Personnel :Note: i�,tt•tNll Izrol,aa Rev 1-2022 Environmental Chemist, Inc., Wilmington, INC Lab #94 Sample Receipt Checklist 6602 Windmill Way Wilmington, NC 28405 910.392,0223 Client: NaAJC P1(—L Date: Report Number: _ 2024 - �O Receipt of sample: ECHEM pickup' Client Delivery 0 UPS ❑ Fed Ex ❑ Other O ❑ YES ❑ NO N/A , Were custody seals present on the cooler? ❑ YES 10 NO N/A 12. If custody seals were present, were they intact/unbroken? Original temperature upon receipt 2.0 °C Corrected temperature upon receipt _ "C How temperature taken: ❑ Temperature Blank Against Bottles IR Gun ID: Thomas Traceable S/N: 230222540 IR Gun Correction Factor QC: 0.0 YES 10 NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./qp, notified? YES YES 10 NO ❑ NO 4. Were proper custody procedures (relinquished/received) followed? 5. Were sample ID's listed on the COC? j8[ YES ❑ NO 6. Were samples ID's listed on sample containers? YES YES YES ❑ NO 0 NO D NO 7. Were collection date and time listed on the COC? 8. Were tests to be performed listed on the COC? 9. Did samples arrive in proper containers for each test? YES 113 YES NO ❑ NO 10. Did samples arrive in good condition for each test? 11. Was adequate sample volume availableT YES ❑ NO 12. Were samples received within proper holding time for requested tests? YES ❑ NO 13. Were acid preserved samples received at a pH of <2? ❑ YES ❑ NO 14. Were cyanide samples received at a pH >12? ❑ YES I0 NO 15. Were sulfide samples received at a pH a9? YES ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <O.S m/L? ** ❑ YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? ❑ YES ❑ NO 18. Were orthophosphate samples filtered in the field within 15 minutes? * TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet. ** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) Sample(s) were received incorrectly preserved and were adjusted accordingly by adding (circle one): H2501 HNO3 HCI NaOH Time of preservation: If more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or notify the state lab if directed to analyzed by the customer. Who was notified, date and time: Volatiles Sample(s) were received with headspace COMMENTS: DOC. QA.002 Rev 1 • - ENVIRONMENTAL CHEMISTS, INC Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY 6602 Windmill Way Wilmington, NC 28WS OFFICE: 910-392-0223 FAX 910-3924424 info c&nvironmentaichemists.com Client: Pender County utilities (Wastewater) PROJECT NAME: Maple Hill WWTP (PPI 001) REPORT NO: OW >'Yi ADDRESS: CONTACT NAME: Chris Pickett, ORC PO NO: REPORT TO: ORC PHONEIFAX: COPY TO: email: Sampled By: J SAMPLE TYPE: t = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection _ a E >1 r H o o m �t9 o Fo`L " m cw = E a Ow Z PRESERVATION ANALYSIS REQUESTED Date Time Temp o H _ o s w o WWTP PPI 001 (composit C P �cj to X BOD, TSS, NO2 S i ,,.o., C P X IN03, NH3, TKN WWTP PPi 001 (composite) Triannuals C P X Chloride, TDS (March, July, Nov) C P G G WWTP Effluent (grab) l� �' X Z Total Phos G phi (field): �' o g C P X Fecal Coliform G G C P G G Samples due 1/month C P G G C P G G limits: 1301) 30 mall-, TSS 30 mall-, NH3 15 mglL, Fecal 200 coloniesl100 ml Transfer Relinquished By: DatelTime Received By: Date/Time 1. 2. r Temperature when Received:y �_ _ _ Accepted: / Re �(tLed Resample R steel: Delivered By: Received By: Time: Z, Y'V Comments: T R AROUND: