WQ0002503_Monitoring - 11-2022_20230103

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�7
(;W-59A COMPLIANCE REPORT FORM Permit #._ WCCQ ✓* '50 j
(Submit one each trrtmhoring pefia / wills C; ti - 59 fivmc)
I
Enter date monitoring results were due. ( 12. $t 122 Will this monitoring report (GW-59 and GW-59A)
l'H;5
NO
be submitted after the established due date?
i
X
2
i Was an) required information missing on the (;W-59 report forms"
YES
O
IF the answer to question 1 or 2 is `YES", list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need or repair or maintenance (damaged easing, unlocked or missing cap, missing
1"FS
VO
identification plate, area overgrown, etc.):' IJ the ans-wer is "Yes" contact lire Regional Qtflce for giddance.
y
4
-
Are any monitored constituents equal to or above the established standards?
--'_
-question
,ti
NO
If the answer to 4 is "--NO0", ski---p-- to section 8.
_._.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards hr the space provided below.
1
Mw �, J KON 01045
-
-
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
VES
NO
same constituent(s) in the same well(s) in the last two years?
X
If the answer to question 5 is `NO", skip to section 8. �
If the answer to question 5 is "YES", list in the space provided below, etch well with°c��tuent(s) exceeding
j standards, concentration(s) reported, and sample collection date for each o2�rreric*rrtt;e,kitst two years).
•�V ��Sie CO� *`��
Are the monitoring wells listed in section 5 located at or beyond the review bau a ?
N()
G„
if the answer is "YES", a groundwater quality problem may be occurring. CONTACT _T'H'9 REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "Vo", monitoring wells may be improperly
located, contact the Regional Office. y� Q
� v
o
Is the petfnitlee implementing previously approv__ed actions req d by the Division involving this
It Es
No
groundwater quality problem? "P
A
If the answer to question 7 is 'YES", describe those actions in the space provided below.
H the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Fallure to do so may subiect the permittee to a Notice of Violation
fines, and/or penalties.
NO EFFWAW-C }1F1S BErN APPLIED 'TO T41E SPRAIfIELD SINGE FIEg, 2019
g
The person completing this portion (GIN--59A) of the monitoring report should sign below and submit this
form with G W 59 forms for required wells to the address provided at the top of the current G W-59 form.
f t`ts)@ tt(t f ,iwt -tend l"1 , lltPrt IINib*wo in this
OA
Signatur of Permittee (or Authorized Agent) Date
(al.-59A 1218/2003

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
COMPLIANCE REPORT FORM
INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 2/28/2029
Facility Name: FRIT CAR, INC.
Non -Discharge UIC
Permit Name (if different): SAME AS ABOVE
NPDES W00002503 Other
Facility Address: 2012 HIGHWAY 17 NORTH
TYPE OF PERMITTED OPERATION BEING MONITORED
BRIDGETON NC 28519
County CRAVEN
❑ Lagoon ❑ Remediation: Infiltration Gallery
0 Spray Field ❑ Remediation:
Contact Person: MICHAEL NEWBY
Telephone#: [phone]
ElRotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: FRIT CAR SPRAYFIELD
No. of wells to be sampled: 4
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-1
Date sample collected: 11 /9/2022
FIELD ANALYSES:
WAS
Well Depth: 15,65 ft
Well Diameter: 2 in.
pH 00400 5.83 units Temp. 000lo: 20.5 °C
DRY at
Depth to Water Level 825a6: 8.23 ft. below measuring
p g point
Screened Interval: ft. to
ft. Spec. Cond. 0009a I lMhos
time of
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor 000m: NONE
sampling,check
Volume of water pumped/bailed before sampling: 3.56
gallons
Appearance CLEAR
here:❑
Samples for metals were collected unfiltered: ❑■ YES ❑
NO and field acidified: ❑■ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed:11/18/2022
Laboratory Name: PACE ANALYTICAL Certification No. EnV375
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N oo615
mg/L
Pb -Lead 01051 <2.0 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620 .156
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <• 10
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 131 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
Di
roc 00680 57.3 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 2.38 mg/L
Cd - Cadmium 01027
ug/L
j,AN f 1
Arsenic 01002 ug/L
Chromium: Total 01034 <2.0
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042 <.005
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 <100
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 18.8 mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑■ Yes (1) ❑ No (0)
Specific Conductance 00095 µMhos
K - Potassium 00937
mg/L
VOC 7873 method #
Total Ammonia 00610 <.25 mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
, method #
TKN as N 00625 mg/L
Ni - Nickel 01067 <2.0
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Michael Newby, Senior Vice President
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.06-07-2018

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
. 4
OIL
DEPARTMENT OF ENVIRONMENTAL QUALITY • OIV. OF WATER RESOURCES
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 2/28/2029
Facility Name: FRIT CAR, INC.
Non -Discharge UIC
Permit Name (if different): SAME AS ABOVE
NPDES W00002503 Other
Facility Address: 2012 HIGHWAY 17 NORTH
TYPE OF PERMITTED OPERATION BEING MONITORED
BRIDGETON NC 28519
County CRAVEN
❑ Lagoon ❑ Remediation: Infiltration Gallery
❑■ Spray Field ❑ Remediation:
Contact Person: MICHAEL NEWBY
Telephone#: [phone]
ElRotary Distributor ElLand Application of Sludge
Well Location/Site Name: FRIT CAR SPRAYFIELD
No. of wells to be sampled: 4
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-5
Date sample collected: 11 /9/2022
FIELD ANALYSES:
WAS
Well Depth: 15.25 ft.
Well Diameter: 2 in.
pH 00400: 5.01 units Temp. 000lo: 19.3 °C
DRY at
Depth to Water Level 82546: 8.05 ft. below measuring point
Screened Interval: ft. to
ft.
Spec. Cond. 00094: µMhos
time of
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
—
Odor 000m: NONE
sampling,
check
Volume of water pumped/bailed before sampling: 3.45
gallons
Appearance CLEAR
here:❑
Samples for metals were collected unfiltered: (M YES ❑
NO and field acidified: ® YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 11/18/2022
Laboratory Name: PACE ANALYTICAL
Certification No. EnV375
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L
Pb -Lead 01051 3.45 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620 <.10
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus:
Total as P 00665 <0.1
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
issolved Solids:Total 703oo 72 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
Uj
roc 0068o 2.75 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 16.3 mg/L
Cd - Cadmium 01027
ug/L
RANT 9 2023
Arsenic 01002 1
Chromium: Total 01034 <2.0
ug/L
Grease and Oils 00552 mg/L
Cu -Copper 01042 <.005
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 176
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 19.2 mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? X Yes (1) ❑ No (0)
Specific Conductance 00095 µMhos
K - Potassium 00937
mg/L
VOC 7873 method #
Total Ammonia 00610 <-25 mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NH,as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
1
, method #
TKN as N 00625 mg/L
Ni - Nickel 01067 <2.0
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Michael Newby, Senior Vice President
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.06-07-2018

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
COMPLIANCE REPORT FORM
INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 2/28/2029
Facility Name: FRIT CAR, INC.
Non -Discharge UIC
Permit Name (if different): SAME AS ABOVE
NPDES WQ0002503 Other
Facility Address: 2012 HIGHWAY 17 NORTH
TYPE OF PERMITTED OPERATION BEING MONITORED
BRIDGETON NC 28519
County CRAVEN
❑ Lagoon ❑ Remediation: Infiltration Gallery
❑■ Spray Field ❑ Remediation:
Contact Person: MICHAEL NEWBY
Telephone#: [phone]
❑ Rotary Distributor ElLand Application of Sludge
Well Location/Site Name: FRIT CAR SPRAYFIELD
No. of wells to be sampled: 4
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-6
Date sample collected: 11 /9/2022
FIELD ANALYSES:
WAS
Well Depth: 19.68 ft.
Well Diameter: 2 in.
pH 00400: 4.89 units Temp. 000lo 19.2 °C
DRY at
Depth to Water Level 82546: 12.13 ft. below measuring point
Screened Interval: ft.
to ft.
Spec. Cond. 00094: µMhos
time of
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor 00085: NONE
sampling,
check
Volume of water pumped/bailed before sampling: 3.63
gallons
Appearance CLEAR
here:❑
Samples for metals were collected unfiltered: N YES ❑
NO and field acidified: ❑■ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed: 11/18/2022
Laboratory Name: PACE ANALYTICAL
Certification No. EnV375
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
rng/L
Pb -Lead 01051 <2.0 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620 <_ 10
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus:
Total as P 00665 <.10
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 56 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
Dd
TOC 00680 1.29 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 14.1 mg/L
Cd - Cadmium 01027
ug/L
JAN
Arsenic 01002 ug/L
Chromium: Total 01034 <2.0
ug/L
Grease and Oils 00552 mg/L
Cu -Copper 01042 <.005
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron o1o45 177
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 10.9 mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑■ Yes (1) ❑ No (0)
Specific Conductance 00095 µMhos
K - Potassium 00937
mg/L
VOC 7873 method #
Total Ammonia 00610 <•25 mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
, method #
TKN as N 00625 mg/L
Ni - Nickel 01067 <2.0
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Michael Newby, Senior Vice President
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.06-07-2018

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1 517 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 2/28/2029
Facility Name: FRIT CAR, INC.
Non -Discharge UIC
Permit Name (if different): SAME AS ABOVE
NPDES WQ0002503 Other
Facility Address: 2012 HIGHWAY 17 NORTH
TYPE OF PERMITTED OPERATION BEING MONITORED
BRIDGETON NC 28519
County CRAVEN
❑ Lagoon ❑ Remediation: Infiltration Gallery
❑■ Spray Field ❑ Remediation:
Contact Person: MICHAEL NEWBY
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: FRIT CAR SPRAYFIELD
No. of wells to be sampled: 4
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-7
Date sample collected: 11 /9/2022
FIELD ANALYSES:
WAS
Well Depth: 16.18 ft.
Well Diameter: 2 in.
pH 00400: 4.82 units Temp. 000lo 19.5 °C
DRY at
Depth to Water Level 82546: 9.02 ft. below measuring point
Screened Interval: ft. to
ft.
Spec. Cond. 00094: FtMhos
time of
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
—
Odor 00085: NONE
sampling,
check
Volume of water pumped/bailed before sampling: 3.44
gallons
Appearance CLEAR
here:❑
Samples for metals were collected unfiltered: N YES ❑
NO and field acidified: ❑■ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 11/18/2022
Laboratory Name: PACE ANALYTICAL
Certification No. EnV375
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L
Pb -Lead 01051 <2.0 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620 .127
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.1
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and C�centration Units):
Dissolved Solids:Total 703oo 480 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC 00680 12.3 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 131 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034 <2.0
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042 <.005
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 5530
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 162 mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? A Yes (1) ❑ No (0)
Specific Conductance 00095 µMhos
K - Potassium 00937
mg/L
VOC 7873 method #
Total Ammonia 00610 <•25 mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
, method #
TKN as N 00625 mg/L
Ni - Nickel 01067 <2.0
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Michael Newby, Senior Vice President
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.06-07-2018

aceAnalXical ® ANALYTICAL REPORT ,
November 28, 2022
Frit Car Inc.
Sample Delivery Group
Samples Received:
Project Number:
Description:
L1556126
11/10/2022
8522112
Groundwater Monitoring
Report To: Connie Pettis
2012 US Hwy 17N
New Bern, NC 28560
Entire Report Reviewed By: 4�,Al
Heather J Wagner
Project Manager
Results relate only to the Items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pac
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL 67
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the informatie9jilLovid
and as the samples are receivedAw
F— ,
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 8522112 L1556126 11/28/22 11:12 1 of 37

TABLE OF CONTENTS
Cp: Cover Page
1
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
MW-1 L1556126-01
5
MW-5 L1556126-02
8
MW-6 L1556126-03
11
MW-7 L1556126-04
14
Qc: Quality Control Summary
17
Gravimetric Analysis by Method 2540 C-2011
17
Wet Chemistry by Method 350.1
19
Wet Chemistry by Method 365.4
20
Wet Chemistry by Method 9056A
21
Wet Chemistry by Method 9060A 23
Metals (ICPMS) by Method 6020B 25
Volatile Organic Compounds (GC/MS) by Method 8260D 27
GI: Glossary of Terms 35
Al: Accreditations & Locations 36
Sc: Sample Chain of Custody 37
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 8522112 L1556126 11/28/22 11:12 2 of 37

SAMPLE SUMMARY
Collected by
Collected date/time
Received date/time
MW-1 L1556126-01 GW
Brent Heard
11/09/221010
11/10/22 09:00
RP
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
Z
Gravimetric Analysis by Method 2540 C-2011
WG1960409
1
11/16/2210:44
11/16/2214:05
SGBa
Mt. Juliet, TN
Wet Chemistry by Method 350.1
WG1958220
1
11/15/2211:12
11/15/2211:12
JAR
Mt. Juliet, TN
Wet Chemistry by Method 365.4
WG1959629
1
11/14/22 07:54
11/14/2219:32
CAT
Mt. Juliet, TN
Wet Chemistry by Method 9056A
WG1957691
1
11/11/22 03:09
11/11/22 03:09
LBR
Mt. Juliet, TN
Wet Chemistry by Method 9060A
WG1964116
10
11/24/22 04:45
11/24/22 04:45
LOH
Mt. Juliet, TN
4
Cn
Metals (ICPMS) by Method 6020B
WG1959108
1
11/18/2210:54
11/18/2218:40
JPD
Mt. Juliet, TN
Metals (ICPMS) by Method 6020E
WG1959267
1
11/18/22 09:05
11/18/2215:12
JPD
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1959639
25
11/15/22 07:49
11/15/22 07:49
ACG
Mt. Juliet, TN
Rr
Collected by
Collected date/time
Received date/time
El
MW-5 L1556126-02 GW
Brent Heard
11/09/2211:38
11/10/22 09:00
G(
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
Gravimetric alysis by Method 2540 C-2011
WG1960409
1
11/16/2210:44
11/16/2214:05
SGB
Mt. Juliet, TN
CAI
Wet Chemistry by Method 350.1
WG1958220
1
11/15/2211:13
11/15/2211:13
JAR
Mt. Juliet, TN
Wet Chemistry by Method 365.4
WG1959629
1
11/14/22 07:54
11/14/2219:34
CAT
Mt. Juliet, TN
Wet Chemistry by Method 9056A
WG1957691
1
11/11/22 04:36
11/11/22 04:36
LBR
Mt. Juliet, TN
RC
Wet Chemistry by Method 9060A
WG1964116
1
11/24/22 05:01
11/24/22 05:01
LOH
Mt. Juliet, TN
Metals (ICPMS) by Method 6020E
WG1959108
1
11/18/22 10:54
11/18/2218:43
JPD
Mt. Juliet, TN
Metals (ICPMS) by Method 6020B
WG1959267
1
11/18122 09:05
11/18/2215:15
JPD
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1958902
1
11/13/2216:36
11/13/2216:36
MGF
Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
MW-6 L1556126-03 GW
Brent Heard
11/09/221344
11/10/22 09:00
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
Gravimetric Analysis by Method 2540 C-2011
WG1960409
1
11/16/2210:44
11/16/2214:05
SGB
Mt. Juliet, TN
Wet Chemistry by Method 350.1
WG1958220
1
11/15/2211:15
11/15/2211:15
JAR
Mt. Juliet, TN
Wet Chemistry by Method 365.4
WG1959629
1
11/14/22 07:54
11/14/2219:39
CAT
Mt. Juliet, TN
Wet Chemistry by Method 9056A
WG1957691
1
11/11/22 05:01
11/11/22 05:01
LBR
Mt. Juliet, TN
Wet Chemistry by Method 9060A
WG1964117
1
11/23/22 21:19
11/23/22 21:19
LOH
Mt. Juliet, TN
Metals (ICPMS) by Method 60208
WG1959108
1
11/18/2210:54
11/18/2219:04
JPD
Mt. Juliet, TN
Metals (ICPMS) by Method 6020B
WG1959267
1
11/18/22 09:05
11/18/2215:19
JPD
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1958902
1
11/13/2216:58
11/13/2216:58
MGF
Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
MW-7 L1556126-04 GW
Brent Heard
11/09/2214:50
11/10/22 09:00
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
Gravimetric Analysis by Method 2540 C-2011
WG1960402
1
11/16/2210:16
_ 11/16/2212:25
DTM
Mt. Juliet, TN
Wet Chemistry by Method 350.1
WG1958220
1
11/15/2211:18
11/15/2211:18
JAR
Mt. Juliet, TN
Wet Chemistry by Method 365.4
WG1959629
1
11/14/22 07:54
11/14/2219:40
CAT
Mt. Juliet, TN
Wet Chemistry by Method 9056A
WG1957691
1
11/11/22 06:16
11/11/22 06:16
LBR
Mt. Juliet, TN
Wet Chemistry by Method 9060A
WG1964117
1
11/23/22 21:42
11/23/22 21:42
LOH
Mt. Juliet, TN
Metals (ICPMS) by Method 6020E
WG1959108
1
11/18/2210:54
11/18/2219:08
JPD
Mt. Juliet, TN
Metals (ICPMS) by Method 6020E
WG1959267
1
11/18/22 09:05
11/18/2215:22
JPD
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1958902
1
11/13/2217:20
11/13/2217:20
MGF
Mt. Juliet, TN
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 8522112 L1556126 11/28/22 11:12 3 of 37

CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
Heather J Wagner
Project Manager
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 8522112 L1556126 11/28/22 11:12 4 of 37

MW-1 SAMPLE RESULTS - 01
Collected date/time: 11/09/22 10:10 L1556126
Gravimetric Analysis by Method 2540 C-2011
Result
Qualifier
ROL
Dilution
Analysis
Batch
Cp
Analyte ug/I
ug/I
date / time
Dissolved Solids 131000
10000
1
11/16/202214:05
WG1960409
RC
Chemistry by Method 350.1
FSSI
Result
Qualifier
RDL
Dilution
Analysis
Batch
Analyte ug/I
ug/I
date / time
Fn
Ammonia Nitrogen ND
250
1
11/15/202211:12
WG1958220
Wet Chemistry by Method 365.4
Result
Qualifier
RDL
Dilution
Analysis
Batch
Analyte ug/I
ug/I
date / time
Q C
Phosphorus,Total NO
100
1
11/14/202219:32
WG1959629
E
Wet Chemistry by Method 9056A
Result
Qualifier
RDL
Dilution
Analysis
Batch
Ai
Analyte ug/I
ug/I
date / time
Chloride 2380
1000
1
11/11/2022 03:09
WG1957691
9
Nitrate as (N) 156
100
1
11/11/2022 03:09
WG1957691
SC
Sulfate 18800
5000
1
11/11/2022 03:09
WG1957691
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/1 date / time
TOC (Total Organic Carbon) 57300 B 10000 _ 10 11/24/2022 04:45 WG1964116
Metals (ICPMS) by Method 6020B
Result
Qualifier RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
date / time
Chromium
ND
2.00
1 11/18/202215:12
WG1959267
Chromium,Dissolved
NO
2.00
1 11/18/202218:40
WG1959108
Copper
ND
5.00
1 11/18/202215:12
WG1959267
Copper,Dissolved
ND
5.00
1 11/18/202218:40
WG1959108
Iron
ND
100
1 11/18/202215:12
WG1959267
Iron,Dissolved
ND
100
1 11/18t202218:40
WG1959108
Lead
ND
2.00
1 11/18/202215:12
WG1959267
Lead,Dissolved
ND
2.00
1 11/18/202218:40
WG1959108
Nickel
ND
2.00
1 11/18/202215:12
WG1959267
Nickel, Dissolved
ND
2.00
1 11/18/202218:40
WG1959108
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier RDL
Dilution
Analysis
Batch
Analyte
ug/I
ug/I
date / time
Acetone
ND
1250
25
11/15/2022 07:49
WG1959639
Acrolein
NO
1250
25
11/15/2022 07:49
WG1959639
Acrylonitrile
ND
250
25
11/15/2022 07:49
WG1959639
Benzene
ND
25.0
25
11/15/2022 07:49
WG1959639
Bromobenzene
NO
25.0
25
11/15/2022 07:49
WG1959639
Bromodichloromethane
ND
25.0
25
11/15/2022 07:49
WG1959639
Bromoform
ND
25.0
25
11/15/2022 07:49
WG1959639
Bromomethane
ND
125
25
11/15/2022 07:49
WG1959639
n-Butylbenzene
ND
25.0
25
11/15/2022 07:49
WG1959639
sec-Butylbenzene
ND
25.0
25
11/15/2022 07:49
WG1959639
tert-Butylbenzene
ND
25.0
25
11/15/2022 07:49
WG1959639
Carbon tetrachloride
NO
25.0
25
11/15/2022 07:49
WG1959639
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 8522112 L1556126 11/28/22 11:12 5 of 37

MW-1 SAMPLE RESULTS - 01
Collected date/time: 11/09/22 10:10 L1556126
Volatile Organic Compounds (GUMS) by Method 8260D
Analyte
Chlorobenzene _
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Di bromo-3-Chloropro pane
1,2-Dibromoethane
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dich loroethen e
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
2,2-Dichloropropane
Di -isopropyl ether
Ethylbenzene
Hexach loro-1,3-butadiene
Isopropylbenzene
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetra chloroethane
1,1,2-Trichlorotrifluoroetha ne
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trich lorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,2,3-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
Xylenes, Total
(S) Toluene-d8
(S) 4-Bromoiluorobenzene
Result
Qualifier RDL
Dilution
Analysis
Batch
ug/I
ug/I
date/time
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
125
25
11/15/2022 07:49
WG1959639
ND
125
25
11/15/2022 07:49
WG1959639
ND
62.5
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
125
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
125
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
250
25
11/15/2022 07:49
WG1959639
ND
125
25
11/15/2022 07:49
WG1959639
ND
250
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
125
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
125
25
11/15/2022 07:49
WG1959639
ND
62.5
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
25.0
25
11/15/2022 07:49
WG1959639
ND
75.0
25
11/15/2022 07:49
WG1959639
101
80.0-120
11115120220749
WG1959639
96.8
77.0-126
1111512022 0749
WG1959639
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 8522112 L1556126 11/28/2211:12 6 of 37

MW-1 SAMPLE RESULTS - 01
Collected date/time: 11/09/22 10:10 L1556126
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier RDL
Analyte ug/I ug/I
(S)1,2-Dichloroethone-d4 100 70.0-130
Sample Narrative:
L1556126-01 WG1959639: Dilution due to foam.
Dilution Analysis
date / time
1111512022 0749
Batch
WG1959639
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 8522112 L1556126 11/28/22 11:12 7 of 37

MW-5
SAMPLE RESULTS - 02
Collected date/time: 11/09/22 11:38
L1556126
Gravimetric Analysis by Method 2540 C-2011
Result
Qualifier
RDL Dilution
Analysis
Batch
E
Analyte ug/I
Solids 72000
ug/I
10000 1
date / time
11/16/202214:05
WG1960409
FCDissolved
Wet Chemistry by Method 350.1
Ss
F
Result
Qualifier
RDL Dilution
Analysis
Batch
Analyte ug/1
ugh
date / time
Ammonia Nitrogen ND
250 1
11/15/202211:13
WG1958220
Rn
Wet Chemistry by Method 365.4
7
Result
Analyte ug/I
Qualifier
RDL Dilution
ug/I
Analysis
date / time
Batch
FQC:
Phosphorus,Total ND
100 1
11/14/202219.34
WG1959629
Wet Chemistry by Method 9056A
F,
Result
Qualifier
RDL Dilution
Analysis
Batch
Analyte ug/I
ug/I
date / time
F
Chloride 16300
Nitrate as (N) NO
1000 1
100 1
11/11/2022 04:36
11/11/2022 04:36
WG1957691
WG1957691
SC
I
Sulfate 19200
5000 1
11/11/2022 04:36
WG1957691
Wet Chemistry by Method 9060A
Result
Qualifier
RDL Dilution
Analysis
Batch
Analyte ug/I
ugh
date / time
TOC (Total Organic Carbon) 2750
B
1000 1
11/24/2022 05:01
WG1964116
Metals (ICPMS) by Method 6020E
Result
Qualifier
RDL Dilution
Analysis
Batch
Analyte ug/I
ug/1
date / time
Chromium ND
2.00 1
111181202215:15
WG1959267
Chromium,Dissolved ND
2.00 1
11/18/202218:43
WG1959108
Copper ND
5.00 1
11/18/202215:15
WG1959267
Copper,Dissolved ND
5.00 1
11/18/202218:43
WG1959108
Iron 176
100 1
11/18/202215:15
WG1959267
Iron,Dissolved ND
100 1
11/18/202218:43
WG1959108
Lead ND
2.00 1
11/18/202215:15
WG1959267
Lead,Dissolved ND
2.00 1
11/18/202218:43
WG1959108
Nickel ND
2.00 1
11/18/202215:15
WG1959267
Nickel, Dissolved ND
2.00 1
11118/202218:43
WG1959108
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier
RDL Dilution
Analysis
Batch
Analyte ugh
ugh
date / time
Acetone ND
50.0 1
11/13/202216:36
WG1958902
Acrolein ND
J4
50.0 1
11/13/202216:36
WG1958902
Acrylonitrile ND
10.0 1
11/13/202216:36
WG1958902
Benzene ND
1.00 1
11/13/202216:36
WG1958902
Bromobenzene ND
1.00 1
11/13/202216:36
WG1958902
Bromodichloromethane ND
1.00 1
11113/202216:36
WG1958902
Bromoform ND
1.00 1
11/13/202216:36
WG1958902
Bromomethane ND
5.00 1
11113/202216:36
WG1958902
n-Butylbenzene ND
1.00 1
11/13/202216:36
WG1958902
sec-Butylbenzene ND
1.00 1
11/13/202216:36
WG1958902
tert-Butylbenzene ND
1.00 1
11/13/202216:36
WG1958902
Carbon tetrachloride ND
1.00 1
11/13/202216:36
WG1958902
ACCOUNT:
PROJECT:
SDG:
DATEMME:
PAGE:
Frit Car Inc.
8522112
L1556126
11/28/22 11:12
8 of 37

MW-5 SAMPLE RESULTS - 02
Collected date/time: 11/09/22 11:38 L1556126
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
date / time
Chlorobenzene
ND
1.00
1 11/13/202216:36
WG1958902
Chlorodibromomethane
ND
1.00
1 11/131202216:36
WG1958902
Chloroethane
ND
5.00
1 11/13/202216:36
WG1958902
Chloroform
ND
5.00
1 11/13/202216:36
WG1958902
Chloromethane
ND
2.50
1 11/13/202216:36
WG1958902
2-Chlorotoluene
ND
1.00
1 11/13/202216:36
WG1958902
4-Chlorotoluene
ND
1.00
1 11/13/202216:36
WG1958902
1,2-Dibromo-3-Chloropropane
ND
5.00
1 11/13/202216:36
WG1958902
1,2-Dibromoethane
ND
1.00
1 11/13/202216:36
WG1958902
Dibromomethane
ND
1.00
1 11/13/202216:36
WG1958902
1,2-Dichlorobenzene
ND
1.00
1 11/13/202216:36
WG1958902
1,3-Dichlorobenzene
ND
1.00
1 11/13/202216:36
WG1958902
1,4-Dichlorobenzene
ND
1.00
1 11/13/202216:36
WG1958902
Dichlorodifluoromethane
ND
5.00
1 11/13/202216:36
WG1958902
1,1-Dichloroethane
ND
1.00
1 11/13/202216:36
WG1958902
1,2-Dichloroethane
ND
1.00
1 11/13/202216:36
WG1958902
1,1-Dichloroethene
ND
1.00
1 11/13/202216:36
WG1958902
cis-1,2-Dichloroethene
ND
1.00
1 11/13/202216:36
WG1958902
trans-1,2-Dichloroethene
ND
1.00
1 11/13/202216:36
WG1958902
1,2-Dichloropropane
ND
1.00
1 11/13/202216:36
WG1958902
1,1-Dichloropropene
ND
1.00
1 11/13/202216:36
WG1958902
1,3-Dichloropropane
ND
1.00
1 11/13/202216:36
WG1958902
cis-1,3-Dichloropropene
ND
1.00
1 11/13/202216:36
WG1958902
trans-1,3-Dichloropropene
ND
1.00
1 11/13/202216:36
WG1958902
2,2-Dichloropropane
ND
1.00
1 11/13/202216:36
WG1958902
Di -isopropyl ether
ND
1.00
1 11/13/202216:36
WG1958902
Ethylbenzene
ND
1.00
1 11/13/202216:36
WG1958902
Nexachloro-1,3-butadiene
ND
1.00
1 11/131202216:36
WG1958902
Isopropylbenzene
ND
1.00
1 111131202216:36
WG1958902
p-Isopropyltoluene
ND
1.00
1 11/13/202216:36
WG1958902
2-Butanone (MEK)
ND
10.0
1 11/13/202216:36
WG1958902
Methylene Chloride
ND
5.00
1 11/13/202216:36
WG1958902
4-Methyl-2-pentanone (MIBK)
ND
10.0
1 11/13/202216:36
WG1958902
Methyl tert-butyl ether
ND
1.00
1 11/13/202216:36
WG1958902
Naphthalene
ND
5.00
1 11/13/202216:36
WG1958902
n-Propylbenzene
ND
1.00
1 11/13/202216:36
WG1958902
Styrene
ND
1.00
1 11/13/202216:36
WG1958902
1,1,1,2-Tetrachloroethane
ND
1.00
1 11/13/202216:36
WG1958902
1,1,2,2-Tetrachloroethane
ND
1.00
1 11/13/202216:36
WG1958902
1,1,2-Trichlorotrifluoroethane
ND
1.00
1 11/13/202216:36
WG1958902
Tetrachloroethene
ND
1.00
1 11/13/202216:36
WG1958902
Toluene
ND
1.00
1 11/13/202216:36
WG1958902
1,2,3-Trichlorobenzene
ND
1.00
1 11/13/202216:36
WG1958902
1,2,4-Trichlorobenzene
ND
1.00
1 11/13/202216:36
WG1958902
1,1,1-Trichloroethane
ND
1.00
1 11/13/202216:36
WG1958902
1,1,2-Trichloroethane
ND
1.00
1 11/13/202216:36
W(31958902
Trichloroethene
ND
1.00
1 11/13/202216:36
WG1958902
Trichlorofluoromethane
ND
5.00
1 11/13/202216:36
WG1958902
1,2,3-Trichloropropane
ND
2.50
1 11/13/202216:36
WG1958902
1,2,4-Trimethylbenzene
ND
1.00
1 11113/202216:36
WG1958902
1,2,3-Trimethylbenzene
ND
1.00
1 11/13/202216:36
WG1958902
1,3,5-Trimethylbenzene
ND
1.00
1 11/13/202216:36
WG1958902
Vinyl chloride
ND
1.00
1 11/13/202216:36
WG1958902
Xylenes, Total
ND
3.00
1 11/13/202216:36
WG1958902
(S) Toluene-d8
100
80.0-120
111131202216.36
WG1958902
(S) 4-Bromofluorobenzene
101
77.0-126
111131202216.36
WG1958902
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 8522112 L1556126 11/28/22 11:12 9 of 37

MW-5 SAMPLE RESULTS - 02
Collected date/time: 11/09/22 11:38 L1556126
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier RDL Dilution Analysis Batch
Analyte ugh ug,/l date / time
(S)1,2-Dichloroethone-0 108 70.0-130 11113120221636 WG1958902
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 8522112 L1556126 11/28/22 11:12 10 of 37

MW-6 SAMPLE RESULTS - 03
Collected date/time: 11/09/22 13:44 L1556126
Gravimetric Analysis by Method 2540 C-2011
Result
Qualifier
RDL
Dilution
Analysis
Batch
Cp
a
Analyte ug/I
ug/I
date / time
zTC
Dissolved Solids 56000
10000
1
11/16/202214:05
WG1960409
Wet Chemistry by Method 350.1
Ss
Result
Qualifier
RDL
Dilution
Analysis
Batch
Analyte ug/I
ug/I
date / time
Fn
Ammonia Nitrogen ND
�250
1
11/15/202211:15
WG1958220
Wet Chemistry by Method 365.4
0
Result
Analyte ug/I
Qualifier
RDL
ug/I
Dilution
Analysis
date / time
Batch
QC
Phosphorus,Total ND
100
1
11/14/202219:39
WG1959629
EWet
Chemistry by Method 9056A
Result
Qualifier
RDL
Dilution
Analysis
Batch
F
Analyte ug/I
ug/I
date / time
Chloride 14100
Nitrate as (N) ND
1000
100
1
1
11/11/2022 05:01
11/11/2022 05:01
WG1957691
WG1957691
RC
Sulfate 10900
5000
1
11/11/2022 05:01
WG1957691
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date / time
TOC (Total Organic Carbon) 1290 B 1000 1 11/23/2022 21:19 WG1964117
Metals (ICPMS) by Method 6020B
Analyte
Chromium
Chromium,Dissolved
Copper
Copper,Dissolved
Iron
Iron,Dissolved
Lead
Lead,Dissolved
Nickel
Nickel, Dissolved
Result
Qualifier RDL
Dilution Analysis
ug/I
ug/I
_
date / time
ND
2.00
1 11/18/202215:19
ND
2.00
1 11/18/202219:04
ND
5.00
1 11/18/202215:19
ND
5.00
1 11/18/202219:04
177
100
1 11/18/202215:19
119
100
1 11/18/202219:04
ND
2.00
1 11/18/202215:19
ND
2.00
1 11/18/202219:04
ND
2.00
1 11/18/202215:19
ND
2.00
1 11/18/202219:04
Volatile Organic Compounds (GC/MS) by Method 8260D
Batch
WG1959267
WG1959108
WG1959267
WG1959108
WG1959267
WG1959108
WG1959267
WG1959108
WG1959267
WG1959108
Result
Qualifier RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
date / time
Acetone
ND
50.0
1 11/13/202216:58
WG1958902
Acrolein
ND
J4 50.0
1 11113/202216:58
WG1958902
Acrylonitrile
ND
10.0
1 11/13/202216:58
WG1958902
Benzene
ND
1.00
1 11/13/202216:58
WG1958902
Bromobenzene
ND
1.00
1 11/13/202216:58
WG1958902
Bromodichloromethane
ND
1.00
1 11/13/202216:58
WG1958902
Bromoform
ND
1.00
1 11/13/202216:58
WG1958902
Bromomethane
ND
5.00
1 11/13/202216:58
WG1958902
n-Butylbenzene
ND
1.00
1 11/131202216:58
WG1958902
sec-Butylbenzene
ND
1.00
1 11/13/202216:58
WG1958902
tert-Butylbenzene
ND
1.00
1 11/13/202216:58
WG1958902
Carbon tetrachloride
ND
1.00
1 11/13/202216:58
WG1958902
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 8522112 L1556126 11/28/22 11:12 11 of 37

MW-6
SAMPLE
RESULTS - 03
Collected date/time: 11/09/22
13:44
L1556126
Volatile Organic Compounds (GC/MS) by Method 8260D
FPAnalyte
Result
Qualifier RDL Dilution Analysis
Batch
ug/I
ug/I
date / time
Chlorobenzene
"
ND
1.00 1
11/13/202216:58
WG1958902
2
Tc
Chlorodibromomethane
ND
1.00 1
11/13/202216:58
WG1958902
Chloroethane
ND
5.00 1
11/13/202216:58
WG1958902
Chloroform
ND
5.00 1
11/13/202216:58
WG1958902
F
Chloromethane
ND
2.50 1
111131202216:58
WG1958902
2-Chlorotoluene
ND
1.00 1
11/13/202216:58
WG1958902
F n
4-Chlorotoluene
ND
1.00 1
11/13/202216:58
WG1958902
1,2-Dibromo-3-Chloropropane
ND
5.00 1
11/13/202216:58
WG1958902
1,2-Dibromoethane
ND
1.00 1
11/13/202216:58
WG1958902
Dibromomethane
ND
1.00 1
11113/202216:58
WG1958902
1,2-Dichlorobenzene
ND
1.00 1
11/13/202216:58
WG1958902
QC
1,3-Dichlorobenzene
ND
1.00 1
11/13/202216:58
WG1958902
1,4-Dichlorobenzene
ND
1.00 1
111131202216:58
WG1958902
Dichlorodifluoromethane
ND
5.00 1
11/13/202216:58
WG1958902
GI
1,1-Dichloroethane
ND
1.00 1
11/13/202216:58
WG1958902
1,2-Dichloroethane
ND
1.00 1
11/13/202216:58
WG1958902
AI
1,1-Dichloroethene
ND
1.00 1
111131202216:58
WG1958902
cis-1,2-Dichloroethene
ND
1.00 1
11/13/202216:58
WG1958902
trans-1,2-Dichloroethene
ND
1.00 1
11/13/202216:58
WG1958902
FS
1,2-Dichloropropane
ND
1.00 1
11/13/202216:58
WG1958902
1,1-Dichloropropene
ND
100 1
11/13/202216:58
WG1958902
1,3-Dichloropropane
ND
1.00 1
11/13/202216:58
WG1958902
cis-1,3-Dichloropropene
ND
1.00 1
11/13/202216:58
WG1958902
trans-1,3-Dichloropropene
ND
1.00 1
11/13/202216:58
WG1958902
2,2-Dichloropropane
ND
1.00 1
11/13/202216:58
WG1958902
Di -isopropyl ether
ND
1.00 1
11/13/202216:58
WG1958902
Ethylbenzene
ND
1.00 1
11/13/202216:58
WG1958902
Hexachloro-1,3-butadiene
ND
1.00 1
11/131202216:58
WG1958902
Isopropylbenzene
ND
1.00 1
11/13/202216:58
WG1958902
p-Isopropyltoluene
ND
1.00 1
11/13/202216:58
WG1958902
2-Butanone (MEK)
ND
10.0 1
111131202216:58
WG1958902
Methylene Chloride
ND
5.00 1
11/13/202216:58
WG1958902
4-Methyl-2-pentanone (MIBK)
ND
10.0 1
11/13/202216:58
WG1958902
Methyl tert-butyl ether
ND
1.00 1
11/13/202216:58
WG1958902
Naphthalene
ND
5.00 1
11/13/202216:58
WG1958902
n-Propylbenzene
ND
1.00 1
11/13/202216:58
WG1958902
Styrene
ND
1.00 1
11/13/202216:58
WG1958902
1,1,1,2-Tetrachloroethane
ND
1.00 1
11/13/202216:58
WG1958902
1,1,2,2-Tetrachloroethane
ND
1.00 1
11/13/202216:58
WG1958902
1,1,2-Trichlorotrifluoroethane
ND
1.00 1
11/13/202216:58
WG1958902
Tetrachloroethene
ND
1.00 1
11/13/202216:58
WG1958902
Toluene
ND
1.00 1
11/13/202216:58
WG1958902
1,2,3-Trichlorobenzene
ND
1.00 1
111131202216:58
WGI958902
1,2,4-Trichlorobenzene
ND
1.00 1
11/13/202216:58
WG1958902
1,1,1-Trichloroethane
ND
1.00 1
11/13/202216:58
WG1958902
1,1,2-Trichloroethane
ND
1.00 1
11/13/202216:58
WG1958902
Trichloroethene
ND
1.00 1
11/13/202216:58
WG1958902
Trichlorofluoromethane
ND
5.00 1
11/13/202216:58
WG1958902
1,2,3-Trichloropropane
ND
2.50 1
11/13/202216:58
WG1958902
1,2,4-Trimethylbenzene
ND
1.00 1
11/13/202216:58
WG1958902
1,2,3-Trimethylbenzene
ND
1.00 1
11/13/202216:58
WG1958902
1,3,5-Trimethylbenzene
ND
1.00 1
11/13/202216:58
WG1958902
Vinyl chloride
ND
1.00 1
11/13/202216:58
WG1958902
Xylenes, Total
ND
3.00 1
11/13/202216:58
WG1958902
(S) Toluene-d8
102
80.0-120
111131202216:58
WG1958902
(S) 4-Bromotluorobenzene
98.9
Tl.0-126
111131202216:58
WG1958902
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 8522112 L1556126 11/28/22 11:12 12 of 37

MW-6 SAMPLE RESULTS - 03
Collected date/time: 11/09/22 13:44 L1556126
Volatile Organic Compounds (GC/MS) by Method 8260D
Analyte
(S) 1,2-Dichloroethone-N
Result Qualifier RDL Dilution Analysis
ug/I ug/I date / time
109 70.0130 11/13/202216:58
Batch
WG1958902
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 8522112 L1556126 11/28/22 11:12 13 of 37

MW-7 SAMPLE RESULTS - 04
Collected date/time: 11/09/22 14:50 L1556126
Gravimetric Analysis by Method 2540 C-2011
Result
Qualifier
RDL
Dilution
Analysis
Batch
Analyte ug/I
ug/I
date / time
Dissolved Solids 480000
10000
1
11/16/202212:25
WG1960402
T C
Wet Chemistry by Method 350.1
Ss
Result
Qualifier
RDL
Dilution
Analysis
Batch
Analyte ug/I ug/I date / time
Ammonia Nitrogen ND
250
1
11/15/202211:18
WG1958220
Rn
Wet Chemistry by Method 365.4
Result
Qualifier
RDL
Dilution
Analysis
Batch
Analyte ug/I
ug/I
date / time
Rc
Phosphorus,Total ND
100
1
11/14/202219:40
WG1959629
Wet Chemistry by Method 9056A
�GI
Result
Qualifier
RDL
Dilution
Analysis
Batch
Analyte ug/I
ug/I
date / time
AI
Chloride 131000
Nitrate as (N) 127
1000
100
1
1
11/11/2022 06:16
11/11/2022 06:16
WG1957691
WG1957691
9SC
Sulfate 162000
5000
1
11/11/2022 06:16
WG1957691
Wet Chemistry by Method 9060A
Result
Qualifier
RDL
Dilution
Analysis
Batch
Analyte ug/I
ug/I
date / time
TOC (Total Organic Carbon) 12300
1000
1
11/23/2022 21:42
WG1964117
Metals (ICPMS) by Method 6020B
Result
Qualifier RDL
Dilution Analysis
Batch
Analyte
ug/I
ugh
date / time
Chromium
ND
2.00
1 111181202215:22
WG1959267
Chromium,Dissolved
ND
2.00
1 11/18/202219:08
WG1959108
Copper
ND
5.00
1 11/18/202215:22
WG1959267
Copper,Dissolved
ND
5.00
1 11/18/202219:08
WG1959108
Iron
5530
100
1 11/18/202215:22
WG1959267
Iron,Dissolved
711
100
1 11/18/202219:08
WG1959108
Lead
ND
2.00
1 11/18/202215:22
WG1959267
Lead,Dissolved
ND
2.00
1 11/18/202219:08
WG1959108
Nickel
ND
2.00
1 11/18/202215:22
WG1959267
Nickel,Dissolved
ND
2.00
1 11/18/202219:08
WG1959108
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
date / time
Acetone
ND
50.0
1 11/13/202217:20
WG1958902
Acrolein
ND
J4 50.0
1 11/13/202217:20
WG1958902
Acrylonitrile
ND
10.0
1 11/13/202217:20
WG1958902
Benzene
ND
1.00
1 11/13/202217:20
WG1958902
Bromobenzene
ND
1.00
1 11/13/202217:20
WG1958902
Bromodichloromethane
NO
1.00
1 11/13/202217:20
WG1958902
Bromoform
ND
1.00
1 11/13/202217:20
WG1958902
Bromomethane
NO
5.00
1 11/13/202217:20
WG1958902
n-Butylbenzene
ND
1.00
1 11/13/202217:20
WG1958902
sec -Butyl benzene
ND
1.00
1 11/13/202217:20
WG1958902
tert-Butylbenzene
ND
1.00
1 11/13/202217:20
WG1958902
Carbon tetrachloride
NO
1.00
1 11/13/202217:20
WG1958902
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 8522112 L1556126 11/28/22 11:12 14 of 37

MW-7 SAMPLE RESULTS - 04
Collected date/time: 11/09/22 14:50 L1556126
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Oualifier RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
date / time
Chlorobenzene
ND
1.00
1 11/13/202217:20
WG1958902
Chlorodibromomethane
ND
1.00
1 11/131202217:20
WG1958902
Chloroethane
ND
5.00
1 11/13/202217:20
WG1958902
Chloroform
ND
5.00
1 11/13/202217:20
WG1958902
Chloromethane
ND
2.50
1 11/13/202217:20
WG1958902
2-Chlorotoluene
ND
1.00
1 11/13/202217:20
WG1958902
4-Chlorotoluene
ND
1.00
1 11/13/202217:20
WG1958902
1,2-Dibromo-3-Chloropropane
ND
5.00
1 11/131202217:20
WG1958902
1,2-Dibromoethane
ND
1.00
1 11/13/202217:20
WG1958902
Dibromomethane
ND
1.00
1 11/13/202217:20
WG1958902
1,2-Dichlorobenzene
ND
1.00
1 11/13/202217:20
WG1958902
1,3-Dichlorobenzene
ND
1.00
1 11/13/202217:20
WG1958902
1,4-Dichlorobenzene
ND
1.00
1 11/13/202217:20
WG1958902
Dichlorodifluoromethane
ND
5.00
1 11/13/202217:20
WG1958902
1,1-Dichloroethane
ND
1M
1 11/13/202217:20
WG1958902
1,2-Dichloroethane
ND
1.00
1 11/13/202217:20
WG1958902
1,1-Dichloroethene
ND
1.00
1 11/13/202217:20
WG1958902
cis-1,2-Dichloroethene
ND
1.00
1 11/13/202217:20
WG1958902
trans-1,2-Dichloroethene
ND
1.00
1 11/13/202217:20
WG1958902
1,2-Dichloropropane
ND
1.00
1 11/13/202217:20
WG1958902
1,1-Dichloropropene
ND
1.00
1 11/13/202217:20
WG1958902
1,3-Dichloropropane
ND
1.00
1 11/13/202217:20
WG1958902
cis-1,3-Dichloropropene
ND
1.00
1 11/13/202217:20
WG1958902
trans-1,3-Dichloropropene
ND
1.00
1 11/13/202217:20
WG1958902
2,2-Dichloropropane
ND
1.00
1 11/13/202217:20
WG1958902
Di -Isopropyl ether
ND
1.00
1 11/13/202217:20
WG1958902
Ethylbenzene
ND
1.00
1 11/13/202217:20
WG1958902
Hexachloro-1,3-butadiene
ND
1.00
1 11/13/202217:20
WG1958902
Isopropylbenzene
ND
1.00
1 11/13/202217:20
WG1958902
p-Isopropyltoluene
ND
1.00
1 11/13/202217:20
WG1958902
2-Butanone (MEK)
ND
10.0
1 11/13/202217:20
WG1958902
Methylene Chloride
ND
5.00
1 11/13/202217:20
WG1958902
4-Methyl-2-pentanone (MIBK)
ND
10.0
1 11/13/202217:20
WG1958902
Methyl tert-butyl ether
ND
1.00
1 11/13/202217:20
WG1958902
Naphthalene
ND
5.00
1 11/13/202217:20
WG1958902
n-Propylbenzene
ND
1.00
1 11/13/202217:20
WG1958902
Styrene
ND
1.00
1 11/13/202217:20
WG1958902
1,1,1,2-Tetrachloroethane
ND
1.00
1 11/13/202217:20
WG1958902
1,1,2,2-Tetrachloroethane
ND
1.00
1 11/13/202217:20
WG1958902
1,1,2-Trichlorotrifluoroethane
ND
1.00
1 11/13/202217:20
WG1958902
Tetra chloroethene
ND
1.00
1 11/13/202217:20
WG1958902
Toluene
ND
1.00
1 11/13/202217:20
WG1958902
1,2,3-Trichlorobenzene
ND
1.00
1 11/13/202217:20
WG1958902
1,2,4-Trichlorobenzene
ND
1.00
1 11/13/202217:20
WG1958902
1,1,1-Trichloroethane
ND
1.00
1 11/13/202217:20
WG1958902
1,1,2-Trichloroethane
ND
1.00
1 11/13/202217:20
WG1958902
Trichloroethene
ND
1.00
1 11/13/202217:20
WG1958902
Trichlorofluoromethane
ND
5.00
1 11/13/202217:20
WG1958902
1,2,3-Trichloropropane
ND
2.50
1 11/13/202217:20
WG1958902
1,2,4-Trimethylbenzene
ND
1.00
1 11/13/202217:20
WG1953902
1,2,3-Trimethylbenzene
ND
1.00
1 11/13/202217:20
WG1958902
1,3,5-Trimethylbenzene
ND
1.00
1 11/13/202217:20
WG1958902
Vinyl chloride
ND
1.00
1 11/13/202217:20
WG1958902
Xylenes, Total
ND
3.00
1 11/13/202217:20
WG1958902
(S) Toluene-d8
102
80.0-120
11113120221720
WG1958902
(S) 4-Bromofluorobenzene
98.8
77.0-126
111131202217:20
WG1958902
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 8522112 L1556126 11/28/22 11:12 15 of 37

MW-7 SAMPLE RESULTS - 04
Collected date/time: 11/09/22 14:50 L1556126
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug!I date / time
(S)1,2-Dichloroethone-N 106 70.0-130 111131202217:20 WG1958902 ITC]
17S
Fri
MC
F
F
FC]
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 8522112 L1556126 11/28/22 11:12 16 of 37

WG1960402 QUALITY CONTROL SUMMARY
Gravimetric Analysis by Method 2540 C-2011 L1556126-04
Wthod Blank (P�i
(MB) R3863236-1 11/16/22 12:25
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/I ug/I ugh TC
Dissolved Solids U 10000 10000
L1555591-09 Original Sample (OS) • Duplicate (DUP)
(OS) L1555591-09 11/16/22 12:25 • (DUP) R3863236-3 11/16/22 12:25
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I % %
Dissolved Solids 26000 28000 1 7.41 _ 5
L1556017-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1556017-01 11/16/22 12:25 • (DUP) R3863236-4 11/16/22 12:25
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I % %
Dissolved Solids 1090000 1140000 1 4.47 5
Laboratory Control Sample (LCS)
(LCS) R3863236-2 11/16/22 12:25
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I ugh % %
Dissolved Solids 8800000 8540000 97.0 77.3-123
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Frit Car Inc.
8522112
L1556126
11/28/22 11:12
17 of 37

WG1960409 QUALITY CONTROL SUMMARY
Gravimetric Analysis by Method 2540 C-2011 L1556126 01.02,03
Metnod Blank (MB)
(MB) R3863629-1 11/16/22 14:05
MB Result MB Qualifier MB MDL MB RDL 2
Analyte ug/I Ug/1 Ug/1 TC
Dissolved Solids U 10000 10000
L1556859-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1556859-02 11/16/22 14:05 • (DUP) R3863629-3 11/16/22 14:05
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/1 % %
Dissolved Solids 593000 602000 1 1.51 5
L1556859-03 Original Sample (OS) • Duplicate (DUP)
(OS) L1556859-03 11/16/22 14:05 • (DUP) R3863629-4 11/16/22 14:05
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte Ug/I ug/I % %
Dissolved Solids 242000 247000 1 2.04 5
Laboratory Control Sample (LCS)
(LCS) R3863629-2 11/16/22 14:05
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I Ug/1 % %
Dissolved Solids 8800000 9080000 103 77 3-123
ACCOUNT: PROJECT: SDG:
Frit Car Inc. 8522112 L1556126
DATE/TIME:
11/28/22 11:12
PAGE:
18 of 37

WG1958220 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 350.1 L1556126-01,02,03,04
Method Blank (MB)
(MB) R3861090-1 11/15/22 10:45
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/I ug/I ug/I
Ammonia Nitrogen U 117 250
L1556O91-01 Original Sample (OS) - Duplicate (DUP)
(OS) L1556091-01 11/15/2210:58 - (DUP) R3861090-5 11/15/2211:04
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/1 % %
Ammonia Nitrogen ND ND 1 0.000 10
L1556126-04 Original Sample (OS) - Duplicate (DUP)
(OS) L1556126-04 11/15/22 11:18 - (DUP) R3861090-7 11/15/22 11:24
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I % %
Ammonia Nitrogen ND ND 1 3.86 10
Laboratory Control Sample (LCS)
(LCS) R3861090-2 11/15/2210:46
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I ug/I % %
Ammonia Nitrogen 7500 7640 102 90.0-110
L1556O79-02 Original Sample (OS) - Matrix Spike (MS) - Matrix Spike Duplicate (MSD)
(OS) L1556079-02 11/15/2210:54 - (MS) R3861090-3 11/15/22 10:55 - (MSD) R3861090-4 11/15/22 10:57
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/I ug/I ug/I ug/I % % % % %
Ammonia Nitrogen 5000 NO 5020 5020 100 100 1 90.0-110 0.120 10
L1556126-03 Original Sample (OS) - Matrix Spike (MS)
(OS) L1556126-03 11/15/2211:15 - (MS) R3861090-6 11/15/2211:16
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte ug/I ugh ug/I % %
Ammonia Nitrogen 5000 ND 5110 102 1 90.0-110
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 8522112 L1556126 11/28/22 1112 19 of 37

WG1959629 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 365.4 L1556126-01,02,03.04
Method Blank (MB)
(MB) R3860876-1 11/14/2219:07
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/1 ug/1 Ug/1
Phosphorus,Total U 35.0 100
L1555749-03 Original Sample (OS) • Duplicate (DUP)
(OS) L1555749-03 11/14/22 19:17 • (DUP) R3860876-9 11/14/22 19:18
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I % %
Phosphorus,Total 4370 4000 1 8.84 20
Laboratory Control Sample (LCS)
(LCS) R3860876-2 11/14/22 19:08
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I Ug/1 % %
Phosphorus,Total 3780 3870 102 83.2-116
ACCOUNT: PROJECT: SDG:
Frit Car Inc. 8522112 L1556126
DATE/TIME:
11/28/22 11:12
PAGE:
20 of 37

WG1957691
QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9056A
L1556126-01,02,03,04
Mettlou Bunk I,MB)
(MB) R3860376-1 11/11/22 00:39
MB Result MB Qualifier MB MDL MB ROL
2
Analyte ug/I ug/I ug/I
TC
Chloride U 379 1000
Nitrate U 48.0 100
F
Sulfate U 594 5000
Fn
L1556135-05 Original Sample (OS) • Duplicate (DUP)
(OS) L1556135-05 11/11/22 07:06 • (DUP) R3860376-5 11/11/22 07:18
Fr
Result DUP Result Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
•
Analyte ug/I ug/I %
%
�
Chloride 20300 20400 1 0.237
Nitrate ND ND 1 0.000
15
15
[Gl
Sulfate 1770000 1780000 1 0.415
_ 15
Al
L1556126-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1556126-01 11/11/22 03:09 • (DUP) R3860376-3 11/11/22 03:22
FSCI
Original Result DUP Result Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I
Chloride 2380 2300
Nitrate 156 160
Sulfate 18800 18800
Laboratory Control Sample (LCS)
1
1
1
%
3.63
3.04
0.169
% _
15
15
15
(LCS) R3860376-2 11/11/22 00:52
Spike Amount LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte ug/I ugh
%
%
Chloride 40000 42100
105
80.0-120
Nitrate 8000 8300
104
80.0-120
Sulfate 40000 42600
107
80.0-120
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc.
8522112 L1556126 11/28/22 11:12 21 of 37

WG1957691 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9056A L1556126-01,02.03,04
L1556135-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (PAiSD)
(OS) L1556135-05 11/11/22 07:06 • (MS) R3860376-6 11/11/22 07:31 . (MSD) R3860376-7 11/11/22 08:08
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution
Rec. Limits MS Qualifier
MSD Qualifier RPD
RPD Limits
Analyte ug/I ug/I ug/I ug/I % %
%
%
%
Tc
Chloride 50000 20300 71500 71500 102 102 1
80.0-120
0.00854
15
Nitrate 5000 ND 5050 5940 101 119 1
80.0-120
16.2
15
F
Sulfate 50000 1770000 1780000 1790000 2.91 37.9 1
80.0-120
_— 0.980
15
Fn
L1556126-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1556126-01 11/11/22 03:09 • (MS) R3860376-4 11/11/22 03:34
FrSpike
Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analy[e ug/I ug/I ug/I % %
Chloride 50000 2380 54900 105 1 80.0-120
Nitrate 5000 156 5390 105 1 80.0-120
Sulfate 50000 18800 70800 104 1 80.0-120
GI
FAI
FSCI
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 8522112 L1556126 11/28/22 11:12 22 of 37

WG1964116 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9060A L1556126-01,02
Method Blank (MB)
Fp
(MB) R3864757-2 11/23/22 20:19
— —
MB Result MB Qualifier MB MDL MB ROL
Analyze ug/I ug/I ug/I
- -- -
- ---
F
TOC (Total Organic Carbon) 665 J 102 1000
FS
L1555559-01 Original Sample (OS) • Duplicate (DUP)
Fn
(OS) L1555559-01 11/23/22 20:36 • (DUP) R3864757-3 11/23/22 20:49
Original Result DUP Result Dilution DUP RPD
DUP Qualifier DUP RPDLimits
Fr
Analyte ug/I ug/I %
%
TOC (Total Organic Carbon) 2420 2230 1 8.05
20
L1555720-05 Original Sample (OS) • Duplicate (DUP)
�GI
(OS) L1555720-05 11/23/22 21:45 • (DUP) R3864757-4 11/23/22 22:01
Original Result DUP Result Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
A
Analyte ug/I ug/I %
%
TOC (Total Organic Carbon) 1610 1400 1 14.0
20
Fc
Laboratory Control Sample (LCS)
(LCS) R3864757-1 11/23/22 20:03
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I ug/I % %
TOC (Total Organic Carbon) 75000 77000 103 85.0-115
L1555720-09 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1555720-09 11/23/22 23:48 • (MS) R3864757-5 11/24/22 00:10 • (MSD) R3864757-6 11/24/22 00:27
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/I ug/I ug/I ug/I % % % % %
TOC (Total Organic Carbon) 50000 1590 63400 63400 124 124 1 80.0-120 _ 0.0158 20
L1555720-10 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1555720-10 11/24/22 00:47 • (MS) R3864757-7 11/24/22 01:10 • (MSD) R3864757-8 11/24/22 01:30
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits
Analyte ug/I ug/I ug/I ug/I % % %
TOC (Total Organic Carbon) 50000 1610 63000 63900 123 d 125 1 80.0-120
MS Qualifier MSD Qualifier RPD
1.42
RPD Limits
20
ACCOUNT: PROJECT: SDG:
Frit Car Inc. 8522112 L1556126
DATE/TIME:
11/28/22 11:12
PAGE:
23 of 37

WG1964117 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9060A L1556126-03.04
Method Blank (MB)
(MB) R3864780-2 11/23/22 20:59
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/1 ug/1 ug/I ZTC
TOC (Total Organic Carbon) 276 J 102 1000
L1556135-04 Original Sample (OS) - Duplicate (DUP)
(OS) L1556135-04 11/24/22 01:01 - (DUP) R3864780-7 11/24/22 01:18
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ugh % %
TOC (Total Organic Carbon) 1010 ND 1 6.24 20
L1556135-05 Original Sample (OS) - Duplicate (DUP)
(0,S) L1556135-05 11/24/22 01:36 - (DUP) R3864780-8 11/24/22 01:53
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I % %
TOC (Total Organic Carbon) 1110 1260 1 12.5 20
Laboratory Control Sample (LCS)
(LCS) R3864780-1 11/23/22 20:43
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/1 ug/I % %
TOC (Total Organic Carbon) 75000 74600 99.4 85.0-115
L1556135-01 Original Sample (OS) - Matrix Spike (MS) - Matrix Spike Duplicate (MSD)
(OS) L1556135-01 11/23/22 21:58 - (MS) R3864780-3 11/23/22 22:21 - (MSD) R3864780-4 11/23/22 22:43
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/1 ug/1 ug/1 ug/1 % % % % %
TOC (Total Organic Carbon) 50000 NO 59100 59200 117 117 1 80.0-120 0.0169 20
L1556135-02 Original Sample (OS) - Matrix Spike (MS) - Matrix Spike Duplicate (MSD)
(OS) L1556135-02 11/23/22 23:01 - (MS) R3864780-5 11/23/22 23:24 - (MSD) R3864780-6 11/23/22 23:46
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/1 ug/1 ug/I ug/I % % % % %
TOC (Total Organic Carbon) 50000 2600 61700 62200 118 119 1 80.0-120 0.920 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 8522112 L1556126 11/28/22 11:12 24 of 37

WG1959108 QUALITY CONTROL SUMMARY
Metals (ICPMS) by Method 6020B L1556126-01,02,03,04
Mutncu t3larlk (ivlfJ)
(MB) R3862940-2 11/18/22 17:33
MB Result
Analyte
ug/1
Chromium,Dissolved
U
Copper,Dissolved
U
Iron,Dissolved
U
Lead,Dissolved
U
Nickel,Dissolved
U
MB Qualifier MB MDL
ug/1
1.24
1.51
28.1
0.849
0.816
Laboratory Control Sample (LCS)
(LCS) R3862940-3 11/18/22 17:37
Spike Amount
LCS Result
LCS Rec.
Analyte
ug/I
ug/I
%
Chromium,Dissolved
50.0
50.0
100
Copper,Dissolved
50.0
50.6
101
Iron,Dissolved
5000
5230
105
Lead,Dissolved
50.0
48.8
97.6
Nickel,Dissolved
50.0
49.3
98.7
MBRDL
ug/1
2.00
5.00
100
2.00
2.00
Rec. Limits LCS Qualifier
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
L1554937-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1554937-03 11/18/2217:40 • (MS) R3862940-5 11/18/22 17:47 • (MSD) R3862940-6 11/18/2217:50
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
ug/I
ug/1
ug/1
ugh
%
%
Chromium,Dissolved
50.0
ND
49.8
52.9
99.7
106
Copper, Dissolved
50.0
9.39
53.9
53.7
89.1
88.6
Iron,Dissolved
5000
ND
5000
5340
100
107
Lead,Dissolved
50.0
ND
48.6
49.6
97.3
99.2
Nickel,Dissolved
50.0
14.8
62.9
64.6
96.3
99.6
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
1 75.0-125
5.89
20
1 75.0-125
0.414
20
1 75.0-125
6.54
20
1 75.0-125
1.97
20
1 75.0-125
2.56
20
6
QC
LN
ACCOUNT: PROJECT: SDG:
Frit Car Inc. 8522112 L1556126
DATE/TIME:
11/28/22 11:12
PAGE:
25 of 37

WG1959267 QUALITY CONTROL SUMMARY
Metals (ICPMS) by Method 6020B L1556126-01,02,03,04
Metkoa Blank (ivD,
(MB) R3862814-1 11/18/22 14:22
MB Result
Analyte
ug/I
Chromium
U
Copper
U
Iron
U
Lead
U
Nickel
U
MB Qualifier MB MDL
ug/I
1.24
1.51
281
0.849
0,816
Laboratory Control Sample (LCS)
(LCS) R3862814-2 11/18/22 14:26
MB RDL
ug/I
2.00
500
100
2.00
2.00
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
ug/I
ug/I
Chromium
500
487
97A
80.0 120
Copper
50.0
48.4
96.8
80.0-120
Iron
5000
4880
9T7
80.0-120
Lead
50.0
46.8
93.6
80.0-120
Nickel
50.0
48.1
96.2
80.0-120
L1556122-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1556122-01 11/18/22 14:29 • (MS) R3862814-4 11/18/22 14:36 • (MSD) R3862814-5 11/18/22 14:39
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
ug/I
ug/1
ug/I
ug/I
%
%
Chromium
50.0
ND
49.7
51.0
99A
102
Copper
50.0
ND
51.4
53.2
103
106
Iron
5000
269
5190
5380
98A
102
Lead
50.0
ND
48.0
47.6
96.1
95.2
Nickel
50.0
ND
48.5
49 5
97.0
99.0
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
1 75.0-125
2.54
20
1 75.0-125
3.43
20
1 75.0-125
3.72
20
1 75.0-125
0.922
20
1 75.0-125
1.98
20
ACCOUNT:
Frit Car Inc.
PROJECT:
8522112
SDG: DATE/TIME:
L1556126 11/28/22 11:12
PAGE:
26 of 37

WG1958002 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1556126-02,03,04
Method Blank (MB)
(MB) R3862848-2 11/13/22 09:36
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
ug/I _
ug/1
ug/1
I c.
17
Acetone
Acrolein
U
U
11.3
2.54
50.0
50.0
F
Acrylonitrile
U
0.671
10.0
Benzene
U
0.0941
1.00
Bromobenzene
U
0.118
1.00
Fn
Bromodichloromethane
Bromoform
U
U
0.136
0.129
1.00
1.00
El
Bromomethane
U
0.605
5.00
n-Butylbenzene
U
0.157
1.00
sec-Butylbenzene
U
0.125
1.00
tert-Butylbenzene
U
0.127
1.00
Carbon tetrachloride
U
0.128
1.00
G
Chlorobenzene
U
0.116
1.00
Chlorodibromomethane
U
0.140
1.00
Chloroethane
U
0.192
5.00
A�
Chloroform
Chloromethane
U
U
0.111
0.960
5.00
2.50
CSC
2-Chlorotoluene
U
0.106
1.00
4-Chlorotoluene
U
0.114
1.00
1,2-Dibromo-3-Chloropropane
U
0.276
5.00
1,2-Dibromoethane
U
0.126
1.00
Dibromomethane
U
0.122
1.00
1,2-Dichlorobenzene
U
0.107
1.00
1,3-Dichlorobenzene
U
0.110
1.00
1,4-Dichlorobenzene
U
0.120
1.00
Dichlorodifluoromethane
U
0.374
5.00
1,1-Dichloroethane
U
0.100
1.00
1,2-Dichloroethane
U
0.0819
1.00
1,1-Dichloroethene
U
0.188
1.00
cis-1,2-Dichloroethene
U
0.126
1.00
trans-1,2-Dichloroethene
U
0.149
1.00
1,2-Dichloropropane
U
0.149
1.00
1,1-Dichloropropene
U
0.142
1.00
1,3-Dichloropropane
U
0.110
1.00
cis-1,3-Dichloropropene
U
0.111
1.00
trans-1,3-Dichloropropene
U
0.118
1.00
2,2-Dichloropropane
U
0.161
1.00
Di -isopropyl ether
U
0.105
1.00
Ethylbenzene
U
0.137
1.00
Hexachloro-1,3-butadiene
U
0.337
1.00
ACCOUNT:
PROJECT:
SDG: DATE/TIME: PAGE:
Frit Car Inc.
8522112
L1556126 11/28/22 11:12 27 of 37

WG1958902
QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method
8260D
L1556126-02,03,04
Method Blank (MB)
(MB) R3862848-2 11/13/22 09:36
MB Result
MB Qualifier
MB MDL
MB RDL
Analyte ug/I
ug/I
ug/I
TC
Isopropylbenzene U
0.105
1.00
p-Isopropyltoluene U
0.120
1.00
FS
2-Butanone (MEK) U
1.19
10.0
Methylene Chloride U
0.430
5.00
4-Methyl-2-pentanone (MIBK) U
0.478
10.0
[7n]
Methyl tert-butyl ether U
0.101
1.00
Naphthalene U
1.00
5.00
Sr
n-Propylbenzene U
0.0993
1.00
Styrene U
0.118
1.00
1,1,1,2-Tetrachloroethane U
0.147
1.00
�
1,1,2,2-Tetrachloroethane U
0.133
1.00
1,1,2-Trichlorotrifluoroethane U
0.180
1.00
7G1
Tetrachloroethene U
0.300
1.00
Toluene U
0.278
1.00
1,2,3-Trichlorobenzene U
0.230
1.00
AI
1,2,4-Trichlorobenzene U
0.481
1.00
1,1,1-Trich loroethane U
0.149
1.00
F
1,1,2-Trichloroethane U
0.158
1.00
Trichloroethene U
0.190
1.00
Trichlorofluoromethane U
0.160
5.00
1,2,3-Trichloropropane U
0.237
2.50
1,2,4-Trimethylbenzene U
0.322
1.00
1,2,3-Trimethylbenzene U
0.104
1.00
1,3,5-Trimethylbenzene U
0.104
1.00
Vinyl chloride U
0.234
1.00
Xylenes, Total U
0.174
3.00
(S) Toluene-d8 105
80.0-120
(S) 4-Bromolluorobenzene 98.8
77.0-126
(S)1,2-Dichloroethone-d4 109
70.0-130
Laboratory Control Sample (LCS)
(LCS) R3862848-1 11/13/22 08:52
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte ug/I
ug/I
%
%
Acetone 25.0
25.8
103
19.0-160
Acrolein 25.0
58.3
233
10.0-160 J4
Acrylonitrile 25.0
28.6
114
55.0-149
Benzene 5.00
5.15
103
70.0-123
ACCOUNT:
PROJECT: SDG: DATE/TIME:
PAGE:
Frit Car Inc.
8522112 L1556126 11/28/22 11:12
28 of 37

WG1958902 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1556126-02,03,04
Laboratory Control Sample (LCS)
FP
(LCS) R3862848-1 11/13/22 08:52
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
2
Analyte ug/1
ug/1
%
°%
TC
Bromobenzene 5.00
4.43
88 6
73.0-121
Bromodichloromethane 5.00
5.59
112
75.0-120
SS
Bromoform 5.00
5,40
108
68.0-132
Bromomethane 5.00
5.28
106
10.0-160
n-Butylbenzene 5.00
4.26
85.2
73.0-125
Cn
sec-Butylbenzene 5.00
4.49
89.8
75.0-125
tert-Butylbenzene 5.00
4.56
91.2
76.0-124
1171
Carbon tetrachloride 5.00
5.44
109
68.0-126
Chlorobenzene 5.00
5,47
109
80.0-121
Chlorodibromomethane 5.00
5.68
114
77.0-125
Chloroethane 5.00
6,18
124
47.0-150
Chloroform 5.00
5A8
110
73.0-120
G
Chloromethane 5.00
6.44
129
41.0-142
2-Chlorotoluene 5.00
4.79
95.8
76.0-123
4-Chlorotoluene 5.00
4.53
90.6
75.0-122
[A]
1,2-Dibromo-3-Chloropropane 5.00
5.49
110
58.0-134
1,2-Dibromoethane 5.00
5.30
106
80.0-122
9
SC
Dibromomethane 5.00
5.89
118
80.0-120
1,2-Dichlorobenzene 5.00
5.33
107
79.0-121
1,3-Dichlorobenzene 5.00
5,24
105
79.0-120
1,4-Dichlorobenzene 5.00
5.13
103
79.0-120
Dichlorodifluoromethane 5.00
4.64
92.8
51.0-149
1,1-Dichloroethane 5.00
5.55
111
70.0-126
1,2-Dichloroethane 5.00
5.32
106
70.0-128
1,1-Dichloroethene 5.00
5.90
118
71.0-124
cis-1,2-Dichloroethene 5.00
5.43
109
73.0-120
trans-1,2-Dichloroethene 5.00
5.36
107
73.0-120
1,2-Dichloropropane 5.00
5.40
108
77.0-125
1,1-Dichloropropene 5.00
5.05
101
74.0-126
1,3-Dichloropropane 5.00
5.24
105
80.0-120
cis-1,3-Dichloropropene 5.00
5.19
104
80.0-123
trans-1,3-Dichloropropene 5.00
4.57
91.4
78.0-124
2,2-Dichloropropane 5.00
463
92.6
58.0-130
Di -isopropyl ether 5.00
5.09
102
58.0-138
Ethylbenzene 5.00
4.94
98.8
79.0-123
Hexachloro-1,3-butadiene 5.00
5.24
105
54.0-138
Isopropylbenzene 5.00
5,30
106
76.0-127
p-Isopropyltoluene 5.00
4.23
84.6
76.0-125
2-Butanone (MEK) 25.0
25.2
101
44.0-160
Methylene Chloride 5.00
5.66
113
67.0-120
ACCOUNT:
PROJECT: SDG: DATE/TIME:
PAGE:
Frit Car Inc.
8522112 L1556126 11/28/22 11:12
29 of 37

WG1958902 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1556126-02,03,04
Laboratory Control Sample (LCS)
(LCS) R3862848-1 11/13/22 08:52
Spike Amount
LCS Result
LCS Rec.
Rec. Limits
Analyte
ug/I
ug/I
%
%
4-Methyl-2-pentanone (MIBK)
25.0
26.4
106
68.0-142
Methyl tert-butyl ether
5.00
5.36
107
68.0-125
Naphthalene
5.00
4.98
99.6
54.0-135
n-Propylbenzene
5.00
4.39
87.8
77.0-124
Styrene
5.00
5.04
101
73.0-130
1,1,1,2-Tetrachloroethane
5.00
5.65
113
75.0-125
1,1,2,2-Tetrachloroethane
5.00
4.70
94.0
65.0-130
1,1,2-Trichlorotrifluoroethane
5.00
5.57
ill
69.0-132
Tetrachloroethene
5.00
5.48
110
72.0-132
Toluene
5.00
4.92
98.4
79.0-120
1,2,3-Trichlorobenzene
5.00
5.38
108
50.0-138
1,2,4-Trichlorobenzene
5.00
4.92
98.4
57.0-137
1,1,1-Trichloroethane
5.00
5.46
109
73.0-124
1,1,2-Trichloroethane
5.00
5.26
105
80.0-120
Trichloroethene
5.00
5.99
120
78.0-124
Trichlorofluoromethane
5.00
5.72
114
59.0-147
1,2,3-Trichloropropane
5.00
5.24
105
73.0-130
1,2,4-Trimethylbenzene
5.00
4.53
90.6
76.0-121
1,2,3-Trimethylbenzene
5.00
4.94
98.8
77.0-120
1,3,5-Trimethylbenzene
5.00
4.35
87.0
76.0-122
Vinyl chloride
5.00
6.53
131
67.0-131
Xylenes, Total
15.0
15.1
101
79.0-123
(S) Toluene -dB
100
B0.0-120
(S) 4-Bromoiluorobenzene
102
T/.0-126
(S)1,2-Dichloroethone-d4
101
70.0-130
LCS Qualifier
ACCOUNT: PROJECT: SDG:
Frit Car Inc. 8522112 L1556126
DATE/TIME:
11/28/22 11:12
PAGE:
30 of 37

WG1959639 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1556126.01
Method Blank (MB)
(MB) R3862910-2 11/15/22 01:44
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
ug/I
ug/I
ug/I
Acetone
U
11.3
50.0
Acrolein
U
2.54
50.0
Acrylonitrile
U
0.671
10.0
Benzene
U
0.0941
1.00
Bromobenzene
U
0.118
1.00
Bromodichloromethane
U
0.136
1.00
Bromoform
U
0.129
1.00
Bromomethane
U
0.605
5.00
n-Butylbenzene
U
0.157
1.00
sec-Butylbenzene
U
0.125
1.00
ter[-Butylbenzene
U
0.127
1.00
Carbon tetrachloride
U
0.128
1.00
Chlorobenzene
U
0.116
1.00
Chlorodibromomethane
U
0.140
1.00
Chloroethane
U
0.192
5.00
Chloroform
U
0.111
5.00
Chloromethane
U
0.960
2.50
2-Chlorotoluene
U
0.106
1.00
4-Chlorotoluene
U
0.114
1.00
1,2-Dibromo-3-Chloropropane
U
0.276
5.00
1,2-Dibromoethane
U
0.126
1.00
Dibromomethane
U
0.122
1.00
1,2-Dichlorobenzene
U
0.107
1.00
1,3-Dichlorobenzene
U
0.110
1.00
1,4-Dichlorobenzene
U
0.120
1.00
Dichlorodifluoromethane
U
0.374
5.00
1,1-Dichloroethane
U
0.100
1.00
1,2-Dichloroethane
U
0.0819
1.00
1,1-Dichloroethene
U
0.188
1.00
cis-1,2-Dichloroethene
U
0.126
1.00
trans-1,2-Dichloroethene
U
0.149
1.00
1,2-Dichloropropane
U
0.149
1.00
1,1-Dichloropropene
U
0.142
1.00
1,3-Dichloropropane
U
0.110
1.00
cis-1,3-Dichloropro pene
U
0.111
1.00
trans-1,3-Dichloropropene
U
0.118
1.00
2,2-Dichloropropane
U
0.161
1.00
Di -isopropyl ether
U
0.105
1.00
Ethylbenzene
U
0.137
1.00
Hexachloro-1,3-butadiene
U
0.337
1.00
ACCOUNT: PROJECT: SDG:
Frit Car Inc. 8522112 L1556126
DATE/TIME:
11/28/22 11:12
PAGE:
31 of 37

WG1959639 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1556126-01
Method Blank j v �-';
(MB) R3862910-2 11/15/22 01:44
Cp
MB Result
Analyte ug/I
.._,_.� ---_ .__-_..__
MB Qualifier
MB MDL
ug/I
MB RDL
ug/I
TC
Isopropylbenzene U
0.105
1.00
p-Isopropyltoluene U
0.120
1.00
2-Butanone (MEK) U
1.19
10.0
FS
Methylene Chloride U
4-Methyl-2-pentanone (MIBK) U
0.430
0.478
5.00
10.0
FCn]
Methyl tert-butyl ether U
0.101
1.00
Naphthalene U
1.00
5.00
n-Propylbenzene U
0.0993
1.00
Sr
Styrene U
1,1,1,2-Tetrachloroethane U
0.118
0.147
1.00
1.00
1,1,2,2-Tetrachloroethane U
0.133
1.00
1,1,2-Trichlorotrifluoroethane U
0.180
1.00
zGl
Tetra chloroethene U
0.300
1.00
Toluene U
1,2,3-Trichlorobenzene U
0.278
0.230
1.00
1.00
AI
1,2,4-Trichlorobenzene U
0.481
1.00
1,1,1-Trichloroethane U
0.149
1.00
1,1,2-Trichloroethane U
0.158
1.00
FC
Trichloroethene U
0.190
1.00
Trichlorofluoromethane U
0.160
5.00
1,2,3-Trichloropropane U
0.237
2.50
1,2,4-Trimethylbenzene U
0.322
1.00
1,2,3-Trimethylbenzene U
0.104
1.00
1,3,5-Trimethylbenzene U
0.104
1.00
Vinyl chloride U
0.234
1.00
Xylenes, Total U
0,174
3.00
(S) Toluene-d8 104
80.0-120
(S) 4-Bromofluorobenzene 99.0
77.0-126
(S) t2-Dichloroethone-d4 101
70.0-130
Laboratory Control Sample (LCS)
(LCS) R3862910-1 11/15/22 01:05
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Oualifier
Analyte ug/I
ug/I
%
%
Acetone 25.0
23.4
93.6
19.0-160
Acrolein 25.0
24.4
97.6
10.0-160
Acrylonitrile 25.0
23.8
95.2
55.0-149
Benzene 5.00
4.96
99.2
70.0-123
ACCOUNT:
PROJECT: SDG: DATE/TIME:
PAGE:
Frit Car Inc.
8522112 L1556126 11/28/22 11:12
32 of 37

WG1959639 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1556126-01
I_db(-)rllloly C CIIIIUI ScilHpil2
(LCS) R3862910-1 11/15/22 01:05
Spike Amount
LCS Result
LCS Rec.
Rec. Limits
Analyte
ug/I
ug/I
Bromobenzene
5.00
5.03
101
73.0-121
Bromodichloromethane
5.00
4.33
86.6
75.0-120
Bromoform
5.00
4.47
89A
68.0-132
Bromomethane
5.00
6.05
121
10.0-160
n-Butylbenzene
5.00
4.84
96.8
73.0-125
sec -Butyl benzene
5.00
4.96
99.2
75.0-125
tert-Butylbenzene
5.00
5.03
101
76.0-124
Carbon tetrachloride
5.00
5.03
101
68.0-126
Chlorobenzene
5.00
4.79
95.8
80.0-121
Chlorodibromomethane
5.00
4.72
94.4
77.0-125
Chloroethane
5.00
4.91
98.2
47.0-150
Chloroform
5.00
4.48
89.6
73.0-120
Chloromethane
5.00
5.31
106
41.0-142
2-Chlorotoluene
5.00
5.10
102
76.0-123
4-Chlorotoluene
5.00
4.86
97.2
75.0-122
1,2-Dibromo-3-Chloropropane
5.00
4.72
94.4
58.0-134
1,2-Dibromoethane
5.00
4.80
96.0
80.0-122
Dibromomethane
5.00
4.70
94.0
80.0-120
1,2-Dichlorobenzene
5.00
4.98
99.6
79.0-121
1,3-Dichlorobenzene
5.00
5.10
102
79.0-120
1,4-Dichlorobenzene
5.00
5.08
102
79.0-120
Dichlorodifluoromethane
5.00
5.64
113
51.0-149
1,1-Dichloroethane
5.00
4.80
96.0
70.0-126
1,2-Dichloroethane
5.00
4.64
92.8
70.0-128
1,1-Dichloroethene
5.00
4.83
96.6
71.0-124
cis-1,2-Dichloroethene
5.00
4.61
92.2
73.0-120
trans-1,2-Dichloroethene
5.00
4.68
93.6
73.0-120
1,2-Dichloropropane
5.00
5.03
101
77.0-125
1,1-Dichloropropene
5.00
4.87
97.4
74.0-126
1,3-Dichloropropane
5.00
5.02
100
80.0-120
cis-1,3-Dichloropropene
5.00
4.50
90.0
80.0-123
trans-1,3-Dichloropropene
5.00
4.95
99.0
78.0-124
2,2-Dichloropropane
5.00
4.61
92.2
58.0-130
Di -isopropyl ether
5.00
5.03
101
58.0-138
Ethylbenzene
5.00
5.10
102
79.0-123
Hexachloro-1,3-butadiene
5.00
4.78
95.6
54.0-138
Isopropylbenzene
5.00
4.87
97.4
76.0-127
p-Isopropyltoluene
5.00
4.92
98.4
76.0-125
2-Butanone (MEK)
25.0
23.9
95.6
44.0-160
Methylene Chloride
5.00
4.87
97.4
67.0-120
LCS Qualifier
ACCOUNT: PROJECT: SDG:
Frit Car Inc. 8522112 L1556126
DATE/TIME:
11/28/22 11:12
PAGE:
33 of 37

WG1959639
QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D
L1556126 01
Laboratory Control Sample (LCS)
R
(LCS) R3862910-1 11/15/22 01:05
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte ug/I
ug/I
%
%
17C
4-Methyl-2-pentanone (MIBK) 25.0
25.2
101
68.0-142
Methyl tert-butyl ether 5.00
4.83
96.6
68.0-125
FS
Naphthalene 5.00
4.56
91.2
54.0-135
n-Propylbenzene 5.00
4.81
96.2
77.0-124
Styrene 5.00
4.90
SIM
73.0-130
[Cn]
1,1,1,2-Tetrachloroethane 5.00
4.50
90.0
75.0-125
1,1,2,2-Tetrachloroethane 5.00
5.18
104
65.0-130
Fr
1,1,2-Trichlorotrifluoroethane 5.00
5.07
101
69.0-132
Tetrachloroethene 5.00
5.22
104
72.0-132
Toluene 5.00
4.95
99.0
79.0-120
1,2,3-Trichlorobenzene 5.00
4.69
93.8
50.0-138
1,2,4-Trichlorobenzene 5.00
4.76
95.2
57.0-137
F
1,1,1-Trichloroethane 5.00
4.75
95.0
73.0-124
1,1,2-Trichloroethane 5.00
5.23
105
80.0-120
s
Trichloroethene 5.00
4.63
92.6
78.0-124
AI
Trichlorofluoromethane 5.00
4.89
97.8
59.0-147
1,2,3-Trichloropropane 5.00
4.94
98.8
73.0-130
FSC
1,2,4-Trimethylbenzene 5.00
5.09
102
76.0-121
1,2,3-Trimethylbenzene 5.00
4.97
99.4
77.0-120
1,3,5-Trimethylbenzene 5.00
5.01
100
76.0-122
Vinyl chloride 5.00
5.33
107
67.0-131
Xylenes, Total 15.0
14.8
98.7
79.0-123
(S) Toluene-d8
101
80.0-120
(S) 4-Bromofluorobenzene
101
77.0-126
(S)1,2-Dichloroethane-d4
98.1
70.0-130
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 8522112 L1556126 11/28/22 1112 34 of 37

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
Fp
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
z
TC
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
PS
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
rn]
RDL Reported Detection Limit.
Rec. Recovery.
RPD Relative Percent Difference.
Fr
SDG Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
El
IS) Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
A
Dilution standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
FSC
Limits for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
E The analyte concentration exceeds the upper limit of the calibration range of the instrument established by the initial
calibration (ICAL).
J The identification of the analyte is acceptable; the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high.
P1 RPD value not applicable for sample concentrations less than 5 times the reporting limit.
v The sample concentration is too high to evaluate accurate spike recoveries.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 8522112 L1556126 11/28/22 11:12 35 of 37

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P330-15-00234
EPA-Crypto
TN00003
Drinking Water ' Underground Storage Tanks ' Aquatic Toxicity ' Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Frit Car Inc. 8522112 L1556126 11/28/22 1112 36 of 37

Company Name/Address
Billing information
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Frit Car Inc.
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Accounts Payable
PO Box 1340
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2012 US Hwy 17N
Brewton, AL 36427
New Bern, NC 28560
mrtF OVAXOSL SCIENCE
MT JULIET, TN
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Email To [e-mail]
Connie Pettis
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Bottles arrive "intact: Y —N
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Condition:
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