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WQ0040918_Monitoring - 11-2022_20221222
GW-59A COMPLIANCE REPORT FORM � Permit 4VQ �l (Submit one each monitoring period with GW-59 forms:) j Enter date monitoring results were due. Will this monitoring report (GW-59 and GW-59A) YES O be submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? YES N IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES O identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Office for guidance. 4 Are any monitored constituents equal to or above the established standards? YES NO If the answer to question 4 is "NO" skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with ons ' uent(s) and concentration(s) geeding st darr/s in the sp ce provided below: MW —3 L4 �, S li C) I 11�1JJ G !-Q 6l 1 �. � 1 `41 4� /� A 3 �c(C(Nk Lk4ks Q l M 13 �1°�k N /G L / v 5 For the constituents identified in question 4 above, have stand been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is 'NO", skip to section 8. If the answer to question 5 is "YES". list in the space provided below, each well with constituents) exceeding sta da s, centration(s) reported, and sample collection dat for each occurren (for the last two years). rn�-� (coolr1- rl - ass 'A r-t aa. Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO". monitoring wells maybe improperly ' located; contact the Regional Office. _. . 7 Is the permittee implementing previously approved actions required by the Division involvin tktis � S NO groundwater quality problem? If the answer to question 7 is "YES", describe those actions in the space provided below. �t If the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subiect the permittee to a Notice of Violation fines and/or Denalties. c O �CeV �ou5 _ c& occ g The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. l hest adage the above kiliornm6m INW evaded and the sSt intilils report (Compilliar sco GW26Wes rue a ` the bes of my _. 2023 Signature of Pe ittee (or Authorized Agent) Date 74� GW-59A 12/8/2003 �Y, .) --m� - 1+ -�\\ 's-, a (, , �JS� 1�7e ca� �22 � rs�3 Ul k�-3-a l s, r) r1 ak 3 ,S `l,S zL SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATInN n . Please Facility Name: Permit Name (if different): Facility Address: l- Contact Person: rc� Well Location/Site Name: Print Clearly or Type County m— 'ipi Telephone#�N" No. of wells to be sampled: u VIV �uw nrrvrtmn i wt� \ t WELL ID NUMBER (from Permit): Well Depth: �� ft. Depth to Water Level 82546: _ft. below measuring point Measuring Point is ft. above land surface Volume of water pumped/bailed before sampling: _*3 CX f gallons Samples for metals were collected unfiltered: © YES NO and field acidified: ❑■ YES ❑ NO Date sample analyzed: `\` -s � A —y' 311-1 )It 1 t 11-11 PARAMETERS NOTE: Valdes sh uld reflect Ism COD 00335 mg/L Coliform: MF Fecal 31616 Co /100mL Coliform: MF Total 31504 /100mL (Note Use MPN method for highly turbid samples) )issolved Solids:Total 70300 tng/L pH (Lab) 00403 units TOC oo68o j mg/L Chloride 00940 - mg/L Arsenic 01002 ug/L Grease and Oils 00552 mg/L Phenol 32730 ug/L Sulfate 00945 mg/L specific Conductance 00095 µMhos Total Ammonia 00610 (�j mg/L (Ammonia Nitrogen, NH3 as N, Ammonia Nitrogen. Total) TKN as N 00625 mg/L DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATEF INFORMATION PROCESSING UNIT 1517 MAIL SERVICE CENTER, RALEIGH, NC 27609.1617 PERMIT Nurnber: t E;xpiration Date Non -Discharge UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED 91-tagoon ❑ Remediation: infiltration Gallery "pray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: Date sample collected:' Well Diameter: in. Screened Interval: ft. to ft. Relative M.P. Elevation: ft. FIELD ANALYSES: pH 0040011114units Spec. Cond. 00094 Odor 00085 11)b Appearance r r - s-t- laboratory Name and colloidal concentrations. Nitrite (NO2) as N 00615 mg/L Pb - Lead olo51 Nitrate (NO.) as N 00620 _LL mg/L Zn - Zinc 01092 Phosphorus: Total as P 00665 mg/L Temp. 000loM i S °C µMhos Certification No. (A ug/L mg/L WELL DRY at time of sampling, check here: ❑ Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Al - Aluminum oilo5 mg/L Ba - Barium 01007 ug/L Ca - Calcium 00916 mg/L Cd - Cadmium 01027 ug/L Chromium: Total 01034 ug/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Hg - Mercury 71900 ug/L Lab Report Attached? Ili Yes (1) No (0) K - Potassium 00937 mg/L p❑ VOC 7873 method # 3 f j) ho 30"[ Mg - Magnesium 00927 mg/L method # Mn - Manganese oloss ug/L Ni - Nickel 01067 ug/L method # method # For Remediation Systems Only (Attach Lab Reports): _ Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: _ t Permit Name (if different): Facility Address: L- Contact Person: 1 Well Location/Site Name: M' Please Print Clearly of A_ I ': •y _ i A!c . Mlt,�;'3 county Telephone#: �0 13 _j iNo. of wells to be sampled: TMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1b17 PERMIT Nwnber i txpiration Date Non -Discharge UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED [�C�a�g.00n El Remediation: Infiltration Gallery t, s ray Field ❑ Remediation ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: ..... -' WELL ID NUMBER (from Permit): 1y� a Well Depth: c; ft. Depth to Water Level 82546:SI,5 ft. below measuring point Measuring Point is ft. above land surfac f - Volume of water pumped/bailed before sampling: -3 C Samples for metals were collected unfiltered: K YES ` ^� Date sample collected: t' 3 - �{ Well Diameter: in. Screened Interval: ft, to ft. Relative M.P. Elevation: ft. � gallons NO and field acidified: ❑■ YES ❑ NO FIELD ANALYSES: a pH o0aoo'�Lrunits Temp. 000lo: a / °C Spec. Cond. 00094 µMhos Odor 0ooa5 Q Appearance If WELL WAS DRY at time of sampling, check here:❑ LABORATORY INFORMATION Date sample analyzed: -3 - I'� t�" �� 1 1' �'o�dJ aboratory Name (\U `_ rO4Z�Nf_ Y� Certification PARAMETERS NOTE: Values !9hould reflect dis olved and colloidal concentrations. No. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 �3 �b�/100mL Nitrate (NO3) as N 00620 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 V_ mg/L Al - Alurninum olim mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 1 7S- mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L. ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L s Lab Report Attached? L!� Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # S'o30� Total Ammonia 00610 C. mg/L (Ammonia Nitrogen, NH3 Mg - Magnesium 00927 mg/L method # as N, Ammonia Nitrogen.Total) Mn - Manganese o1o55 u /L g ,method # TKN as N 00625 mg/L Ni - Nickel 01067 uglL method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs mg/L Effluent Total VOCs: mg/L VOC Removal% and Title - Please print or type GW-59 Rev.06-07-2018 Agent) (natei GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: Permit Name (if different): `1r Facility Address: C \ act Person: Cc�\► t\ Location/Site Name:. 10 Z SUBMIT FORM ON YELLOW PAPER ONLY • DEPARTMENT OF ENVIRONMENTAL QUALITY • DIV. OF WATERRESOU • • • • INFORMATION PROCESSING UNIT 1017 MAIL SERVICE CENTER, RALEIGH, NC,ti7H99.1617 Print Clearly lor,Type PERMIT Number:: _ L:.xpnation Date: J"C �iA(f Non -Discharge � i � �' UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED County q b'Cagoon ❑ Remediation: Infiltration Gallery pray Field ❑ Remediation: Telephone#: �G ` 3 ❑ Rotary Distributor ❑ Land Application of Sludge No. of wells to be sampled: LV ❑ Water Source Heat Pump ❑ Other: . .... W_nn. I IWIM WELL ID NUMBER (from Permit): LSV Date sample collected: '� FIELD ANALYSES: If WELL WAS Well Depth: ft. Well Diameter: =L. in. ` pH 0oa00 1 •_W) units Temp. 000io: t °C DRY at Depth to Water Level 82546:\C)_ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. 00094 µMhos time of Measuring Point is ft. above land surface •p, � Relative M.P. Elevation: ft. Odor 000s5 -"(V sampling, check Volume of water pumped/bailed before sampling: CtC gallons Samples Appearance G t,u (\�� here:❑ for metals were collected unfiltered: © YES ❑ NO and field acidified: ❑■ YES ❑ NO Date sample analyzed: 1ES , 1, - 1 ,`t `l I t`-IS-' r' 4aboratory Name �(�� (a e � Im PARAMETERS NOTE: Valdes sh uld reflect dfssolved and colloidal concentrations. tl(\ Certification No. COD 00335 mg/L Nitrite (NOZ) as N 00615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 C_r� /100mL Nitrate (No,) as N oos20 , mg/L Zn -Zinc oios2 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 , mg/L (Note Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 mg/L At - Aluminum oiio5 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC oosso mg/L Ca - Calcium 00916 mg/L Chloride oosso mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. TTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? Yes (1) ❑ No (0) Specific Conductance 000s5 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia oosso mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH3 as N, AmNitrogen, Total) Mn - Manganese 01055 9monia u /L ,method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs mg/L Effluent Total VOCs mg/L VOC Removal% SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM ity Name: _i lit Name (if different):' ity Add ess: (t0 ` Cf` 1 iCav) act Person: Location/Site Name: ( Pi.-, C--, -r or Telephone#q10 _a (3 No. of wells to be sampled: DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER INFORMATION PROCESSING UNIT 1417 MAIL SERVICE CENTER, RALEIGH, NC 27609.1617 PERMIT Number;, r' xpration Date Non -Discharge / UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ti-goon ❑ Remediation: Infiltration Gallery ray Field ❑ Remediation. ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: WELL ID NUMBER (from Permit): �� Date sample collected:] 1 Well Depth: 1 j ft. Well Diameter: � in. Depth to Water Level 82546: Q, ft. below measuring point Screened Interval: ft. to ft. Measuring Point is ft. above land surface Relative M.P. Elevation: ft Volume of water pumped/bailed before sampling: __JQ� ,gallons FIELD ANALYSES: pH ooaoo �u f a units Spec. Cond. 000sa. Odor 000m Appearance Samples for metals were collected unfiltered: © YES ❑ NO and field acidified K YES ❑ NO Date sample analyzed: ,--S,11—It Ik) ti111 a 11—IU PARAMETERS NOTE: Values s ould teflect dissol c COD 00335 mg/L Coliform: MF Fecal 31616 /100mL Coliform: MF Total 31504 /100mL (Note Use MPN method for highly turbid samples) )issolved Solids:Total 70300 1a,) mg/L pH (Lab) 00403 units TOC oosao Q _ mg/L Chloride aosao a mg/L Arsenic 01002 ug/L Grease and Oils 00552 mg/L Phenol 32730 ug/L Sulfate 00945 mg/L pecific Conductance 000m µMhos Total Ammonia 00610 mg/L (Ammonia Nitrogen. NH3 as N, Ammonia Nitrogen, Total) TKN as N 00625 mg/L For Remediation Systems Only (Attach Lab Reports) Temp. 000lo: I I I °C uMhos Laboratory Name: ��U i I^0(Y�Q.{.{� Certification No. d and colloidal concentrations. Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L Nitrate (NO.) as N 00620—� mg/L Zn - Zinc 01092 mg/L Phosphorus: Total as P 00665 mg/L Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Al -Aluminum o11o5 mg/L Ba - Barium 01007 ug/L Ca - Calcium 00916 mg/L Cd - Cadmium 01027 ug/L Chromium: Total 01034 ug/L If DRY at time of sampling, here:❑ Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Fe - Iron 01045 ug/L (Specify test and method #.i4TTACH LAB REPORT.) Hg - Mercury 71900 ug/L Lab Report Attached? •Ll~1/ Yes (1) ❑N�o'(0e),, K - Potassium 00937 mg/L VOC 7873 method # Mg - Magnesium 00927 mg/L method # Mn - Manganese o1o55 ug/L method # Ni - Nickel 01067 ug/L method # Influent Total VOCs mg/L Effluent Total VOCs: VOC Removal% [enviroehe]m ANALYTICAL & CONSULTING CHEMISTS Smithfield Hog Productions - Warsaw Post Office Box 856 Warsaw NC 28398 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 ` 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Nov 16, 2022 Customer PO #: Customer ID: 08110011 Report #: 2022-22012 Project ID: AG Protein Lab ID Sample ID: Collect Date/Time Matrix Sampled by 22-53960 Site: MW-1 11/3/2022 12:25 PM Water JCB/Envirochem Test Method Results Date Analyzed Color Color Brown/Tan 11/03/2022 Depth to water, ft. Depth to water, Ft. 13.0 feet 11/03/2022 Ammonia Nitrogen EPA350.1, Rev.2.0, 1993 < 0.2mg/L 11/11/2022 Gallons bailed before sampling Gallons Bailed before sampling 5(dry) gallons 11/03/2022 Odor Qualitative None 11/03/2022 Total Dissolved Solids (TDS) SM 2540 C-2015 59 mg/L 11 /04/2022 Temperature SM 2550 B-2010 21.5 C 11/03/2022 pH SM 4500 H B-2011 4.6 units 11/03/2022 Total Phosphorus SM 4500 P (F-H)-2011 12.8 mg/L 11/11/2022 Total Organic Carbon (TOC) SM 5310 B-2014 2.1 mg/L 11/07/2022 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 11/03/2022 Chloride SM4500 Cl E-2011 < 5 mg/L 11/04/2022 1, 1, 1,2-Tetrachloroethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1, 1, 1 -Trichloroethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,1,2,2-Tetrachloroethane SW 846 Method 8260D15030B <0.5 pg/L 11/09/2022 1,1,2-Trichloroethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,1-Dichloroethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,1-Dichloroethene SW 846 Method 8260D15030B <0.5 pg/L 11/09/2022 1,1-Dichloropropene SW B46 Method 826OD15030B <0.5 pg/L 11/09/2022 1,2,3-Trichlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,2,3-Trichloropropane SW 646 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,2,4-Trichlorobenzene SW 846 Method 6260D/5030B <0.5 pg/L 11/09/2022 1,2,4-Trimethylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,2-Dibromo-3-Chloropropane SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2022 1,2-Dibromoethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,2-Dichlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Report #:: 2022-22012 Page 1 of 12 Environmental Chemists, Inc. envirochem J 6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ` 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax Hsu 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Smithfield Hog Productions -Warsaw Date of Report: Nov 16, 2022 Post Office Box 856 Customer PO #: Warsaw NC 28398 Customer ID: 08110011 Attention: Report #: 2022-22012 Project ID: AG Protein 1,2-Dichloroethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,2-Dichloropropane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,3,5-Trimethylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,3-Dichlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,3-Dichloropropane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,4-Dichlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 2,2-Dichloropropane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 2-Chlorotoluene SW 846 Method 8260D15030B <0.5 pg/L 11/09/2022 4-Chlorotoluene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Benzene SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2022 Bromobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Bromochloromethane SW 846 Method 826013/503013 <0.5 pg/L 11/09/2022 Bromodichloromethane SW 846 Method 8260D15030B <0.5 pg/L 11/09/2022 Bromoform SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Bromomethane SW 846 Method 8260D15030B <0.5 pg/L 11/09/2022 Carbon tetrachloride SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Chlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Chloroethane SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2022 Chloroform SW 846 Method 8260D15030B <0.5 pg/L 11/09/2022 Chloromethane SW 846 Method 8260D150308 <0.5 pg/L 11/09/2022 cis-1,2-Dichloroethene SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2022 cis- 1,3-Dichloropropene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Dibromochloromethane SW 846 Method 8260D15030B <0.5 pg/L 11/09/2022 Dibromomethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Dichlorodifluoromethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Ethylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Hexachlorobutadiene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Isopropyl benzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 M+P Xylene SW 846 Method 8260D/50308 <1.0 pg/L 11/09/2022 Methylene chloride SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Report #. 2022-22012 Page 2 of 12 NEe7n virochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 " 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 ` 910.347.5843 Lab/Fax info@environmentalchemists.com Smithfield Hog Productions - Warsaw Date of Report: Nov 16, 2022 Post Office Box 856 Customer PO #: Warsaw NC 28398 Customer ID: 08110011 Attention: Report #: 2022-22012 Project ID: AG Protein Naphthalene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 n-Butylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 n-Propylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 ortho-Xylene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 p-Isopropyltoluene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 sec -Butyl benzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Styrene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 te rt-Butyl benzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Tetrachloroethene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Toluene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Trans- 1,2-Dichloroethene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Trans-1,3-dichloropropene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Trichloroethene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Trichlorofluoromethane SW 846 Method 826013/503013 <0.5 pg/L 11/09/2022 Vinyl chloride SW 846 Method 826013/50308 <0.5 pg/L 11/09/2022 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 0.11 mg/L 11/03/2022 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev, 2.0, 1993 1.56 mg/L 11/07/2022 Nitrate Nitrogen Subtraction Method 1.45 mg/L 11/15/2022 Report #!. 2022-22012 Page 3 of 12 r7_7441 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Smithfield Hog Productions -Warsaw Post Office Box 856 Warsaw NC 28398 Attention: Date of Report: Nov 16, 2022 Customer PO #: Customer ID: 08110011 Report #: 2022-22012 Project ID: AG Protein Lab ID Sample ID: Collect Date/Time Matrix Sampled by 22-53964 Site: MW-2 11/3/2022 12:45 PM Water JCB/Envirochem Test Method Results Date Analyzed Color Color Wh ite/Turb 11/03/2022 Depth to water, ft. Depth to water, Ft. 15.5 feet 11/03/2022 Ammonia Nitrogen EPA 350.1, Rev. 2.0, 1993 < 0.2 mg/L 11/11/2022 Gallons bailed before sampling Gallons Bailed before sampling 3(dry) gallons 11/03/2022 Odor Qualitative None 11/03/2022 Total Dissolved Solids (TDS) SM 2540 C-2015 143 mg/L 11/04/2022 Temperature SM 2550 B-2010 21.0 C 11/03/2022 pH SM 4500 H B-2011 3.96est. units 11/03/2022 Total Phosphorus SM 4500 P (F-H)-2011 0.29 mg/L 11111 /2022 Total Organic Carbon (TOC) SM 5310 B-2014 1.5 mg/L 11/07/2022 Fecal Coliform SM 9222 D-2015 MF 3 Colonies/100mL 11/03/2022 Chloride SM4500 Cl E-2011 9 mg/L 11/04/2022 1, 1, 1,2-Tetrachloroethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1, 1, 1 -Trichloroethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,1,2,2-Tetrachloroethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,1,2-Trichloroethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1, 1 -Dichloroethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,1-Dichloroethene SW 846 Method 826OD15030B <0.5 pg/L 11/09/2022 1,1-Dichloropropene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,2,3-Trichlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,2,3-Trichloropropane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,2,4-Trichlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,2,4-Trimethylbenzene SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2022 1,2-Dibromo-3-Chloropropane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,2-Dibromoethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,2-Dichlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Report #:: 2022-22012 Page 4 of 12 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Smithfield Hog Productions - Warsaw Date of Report: Nov 16, 2022 Post Office Box 856 Customer PO #: Warsaw NC 28398 Customer ID: 08110011 Attention: Report #: 2022-22012 Project ID: AG Protein 1,2-Dichloroethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,2-Dichloropropane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,3,5-Trimethylbenzene SW 846 Method 826OD15030B <0.5 pg/L 11/09/2022 1,3-Dichlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,3-Dichloropropane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,4-Dichlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 2,2-Dichloropropane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 2-Chlorotoluene SW 846 Method 826OD15030B <0.5 pg/L 11/09/2022 4-Chlorotoluene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Benzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Bromobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Bromochloromethane SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2022 Bromodichloromethane SW 846 Method 8260D150308 <0.5 pg/L 11/09/2022 Bromoform SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Bromomethane SW 646 Method 8260D/5030B <0.5 pg/L 11/09/2022 Carbon tetrachloride SW 846 Method 8260D/5030B <0.5 pg/L 11 /09/2022 Chlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Chloroethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Chloroform SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Chloromethane SW 646 Method 8260D150308 <0.5 pg/L 11/09/2022 cis- 1,2-Dichloroethene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 cis- 1,3-Dichloropropene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Dibromochloromethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Dibromomethane SW 846 Method 826oD/5030B <0.5 pg/L 11/09/2022 Dichlorodifluoromethane SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2022 Ethylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Hexachlorobutadiene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Isopropylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 M+P Xylene SW 846 Method 826oD/5030B <1.0 pg/L 11/09/2022 Methylene chloride SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Report #:: 2022-22012 Page 5 of 12 envirochem •'sM ANALYTICAL & CONSULTING CHEMISTS Smithfield Hog Productions -Warsaw Post Office Box 856 Warsaw NC 28398 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab f 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Nov 16, 2022 Customer PO #: Customer ID: 08110011 Report #: 2022-22012 Project ID: AG Protein Naphthalene SW 846 Method B260D/5030B <0.5 pg/L 11/09/2022 n-Butylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 n-Propylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 ortho-Xylene SW B46 Method 8260D/5030B <0.5 pg/L 11/09/2022 p-Isopropyltoluene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 sec-Butylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Styrene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 te rt-B utyl benzene SW 846 Method 826013/50306 <0.5 pg/L 11/09/2022 Tetrachloroethene SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2022 Toluene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Trans-1,2-Dichloroethene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Trans- 1,3-dichloropropene SW 846 Method 0260D/50308 <0.5 pg/L 11/09/2022 Trichloroethene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Trichlorofluoromethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Vinyl chloride SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 3532, Rev. 2.0, 1993 0.05 mg/L 11/03/2022 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0, 1993 16.7 mg/L 11/07/2022 Nitrate Nitrogen Subtraction Method 16.6 mg/L 11/15/2022 Report #: 2022-22012 Page 6 of 12 :envirochem ANALYTICAL & CONSULTING CHEMISTS Smithfield Hog Productions - Warsaw Post Office Box 856 Warsaw NC 28398 Attention: Environmental Chemists, Inc® 6602 Windmill Way, Wilmington, NC 28405 s 910.392.0223 Lab ' 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 ° 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Nov 16, 2022 Customer PO #: Customer ID: 08110011 Report #: 2022-22012 Project ID: AG Protein Lab ID Sample ID: Collect Date/Time Matrix Sampled by 22-53965 Site: MW-3 11/3/2022 1:00 PM Water JCB/Envirochem Test Method Results Date Analyzed Color Color Brown/Tan 11/03/2022 Depth to water, ft. Depth to Water, Ft 10.0 feet 11/03/2022 Ammonia Nitrogen EPA 350 1, Rev. 2 0, 1993 < 0.2 mg/L 11/11/2022 Gallons bailed before sampling Gallons Bailed before sampling 4(dry) gallons 11/03/2022 Odor Qualitative None 11/03/2022 Total Dissolved Solids (TDS) SM 2540 c-2015 179 mg/L 11 /04/2022 Temperature SM 2550 B-2010 21.9 C 11/03/2022 pH SM 4500 H B-2011 4.5 units 11/03/2022 Total Phosphorus SM4500 P (F-H)-2011 1.88 mg/L 11/11/2022 Total Organic Carbon (TOC) SM 5310 B-2014 17.3 mg/L 11/07/2022 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 11/03/2022 Chloride SM4500 cl E-2011 7 mg/L 11/04/2022 1, 1, 1,2-Tetrachloroethane SW 846 Method 826OD15030B <0.5 pg/L 11/09/2022 1, 1, 1 -Trichloroethane SW 646 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,1,2,2-Tetrachloroethane SW 846 Method 8260015030B <0.5 pg/L 11/09/2022 1,1,2-Trichloroethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1, 1 -Dichloroethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,1-Dichloroethene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,1-Dichloropropene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,2,3-Trichlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,2,3-Trichloropropane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,2,4-Trichlorobenzene SW 846 Method 826OD15030B <0.5 pg/L 11/09/2022 1,2,4-Trimethylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,2-Dibromo-3-Chloropropane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,2-Dibromoethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,2-Dichlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Report p:: 2022-22012 Page 7 of 12 �sM ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 ! 910.392.0223 Lab ` 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Smithfield Hog Productions - Warsaw Date of Report: Nov 16, 2022 Post Office Box 856 Customer PO #: Warsaw NC 28398 Customer ID: 08110011 Attention: Report #: 2022-22012 Project ID: AG Protein 1,2-Dichloroethane SW 646 Method 82600/5030B <0.5 pg/L 11/09/2022 1, 2-Dichloropropane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,3,5-Trimethylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1, 3-Dichlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1, 3-Dichloropropane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,4-Dichlorobenzene SW 846 Method 6260D/5030B <0.5 pg/L 11/09/2022 2,2-Dichloropropane SW 846 Method 8260D15030B <0.5 pg/L 11/09/2022 2-Chlorotoluene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 4-Chlorotoluene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Benzene SW 846 Method 826OD15030B <0.5 pg/L 11/09/2022 Bromobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Bromochloromethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Bromodichloromethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Bromoform SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2022 Bromomethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Carbon tetrachloride SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2022 Chlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11 /09/2022 Chloroethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Chloroform SW 846 Method 8260D15030B <0.5 pg/L 11/09/2022 Chloromethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 cis- 1,2-Dichloroethene SW B46 Method 82BOD/5030B <0.5 pg/L 11/09/2022 cis-1,3-Dichloropropene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Dibromochloromethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Dibromomethane SW 846 Method 6260D/5030B <0.5 pg/L 11/09/2022 Dichlorodifluoromethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Ethylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Hexachlorobutadiene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1sopropylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 M+P Xylene SW 846 Method 8260D15030B <1.0 pg/L 11/09/2022 Methylene chloride SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Report # 2022-22012 Page 8 of 12 ffe7nviroe7heml ANALYTICAL & CONSULTING CHEMISTS Smithfield Hog Productions - Warsaw Post Office Box 856 Warsaw NC 28398 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 ° 910.392.0223 Lab ° 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Nov 16, 2022 Customer PO #: Customer ID: 08110011 Report #: 2022-22012 Project ID: AG Protein Naphthalene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 n-Butylbenzene SW 846 Method 826013/503013 <0.5 pg/L 11/09/2022 n-Propylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 ortho-Xylene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 p-Isopropyltoluene SW 846 Method 626OD15030B <0.5 pg/L 11/09/2022 sec -Butyl benzene SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2022 Styrene SW 846 Method 8260D150306 <0.5 pg/L 11/09/2022 tert-Butylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Tetrachloroethene SW 846 Method 826OD15030B <0.5 pg/L 11/09/2022 Toluene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Trans-1 ,2-Dichloroethene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Trans- 1,3-dichloropropene SW 846 Method 8260D15030B <0.5 pg/L 11/09/2022 Trichloroethene SW 846 Method 826013/503013 <0.5 pg/L 11/09/2022 Trichlorofluoromethane SW 846 Method 6260D/5030B <0.5 pg/L 11/09/2022 Vinyl chloride SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 0.10 mg/L 11 /03/2022 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0, 1993 13.0 mg/L 11/07/2022 Nitrate Nitrogen Subtraction Method 12.9 mg/L 11 /15/2022 Report #.: 2022-22012 Page 9 of 12 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ` 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 ` 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Smithfield Hog Productions - Warsaw Post Office Box 856 Warsaw NC 28398 Attention: Date of Report: Nov 16, 2022 Customer PO #: Customer ID: 08110011 Report #: 2022-22012 Project ID: AG Protein Lab ID Sample ID: Collect Date/Time Matrix Sampled by 22-53966 Site: MW-4 11/3/2022 1:20 PM Water JCB/Envirochem Test Method Results Date Analyzed Color Color Tan 11/03/2022 Depth to water, ft. Depth to Water, Ft. 2.8 feet 11/03/2022 Ammonia Nitrogen EPA 350.1, Rev. 2.0, 1993 < 0.2 mg/L 11/11/2022 Gallons bailed before sampling Gallons Bailed before sampling 10 gallons 11/03/2022 Odor Qualitative None 11/03/2022 Total Dissolved Solids (TDS) SM 2540 C-2015 127 mg/L 11/04/2022 Temperature SM 2550 B-2010 19.2 C 11/03/2022 pH SM 4500 H B-2011 5.2 units 11/03/2022 Total Phosphorus SM 4500 P (F-H)-2011 1.40 mg/L 11 /11/2022 Total Organic Carbon (TOC) SM 5310 B-2014 0.7 mg/L 11/07/2022 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 11/03/2022 Chloride SM4500 Cl E-2011 21 mg/L 11/04/2022 1, 1, 1,2-Tetrachloroethane SW B46 Method 82600/5030B <0.5 pg/L 11/09/2022 1, 1, 1 -Trichloroethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,1,2,2-Tetrachloroethane SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2022 1,1,2-Trichloroethane SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2022 1,1-Dichioroethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,1-Dichloroethene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1, 1 -Dichloropropene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1, 2, 3-Trichlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,2,3-Trichloropropane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,2,4-Trichlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,2,4-Trimethylbenzene SW 846 Method 826OD/50308 <0.5 pg/L 11/09/2022 1,2-Dibromo-3-Chloropropane SW 846 Method 82BOD150308 <0.5 pg/L 11/09/2022 1,2-Dibromoethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 1,2-Dichlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Report #, 2022.22012 Page 10 of 12 11 envirochem ANALYTICAL & CONSULTING CHEMISTS Smithfield Hog Productions -Warsaw Post Office Box 856 Warsaw NC 28398 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ' 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax info(a environmentalchemists.com Date of Report: Nov 16, 2022 Customer PO #: Customer ID: 08110011 Report #: 2022-22012 Project ID: AG Protein 1,2-Dichloroethane SW 846 Method 826013/50308 <0.5 pg/L 11/09/2022 1,2-Dichloropropane SW 846 Method 8260D/5030B <0.5 Ng/L 11/09/2022 1,3,5-Trimethylbenzene SW 846 Method 8260D15030B <0.5 pg/L 11/09/2022 1,3-Dichlorobenzene SW 846 Method 826OD/5030B <0.5 pg/L 11/09/2022 1, 3-Dichloropropane SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2022 1,4-Dichlorobenzene SW 846 Method 826OD/5030B <0.5 pg/L 11/09/2022 2,2-Dichloropropane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 2-Chlorotoluene SW 846 Method 826OD/5030B <0.5 pg/L 11/09/2022 4-Chlorotoluene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Benzene SW 846 Method 826OD/5030B <0.5 pg/L 11/09/2022 Bromobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Bromochloromethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Bromodichloromethane SW 846 Method 826OD/5030B <0.5 pg/L 11/09/2022 Bromoform SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Bromomethane SW 846 Method 828OD/5030B <0.5 pg/L 11/09/2022 Carbon tetrachloride SW 846 Method 8260D/5030B <0.5 Ng/L 11/09/2022 Chlorobenzene SW 846 Method 6260D/5030B <0.5 pg/L 11/09/2022 Chloroethane SW 846 Method 826OD/5030B <0.5 pg/L 11/09/2022 Chloroform SW 846 Method 826OW5030B <0.5 dig/L 11/09/2022 Chloromethane SW 846 Method 8260D15030B <0.5 pg/L 11/09/2022 cis-1,2-Dichloroethene SW 846 Method 826OD/5030B <0.5 pg/L 11/09/2022 cis- 1,3-Dichloropropene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Dibromochloromethane SW 846 Method 826OD/50308 <0.5 pg/L 11/09/2022 Dibromomethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Dichlorodifluoromethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Ethylbenzene SW 846 Method 826OD/5030B <0.5 pg/L 11/09/2022 Hexachlorobutadiene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Isopropylbenzene SW 846 Method 826OD/5030B <0.5 pg/L 11/09/2022 M+P Xylene SW 846 Method 626OD/5030B <1.0 pg/L 11/09/2022 Methylene chloride SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Report # 2022-22012 Page 11 of 12 a I . r Eenv:iirroehem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax info@environmentalchemists.com Smithfield Hog Productions - Warsaw Date of Report: Nov 16, 2022 Post Office Box 856 Customer PO #: Warsaw NC 28398 Customer ID: 08110011 Attention: Report #: 2022-22012 Project ID: AG Protein Naphthalene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 n-Butylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 n-Propylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11 /09/2022 ortho-Xylene SW 846 Method 82600/5030B <0.5 pg/L 11/09/2022 p-Isopropyltoluene SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2022 sec-Butylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Styrene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 te rt-B utyl benzene SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2022 Tetrachloroethene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Toluene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2022 Trans-1,2-Dichloroethene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Trans-1,3-dichloropropene SW 846 Method 82600/50308 <0.5 pg/L 11/09/2022 Trichloroethene SW 646 Method 8260D/5030B <0.5 pg/L 11/09/2022 Trichlorofluoromethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Vinyl chloride SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2022 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 0.15 mg/L 11/03/2022 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0, 1993 0.19 mg/L 11/07/2022 Nitrate Nitrogen Subtraction Method 0.04 mg/L 11/15/2022 Comment: Reviewed by: r 1 L Report #i 2022-22012 Page 12 of 12