WQ0000672_2017 Land App_20180222

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: WQ0000672 County Robeson Year 2017
Facility Name (as shown on permit) City of Lumberton WWTP NPDES No. NCO024571
Land Application Operator Svnaero Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip PartA, and Part Band proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: 43
Total number of fields utilized for land application during the year: 21
Total amount of dry tons applied during the year for all application sites: 1.289.66
Total number of acres utilized for land application during the year: 379.8
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2017 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES _ NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1.
Only residuals approved for this permit were applied to the permitted sites.
2.
Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3.
Annual soils analysis was performed.on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4.
Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5.
All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6.
The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T . 1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
�7.
All general requirements as specified in the Land Application Permit were complied with'(applicable to 40 CFR Part 503
\ /
regulated facilities).
8.
All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part503
regulated facilities).
9.
All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water _Quality.
10.
No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11.
Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12.
No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13.
All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations."
Jireite Director of EUS Dept.---��!/�
Permittee Name and Title (type or print) Signature of Permittee Date
S 2!-1,9
Signature ofPreparer* Date Date
(if different from Permittee) (if different fr e ee an reparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

2017 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION
LUMBERTON, NC
LUMBERTON, NC WWTP AEROB. DIGESTED LIQUID,
DRY METRIC
MONTHNEAR
AMOUNT
UNIT
DRY TONS
UNIT
TONS
March 2017
2,238,200.00
G
427.47
D
387.71
May 2017
1,016,800.00
G
248.90
D
225.75
June 2017
1,109;800.00
G
271.65
D
246.39
August 2017
1,928,200:00
G
83.62
D
75.85
October 2017
427,800.00
G
57.80
'D
52.43
November 2017
1,413,600.00
G
1.91.00
D
173.23
December 2017
68,200.00
G
9.22
D
8.36
YEARLY TOTAL
8,202,600.00
G
1,289.66
D
1,169.72
2/8/2018

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0000672 Laboratory
Facility Name: LUMBERTON, NC Waypoint Analytical Virginia Inc.
NPDES# : NCO024571
or WQ# (residual only)
WWTP Name: LUMBERTON WWTP
Residuals Analysis Data
Product Type
Date Sampled (grab) or
Date Composited
Percent Solids
AEDLIQ AEDLIQ AEDLIQ AEDLIQ AEDLIQ
01/30/17 04/27/17 06/28/17 08/03/17 10/04/17
PARAMETERS (mg/kg dry weight)
Arsenic
Cadmium
Mercury
Chromium
Copper
Lead
Molybdenum
Nickel
Selenium
Zinc
Total Phosphorus
TKN
Ammonia -Nitrogen
Nitrate and Nitrite
4.58
5.87
2.49
1.04
3.24
5.33
<3
4.54
6.2
3.81
<2
<2
- <2
<2 _
<2
<0.4
<0.4
<0.4
<0.4
<0.4
196
177
185
157
218
2.33
306
278
269
296
16.3
13.7
18.1
21.6
15
<5
<5
<5
<5
<5
26.3
25.3
27.1
•17.9
24'.9
<5
<5
<5
<5
<5
378
411
393
275
589
16400
19000
17500
21500-
19000
53600
25500
35600
43800
40400
5660
3060
2800
<50
2780
68.2
167
253
21000
1480..
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
.significant penalties for submitting false information, including the possibility of fines -and imprisonment for knowing violations."
KI
Date --7 � 5� ( / P°
DENR FORM RSSF (5/2003) Printed: Friday - February 9, 2018 at 08:23:39 for: 2101 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0000672
Laboratory
Facility Name: LUMBERTON, NC
Waypoint Analytical Virginia Inc.
NPDES# : NCO024571
or WQ# (residual only)
-WWTP Name: LUMBERTON WWTP
Residuals Analysis Data
Product Type AEDLIQ AEDLIQ
AEDLIQ AEDLIQ AEDLIQ
Date Sampled (grab) or 01/30/17 04/27./17
06/28/17 08/03/17 10/04/17
Date Composited
Percent Solids 4.58 5.87
2.49 1.04 3.24
PARAMETERS (mg/kg dry weight)
Aluminum
31900
2.7400
35000
35700
43900
Calcium
11200
12100
12100
8330
12000
Magnesium
1590
1420
1550
1120
1330
pH
7.36
7.22
6.72'
3.71
6.58
Potassium
2890
2630
2430
2430
2090
Sodium
5650
7310
8290
9730
15300
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X. Date �-� ZZ
(SIGNATURE OF PREPARER)
NR - Data Not Reported or Data Not Required
DENR FORM RSSF-B (7/2002) Printed: Friday - February 9, 2018 at 08:24:06 for: 2101 01

Page: 1 of 2
Report Number: 17-03170203
Account Number: 46525
7621 Whitepine Road, Richmond, VA 23237
Submitted By: ChadHayes .
Waypigint
Main 804-743-9401 ° Fax [phone]
AYTICAL
- www.wayppintanalytical.com
Send To: Synagro Central LLC/ Lumberton.
Project : Lumberton -
Mary Brewer
NC Cert#257
284 Boger Road
t
_
Mocksville;, NC 27028 =
"
REPORT -OF ANALYSIS
.,Date sampled: 1/30/2017 10:50:00
:Lab -Number•: 61962
Date Received: 01/31/2017 00'-00`
Sample Id : Lumberton
Date Reported: 02/06/2017
PARAMETER
RESULT
RESULT
QUANTITATION
Total Solids*
4.58
45800
100.0.
BW1
01/31/2017 14:45 SM-2540G
Moisture *
95.41
100.0
BW1
01/31/2017 14:45 SM-2540G -
Total Kjeldahl Nitrogen
5.36
-53600
10.0
JM
02/04/2017 11:00 SM-4500-NH3C-TKN
Total Phosphorus
1.64
16406
100
JTR. ,.
02/03/2017 21:11 6010C
Total Potassium _
0.29
2890
1000
.JTR
02/03/2017 21:16 . 6010C
Total Sulfur
6.67
6670
100
JTR
02/03/2017 21:11. 6010C
Total Calcium
1:12
11200
100
JTR
02/03/2017 21,11 6010C
Total Magnesium
0.1.6
1590
100 ..
"JTR
02/03/2017 21:11 6010C
Total Sodium
0.57
5650
100-
JTR _
02/03/2017-21:11 6010C ..
Total Iron
14800
100
JTR
02/03/2017 21:11 6010C
Total Aluminum
31900
100
JTR
02/03/2017 21:11 6010C• "
Total Manganese
295
5.00
JTR
02/03/2017 21:11, 6010C
Total Copper.-
233
5.00
JTR
02/03/2017 21:11 (010C-
Total Zinc
378
5.00
JTR
02/03/2017 21:11 6010C
Ammonia Nitrogen
0.57
5660
10.0
JM
02/04/2017 10:50 SM-4500-NH3C
Organic N
4.79
47940
10.0
02/04/2017,10:50 CALCULATION
Nitrate+Nitrite=N
68.2
2.45
SJB
02/01/201713:30 4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
,
Our reports and letters are for the exclusive and confidential use of
our clients, and may not be reproduced in whole or•part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Laboratory Supervisor.

Page: 2 of 2
Report Number: 17-0311-0203
Account Number: 46525
Submitted By: Chad.Hayes
Send To: Synagro Central LLC/-Lumberton
Mary Brewer -
284'Boger Road
Mocksville , NC 27028
Lab Number:! 61962
Sample Id : Lumberton
Total Chromium
Total Nickel
Total Lead
Total Arsenic
Total Mercury
Total Selenium
PH (Standard Units)
--,Total Molybdenum
Comments:
7.36
�nt.
PVPOI7621 Whitepine Road, Richmond, VA 23237
(2)
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Project: Lumberton
NC Cert#257
REPORT OF ANALYSIS Date sampled: 1/30/2017 10:50:00
-Date Received:'01/31/2017 00:00
Date Reported:-02/06/2017
996
26.3
16.3
5.33'
<0.400
<5.00
Mil
2.00
JTR
02/03/2017 21:11
.601 OC
5.00
JTR,
02/03/2017 21:11
6010C
5.00
JTR
02/03/2017 21:11
601 OC
5.00
JTR
02/03/2017 21:11
6010C
3.00
JTR
'02/03/2017 21:11.
601 OC
0.400
SJB
02/02/201710:45
SW-7411B
5.00
JTR
02/03/2017 2.1:11
601 OC
1.00
R D
02/01/2017 08.-30
SW-9045D
5.00
JTR
02/03/2017 21:11
601 OC
'All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
Our reports and letters are for the exclusive and confidential use of our clients, and, may not be reproduced in whole. or part nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Laboratory Supervisor

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date, Report Range Ratio
2101-01-AEDLIQ-NC LUMBERTON, NC WWTP AEROB. DIGESTED 1/30/2017 1/112017-3131/2017 2.8253
LIQUID
Na mg/I = (Na mg/kg?( % Solids) = 100 = (5650 x 4.5800) = 100 = 258.77
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (11200 x 4.5800) : 100 = 512.96
Mg mg/I = (mg mg/kg x % Solids) = 100 = (1590 x 4.5800) _ 100 = 72.822
Na meq = Na mg/I : Molec.Wgt.Na = 258.77 : 23 = 11.2509
Ca meq = Ca mg/I + Molec.Wgt.Ca = 512.96 - 20 = 25.648
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 72.822 _ 12 = 6.0685
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)],= 11.2509 _ SgrRoot[0.5(25.648+6.0685)] = 2.82526
Printed: 2/9/2018
Page 1 08:33

Page: 1 of 2
Report Number: 17-118-0202
Account Number: 46525
Submitted By: Chad Hayes
Send To Syhagro. Central LLC/.Lumberton
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 63628
Sample Id : 'Lumberton WWTP
Wavooint'.......�
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Project: Lumberton WWTP-
REPORT OFANA_ LYSIS Date sampled: 4/27/201712:00:00
Date Received: 04/28/2017 00:00
Date Reported: 05/04/2017
Total Solids *
5.87
58700
.100.0
R D
04/28/2017 14:45
SM-2540G
Moisture *
94.12
1100.0
R D
04/28/2017 14:48
SM-2540G
Total Kjeldahl Nitrogen
2..55.
2.5500
50.0
R D
05/01/2017 07:45
SM-4500-NH3C-TKN
Total Phosphorus
1:90
19000
100
MOS
05/01/2017 13:11
6010C
Total Potassium
0.26
2630
100
MOS
05/01/2017 13:11
; - 6010C
Total Sulfur
0.81
8140
100
MOS
05/01/2017,13:11
6010C
Total:Calcium
1.21
12100 ,
100
MOS
'05/01/2017 13:11
. , 6010C
Total Magnesium
0.14
1420
100
MOS
06/01/2017 13:11
6010C
Total Sodium
0.73
7310
100
MOS -
05/01/2017 13:11
6010C
Total Iron
15000
100
MOS
.05/01/201713:11
6010C
Total -Aluminum
27400
100
MOS
'05/03/201712:48
6010C
Total Manganese
294
.5.00
MOS
05/01/2017 13:11
6010C
Total Copper
306
5.00 -
MOS
05/01/2017 19:11
6010C
Total Zinc
411
5.00
MOS
"05/01/2017 13:11
.6010C
Ammonia Nitrogen
0.31
.3060
50.0
R D
05/61/2017 07:45
SM-4500-NH3C
Organic N
2.24
22440
50.6
05/01/2017 07:45
CALCULATION
Nitrate+Nitrite-N
167
2.34
SJB
05/03/2017-13:56
4500NO3F-2011 "
All values are .on a dry weight basis except as noted
by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any
reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining ourprior written authorization.
Pauric McGroary
Agronomist

Page: 2 of 2
Report Number: 17-118-0202
Account Number: 46525
Submitted.By: Chad Hayes
Send To: Synagro Central LLC/ Lumberton
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 63628
Sample Id : Lumberton WWTP
Wayoint,w
-ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytica Isom
Project: Lumberton WWTP
REPORT OF ANALYSIS Date Sainpled:.4/27/2017 12:00:00
Date Received: 04/28/2017 00:00
Date Reported: 05/04/2017
Total Cadmium
<2.00
Total Chromium
177
Total Nickel
25.3
Total Lead
13.7
Total Arsenic
<3.00
Total Mercury
<0.400
Total Selenium
<5.00
pH (Standard Units).*.
7.22
Total Volatile Solids
36:42 364200
Total Molybdenum
<5.00
Comments:
NC CERT#257, -SC CERT#9300 7001
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
2.00
MOS
05/01/201713:11
'6010C
5.00
-MOS
05/01/201713:11
6010C
5.00
MOS
05/01/201713:11
6010C
5.00
MOS
05/01/201713:11
6010C
3.00
MOS
05/01/201713:11
6010C
0.400
SJB
05/03/2017 11:46
SW-7471 B
5.00
MOS
05/01/201713-:11
6010C
1.00
R D
05/01/2017 0.7:45
SW-9045D
100.0
R D
04/28/2017 14:45'
_ SM-2540G
5.00
MOS
05/01/2017 13:11
6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, orotherpublic announcements without obtaining ourprior written authorization.
?W« imp 60wr
Pauric McGroary
Agronomist

Sodium -Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
2101-01-AEDLIQ-NC . LUMBERTON, NC WWTP AEROB. DIGESTED 4/27/2017 51112017-6/3012017 4.0491
LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (7310x5.8700) _ 100 = 429.097
Ca mg/1= (Ca mg/kg x % Solids) + 100 = (12100.x 5.8700) = 100 = 710.27
Mg mg/I = (mg mg/kg x % Solids) = 100 = (1420 x 5.8700) _ 100 = 83.354
Na meq = Na mg/I,- Molec.Wgt.Na = 429.097 _ 23 = 18.6564
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 710.27 _ 20 = 35.5135'
Mg meq = Mg mg/I = Molec.Wgt.Mg = 83:354 =12 = 6.94617
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 18.6564 _ SgrRoot[0.5(35.5135+6.94617)] = 4.04906
Printed: 2/9/2018
Page 1 08:33

i III
1 /
Page: 1 of 2
Report Number: 17-180=0203
Account Number: 46525 of nt.w 7621 Whitepine Road, Richmond, VA 23237
WaypSubmitted By: -Chad-Hayes Main 804-743-9401 ° Fax [phone] "
ANALYTICAL www.waypointanalytical.com
Send To: Synagro Central.L_LC/ Lumberton Project : Lumberton
Mary Brewer
284 Boger Road
Mocksville , NC 27028
REPORT OFANALYSIS Date sampled: 6/28/2017 09:28:00 .
Lab Number: 55061 Date Received: 06/29/2017 00:00
Sample Id : Lumberton WWTP Date Reported: 07/07/2017
Total Solids *
2.49
24900
100.0
JM
06/29/2017 15:00
SM-2540G
Moisture *
97.50
100.0
JM
06/29/2017 15:00
SM-2540G
Total Kjeldahl Nitrogen
3.56
35600
50.0
R D
06/30/2017 08:30
SM-4500-NH3C-TKN
Total Phosphorus
1.75
17500
100
-MOS
07/06/2017 14:56.
6010C .
,Total Potassium
0.24
2430
100
MOS
07/06/2017 14i56
6010C
Total Sulfur
0.79
7860
100
MOS
07/06/2017 14:56
6010C
Total Calcium
1.21
12100
100
MOS
07/06/2017 14:56'
6010C
Total_ Magnesium
0.16
1550
100.
MOS -
07/06/2017 14:56
6010C
Total'Sodium,
0.83 ' .
8290
100
MOS
07/06/2017 14:56
6010C
Total Iron
16900
100
MOS
07/06/2017 14:56
6010C
Total Aluminum
35000
100
MOS
07/06/2017 14:56
6010C
Total Manganese
307
5.00--
MOS
07/06/201714'.56
6010C
Total Copper
278
5.00
MOS
07/06/2017 14:56
6010C
Total Zinc
393
5.00
MOS
07/06/2017 14:56
.601 OC
Ammonia Nitrogen
0.28
2800
50.0
R D
06/30/2017 08:30
SM-4500-NH3C
. - Organic:N
3.28
32800
50.0
06/30/2017`08:30
CALCULATION _
Nitrate+Nitrite-N
253
2.04
SJB
07/06/201714:21
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk.' Detection
limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in
whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Pauric McGroary
Agronomist _

Page: 2 of 2
Report Number: 17-180-0203
Account Number: ' 46525
Submitted By: Chad Hayes
Send To: Synagro-Central LLC/ Lumberton
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 55061
Sample Id : Lumberton WWTP
WayintrvPARTICAL
Project :,Lumberton
REPORT. OF ANALYSIS
Total Cadmium
<2.00
2.00.
Total Chromium
185
5.00
Total Nickel
27.1
5.00
Total Lead
18.1
5.00
Total Arsenic
4.54
3.00
Total Mercury
<0.400
0.400
Total Selenium
<5.00 .
5.00
pH * ,
6.72'
1.00
Total Volatile. Solids
61.90-619000
100.0 "
Total Molybdenum
-<5.00
5.00.
Comments:
NC CERT#257, SC CERT#9300 7001.
SULFUR AND ORGANIC NITROGEN NOT FOR
COMPLIANCE PURPOSES.
7621 Whitepine Road, Richmond, VA 23237
Main'804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Date Sampled: 6/28/2017 09:28:00
Date Received: 08/29/2017 00:00
Date Reported: 07/07/2017
MOS
07/06/201714:56
6010C
MOS
07/06/201714:5.6
6010C
MOS
07/06/201714:56
6010C
MOS
07106/201714:56
6010C
MOS
07/06/201714:56
6010C
SJB
' • 07/06/2017 11:31
SW-7471 B
SJB
07/06/201714:56
6010C
R. D -
06/30/2017 08:30
SW-9045D
JM
06/29/201715:00
SM-2540G
SJB
07/07/201712:30
6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Pauric McGroary
Agronomist

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange - Ratio
2101-01-AEDLIQ-NC LUMBERTON, NC WWTP AEROB. DIGESTED 6/28/2017 7/1/2017-7/31/2017 2.9685
LIQUID
Na mg/I = (Na mg/kg x % Solids) + 100 = (8290 x 2.4900) + 100 = 206.421
Ca mg/I = (Ca mg/kg x % Solids) + 100 = (12100 x 2.4900) + 100 = 301.29.
Mg mg/I = (mg mg/kg x % Solids) = 100 = (1550 x 2,4900) + 100 = 38.595
Na meq = Na mg/I _ Molec.Wgt.Na = 206.421 _ 23 = 8.97483
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 301.29 + 20 = 15.0645
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 38.595 = 12 = 3.21625
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 8.97483 = SgrRoot[0.5(15.0645+3.21625)] = 2.96855
Printed: 2/9/2018
Page 1 08:33

l
Page:, 1 of 2
Report Number: .17-216-0201
Account Number: 46525 7621 White'pine Road, Richmond, VA 23237
Waypoint Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com.
Send To Synagro Central LLC/Lumberton Project Lumberton WWTP
Mary Brewer
'284 Boger Road
Mocksville , NC 27028
REPORT OF ANALYSIS Date Sampled:, 8/3/2097 09:30:00
Lab Number: 55541 Date Received: 08/04/2017 00:00
Sample Id"Lumberton WWTP Date Reported: 08/11/2017
Total Solids *
1.04
10400
100.0
R D
08/04/201T 14:10
SM-25400
Moisture *
98.95
_ 100.0
R D
08/04/2017 14:10
SM-25406
Total Kjeldahl Nitrogen
4.38
43800
.50.0
_ R D
08/07/2017 09:00
SM-4500-NH3C-TKN
Total Phosphorus
2.15
21500
100'
MOS
08/08/2017 12:41
60,10C'
Total Potassium
0.24
2430
100
M08
08/07/2017 17:37
6010C
Total Sulfur
0.87
8700
100
MOS
08/08/2017 12:41
6010C '
Total Calcium
0.83'
8330
100
MOS
0810.7/2017 17:37
6010C
Total Magnesium
0.11
1120
100 ,
MOS
08/07/2017 17:37
60.10C
Total Sodium -
-0.97
9730
-100
MOS
08/09/2017 12:41
6010C
Total Iron
19000
100.
MOS
08/07/2017 17:37
6010C
Total Aluminum
35700
100
MOS
08/07/2017 17:37
6010C .
Total Manganese
164
5.00
MOS
08/07/2017 17:37
6010C
Total Copper
269
5-00
MOS
08/07/2017 17:37
6010C
Total Zinc
275
5:00
MOS
08/07/2017 17:37
. • 6010C
'Ammonia.Nitrogen
<50.0
. 50.0
R D
08/07/2017 09:00
SM-4500-NH3C
Organic N •
43800
50.0
08/0712017,09:00
CALCULATION
Nitrate+Nitrite-N
21000
20.0
SJB
08/07/2017.15:33
4500NO3F-2011
All values are on a dry weight basis except as noted
by asterisk.
Detection limit on all N series is on a wet basis.
. P;em
we
Our reports and letters are for the exclusive and confidential use ofourclients, and may not be reproduced in whole orpart nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prlor written authorization.
Pauric McGroary
Agronomist

Page: 2 of 2
ReportNumber: 17-216-0201
Account Number: 46525
Waypoint7621
Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax.[phone] '.
ANALYTICAL' =
www.waypointanalytical.com
Send To: Synagro Central LLC/ Lumberton
Project: Lumberton WWTP
Mary Brewer
284 Boger Road
Mocksville., NC 27028
REPORT OFANALYSIS
Date Sampled: 8/3/2017 09:30:00 - =
Lab Number:. 55541
Date Received: 08/04/2017 00:00 .
Sample Id : Lumberton WWTP
Date Reported: 08/11/2017
RESULT
RESULT QUANTITATION
.
DATEITIME METHOD
Total Cadmium. -.
<2.00 2.00 MOS
08/07/2017 17:37 601OC
Total Chromium
" 157 5.00 MOS
08/09/2017 12:43 6010C
Total Nickel
17.9 5.00 MOS
08/09/2017 12:43 6010C
Total Lead
21..6 5.00 MOS,
08/07/2017 17:37 6010C
Total Arsenic
6:20 ` 3.00 MOS
'08/07/2017 17:37 6010C
Total Mercury
<0.400 0.400 SJB
08/08/2017 15`.37 SW-7471B
Total Selenium
<5.00 5.00 MOS
08/07/2017 17:37. 60.10C
p-H *.. 3.7.1
• -1.00 R D
08/07/2017 09:00 SW-9045D
Total Volatile Solids . 5000
500000" - 100.0.. R.D'
08/04/2017 14:10 SM-2540G
Total Molybdenum
<5.00 5.00 MOS
08/07/2017 17:37 601OC
Comments:
NC CERT#257, SC CERT#9300 7001
SULFUR'AND ORGANIC 'NITROGEN -NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk'. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining ourprior written authorization.
Pauric McGroary
Agronomist

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2101-01-AEDLIQ-NC LUMBERTON, NC WWTP AEROB. DIGESTED 8/3/2017 - 81112017-9/30/2017 2.7021
LIQUID
Na mg/I = (Na mg/kg x % Solids) =.100 = (9730 x 1.0400) — 100 = 101.192
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (8330 x 1.0400) _ 100 = 86.632
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (1120 x 1.0400) = 100 = 11.648
Na meq = Na mg/I _ Molec.Wgt.Na = 101.192 _ 23 = 4.39965
Ca meq = Ca mg/I = Molec.Wgt.Ca = 86.632 _ 20 = 4.3316
Mg meq = Mg mg/I = Molec.Wgt.Mg = 11.648 = 12 = 0.970667
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.39965 _ SgrRoot[0.5(4.3316+0.970667)] = 2.70211
Printed: 2/9/2018
Page 1 08:34

Page: 1 of 2
.Report Number: 17-278=0209
Account Number: 46525
Waypolnt.-.7621
Whitepine Road, Richmond, VA 23237
Submitted By: Chad Hayes
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www.waypointanalytical.com
Send To: Synagro Central LLC/ Lumberton
Project : Lumberton WWTP
Mary Brewer
284 Boger Road
Mocksville , NC 27028
-
REPORT OF ANALYSIS
Date Sampled: 10/4/2017 09:45:00
Lab Number: 56510
Date Received: 10/05/2017 00:00
Sample Id : Lumberton WWTP
Date Reported: 10/12/2017.-
PARAMETER
RESULT
RESULT
QUANTITATIONANALYST
METHOD
Total Solids *
3.24 -
"• 32400
100.0
R D
10/05/2017 14:50 '. SM-2540G
Moisture *
96.76
100.0
R D
10/05/2017 14:50 SM-2540G
Total Kjeldahl Nitrogen
4.04
40400
50.0
R D.
10/06/2017 08:40 SM-4500-NH3C-TKN
Total Phosphorus
1.90-
19000
100
MOS
1,01-10/2017 14:04 '6010C
Total Potassium
0.21- "
2090
100
MOS
=10/10/2017 14:04 6010C
Total Sulfur
0.89
8890
100"
MOS
10/10/2017 14:04 6010C-
Total Calcium.
1.20
12000
100'
MOS
10/10/2017 14:04 6010C
'.Total Magnesium
0.13
1330
- 100"
MOS
10/10/2017 14:04 6010C
Total Sodium"
1.53
15300
1000
MOS
10/12/2017 13:29 : 6010C
. Totallron
14500
1001MOS
10/10/2017 14:04 6010C
Total Aluminum
43900
100
MOS .
10/10/2017 14:04 6010C
Total Manganese "
361
5.00
MOS
10/10/2017 14:04 .6010C
Total Copper
296
5.00
MOS
10/10/2017 14:04 6010C .
Total Zinc
589
5.00
MOS '
10/10/2017 14:04 6010C
Ammonia Nitrogen
0:28
-2780
50.0
R D
10/06/2017 08:40 _ SM-4500-NH3C
Organic N, ..
3.76
37620
•50.0
10/06/2017 08:40 CALCULATION
Nitrate+Nitrite-N
1480
2.31
SJB
10/10/201714:55 4500NO3F=2011
All values are on a dry weight basis except as noted by asterisk.
Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of
our clients, and may not be reproduced in whole or part normay any reference be made
{I -
'to the work, the results, or the company in any advertising, news release, orothet public"announcements without obtaining our prior written authorization:
Pauric McGroary
Agronomist

Page: -2 of 2 %
Report Number: 17-278-0209
Account Number: 46525
Waypoin
t,W
7621 Whitepine Road, Richmond, VA 23237
Submitted By: Chad Hayes "
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www:waypointan6lyti6al.com
Send To: Synagro Central LLC/ Lumberton
Project: Lumberton WWTP
Mary Brewer
284 Boger Road
Mocksville , 'NC 27028
REPORT,OFANALYSIS ;
Date Sampled: 10/4/2017 09'.45 00
Lab Number: 56510
Date Received: 10/05/2017 00:00
Sample Id ; Lumberton WWTP
Date Reported: 10/12/2017
RESULT
RESULT
QUANTITATION
PARAMETER
.
,, •.
Total Cadmium
<2.00
2.00
MOS
10/10/2017 14:04 6010C
Total Chromium
218
5.00
MOS
10/10/2017 14:04 6010C
Total Nickel
24.9 -
` 5.00
MOS
.10/10/2017 14:04 6010C "
Total Lead
15.0
5.00
MOS •
10/10/2017 14:04 6010C
Total Arsenic
3.81
3.00
MOS
10/10/2017 14:04 6010C
Total Mercury'
<0.400
0.400
SJB
10/10/2017 14:14 SW-7471B
Total Selenium "
<5.00
5.00 , ""
MOS
10/10/2017 14:04 6010C
PH * 6.58
1.00
R D -"
10/06/2017 08:40 SW-9045D
Total Volatile Solids" 64.19
641900
100.0
R D
10/05/2017 14:50 SM-2540G "
• Total Molybdenum
<5.00
5.00
MOS
10/10/2017 14:04 6010C
Comments:
NC CERT#257, SC CERT#9300 7001 .
SULFUR AND ORGANIC -NITROGEN NOT FOR COMPLIANCE
-PURPOSES..
All values are on a dry weight basis except as noted. by asterisk. Detection limit on all N. series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made
to the work, the results, or the company in any advertising, news release, orother public announcements without obtaining ourprior written authorization.
`60w
Pauric McGroary
Agronomist

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
2101-01-AEDLIQ-NC LUMSERTON, NC WWTP AEROB. DIGESTED 10/4/2017 10/l/2017-12/31/2017 6.3514
LIQUID
Na mg/I = (Na mg/kg x % Solids) _ 100 = (15300 x 3.2400) _ 100 = 495.72
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (12000 x 3.2400) + 100 = 388.8
Mg mg/I = (mg mg/kg x % Solids) + 100 = (1330 x 3.2400) + 100 = 43.092
Na meq = Na mg/I = Molec.Wgt.Na = 495.72 = 23 = 21.553
Ca meq = Ca mg/I - Molec.Wgt.Ca =.388.8 _ 20 = 19.44
Mg meq = Mg mg/I + Molec.Wgt.Mg = 43.092 = 12 = 3.591
SAR = Na meq : SgrRoot[0.5 x (Ca meq + Mg meq)] = 21.553 = SgrRoot[0.5(19.44+3.591)] = 6.35137
Printed: 2/9/2018
Page 1 - 08:34

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
'ACILITY NAME: LUMBERTON, NC PREDOMINANT SOIL SERIES: RAINS
iWNER: OZZELL BAKER PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 55.65
ITE #: NC RO 00016 FIELD# : RO 00016 0001 OPERATOR: OZELL BAKER CATION EXCHANGE CAPACITY (NON-503):
:ESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 16.90 ACRES PERMITTED: 16.90
Page : 1
Lune Applied ***
Date
Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(pp-)
Crop
Total
Per Acre
MONTH
3/9/17
248,000.00 (G)
14674.556
4.58
2.803
LUAEDL
DRY
"0-<1/2"
SUR
0.5
0.30
53,600. p
5,660.00 p
68.20 p
17280
I BERMUDAGRASS, COASTAL
3/10/17
43,400.00 (G)
2568.047
4.58
0.490
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30 ,
53,600. p
5,660.00 p
68.20 p
17211
BERMUDAGRASS, COASTAL
Mar-17
1 291,400.00 (G)
17,242.603
Total Gallons/Ac: 17,242.60
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
knnual lbs/acre
114
• 0.035
0.013
1.291
1.535
0.107
0.003
0.033
0.173
0.033
2.490
108.01
umulative lbs/acre
0.057
0.024
1.987
2.872
0.177
0.003
0.060
0.286
0.060
4.410
s
L
ermit PAN Limit (lbs/acre) , 1st Crop/2nd Crop
M : i
ti
194
FD Cumulative Pollutant LoadingRate Limit lbs/acre
( )
36.6
34.8
1339.0 267.9
i
15.0 375.0
89.0
2500.0
,
UAEDL = LUMBERTON, NC W WTP AEROB. DIGESTED LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppm ormg/kg _** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

ACILITYNAME: LUMBERTON,NC
)WNER: OZZELL BAKER
ITE #: NC RO 00016 FIELD# : RO 00016 0002
:ESIDUAL SOURCE(S):* See list at bottom of report
I
i
ANNUAL LAND APPLICATION (FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GOLDSBORO
PERMIT #: WQ0000672 ANNUAL DRY TONS APPLIED: 14.21
OPERATOR: OZELL BAKER CATION EXCHANGE CAPACITY (NON-503):
I ACRES UTILIZED: 3.60 ACRES PERMITTED: 3.60
Page
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards.(CY)
Dry
Site
Inches ,
Appli-
Vola-
Miner -
or Wet Tons (VM (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
pC1
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pp-)
Crop
MONTH
Total
Per Acre
Solids
3/13/17
74,400.00 (G)
20666.667
4.58
3.947
LUAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
53,600. p
5,660.00 p
68.20 p
17280
BERMUDAGRASS, COASTAL
Mar-17
74,400.00 (G)
20,666.667
J
1
1
Total Gallons/Ac: 20,666.67
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annual lbs/acre
136
0.042
0.016
1.547
1.839
0.129
0.003
0.039
0.208
0.039
2.984 129.46
Cumulative lbs/acre
0.074
0.032
3.107
4.682
0.255
0.005
0.089
0.451
0.080
7.003
{
'ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop
'-
s
i
;.
184
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 1 375.0
89.0
2500.0
, ,
LUAEDL = LUMBERTON, NC WWI? AEROB. DIGESTED LIQUID
I
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required Vo = percent p = ppm or mg/kg ** Vol atilization Rate : Surface 0.5, Injection/Incorporation 1.0
k Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation * ** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

ACILITY NAME: LUMBERTON, NC
WNER: OZZELL BAKER
lTE #: NC RO 00016 FIELD# : RO 00016 0003
ESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION
PREDOMINANT SOIL SERIES:
PERMIT #: WQ0000672
OPERATOR: OZELL BAKER.
SUMMARY FORM
ANNUAL DRY TONS APPLIED: 9.47
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 3.40 ACRES PERMITTED: 3.40
Page
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
'ali-
Ammonia
Nitrate
PAN
DATE or
per
Residual
Dry, Wet,
Past 24
Method
zation
ization
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
3/17/17
49,600.00 (0)
14588.235
4.58
2.786
LUAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
53,600. p
5,660.00 p
68.20 p
17280
BERMUDAGRASS, COASTAL
Mar-17
49,600.00 (G)
14,588.235
1
Total Gallons/Ac: 14,588.24
As Cd Cr Cu
Pb "
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
knnuallbs/acre
0.030
0.011
1.092
1.298-
�
0.091
0.002
0.028
0.147
0.028
2.106
91.39
96
cumulative lbs/acre
0.078
0.035
3.150
5.105
0.269
0.004
0.097
0.472
0.088
7.512
!
ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop
!
i
t
, i
299
_
?D Cumulative Pollutant LoadingRate Limit lbs/acre
( )
36.6
34.8
i
1339.0
! 267.9
-
15.0 375.0
89.0
2500.0
,UAEDL = LUMBERTON, NC W WTP AEROB, DIGESTED LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision:in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for latowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
r. Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** SeelSite pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

ANNUAL LAND APPLICATION FIELD _SUMMARY FORM
ACILITY NAME: LUMBERTON, NC PREDOMINANT SOIL SERIES: RAINS
WNER: OZZELL BAKER PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 13.03
ITE #: NC RO 00016 FIELD# : RO 00016 0004 OPERATOR: OZELL BAKER CATION EXCHANGE CAPACITY (NON-503):
ESIDUAL SOURCES):* See list at bottom of report ACRES UTILIZED: 3.60 ACRES PERMITTED: 3.60
Page : 1
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total -
Per Acre
Solids
3/16/17
68,200.00 (G)
18944.444,
4.58
3.618
LUAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
. 53:,600. p
5,660.00 p
68.20 p
17280.7
BERMUDAGRASS, COASTAL
Mar-17
68,200.00, (G)
18,944.444
Total Gallons/Ac: 18,944.44
"
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
knnual lbs/acre
125
0.039
0.014
1.418
1.686
0.118
0:003
0.036
0.190
0.036
2335 118.67
-
3umulative lbs/acre
0.074
0.032
3.040
4.663
0.254
0.004
0.089
0.445
0.081
6.954 s
ermit PAN Limit (lbs/acre). 1st Crop/2nd Crop
. 5 ;
I
j
{
1 t
IY ^ Y a
194
?D Cumulative Pollutant Loading Rate Limit (lbs/acre)'
36.6
34.8
J
1339.0
267:9
15.0
-375.0
89.0
2500.0 ,
jT ,
,..i...L.r:
,UAEDL=LUMBERTON, NC WWTP AEROB. DIGESTED LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with -a system designed to assure that qualified personnel properly gathered and,
evaluated the information submitted: I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate - Surface '0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
ACILITY NAME: -LUMBERTON, NC PREDOMINANT SOIL SERIES: RAINS
WNER: OZZELL BAKER PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 35.52
TE #: NC RO 00016 FIELD# : RO 00016 0005 OPERATOR: OZELL BAILER CATION EXCHANGE CAPACITY (NON-503):
ESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 8.70 ACRES PERMITTED: 8.70
Page: 1
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches.
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
)ATE or
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
m
(pp )
Cro p
MONTH
Total
Per Acre
Solids
3/16/17
186,000.00 (G)
21379.310
4.58
4.083
LUAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
53,600. p-
5,660.00 p
68.20 p
17280
'BERMUDAGRASS, COASTAL
Mar-17
186,000.00 • (G)
21,379.310
Total Uallons/Ac: 21,379.31
As
Cd
Cr
Cu
Pb
Hg
Mo.
Ni
Se
Zn
P
PAN
TOTALS:
-
mnuallbs/acre
141
0.044
0.016
1.601
1.903
0.133
0.003
0.041
0.215
0.041
3.087
133.93
;umulative lbs/acre
0.073
0.031
2.814
4.160
1 0.241
0.004
0.082
0.407
0.078
6.298
t
g17
194
mnit PAN Limit (lbs/acre) 1st Crop/2nd Crop
..
j
1
iY
3 3
r lI it 4 l
} t 1
#
S
t,
_
D Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
'
1339.0
15.0
G,
267.9
375.0
1�
89.0
2500.0
"UAEDL = LUMBERTON, NC W WTP AEROB. DIGESTED LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am�aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for lmowing violations."
N/A = Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
s Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

'ACILITY NAME: LUMBERTON, NC
)WNER: OZZELL BAKER
ITE #: NC RO 00016 FIELD# : RO 00016 0006
:ESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: NORFOLK
PERMIT #: WQ0000672 ANNUAL DRY TONS APPLIED: 52.10
OPERATOR: OZELL BAKER CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 14.80 ACRES PERMITTED: 14.80
Page: 1
Lune Applied***
Date
Lbs/Ac
DATE or .
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
Wirt)
crop
Total
Per Acre
3/10/17
241,800.00 (G)
16337.838
4.58
3.1W
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
53,600. p
5,660.00 p
68.20 p
17280
I BERMUDAGRASS, COASTAL
3/13/17
31,000.00 (G)
2094.595
4.58
0.400
LUAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
53,600. p
5,660.00 p
68.20 p
17280
BERMUDAGRASS, COASTAL
Mar-17
272,800.00 (G)
18;432.433
Total Gallons/Ac: 18,432.43
As
Cd
Cr
Cu
'Pb
Iig
Mo
Ni
Se
Zn-
P
PAN
TOTALS:
Annuallbs/acre
122
0.038
0.014
1.380
1.640
0.115
0.003
0.035
0.185
0.035
2.661
1-15.47
Cumulative lbs/acre
0.079
0.035
3.562
5.585
0.286
0.006
0.101
0.524
0.087
8.225rs
'emiit PAN Limit (lbs/acre) 1st Crop/2nd Crop
161
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
r ?
1339.0
267.9
15.0 Yj� 375.0
89.0
2500.0 =
7
F`
� ._._.
M.../w'[
LUAEDL = LUMBERTON, NC W WTP AEROB. DIGESTED LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/lcg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
'k Application Method: SUR - Surface, INJ - hijection, SURIN -•Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
ACILITY NAME: LUMBERTON, NC PREDOMINANT SOIL SERIES: WAGRAM
WNER: OZZELL BAKER PERMIT #: WQ0000672 ANNUAL DRY TONS APPLIED: 28.42
iTE #: NC RO 00016 ' FIELD# : RO 00016 0008 OPERATOR: OZELL BAKER CATION EXCHANGE CAPACITY (NON-503):
ESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 7.60 ACRES PERMITTED: 7.60
Page : I
Lime Applied ***
Date
.Lbs/Ac
allons (G) or Cubic Yards (CY)
'
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
THIN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
3/17/17 .
148,800.00 (G)
19578.947
.4.58
3.739
LUAEDL .
MOLST
0-<1/2"
SUR
0.5
0.30
53,600. p
5,660.00 p
68.20 p
17280
BERMUDAGRASS, COASTAL
Mar-17
148,800.00 (G)
19,578.947
Total Gallons/Ac: 19,578.95
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Unnual lbs/acre
129
0.040.
0.015
1.466
1.743
0.122
0.003
0.037
0.197
0.037
2.827
122.65
:umulative lbs/acre
0.090
0.040
3.089
4.863"
0.285
0.003
0.100
0.461
0.100
7.307
f
t t
ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop
', i
(
j
€
s
264
,D Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 { ;. " 375.0
89.0
2500.0
,UAEDL = LUMBERTON, NC W WTP AEROB. DIGESTED LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

FACILITY NAME: LUMBERTON, NC
JWNER: J T CAMPEN
SITE #: NC RO 00016 FIELD# : RO 00016 0016
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: WAGRAM
PERMIT #: WQ0000672 ANNUAL DRY TONS APPLIED: 15.08
OPERATOR: OZELL BAKER CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 5.00 ACRES PERMITTED: 5.00
Page: I
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (VM (specify)
-
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
MONTH
Total
Per Acre
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
T N
Nitrogen
and
m
(pp )
Cro p
11/3/17
111,600.00 (G)
22320.000
3.24
3.016
LUAEDL
DRY
0- 1/2"
SUR
0.5
0.30
40,400. p
2,780.00 p
1,480.00 p
14156
BERMUDAGRASS, COASTAL
Nov-17
111,600.00 (G)
22,320.000
1
Total Gallons/Ac: 22,320.00
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annuallbs/acre
85
0.023
0.012
1.315
1.785
0.090
0.002
0.030
0.150
0.030
3.552
114.59
Cumulative lbs/acre
0.269
0.155
11.247
40.093
3.872
0.036
0.742
3.247
0.238
33.023
„-r , ;__: �-,`•,-,
,-,,.� �, <<--;::,'.
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
j
- j
t
s
264
I
i
^i
l
?
"+
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
!
1339.0
267.9
15.0 375.0
89.0
2500.0
s
LUAEDL = LUMBERTON, NC W WTP AEROB. DIGESTED LIQUID
X Z_!1 � 7
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

,ACILITY NAME: LUMBERTON, NC
)WNER: J T CAMPEN
iITE #: NC RO 00016 FIELD# : RO 00016 0017
tESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: WAGRAM
PERMIT #: WQ0000672 ANNUAL DRY TONS APPLIED: 18.43
OPERATOR: OZELL BAKER CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 6.00 ACRES PERMITTED: 6.00
Page
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
11/3/17
136,400.00 (G)
22733.333
3.24
3.071
FUAEDL
DRY
0- 1/2"
SUR
0.5
0.30
40,400. p
2,780.00 p
1,480.00 p
14156
BERMUDAGRASS, COASTAL
Nov-17
136,400.00 (G)
22,733.333
1
Total Gallons/Ac: 22,733.33
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annual lbs/acre
87
0.023
0.012
1.339
1.818
0.092
0.002
0.031
0.153
0.031
3.618 116.72
Cumulative lbs/acre
0.227
0.135
10.065
36.673
3.969
0.034
0.760
1 3.025
0.202
28.891
1
'ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop
', S
s f
'
i 1
!
s t
264
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 ! 375.0
89.0
2500.0 ;
.
7
LUAEDL = LUMBERTON, NC W WTP AEROB. DIGESTED LIQUID
X Z
e
(SIGNATURE OF LAND APPLIER) ' DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

FACILITYNAME: LUMBERTONNC
OWNER: J T CAMPEN
SITE #: NC RO 00016 FIELD#: RO 00016 001&
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: WAGRAM
PERMIT, #: W00000672 -ANNUAL DRY TONS APPLIED: 33.51
OPERATOR: OZELL BAKER CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 12.30 ACRES PERMITTED: 12.30
Page: 1
. Lime Applied
***
Date
LbdAc
3allons (G) or Cubic Yards'(CY)
Dry
Site
Inches
Appli-
Vola-
Miner-
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE -or
Per
Residual
, t,
DryWe
Past 24
Method
zation
zati6n
TKN
Nitrogen
and
(PPM)
Crop
-MONTH
Total
Per Acre
Solids
11 /6/17
248,000.00 (G)
20162.602
3.24
2.724
LUAEDL
DRY.
0-<1/2"
SUR
0.5
7.30
4Q400.p
2,780.00 P,
1,480.00 p
14156
BERMUDAGRASS, COASTAL
Nov-17,
248,000.00 (G)
20,162.602
Total Gallons/Ac: . 20,162.60
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P.
PAN
Annual lbs/acre
0.021'
0.011:
1.188
1.613-
0.082
:0.002
0.027
0.136.
0.027
3 - .209
103.52
77
Cumulative lbs/acre
0.258
.0.122
10.885
40.565
3.631
0.046
0.755
2.999
0.234
31.549
r:
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 264
.47
td
Fl) Cumulative Pollutant Loading Rate Limit (lbs/a e) 36.6 34.8 1339.0 267.9 4 15.0 375.0 89.0 2500.0
LUAEDL = LUMBERTON, NC WWTP AEROB. DIGESTED LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and -
.evaluated the information submitted. I am aware.that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA` Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg Volatilization Rate: Surface 0.5, Injection/Incor'p'o'r.ation 1.0
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

'ACILITY NAME: LUMBERTON, NC
)WNER: J T CAMPEN
11TE #: NC RO 00016 FIELD# : RO 00016 0019
MSIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: WAGRAM
PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 4.19
OPERATOR: OZELL BAKER CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 1.60 ACRES PERMITTED: 1.60
Page: 1
Lime Applied
***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
1116/17
31,000.00 (G)
19375.000
3.24
2.618
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
40,400. p
2,780.00 p
1,480.00 p
16
BERMUDAGRASS, COASTAL
Nov-17
1 31,000.00 (G)
19,375.000
1
Total Gallons/Ac: 19,375.00
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
74
0.020
0.010
1.141
1.550
0.079
0.002
0.026
0.130
0.026
3.084
99.47
Cumulative lbs/acre
0.134
0.117
7.017
35.736
2.388
0.020
0.375
2.253
0.150
22.778
'ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop
I
f 1�
1
7�
I
+ L
} 1
9
;
L 1 i 41t
' %
264
(lbs/acre)
FD Cumulative Pollutant LoadingRate Limit lbs/acre2500.0
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
LUAEDL = LUMBERTON, NC W WTP AEROB. DIGESTED LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/lcg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
?ACILITY NAME: LUMBERTON, NC PREDOMINANT SOIL SERIES: JOHNS
)WNER: CITY OF LUMBERTON (AIRPOR PERMIT #: WQ0000672 ANNUAL DRY TONS APPLIED: 43.56
;ITE #: NC RO 00017 FIELD# : RO 00017 0001 OPERATOR: DELOIS ALLEN CATION EXCHANGE CAPACITY (NON-503):
tESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 36.40 ACRES PERMITTED: 36.40
Page
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pp m)
Crop
Total
Per Acre
11/14/17
322,400.00 (G)
8857.143
3.24
1.197
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
40,400.p
2,780.00 p
1,480.00 p
14111
WHEAT
Nov-17
322,400.00 (G)
8,857.143
1
1
l otal Gallons/Ac: 8,857.14
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
34
0.009
0.005
0.522
0.708
0.036
<.001
0.012
0.060
0.012
1.410
45.47
Cumulative lbs/acre
0.099
0.045
6.267
11.884
1.906
0.021
0.636
1.111
0.090
10.154
'ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop
�'
;
; i
i ,'
106
r'
. 1
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 t 375.0
89.0
2500.0
LUAEDL = LUMBERTON, NC WWTP AEROB. DIGESTED LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent " p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Page: 1
FACILITY NAME: LUMBERTON, NC PREDOMINANT SOIL SERIES: L_UMBEE
OWNER: CITY OF LUMBERTON (AIRPOR PERMIT #: ' WQ0000672 ANNUAL DRY TONS APPLIED: 174.33
SITE #: NC RO 00017 FIELD# : RO 00017 0002. OPERATOR: DELOIS'ALLEN CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 25.40 ACRES PERMITTED: 25.40'
Lime Applied
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
-tili- ,
ali-
Ammonia -
Nitrate
p
DATE or
MONTH
Solids
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TIN
Nitrogen
and
(ppm)
Crop
Total
Per Acre
• 5/31/17
117,000.00 - (G)
8543.307
5.87
2.091
LUAEDL
MOIST:
0-<1/2"
SUR
0.5
0.30
25,500. p
3,060.00 p ,
,167.00 p .
8429
SOYBEANS
May-17
217,000.00 (G)
8,543.307
6/1/17
372,000.00- (G)
14645.669
5.87
3.585
LUAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
25,500. p _
3,060:00 p
167.00 p
8429
SOYBEANS
Jun-17
-372,000.00 (0)
14,645.669
11/30/17
167,400.00 (G).
6590.5511
3.24
0.890
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
40,400.p
2,780.00 p-
1,480.00p.
14156
WHEAT
Nov-17
167,400.00 (G)
6,590.551
-
12/1/17
55,800.00 .- (G)
2196.8501
3.24
0.297
LUAEDL
DRY
0-<1/2"
SUR
0.5.
0.30
40,400. p
2,780.00 p
1,480.00 p
14156
WHEAT
Dec-17
55,800.00 (G)
2,196.850

ACILITY NAME: LUMBERTON, NC
IWNER: ,CITY OF LUMBERTON (AIRPOR
ITE #: NC RO 00017 FIELD# : RO 00017 0002
J SIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: LUMBEE
PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 174.33
OPERATOR: DELOIS ALLEN CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 25.40 ACRES PERMITTED: 25.40
Page: 2
Lune Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
m
(pp )
Crop
p
Total
Per Acre
ioratvanons/Ac:
As.
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
P
PAN
TOTALS:
),nnuallbs/acre
F6.O64
96
0.043
0.027
2.527
4.177
0.191
0.005
0.069
0.346
0.069
260.81
34
Junmlative Ibs/acre
0.140
0.074
7.912
18.796
1.599
0.032
0.387
1.867
0.160
17.873
J
<_
ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop
I`
? 1'
_
71
!
j4,'T
174
t.
50
,D Cumulative Pollutant LoadingRate Limit Ibs/acre
( )
36.G
34.8
. < '
1339.0
267.9
'.
15.0 ) 375.0
89.0
2500.0 "
,UAEDL = LUMBERTON, NC WWTP AEROB. DIGESTED LIQUID
X ( /
r
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

FACILITY NAME: LUMBERTON, NC
OWNER: CITY OF LUMBERTON (AIRPOR
S= #: NC RO 00017 FIELD# : RO 00017 0003
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: LUMBEE
PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 224.99
OPERATOR: DELOIS ALLEN CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 28.00 ACRES PERMITTED: 28.00
Page : I
Lune Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (VM (specify)
oho
Tons
Cond.
Precip.
cation
tili-
ali- .
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
)
(pp-)
Crop
6/2/17
328,600.00 (G)
11735.714
5.87
2.873
LUAEDL
MOIST
0-<1/2"
SUR,
0.5
0.30
25,500.p
3,060.00 p
167.00 p
8429
SOYBEANS
6/3/17
210,800.00 (G)
7528.571
5.87
1.843
LUAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
25,500. p
3,060.00 p
167.00 p
8429
SOYBEANS
6/5/17
198,400.00 (G)
7085.714
5.87
1.734
LUAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
25,500. p
3,060.00 p
167.00 p
8429
SOYBEANS
Jun-17
737,800.00 (G)
26,349.999
11/29/17
229,400.00 (G)
8192.857
3.24
1.107
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
40,400. p
2,780.00 p
1,480.00 p
14156
I WHEAT
11/30/17
86,800.00 (G)
3100.000
3.24
0.419
LUAEDL
DRY
0-<I/2"
SUR
0.5
0.30
40,400. p
2,780.00 p
1,480.00 p
14116
WHEAT
Nov-17
316,200.00 (G)
11,292.857
12/1/17
12,400.00 (G)
442.8571
3.24
0.060
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
40,400. p
2,780.00 p
1,480.00 p
14156
WHEAT
Dec-17
12,400.00 (G)
442.857

'ACILITY NAME: LUMBERTON, NC
)WNER: CITY OF LUM13ERTON (AIRPOR
ITE #: NC RO '00017 FIELD# : RO 00017 0003
:ESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: LUMBEE
PERMIT #: WQ0000672 ANNUAL DRY TONS APPLIED: 224.99
OPERATOR: DELOIS ALLEN CATION EXCHANGE CAPACITY'(NON-503):
ACRES UTILIZED: 28.00 ACRES PERMITTED: 28.00
Page: 2
Lime Applied ***
Date:4
Lbs/Ac
alloiis (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TI4N
Nitrogen
and
(pprn)
Crop
MONTH
Total
Per Acre
Solids
Dotal Gallons/Ac: 38,085.71
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annuallbs/acre
109
0.051
0.032
2.975
4.886
0.224
0.006'
0.080
0.405
0.030
7.170 305.35
45
cumulative lbs/acre
0.083
0.051
4.857
7.216
0.337
0.010-
0.129
0.666
0.115
10.450
ermit PAN Limit Ibs/acre
( ) 1st Crop/2nd Crop
i ;
;
i
174
50
?D Cumulative Pollutant LoadingRate Limit Ibs/acre
( )
36.6
34.8
1339.0
2679
15.0 ), 375.0
89.0
3
2500.0
;UAEDL = LUMBERTON, NC WWTP AEROB. DIGESTED LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/lcg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

'ACILITY NAME: LUMBERTON, NC
)WNER: CITY OF LUMBERTON (AIRPOR
1TE #: NC RO 00017 FIELD# : RO 00017 0004
ZESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: JOHNS
PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 195.77
OPERATOR: DELOIS ALLEN CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 47.70 ACRES PERMITTED: 47.70
Page
Lune Applied ***
Date
Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry
Tons
per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
Per Acre
Solids
5/17/17
248,000.00 (G)
5199.161
5.87
1.273
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
25,500. p
3,060.00 p
167.00 p
8429
SOYBEANS
5/18/17
217,000.00 (G)
4549.266
5.87
1.114
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
25,500. p
3,060.00 p
167.00 p
8429
SOYBEANS
5/19/17
334,800.00 (G)
7018.868
5.87
1.718
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
25,500. p
3,060.00 p
167.00 p
8429
SOYBEANS
May-17
799,800.00 (G)
16,767.295
Total Gallons/Ac: 16,767.30
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual ibs/acre
69
0.025
0:016
1.453
2.512
0:112
0.003
0.041
0.208
0.041
3.374
155.96
Cumulative lbs/acre
0.181
0.090
9.408
30.932
1.862
0.020
0.502
1.905
0.149
19.804
'ermit PAN Limit (lbs/acre) Ist Crop/2nd Crop
I
a
i
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0 I
} 7
LUAEDL = LUMBERTON, NC W WTP AEROB. DIGESTED LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

FACILITY NAME: LUMBERTON,NC
DWNER: R G HAMMONDS
SITE #: NC RO 00020 FIELD# : RO 00020 0003
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: WAKULLA
PERMIT #: WQ0000672 ANNUAL DRY TONS APPLIED: 99.47
OPERATOR: R G HAMMONDS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 26.10 ACRES PERMITTED: 26.10
Page: I
Lime Applied ***
Date Lbs/Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
Per Acre
3/2/17
161,200.00 (G)
6176.245
4.58
1.180
LUAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
53,600. p
5,660.00 p
68.20 p
17280
I BERMUDAGRASS, COASTAL
3/3/17
266,600.00 (G)
10214.559
4.58
1.951
LUAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
53,600.p
5,660.00 p
68.20 p
17280
BERMUDAGRASS, COASTAL
3/4/17
93,000.00 (G)
3563.218
4.58
0.681
LUAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
53,600. p
5,660.00 p
68.20 p
17280
BERMUDAGRASS, COASTAL
Mar-17
520,800.00 (G)
19,954.022
1 MUL 1Td11U118/tic: 1J,Y34.uz
TOTALS:
i
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
132
0.041
0.015
1.494
1.776
0.124
0.003
0.038
0.200
0.038
2.881
125.00
Cumulative lbs/acre
0.185
0.076
6.036
11.738
0.818
0.029
0.239
1.294
0.165
19.888
-. 1
'ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop
147
!'
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 f 375.0
89.0
2500.0
LUAEDL = LUMBERTON, NC WWTP AEROB. DIGESTED LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/lcg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

�ACILITYNAME: LUMBERTON,NC
)WNER: R G HAMMONDS
ITE #: NC RO 00020 FIELD# : RO 00020 0004
:ESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: WAKULLA
PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 119.60
OPERATOR: R G HAMMONDS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 33.40 ACRES PERMITTED: 33.40
Page: 1
Lime Applied ***
Date Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Armnonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
Per Acre
Solids
3/6/17
204,600.00 (G)
6125.749
4.58
1.170
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
53,600. p
5,660.00 p
68.20 p
17280
I BERMUDAGRASS, COASTAL
3/7/17
266,600.00 (G)
7982.036
4.58
1.524
LUAEDL
DRY
0-<I/2"
SUR
0.5
0.30
53,600. p
5,660.00 p
68.20 p
17280
I BERMUDAGRASS, COASTAL
3/8/17
155,000.00 (G)
4640.719
4.58
0.886
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
53,600. p
5,660.00 p
68.20 p
17280
BERMUDAGRASS, COASTAL
Mar-17
626,200.00 (G)
18,748.504
Total Gallons/Ac: 18,748.50
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual Ibs/acre
124
0.038
0.014
1.404
1.669
0.117
0.003
0.036
0.188
0.036
2.707
117.45
Cumulative lbs/acre
0.286
0.094
7.917
16.715
1.216
0.040
0.350
1.914
0.215
29.038
'ermit PAN Limit (Ibs/acre) 1st Crop/2nd Cropl
` �',
: t
{
1
196
I
;4
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 s 375.0
89.0
2500.0
a
LUAEDL = LUMBERTON, NC. W WTP AEROB. DIGESTED LIQUID
X
(SIGNATURE OF LAND APPLIER)
DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for Imowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

'ACILITY NAME: LUMBERTON, NC
)WNER: ROBERT BASKERVILLE, JR
ITE #: NC RO 00028 . FIELD# : RO 00028 0001
MSIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: DUNBAR
PERMIT #: WQ0000672 ANNUAL DRY TONS APPLIED: 31.83
OPERATOR: CARNELL LOCKLEAR CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 11.60 ACRES PERMITTED: 11.60
Page: 1
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)-
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
10/27/17
24,800.00 (G)
2137.931
3.24
0.289
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
40,400. p
2,780.00 p
1,480.00 p
14156
WHEAT
10/31/17
130,200.00 (G)
11224.138
3.24
1.516
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
40,400. p
2,780.00 p
1,480.00 p
14111
WHEAT
Oct-17
155,000.00 (G)
13,362.069
11/1/17
80,600.00 (G)
6948.2761
3.24
r93
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
40,400. p
2,780.00 p
1,480.00 p
14156
WHEAT
Nov-17
80,600.00 (G)
6,948.276
1
1
Total Gallons/Ac: 20,310.34
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
—
Animal lbs/acre
78
0.021
0.011
1.196
1.625
0.082
0.002
0.027
0.137
0.027
3.233
104.28
cumulative lbs/acre
0.036
1 0.021
1 2.239
1 3.343
0.160
0.004
0.053
0.276
0.053
5.204
ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop
E
;
10
534.8
FD Cumulative Pollutant LoadingRate Limit lbs/acrej
(lbs/acre)
36.6'
1339.0
267.9
15.0 375.0
89.0
2500.0
LUAEDL = LUMBIRTON, NC WWTP AEROB. DIGESTED LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR =Not Reported or Not Required % = percent p = ppm or mg&g ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

'ACILITYNAME: LUMBERTON,NC
)WNER: ROBERT BASKERVILLE, JR
;ITE #: NC RO 00028 FIELD# : RO 00028 0003
tESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GOLDSBORO
PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 36.86
OPERATOR: CARNELL LOCKLEAR CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 10.40 ACRES PERMITTED: 10.40
Page
Lune Applied ***
Date
LWAc
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TI�I
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
Per Acre
Solids
10/26/17
192,200.00 (G)
18480.769
3.24
2.497
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
40,400.p
2,780.00 p
1,480.00 p
14156
I WHEAT
10/27/17
74,400.00 (G)
7153.846
3.24
0.967
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
40,400. p
2,780.00 p
1,480.00 p
14156
WHEAT
10/31/17
6,200.00 (G)
596.154
3.24
0.081
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
40,400. p
2,780.00 p
1,480.00 p
14156
WHEAT
Oct-17
272,800.00 (G)
26,230.769
Total Gallons/Ac: 26,230.77
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annual lbs/acre
100
0.027
0.014
1.545
2.098
0.106
0.003
0.035
0.176
0.035
4.175 134.67
Cumulative lbs/acre
0.027
0.014
1.545
2.098
1 0.106
0.003
0.035
1 0.176
0.035
4.175
'ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop
{'
_
136
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
4
1339.0
267.9
15.0 ! 375.0
89.0
2500.0 S
!
LUAEDL = LUMBERTON, NC WWTP AEROB. DIGESTED LIQUID
4/_
X J
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppmormg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
'J` Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

ACILITY NAME: LUMBERTON, NC
iWNER: QUINDALE BULLARD
ITE #: NC RO 00039 FIELD# : RO 00039 0004
'.ESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: LYNCHBURG
PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 21.51
OPERATOR: PATRICK BULLARD CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 14.80 ACRES PERMITTED: 14.80
Page: 1-
Lime Applied
***
Date
Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
Per Acre
Solids
8/15/17
186,000.00 (G)
12567.568
1.04
0.545
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
43,800.p
50.00 p .
21,000.01p
34165
I BERMUDAGRASS, COASTAL
8/16/17
310,000.00 (G)
20945.946
1.04
0.908
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
43,800.p
50.00 jn
21,000.01p
34165
BERMUDAGRASS, COASTAL
Aug-17
1 496,000.00 (G)
33,513.514
Total Gallons/Ac: 33,513.51
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
99
0.018
0.006
0.456
0.782
0.063
0.001
0.015
0.052
0.015
0.799
62.50
2umulative Ibs/acre
0.018
0.006
0.456
0.782
0.063
0.001
0.015
0.052
0.015
0.799
Y
ermit PAN Limit (Ibs/acre) 1st Crop/2nd Crop
Ir 1 y
237
?D Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
'
1339.0
267.9
7.
15.0 i 375.0
89.0
2500.0
-1
T)
:UAEDL = LUMBERTON, NC W WTP AEROB. DIGESTED LIQUID
X J % / .
(SIGNATURE OF LAND APPLIER) DATE / F
'Tcertify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, hijection/Incorporation 1.0
.r Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

?ACILITY NAME: LUMBERTON, NC
)WNER: PATRICK BULLARD
;ITE #: NC RO 00039 FIELD# : RO 00039 0009
2ESIDUAL SOURCE(S):* See list at bottom of report
f
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: WAGRAM
PERMIT #: WQ0000672 ANNUAL DRY TONS APPLIED: 62.11
OPERATOR: PATRICI{ BULLARD CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 62.50 ACRES PERMITTED: 62.50
Page: 1
Lune Applied ***
Date Lbs/Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
Per Acre
8/7/17
148,800:00 (G)
2380.800
1.04
0.103
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
43,800.p
50.00 p
21,000.01p
34165
I BERMUDAGRASS, COASTAL
8/8/17
297,600.00' (G)
4761.600
1.04
0.206
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
43,800.p
50.00 p
21,000.01p
34165
BERMUDAGRASS, COASTAL
8/9/17
378,200.00 (G)
6051.200
1.04
0.262
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
43,800.p
50.00 p
21,000.01p
34165
BERMUDAGRASS, COASTAL
8/10/17
279,000.00 (G)
4464.000
1.04
0.194
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
43,800.p
50.00 p
21,000.01p
34165
BERMUDAGRASS, COASTAL
8/11/17 -
254,200.00 (G)
4067.200
1.04
0.176
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
43,800.p
50.00 p
21,000.01p
34165
I BERMUDAGRASS, COASTAL
8/14/17
74,400.00 (G)
1190.400
1.04
0.052
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
43,800.p
50.00 p
21,000.01p
34165
BERMUDAGRASS, COASTAL
Aug-17
1,432,200.09 (G)
1 22,915.200
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
Annual Ibs/acre
68
0.012
0.004
0.312
0.535
0.043
<.001
0.010
0.036
0.010
0.547 42.73
cumulative lbs/acre
0.067
0.037
3.455
5.681
0.306
0.010
0.097
0.564
0.092
7.335
errriit PAN Limit (Ibs/acre) 1st Crop/2nd Crop
r
264
?D Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
! 1
1339.0
267.9
15.0 375.0
89.0
2500.0
[, s
:?
r
- i
,UAEDL = LUMBERTON, NC W WTP AEROB. DIGESTED LIQUID
X. z- t 1
/4
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

Summit Environmental Technologies, lhc.
3310 Win St.
FhArIROtJ6ii FlIItL3� 4E.OLOe1=S, 1ht0 Cuyahoga Falls, Ohio 44223
Arralyffcal LahomtofaPs TEL: [phone] FAX.- [phone]
Website: httn:/fwivtv.settekcon:
February 24, 2017
Chad M. Hayes
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Lumberton
Dear Chad M. Hayes:
Order No.: 17011492
Summit Environmental Technologies, Inc. received 1 sample(s) on 1/31/2017 for the
analyses presented in the following. report.
There were no problems with the analytical events associated with this report unless noted .
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you, have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
il-)�-
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Alabama 41600, Arkansas 88-0735, California 07256CA; Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia E87688, Idaho
OH00923, Illinois 200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3; Kentucky 90146, Louisiana 04061, Maryland
339, Massachusetts M-OPH923, Minnesota 409711, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North
Dakota R-201, Ohio Drinking Water 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon OH2O0001, Rhode Island LA000317, South Carolina 92016001,
Texas T1047044667I1-5, Region 8 8TMS-L, USDA/APHIS P330-11-00244, Utah OH00923201 1- 1, Vermont VT-87688, Virginia 00440 and 1581,
Washington C891, West Virginia 9957C
Page 1 of 40

_ Summit Environmental Technologies, Inc.
- sus"MIT 3310Win St. Case Narrative
ENVIRONMEWAL TECHNOLOGIES: Pte.. Cuyahoga Falls, Ohio 44223 WO#: 17011492
_ hp, lrry rcal Lishaaaporieq TEL: [phone] FAX: [phone]
Website: hM.-Ilwiviv.settek.com Date: 2/24/2017-
CLIENT: Synagro
Project: Lumberton
WorkOrder Narrative:
17011492: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit .
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not certified."
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received".or "wet weight" basis unless indicated as
"dry weight" using the %dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Prep Sample Comments:
17011492-OOIA 306581: Prep Comments for SVPrep_TCLP(8151), Sample 17011492-OOIA: Prep's
Prep Method hold time was exceeded.
Analytical Sequence QC Comments:
ccv-24115 1076184: Analytical Comments for svoc-cpest npw(8081), Sample ccv-24115, Batch ID
R65294 : The Pesticide Ending. CCV (24115/R65294) exhibited high recovery for Analyte: 4,4'-DDT;
4,4-DDT is not an Analyte of interest.
lcsd 1076609: Analytical Comments for tclp-VOC-MSTR_tclp(8260), Sample lcsd, Batch -ID R65312 :
The VOC LCSD exhibited high RPD for Vinyl chloride; This did not adversely impact the analysis. All
Original
Page 2 of 40

I
Summit Environmental Technologies, Inc. Case Narrative
3310 Win St.
iRVInOWMEKHALTZr-HUOLOG] FS, wq. Cuyahoga Falls, Ohio 44223 WO#: 17011402
Arraf rticaf Lsbaraiorie:, TEL: [phone] FAX. [phone]
Website: htto://wiviv.settekcom Date: 2/24/2017
CLIENT:, Synagro
Project: Lumberton
samples were ND.
BNA CCV 40ng 1076711: Analytical Comments for SVOC-MSTR_NPW(8270), Sample BNA CCV
40ng, Batch ID R65321 : The SVOC CCV (Batch R65321) exhibited outlying recoveries for numerous
analyes; All analytes of interest met Acceptance Criteria.
MB-25351 1076741: Analytical Comments for SVOC-BNA_TCLP(8270), Sample MB-25351, Batch
ID 25351 : The TCLP SVOC Method Blank (Batch 25351) exhibited high recoveries for Surrogate:
2,44,6-Tribromophenol and Surrogate: p-Terphenyl-d14.
Original
Page 3 of 40

Rai -
Summit Environmental Technologies, In Qualifiers and Acronyms
3310 Win 5
eia�LiC1NtAE 1TA.LS'E 3 idtSLantes, irtG. Cuyahoga Falls, Ohio4421 WO#: 17011492
AnHlyrfical LzboratQrfes TEL: [phone] FAX: [phone],
Website: hM.-1Avwiv.settek.co. Date: 2/24/2017
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported'value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recoveryfailed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low-(-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit,
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.,
Original
Page 4 of 40

Summit Environmental Technologies, Inc.
ram_ Workorder
Sum 3310 Win St.
ONVIftONMENTAL T€CHNOLOnjes, i t_ ' Cuyahoga Falls, Ohio 44223 Sample. Summary
_ tin -ail rical Labaralat'le5 TEL: [phone] FAX. [phone] WO#: 17011492
Website: huv.-1Avww.settekcon: 27-Feb-17
CLIENT: Synagro
Project: Lumberton
Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix
17011492-001 Lumberton VJWTP 1/30/2017 10:50:00 AM 1/31/2017 10:00:00 AM Sludge
Page 5 of 40

"-
Summit Environmental Technologies, Inc.
3310 Win St.
DATES REPORT
ENVIR J 14PIlENTA! rt C9id40L4Si155, INC.
Cuyahoga Falls, Ohio 44223
AralyHr,irf LeboratDtiog
TEL: [phone] FAX. [phone]
WO#: 17011492
Website: hgp://ivwiy.sette1ccom
27-Feb-17
Client:
Synagro
Project:
Lumberton ,
Sample ID
Client Sample ID Collection Date Matrix Test Name Leachate Date "
Prep Date Analysis Date
17011492-001A Lumberton WWTP 1/30/2017 10;50:00 AM Sludge Ignitability of Solids (SW-846: 1030)
2/1/2017 10:15:00 AM
pH (SW9045D)
2/2/2017 3:15:00 PM
Reactive Cyanide (9014/7.3.3.2)-Solid
2/1/2017 3:29:00 PM
Reactive Sulfide (9034)
2/1/2017 3:29:00 PM
SVOC.8270 TCLP BNA List 2/6/2017 3:54:19 PM
2/7/2017 8:00:00 AM 2/8/2017 6:24:00 PM
SVOC SW-846: 8081-TCLP Pesticide;2/6/2017 3:54:19 PM
2/8/2017 8:00:00 AM 2/8/2017 4:24:00 PM
SVOC SW-846: 8151 Herbicides-TCL2/6/2017 3:54:19 PM
2/22/2017 4:30:00 PM 2/23/2017 8:43:00 PM
SVOC SW-846: 8321 Herbicides-TCL
2/6/2017 12:58:00 PM
TCLP Mercury Analysis (1311/7470) 2/6/2017 3:54:19 PM
2/7/2017 11:00:00 AM. 2/7/2017 5:18:00 PM
TCLP Metals Analysis (6010) 2/6/2017 3:54:19 PM
2/7/2017 11:02:26 AM 2/7/2017 1:14:13 PM
VOC by GUMS (8260)-TCLP
2/8/2017 2:42:00 PM
Original
Page 6 of 40

Summit Environmental Technologies, Inc. Analytical Report
S U'M. MAI i or 3310 Win St.
ribt9ROYd 'PkL 3 =C; CdoLOGI ; Pkcq Cuyahogd Falls, Ohio 44223 (base report)
Analytical Lahnratorje5 TEL: [phone] FAX.• [phone] WO#: 17011492'
Website: h0.-1Avww.settekcom Date Reported: 2/24/2017
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 1/30/2017 10:50:00 AM
Lab ED: 17011492-OOIA
Project: Lumberton
Client Sample ID Lumberton WWTP
Analyses Result PQL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW7470A
SW7470A Analyst: ALJ
TCLP MERCURY ANALYSIS (131117470)
TCLP Mercury
ND
0.00200
mg/L
1
2/7/2017 5:18:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW6010C
SW3010A Analyst: VVK
TCLP METALS ANALYSIS (6010)
TCLP Arsenic(As)
ND
0.500
mg/L
1
217/2017 1:14:13 PM
TCLP Barium(Ba)
ND
5.00
mg/L
1
2/7/2017 1:14:13 PM
TCLP Cadmium(Cd)
ND
0.100
mg/L
1
2/7/2017 1:14:13 PM
TCLP Chromium(Cr)
ND
0.200
mg/L
1
2/7/2017 1:14:13 PM
f' TCLP Lead(Pb)
ND
0.500
mg/L
1
2/7/2017 1:14:13 PM
TCLP Selenium(Se)
ND
0.500
mg/L
1
2/7/2017 1:14:13 PM
TCLP Silver(Ag)
ND
0.500
mg/L
1
2/7/2017 1:14:13 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
8W8270C
SW351OC Analyst: CxA
SVOC 8270 TCLP BNA LIST
1,4-Dichlorobenzene
ND
0.0800
mg/L
2
• 2/8/2017 6:24:00 PM
2,4,5-Trichlorophenol
ND
0.200
mg/L
2
2/8/2017 6:24:00 PM
2,4,6-Trichlorophenol
ND
0.200
mg/L
2
2/8/2017 6:24:00 PM
2,4-Dinitrotoluene
ND
0.100
mg/L
2
2/8/2017 6:24:00 PM
Cresols, Total
ND
4.00
mg/L.
2
2/8/2017 6:24:00 PM
Hexachloro-1,3-butadiene
ND'
0.100
mg/L
2
2/8/2017 6:24:00 PM
Hexachlorobenzene
ND
0.100
mg/L
2
2/8/2017 6:24:00 PM
Hexachloroethane
ND
0.0800
mg/L
2
2/8/2017 6:24:00 PM
Nitrobenzene
ND
0.0800
mg/L
2
2/8/2017 6:24:00 PM
Pentachlorophenol
ND
0.200
mg/L
2
2/8/2017 6:24:00 PM
Pyridine
ND
0.200
mg/L
2
2/8/2017 6:24:00 PM ,
Surr: 2-Fluorophenol
73.2
10 - 109
%Rec
2
2/8/2017 6:24:00 PM
Surr: Phenol-d6
66.4
10 - 109
%Rec
2
2/8/2017 6:24:00 PM
Surr: Nitrobenzene-d5
78.1
19 - 120,
%Rec -
2
2/8/20W 6:24:00 PM
Surr: 2,4,6-Tribromophenol
105
10 - 120 ' •
%Rec
2
2/8/2017 6:24:00 PM
Surr: 2-Fluorobiphenyl
88.1
22 - 117
%Rec
2
2/8/2017 6:24:00 PM
Surr:_p-Terphenyl-dl4
113
34 - 116
%Rec
2
2/8/2017 6:24:00 PM
Qualifiers' H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected at the Reporting Limit PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit
W Sample container temperature is out of limit as specified at testcode
Original
Page 7 of 40

Summit Environmental Technologies, Inc.
Analytical Report
-
3310 Win St.
OiFtrlRllhlhlENY,AL3P1tt�Lt��tcs,��t'_'
Cuyahoga Falls, Ohio44223
(base report)
Anaiytisa; L:sbarafurle5
TEL: [phone] FAX: [phone]
WO#: 17011492
Website: hM.-1 vww.settek.com
Date Reported: 2/24/2017
CLIENT: Synagro
Tag Number:
Matrix: SLUDGE
Collection Date:
1/30/2017 10:50:00 AM
Lab ED: 17011492-001A
Project: Lumberton
Client Sample ID Lumberton WWTP
Analyses
Result
PQL
Qual Units
DF Date Analyzed
TCLP METALS, VOC, 8NA, PEST, HERB -SOLID
SW8081A
SW3510C Analyst: JBN
SVOC SW-846: 8081-TCLP PESTICIDES
Chlordane, total
ND
0.0100
mg/L
1 2/8/2017 4:24:00 PM
Toxaphene
ND
0.0200
mg/L
1 2/8/2017 4:24:00 PM
Endrin
ND
0.00100
mg/L
1 2/8/2017 4:24:00 PM
gamma-BHC
ND
0.00100
mg/L
1 2/8/2017 4:24:00 PM
Heptachlor
ND
0.00100
mg/L
1 2/8/2017 4:24:00 PM
Heptachlor epoxide
ND
0.00100
mg/L
1 2/8/2017 4:24:00 PM
Methoxychlor
ND
0.00100
d mg/L
1 2/8/2017 4:24:00 PM
Surr: TCMX
42.1
10 - 119
%Rec •
1 2/8/2017 4:24:00 PM
Surr: DCB
47.1
10 - 119
%Rec
1 2/8/2017 4:24100 PM
TCLP HERBICIDES ANALYSIS (SW846131118151)
SW8151A
SW8151A Analyst: JBN
SVOC SW-846: 8151 HERBICIDES-TCLP
2,4-D
ND
1.00
H mg/L
1 2/23/2017 8:43:00 PM
2,4,5-TP
ND
0.500
H mg/L
1 2/23/20,17 8:43:00 PM
Surr: DCAA
76.7
20 - 140
H %Rec
1 2/23/2017 8:43:00 PM
TCLP METALS, VOC, BNA, PEST,'HERB-SOLID
VOC BY GC/MS (8260)-TCLP
1,1-Dichloroethene :..
ND
1,2-Dichloroethane
ND
MEK
ND
Benzene
ND
Carbon tetrachloride
ND
Chlorobenzene
ND
Chloroform
ND
Tetrachloroethene
ND
Trichloroethene
ND
Vinyl chloride
ND
Surr: 4-Bromofluorobenzene
90.6
Surr: Dibromofluoromethane
97.3
Surr: Toluene-d8
104
SW8260B
Analyst: MES
0.100
mg/L
1
2/8/2017 2:42:00 PM
0.100
mg/L
1
2/8/2017 2:42:00 PM
2.00 .
mg/L
1
2/8/2017 2:42:00 PM
0.100
mg/L
1
2/8/2017 2:42:00 PM
0.100
mg/L
1
2/8/2017 2:42:00 PM
0.100
mg/L
1
2/8/2017 2:42:00 PM
0.100
mg/L
1
2/8/2017 2:42:00 PM
0.100
mg/1_
1
2/8/2017 2:42:00 PM
0.100
mg/L
1
2/8/2017 2:42:00 PM
0.200
mg/L
1
2/8/2017 2:42:00 PM
70 - 130
%Rec
1
2/8/2017 2:42:00 PM
70 - 130
%Rec
1
2/8/201-7 2:42:00 PM
70 - 130
%Rec
1
2/8/2017 2:42:00 PM
Quahllers'• H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected at the Reporting Limit PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit
W Sample container temperature is out of limit as specified at testcode
Original
Page 8 of 40

•-_ Summit Environmental Technologies, St.
331010 Win St.
I-SUMIT
Analytical Report
f� V1R0t4h1SW'rAL1-2CPNOLOGIES?WQQ
T
CuyahogaFalls,'Ohio44223
(base report)
Analyffoaf Laboraiories TEL: (330)
253-8211,FAX.• [phone]
WO#: 17011492
Website:,h9R.-1 tvivtv.settekcom
Date Reported: 2/24/2017
CLIENT: Synagro
Tag Number:
Matrix: SLUDGE
Collection Date:
1/30/2017 10:50:00 AM
Lab ID: 17011492-001A
Project:" Lumberton
Client Sample ID Lumberton WWTP
Analyses Result
PQL Qual Units
DF Date Analyzed
RCI
SW9014
Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive. ND
0.500 mg/Kg
1 2/1/2017.3`:29:00 PM
IGNITABILITY OF SOLIDS (SW-846: 1030)
SW1030
Analyst: RMT
Ignitability Non-flammable..
1 2/1/2017 10:15:00 AM
RCI
SW9045D
:Analyst: DHC
PH (8W9045D)
pH 6.8
s.u.@20.6C
1 2/2/2017 3:15:00 PM
-RCI
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)
Sulfide, Reactive ND
25.0 mg/Kg
1 - 2/1/2017 3:29:00 PM
Qualifiers' H Holding times for preparation or analysis exceeded M ManualTntegrationused todetermine area response
_ ND Not Detected at the Reporting Limit PL Permit Limit
R. RPD outside accepted recovery limits RL Reporting Detection Limit -
W Sample container temperature is out oflimit as specified at testcode
Original
Page 9 -of 40

Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
5
tMINVIwrPv N IAI,. r t �:¢1taoLct ��s, r r, Cuyahoga Falls, Ohio 44223 WO#: 17011492
a'1, taiytl:caP '17baartPgfile TEL: [phone] FAX.- [phone]
Website: hgp.-Mwww.settelccom 27-Feb-17
Client: Synagro
Project:. Lumberton BntchID: 25347
Sample ID MB-25347 -.
SampType: MBLK,
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 2/7/2017
RunNo: 65248
Client ID: PBW
Batch ID: 25347
TestNo: SW6010C SW3010A
Analysis Date: 2/7/2017
SegNo: 1075536
Analyte
Result'
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val .
%RPD . RPDLimit Qua]
TCLP Arsenic(As)
ND
0.500
TCLP Barium(Ba)
ND
5.00
TCLP Cadmium(Cd)
ND
0.100
TCLP Chromium(Cr)
ND
0.200..
TCLP Lead(Pb)
ND
0.500
TCLP Selenium(Se)
ND
0.500
TCLP Silver(Ag)
ND
0.500
Sample ID LCS-25347
SampType: LCS
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 2/7/2017
RunNo: 65248 -
Client ID: LCSW
Batch ID: 25347
TestNo: SW6010C SW3010A
Analysis Date:' 2/7/2017
SegNo: 1075637
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
2.15
0.500
2.000
.0
108
TCLP Barium(Ba)
ND
5.00
2.000
0
110
TCLP Cadmium(Cd)
2.22
0.100.
2.000
0 _
ill
TCLP Chromium(Cr)
2.19,
0.200
2.000
0
110
TCLP Lead(Pb)
2.18
0.500.
2.000
0
109
TCLP Selenium(Se)
2.23
0.500'
2.000
0
112
TCLP Silver(Ag)
1.08.
0.500
1.000
0
108
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
80
120
80,
in
80
120
80
120
80
120
80
120
80
120
B 'Analyte detected in the associated Method Blank E Value above quantitation range
J Analyte detected below quantitation limits M Manual Integration used to determine
ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
PL Permit Limit R RPD outside accepted recovery limits
Page 10 of 40

S�f
I�'�J6
Sumnsit Environmental Tech w1ogies, lrtc.
3310 Win St.
QC SUMMARY REPORT
L-NIVIx[�INN ah. A a:a HF49LDGI . sNC.
Cuyahoga Falls, Ohio 44223
WO#: 17011492
R},rwlyrn,r,aP f b,prw#orl �
TEL: (330)' 253-8211 FAX.- [phone]•
Website: ham://www.settelc.con:
27-Feb-17
Client:
Synagro
Project:
Lumberton
BatchID: ..25347-
Sample ID' 17011327-001AMS
SampType: MS
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 21W2017
RunNo: 65248
Client ID: BatchQC
Batch ID: 25347
TestNo: SW6010C SW3010A
Analysis Date: 2/7/2017
SegNo: 1075539
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit , RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
2.56
0.500
2.000
0
128
70
130
TCLP Barium(Ba)
ND
5.00
2.000
0.3300
108
70
130
TCLP Cadmium(Cd)
2.39
0.100
2.000
0
120
70
130
TCLP Chromium(Cr)
2.30
0.200
2.000
0
115
70
130
TCLP Lead(Pb)
2.43
0.500
2.000
0
122
70
130
TCLP Selenium(Se)
2.79
0.500
2.000
0
140
70
130 S
TCLP Silver(Ag)
1.22
0.500
1.000
0
122
70
130
Sample ID 'I7011327-001AMSD
SampType: MSD
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 2/7/2017
RunNo: 65248
Client ID: BatchQC
Batch ID: 25347
TestNo: SW6010C SW3010A
Analysis Date: 2/7/2017
SegNo: 1075540
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
2.50
0.500
2.000
0
125
70
130
2.560
2.37
20
TCLP Barium(Ba)
ND
5.00
2.000
0.3300
108
70
-130
0
0
20
TCLP Cadmium(Cd)"
2.38
0.100
2.000 -
0
119
70
130
2.390
0.630
_20
TCLP Chromium(Cr)
2.30
0.200
2.000
0
115
70
130
2.300
0
20
TCLP Lead(Pb)
2.44
0.500
2.000
0
122
70
130
2.430
0.411
20
TCLPSelenium(Se)
2.80
0.500
2.000
0
140
70
130
2.790
0.358
20 S
TCLP Silver(Ag).
- 1.22
0,.500
1.000'
0
122
70
130
1.220,
0.411'
20
Qualifiers: k Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 11 of 40

m 1
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
__
IrcU+'N IAI.. I hCHNULOGI3 -S, JPtC,
�1.r�tds{2t�u�l L�rhp,r,�taFies
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
WO#: 17011492
Website: http:/bvivw.settelc.coni
27-Feb-17
Client:
Synagro
Project:
Lumberton
BatchID• 25351
Sample ID MB-25351
SampType: MBLK
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 2/7/2017
RunNo: 65321
,lient ID: PBW
Batch lb:. 25351
TestNo: SW8270C SW3510C
Analysis Date: 2/8/2017
SegNo: 1076741
\nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
ND
0.0200
2,4,5-Trichlorophenol
ND
0.0500
2,4,6-Trichlorophenol
ND
0.0500
2,4-Dinitrotoluene
ND
0.0100
Cresols, Total
ND
1.00
Hexachloro-1,3-butadiene
ND
0.00400
Hexachlorobenzene
ND
0.0100
Hexachloroethane
ND
0.0200
Nitrobenzene
ND
0.0200
Pentachlorophenol
ND
0.0500
Pyridine '
ND
0.0500
Surr: 2-Fluorophenol
0.428
Surr: Phenol-d6
0.415
Surr` Nitrobenzene-d5
0.440
Surr: 2,4,6-Tribromophenol
0.647
Surr: 2-Fluorobiphenyl
0.476
Surr: p-Terphenyl-d14
0.683
0.5000
85.6
10
109
0.5000
83.1
10
109
0.5000
88.0
19
120
0.5000
129
10
120 S
0.5000
95.2
22
117
0.5000
137
34
116 S
Sample ID LCS-25351
SampType: LCS
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 2/7/2017
RunNo: 65321
Client ID: LCSW
Batch ID: 25351
TestNo: SW8270C SW3510C
Analysis Date: 2/8/2017
SegNo: 1076742
Anaiyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to detennine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 12 of 40

sumian
Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
t-AlIRUVT NN IAl.. w U+. HNULttc3ihS, JKG. Cuyahoga Falls, Ohio 44223
Anall-Waal Laboratories, TEL: [phone] FAX.- [phone] WO#: 17011492
Website: hgp.-Ilwww.settelc.com 27-Feb-17
CIient: Synagro
Project: Lumberton BatchID: 25351
Sample ID LCS-25351
SampType: LCS
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 2/7/2017
RunNo: 65321
client ID: LCSW
Batch ID: 25351
TestNo: SW8270C SW3510C
Analysis Date: 2/8/2017
SegNo: 1076742
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.151
0.0200
0.2000
0
75.7
19.1
126
2,4,5-Trichlorophenol
0.170
0.0500
0.2000
0
'85.0
11.7
151
2,4,6-Trichlorophenol
0.170
0.0500
0.2000
0
85-.0
12.4
150
2,4-Dinitrotoluene
0.214
0.0100
0.2000
0
107
20.6
140
Cresols, Total
ND
1.00
0.40D0
0
78.1
10
129
Hexachloro-1,3-butadiene
0.154
0.00400
0.2000
0
77.1
14.7
137
Hexachlorobenzene
0.205
0.0100
0.2000
0
103
12
139
Hexachloroethane
0.143
0.0200
0.2000
0
71.7
14.8
132
Nitrobenzene
0.160
0.0200
0.2000
0
80.1
15.6
138
Pentachlorophenol
0.150
0.0500
0.2000
0
.75.2
10
156
Pyridine
0.0798
0.0500
0.2000
0
39.9
10
126
Surr: 2-Fluorophenbl
0.305
0.5000
60.9
10
147
Surr: Phenol-d6
0.321
0.5000
64.2
10
140
Surr: Nitrobenzene-d5
0.419
0.5000
83.8
10
169
Surr: 2,4,6-Tribromophenol
0.479
0.5000
95.7
10
185
Surr: 2-Fluorobiphenyl
0.476
0.5000
95.2
10
169
Surr: p-Terphenyl-d14
0.651
0.5000
130
10
179
Sample ID 17011498-001AMS
SampType: MS
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 2/7/2017 -
RunNo: 65321
Client ID: BatchQC
Batch ID: 25351
TestNo: SW8270C SW3510C
Analysis Date: 2/8/2017
SegNo: 1076744-
Analyte
Result
PQL SPK value SPK Ref Val
%oREC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is'below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 13 of 40

Summit Environmental Technologies, Inc.
g 3310 Win St. QC SUMMARY REPORT
LeavIKvirirAL-NIALRWZHWULatWzS.,IN . Cuyahoga Falls, Ohio44223 WO#: 17011492
Anattr2i;rAf TEL: [phone] FAX.- [phone]
Website: http.-Mvww.seue1acom 27-Feb-17
Client: Synagro
Project: Lumberton BatchlD: 25351
Sample ID 17011498-001AMS
SampType: MS
TestCode: SVOC-BNA T Units: mg/L
Prep Date: ' 2/7/2017
RunNo: 66321
:lient ID: BatchQC
'Batch ID: 25351
TestNo: SW8270C SW3510C
Analysis Date: 2/8/2017
SegNo: 1076744
\nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.393
0.0800
0.4000
0
98.2
29
112
2,4,5-Trichlorophenol
0.532
0.200
0.4000
0
133
53
123
S
2,4,6-Trichlorophenol
0.524
0.200
0.4000
0
131
50
125
S
2,4-Dinitrotoluene
0.460
0.0400
0.4000
0
115
57
128
Cresols, Total
ND
4.00
0.8000
0
103
20
125
Hexachloro-1,3-butadiene
0.396
0.0160
0.4000
0-
99.0
22
124
Hexachlorobenzene
0.464
0.0400
0.4000
0
116
53
125
Hexachloroethane
0.380
0.0800
0.4000
0
95.1
21
115
Nitrobenzene
0.518
0.0800
0.4000
0
130
45
121
S
Pentachlorophenol
0.397
0.20b
0.4000
0
99.3
35
138
Pyridine
ND
0.200
-0.4000
0
22.7
10
126
QMR
Surr. 2-Fluorophenol
0.762
-1.000
76.2
10
147
Surr: Phenol-d6
0.741
1.000
74.1
10
140
Surr: Nitrobenzene-d5
0.786
1.000
78.6
10
169
Surr: 2,4,6-Tribromophenol
0.995
1.000
99.5
10
185
Surr: 2-Fluorobiphenyl
0.912
1.000
91.2
10
169
Surr: p-Terphenyl-d14
1.14
1.000
114
10
179
Sample ID 17011498-001AMSD
SampType: MSD
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 217/2017
RunNo: 65321
Client ID: BatchQC
Batch ID: 25351
TestNo: SW8270C SW3510C
Analysis Date: 2/8/2017
SegNo: 1076745
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: k Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 14 of 40

• ;
I
SITummit Environmental Technologies, Inc.
33LO Wits St.
QC SUMMARY REPORT
+-IrsVNrAI N JAI, P S:d:•HNULDi: IES, AMC Cuyahoga Falls, Ohio 44223
Arw11,Pbc-P C Th, pratorip� .' TEL: [phone] FtIX.• [phone]
WO#: 17011492
Website: http:/hvww.settelc.com
27-Feb-17
Client:
Synagro
Project:
Lumberton
BatchID: 25351
Sample ID 17011498-001AMSD
SampType: MSD
TestCode: SVOC-BNAi T Units: mg/L
Prep Date: 2/7/2017
RunNo: 65321,
Client ID: BatchQC
Batch ID: 25351
TestNo: SW8270C SW3510C
Analysis Date: 2/8/2017
SegNo: 1076746
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.359
0.0800
0.4000
0
89.8
29
112
0.3928.
8.94
30
2,4,5-Trichlorophenol
0.498
0.200
0.4000
0
125
53
123
0.5320
6.52
30 S
2,4,6-Trichlorophenol
0.486
0.200
0.4000
0
122
50
125
0.5236
7.37
30
2,4-Dinitrotoluene
0.436
0.0400
0.4000
0
109
57
128
0.4604
5.35
30
Cresols, Total
ND
4.00
0.8000
0
97.4
20
125
0
0
30
Hexachloro-1,3-butadiene
0.357
0.0160
0.4000'
0
89.3
22
124
0.3960
10.3
30
Hexachlorobenzene
0.427
0.0400
0.4000
0
107
53
125
0.4640
8.26
30
Hexachloroethane
0.350
0.0800
0.4000
0
87.6
21
115
0.3804
8.21
30
Nitrobenzene
0.480
0.0800
0.4000
0
120
45
121
.0.5180
7.62
30
Pentachlorophenol
0.391
0.200
-0.4000
0
97.8
35
138
0.3972
1.52
30 m
Pyridine
ND
0.200
0.4000
0
44.5
10
126
0
0
30 R
Surr: 2-Fluorophenol
0.734
1.000
73.4
10
147
0
Surr: Phenol-d6
0.756
1.000
75.6
10
140
0
Surr: Nitrobenzene-d5
0.786
1.000
78.6
10
169
0
Surr: 2,4,6-Tribromophenol
1.0D
1.000
100
10
185
0
Surr: 2-Fluorobiphenyl
0.907
1.000
90.7
110
169
0
Surr: p-Terphenyl-d14
1.11
1.000
ill
10
179
0
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits •M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirniation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 15 of 40

swilva"1121
Summit Environmental Technologies,Inc.QC SUMMARY REPORT
3310 Win St.
cry lHrJ!NN4N IAl.. I hi.; NULU€M S, arks, Cuyahoga Falls, Ohio 44223
a�rPat M-=T C Iaca,r,�to,riF�y TEL: [phone] FAX.- [phone] WO#: 17011492
Website: http:/hvivw.settelaconz 27-Feb-17
Client: Synagro
Project: Lumberton BatchID: 25358
Sample ID MB-25358
SampType: MBLK
TestCode: HG TCLP(74 Units: PPM
Prep Date: 2/7/2017
RunNo: 65223
Client ID: PBW
Batch ID: 25358
TestNo: SW7470A SW7470A
Analysis Date: 2/7/2017
SegNo: 1075037
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury ND 0.00200
Sample ID LCS-25358
SampType: LCS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 2/7/2017
RunNo: 65223
Client ID: LCSW
Batch ID: 25358
TestNo: SW7470A SW7470A
Analysis Date: 2/7/2017
SegNo: 1075038
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00417 0.00200 0.00400 0 104 80 120
Sample ID 17011496-001AMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 2/7/2017
RunNo: 65223
Client ID: BatchQC
Batch ID: 25358
TestNo: SW7470A SW7470A
Analysis Date: 2/7/2017
SegNo: 1076042
Analyte
Result
PQL SPK value SPK Ref Val
%REC ' Lowl-imit , HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00390 0.00200 0.00400 0 97.5 75 125
Sample ID 17011496-001AMSD SampType: MSD TestCode: HG_TCLP(74 Units: PPM Prep Date: 2/7/2017 RunNo: 65223
r
Client ID: BatchQC Batch ID: 25358 TestNo: SW7470A SW7470A Analysis Date: 2/7/2617 SegNo: 1075043
Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit- Qual
TCLP Mercury 0.00390 0.00200
0.00400 0 97.5 75
125
0.00390 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M
Manual Integration used to determine
MC Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit Original
P Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits
Page 16 of 40

Summit Environmental Technologies, Inc.QC
3310WinSt.trVOWsuU''VAMIlt
SUMMARY REPORT
NrnUN IAA- s rtirutaoLcttm�ts, INC.Cuyahoga
Falls, Ohio 44223
WO#: 17011492
Anai`yifraf Lsrbar�trrriE?4
TEL: [phone] FAX. [phone]
Website: hQ.lwww.settelccom
27-Feb-17
Client:
Synagro
Project:
Lumberton
BatchID: 25358
Sample ID 17011496-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 2/7/2017
RunNo: 65223
;lient ID: BatchQC
Batch ID: 25358
TestNo: SW7470A SW7470A
Analysis Date: 2/7/2017
SegNo: 1075043
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
-%RPD RPDLimit Qual
QuafiCers: * Value exceeds Maximum Contaminanf Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded 1 Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD'is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 17 of 40

surmalor
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
L-rVlKW1G1UNIAl- IL-4l:l%t4uLtJ31WS,INC.
Cuyahoga Falls, Ohio44223
r� nakF,R,r, of L.7borgiarffS,5 TEL: [phone] FAX. [phone]
WO#: 17011492
Website: http://lvww.settelcconi
27-Feb-17
Client:
Synagro
Project:
Lumberton
BatchED: 25379
Sample ID mb-25379
SampType: mblk
TestCode: tclp-svoc-cpe Units: mg/L
Prep Date: 2/8/2017
RunNo: 65294
client ID: PBW
Batch ID: 25379
TestNo: SW8081A SW3510C
Analysis Date: 2/8/2017
SegNo: 1076186
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, total
ND
0.00500
Toxaphene
ND
0.0100
Endrin
ND
0.000500 d
gamma-BHC
ND
0.000500
Heptachlor
ND
0.000500
Heptachlor epoxide
ND
0.000600
Methoxychlor
ND
0.000500 d
Surr: T.CMX
5.13
10.00 51.3 10 119
Surr: DCB
8.00
10.00 80.0 10 119
Sample ID Ics-25379
SampType: Ics
TestCode: tclp-svoc-cpe Units: mg/L
Prep Date: 2/8/2017
RunNo: 65294
;lient ID: LCSW
Batch ID: 25379
TestNo: SW8081A SW3510C
Analysis Date: 2/8/2017
SegNo: 1076187
Malyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
0.00517
0.000500
0.00500
0
103
20
157
gamma-BHC
0.00406
. 0.000500
0.00500
0
81.3
22
137
Heptachlor
0.00454
0.000500
0.00500
0
90.8
24
121
Heptachlor epoxide
0.00427
0.000500
0.00500
0
85.4
27
152
Methoxychlor
0.00723
0.000500
0.00500
0
145
10
199
Surr: TCMX
7.53
10.00
75.3
10
119
Surr: DCB
10.2
10.00
102
10
119,
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 18 of 40

surnmur
Summit Environmental Technologies,Inc. QC SUMMARY REPORT
3310 Win St.
L- +�I VINNI:IVI .I. I'Ll:KNULUU1; PiG. Cuyahoga Falls, Ohio 44223
AnatvilmT tabo,rwtncico TEL: [phone] FAX. [phone] WO#: 17011492
Website: http://wivw.settelc.com 27-Feb-17
Client: Synagro
Project: Lumberton BatchID: 25379
Sample ID 17011492-001ams
SampType: ms
TestCode: tclp-svoc-cpe Units: mg/L
Prep Date: 2/8/2017
RunNo: 65294
Client ID: Lumberton WWTP
Batch ID: 25379
TestNo: SW8081A SW351DC
Analysis Date: 2/8/2017
SegNo: 1076188
Analyte . '
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDL]mit Qua]
Endrin
0.00728
0.00100
0.0100
0
72.8
20
157
gamma-BHC
0.0059D
0.00100
0.0100
0
59.0
22
137
Heptachlor
0.00638
0.00100
0.0100
0
63.8
24
121
Heptachlor epoxide
0.00612 '
0.00100
0.0100
0
61.2
27
152
Methoxychlor
0.0103
0.00100
0.0100
0
103
10
199
Surr: TCMX
9.59
20.00
48.0
10
119
Surr: DCB
14.3
20.00
71.4
10
119
Sample ID 17011492-001amsd
SampType: msd
TestCode: tclp-svoc-cpe Units: mg/L
Prep Date: 2/8/2017
RunNo: 65294
Client ID: Lumberton WWTP
Batch ID: 25379
TestNo: SW8081A SW3510C
Analysis Date: 2/8/2017
SegNo: 1076189
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
0.00749
0.00100
0.0100
0
74.9
20
157
0.00728
2.89
30
gamma-BHC
0.00618
0.00100
0.0100
0
61.8
22
137
0.00590
4.66
30
Heptachlor
0.00659
0.00100
0.0100
0
65.9
24
121
0.00638
3.19
30
Heptachlor epoxide
0.00647
0.00100
0.0100
0
64.7
27
152
0.00612
5.67
30
Methoxychlor
0.0104
0.00100
0.0100
0
104
10
199
0.0103
1.57
30
Surr: TCMX
10.2
20.00
51.0
10
119
0
Surr: DCB
13.0
20.00
65.0
10
119
0
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 19 of 40

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
tCSV1KVtN61I:NIN. IL-9.:HNULOG1�S,JKC. Cuyahoga Falls, Ohio44223
msumialar
3310 Win St.
,<1!13fyP1:i:aP Lattar9torie;, TEL: [phone] FAX.- [phone]
WO#: 17011492
Website: hqp.-11iv1vw.sette1ccom 27-Feb-17
Client: Synagro
Project: Lumberton BatchID: 25636
Sample ID mb-25636
SampType: mbik
TestCode: tclp-svoc-her Units: mg/L
Prep Date: 2/22/2017
RunNo: 66032
Client ID: PBW
Batch ID: 25636 -
TestNo: SW8151A SW8151A
Analysis Date: 2/23/2017
SegNo: 1088535
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D ND 1.00 0 0
2,4,5-TP ND 0.500 0 0
Surr: DCAA 291 500.0 58.2 20 140
Sample ID Ics-25636
SampType: Ics
TestCode: tclp-svoc-her Units: mg/L
Prep Date: 2/2212017
RunNo: 66032
Client ID: LCSW
Batch ID: 25636
TestNo: SW8151A SW8161A
Analysis Date: 2/23/2017
SegNo: 1088536
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
2,4-D
ND
1.00 0.500
0 84.9
62.6
125
2,4,5-TP
ND
0.500 0.500
0 80.1
52.5
128
Surr: DCAA
468
500.0
93.5
20
140
Sample ID 17011333-009ams
SampType: ms
TestCode: tclp-svoc-her Units: nag/L
Prep Date: 212212017
RunNo: 66032
Client ID: BatchQC
Batch ID: 25636
TestNo: SW8151A SW8151A
Analysis Date: 2/23/2017
SegNo: 1088537
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
ND 1.00
0.500 0 91.8 37
105
HQMR
2,4,5-TP
ND 0.500
0.500 0 85.9 38
106
HQMR
Surr: DCAA
1310
500.0 261 20
140
SH
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H
MC
Holding times for preparation or analysis • exceeded
Value is below Minimum Compound Limit.
J Analyte detected below quantitation limits
ND. Not Detected at the Reporting Limit
M
0
Manual Integration used to determine
RSD is greater than RSDlimit
Original
P
Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits
Page 20 of 40

MIT Summit Environmental Technologies,Inc.Sum, QC SUMMARY REPORT
3310 Win in St.
er.v1MVNrALN1A1.IW;H?4taLUUJ!::S,aetc•. Cuyahoga Falls, Ohio44223
At T81�2dcaP Crabpr,�toFes TEL: [phone] FAX: [phone] WO#: 17011492
Website: http://lvivw.settelc.cQn 27-Feb-17
Client:
i Synagro
Project:.
i Lumberton
BatchID:
25636
Sample ID
17011333-009amsd
SampType: msd
TestCode: tclp-svoc-her
Units: mg/L
Prep Date:
2/22/2017
RunNo: 66032
Client ID:
1 BatchQC
Batch ID: 25636
TestNo: SW8151A
SW8151A
Analysis Date:
2/23/2017
Seq'No: 1088538
Analyte
Result
PQL SPK value SPK Ref Val
%REC
LowLimit Highl-imit
RPD Ref Val'
%RPD RPDLimit
Qual
2,4-D
I
ND
1.00 0.500
0
61.7
37
105 0
0 30
RH
2,4,5-TP
I
ND
0.500 0.500
0
52.3
38
106 0
0 30
RH
Surr: DCAA
i
843
500.0
169
20
140
0
SH
Qualifiers: k Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit - R RPD outside accepted recovery limits
Page 21 of 40

Summit Environmental Technologies, Inc.. QC SUMMARY REPORT
R1 zui"&IT 3310 Win St.
tcV1HVEwrneNIRl.1TA;HW1cauos:ar;a.rrKC. Cuyahoga Falls, Ohio44223
Ana'Ylfcr7f CrTlaor�toFleS TEL: [phone] FAX.' [phone] WO#: 17011492
Website: http://ivwiv.settekcom 27-Feb-17
Client: Synagro
Project: Lumberton BatchID: R64993
Sample ID 17010155-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 64993
Client ID: BatchQC
Batch ID: R64993
TestNo: SW1030
Analysis Date: 2/1/2017
SegNo: 1070888
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Ignitability ]on -flammable. 0 0 20
Sample ID 17010165-001ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 64993
Client ID: BatchQC
Batch ID: R64993
TestNo: SW1030
Analysis Date: 2/1/2017
SegNo: 1070889
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Ignitability lon-flammable. 0 0 20
Sample ID 17010155-002ADUP
-SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 64993
Client ID: BatchQC
Batch ID: R64993
TestNo: SW1030
Analysis Date: 2/1/2017
SegNo: 1070891
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability Ion -flammable. 0 0 20
Sample ID 17010155-002ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 64993
Client ID: BatchQC
Batch ID: R64993
TestNo: SW1030
Analysis Date: 2/1/2017
SegNo: 1070892
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability Ion -flammable. 0 0 20
Qualifiers: :k Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 22 of 40

�1
i
R1
SuA414111-
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
m ,V1X[d=r•+rniaN IAl. I M;d9tarat.vut.-S, JP� .
Cuyahoga Falls, Ohio 44223
WO#: 17011492
Ax4:r15tU=1 C�r2a.ar �tnFlea
TEL: [phone] FAX.- [phone]
Website: hup:/hvww.settelc.com
27-Feb-17
Client:
Synagro
Project:
Lumberton
BatchED: R64993
Sample ID 17010166-002ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 64993
Client ID: BatchQC
Batch ID: R64993
TestNo: SW1030
Analysis Date: 2/1/2017
SegNo: 1070892
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sample ID 17010184-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 64993
Client ID: BatchQC
Batch ID: R64993
TestNo: SW1030
Analysis Date: 2/1/2017
SegNo: 1070894
Analyte
Result .
PQL SPK value SPK Ref Val
%REC Lowl-imit - HighLimit RPD Ref Val
%RPD RPDLimit Qual
gnitability Jon -flammable. 0 0 20
Sample ID 17010184-001ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 64993
Client ID: BatchQC
Batch ID: R64993 '
TestNo: SW1030
Analysis Date: 2/1/2017
SegNo: 1070895
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
ignitability Jon -flammable. 0 0 20
Sample ID 17010235-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 64993
Client ID: BatchQC
Batch ID: R64993
TestNo: SW1030
Analysis Date: 2/1/2017
SegNo: 1070897
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability Ion -flammable. 0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds. PL Permit Limit R RPD outside accepted recovery limits
Page 23 of 40

' a IT Summit Environmental Technologies, Q C SUMMARY REPORT
' 3310 10 Win
St
n St.
r NN11-1VINTPINN I Al.. 11;t;H-0ULUCn:s, aPiQ Cuyahoga Falls, Ohio 44223 WO#: 17011492
&WINr f Lzboxalo io6 TEL: [phone] FAX.' [phone]
Wehsite: htty://wivw.settelcconz 27-Feb-17
Client: Synagro
Project: Lumberton BatchID: R64993
Sample ID 17010235-001ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 64993
Client ID: BatchQC
Batch ID: R64993
TestNo: SW1030
Analysis Date: 2/1/2017
SegNo: 1070898
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Ignitability Ion -flammable. 0 0 20
Sample ID 17010900-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 64993
Client ID: BatchQC
Batch ID: R64993
TestNo: SW1030
Analysis Date: 2/1/2017
SegNo: 1070900
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability Ion -flammable. 0 0 20
Sample ID 17010900-001ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 64993
Client ID: BatchQC
Batch ID: R64993
TestNo: SW1030
Analysis Date: 2/1/2017
SegNo: 1070901
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDL]mit Qual
Ignitability Jon -flammable. 0 0 20
Sample ID 17011492-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 64993
Client ID: Lumberton WWTP
Batch ID: R64993.
TestNo: SW1030
Analysis Date: 2/1/2017
SegNo: 1070903
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability Ion -flammable. 0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded 7 Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 24 of 40

sunimlor
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
trW1KQ(NrA1:NIA1.t3:+:aaaaourts3tea,ttti�.
Cuyahoga Falls, Ohio44223
WO#: 17011492
+1.��ltril;cRP C rh��,r,9ip�ieti
TEL: [phone] FAX. [phone]
Website: http:/hvtvw.settekcon:
27-Feb-17
Client:
Synagro
Project:
Lumberton
BatchID: R64993
Sample ID 17011492-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 64993
Client ID: Lumberton WWTP
Batch ID: R64993
TestNo: SW1030
Analysis Date: 2/1/2017
SegNo: 1070903
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Sample ID 17011492-001ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 64993
Client ID: Lumberton WWTP
Batch ID: R64993
TestNo: SW1030
Analysis Date: 2/1/2017
SegNo: 1070904
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD - RPDLimit Qual
Ignitability Ion -flammable. 0 0 20
Sample ID 17010237-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 64993
Client ID: BatchQC
Batch ID: R64993
TestNo: SW1030
Analysis Date: 2/1/2017
SegNo: 1070906
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability Ion -flammable. 0 0 20
Sample ID 17010237-001ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 64993
Client ID: BatchQC
Batch ID: R64993
TestNo: SW1030
Analysis Date: 2/1/2017
SegNo: 1070907
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability
Ion -flammable.
0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding tunes for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 25 of 40

a _ _ Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
' l
trslINVINOUNga:i;H?4 aLU€n:S, JKC. Cuyahoga Falls, Ohio44223
16a7:3d1�P%cx1 Lrrh.�a,r;�to,�F�;s TEL: [phone] FAX.- [phone]
WO#: 17011492
Website: hitp://www.settelc.com 27-Feb-17
Client: Synagro
Project: Lumberton BatchED: R65064
Sample ID LCS-R65664
SampType: LCS
TestCode: pH_Oil(9045 Units: s.u.@20.6C
Prep Date:
RunNo: 65064
Client ID: LCSW
Batch ID: R65064
TestNo: SW9045D
Analysis Date: 2/2/2017
SegNo: 1072217
Analyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
pH 7.0 7.0 0 100 90 110
Sample ID 17020101-001ADUP
SampType: DUP
TestCode: pH_Oil(9045 Units: s.u.@21.00
Prep Date:
RunNo: 65064
Client ID: BatchQC
Batch ID: R65064
TestNo: SW9045D
Analysis Date: 212/2017
SegNo: 1072219
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 6.1 0 0
6.1 0.5 10
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 26 of 40

}
w SuntmitEnvironmental Technologies, Inc. QC SUMMARY REPORT
qa ' ' 17 3310 Win St.
eV,'N1KQ 11 I.91.1a:tasdlUl�rCta�S,a Cuyahoga Falls, Ohio44223
AdTa,P,ffi,r.AI C<Tb,p,raiIIFlc:4 TEL: [phone] FAX.- [phone]
WO#: 17011492
Website: htty.-#wivw.settelc.cont 27-Feb-17
Client: Synagro
Project: Lumberton BatchID: R65086
Sample ID 17011466-009AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 65086
Client ID: BatchQC
Batch ID: R65086
TestNo: SW9014
Analysis Date: 2/1/2017
SegNo: 1072666
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 1.09 0.500 1.000, 0 109 81.6 122 QMR
Sample ID 17011466-009AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 65086
Client ID: BatchQC
Batch ID: R65086
TestNo: SW9014
Analysis Date: 2/1/2017
SegNo: 1072666
Analyte
Result -
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 1.01 0.500 1.000 0 101 61.6 122 1.093 8.09 5 R
Qualifiers: r Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 27 of 40

Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
e %-1K TJr,11;NIAI_ aq;A;,HNULUUU—;S,INC.
A naty fl-rx1 tabo,rafDfie6
Cuyahoga Falls, Ohio44223
TEL: [phone] FAX.- [phone] -
WO# 17011492
Website: http:/Avww.settek.com
27-Feb-17
Client:
Synagro
Project:
Lumberton
BatchID: R65086
Sample ID MB-R65086
SampType: MBLK
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 65086
Client ID: PBW
Batch ID: R65086
TestNo: SW9014
Analysis Date: 2/1/2017
SegNo: 1072660
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
ND 0.500
Sample ID LCS-R65086
SampType: LCS
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 65086
Client ID: LCSW
Batch ID: R65086
TestNo: SW9014
Analysis Date: 2/1/2017
SegNo: 1072661
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
anide, Reactive 1.06 0.500 1.000
0 106 85 115
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND 'Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 28 of 40

{
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
tMA-19UNTOLN1AL IriMUCILUt3IES:3tvr:, Cuyahoga Falls, Ohio44223
Pl:rratS{2Sgaf LxTbgrai'ap•1os TEL: [phone] FAX. [phone]
WO#: 17011492
Website: http://www.settelc.con: 27-Feb-17
Client: Synagro
Project: Lumberton BatchIl): R65087
Sample ID 17011466-009AMS
SampType: MS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 65087
Client ID: BatchQC
Batch ID: R65087
TestNo: SW9034
Analysis Date: 21112017.
SegNo: 1072688
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 2780 25.0 2750 0 101 80 120
Sample ID 17011466-009AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 65087
Client ID: Batch=
Batch ID: R65087
TestNo: SW9034
Analysis Date: 2/1/2017
SegNo: 1072689
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit' RPD Ref Val
%RPD RPDLimit Qual
:ide, Reactive 2640 25.0 2750 0 96.0 80 120 2780 5.17 30
Qualifiers: k Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlanit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 29 of 40
Original

Sum
Summit Environmental Technologies, St. QC SUMMARY REPORT
3310 10 Grin St.
fm MIL
er.v1Huir•Jr,i1.NIAh1$;k;Hr4fJLUGi;a,;r5.-. Cuyahoga Falls, Ohio44223 WO#: 17011492
�t,rudyUcal LaborwtQfie, TEL: [phone] FAX.- [phone]
Website: hQ.-Ilivivw.settek.con: 27-Feb-17
Client: Synagro
Project:. Lumberton BatchID• R65087
Sample ID MB-R65087
SampType: MBLK
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 65087
Client ID: PBW
Batch ID: R65087
TestNo: SW9034
Analysis Date: 2/1/2017
SegNo: 1072686
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
-5wtlae, Keactive ND 25.0
Sample ID LCS-R65087
SampType: LCS
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 65087
Client ID: LCSW
Batch ID: R65087
TestNo: SW9034
Analysis Date: 2/1/2017
SegNo: 1072687
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 2750 25.0 2750
0 100 85 115
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 30 of 40

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
suannuT 3310 Win St.
��iv�xf.�iNra4:h1AJ,4hi;HNULrJU1!;5,Mi . Cuyahoga Falls, Ohio44223 WO#: 17011492
Ana(1-,Ucvf L,7Z;o ,3hv ies TEL: [phone] FAX.- [phone]
Website: htty.1Avrvm,.set1e1r.com 27-Feb-17
Client: Synagro
Project: Lumberton BatchED: R65312
Sample ID Ics 20ppb L02071
SampType: LCS
TestCode: tclp-VOC-MS Units: mg/L
Prep Date:
RunNo: 65312
'lient ID: LCSW
Batch ID: R65312
TestNo: SW8260B
Analysis Date: 2/8/2017
SegNo: 1076585
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.210'
0.100
0.200
0
105
79.4
131
1,2-Dichloroethane
0.225
0.100
0.200
0
112
73.6
137
MEK
0.939
0.500
1.00
0
93.9
55.1
163
'Benzene
0.224
0.100
0.200
0
112
73.1
132
Carbon tetrachloride
0.219
0.100
0.200
0
110
63.7
139
Chlorobenzene
0.224
0.100
0.200
0
112
72.3
139
Chloroform
0.202
0.100
0.200
0
101
79.3
129
Tetrachloroethene
0.211
0.100
0.200
0
106
56.2
187
Trichooroethene
0.219
0.100
0.200
0
110
64.1
138
Vinyl chloride
0.236
0.200
0.200
0
118
22.1
147 QLR
Surr: 4-Bromofluorobenzene
495
500.0
99.1
80.4
126
Surr: Dibromofluoromethane
509
500.0
102
70.3
125
Surr: Toluene-d8
523
500.0
105
82
117
Sample ID mblk
SampType: MBLK
TestCode: tclp-VOC-MS Units: mg/L
Prep Date:
RunNo: 65312
:lient ID: PBW
Batch ID: R65312
TestNo: SW8260B
Analysis Date: 2/8/2017
SegNo: 1076589
%nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
ND
0.100
1,2-Dichloroethane
ND
0.100
MEK
ND
2.00
Benzene
ND
0.100
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M Manual Integration used to determine
Original
MC
Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
O RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL Permit Limit
R RPD outside accepted recovery limits
Page 31 of 40

SUMMINt
Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
cr4v1HU1rrlrl11aNUILIblHNQL UIL-S,JNC. Cuyahoga Falls, Ohio44223
Alva/S�fdcaf CaTba.r�to�ira� TEL: [phone] FAX.- [phone]
WO#: 17011492
Website: htto:11wwiv.settelccom 27-Feb-17
Client: Synagro
Project: Lumberton BatchID: R65312
Sample ID mblk
SampType: MBLK
TestCode: tclp-VOC-MS Units: mg/L
Prep Date:
RunNo: 65312
Nent ID: PBW
Batch ID: R65312
TestNo: SW8260B
Analysis Date: 2/8/2017
SegNo: 1076589
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Carbon tetrachloride
ND
0.100
Chlorobenzene
ND
0.100
Chloroform
ND
0.100
Tetrachloroethene
ND
0.100
Trichloroethene
ND
0.100
Vinyl'chloride
ND
0.200
Surr: 4-Bromofluorobenzene
468
Surr: Dibromofluoromethane
494
Surr: Toluene-d8
488
500.0 93.7 70 130
500.0 98.9 70 130
500.0 97.7 70 130
Sample ID Icsd
SampType: LCSD
TestCode: tclp-VOC-MS Units: mg/L
Prep Date:
RunNo: 65312
,lient ID: LCSS02
Batch ID: R65312:
TestNo: SW8260B
Analysis Date: 2/8/2017
SegNo: 1076609
\nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.246
0.100
0.200
0
123
79.4
131
0.210
15.7
25
1,2-Dichloroethane
0.234
0.100
0.200
0
117
73.6
137
0.225
3.97
25
MEK
0.940
0.500
1.00
0
94.0
55.1
163
0.939
0.160
25
Benzene
0.223
0.100
0.200
0
ill
73.1
132
0.224
0.538
25
Carbon tetrachloride
0.218
0.100
0.200
0
109
63.7
139
0.219
0.411
25
Chlorobenzene
0.223
0.100
0.200
0
112
72.3
139
0.224
0.0448
25
Chloroform
0.224
0.100
0.200
0
112
79.3
129
0.202
9.95
25
Tetrachloroethene
0.229
0.100
0.200
0
115
56.2
187
0.211
8.27
25
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 32 of 40

sul"hirt
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
Lruvl+cUNTAU.N l.v.. a htHNULU,1i: S,, ahC.
Cuyahoga Falls, Ohio 44223
WO#: 17011492
E4 tdr4'tdcst C:Ttapr�Io�ir 5 TEL: [phone] FAX.- [phone]
Website: http://wivw.settelacom
27-Feb-17
Client:
Synagro
Project:
Lumberton
BatchID: - R6S312
iample ID Icsd
SampType: LCSD
TestCode: tclp-VOC-MS Units: mg/L
Prep Date:
RunNo: 65312
;lient ID: LCS502
Batch ID: R65312
TestNo: SW8260B
Analysis Date: 2/8/2017
SegNo: 1076609
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Trichloroethene
0.234
0.100 0.200
0 117
64.1
138 0.219
6.70
25
Vinyl chloride
0.183
0.100 0.200
0 91.5
22.1
147 0.236
25.4
25 R
Surr:4-Bromofluorobenzene
508
500.0
102
80.4
126
0
25
Surr: Dibromofluoromethane
541
500.0
108
70.3
125
0
25
Surr: Toluene-d8
538
500.0
108
82
117
0
25
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit
P Second column confirmation exceeds PL Permit Limit
Page 33 of 40
B Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
r 3310 Win St.
4vJKV,NrntiNIALULrHNULUtIlI:K,Jena::. Cuyahoga Falls, Ohio44223
A1H3,tyr2f.qaP Ca.taoXa:rnpteg TEL: [phone] FAX. [phone]
WO#: 17011492
Website: hM.-Ilwww.settelc.com 27-Feb-17
Client: Synagro
Project: Lumberton BatchID: R65323
Sample ID MB-R65323
SampType: MBLK
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 65323
Client ID: PBW
Batch ID: R65323
TestNo: SW8321A
Analysis Date: 2/6/2017
SegNo: 1076727
Analyte
Result
- PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D ND 5.00 0 0
2,4,5-TP 'ND 0.500 0 0
Sample ID LCS-R65323
SampType: LCS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 65323
Client ID: LCSW
Batch ID: R65323
TestNo: SW8321A
Analysis Date: 2/6/2017
SegNo: 1076728
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
2,4-D 50.6 5.00 50.00 0 101 60.5 141
2,4,5-TP 47.6 0.500 50.00 0 95.2 68.3 144
Sample ID 17011333-010AMS
SampType: MS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo:, 65323
Client ID: BatchQC
Batch ID: R65323
TestNo: SW8321A
Analysis Date: 2/6/2017
SegNo: 1076729
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val,
%RPD RPDLimit Qua[
2,4-D
53.0
5.00
50.00
0
106
2,4,5-TP
51.0
0.500
50.00
0
102
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit
P Second column confirmation exceeds PL Permit Limit
Page 34 of 40
37 105 SH
38 106 H
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlirn t Original
R RPD outside accepted recovery limits

hi I
Summit Environmental Technologies,Inc.
331010 Win St
n St.
QC SUMMARY REPORT
trWIt1UXN 6111N I AL 11:1;HNULUU1WS, JNC.
Cuyahoga Falls, Ohio 44223
WO#: 17011492
_
.��!t:�/yUpa/ Lnbt�a•atoriaa TEL: [phone] FAX. [phone]
JVebsite: hW.-11www.seuekcom
27-Feb-17
Client:
Synagro
Project:
Lumberton
BatchED: R65323
iample ID 17011333-010AMSD
SampType: MSD
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 65323
lient ID: BatchQC
Batch ID: R65323
TestNo: SW8321A
Analysis Date: 2/6/2017
SegNo: 1076730
\nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
2,4-D 51.6 5.00 50.00 0 103 10 150 52.97 2.55 30 H
2,4,5-TP 49.7 0.500 50.00 0 99.4 10 150 50.96 2.54 30 H
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 35 of 40

-1 Tech"0102ies,.11ac-
Sunit-nit Environment
3310 AVill: SLrW
Cuynhoga,Falls, O.Ilio 44223
Analysis Requegt/Chain of Custody
F.pr Summit En iannent4i Tecl1010�2`, Inc. 11"e only
LNotes/comme[ILS:
fjA-
J

DC-7
Rev '6
Summit Environmental Technologies, Inc.
Cooler Receipt Form
Effective DAU. 0717gN4
Initials of person inspecting cooler and samples; SC_
Client: tnCLG�
Order Number.
Date PeceNed: - l� Time Received: IC'CQ
rY, ,
Data coolers) opened and samples inspected: t , �t "17
Number of Coolers(Eoxes:
NIA
Shipper; UPS DHL Aliborne US Postal
Walk-in Pickup Other:
Packaging; Peanuts ubbte VJll Paper Foam None Other.
Tapp an cooledbox: 1(�
N
NIA
Custody Seats intact
Y N
N(
C-O-C in plastic
N
NIA
Irn_ Blue ice
p -se I I melted
NIA
Sampla Temperature IR Gun ni 020459 CF_O.O °C
/absent
�"i °C
N/A
Radiological Testing Instrument serial #251127
Y
NIA
(see pagge.2 for scan results)
^" Use 1 sheet per sample for Radiological Testing. If sample is HOT, the Radiological Safety Officer must be notified
immediately.
C-O-C flRed out properly
N
WA
Samples in s_pamte bags
N.
WA
Sample containers intact`
G N
NIA
'if no, ist broken sample(s):
Sample labal(s) complete (ID, date, etc.)
YJ
N
NIA
Label(s) agree with C,D-C
N
NIA
Correct container's used
(DY
N
NIA
Sufficient sample recelved
N
NIA
Samples received vAthin holding time
0
N
Bubbles absent from 4o mL vials"
Y
N
" Samples with bubbles <6mnl Am.accepisbie.
Indicate bubble size if =Srnm,
Was client contacted'about samples
Y N
Will ctient send new samples
Y N
Client contact:
Datalrme:
Logged in by:
Comments;..._ _--
Pagq 1 of 2
Page 37 of 40 •

Kofth;�Caral7na'Ll4P'as�ewatel'fGr�U�dw.'�ter L.ab�ra�ary ��r�I�i�.atEon
C6rt1f ed:Parattic'kers Ustin*g -
Wb warm:' SuinrnitEnvirunmei:al Techno(oyll�s. P!Ic
CBIIJficale 1 lurDt:E: t131 ,
$:ddrayfi: 331a.t+d111s1ruet
E fezhou Dam; VIt2017
Cit'tfithopa Fats. Oil 44220.
Expira9lon Date: fi2r31f2[!17 . .
Vold of Easi .9menrlrneni 20IN 7
Ttlo- ahm t namul. ;501300, is 66eb ceffiliaflar Lhe'inms •ement of the pafawl?rS MW WIM
_ -
�—_
CERTIFIED PARAMETERS
6NOF2GkJJIC
RrSJr,1UF SLi$PE!Nr19in
BOO
$tv1 2940IJ-1997 (Aqueous)
.. " .
5�[phone] iF:quFouy}.
RESIDUE, TOTAL
GF.L7r�lfr=
anti 259L1� 1°"`PF.(13.gV4'UU5)
,SVi,840 913,513 A V'tqueuil�P
SILICA
(iJD'
EPA•2W.7. Reu.4 4 Lgele (.Sgt;e:Dtjs)
EPA G220 C-1 Q97 r p g9Cokm)
6010 C ,ftieo um'
r-LUORIDx
SULFATC
L:uit 3W.C. Rev. 2.1. 101(Aquaotlsl .t
EPA D�u:O. Rev. 2 1 1003 (fig reousi
uW-•fM{3.1456A A;l,l;eol_�I
IGPr'ITA.l31LITY
SULP°I[)L-
¢�
-U
S'Lrtf•Bti1J3D(P;cd•Aqu6olto)
SW4469-334(,4qucous)
I J()A.GA;+IC PHEMO:S
METAL
W
(D
E13A 420. t, Rev, 19172 tCcjn itr6)
TCIP 6tFFN.S.
00
�.
NITROGEN, ral`I'I2,n'II:
(Aquuous)
0.
O '
S'h 30e Q' Rev, 2.1;1993 (Aqur,ous)
ALUMINUM
h
5 0-G«i 995: A(Aqueous)A
2UTJ.7, R
p
NaTft4r , r11'razlS'E
S'Ar a49 001 U V (Aqum l
PvA •ip€1. G. R0u�2 1 199,�.(AqueoUt)
EPA.200-8. Rev. 6A. i I941 queuus;
'5V0-$4fs 8950 A (A,Etietar,$)
!k(V,a4i3 15020 H (3gaikablls)
NITROG0 !..N09 *'W)2
ANTLf OIVY
F!'14$GO.C.,Ruu.2,1, 1993:(a tllxuus)
EPA2D0.7, Rep:4:1, IViA{Ague0us;
S'i"d-i�it5 J45f,;4 (i,+;uevusj
SVIF.841i 1'in111 D (Ag0pat sI.
NITROGEN. ToTALKIELOAFIL
EPAs200-6.Rev.5.4,1994* -[Aquubut*
V414500 Now U-I9137 (Sl'. 4511O N113 D] !! 9?1 lAgtieous)'
S1h'-B-0G 6020 E (Aq,leousl '
OIL E GREASE
ARSENIC
E1�A'1£5c I2@•r. 13 (Aawe0ct3h:
EPA 209.T, Rov. 9A, 1994 (ActuoDum l
F1971 c:, (:Nur?,AqucdAip1
51h''-A49'60110 D (AgtmoL:EI
PH,
1=f'A 200.6, Rev, 5,4, 1 �q4 (,%quE;OtaS
S'N-8146204$ G (Won•Aq;jeqrj #)
:iNlr^S-0�J Gb'lS] L I,'tUaeeus)
PHOSPHORUS. TOTAL
BARIUM
EPA 2bQ'7. Rev, 4.4 f l W4) (Atquo0uf)
EPA 209 7, Rev. 4 ., 199 d (AqueDtr.J
&N-S4f 6010 G (AgLttrDUP:
riff-'S-711uh ❑KRUOLV- D iPG C
EPA 209.8, zZCv. 5.4 99.4 iAqucuusl
"M 25fI] C-1997 ;F uatris)
S44'-E46E420.13(Aqueoae)
Ths.CMt cairn req,i:x m6irYanCO A!an G,4(?;7 1a'iL itY a55urimp :7r3grin C5e CI' 1prf:!Vt1
r Ht5{pWatTp.'&nil ]ttclFLlcry.L6Anr ti5n.e tin aviltdC., b L sTrfrJ9&' L Wraiceioo are at by=lc. f�v'p9R.::SE and! CaaaiUl,� sUon tStrdrFGlienS

Noah 0aro ins WastewatedGromdw'ip#gr Laboratbry.Caii iic.atwn
'
CMlf[ed-Para etrsrs Listing
.Lat�{Wn«:: 5anni;,ii EnvircntneuCa:'Felc,9i+lofo$ias, Ina
-
CuclaGs:ule Nuniiier
Addrms: :VfZ0'AQn ,re9.I
ffec*ivol]ale Ii! 291;
- �alpgfta0fi Falls,:'OH. 44-AZU-
bale: - 12'P3117[1'I.7
_
Date of Last ArrIentirr-nt 202017
Tlw^�'toua are:nrctl lauemsl rf. hc,inr..rl:lly n ct It7et-qulTemn rt*af 1:rA N09C an 000,:y 12=1el7)•
ce:4r1W.f0r qla mmeuremal of the p5.2niem liRfU4lxalgv'.
ceRfrFl a PARAMETERS _
BERYLLIUM
EPA 2008. R=v.•5 . 19fiw(Aqua,-763)---
EPA2n0.E. Rev. 5.4, fulie, (.Iiqukutl8l
GW-840 002U B fAgttous)
SW-84f5 60205
LITHIUM
BORONEM'200.;'
Rev. 44,194,4 ftuj:uusF
EPA 20(l 8, Rev. 5.4. 19c14:;A4w ot:9 )
SW4046 0010 U (Arpeous)
SSM-54(i 6320 S (gqueclus;
MAGNESC,.'M
LADMIUNI-
EPA 200.7- Rcv.4.'4.290.4.Mof-0im
EPA 200,1, Rev. 4.4, F5f14 (Aqut� nsl
�Vtr EEO 601-0 C tAgtlP_ova�
0-N-4466010 D (Agupoubl
MANGANESE'
EPA 200.4 Rev, i.4; 1394 (Aai mis)
L-PA -')DO ?, tie4. 44,19 4 (Aqupbusj
SW-846 ci020 t3 (Aqueoss'J
'
S1"1-6-0+i 60t©b (�•que4u,}
-�
CALCIUM
EPA 200.8, Rev. 5.4. 1904 (Aq n pals}
ra
[PA 200.7. Rev. 4.4. 1yBd (Acueousj
S'A;-754i s<�lU r� (At(•dUeusf
-5W-6413 6PSO0 (Aqueou.YCID
.
g1tHG3UF{Y
CO N _
CHfROhii1JQ1 `U7J1L
'f
EPA 245.1. 1lev 320 19144 (Aqueacrsl
0 o
Er1A 200.7. Rev. ,1, 3. g!-M (ru ucumi,
Suu-640 7e47rLA (Aq"00L z)
'-n -'�
W
s'r�-1t41� �o la D'(Jklc+cavcp
F-r-A 1rr:11 P {kyu©ousy
p
EPA 200.8. Mou. 5.4. 1%4 (i> �uecue
4 ? ..
hiCsl_irtlrlClti41M.
"
S4Nh94L 6020S.(M1cuew,u
E°A 200 7;.Reu 4 4. 19S4 (Atruerlus)
_
COSAI.T
S110-640 5010 D Am it
rPk 20(}:7. Itev,;L,4.19f1� $Atluecua� =
EPA 200.8,16 uv. 5A, 4f194 ("we o115Y
SW-840'6010 D (A'g6Dus)u^^y1
C•46'a' 2R �'(kum�lus}
FP A•200.6•Rev. 94, 19S4 (k ibc}uusf
%IC1(EL
Sri'-?i1G LitI2R.E1 {A.a(UecusJ
EPA 200.7: Ray. 4.;. 604 rAsugriu ()
=
COPPER
SVV440 0010 17 (Apicews]
E15A 200:7, Rev 4.4. I k�4 IP queaus)
EPA 2UU.fi,.Rev 5.� 193?#.(Aqueag8�
S W-940 66.20 8iAaueuus}
EPA 2W,8..Rev.5.4. 1<194 (, qui+n:tu)
''Fjf' --slu ! _
SVvtS40 6020 9 (A4uebtm%
I- PA 210 r Row. 4.4'1-904 (Aquecuo
113U'h'
$Vd•B46 6010 D (Aquarma)
EPA,,100.7 Rc•a 4A, t90W'(p.qucua3}
SELENIUM -
SW-946 6011) D ikcsleonsp
EPA 2C0 ?'•-Rev, 4A. 101 4 4&juccua}
LEAD
EPA 200.7 Rev 4.4, 1 N$4 Ifti.eousj
-PA 200 S. Rev. 6.4;16Ye (A(T P,c,7tt5•J
SL1r'•8r6 EC10 b{4ytaecusl
3v'd-840 0u2u BJACIuec44,}
•
1 yk c i,7ilicatim requires memle••ee of a r azmptc4fo c'JEgy kt `*jrau,x 1:mgFcn: uco of wafc4ea
15-1 N; Ali r,$fJ7
St'f_•u cilaletl :inrl.:mir-,R b! "--r^pixo pe. vaaolian Sam Qa,
Y• _Y n . a FI I:ab:r;,ltnu8nre
.
eu0, mt la civW �craa es ard+arorxmrillc au x+fur mfraGliu"_
!7H

worl.h••C.ar'olItiaWastmake! rid r-oundva'Jitar.Labbratary.Cerk1flantio9r
CPdif ed Parameters' Listing
Lk�'14aIrIt�. Sttl IMA FaWroamunlei'(eelunul0gte^: Iraq
CceriJ6cttte yuroher. 607
FuJafess: n'M0VMM',31ra 1
&ift ClovC C]a1c' 1t1t2Qi i
.
€.:gya116.r..AA223•
E'xpimUort 7atu:-12131J2017
Date -PE Lut AMendrnnol: 21212017
71r� ht�ca nolnod leCofn&ry, hgyiug c:dy mct tfip mqi ircm,DnI. of ISA NCAC 21;:Oftw io hercb} wilup ror l6p moiE su mut or lho parepluaer5 li rJ Lml=.
- -
--._
CERTIF11ED PARAMETERS.
41_t1ER
EPA.6C5 ShgacOfrus$ .
E0A71:6.7, 13ov. A.A. 199k
81,M-8448270 0Oquegl7Ef-
SmY-Adr, 0 D (Aqueous)
CHLORIN'AT=D ACID HERCiICI(ICS
EPA-21 {).A lir:v 5.4. 15u'(Aqueousl.
Sti/a''-89d $164 h (ltqut bu: )
S%I -R-Ci R0205 (Aaueaus)
- . CHLORINATED PHENOLICS
SOOK'A1
EPA-IG53, R.ov. A:1397 (AgLLku;:J
EPA ZDU.? Re' A 4. I894 (AtlCeuusY
Ex:I}'M I'AT3-Lk PETROLEUM FYOROCARBON5
SV�_j a(; 4U1U G' (A:1ue_us) -
f 1A47LP. fuidy 2G04, Ray. 7 1 IrnqueausJ
S3'RLhi?UtA
lq NHALOGENATED voLA+ I.L.1ORGiXNfGS
EM 200.7. Ray. 4.4, 1994 V%queubs)
S'111-11d(i 7 915 C iAquQaus}
SV-' A4136010 C (Pgmousy
r?FST GIRES., ORGMQCkL'JRINE
EPA 21&;? 4. R•_r, !;.4, 19.N SAg6eoVai
FPA'GG#!'(At1t t0asf
N..
StN'.;dir'FiDiO,g (,4queoUsl
SIA''-84C $08', 2 jAgtta,�n;J
CD
I I Ifi LL IU GI
POLYCHa S] ii1NA7FI7 i3FP'+ Ir N'Y: S (Pt .;iq l
O_ W
EPA 20G.7, kulv..4.0,;1004 (Aqueoual '
EPA O08 (Aquiruust
O O
SW-940 53510 0 (AqueouaJ
'SW-040 905-2 A. (Aqueaus),
—t+ '--h
WA7t1O.S,Rev. 5.4,1094(Aquogmj
- PLIRGE4BLE,'?RGr;1Jl S '
O .
(q
SERA 624 (Auu.00usl
-Trr! -
�J1'-64G1S2GO B (:44ueoUsl-
... ,
FRP+•2t1{I.7, Rev. d.4, 1494 {Agl*,pus)
TOTAL ORGAWC-:11 ,I, ILMIS
aV'-81i�J1U p (Aguaoc'tj
::tV-(V4G.80z0 D (Auueuu i
b'ANADflipA
TFH.171@GEL RAROE, ORGANICS
F17&20p.S. Rav_ 5.C, 1,984fAgU29uG)
� SW446016 C (.4quaaus}.
Sv'1 '4 3 f3n2n R;(+7 Aireaus]
TPH G1SaL1N:: Rnrd(aE.:tF G;,h ICS
" 20t`vi:
- S'!'i-11468£1a:G(,�iqueozvp
•
F°r1 2tJC.7, Rev. A.w, 19y4 (Fggitr4s}.
VOLATILE PETRflLEt1Fr11�4'CROi AFiQQh1S
-
5'�'d-L'+:�4gG9U Q'i`i"gin�uusi•
Iu1FtLEP, IdBy2U�!i, RrycY1`1 (ItCJ7i9�71FV
-
' ErA' (Id:6. C4uY. J:4. tfl9�i (Aqw-must
c'Pd.-240- 0020 B (AgkjeXg5).
QRGAWC,
-C LP l3RC-AWC5
`VeN-eery 1311(Aquacus).
ADS'OREA6LE.t1rRrANIC fM.IDES
EPA. 1660; Rf'.1, C. 1 W (Aquaaus)
-
BASE N'rIJ'I"FAUACILI, ORG,ANiGS "
I'Ia;cilrfeoLorlreq,it�eyn�7vsto.'1W;of,#meoc�Is'afiequg4ty5+5Ui'i�CGnrC,SIfa71mU:,'JCfr]p4rv9'rcrnelNvlcdlxpi;unu=::tt1.fa'atolyp-.�iwman:gonaval•lalrarfsarnoae,
Lea�tonesa'espy+�teocr�nlrrrau�ar.,minrtwrarfinK,auamnrinfs�yons
'

ANNUAL PATAOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Lumberton WQ Permit Number: WQ0000672
WWTP Name: City of Lumberton WWTP NPDES Number: NCO024571
Monitoring Period: From 01/01/17 To 03/31/2017
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray _ Gamma Ray Pasteurization
.Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to,alternative performed (C1ass.B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
tr appucavie to alternative periormeu t-ass
a or t.,iass n com iete the iouowing monitoring
aata:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum. Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6'h
MPN
MPN/g
Coliform
power per gram
of total solids
CFU
<21300
<22000
<23100
CFU/g
0
quarterly
grab
9222D
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC b2T.1107) - Please indicate option/alternative performed:
0ption/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(4.0-day bench)
(30-day bench) (Spdc. 02 uptake) X
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
. (Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware, that there are significant penalties for false certification including fine and imprisonment."
Corey Walters, Assistant Director of EUS Dept.
Preparer Name and Title (type or print)
Signature of Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Canid Ton Testing Services, Inc. Laboratory Report
Synagro 1701
Lumberton VMTP Yet
i
Sample Info
sm
r'mation
C. Hayes' 01/30117 - V M
f M �M C. Cameron
Analyses and Results
170150 -1
Sludgc Gr FeQ. Cofiform-S < 22100
Mfg 22100 01/31117
2
<21.800
CFU19 21800
-3
<21800
cOUID 21800
4.
<21.'800
cFU19 21.300
<22200
F A 21200
-6
<22200
cFulg 22200
<23100
CFU/g 2-3100
Geomean <22000
170150
gludge Gr TS N 4.52%
0.01 01131/17
-2
4.0%
0.01
-3
4.69%
1101
-4
4.690/a,
oat
-5
4.60%
o-oi
-6
4.51 3/c
0.01
-7
4,32%
0.61
Repbrt
Review
.tali Diredtor
219. S. steq.e Str.
WfordNC. 2733.0
NC DENR #664
NC PHHS #37799'
US EPA #NCO1916
M
SB - 9222D - MF

Stee
21.9.5. .NC Cameron Testing S
Sanford,.NC 2737330 s � @d"V1G@S Inc. Chain of Custody
Phone:•919-208-4240 NC WW/GW Cert:.#554 NC PHHS Cert#37799 US EPA NC01918 Page of
S� -� -
� ynagro� , � [e-mail]. �
ag .>M.
Chad Hayes i 919-799-0766
284 Boger Rd. �} .
&tr �-,, Mocksville, 'NC 27028 F
R LU
#i Name: Signature:
M .
��'ij r5� lA 'WLw', SAyI �6#�i s {a��YY.Pvsat M .C-F+. >_ +JT4y{'• ,..k. .y
ii N ' nw3 �
Ix `r a c.a ti
RCS' _ r?;"�s�l �i�'� R-. 3 '� • .
LQ1. 2 O�( 7a3 le ID ns E o `R, Q NN jj
P 0 E8 a N, fI w lri2a(nSP)tQers4e; rHvat(Nw1)0e1 s3kt((tN7�aYnt )pTrYheisoe¢lknurlp
., r I m
Indjcate��� �{
S '1 -col 1 N It7 �a 5d i I I .�-
S! (� �� Set 7 (Fec S, TS) nS 1
d 2—
0305
147
— ---�--�--�---III i � - -- —
i � °: °+�`54Cifi7i '� ,. ,rifii• rY.a sw,aa. - ii rrysyr u: ,y;'v cr
n4' " sw
Rush work will require prior approval. Additional charges will apply

.city of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Wo.rksheet
Date & Analyst: T! d
Sample # 1
Total Solids
Sample volume used for total solids test:
Weight of dish:
Weight of dish. + dried -solids: 4,
Weight of dried solids: 0.43
Total Solids: 17.236,
mL
9
9
9
g/L 1 .9,
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
0C
0
M
2,
3
4
E, —"-' _" YEN E
5
7
L 7
M 0A)
'422-
8
P0
9
10
12
13.
14
15
11
0,
N�
Oxygen Consumption Rate 0.28 mg/L/minute
SOUR Or. 97 (mg/g)/hr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
0C
18
If sewage sludge is > 20°C, SOUR = o (mg/g)/hr
If sewage sludge is < 20°C, SOUR (mg/g)/hr
SOUR passes if result is:5 1.5 (mgfg)hr
Version I I/l/I I

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 011gesterw#:1L j r1,1/1fi/16 Coll at° 8 1a6 amp KCL / TLS1 4 �1�
Sample # 2
Total Solids
Sample volume used for total solids test:
Weight of dish:
;;:- :, 25: mL .
; { _ �1205'4' g .
Weight of dish+ dried solids:
E g
Weight of dried solids:
Total Solids:
0'.42 g
16.948 g/L , I % S
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
01r4r00
2
3
firs �14
OUP r.r—723�.,
4
1r4:00#
`Y
k7Y 00=
5
J
LW
7
L`;y `r' '1r400i
r
10
L . 15
00
U—" K43
12
TT
T 1:
r � 1'1-11-11 01��
13.
14
;)„5.00}
rf
i�442r T
Oxygen Consumption' Rate 0.24 mg/L/minute
SOUR 0.87 . (mg/g)/hr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
oC
14.5
If sewage sludge is > 20°C, SOUR = ��. (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 1i (mg/g)/hr
SOUR passes if result is 51.5 (mg/g)hr
Version 11/1111

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: L
Sample # 3
Total Solids
Sample volume used for total solids test:
Weight of dish:
Weight of dish + dried solids: 4
Weight of dried solids: 0.43
Total Solids: 17.068_
mL
9
9
9
.SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
0C
0
2
4
5
6
L=1,1-w--'-�---':L—��
E___" __X12-H
7
8
9
AMU
10
41
12
7_11, T,
14
15
10 XOT�l
91-
Oxygen Consumption Rate 0.23 mg/L/minute
SOUR 0.80 (mglg)/hr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
0C
14.8125
If sewage sludge is > 20°C, SOUR = 6111103 (mg/g)/hr.
If sewage sludge is < 20°C, SOUR = ffljj1 13 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11 '

_ City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst:
Total Solids
Sample volume used for total solids test:
Weight of dish:
Weight of dish + dried solids:
Weight of dried solids:
Total Solids:
mL
9
9
9
g/L
SOUR
0.42
16.948
Time
(Minutes)
Temperature
-Dissolved
Oxygen (mg/L)
oC
:,---
s
1�.
15
001 ---
C 830 ;r w.
2
w1j5001..
R ,
i 82�1C_'
4:"
1'S00
s
L_ 786 "
7
9
10
l _6
12s
415r001
=,r I
(�;� ..i:6°28 `=?
13
L..: L k ; ; 1:5
OOi
14
R` . n � '1�5
5t90
15
Oxygen Consumption Rate - 0.16 mg/L/minute .
SOUR 0.58 (mg/g)/hr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
15
If sewage sludge is > 20°C, SOUR = 0 74 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = N M (mg/g)/hr
SOUR passes if result is 51.5 (mg/g)hr
Version 91/1111

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) W orkshe-et
Date & Analyst:
Sample # 5
Total Solids
Sample volum4 used for total solids test:
Weight of dish:
Weight,of dish + dried solids:
Weight of dried solids:
Total Solids:
m L
9
9
9
g/L
SOUR
FI-7R.,
E_""f
cl� 2 i'22
0.43
17.072
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oc
0,
2
P
LEE!
3
4-
7a7
6
7
8
E_f1ZT_Y'__
01
9-
10
2_11
A GO- E _.: 27
E-1- 8x88, _
1.11
LILI* _,"ZI Z �_�i 15,AI
X-21
12
13
EJ:_
14,
Oxygen Consumption Rate 0.14.-' mg/L/minute,
SOUR 0.48 (mg/g)lhr
SOUR Teimperaturd'Correction
-Average Sewage Sludge
Temperature During Test
oc
15
If sewage sludge is > 20°C, SOUR = o s (mg/g)/hr
lf.sewage sludge is < 20°C, SOUR = fflo ss=(ng/g)/hr
SOUR passes if result is:5 1-.5 (mg/g)hr
Version 11/1111

City of Lumberton
Environmental Laboratory.
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: F 71- LN 6
Sample # 6
Total Solids
Sample volume used for total solids test:
Weight of.dish:
Weight of dish + dried solids:
Weight of dried solids:'
Total Solids:
9 (0
9
9
g/L --7 04 -Sc)
SOUR
A
0.42
16.628
Time-
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
0C
0
L= ZZ- PQ ; ONE" V
U2
AF4
2
3
4
i 4 rlot,
91
5
6
.0
7
1 E - 3-1 ORY-2-.11.
8
9
:—A
z_
L,'I'l LO
10
11
12
L7v 1-1 O'
4
13
WWOE.-, 1=11
-t� A
14-
11 LO —0V
El-- RAF --
15
E AM1rAV111-z1-`--_1,`--
Oxygen Consumption Rate 0;09 mg/L./minute
SOUR 0.33 (mg/g)/hr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
0C
10
If sewage sludge is > 20°C, SOUR —
(mg/g)/hr
If sewage 'sludge is < 20 'C, SOUR = (r-pg/g)/hr
SOUR passes if result is:5 1.5 (mglg)hr
VerMon 1111/11

City of Lumberton
Environmental, Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Palo
Sample # 7
Total Solids
Sample volume used for total solids test:
Weight of dish:
Weight of dish + dried solids:
Weight of dried solids:
Total Solids:
mL
g
g
g.
E'-7- A-41 82
0.41
16.576_g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
-0C
0
1117r2
A
21
IV.2,0C, 21
3
K
4
1010,0f,,
5
T
.37/L
6
7
T Al
8
9
Or94
10
12
15(0-
f-774
7
'13
L
0 �74
14
11,0M.
15
Oxygen Consumption Rate 0.11 mg/L/minute
SOUR 0.39 (mg/g)/hr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
0C
10
If sewage sludge is > 20°C, SOUR = (mg/g)/hr
If sewage sludge is < 20°C, SOUR = (mg/g)/hr
SOUR passes if result is 1.5 (mg/g)hr
Version 11 /1 /11

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Lumberton WQ Permit Number: WQ0000672
WWTP Name: City of Lumberton WWTP NPDES Number: NCO024571
Monitoring Period: From 04/01/17 To 06/30/17
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
It applicanle to alternative performea Mass
A or l lass ti com fete ine ionowinv monitoring
oata:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2xl0.to the 6th
MPN
MPN/g
Coliform
power per gram
of total solids
<32300
<32700
<33100
CFU/g
0
Quarterly
Grab
SM9222D
CFU
39500
44200
7 700
0
uarterly
grab
SM9222D
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Mt. 1
Option/Mt. 2
Option/Alt. 3 Option/Mt. 4
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake) X
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Corey Walters, Assistant Director of EUS Dept.
Preparer Name (type or print)
,c +s.
Signature of Preparcr* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

i
Cameron 'resting Services,. Inc; Laboratory Report "° °ENR#554
NC PHHS #37199
US EPA*NC01918
h�Clreni SYn; '9 ro -MOUSE R '170716
UN WMT
i EN�ii�� Tti
F PrOJ c � lLumberfion egu 0 � Yes
LAM
Sample Information
C. Hayes G f y 05/021, t Re Uved S. Bullard D om; 05/Q2I17
iAna'yses and Results
ti. i'- w s-j-•.x�-
w. i��' axe- 'T `. $'� rt �. 3 � tru„yi 9 •4l { it ++- - -1f1 CIS�a'i." r 'n '.e "S 4 Me dd�
rr '+•ti{ t1., i cev �....� .u- .J'.tin r"Y c`a"`s .G+ µ-or r� �r
y -�+
;fia�p Sample 1 :ifl one Ana6y x R�1t F
�C@nC�t:.
..�.�� '•,-�..�.._.C-j.. �i�.�L�a:'7s'�.,.._._,�.� ..,:,t.., c � a'! a..a}s�.:�a,.. ..�. 01s,�,,.._..�.W✓....sue
170716 01 a sludge Gr Fec. Coliform-S <32300 CFulg 32300 05/02/17 ERP 9222D - MF
b . I <32400 CFUfg 32400
C <32900 CFUrg 32900
d <32700 cFUrg 32700
e i <33100 - CFUfg 33100
f <32800 CFU19 32800
9 <32800 CFUrg 32800
Geomean <32700
170716 Q1 a Sludge Gr Ts 3.10/o
0 0 o-01 05104117, SB 2540 G -TS
_ • (io)
b j 3.09% 0.01
. 3.04% 0.01
d .3,06% 0.01
e 3.02% 0,01
f 3.05°/n
0 3.05%
Report �/j
� _
Date
Lab Director, {
219 S. Steele Str. 919-208-4240
Sanford NC 27330 - Chris a camerontesting.coni

219 S. Steele: Str.
Sanford, NC 27330
1
Cameron Testing Services, Inc.
Mr. WW/GW Cnrt_ #654 NC PHHS-Cert# 37799 US EPA NC01918
J
Chain of Custody
Page { of ii
rnone: pia-<uo-vc�ry
Company:. I Synagro
Emaii:`
CHayes@synagro_com —
_ - CTS lab use only -
Contact:' .Chad Hayes.
Phone
-
919-799=0766 -
Sample Temp ' ! 7 -7
Proj• 0 r t`
5 (
(C) __ _`� .-_-
j
4dd1ress.•(Gjty, 284 Boger Rd.
Fax::
--
Arrive:
_ __--------•- ---
state; Zp)
Mocksville, NC 27028
Notes:
Due:
-- —
Project;' � e CSY�
Reg ulatory -..
Rush
(Y/N) (Y1N) ,
r
:Gollectedt.. Name:
f Snaiure: A
9
'
Sample lnformation
Number of bottles
Requested Analysis
(V
an
x Z
ca
@ O �,
m
._
Preservatives: (Ujripreserved, H(C)1,
_:j=S_l_ab-
ID
Sample ID
ro E
S �
m }
o
o 0 � - a
�5
H2(S)04, H(N)03, (Na)ThiosuIfate, Na(0)H,
1—
U C3
a
r
"' co r r
o
Other (X), Indicate
S c�k
f1�2 l °o
�r'
S t
/
_r
Set 7 (Fec -S, TS)
- U 7
Ike hT4uished`:
Received.:
QatelTline
.Rush work will require prior approval. Additional charges will apply

Cameron. Testing Services, Inc. Laboratory Report - - NC DENR#E54
NC PHHS #37799
t PS EPA#NC01918
!� �C1j� Synagro 171052
�.�h��
Project Lumberton WWTP g T, Yes
Sample Information
r e = C. Hayes i ,Date 06/28/17 N M. Sims Date j 06/28117'
i'str >-.jam i
Analyses and Results
t y�" trt- ;s''.1,�F '"n.. i�' �3 � �i �—..� �;��i�£�"'s t�,1 ��z s� � ^4-y'4 Fct j+z-�.�-�r i,i�.✓�r^,� 4i -s.� 1,� r�- -�,i'e " 3 �,;- '� sy,� rr r�z—�:
]e1�,,.,sY'2>ins Y,i��.��,�,�','�'''+.-t���'%Y.. Sr ���Try � x:�::fy�+, ��"rw�; `.H t�'tiatiStgj�fy�wray� ii"x' is�.l'F`�;jyit y���.('.��,,,''`�+��}"�,�„'�.'�`r•�"�� ��e�Yf° °1�.d�� �. ;,,�''„�r+
t..j.v,y+s
iTS Lab ID�+�r�S'atnjitf�p r ray '�c:�' r;+�. SiciUiehods.i
Fxa .,,a �s Gl6k a.C��`� �ttal�ite ;��h��� �� ,it7�B�SU�tF ,� xG� � �� 'n
�s�-".a�'"�.i�-l'j�-ti `�p�i�W
171052 - 71 Sludge Gr ':Fec. Coliform-5 39700 cFui9 39700 06/29117 SBIERP 9222D, MF
-2 .` : 39800 mig 39800
-3 ' 40300 cmg 40360
-4 41500 cFuig 41600
-5 39800 cFurg 39800
-6. 39500 mig 39500
-7 • 79700 CFU19 39800
Geomean, 44200
.171052 -1 >tudge Gr TS (%) .2.52% 0.01 06/29117 SB 2540 G -TS
-2 2.51 % 0.01
-g 2.483/6 o.0t
-4 2.41 % 0.01
`5 . 2.51 % . 0.01
-6 2.53% . 0.01
-7 - 2.51 _% 0.01
Report' . I
Review
Lab Director Date
219 S. Steele Str. 919 208-4240 .
.Sanford NC 27330 [e-mail]

'219 S. Steele Str_
Sanford, NC 27330
Phone;919-208-4240
Cameron Testing Services, Inc.
NC WWIGW Cert. #654 NC PHHS Cert# 37799 US EPA'NC01918
Chain of Custody
Page of
CQrrmariy:- 4Synagro
Email,
[e-mail]
CTS lab use only
Corifadt: Chad Hayes
Phone:
919-799-0766
Sample Temp o Pral.+-
284g Boger Rd.
.Pax:
Arrive:
_ —
stafe,:Z1?) MoCksville, NC 27028
Motes:
Due:
PYojeet:
Regulatory ulat - - Rush I —
(YIN) (YIN)-
Collectedb "Name:
Signature:
Sample Information
Nurriber of bottles
;Requested Analysis
Sample ID"
m CL -0 x
Z
m `° Q N N
a"
Preservatives: (U)npreserved, H(C)I,
CTS Lab
ID
©E
a
J
N O
H2(S)04, H(N)O3, (Na)Thiosulfate, Na(0)H,
UE
Other (X), Indicate
_
-�
Set 7 (Fec -S, TS)
Q
: --
—
------- - .. _
.. - -
d
Re{ir ui'sh'eda
Receive
ate/Time
Rush work will require prior approval. Additional charges will apply

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
T �pv " Da 11
Date &Analyst
Total Solids
Sample volume..used for total solids,test:
Weight of dish:
Weight of dish + dried solids:
Weight of dried solids:-
Total Solids:
w 'TZrS;
mL
g
g
g
g/L
'°+, `'12053'
w,
r y129:98
0.45
17.928
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
`_ _. 14OOir
w597r�
2
`" 13OU
4
5a73_
3
`- 5143
00
l 5 53 - ry1
4
5
_
7"'
.� �� 14T00
r
4j',74-
8
_....,
4 OOF =
fC_a 449
9
E,: f14r00;
C €4r31i
.10
C. 1r4
0:0
11
,1400.
_3t86L�
fi
12 .
EZVty40Or
=
366 r;
13
�344r
14
00�___'
�21i ` a
15
F, } - 21-199
Oxygen -Consumption Rate 0.21 : mg/L/minute
SOUR 0.69 (mg/g)/hr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
13.875
If sewage sludge is > 20°C, SOUR = U sa (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 7.05 (mg/g)/hr
SOUR passes if result is <_ 1.5 (mg/g)hr
Version 11/1111

City of Lumberton
Specific Oxygen Uptake Rate (SOUR)
Date /Time Collected: TUes •� J� �° g • �5 Q1EYl
Analyst Initial: T / YCL
Sample Location:
=��
©��
=��
©Ems
=Em�
qun
I
�. 9
9
®Rm�
SOUR for Digested Sludge
SOUR for Mixed Liquor
�);n t2. �)rv\I#9
Interpretation of SOUR Test Results for ML Samples
High
This may indicate that there are not enough solids (MLSS) for the COD
> 20 mg 02 / g-MLVSS / Hr
Loading
12 - 20 mg 02 / g-MLVSS / Hr
Normal
This range will usually produce good solids settling and COD removal.
This may indicate that there are too many solids (MLSS) or there has
< 12 mg 02 / g-MLVSS / Hr
Low
been a toxic occurrence.
Try and maintain the sample temperature at 25°C t 1°C during the test. If the temperature is out of the set criterion use the excel
worksheet (labeled "SOUR BLANK Calculations" in the SOURS Tests File on the Desk top) and enter the DO readings. The
temperature compensation formula will correct for the temperature. Print and attach the worksheet
SOUR Procedure for Mixed Liquor Samples:
Collect at least 500mis of the sample to be tested.
Run Total Suspended and Volatile Solids on a Mixed Liquor sample: Follow the steps in the TSSNSS SOP. Other than the solids test,
the procedure is the same for reading the disolved oxygen. See Below.
SOUR Procedure for Digested Sludge for Disposal:
Collect at least 500mis of the sample to be tested. Run Total Solids on sample: Use at least 25mis of sample and follow the steps in
the TS SOP.
Reading the Do:
Pour the remaining sample into a 1 liter beaker with a stir bar, place the beaker on a stir plate on a moderate mixing speed then add an
aeration stone to the beaker and aerate for 5 minutes.
While the sample is being aerated Calibrate the DO Meter.
After 5 minutes of aeration, Pour the aerated sample into a 300ml BOD bottle with a stir bar and place the bottle onto a stir plate. While
mixing, place the BOD probe into the bottle and start to measure the DO.
Wait until meter reading has stabilized (no more than 30 sec) and start recording the DO and Temp every (1) minute for 15 minutes or
until there is no more DO remaining. When all the readings have been recorded, clean bottles, probes and equipment properly.
Proceed with the calculations below to complete test. In the event that the DO is exhausted before the 15 minute mark, use the last
recordable DO reading prior to the oxygen reading zero.
For the Calculation: Use the DO in the last recordable minute and the number of readings. Example: If the oxygen zeroed at the 11
minute mark then you would use the DO that was recorded for the 11th minute and then divide it by 11 because you have eleven
readings total.
S qD — / 1_ = OZ mg/Umin .
Initial DO Reading 15 min DO 15 or # of Oxygen
(mgll) Reading (mgfl) Readings Consumption
Rate
X 60
02 mg/Umin Hour Total Solids
Consumption Rate (mg/L)
X 60
02 mg/Umin Hour MLVSS
Consumption Rate (mglL)
SOUR mg/g/hr
SOUR mg/g/hr
Vector Attraction Reduction Requirements: (listed are the typical Alternatives we use for Sludge Disposal)
Alternative 1: The mass of volatile solids in the sewage sludge shall be reduces by a minimum of 38%.
Alternative 3: If Alternative 1 cannot be met for anaerobically digested sludge, demonstration can be made by digesting a portion of the previously
digested sludge anaerobically in the laboratory in a bench -scale unit for 30 additional days at 20oC. Volatile Solids must be reduced by
less than 15% to demonstrate compliance.
Alternative 4: The specific oxygen rate (SOUR) for sewage sludge treated in an aerobic process shall be equal to or less than 1.5 mg of oxygen per
hour per gram of total solids (dry weight basis) at a temperture of 20oC.
Alternative 6: The pH of sewage sludge shall be rasied to 12 or higher by alkali addition and, without the addition of more alkali shall remain at 12 or
higher for two hours and then at 11.5 or higher for an additional 22 hours.
7/13/16 T.Smith

City of Lumberton
Total Solids Analysis Worksheet
SM 2540 B. 1997
FOR PROCESS CONTROL ONLY
Sample # G
D15.
Checked by: -Sample Day & Date: !21- 1-7
Date & Time IN Oven: T a •2-1 . 1 1 8.2J Qm Date & Time OUT of Oven: 3- L� ��� Co • �Q c�
Analyst(s): Analyst(s):
g = Grams, Wt = Weight Date & Time Completed: W , 3 2 »y-1 -,r-2awn
Dish #
Volume
(MIS)
Tare Wt.
(g)
Tare.+
Sample Wt.
(g)
Sample Wet
Wt.
(g)
Dried Wt.
(g)
'Dried Wt.
Difference
(g)
o
/o
Solids
Total Solids
(Mg/1)
5
120531S
1
0.4gj2_
1.
�--� % Solids Calculation: Total Solids mg/I Calculation:
' Dried Wt. Diff (g) %Total Dried Wt. Diff (g) x 1000 = Total Solids
X 100
Sample Wet Wt. (g) solids Volume (MIS) mg/1
—._:_,_:_.-_ ._._.`--------,--_-_
Section below is to show your work.
03 0 X100. = a =
2z-1. Co1131.� 2 ,.
X 100 =
X 100 = _
1. Initially use 50mis for Known and Unknowns samples and 25mis for regular samples.
2. The sample volume must yeild at least 2.5 mg of residue.
3. To get the Wet Weight; subtract the Tare Weight from the Tare + Sample Weight
Known Certified Value:
Known Value Obtained:
Limit Range:
Revised 8/24116 T. Smith

City of Lumberton
Environmental .Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
`Date & Analyst: 3/22117 8 ,14am ' KCL•' Digester#,2r Day2
Total Solids
Sample -volume used for total solids test: r._,, , ; �._ }25
Weight of dish:
Weight of dish +dried solids_:.-h,• , , ;,,s4i89 10`
Weight'of dried solids: 0.45
Total Solids:, 17.884
mL'
9
9
9
g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
2
3
1+48, i"
4
_..�.._r� 1.17.0
y=
fit �1f 3*
6
1�7�FOOE
t
s` , z 079i =u
7
(' { 1r7
00' r _15
`0's531 � is
9
_.U07�
10
121t7Aa
:
[7HT Or05 w
13
14
18
CL(r x
l
15'
1. J�
Oxygen; Consumption Rate ' 0.16 - mg/L/minute
SOUR 0.54 ' (m9/g)/hr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
-oC
17.125 . •-
If sewagesludge is > 20°C, SOUR = os3 ' ' (mg/g)/hr '
If sewage sludge is <�20°C, SOUR (mg/g)/hr
SOUR passes,if result is <_ 1.5 (mg/g)hr
Version '11/1/11,

City of Lumberton
Specific Oxygen Uptake Rate (SOUR)
Date / Time Collected: �� • ?2 • �� E� Q m
�"� Dy
Analyst Initial: Z) V V L �� C-R n-}y
2
Sample Location: Na -A 2 �exy 2..
©
1 •
0
0
e
rel s
r �r
®�
•
m•
Interpretation of SOUR Test Results for ML Samples
High
This may indicate that there are not enough solids (MLSS) for the COD
> 20 mg OZ / g-MLVSS / Hr
Loading
12 - 20 mg OZ / g-MLVSS / Hr
Normal
This range will usually produce good solids settling and COD removal.
This may indicate that there are too many solids (MLSS) or there has
< 12 mg OZ / g-MLVSS / Hr
Low
been a toxic occurrence.
Try and maintain the sample temperature at 25eC t loC during the test. If the temperature is out of the set criterion use the excel
worksheet (labeled "SOUR BLANK Calculations" in the SOURS Tests File on the Desk top) and enter the DO readings. The
temperature compensation formula will correct for the temperature. Print and attach the worksheet.
SOUR Procedure for Mixed Liquor Samples:
Collect at least 500mis of the sample to be tested.
Run Total Suspended and Volatile Solids on a Mixed Liquor sample: Follow the steps in the TSSNSS SOP. Other than the solids test,
the procedure is the same for reading the disolved oxygen. See Below.
SOUR Procedure for Digested Sludge for Disposal:
Collect at least 500mis of the sample to be tested. Run Total Solids on sample: Use at least 25mis of sample and follow the steps in
the TS SOP.
Reading the Do:
Pour the remaining sample into a 1 liter beaker with astir bar, place the beaker on a stir plate on a moderate mixing speed then add an
aeration stone to the beaker and aerate for 5 minutes.
While the sample is being aerated Calibrate the DO Meter.
After 5 minutes of aeration, Pour the aerated sample into a 300ml Boo bottle with a stir bar and place the bottle onto a stir plate. While
mixing, place the BOD probe into the bottle and start to measure the DO.
Wait until meter reading has stabilized (no more than 30 sec) and start recording the DO and Temp every (1) minute for 15 minutes or
until there is no more DO remaining. When all the readings have been recorded, clean bottles, probes and equipment properly.
Proceed with the calculations below to complete test. In the event that the DO is exhausted before the 15 minute mark, use the last
recordable DO reading prior to the oxygen reading zero.
For the Calculation: Use the DO in the last recordable minute and the number of readings. Example: If the oxygen zeroed at the 11
minute mark then you would use the DO that was recorded for the 11th minute and then divide it by 11 because you have eleven
readings total.
= 02 mg/Umin
Initial DO Reading
15 min DO
15 or # of Oxygen
(mg/1)
Reading (mg/I)
Readings Consumption
Rate
SOUR for Digested Sludge X
60
= SOUR mg/g/hr
Oz mg/Umin
Hour
Total Solids
consumption Rate
(mg/L)
SOUR for Mixed Liquor X
60
= SOUR mg/g/hr
Oz mg/Umin
. Hour
MLVSS
consumption Rate
(mg/L)
Vector Attraction Reduction Requirements: (listed are the typical Alternatives we use for Sludge Disposal)
Alternative 1: The mass of volatile solids in the sewage sludge shall be reduces by a minimum of 38%.
Alternative 3: If Alternative 1 cannot be met for anaerobicaliy digested sludge, demonstration can be made by digesting a portion of the previously
digested sludge anaerobically in the laboratory in a bench -scale unit for 30 additional days at 20aC. Volatile Solids must be reduced by
less than 15% to demonstrate compliance.
Alternative 4: The specific oxygen rate (SOUR) for sewage sludge treated in an aerobic process shall be equal to or less than 1.5 mg of oxygen per
hour per gram of total solids (dry weight basis) at a temperture of 20oC.
Alternative 6: The pH of sewage sludge shall be rasied to 12 or higher by alkali addition and, without the addition of more alkali shall remain at 12 or
higher for two hours and then at 11.5 or higher for an additional 22 hours.
7/13/16 T.Smith

Sample #
City of Lumberton
Total Solids Analysis Worksheet
SM 2540 B. 1997
FOR PROCESS CONTROL ONLY
Checked by: Sample Day & Date:
Date & Time IN Oven: 3 v
- 2. 1- mq(m Date & Time OUT of Oven: ,-" %n • 1-7 @-C.-. 4( - am
Analyst(s): t0 Analyst(s): VI
g = Grams, Wt = Weight
Date & Time Completed:
Dish #
Volume
(MIS)
Tare Wt..
(g)
Tare +
Sample Wt.
(g)
Sample Wet
Wt.
(g)
Dried Wt.
(g)
Dried Wt.
Difference
(g)
%
Solids
Total Solids
(Mg/1)
0
2
, L4 q,1(
I. g 7
% Solids Calculation: Day*2 Total Solids mg/l Calculation:
Dried Wt. Diff (g) X 100 = %Total Dried Wt. Diff (g) x 1000 = Total solids
Sample Wet Wt. (g) solids Volume (MIS) . mg/l
—- I --------®—I -- ---_-I -------„---
Section below is show your work.
0 X100
X 100 = _
X 100 = _
X 100 = _
1. Initially use 50mis for Known and Unknowns samples and 25mis for regular samples.
2. The sample volume must yeild at least 2.5 mg of residue.
3. To get the Wet Weight; subtract the Tare Weight from the Tare + Sample Weight
Known Certified Val
Known Value Obtained:
Limit Range:
RP%/igPH R/9AMA T Cmi+k

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date &Analyst:
Total Solids
Sample volume used for total solids test:
Weight of dish:
Weight of dish + dried solids:
Weight,of dried solids:
Total Solids:
SOUR
13008
—,71030-1- --2,- -
0.44
17.468,
Time
(Minutes)
Temperature
Dissolved
Oxygen (Tg/L)
0C
0
j
2
3
E—Elf
4
5
j"9L0-
.:184�%C-7
6
7
8
Y
.9
L-j
10
AM
OE-,
0884
q4_
12
A
,
M0
m L
9
9
9.
g/L
14
1 15 V
Oxygen Consumption Rate 0.19 md/L/minute
SOUR 0.65 (mg/g)/hr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
0C
19,
If sewage sludge. is > 20°C, SOUR = 4 o ss (mg/g)/hr,
If sewage sludge is < 20°C, SOUR (rng/g)/hr
SOUR passes if result is:5 1.5 (mglg)hr
Version 11/1/11

City of Lumberton
Specific Oxygen Uptake Rate (SOUR)
Date / Time Collected:
Analyst Initial: K® / y4lcll,_
Sample Location:
O
o •
:. •
®row
�ft
®re=a�
0
Interpretation of SOUR Test Results for MIL SamDles
High
This_may. indtc"ate_thatthere_are_not enough solids (MLSS)_for.tha COD _
> 20 mg O2 / g-MLVSS / Hr -
Loading
12 - 20 mg OZ / g-MLVSS / Hr
Normal
This range will usually produce good solids settling and COD removal.
This may indicate that there are too many solids (MLSS) or there has
< 12 mg O, / g-MLVSS / Hr
Low
been a toxic occurrence.
Try and maintain the sample temperature at 25eC t 1eC during the test. If the temperature is out of the set criterion use the excel
worksheet (labeled "SOUR BLANK Calculations" in the SOURS Tests File on the Desk top) and enter the DO readings. The
temperature compensation formula will correct for the temperature. Print and attach the worksheet.
SOUR Procedure for Mixed Liquor Samples:
Collect at least 500mis of the sample to be tested.
Run Total Suspended and Volatile Solids on a Mixed Liquor sample: Follow the steps in the TSSNSS SOP. Other than the solids test,
the procedure is the same for reading the disolved oxygen. See Below.
SOUR Procedure for Digested Sludge for Disposal:
Collect at least 500mis of the sample to be tested. Run Total Solids on sample: Use at least 25mis of sample and follow the steps in
the TS SOP.
Reading the Do:
Pour the remaining sample into a 1 liter beaker with a stir bar, place the beaker on a stir plate on a moderate mixing speed then add an
aeration stone to the beaker and aerate for 5 minutes.
While the sample is being aerated Calibrate the DO Meter.
After 5 minutes of aeration, Pour the aerated sample into a 300ml BOD bottle with a stir bar and place the bottle onto a stir plate. While
mixing, place the BOD probe into the bottle and start to measure the DO.
Wait until meter reading has stabilized (no more than 30 sec) and start recording the DO and Temp every (1) minute for 15 minutes or
until there is no more DO remaining. When all the readings have been recorded, clean bottles, probes and equipment properly.
Proceed with the calculations below to complete test. In the event that the DO is exhausted before the 15 minute mark, use the last
recordable DO reading prior to the oxygen reading zero.
For the Calculation: Use the DO in the last recordable minute and the number of readings. Example: If the oxygen zeroed at the 11
minute mark then you would use the DO that was recorded for the 11th minute and then divide it by 11 because you have eleven
readings total.
= Oz mg/L/min
Initial DO Reading
15 min DO
15 or # of Oxygen
(mg/0
Reading (mg/1)
-
Readings Consumption
Rate
SOUR for Digested Sludge X
60
= SOUR mg/g/hr
Oz mg/Umin
Hour
Total Solids
Consumption Rate
(mg/L)
SOUR for Mixed Liquor X
60
= SOUR mg/g/hr
Os mg/IJmin
Hour
MLVSS
' Consumption Rate
(mglL)
Vector Attraction Reduction Requirements: (listed are the typical Alternatives we use for Sludge Disposal)
Alternative 1: The mass of volatile solids in the sewage sludge shall be reduces by a minimum of 38%.
Alternative 3: If Alternative 1 cannot be met for anaerobically digested sludge, demonstration can be made by digesting a portion of the previously
digested sludge anaerobically in the laboratory in a bench -scale unit for 30 additional days at 20eC. Volatile Solids must be reduced by
less than 15% to demonstrate compliance.
Alternative 4: The specific oxygen rate (SOUR) for sewage sludge treated in an aerobic process shall be equal to or less than 1.5 mg of oxygen per
hour per gram of total solids (dry weight basis) at a temperture of 20'C.
Alternative 6: The pH of sewage sludge shall be rasied to 12 or higher by alkali addition and, without the addition of more alkali shall remain at 12 or
higher for two hours and then at 11.5 or higher for an additional 22,hours.
7/13/16 T.Smith

City of Lumberton
Total Solids Analysis Worksheet
SM 2540 B. 1997
FOR PROCESS CONTROL ONLY
Sample # IS
Dag. -*2
Checked by: S
Sample Day & Date:
Date &Time IN Oven: 1�
S-530 rn Date & Time OUT of Oven:
3 [ 28 (I?
� 2,'•�{S�
Analyst(s):
Analyst(s): '
R Sf
g = Grams, Wt = Weight
Date & Time Completed:
$ l 2? ` -7
(2 5 _ SOS
Dish #
Volume
(MIS)
Tare Wt.
(g)
Tare +
Sample Wt.
(g)
Sample Wet
Wt.
(g)
Dried Wt.
(g)
Dried Wt.
Difference
(g)
o
/o
Solids
Total Solids
(mg/I)
O
23 M.
E 3d .5 -75-
L) .t i (Q
�o
% Solids Calculation: Total Solids mg/I Calculation:
Dried Wt. Diff (g) X 100 = %Total � � Dried Wt. Diff (g) x 1000 = Total Solids
Sample Wet Wt. (g) solids Volume (MIS) mg/1
-----------------------------------------------------------------
Section below is to show your Work.
05 D X 100 = I b � _
22) —1 o
X 100 = _
X 100 —
X 100 = _
1. Initially use 50mis for Known and Unknowns samples and 25mis for regular samples.
2. The sample volume must yeild at least 2.5 mg of residue.
3. To get the Wet Weight; subtract the Tare Weight from the Tare + Sample Weight
Known Certified Value: Known Value Obtained: Limit Range:
Revised 8/24/16 T. Smith

City of Lumberton
Environmental Laboratory
'Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analysfi F '.3r129/F1,78 "03am ; KCLt ;, Digester,,#2' fDay6� , ,.;
Total Solids
Sample volume used for total solids test �,i�`;;' u'- 5
Weight of dish: ~Y. "1r2575:
Weight of dish +dried solids: a`asmr _1>1fi'1a8
Weight of dried solids 0.43
Total Solids:. 17.336
mL
9
9
9
g/L
SOUR
Time
(Minutes)
Temperature
Dissolved'
Oxygen (mg/L)
oC
2
3
=1900'
L:3408 c
4
5
L 1A
00 T`
f.- 2 ^74
.6
'19
00
[ 257r
7
E19
00 <
�7 2447 —
8
C: 1i900
r222�
9
1900I.r2h05i
—
12
15
C' 19?,
'91
Oxygen Consumption Rate ` 0.17 mg/L/minute
SOUR 0.59 (mg/g)/hr
SOUR Temperature, Correction
Average Sewage Sludge
Temperature During Test
oC
19
If sewage sludge is > 20°C, SOUR =! o rr (mg/g)/hr.
If sewage sludge is <20°C, SOUR = o, a (mg/g)/hr
SOUR -passes if -result is 5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Specific Oxygen Uptake Rate (SOUR)
Date / Time Collected: W 3 • �q I-7 °�, IR ; c3
Analyst Initial: ka
Sample Location:
I•
SOUR for Digested Sludge
SOUR for Mixed Liquor
DI,(A t 2 V)av #G
Interpretation of SOUR Test Results for ML Samples
High—
Thismayindicatethatthere. are noteriougtLsolids_(MLSS)_for.the_C.OD_.
> 20 mg 02 / g-MLVSS / Hr
Loading
12 - 20 mg 02 / g-MLVSS / Hr
Normal
This range will usually produce good solids settling and COD removal.
This may indicate that there are too many solids (MLSS) or there has
< 12 mg 02 / g-MLVSS / Hr
Low
been a toxic occurrence.
Try and maintain the sample temperature at 25eC t 1 eC during the test. If the temperature is out of the set criterion use the excel
worksheet (labeled "SOUR BLANK Calculations" in the SOURS Tests File on the Desk top) and enter the DO readings. The
temperature compensation formula will correct for the temperature. Print and attach the worksheet.
SOUR Procedure for Mixed Liquor Samples:
Collect at least 500mis of the sample to be tested.
Run Total Suspended and Volatile Solids on a Mixed Liquor sample: Follow the steps in the TSSNSS SOP. Other than the solids test,
the procedure is the same for reading the disolved oxygen. See Below.
SOUR Procedure for Digested Sludge for Disposal:
Collect at least 500mis of the sample to be tested. Run Total Solids on sample: Use at least 25mis of sample and follow the steps in
the TS SOP.
Reading the Do:
Pour the remaining sample into a 1 liter beaker with a stir bar, place the beaker on a stir plate on a moderate mixing speed then add an
aeration stone to the beaker and aerate for 5 minutes.
While the sample is being aerated Calibrate the DO Meter.
After 5 minutes of aeration, Pour the aerated sample into a 300ml BOD bottle with a stir bar and place the bottle onto a stir plate. While
mixing, place the BOD probe into the bottle and start to measure the DO.
Wait until meter reading has stabilized (no more than 30 sec) and start recording the DO and Temp every (1) minute for 15 minutes or
until there is no more DO remaining. When all the readings have been recorded, clean bottles, probes and equipment properly.
Proceed with the calculations below to complete test. In the event that the DO is exhausted before the 15 minute mark, use the last
recordable DO reading prior to the oxygen reading zero.
For the Calculation: Use the DO in the last recordable minute and the number of readings. Example: If the oxygen zeroed at the 11
minute mark then you would use the DO that was recorded for the 11th minute and then divide it by 11 because you have eleven
readings total.
3.145 — , (::0 / = OZ mg/L/min
Initial DO Reading 15 min DO 15 or # of Oxygen
(mgll) Reading (mg/l) Readings Consumption
Rate
X 60 = SOUR mg/g/hr
02 mglUrnin Hour Total Solids
Consumption Rate (mglL)
X 60 = SOUR mg/g/hr
Oz mg1Umin Hour MLVSS
Consumption Rate (mglL)
Vector Attraction Reduction Requirements: (listed are the typical Alternatives we use for Sludge Disposal)
Alternative 1: The mass of volatile solids in the sewage sludge shall be reduces by a minimum of 36%.
Alternative 3: If Alternative 1 cannot be met for anaerobically digested sludge, demonstration can be made by digesting a portion of the previously
digested sludge anaerobically in the laboratory in a bench -scale unit for 30 additional days at 20eC. Volatile Solids must be reduced by
less than 15% to demonstrate compliance.
Alternative 4: The specific oxygen rate (SOUR) for sewage sludge treated in an aerobic process shall be equal to or less than 1.5 mg of oxygen per
hour per gram of total solids (dry weight basis) at a temperture of 20eC.
Alternative 6: The pH of sewage sludge shall be rasied to 12 or higher by alkali addition and, without the addition of more alkali shall remain at 12 or
higher for two hours and then at 11.5 or higher for an additional 22 hours.
7/13/16 T.Smith

Sample #
City of Lumberton
Total Solids Analysis Worksheet
SM 2540 B. 1997 ;
FOR PROCESS CONTROL ONLY
Checked by: Sample Day & Date: �1 �Y �.} 29 • 0�
Date & Time IN Oven: + L_"9 1 -leg; �(Dav�n Date &.Time OUT of Oven: � � • � • ��e�•®I Clf�c�
Analyst(s): Analyst(s):
g = Grams, Wt = Weight -Date & Time Completed: • .� • �� ��� Cktf�
Dish #
Volume
(MIS)
:Tare Wt.
(g)
Tare +
Sample Wt..
(g)
Sample Wet
Wt.
(g)
,
Dried Wt.
(g)
=Dried Wt.
Difference
(g)
o
/o
Solids
Total Solids
(mg/1)
25
05
ORWAC23,91
a., is i u
0
% Solids Calculation: Total Solids-mg/l Calculation:
Dried Wt. Diff (g)' X 100 —_ 'O/c y Dried Wt.-Diff (g)'X 1000 ' = Total solids
Sample Wet Wt. (g) solids Volume (MIS) Mgt[
Section below is to show your work.o -
X 100
23.q t6s
X 100 =
X 100 _
X 100. _
I. Initially use 50mis for Known and Unknowns samples and 25mis for"regular samples.
2. The sample volume must yeild at least 2.5 mg of residue. .
3. To get the Wet Weight; subtract the Tare Weight from the Tare + Sample Weight
Known Certified Value:, Known Value Obtained: Limit Range:
Revised 8/24116'T. Smith-

City.of Lumberton
Envillonment'al Labor6tory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date 8, Analyst:
­_­7­­0
Total Solids
Sample volume used for total solidstest:
Weight of dish:
Weight of dish + dried solids:
Weight of dried solids-.
Total Solids:
SOUR
0.44
17.516
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
aC
0
2
r
3
4
5
4�
6
7-
8
511
fli_," _,714R
T
10
`7 2_gj
12
13
IF
14
15
mL
9
9
9
g/L
Oxygen -Consumption Rate 0.13 mg/L/minute
SOUR 0.44 (mg/g)/hr
SOUR Temperature Correction
Average Sewage Sludge
-Temperature During Test
0C
19
If sewage sludge is > 20°C, SOUP, = o (mg/g)/hr
If sewage sludge is < 20°C, SOUR = o r4 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1111

Date / Time Collected:
Analyst Initial
Sample Location:
=
=L1✓`—J�
©UMM�
©
M�
M
'm
Lq Me
�m
��41
®
a*
SOUR for Digested Sludge
SOUR for Mixed Liquor
City of Lumberton
Specific Oxygen Uptake Rate (SOUR)
Rt< / �Jcc / KcL
4-7
Interpretation of SOUR Test Results for ML Samples
--
-_High - -
Ibis may.iridiicate thatthere_a[e-notenough_solids-(MLS.S)-for_the_COD._
> 20 mg OZ / g-MLVSS / Hr
Loading
12 - 20 mg OZ / g-MLVSS / Hr
Normal
This range will usually produce good solids settling and COD removal.
This may indicate that there are too many solids (MLSS) or there has
< 12 mg 02 / g-MLVSS / Hr
Low
been a toxic occurrence.
Try and maintain the sample temperature at 260C t 1eC during the test. If the temperature is out of the set criterion use the excel
worksheet (labeled "SOUR BLANK Calculations" in the SOURS Tests File on the Desk top) and enter the DO readings. The
temperature compensation formula will correct for the temperature. Print and attach the worksheet
SOUR Procedure for Mixed Liquor Samples:
Collect at least 500mis of the sample to be tested.
Run Total Suspended and Volatile Solids on a Mixed Liquor sample: Follow the steps in the TSSNSS SOP. Other than the solids test,
the procedure is the same for reading the disolved oxygen. See Below.
SOUR Procedure for Digested Sludge for Disposal:
Collect at least 500mis of the sample to be tested. Run Total Solids on sample: Use at least 25mis of sample and follow the steps in
the TS SOP.
Reading the Do:
Pour the remaining sample into a 1 liter beaker with a stir bar, place the beaker on a stir plate on a moderate mixing speed then add an
aeration stone to the beaker and aerate for 5 minutes.
While the sample is being aerated Calibrate the DO Meter.
After 5 minutes of aeration, Pour the aerated sample into a 300ml BOD bottle with a stir bar and place the bottle onto a stir plate. While
mixing, place the BOD probe into the bottle and start to measure the DO.
Wait until meter reading has stabilized (no more than 30 sec) and start recording the DO and Temp every (1) minute for 15 minutes or
until there is no more DO remaining. When all the readings have been recorded, clean bottles, probes and equipment properly.
Proceed with the calculations below to complete test. In the event that the DO is exhausted before the 15 minute mark, use the last
recordable DO reading prior to the oxygen reading zero.
For the Calculation: Use the DO in the last recordable minute and the number of readings. Example: If the oxygen zeroed at the 11
minute mark then you would use the DO that was recorded for the 11th minute and then divide it by 11 because you have eleven
readings total.
-
3 .cco
15 = 02 mg/L/min
Initial DO Reading
15 min DO
15 or # of Oxygen
(MA
Reading (mg/1)
Readings Consumption
Rate
X
60
= SOUR mg/g/hr
Oz mg/L/min
Hour
Total Solids
consumption Rate
(mg/L)
X
60
= SOUR mg/g/hr
Oz mg/L/min
Hour
MLVSS
Consumption Rate
(mg/L)
Vector Attraction Reduction Requirements: (listed are the typical Alternatives we use for Sludge Disposal)
Alternative 1: The mass of volatile solids in the sewage sludge shall be reduces by a minimum of 38%.
Alternative 3: If Alternative 1 cannot be met for anaerobically digested sludge, demonstration can be made by digesting a portion of the previously
digested sludge anaerobically in the laboratory in a bench -scale unit for 30 additional days at 20oC. Volatile Solids Must be reduced by
less than 15% to demonstrate compliance.
Alternative 4: The specific oxygen rate (SOUR) for sewage sludge treated in an aerobic process shall be equal to or less than 1.5 mg of oxygen per
hour per gram of total solids (dry weight basis) at a temperture of 20eC.
Alternative 6: The pH of sewage sludge shall be rasied to 12 or higher by alkali addition and, without the addition of more alkali shall remain at 12 or
higher for two hours and then at 11.5 or higher for an additional 22 hours.
7/13/16 T.Smith

Checked by:
City of Lumberton
Total Solids Analysis Worksheet
SM 2540 B. *1997
FOR PROCESS CONTROL ONLY
Sample #
15*2
Sample Day & Date: �ht`►r 3 • ?ICJ - 1-7
Date & Time IN Oven: S 5 -orn Date & Time OUT of Oven:
Analyst(s): KCL Analyst(s):
g = Grams, Wt = Weight Date & Time Completed: _
Dish #
Volume
(MIS)
Tare Wt.
(g)
Tare +
Sample Wt.
(g)
Sample Wet
Wt.
(g)
Dried Wt(g) .
Dried Wt.
Difference
(g)
%
Solids
Total Solids
(Mg/1)
04
251
n
0.4379
% Solids Calculation: Total Solids mg/I Calculation:
Dried Wt. Diff (g) X 100 = %TotalDried Wt. Diff (g) x 1000 = Total solids
Sample Wet Wt. (g) solids Volume (MIS) mg/I
-----------------------------------------------------------------
Section below is to show your work.
OO4 0 A sr)9 X 100
24.0322
x 100 =
X 100 =
X 100 . =
1. Initially use 50mis for Known and Unknowns samples and 25mis for regular samples.
2. The sample volume must yeild at least 2.5 mg of residue.
3. To get the Wet Weight; subtract the Tare Weight from the Tare + Sample Weight
Known Certified Value: Known Value Obtained:
Limit Range:
Revised 8/24/16 T. Smith

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Lumberton WQ Permit Number: WQ0000672
WWTP Name: City of Lumberton WWTP NPDES Number: NCO024571
Monitoring Period: From 07/01/17 To 09/30/17
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If nnnlirnhle to alternative nerformed (Class A or Class R) comnlete the following monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6 th
MPN
MPN/g
Coliform
power per gram
of total solids
<87000
<87500
<87700
CFU/g
0
quarterly
grab
9222D
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0ption/Alt. 1
Option/Mt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake) X
Option/Alt. 5
Option/Alt. 6
/Al
Optiont _7- Option/Alt. 8
(14-Day Aerobic)
'(Alk Stabilization)
.(Drying—. Stable)' (Drying — Unstable) _
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification inclding fine and imprisonment."
Corey Walters, Assistant Director of EUS Dept.
Preparer/Name and Title (Type or print)
Signature of Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Cameron Testing Services, Inc. Laboratory Report
NC DENR #654
NC PHHS #37799
US EPA #NC0191 B
Client° �=
Synagro �Ts PF j
171293
r
Pro]ecfi
Lumberton rdegUlat01'/'
Yes
Sample Information
4j Samptt�
C. Hayes
Date 08/03/17 Recetver3.
M. 511115 -Date.
08/03/17
4
Analyses and Results
a�: V�
tLab II] ';
Sain teilD
1= r Analyte Result;
fl
Refierence
171293 01
-1
Mudge Gr Fec. Coliform-S <87700 CFUra
87700 08103/17 SB
92221D - MF
-2
<87700 CFU/9
87700
-3
<87000 CFU/9
87000
-4
.<87700 CFU1g
87700
-5
<87700 CFU/9
87700
-6
<87000 cr•Utg
87000
-7
<87700 CrU1a
87700
Geomean <87500
171293 01
-1
Mudge Gr TS (%) 1.14%.
a.0i 08/07/17 ERP
2540 G TS
-2
1.14%
0.01
-3
1.15%
o.ot
-4
1.14%
0.01
_5
1,14%
0.01
-6
1.15%
0.01
-7
1.14%
0.01
Report
Review
Lab Director ^� Date
919-208-4240
219 S. Steele Sir.
clrris
Sanford NC 2733b _ ci camerontestin�.com

219 S. Steele str. Cameron Testing Services, Inc. Chain of Custody
Sanford, NC 27330 NG WW/GW Gert. #654 NC PHHS Cert# 37799 US EPA NCO1918 Page of
Phone [phone]
Y
.
4
}{.. iGtTSIabNYS
[
nMr, �'tlyt:1
s3k k�ry�Yf57j t13 A:t t 1�15.
Y
n1:a�i,, ty +r'
`;,�-�,y�'��
r}i LTA.4l4 `
�.,��
P�o
Cam• GS/—�^^•[,��
��y} c, �y
(_S J / -! �. Ca � �O �
i tSf ,
kSamples
� ���•"-(Gl�
"tl ll.. f11.�1 .. 1
� '
i ;' k ur I
It {��tU�3F£�{3�4
,.
rid 'ass" SS�}���yy
(ON,
_—. -
qq
Y�t�x s.�.l
z
Fax ;
'��`-�,
� ✓�� rs-.}Cj-sS a;
t y N �;
" � r�r
{� }i..
1
t c'c'��S
'arrive
"'
1
.��i
1
S te>1
� _ y
�
� I,{Ay,,
PM
i
�4Rushrt,
�rRegulatory
VIM
I
�Coli�Jtedj�), j Name
��
.
gnature.
� na
Si9
.. .. .. ,.
•e:, r. .z M:.:Fr"c, r-.•-=.r.
.,... .,..-..-...,._.�. ..,,,.,r..r c.:.f:.;i .-..- v .....•-...,' �•�, r's�•:^. ";:y;•c-, 1. r� 'r 1' . �.,•Ya .4� �,'i.'�Y -,F �. •Fi.
i!kd T� -1. ..r.T�f',:�^', .,�,{'4.. .Sl: l a P r C.� :�-" i f_ J,. t.. :�-r^ ^'.a f..iu�+'C; a.,:.. + i, w;i:� f,�,;•,:,
NumberAof�boitles 4 1 , equ>sted Analy��s i, ,
� ) 7�
h Il Llf 'I} 1 f j
�hl ..f 41 ry I`rF�l T.t IJ7�+ NyRI ram, r'.
Q L Z
@
o > -
a
Preservatrves (U)npreseNed
H2(3)O4, Fi(NjO3"(Na}Thiosul#ate;
Sample �❑
p
i
❑ i 0 �,
-
N. i m r
o O
f.?o?fe?
I
--; -
07
,
I
A r� I
..r-.....:.. r.� V
7�p ::,y: .�,1 ,..� �a�:: �} .4 - ,� , 5 -.r �� -, ,4 ��x I`'. _�•.Kr:.:n --:.,� s..��;Rece>Irred.<���.:�,.Datel�T>;r1.b, .�:;,,1.. ��?.�:w. _r�,r_�•.:
�c d5'.5.1`.,1 -
'RTnl tl,':II.' Y�.CJB.►].1•
.tii :.Iv,LY ,.c,. ..3..f ,f. 2w...,.d: ... r..
Rush work will require prior approval. Additional charges will apply

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst:
Total Solids
Sample volume used for total solids test:
Weight of dish:
Weight of dish + dried solids:
Weight of dried solids:
Total Solids:
SOUR
E _ '25.
:n
0.26
10.484
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
E_ 23 00
2
3
9
�`; - 23,ti0�03 -.
C`` 749 -- --
10
-
t� - _ °23f U0f
i _ : _ -7547
12
13
1428�OOii.:_.
_Z351V-
15
t� -,.,_ :23v0,0a -`
- '73.3; .
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
mL
9
9
9
g/L
0.04 mg/L/minute
0.24 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
23
If sewage sludge is > 20 C, SOUR = 0. (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0 20 (mg/g)/hr
SOUR passes if result is 51.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Specific Oxygen Uptake Rate (SOUR)
Date & Time Collected: `®• C�_M Collected by: ?h K.CrAL
Sample Location: A?s d'V- t Day # : I
02 Uptake performed by: KC L
Interpretation of SOUR Test Results for ML Samples
High
This may indicate that there are not enough solids (MLSS) for the COD
> 20 mg OZ / g-MLVSS / Hr
Loading
Normal
This range will usually produce good solids settling and COD removal.
12 - 20 mg OZ / g-MLVSS / Hr
This may indicate that there are too many solids (MLSS) or there has
< 12 mg OZ / g-MLVSS / Hr
I Low
been a toxic occurrence.
Try and maintain the sample temperature at 25°C t 1°C during the test. If the temperature is out of the set criterion use the excel
worksheet (labeled "SOUR BLANK Calculations" in the SOURS Tests File on the Desk top) and enter the DO readings. The temperature
compensation formula will correct for the temperature. Print and attach the worksheet.
SOUR Procedure for Mixed Liquor Samples:
Collect at least 500mis of the sample to be tested.
Run Total Suspended and Volatile Solids on a Mixed Liquor sample: Follow the steps in the TSSIVSS SOP. Other than the solids test,
the procedure is the same for reading the disolved oxygen. See Below.
SOUR Procedure for Digested Sludge for Disposal:
Collect at least 500mis of the sample to be tested. Run Total Solids on sample: Use at least 25mis of sample and follow the steps in
the TS SOP.
Reading the Do:
Pour the remaining sample into a 1 liter beaker with a stir bar, place the beaker on a stir plate on a moderate mixing speed then add an
aeration stone to the beaker and aerate for 5 minutes.
While the sample is being aerated Calibrate the DO Meter.
After 5 minutes of aeration, Pour the aerated sample into a 300ml Boo bottle with a stir bar and place the bottle onto a stir plate. While
mixing, place the Boo probe into the bottle and start to measure the DO.
Wail until meter reading has stabilized (no more than 30 sec) and start recording the DO and Temp every (1) minute for 15 minutes or
until there is no more DO remaining. When all the readings have been recorded, clean bottles, probes and equipment properly. Proceed
with the calculations below to complete test. In the event that the DO is exhausted before the 15 minute mark, use the last recordable
DO reading prior to the oxygen reading zero.
For the Calculation: Use the DO in the last recordable minute and the number of readings. Example: If the oxygen zeroed at the 11
minute mark then you would use the DO that was recorded for the 1 ith minute and then divide it by 11 because you have eleven
readings total.
�g
Date & Time IN Oven: 3/� �� I I • `1 ClrYl Analyst: L L�CL
Date & Time OUT of Oven: 113 l -7 9 3 30 M Analyst: TC�S
Date & Time Complete: (3� t �? Analyst: ZS
Dish
Volume
Tare Wt.
Tare + Sample
Sample Wet
Dried Wt.
Dried Wt. Diff.
%
Total Solids
#
(MIS)
(g)
Wt. (g)
Wt. (g)
(g)
(g)
Solids
(ml
_6-D
g = Grams, Wt = Weight
% Total Solids Calculation:
Dried Wt. Diff (g)
X 100 = %Total Solids
Sample Wet Wt. (g)
lector Attraction Reduction:
Total Solids mg/I Calculation:
Dried Wt. Diff (g) x 1000 _
— Total Solids mg/I
Volume (mis)
The specific oxygen rate (SOUR) for sewage sludge treated in an aerobic process shall be equal to or less than 1.5 mg of oxygen per hour
Alternative 4: per gram of total solids (dry weight basis) at a temperture of 20°C.
41612017

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
"
Date & Analyst: Lx .,
Total Solids
Sample volume used for total solids test:
Weight of dish: 2
Wejght of'dish + dried solids:
Weight of dried solids: 0.42
Total Solids: 17
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L).
0C
0
j_
L
101 'Z
2
A-0 —I.
�12
3
4
L
5
6
7,
-,Z3101F�� ;, 7--1
-"F., Bf,
8
L1-- AZ
7,
9
3 01�,' �10_
10
12
13
i229Q0L==31F--,
14
- - I- - - -, -.-
15
3 QQL' Zj
JLt
mL
9
9
9
g/L
Oxygen Consumption Rate 0.04 mg/L/minute
SOUR 0.14 (mg/g)/hr
SOUR Temperatdre,Correction
Average Sewage Sludge
Temperature During Test
oc
23
If sewage sludge is > 20°C, SOUR =
If sewage sludge is < 20°C, SOUR =
SOUR passes if result is:5 1.5 (mg/g)hr
(mg/g)/hr
(mg/g)/hr
Version 11/1/11

City of Lumberton
Specific Oxygen Uptake Rate (SOUR)
Date & Time Collected: • �' i� @1 S : 30ck rn Collected by: 'DL / KCL,
Sample Location: Aa Day # :
02 Uptake performed by: h.CL
w
•
©®
©ilil
M—
M
©MDM—
OEM
MI7F
W
MqWa
a1=*A—
wmm�,'
•
WON
®fulm
®WI
®mm
Interpretation of SOUR Test Results for ML Samples
High
This may indicate that there are not enough solids (MLSS) for the COD
> 20 mg Oz / g-MLVSS / Hr
Loading
Normal -
This range will usually produce good solids settling and COD removal.
12 - 20 mg Oz / g-MLVSS / Hr
This may indicate that there are too many solids (MLSS) or there has
< 12 mg 021 g-MLVSS / Hr
Low
been a toxic occurrence.
Try and maintain the sample temperature at 25°C t 1°C during the test. If the temperature is out of the set criterion use the excel
worksheet (labeled "SOUR BLANK Calculations' in the SOURS Tests File on the Desk top) and enter the DO readings. The temperature
compensation formula will correct for the temperature. Print and attach the worksheet.
SOUR Procedure for Mixed Liquor Samples:
Collect at least 500mis of the sample to be tested.
Run Total Suspended and Volatile Solids on a Mixed Liquor sample: Follow the steps in the TSSNSS SOP. Other than the solids test,
the procedure is the same for reading the disolved oxygen. See Below.
SOUR Procedure for Digested Sludge for Disposal:
Collect at least 500mis of the sample to be tested. Run Total Solids on sample: Use at least 25mis of sample and follow the steps in
the TS SOP.
Reading the Do:
Pour the remaining sample into a 1 liter beaker with a stir bar, place the beaker on a stir plate on a moderate mixing speed then add an
aeration stone to the beaker and aerate for 5 minutes.
While the sample is being aerated Calibrate the DO Meter.
After 5 minutes of aeration, Pour the aerated sample into a 300ml BOD bottle with a stir bar and place the bottle onto a stir plate. While
mixing, place the BOD probe into the bottle and start to measure the DO.
Wait until meter reading has stabilized (no more than 30 sec) and start recording the DO and Temp every (1) minute for 15 minutes or
until there is no more DO remaining. When all the readings have been recorded, clean bottles, probes and equipment properly. Proceed
with the calculations below to complete test. In the event that the DO is exhausted before the 15 minute mark, use the last recordable
DO reading prior to the oxygen reading zero.
For the Calculation: Use the DO in the last recordable minute and the number of readings. Example: If the oxygen zeroed at the 11
minute mark then you would use the DO that was recorded for the 11th minute and then divide it by 11 because you have eleven
readings total,
VY n
Date & Time IN Oven: S • 0 ' 1-7�. 9 •52 t �
Date & Time OUT of Oven: ! h 1 1 ( -7 en
Date & Time Complete: J` 3 l t Z �'• fYJ to r�
Analyst:
Anil„�+• Z S
Analyst: - -IC S
Dish
#,
Volume
(MIS)
Tare Wt.
(g)
Tare + Sample
Wt. (g)
Sample Wet
Wt. (g)
Dried Wt.
(g)
Dried Wt. Diff..
(g)
%
Solids
Total Solids
(Mgt])
1q
25
G2 . G311-7.
UP3
, o �.
qS - AD F 3
0 4M�
I - (0 q °o
g = Grams, Wt = Weight
% Total Solids Calculation:
Dried Wt. Diff (g)
Sample Wet Wt. (g)
rector Attraction Reduction:
X 100 = % Total Solids
Total Solids mg/I Calculation:
Dried Wt. Diff (g); ,x 1000 _
i— Total Solids mg/I
Volume (MIS)
The specific oxygen rate (SOUR) for sewage sludge treated in an aerobic process shall be equal to or less than 1.5 mg of oxygen per hour
Alternative 4: per gram of total solids (dry weight basis) at a temperture of 20oC.
4/6/2017

City of Lumberton
Environmental .Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date &Analyst: i`. ;;< r6/1h17,84Qam; µ, RCL
Total Solids
Sample volume used for total solids test:
Weight of dish:
Weight of dish + dried solids:
Weight of dried solids:
Total Solids:
SOUR
0.25
9.976
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
23}-00' - =
L �794 ._,L_._.
2
{ ` i ^ 23t 001 i
C '785
3
4
2300` i
t: 77�7�
5
i 23€UO �!
L J7X75� --
6
I 7I:7r2
7
!t 23'00a LIE,-
F 7766P
8
62
9
1. 23�'00 a�
"
`7:r57
10
12
j' w 23� 0_OY '
L,� 7, 46
13
2300 - 1
i r7.4r4r —
14
{ ^ 23'00
7^ 41:_
15
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
oC
23
mL
9
9
9
g/L .
0.04 mg/L/minute
0.23 (mg/g)/hr
If sewage sludge is > 20°C, SOUR =0..20 ' (mg/g)/hr
If sewage sludge is < 20°C, SOUR = o. 9; (mg/g)/hr
SOUR passes if result is <_ 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Specific Oxygen Uptake Rate (SOUR)
Date & Time Collected: �—j �•• "' o 0Xn Collected by: W L K(� L
Sample Location: A R # Day
02 Uptake performed by: 11111—C-L
Interpretation of SOUR Test Results for ML Samples
High
This may indicate that there are not enough solids (MLSS) for the COD
> 20 mg Oz / g-MLVSS I Hr
Loading
12 - 20 mg 02 / g-MLVSS / Hr
Normal
This range will usually produce good solids settling and COD removal.
This may indicate that there are too many solids (MLSS) or there has
< 12 mg OZ / g-MLVSS / Hr
Low
been a toxic occurrence.
Try and maintain the sample temperature at 25°C i 1°C during the test. If the temperature is out of the set criterion use the excel
worksheet (labeled "SOUR BLANK Calculations" in the SOURS Tests File on the Desk top) and enter the DO readings. The temperature
compensation formula will correct for the temperature. Print and attach the worksheet.
SOUR Procedure for Mixed Liquor Samples:
Collect at least 500mis of the sample to be tested. '
Run Total Suspended and Volatile Solids on a Mixed Liquor sample: Follow the steps in the TSS/VSS SOP. Other than the solids test,
the procedure is the same for reading the disolved oxygen. See Below.
SOUR Procedure for Digested Sludge for Disposal:
Collect at least 500mis of the sample to be tested. Run Total Solids on sample: Use at least 25m1s of sample and follow the steps in
the TS SOP.
Reading the Do:
Pour the remaining sample into a 1 liter beaker with a stir bar, place the beaker on a stir plate on a moderate mixing speed then add an
aeration stone to the beaker and aerate for 5 minutes.
While the sample is being aerated Calibrate the DO Meter.
After 5 minutes of aeration, Pour the aerated sample into a 300ml SOD bottle with a stir bar and place the bottle onto a stir plate. While
mixing, place the Boo probe into the bottle and start to measure the DO,
Wait until meter reading has stabilized (no more than 30 sec) and start recording the DO and Temp every (1) minute for 15 minutes or
until there is no more DO remaining. When all the readings have been recorded, clean bottles, probes and equipment properly. Proceed
with the calculations below to complete test. In the event that the DO is exhausted before the 15 minute mark, use the last recordable
DO reading prior to the oxygen reading zero.
For the Calculation: Use the DO in the last recordable minute and the number of readings. Example: If the oxygen zeroed at the 11
minute mark then you would use the DO that was recorded for the 11th minute and then divide it by 11 because you have eleven
readings total.
Date & Time IN Oven: IGO ' E @ l R �. � � 4 kla)
Date & Time OUT of Oven: (n � A -7
Date & Time Complete: (e � ( /(-7
Analyst:
YC�-
Analyst:
Z S
Analyst:
-FZ
Dish
Volume
Tare Wt.
Tare + Sample
Sample Wet
Dried Wt.
Dried Wt. Diff.
%
Total Solids
#
(mis)
(g)
Wt. (g)
Wt. (g)
(g)
(g)
Solids
(mg/1)
% Total Solids Calculation:
Dried Wt. Diff (g) X 100 = % Total Solids
Sample Wet Wt. (g)
'(ectorAttraction Reduction:
Total Solids mg/I Calculation:
Dried Wt. Diff (g) x 1000
= Total Solids mg/I
Volume (MIS)
The specific oxygen rate (SOUR) for sewage sludge treated in an aerobic process shall be equal to or less than 1.5 mg of oxygen per hour
Alternative 4: per gram of total solids (dry weight basis) at a temper(ure of 20°C.
4/6/2017

/
��^�«x m� Lumberton
��^�
=U"� v�v ~.�00=��" ~=n
Environmental
�mK Laboratory
���m`
~~���V���K���==" �.==��"=~~^ry
Specific Oagen Uptake Rate (SOUR) Worksheet
Oab*&Anolyot 0`�/
Total Solids
Sample volume used for total solids test:
Weight ofdish:
Weight ofdish + dried solids:
Weight ofdried solids:
Total Solids:
mL
Q
g
g
�g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
0C
OL
'84-
12
13
0-
14
15
Oxygen Consumption Rate 0.04 inuta
' SOUR 0.24 hng/gVhr
SOUR Temperature Correction
Temperature During Test
23
Ifsewage sludge ka>2O'C.SOUR
= r
|faovwageu|udgeka<20"C.SOUR= g/gVhr
SOUR passes ifresult io:51'5(nglg)hr
Version 11/1 /11

City of Lumberton
Specific Oxygen Uptake Rate (SOUR)
We & Time Collected: f7 • B ?k ow n Collected by: 3_ V u /Y-C—L
Sample Location: AR # Day # : 4
02 Uptake performed by: C—L
of
0
M.
a.
'
a=WARI'
E
IN
0-o'bre"WRIal
WSW
W
®aMIN
Intemretatlon of SOUR Test Results for ML Samples
High
This may indicate that there are not enough solids (MLSS) for the COD
> 20 mg 021 g-MLVSS / Hr
Loading
Normal
This range will usually produce good solids settling and COD removal.
12 - 20 mg 02 / g-MLVSS / Hr
This may Indicate that there are too many solids (MLSS) or there has
< 12 mg 021 g-MLVSS / Hr
Low,
been a toxic occurrence.
Try and maintain the sample temperature at 25°C i 1°C during the test. If the temperature is out of the set criterion use the excel
worksheet (labeled "SOUR BLANK Calculations" in the SOURS Tests File on the Desk top) and enter the DO readings. The temperature
compensation formula will correct for the temperature. Print and attach the worksheet.
SOUR Procedure for Mixed Liquor Samples:
Collect at least 50.Omis of the sample to be tested.
Run Total Suspended and Volatile Solids on a Mixed Liquor sample: Follow the steps in the TSSNSS SOP. Other than the solids test,
the procedure is the same for reading the disolved oxygen. See Below.
SOUR Procedure for Digested Sludge for Disposal:
Collect at least 500mis of the sample to be tested. Run Total Solids on sample: Use at least 25mis of sample and follow the steps in
the TS SOP.
Reading the Do:
Pour the remaining sample into a 1 liter beaker with a stir bar, place the beaker on a stir plate on a moderate mixing'speed then add an "
aeration stone to the beaker and aerate for 5 minutes.
While the sample is being aerated Calibrate the DO Meter.
After 5 minutes of aeration, Pour the aerated sample into a 300ml BOD bottle with a stir bar and place the bottle onto a stir plate. While
mixing, place the Boo probe into the bottle and start to measure the DO.
Wait until meter reading has stabilized (no more than 30 sec) and start recording the DO and Temp every (1) minute for 15 minutes or
until there is no more DO remaining. When all the readings have been recorded, clean bottles, probes and equipment properly. Proceed
with the calculations below to complete test. In the event that the DO is exhausted before the 15 minute mark, use the last recordable
DO reading prior to the oxygen reading zero.
For the Calculation: Use the DO in the last recordable minute and the number of readings. Example: If the oxygen zeroed at the 11
minute mark then you would use the DO that was recorded for the 11th minute and then divide it by 11 because you have eleven
readings total.
^-� i" n
Date & Time IN Oven: � ' ' 1 1 ��� �l ' �-7 Q1M
Date & Time OUT of Oven: G - 2 • D \`� , ` 3 I am
Date & Time Complete: CD • 2 - o F 2' OStDm
11
Analvst: YIU
Analyst: KCA_
Analyst:
V-CA—
Dish
#
Volume
(MIS)
Tare Wt.
(9)
Tare + Sample
Wt. (g)
Sample Wet
Wt. (I
Dried Wt.
(9)
Dried Wt. Diff.
(g)
%
Solids
Total Solids
(mg/1)
11012.5
1111
"-kS-cl401
1111 Cos -IL
o.aggl
I - o.qq 010
g = Grams, Wt = Weight
% Total Solids Calculation:
Dried Wt. Diff (g)
Sample Wet Wt. (g)
lector Attraction Reduction:
X 100 = % Total Solids
Total Solids mg/I Calculation:
Dried Wt. Diff (g) x 1000
Volume (MIS) Total Solids mg/1
The specific oxygen rate (SOUR) for sewage sludge treated in an aerobic process shall be equal to or less than 1.5 mg of oxygen per hour
Alternative 4: per gram of total solids (dry weight basis) at a temperture of 20°C.
4/6/2017

City of Lumberton
Environmental Laboratory
Specific OxVqen Uptake Rate (SOUR) Worksheet
Date & Analyst: .4 X Total Solids
Sample volume used for total solids test:
Weight of dish:
Weight of dish + dried solids:
Weight of dried solids:
Total Solids:
:25
mL
g
g
g
0.33
13.36g/l-
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
0C
.0
E
A
2
4
A
3
'4000
L'%
4
r 24r`U:O
5
6
L�
A
NO
8
- - ----- -----
0"y
9
10
4
t7
-
E, --
11
4t�
9
E71.
12
L..,. -
13
",—Z
00
Fr 7
14
Z
QQ�
7,:
U84
15
It, 7
Oxygen Consumption Rate 0.03 mg/L/minute
SOUR 0.14. (mg/g)/hr
SOUR Temperaftire Correction
Average Sewage Sludge
Temperature During Test
0C
24
If sewage sludge is > 20'C, SOUR = R (mg/g)/hr
If sewage'sludge is < 20°C, SOUR = -�m,, EL01 E (mg/g)/hr
SOUR passes if result is 1.5 (mg/g)hr
Version 11/1111

City of Lumberton
Specific Oxygen Uptake Rate (SOUR)
Date & Time Collected: Collected by: W —
Sample Location: Al� -t1 bay # : 15
02 Uptake performed by: KC —L—
a
•
WE
n
•
e
•
amm
I f�
M
l
o
elm
®
NO
®
4
Interpretation of SOUR Test Results for ML Samples
High
This may indicate that there are not enough solids (MLSS) for the COD
> 20 mg 02 / g-MLVSS / Hr
Loading
12 - 20 mg OZ / g-MLVSS / Hr
Normal
This range will usually produce good solids settling and COD relnoval.
This may indicate that there are too many solids (MLSS) or there has
< 12 mg Oz 1 g-MLVSS / Hr
Low
been a toxic occurrence.
Try and maintain the sample temperature at 25°C t 1°C during the test. If the temperature is out of the set criterion use the excel
worksheet (labeled "SOUR BLANK Calculations" in the SOURS Tests File on the Desktop) and enter the DO readings. The temperature
compensation formula will correct for the temperature. Print and attach the worksheet.
SOUR Procedure for Mixed Liquor Samples:
Collect at least 500mis of the sample to be tested.
Run Total Suspended and Volatile Solids on a Mixed Liquor sample: Follow the steps in the TSS/VSS SOP. Other than the solids test,
the procedure is the same for reading the disolved oxygen. See Below.
SOUR Procedure for Digested Sludge for Disposal:
Collect at least 500mis of the sample to be tested. Run Total Solids on sample: Use at least 25mis of sample and fallow the steps in
the TS SOP.
Reading the Do:
Pour the remaining sample into a 1 liter beaker with a stir bar, place the beaker on a stir plate on a moderate mixing speed then add an
aeration stone to the beaker and aerate for 5 minutes.
While the sample is being aerated Calibrate the DO Meter.
After 5 minutes of aeration, Pour the aerated sample into a 300ml Boo bottle with a stir bar and place the bottle onto a stir plate. While
mixing, place the Boo probe into the bottle and start to measure the DO.
Wait until meter reading has stabilized (no more than 30 sec) and start recording the DO and Temp every (1) minute for 15 minutes or
until there is no more DO remaining. When all the readings have been recorded, clean bottles, probes and equipment properly. Proceed
with the calculations below to complete test. In the event that the DO is exhausted before the 15 minute mark, use the last recoidable
DO reading prior to the oxygen reading zero.
For the Calculation: Use the DO in the last recordable minute and the number of readings. Example: If the oxygen zeroed at the 11
minute mark then you would use the DO that was recorded for the 11th minute and then divide it by 11 because you have eleven
readings total.
Date & Time IN Oven: 5 ` b CJ�YY�
Date & Time OUT of Oven: _� - S -1-7
Date & Time Complete: CO • ' �� M 1. 1�rr�
Analyst: Ale r-�_
Analyst:
Ana
M{�
Dish
#
Volume
(MIS)
Tare Wt.
(g)
Tare + Sample
Wt. (g)
Sample Wet
Wt. (g)
Dried Wt.
(g)
Dried Wt. Diff.
(g)
%
Solids
Total Solids
(mg/1)
Fos[2S
1 13T.,--N1. 1
Igo.
I-S
1 13.3
g = Grams, Wt = Weight
% Total Solids Calculation:
- 3' LIQ Dried Wt. Diff (g) X 100 = % Total Solids
2mple Wet Wt. (g)
71.3
rector Attraction Reduction:
Total Solids mg/I Calculation:
';k;340Dr1ed Wt. Diff (g) x 1000
— Total Solids mg/1
Q 5 Volume (MIS)
Alternative 4:
The specific oxygen rate (SOUR) for sewage sludge treated in an aerobic process shall be equal to or less than 1.5 mg of oxygen per hour
per gram of total solids (dry weight basis) at a temperture of 20oC.
4/612017

����m�Lumberton
~~"^� ^^"
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date &Ana��� ��. �^, ����c��+��' �/` 04W6:�Total Solids
Sample volume used for total solids test:
Weight ofdish:
Weight ofdish + dried solids:
Weight cfdried solids:
Total Solids:
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
0C
10
12
13
mL
g
g
9
Oxygen Consumption Rate 0.03 h1uta
'
SOUR 0\16 (no/g)/hr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
24
Ifsewage sludge k*>28"C.SOUR = r
|fsewage sludge io<2O"C.SOUR = (mg/gVhr
SOUR passes ifresult hy:51.5(nQ/g)hr

City of Lumberton
Specific Oxygen Uptake Rate (SOUR)
Date & Time Collected: �Q (Q 1� °, 8 ^ 2q Qtr� Collected by: TW L&a—
Sample Location: AR -W ' Day # : (y
OZ Uptake performed by:
a
M
0
: r_
o
! .
aff
♦ •
IN - 21
rim
1
kfL
Interpretation of SOUR Test Results for ML Samples
High
This may Indicate that there are not enough solids (MLSS) for the COD
> 20 mg OZ / g-MLVSS / Hr
Loading
12- 20 mg OZ / g-MLVSS / Hr
Normal
This range will usually produce good solids settling and COD removal.
This may indicate that there are too many solids (MLSS) or there has
< 12 mg Oz / g-MLVSS / Hr
I Low
been a toxic occurrence.
Try and maintain the sample temperature at 25°C t 1°C during the test. If the temperature is out of the set criterion use the excel
worksheet (labeled "SOUR BLANK Calculations" in the SOURS Tests File on the Desk top) and enter the DO readings. The temperature
compensation formula will correct for the temperature. Print and attach the worksheet.
SOUR Procedure for Mixed Liquor Samples:
Collect at least 500mis of the sample to be tested.
Run Total Suspended and Volatile Solids on a Mixed Liquor sample: Follow the steps in the TSSIVSS SOP. Other than the solids test,
the procedure is the same for reading the disolved oxygen. See Below,
SOUR Procedure for Digested Sludge for Disposal:
Collect at least 500mis of the sample to be tested. Run Total Solids on sample: Use at least 25mis of sample and follow the steps in
the TS SOP.
Reading the Do:
Pour the remaining sample into a 1 liter beaker with a stir bar, place the beaker on a stir plate on a moderate mixing speed then add an
aeration stone to the beaker and aerate for 5 minutes.
While the sample is being aerated Calibrate the DO Meter.
After 5 minutes of aeration, Pour the aerated sample into a 300m] Boo bottle with a stir bar and place the bottle onto a stir plate. While
mixing, place the BOD probe into the bottle and start to measure the DO.
Wait until meter reading has stabilized (no more than 30 sec) and start recording the DO and Temp every (1) minute for 15 minutes or
until there is no more DO remaining. When all the readings have been recorded, clean bottles, probes and equipment properly. Proceed
with the calculations below to complete test. In the event that the DO is exhausted before the 15 minute mark, use the last recordable
DO reading prior to the oxygen reading zero.
For the Calculation: Use the DO in the last recordable minute and the number of readings. Example: If the oxygen zeroed at the 11
minute mark then you would use the DO that was recorded for the 11th minute and then divide it by 11 because you have eleven
readings total.
Date & Time IN Oven: - 1-7 F, q'• `ICo ® m Analyst: KCL
Date & Time OUT of Oven: �, ��, // `7 Analyst: ZS
Date & Time Complete: —�P l (� �(� 3 "So Analyst: 'fZS
Dish
Volume
Tare Wt.
Tare + Sample
Sample Wet
Dried Wt.
Dried Wt. Diff.
%
Total Solids
#
(MIS)
(9)
Wt. (9)
Wt. (9)
(9)
(g)
- Solids
(mg/I)
10-212-5 I�g►�� �I►�5.� �-� a� ���3 ia�. �s�r o a� 1 -Yo
g = Grams, Wt = Weight
% Total Solids Calculation:
Dried Wt. Diff (g)
Sample Wet Wt. (g)
lector Attraction Reduction:
X 100 = % Total Solids
Total Solids mg/I Calculation:
Dried Wt. Diff (g) x 1000
— Total Solids mg/I
Volume (MIS)
The specific oxygen rate (SOUR) for sewage sludge treated in an aerobic process shall be equal to or less than 1.5 mg of oxygen per hour
Alternative 4: per gram of total solids (dry weight basis) at a temperture of 20°C.
4/G/2017

City of Lumberton
Environmental -Laboratory
Specific Oxygen Uptake Rate -(SOUR) Worksheet
Date & Analyst: 6L7117,; 8.00amt'. ,F.^KCL AB#„1 Day 7
"Total Solids
Sample volume used for total solids test:'',_"rrY"
Weight of dish:
Weight of dish +'dried solids-..'
Weight of dried solids: 0.24
Total Solids: 9 j6
mL ;
9
9
9
g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
1
23_t+00rs.
8'0Z
32
- 3
1
6
IT
i� Y:
8
i� 826a -
9
T23 00)
10
r 23'00ff
y 8423'
13
_ Y23C0OI�
►' 819
14_
Oxygen Consumption Rate 0.01 mg/L/minute
SOUR , 0.09 (mg/g)/hr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
oC
23.0625 .
If sewage sludge is > 20C, SOUR = Y' 0 08 ,i m /
, 9 °
9 . ��.�..w ( 9 9/hr )
If sewage'sludge is < 20°C, SOUR = a g)
SOUR passes if result is 51.5 (mg/g)hr
Version 11/1111

City of Lumberton
Specific Oxygen Uptake Rate (SOUR)
Date & Time Collected: _(0 • —� - V1 @ U - l.-JL 1 nno _ Collected by: 3W1_ 1<-C-L
Sample Location: AD 1 . Day #
02 Uptake performed by:
Interpretation of SOUR Test Results for ML Samples
High
This may indicate that there are not enough solids (MLSS) for the COD
> 20 mg Oz / g-MLVSS / Hr
Loading
12 - 20 mg OZ 1 g-MLVSS 1 Hr
Normal
This range will usually produce good solids settling and COD removal.
This may indicate that there are too many solids (MLSS) or there has
< 12 mg 02 / g-MLVSS / Hr
Low
been a toxic occurrence.
Try and maintain the sample temperature at 25°C t 1°C during the lest. If the temperature is out of the set criterion use the excel
worksheet (labeled "SOUR BLANK Calculations" in the SOURS Tests File on the Desk top) and enter the DO readings. The temperature
compensation formula will correct for the temperature. Print and attach the worksheet.
SOUR Procedure for Mixed Liquor Samples:
Collect at least 500mis of the sample to be tested.
Run Total Suspended and Volatile Solids on a Mixed Liquor sample: Follow the steps in the TSS/VSS SOP. Other than the solids test,
the procedure is the same for reading the disolved oxygen. See Below.
SOUR Procedure for Digested Sludge for Disposal:
Collect at least 500mis of the sample to be tested. Run Total Solids on sample: Use at least 25mis of sample and follow the steps in
the TS SOP.
Reading the Do:
Pour the remaining sample into a 1 liter beaker with a stir bar, place the beaker on a stir plate on a moderate mixing speed then add an
aeration stone to the beaker and aerate for 5 minutes.
While the sample is being aerated Calibrate the DO Meter.
After 5 minutes of aeration, Pour the aerated sample Into a 300ml BOD bottle with a stir bar and place the bottle onto a stir plate. While
mixing, place the Boo probe into the bottle and start to measure the DO.
Wait until meter reading has stabilized (no more than 30 sec) and start recording the DO and Temp every (1) minute for 15 minutes or
until there is no more DO remaining. When all the readings have been recorded, clean bottles, probes and equipment properly. Proceed
with the calculations below to complete test. In the event that the DO is exhausted before the 15 minute mark, use the last recordable
DO reading prior to the oxygen reading zero.
For the Calculation: Use the DO in the last recordable minute and the number of readings. Example: If the oxygen zeroed at the 11
minute mark then you would use the DO that was recorded for the 11th minute and then divide it by 11 because you have eleven
readings total.
--7 V V
Date & Time IN Oven: & I 1—!7 q • t3,fil
Date & Time OUT of Oven: � 7 // 7 . (�2 Q'. fS- D r+'�
Date & Time Complete: 17 nM
Analyst:
YIC,i_
Analyst:
tZ S
Analyst:
�-s
Dish
#
Volume
(MIS)
Tare Wt.
(g)
Tare + Sample
Wt. (g)
Sample Wet
Wt. (g)
Dried Wt.
(g)
Dried Wt. Diff.
(g)
%
Solids
Total Solids
6q.0':)
p.ay
a7j
g = Grams, Wt = Weight
% Total Solids Calculation:
Dried Wt. Diff (g)
Sample Wet Wt. (g) X 100 = % Total Solids
'lector Attraction Reduction:
Total Solids mg/I Calculation:
Dried Wt. Diff (g) x 1000
Volume (MIS)
= Total Solids mg/1
The specific oxygen rate (SOUR) for sewage sludge treated in an aerobic process shall be equal to or less than 1.5 mg of oxygen per hour
Alternative 4: per gram of total solids (dry weight basis) at a temperture of 20°C.
4/6/2017

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Lumberton WQ Permit Number:
WWTP Name: City of Lumberton WWTP NPDES Number:
Monitoring Period: From 10/01/17 To 12/31/17
WQ0000672
NCO024571
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying, Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Tf nnnlirnhle to alfernntivr nrrfnrmedl (Ghee A nr ('lace R) rmmnlntn the fnllnwina mnnifnrina dlata-
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x10 to the 6th
MPN
MPN/g
Coliform
power per gram
of total solids
CFU
<30400
<30500
<30500
CFU/g
0
quarterly
grab
9222D
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0ption/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-daybench) (Spec. 02 uptake) X
Qption/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Mt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Corey Walters, Assistant Director of EUS Dept.
Preparer Name and Title e or print)
Signat re ofPreparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Cameron -Tasting Services, fnc. Labbra#orry Deport rrceriaae W654
NO PHHS 437799
q �. �.�y.�.y�. tpi.�yr4�
• Y)A1isJ�i...b`i ,. Sy�nagrp �L9�T/4�J 171860
r4.+'r�3YYY�ItL�F'x'{�
9l - o
LUt1i�5FfA >' �j
L �t�=�egFatl�ry►,4. Yes
� ,
Sample: Information
C- FlayesyDate 1 10104117 i2 cei ; m. Sims t� ; 10104117
Analyses and Results
'�� �i+t,. -fo`-� -��I-- lr kr .fir �'9 t t - 9'H •
Y.w'=' f `+ 7� F.s b Y_i �•�'�� b�•�,-�� 4 r•- S i 7. ^� �s.-, {� a"-�` 'hYL'7i ""yi j t r Ti ' -ac ;77*. -xt:`� •.�.
'c;
`G`�hsyfl�,r.ItF
e�eT:.11�J���� � w�`map`��-cy.a^r+14��-.��-w{,,��`n�'�f F�j,. �,��.�tA �. ��..nt��x�'Y'���;r4C,�� ✓:t��te�,'3�;•.�-s3pttr�'� fij
- � � .i:a4?".,-I 't`jk z..'1•� �1_�}i_�„�.¢z f�Ff--�^°n`'.�-� 4'e�,'S: �"k�.�eS" t5��� .-,:,-5ft �r��' ' � } �S` y� �^ ''4 �2' ar�C �: -�� f�$IICBi �}� ,
�::b +` i [ s � . 9' rn(�^.. �:4��n h ?�.'•�1-���.t �ti;,i"tn r.cai...t:-��%�
179850 .01 g Gr , Fec. Coff'orrn ,S <30500 cFurq. 3060 10 WIT ERP '+9 D - MF
<0400 F1N9 3W1°n
` <30500 cFulp MMM
<30500 CFuro
<30500 CFure ' Iowa
<30400 Cru10 sow
" . {30400 CFl1&.j sma
Geomean <30500
F
171650 01: srddac Gr lS{9ro} 3,28% am 10I€15Jt7 ERP' 2540 G :TS
C 128°Yo a.o1
3.280, 0.01
e 3,28°!° aa9
f 3,29°Io n,o�
9
Lab Director- Date .
t -
219 113. Sudc Sir. $19-2iJ8 2 U
•SiEnl'°rd•1vC 27330 cures r�:e�;ritemn�cstiis;. aril

219 S. •Steals Str.
Sanford; NG 27330
Rhona: 919-20a-4240
Cameron Testing Services, Inc,
NC INOGtii'7{•C+ rt. 0954 NC pHHS Cert# 37..799 U5 EPIC N001918
Chain of Custody
Page of
;Company -��
ram. ,
----- — _ _ _
EmafF:(
- - �
-
CTS dab use
_:SarSiple Ton'lP.:�-
I.-
—{,t - ,f,/.� - --
_ CnntaCt
/fit-�•-
�..�
t?kiaao:�
tiaEa�9A �
'�id�cess?{C1ty;:
�:Fsz''
Ise' Y1N}. .;=�.i:• � ,.,
r
�° {'Pro,}rrct
�
� •��
sFiosh (Y!N}; • t �0ue p
„Califlcted 3
blame_ �� ,
Slgriature;
.. ': _l- `%'I
_ ,. r
_-7 I'.•-:,7if1.`ii:-' f:t :v
'• Sam la 10f.0 elian:::;.:
,
- 1'J'r•.lif..7c.,_�_i..='t�-.��v:.�;S•.•.�'.:
� , .. _.Nlartntaerntif 6o�tles:;,
-
;�;-
-
-
_ _
n
nuested.Ana[`
.'C...S,.-
i;
',�,
c ..I
-rHicil,
Cft'�S1Lab
Pms'aruaUves,{U}r�preserue
sample I
_
° iu
E'
•'�-
w
o 4:
s
`
h32(S)p4, Fi(W)C3. {t;la)Thiosulfater:'h1a�fl}Fp:
tr' +ICE
CD
m y r
Qther.(X), Indicate
•
r
Ad'
R61in
_ eC6{V0d
' �' :
:C�atelTirne
Rush work will require,p.rior approval, additional charges will apply

o
��*�m�Lumberton
~~°�� ~vo'
Environmental
tmU Laboratory
����n
�~���K�0�00�K�=°. ===K�.��=ry
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst,
Sample Location
Total Solids
Sample volume used for total solids test:
Weight ofdish:
Weight cfdish + dried solids:
Weight ofdried solids:
Total Solids:
SOUR
Time
(Minutes)
Temperature
. Dissolved
Oxygen (mg/L)
0C
12
13
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
23.4375
�
Ifsewage sludge is > 20'C.SOUR =
Ifsewage sludge ha<2O"C.SOUR =
mL
g
g
g
0.15 m8/L/m|nute
SOUR passes if result is equal to or less than 1.5 (mglg)hr
r

City of Lumberton
Specific Oxygen Uptake Rate (SOUR)
Date & Time Collected: W q • CD I � °G 66 -- L43 m Collected by: UW L
Sample Location: pip. I Day # :
02 Optake performed by: KC-1
MEMO�
r
Interpretation of SOUR Test Results for ML Samples
High
This may indicate that there are not enough solids (MLSS) for the COD
> 20 mg 021 g-MLVSS / Hr
Loading
12 - 20 mg 02 / g-MLVSS / Hr
Normal
This range will usually produce good solids settling and COD removal.
This may indicate that there are too many solids (MLSS) or there has
< 12 mg 021 g-MLVSS / Hr
Low
been a toxic occurrence.
Try and maintain the sample temperature at 25°C t 1 °C during the test. If the temperature is out of the set criterion use the excel
worksheet (labeled "SOUR BLANK Calculations" in the SOURS Tests File on the Desk top) and enter the DO readings. The temperature
compensation formula will correct for the temperature. Print and attach the worksheet,
SOUR Procedure for Mixed Liquor Samples:
Collect at least 500mis of the sample to be tested.
Run Total Suspended and Volatile Solids on a Mixed Liquor sample: Follow the steps in the TSSIVSS SOP. Other than,the solids test,
the procedure is the same for reading the disolved oxygen. See Below.
SOUR Procedure for Digested Sludge for Disposal:
Collect at least 500mis of the sample to be tested. Run Total Solids on sample: Use at least 25mis of sample and follow the steps in
the TS SOP.
Reading the Do:
Pour the remaining sample into a 1 liter beaker with a stir bar, place the beaker on a stir plate on a moderate mixing speed then add an
aeration stone to the beaker and aerate for 5 minutes.
While the sample is being aerated Calibrate the DO Meter.
After 5 minutes of aeration, Pour the aerated sample into a 300m] Boo bottle with a stir bar and place the bottle onto a stir plate. While
mixing, place the BOD probe into the bottle and start to measure the DO.
Wait until meter reading has stabilized (no more than 30 sec) and start recording the Do and Temp every (1) minute for 15 minutes or
until there is no more DO remaining. When all the readings have been recorded, clean bottles, probes and equipment properly. Proceed
with the calculations below to complete test. In the event that the DO is exhausted before the 15 minute mark, use the last recordable
DO reading prior to the oxygen reading zero.
For the Calculation: Use the DO in the last recordable minute and the number of readings. Example: If the oxygen zeroed at the 11
minute mark then you would use the DO that was recorded for the 11th minute and then divide it by 11 because you have eleven
readings total.
Date & Time IN Oven:
Date & Time OUT of Oven: w- q • G • 1-1 •• ;� �m
Date & Time Complete: I,V -g� � ha /1 ? 2 : SSA m
Analyst: k--
Analyst: L
Analyst: Z�
Dish
#
Volume
(MIS)
Tare Wt.
(g)
Tare + Sample
Wt. (g)
Sample Wet
Wt. (g)
Dried Wt.
(g)
Dried Wt. Diff.
(g)
%
Solids'
Total Solids
(mg/1)
kiT
251(29—.Q2-(D21113.a-13B114.3�&
I 3q.40'1S
)
t;
g = Grams, Wt = Weight
% Total Solids Calculation:
Dried Wt. Diff (g)
Sample Wet Wt. (g)
ector Attraction Reduction:
X 100 = % Total Solids
Total Solids mg/I Calculation:
Dried Wt. Diff (g) x 1000
- Total Solids mg/I
Volume (MIS)
Alternative 4: The specific oxygen rate (SOUR) for sewage sludge treated in an aerobic process shall be equal to or less than 1.5 mg of oxygen per hour
per gram of total solids (dry weight basis) at a temperture of 20oC.
4/612017

��^�x v�� Lumberton x�x� *
=K�� ^^. °~�00��" ^=�
�
Environmental
��UU�� ����
�~��yU���00��~=" ��^�K�"===ry
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst:
Sample Location:
Total Solids
Sample volume used for total solids teot
Weight ofdish:
Weight ofdish + dried solids:
Weight ofdried solids:
Total Solids:
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg1L)
0C
75.
8
SUN-
70
12
13
15
Oxygen Consumption Rate 0'12 m0/L/minute
SOUR 0.47 hmQ/gVhr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
22
ifsewage sludge is > 20*C.SOUR =
ifsewage sludge is < 20*C.SOUR =
r
(mg/g)/nr
SOUR passes if result is equal too,less than 1.5 (mg/g)hr

City of Lumberton
Specific Oxygen Uptake Rate (SOUR)
Date & Time Collected: R q • -ll . 1-7 �, (S 14 5 Y,r, Collected by: D-WL
Sample Location: �� n # ` Day # :
02 Uptake performed by: i\.L.l.-..
©
•�
�F
MUTO
�c�iliaS!
Interpretation of SOUR Test Results fnr MI Samnlas
High
This may indicate that there are not enough solids (MLSS) for the COD
> 20 mg 02 / g-MLVSS / Hr
ILoading
12 - 20 mg 021 g-MLVSS / Hr
Normal
This range will usually produce good solids settling and COD removal.
This may indicate that there are too many solids (MLSS) or there has
< 12 mg O2 / g-MLVSS / Hr
Low
been a toxic occurrence.
Try and maintain the sample temperature at 25°C t 1°C during the test. If the temperature is out of the set criterion use the excel
worksheet (labeled "SOUR BLANK Calculations" in the SOURS Tests File on the Desk top) and enter the DO readings. The temperature
compensation formula will correct for the temperature. Print and attach the worksheet.
SOUR Procedure for Mixed Liquor Samples:
Collect at least 500mis of the sample to be tested.
Run Total Suspended and Volatile Solids on a Mixed Liquor sample: Follow the steps in the TSS/VSS SOP. Other than the solids test,
the procedure is the same for reading the disclved oxygen. See Below.
SOUR Procedure for Digested Sludge for Disposal:
Collect at least 500mis of the sample to be tested. Run Total Solids on sample: Use at least 25mis of sample and follow the steps in
the TS SOP.
Reading the Do:
Pour the remaining sample into a 1 liter beaker with a stir bar, place the beaker on a stir plate on a moderate mixing speed then add an
aeration stone to the beaker and aerate for 5 minutes.
While the sample is being aerated Calibrate the DO Meter.
After 5 minutes of aeration, Pour the aerated sample into a 300ml BOD bottle with a stir bar and place the bottle onto a stir plate. While
mixing, place the BOD probe into the bottle and start to measure the DO.
Wait until meter reading has stabilized (no more than 30 sec) and start recording the DO and Temp every (1) minute for 15 minutes or
until there is no more DO remaining. When all the readings have been recorded, clean bottles, probes and equipment properly. Proceed
with the calculations below to complete test. In the event that the DO is exhausted before the 15 minute mark, use the last recordable
DO reading prior to the oxygen reading zero.
For the Calculation: Use the DO in the last recordable minute and the number of readings. Example: If the oxygen zeroed at the 11
minute mark then you would use the DO that was recorded for the 11th minute and then divide it by 11 because you have eleven
readings total.
Date & Time IN Oven: R q •--I
• i [
E
8 = C-Dg
Date & Time OUT of Oven: _` M u f`
QI it --?
It 7
P 12 ; -Op,,
Date &Time Complete; _ 1,�t,
°t [-7
I (-M
Analyst:
Ku
Analyst:
ZS
Analyst: _
�S
Dish
Volume
Tare Wt.
Tare + Sample
Sample Wet
Dried Wt.
Dried Wt. Diff.
%
Total Solids
#
(MIS)
(g)
Wt. (g)
Wt. (g)
(g)
(g)
Solids
(mg/1)
25�12C�°1192�1u5 C�9���1 ��-�? I t2► 302� I 0 3$3 -S
g — Grams, Wt = Weight
% Total Solids Calculation: Total Solids mg/1 Calculation:
Dried Wt. Diff (g) Dried Wt. Diff (g) x 1000
Sample Wet Wt. X 100 =
P (g) Volume (mis)
'ector Attraction Reduction:
Alternative 4: The specific oxygen rate (SOUR) for sewage sludge treated in an aerobic process shall be equal to or less than 1.5 mg of oxygen per hour
per gram of total solids (dry weight basis) at a temperture of 20°C.
4/6/2017

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst:.
Sample Location:
Total Solids
Sample volume used for total solids test:
Weight of dish:
Weight of dish + dried solids:
Weight of dried solids:
Total Solids:
SOUR
D'aY'3.
0.40
16.172
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
1
20'00
3
6
77,25<:
8
'' . ' :20`OOisy
10
11
i :' . 201 00)
'
Y "
12
20?OOs _ - -
h: ;f:T 6'73it.`
13
14
15
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
oC
20
If sewage sludge is > 20°C, SOUR =
If sewage sludge is < 20°C, SOUR =
mL
9
9
9
g/L
0.10 mg/L/minute
0.37 (mg/g)/hr
(mg/g)/hr
(mg/g)/hr
SOUR passes if result is equal to or less than 1.5 (mg/g)hr

City of Lumberton
Specific. Oxygen Uptake Rate (SOUR)
Date& Time Collected: q • g (X Wx Collected by: �YV L
Sample Location: o t it I Day #
Oz Uptake performed by: KCAZ
©MW!
01
©�li��yf�I_40
mi�
MMm
�
• •,
A
I
l[•E�L�
H
M
®
• .
Interpretation of SOUR Test Results for ML Samples
High
This may indicate that there are not enough solids (MLSS) for the COD
> 20 mg 02I g-MLVSS I Hr
Loading
Normal
This range will usually produce good solids settling and COD removal.
12 - 20 mg OZ / g-MLVSS I Hr
This may indicate that there are too many solids (MLSS) or there has
< 12 mg Oz / g-MLVSS / Hr
Low
been a toxic occurrence.
Try and maintain the sample temperature at 25°C t 1°C during the test. if the temperature is out of the set criterion use the excel
worksheel (labeled "SOUR BLANK Calculations" in the SOURS Tests File on the Desktop) and enter the DO readings. The temperature
compensation formula will correct for the temperature. Print and attach the worksheel.
SOUR Procedure for Mixed Liquor Samples:
Collect at least 500mis of the sample to be tested.
Run Total Suspended and Volatile Solids on a Mixed Liquor sample: Follow the steps in the TSSIVSS SOP. Other than the solids test,
the procedure is the same for reading the disolved oxygen. See Below.
SOUR Procedure for Digested Sludge for Disposal:
Collect at least 500mis of the sample to be tested. Run Total Solids on sample: Use at least 25mis of sample and follow the steps in
the TS SOP.
Reading the Do:
Pour the remaining sample into a 1 liter beaker with a stir bar, place the beaker on a stir plate on a moderate mixing speed then add an
aeration stone to the beaker and aerate for 5 minutes.
While the sample is being aerated Calibrate the DO Meter.
After 5 minutes of aeration, Pour the aerated sample into a 300ml BOD bottle with a stir bar and place the bottle onto a stir plate. While
mixing, place the BOD probe into the bottle and start to measure the DO.
Wait until meter reading has stabilized (no more than 30 sec) and start recording the DO and Temp every (1) minute for 15 minutes or
until there is no more DO remaining. When all the readings have been recorded, clean bottles, probes and equipment properly. Proceed
with the calculations below to complete test. In the event that the DO is exhausted before the 15 minute mark, use the last recordable
DO reading prior to the oxygen reading zero.
For the Calculation: Use the DO in the last recordable minute and the number of readings. Example: If the oxygen zeroed at the 11
minute mark then you would use the DO that was recorded for the 11th minute and then divide it by 11 because you have eleven
readings total.
Date &Time IN Oven: F Q - 08 • 1-7 @ 1 • aam
Date & Time OUT of Oven:
Date & Time Complete: / -7
Analyst: U
Analyst: jZ S
Analyst: 'R 5
Dish
#
Volume
(MIS)
Tare Wt.
(g)
Tare + Sample
Wt. (g)
Sample Wet
Wt. (g)
Dried Wt.
(g)
Dried Wt. Diff.
(g)
%
Solids
Total Solids
(mg/1)
. (o�{o
11� . 010-1
a . o'ft�'1
3. 3c�83
z .z4o �3
).s,,%
I co • r 7�rsl
g = Grams, Wt = Weight
% Total Solids Calculation:
Dried Wt. Diff (g)
Sample Wet Wt. (g)
ector Attraction Reduction:
X 100 = % Total Solids
Total Solids mg/l Calculation:
Dried Wt. Diff (g) x 1000
Volume (MIS)
= Total Solids mg/I
The specific oxygen rate (SOUR) for sewage sludge treated in an aerobic process shall be equal to or less than 1.5 mg of oxygen per hour
Alternative 4: per gram of total solids (dry weight basis) at a temperture of 20oC.
4/6/2017

Date & Analyst:
Sample Location
Total Solids
City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
17 7$1am KCLITLS Collected by:' KO':'
Sample volume used for total solids test:
Weight of dish:
Weight of dish + dried solids:
Weight of dried solids:
Total Solids:
SOUR
41
0.41
16.284
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
319�s00t
4
1'.900'
8
12
13
14
15
_
5983
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
oC
19
If sewage sludge is > 20°C, SOUR =
0.07 mg/L/minute
0.27 (mg/g)lhr
(mg/g)/hr
If sewage sludge is < 20°C, SOUR = .i (mg/g)/hr
SOUR passes if result is equal to or less than 1.5 (mg/g)hr

City of Lumberton
Specific Oxygen Uptake Rate (SOUR)
Date & Time Collected: 1 ) q • ' � . -'� °� �a-rn Collected by: KO
Sample Location:' Day # :
Oz Uptake performed by: �G
Interpretation of SOUR Test Results for ML Samples
High
This may indicate that there are not enough solids (MLSS) for the COD
> 20 mg OZ / g-MLVSS I Hr
Loading
12 - 20 mg 02 / g-MLVSS / Hr
Normal
This range will usually produce good solids settling and COD removal.
This may indicate that there are too many solids (MLSS) or there has
< 12 mg 02 / g-MLVSS / Hr
Low
been a toxic occurrence.
Try and maintain the sample temperature at 25°C t 1°C during the test. If the temperature is out of the set criterion use the excel
worksheet (labeled "SOUR BLANK Calculations" in the SOURS Tests File on the Desk top) and enter the DO readings. The temperature
compensation formula will correct for the temperature. Print and attach the worksheet.
SOUR Procedure for Mixed Liquor Samples:
Collect at least 500mis of the sample to be tested.
Run Total Suspended and Volatile Solids on a Mixed Liquor sample: Follow the steps in the TSS/VSS SOP. Other than the solids test,
the procedure is the same for reading the disolved oxygenSee Below.
SOUR Procedure for Digested Sludge for Disposal:
Collect at least 500mis of the sample to be tested. Run Total Solids on sample: Use at least 25mis of sample and follow the steps in
the TS SOP.
Reading the Do:
Pour the remaining sample into a 1 liter beaker with a stir bar, place the beaker on a stir plate on a moderate mixing speed then add an
aeration stone to the beaker and aerate for 5 minutes.
While the sample is being aerated Calibrate the DO Meter.
After 5 minutes of aeration, Pour the aerated sample into a 300ml BOD bottle with a stir bar and place the bottle onto a stir plate. While
mixing, place the SOD probe into the bottle and start to measure the DO.
Wait until meter reading has stabilized (no more than 30 sec) and start recording the DO and Temp every (1) minute for 15 minutes or
until there is no more DO remaining. When all the readings have been recorded, clean bottles, probes and equipment properly. Proceed
with the calculations below to complete test. In the event that the DO is exhausted before the 15 minute mark, use the last recordable
DO reading prior to the oxygen reading zero.
For the Calculation: Use the DO in the last recordable minute and the number of readings. Example: If the oxygen zeroed at the 11
minute mark then you would use the DO that was recorded for the 11th minute and then divide it by 11 because you have eleven
readings total.
Date & Time IN Oven: 1- I 9 • 1 1 • 17 P, O ' Mon-)
Date & Time OUT of Oven:
Date & Time Complete: Q f (l if —I G� t :30
Analyst:
Analyst:
Analyst:_ Z_S
Dish
#
Volume
(MIS)
Tare Wt.
(g)
Tare + Sample
Wt. (g)
Sample Wet
Wt. (g)
Dried Wt.
(g)
Dried Wt. Diff.
(g)
%
Solids
Total Solids
(mgll)
110125-9
22,Tng
I A& .599 3
1 111. 9 Z
0.4 o?
1-i-o-
/&- 12,„sl�
g = Grams, Wt = Weight
% Total Solids Calculation:
Dried Wt. Diff (g)
Sample Wet Wt,. (g)
X 100 = % Total Solids
-mtorAttraction Reduction:
Total Solids mg/l Calculation:
Dried Wt. Diff (g) x 1000
Volume (MIS)
= Total Solids mg/I
Alternative 4: The specific oxygen rate (SOUR) for sewage sludge treated in an aerobic process shall be equal to or less than 1.5 mg of oxygen per hour
per gram of total solids (dry weight basis) at a temperture of 20°C.
4/6/2017

Date & Analyst:
Sample Location:
Total Solids
City of Lumberton
Environmental Laboratory
Specific Oxvaen Uptake Rate (SOUR) Worksheet
9=1117' ;fi 59Ath KC r r !LS' :C;olleeted by=JV11L;
�.
Sample volume used for total solids test:
Weight of dish:
Weight of dish + dried solids:
Weight of dried solids:
Total Solids:
SOUR
0.38
15.3
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
2
_ - � ',20'001
- ., _. .- -
5
l`:,._v �200,'0':=_.V .."_�
�✓- '803s -
7
i . _200.0 - -;1-:.
74,8711.
- 7 69' --
10
AP
91
13
14
15
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
oC
20
0.10 mg/L/minute
0.40 (mg/g)/hr
If sewage sludge is > 20°C, SOUR = (mg/g)/hr
If sewage sludge is < 20°C, SOUR = ..,o.e . (mg/g)/hr,
SOUR passes if result is equal to or less than 1.5 (mg/g)hr

City of Lumberton
Specific Oxygen Uptake Rate (SOUR)
Date & Time Collected: T q • 12 • `� �q pLm Collected by: OWL_
Sample Location: M att Day # :
02 Uptake performed by: KCL
Interpretation of SOUR Test Results for ML Samples
High
This may indicate that there are not enough solids (MLSS) for the COD
> 20 mg OZ / g-MLVSS / Hr
Loading
12 - 20 mg OZ / g-MLVSS / Hr
Normal
This range will usually produce good solids settling and COD removal.
This may indicate that there are too many solids (MLSS) or there has
< 12 mg OZ / g-MLVSS / Hr
Low
been a toxic occurrence.
Try and maintain the sample temperature at 25°C t 1°C during the test. If the temperature is out of the set criterion use the excel
worksheet (labeled "SOUR BLANK Calculations" in the SOURS Tests File on the Desk top) and enter the DO readings. The temperature
compensation formula will correct for the temperature. Print and attach the worksheet.
SOUR Procedure for Mixed Liquor Samples:
Collect at least 500mis of the sample to be tested.
Run Total Suspended and Volatile Solids on a Mixed Liquor sample: Follow the steps in the TSS/VSS SOP. Other than the solids test,
the procedure is the same for reading the disolved oxygen. See Below
SOUR Procedure for Digested Sludge for Disposal:
Collect at least 500mis of the sample to be tested. Run Total Solids on sample: Use at least 25mis of sample and follow the steps in
the TS SOP,
Reading the Do:
Pour the remaining sample into a 1 liter beaker with a stir bar, place the beaker on a stir plate on a moderate mixing speed then add an
aeration stone to the beaker and aerate for 5 minutes.
While the sample is being aerated Calibrate the DO Meter.
After 5 minutes of aeration, Pour the aerated sample into a 300ml Boo bottle with a stir bar and place the bottle onto a stir plate. While
mixing, place the Boo probe Into the bottle and start to measure the DO.
Wait until meter reading has stabilized (no more than 30 sec) and start recording the DO and Temp every (1) minute for 15 minutes or
until there is no more DO remaining. When all the readings have been recorded, clean bottles, probes and equipment properly. Proceed
with the calculations below to complete test. In the event that the DO is exhausted before the 15 minute mark, use the last recordable
DO reading prior to the oxygen reading zero.
For the Calculation: Use the DO in the last recordable minute and the number of readings. Example: If the oxygen zeroed at the 11
minute mark then you would use the DO that was recorded for the 11th minute and then divide it by 11 because you have eleven
readings total.
Date & Time IN Oven: -T q - 12.11-� e • M c,
Date & Time OUT of Oven:
Date & Time Complete: I q1 l21 l 2 P-
Analyst: 1<37-I.
Analyst: 7TC S
Analyst: I L
Dish
Volume
Tafe Wt.
Tare + Sample
Sample Wet
Dried Wt.
Dried Wt. Diff.
%
Total Solids
#
(MIS)
(g)
Wt. (g)
Wt. (g)
(g)
(g)
Solids
(mg/4
? �8�. 24� 113. iu��a .�3�� (29.o449 1 o-38aS 0�10
g = Grams, Wt = Weight
% Total Solids Calculation:
Dried Wt. Diff (g)
Sample Wet Wt. (g)
lector Attraction Reduction:
X 100 = % Total Solids
Total Solids mg/I Calculation:
Dried Wt. Diff (g) x 1000
Volume (MIS)
= Total Solids mg/I
The specific oxygen rate (SOUR) for sewage sludge treated in an aerobic process shall be equal to or less than 1.5 mg of oxygen per hour
Alternative 4: per gram of total solids (dry weight basis) at a temperture of 20oC.
4/6/2017

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rote (SOUR) Worksheet
Date & Analyst:
Sample Location:
Total Solids
Sample 'Volume used for total solids test:
Weight of dish:
Weight of dish + dried solids:
Weight of dried solids:
Total Solids:
SOUR
E- 2-,{2`r
0.34
13.692
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
0C
0-
4
-8
2
3
4
'A-
11.'V.
EL7
5
OT
L t- 7',- A
6
E, ---'Z ,_745' L,
.7
L7--,
8
=11-11910(k
9
10
2110
F
12
tj
00",
E 2794-0j
13
14
7­21"
15
irl�-..i-�.�,-",-,;��-�i-t'?ili—."Ql0l:".".�-,�',_Z
7-,
2,1[,14�_-
mL
9
9'
9
g/L
Oxygen Consumption Rate 0.09 mg/Ltminute
SOUR 0.38 (mg/g)lhr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
0C
21
If sewage sludge is > 20'C, SOUR =
If sewage sludge is 5 20°C, SOUR =
.(Mg/g)/hr
(mg/g)/hr
SOUR passes if result is equal to or less than 1.5 (mg/g)hr

City of Lumberton
Specific Oxygen Uptake Rate (SOUR)
Date & Time Collected: v q 13 • in S G •• 49 p nn Collected by: �wL
Sample Location: -t I Day #
Oz Uptake performed by: VICL
G
Interpretation of SOUR Test Results for ML Samples
High
This may indicate that there are not enough solids (MLSS) for the COD
> 20 mg OZ / g-MLVSS / Hr
Loading
12 - 20 mg OZ / g-MLVSS / Hr
Normal
This range will usually produce good solids settling and COD removal.
This may indicate that there are too many solids (MLSS) or there has
< 12 mg OZ / g-MLVSS / Hr
Low
been a toxic occurrence.
Try and maintain the sample temperature at 25°C t 1°C during the test. If the temperature is out of the set criterion use the excel
worksheet (labeled "SOUR BLANK Calculations" in the SOURS Tests File on the Desk top) and enter the DO readings. The temperature
compensation formula will correct for the temperature. Print and attach the worksheet.
SOUR Procedure for Mixed Liquor Samples:
Collect at least 500mis of the sample to be tested.
Run Total Suspended and Volatile Solids on a Mixed Liquor sample: Follow the steps in the TSSNSS SOP. Other than the solids test,
the procedure is the same for reading the disolved oxygen. See Below.
SOUR Procedure for Digested Sludge for Disposal:
Collect at least 500mis of the sample to be tested. Run Total Solids on sample: Use at least 25mis of sample and follow the steps in
the TS SOP.
Reading the Do:
Pour the remaining sample into a 1 liter beaker with a stir bar, place the beaker on a stir plate on a moderate mixing speed then add an
aeration stone to the beaker and aerate for 5 minutes.
While the sample is being aerated Calibrate the DO Meter.
After 5 minutes of aeration, Pour the aerated sample into a 300ml Boo bottle with a stir bar and place the bottle onto a stir plate. While
mixing, place the Boo probe into the bottle and start to measure the DO.
Wait until meter reading has stabilized (no more than 30 sec) and start recording the DO and Temp every (1) minute for 15 minutes or
until there is no more DO remaining. When all the readings have been recorded, clean bottles, probes and equipment properly. Proceed
with the calculations below to complete test. In the event that the DO is exhausted before the 15 minute mark, use the last recordable
DO reading prior to the oxygen reading zero.
For the Calculation: Use the DO in the last recordable minute and the number of readings. Example: If the oxygen zeroed at the 11
minute mark then you would use the DO that was recorded for the 11th minute and then divide it by 11 because you have eleven
readings total.
Date & Time IN Oven:
Date & Time OUT of Oven: W �} ((3 (( -7 2 , r-i 0 rt�
Date & Time Complete: Vy q' 1 B0 2 1 4k om
Analyst: KCL
Analyst:
Analyst:
fDish
#
Volume
(mis)
Tare Wt.
(g)
Tare + Sample
Wt. (g)
Sample Wet
Wt. (g)
Dried Wt.
(g)
Dried Wt. Diff.
(g)
%
Solids
Total Solids
(mg/1)
10
2S11IL412011*2�.54YJAW-
11 5
q.3�a-
t -406
13. 69„ !
g = Grams, Wt = Weight
% Total Solids Calculation:
Dried Wt. Diff (g)
Sample Wet Wt. (g) X 100 = %Total Solids
rector Attraction Reduction:
Total Solids mg/I Calculation:
Dried Wt. Diff (g) x 1000
= Total Solids mg/1
Volume (MIS)
Alternative 4: The specific oxygen rate (SOUR) for sewage sludge treated in an aerobic process shall be equal to or less than 1.5 mg of oxygen per hour
per gram of total solids (dry weight basis) at a temperture of 20°C.
4/6/2017

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 9=14'=11j,", 41_amj KCLLTLSi _Collectetl by;JINL.
Sample Location: D1 esfer`1l. Da f 7 :_
Total Solids
Sample volume used for total solids test:
Weight of dish:
Weight of dish + dried solids:
Weight of dried solids:
Total Solids:
SOUR
--- 25
t... }
0.36
14.308
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
224
- - - -
10
f=
12
13
14
.: -210i0;
15
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
22.3125
If sewage sludge is > 20°C, SOUR =
mL
9
9
9
g/L
0.08 mg/L/minute
0.35 (mg/g)/hr
(mg/g)/hr
If sewage sludge is < 20°C, SOUR = �'� U 3_o"`� (mg/g)/hr
SOUR passes if result is equal to or less than 1.5 (mg/g)hr

City of Lumberton
Specific Oxygen Uptake Rate (SOUR)
Date &Time Collected: la q • ' 1-7 @ G 1410,E Collected by:
Sample Location: 1 Q - 1 Day # :
02 Uptake performed by: ,
Interpretation of SOUR Test Results for ML Samples
High
This may indicate that there are not enough solids (MLSS) for the COD
> 20 mg OZ / g-MLVSS / Hr
Loading
12 - 20 mg Oz / g-MLVSS / Hr
Normal
This range will usually produce good solids settling and COD removal.
This may indicate that there are too many solids (MLSS) or there has
< 12 mg 02 / g-MLVSS / Hr
Low
been a toxic occurrence.
Try and maintain the sample temperature at 25°C t 1°C during the test. If the temperature is out of the set criterion use the excel
worksheet (labeled "SOUR BLANK Calculations" in the SOURS Tests File on the Desk top) and enter the DO readings. The temperature
compensation formula will correct for the temperature. Print and attach the worksheet.
SOUR Procedure for Mixed Liquor Samples:
Collect at least 500mis of the sample to be tested.
Run Total Suspended and Volatile Solids on a Mixed Liquor sample: Fallow the steps in the TSSIVSS SOP. Other than the solids test,
the procedure is the same for reading the disolved oxygen. See Below.
SOUR Procedure for Digested Sludge for Disposal:
Collect at least 500mis of the sample to be tested. Run Total Solids on sample: Use at least 25mis of sample and follow the steps in
the TS SOP.
Reading the Do:
Pour, the remaining sample into a 1 liter beaker with a stir bar, place the beaker on a stir plate on a moderate mixing speed then add an
aeration stone to the beaker and aerate for 5 minutes.
While the sample is being aerated Calibrate the DO Meter.
After 5 minutes of aeration, Pour the aerated sample into a 300ml Boo bottle with a stir bar and place the bottle onto a stir plate. While
mixing, place the Boo probe into the bottle and start to measure the DO.
Wait until meter reading has stabilized (no more than 30 sec) and start recording the DO and Temp every (1) minute for 15 minutes or
until there is no more DO remaining. When all the readings have been recorded, clean bottles, probes and equipment properly. Proceed
With the calculations below to complete test. In the event that the DO is exhausted before the 15 minute mark, use the last recordable
DO reading prior to the oxygen reading zero.
For the Calculation: Use the DO in the last recordable minute and the number of readings. Example: If the oxygen zeroed at the 11
minute mark then you would use the DO that was recorded for the 11th minute and then divide it by 11 because you have eleven
readings total.
Date & Time IN Oven: 9 —1 • � "i - n —T9 ys C� - Im
Date & Time OUT of tt Oven: R 9 • W • 1 f G k n:- 22 prn
"6 Date & Time Complete: R • IL4 •1-7 @ I • r�— 1 pon
Analyst:
Analyst:
Analyst: KC-L
Dish
#
Volume
(MIS)
Tare Wt.
(g)
Tare + Sample
Wt. (g)
Sample Wet
Wt. (g)
Dried Wt.
(g)
Dried Wt. Diff.
(g)
%
Solids
Total Solids
(mg/1)
25
I n.aa5l
A cozo
-p
1 i-go-T
i •3
g j�Fra'ms, Wt = Weight
W.►4.1.7
% Total Solids Calculation:
Dried Wt. Diff (g)
X 100 = %Total Solids
Sample Wet Wt. (g)
Vector Attraction Reduction:
Total Solids mg/I Calculation:
Dried Wt. Diff (g) x 1000
= Total Solids mg/I
Volume (MIS)
The specific oxygen rate (SOUR) for sewage sludge treated in an aerobic process shall be equal to or less than 1.5 mg of oxygen per hour
Alternative 4: per gram of total solids (dry weight basis) at a temperture of 20°C.
416/2017

Agricultural Lime Application Log
-Year: 2017
Project: Lumberton
Field Soil Lime Requirement Tons/Acre Date Applied
(state -county -site -field) pH 11 (from soil analysis)IF. . Applied
NC-RO-16-1
5.9
0.8 T/Ac.
Ordered*
NC-RO-16-2
5.7
0.8 T/Ac.
Ordered*
NC-RO-16-3
5.8
0.8:T/Ac.
Ordered*
NC-RO-164
5.9
0.8 T/Ac.
'Ordered*
NC-RO-16-5
6.4
O.OT/Ac.
NC-RO-16-6
6.0
O.OT/Ac.
NC-RO-16-8
.7.2
O.OT/Ac.
NC-RO-16-16
5.7
0.8 T/Ac.
Ordered*
NC-RO-16-17
6.5
O.OT/Ac.
NC-RO-16-18
6.2
O.OT/Ac.
NC-RO-16-19
5.6 -
0.8 T/Ac.
Ordered*
NC-RO-17-01
5.8 .
0-.8T/Ac.
Ordered*
NC-RO-17702
6.1
O.OT/Ac.
NC-R0-17-03,
5.7
0.8'T/Ac.
Ordered*
NC-RO-17-04
6.2
O.OT/Ac.
NC-RO-20-03
5:8
0.8T/Ac.
Ordered*
NC-RO-20-04
5.7
0.8T/Ac.
Ordered*
NC-RO-28-01
6.2
O.OT/Ac.
NC-RO-28-03
4.9
2.OT/Ac.
Ordered*
NC-RO-39-04
6.6
O.OT/Ac.
NC-RO-39-09
6.6
1 O.OT/Ac.
* Ag lime -will be applied once field and crop conditions are suitable

Page 1 of 5
Report Number: 17-020-0622
Account Number: 46525
Send To: Synagro Central LLC/ Lumberton
Mary Brewer
284 Boger Road
Mocksville NC 27028
i
WaypANALYTICAL
"Every acre... Every year."ru
Date Received: 01/20/2017 Date Of Analysis: 01/23/2017
Farm' ID: R016
SOIL ANALYSIS REPORT
Date Of Report: 01/23/2017
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Grower: Ozzeu Buker/ Lumberton -
Analytical Method(s): SMP Buffer pH Mehlich 3 Loss On Ignition Water pH
OM
WN
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Field ID
Lab
Number
. o �°
Rate
Soil
Class
Ibs/A
M3
ppm Rate
ppm Rate
ppm Rate
K
ppm Rate
Mg
ppm Rate
Ca
ppm Rate
Na
ppm Rate
Soil
PH
Buffer
Index
H
meg1100g
meq/100g
R016-1
12924
1.7
L
78
162 VH
NC = 135
67 M
NC = 34
70 M
553 M
5.9
6.86
0.7
4.2
MIN
R016-2
12925
3.4
M
111
98 H
NC = 82
86 M
NC = 44
94 H
567 M
5.7
6.83
1.0
4.8
MIN
R016-3
12926
2.2
L
87
166 VH
NC = 138
69 L
NC = 35
78 M
675 M
5.8
6.83
1.0
5.2
MIN
R016-4
12928
3.3
M
106
68 H
NC = 57
69 L
NC = 35
147 H
841 M
5.9
6.81
1.2
6.8
MIN
R016-5
12929
1.9
L
82
213 VH
NC = 177
93 H
NC = 48
80 'H
577 M
6.4
0.4
4:2
MIN
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble salts
Sample ID
Field 1D
K
%
Mg
%
Ca
%
Na
%
H
%
NO, N
ppm Rate
S
ppm Rate
Zn
ppm Rate
Mn
ppm Rate
Fe
ppm Rate
Cu
ppm Rate
B
ppm Rate
SS
ms/cm Rate
_
R016-1
4.1
13.9
65.8
16.7
R016-2
4.6
16.3
59.1
20.8
R016-3
3.4
12.5
64.9
19.2
R016-4
2.6
18.0
61.8
17.6
RO16-5
5.7
15.9
68.7
9.5
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by; {�gµric m� G�
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble [,
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysts prepared by: WaypointAnalytical Virginia, Inc.
Pauric McGroary

Page 2 of 5
Report Number: 17-020-0622
Account Number: 46525
Send To: Synagro Central LLC/ Lumberton
Mary Brewer
284 Boger Road
Mocksville NC 27028
Date Received: 01/20/2017
Date Of Report: 01/23/2017
Waypoint.
ANALYTICAL
"Every acre... Every year. "TM
Farm ID: R016
SOIL FERTILITY RECOMMENDATIONS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Grower: Ozzeu Buker/ Lumberton
Nitrogen
Phosphate
Potash
Magnesium
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Sample ID
Intended Crop
Yield Goal
Lime
N
P205
K20
Mg
S
Zn
Mn
Fe
Cu
B
Field ID
Tons/A
lb/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
R016-1
Adjust pH to 6.0
0
0.8
10
R016-1
-T
Bermuda, Coastal
5
0.8
75
0
368
10
R016-2
Bermuda, Coastal
5
0.8
75
30
329
0
R016-2
Adjust pH to 6.0
0
0.8
0
R016-3
.
Bermuda, Coastal
5
0.8
75
0
375
2
R016-3
Adjust pH to 6.0
0
0.8
2
R016-4
Adjust pH to 6.0
0
0.8
0
R016-4
Bermuda, Coastal
'5
0.8
75
30
394
0
R016-5
Bermuda, Coastal
5
0.0
75
0
305
0
R016-5
Adjust pH to 6.0
0
0.0
0
Comments
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." {� M
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Pauric McGroary

Page 3 of 5
Report Number: 17-020-0622
Account Number: 46525
Send To: Synagro Central LLC/ Lumberton
Mary Brewer
284 Boger Road
Mocksville NC 27028
Waypolnt,�ANALYTICAL
"Every acre... Every year."m
Farm ID: R016
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.wayp.ointanalytical.com
Grower: Ozzeu Buker/ Lumberton
Sample(s) : R016-3 Crop: Adjust pH to 6.0
Apply dolomitic lime to raise pH and improve the magnesium level.
If dolomitic lime is not used, apply required magnesium with magnesium oxide. Epsom Salts, K-Mag or Sul-PO-Mag.
Sample(s) : R016-2,R016-3,R016-4,R016-5 Crop: Bermuda, Coastal
Apply additional 65 pounds of.nitrogen after every cutting and harvest of hay.
The recommended potash is the total pounds/acre needed to achieve the specified yield goal. Apply 1/2 or 1/3 (100-150 pounds) of the total at the first application in
spring or fall. Application of the remaining should be determined by the yield achieved after the first cutting and the moisture condition. If in drought condition and yield
is low the following applications should be reduced or eliminated.
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made:" MM
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, -nor may any reference be made to the
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Pauric McGroary

Page 4 of 5 `
Report Number: 17-020-0622
Account Number:46525
Send To: Synagro Central LLC/ Lumberton
Mary Brewer -
284 Boger Road
Mocksville'NC 27028
Waypoint.
ANALYTICAL
"Every acre... Every year. "rm
Date Received:' 01/20/2017 Date Of Analysis: 01/23/2017
Farm ID: R016
SOIL ANALYSIS REPORT
Date Of Report: 01/23/2017
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointa na lyti ca I.com
Grower: Ozzeu Buker/ Lumberton
Analytical Method(s): SMP Buffer pH Mehlich 3 Loss On Ignition Water pH
Sample ID
Field ID
Lab
Number
OM
WN
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
o �0
Rate
Soil
Class
Ibs/A
M3
ppm Rate
ppm -Rate
ppm Rate
K
ppm Rate
Mg
ppm Rate
Ca
.ppm Rate
Na
ppm Rate
Soil
pH
Buffer
Index
H
meq/100g
meq/100g
R016-6
12930
1.5
L
74
329 VH
NC = 274
134 VH
NC = 69
87 H
546 M
6.0
0.7
4.5
MIN
R016-8
12931
2.2
L
83
257 VH
NC = 214
56 L
NC = 29
84 L
1321 VH
7.2
0:0
7.4
MIN
Sample ID
Field ID
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
K
%
Mg
%
Ca
%
Na
%
H
%
NON
ppm Rate
S
ppm Rate
Zn
,ppm Rate
Mn
ppm Rate
Fe
ppm Rate
Cu
ppm Rate
B
ppm Rate
SS
ms/cm Rate
R016-6
7.6
16.1
60.7
15.6
R016-8
1.9
9.5
89.3
0.0
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by; {�auri� m� G
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: Waypoint Analytical Virginia, Inc. v
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
Pauric McGroary

Page 5 of 5
Report Number: 17-020-0622
Account Number: 46525
Send To: Synagro Central LLC/ Lumberton
Mary Brewer
284 Boger Road
Mocksville NC 27028
Date Received: 01/20/2017
Date Of Report: 01/23/2017
Waypoint.
ANALYTICAL
Every acre..:Every year".
Farm ID: R016
SOIL FERTILITY RECOMMENDATIONS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Grower: Ozzeu Buker/ Lumberton
Nitrogen
Phosphate
Potash
Magnesium
_Sulfur
Zinc
Manganese
Iron
Copper
Boron
Sample ID
Intended Crop
Yield Goal
Lime
N
P205
K20
Mg
S
Zn
Mn
Fe
Cu
B
Field ID
Tons/
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
R016-6
Adjust pH to 6.0
0
0.0.
0
R016-6
-
Bermuda, Coastal
5
0.0
75
0
210
0
R016-8
Adjust pH to 6.0
0
0.0
0
R016-8
Bermuda, Coastal
5
0.0
75
0
432
0
Comments:
Sample(s) : R016-8 Crop: Bermuda, Coastal
Apply additional 65 pounds of nitrogen after every cutting and harvest of hay.
The recommended potash is the total pounds/acre needed to achieve the specified yield goal. Apply 1/2 or"1/3 (100-150 pounds) of the total at the first application in
spring or fall. Application of the remaining should be determined by the yield achieved after the first cutting and the moisture condition. If in drought condition and yield
is low the following applications should be reduced or eliminated.
Use ammonium sulfate as all or portion of the N requirement to reduce pH.
Use K-Mag as part of the potassium source to increase magnesium level
"The recommendations are based'on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Q M
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be -reproduced in whole or part, nor may any reference be made to the
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Pauric McGroary

Page 1 of 3
Report Number: 17-020-0621
Account Number: 46525
Send To: Synagro Central LLC/ Lumberton
Mary Brewer
284 Boger Road
Mocksville NC 27028
•
Waypoint
ANALYTICAL
Every acre... Every year. "rM
Date Received: 01/20/2017 Date Of Analysis: 01/23/2017
Farm ID: R016
SOIL ANALYSIS REPORT
Date Of Report: 01/23/2017
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 a Fax [phone]
www.waypointanalytical.com
Grower: Campen Farms/ Lumberton
Analytical Method(s): SMP Buffer pH Mehlich 3 Loss On Ignition Water pH
OM
WN
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Field ID
Lab
Number
o �°
Rate
Soil
Class
Ibs/A
M3
ppm Rate
ppm Rate
ppm Rate
K
ppm Rate
Mg,
ppm Rate
Ca
ppm Rate
Na
ppm Rate
Soil
pH
Buffer
Index
H
meq/100g
meq/1009
RO16-16
12920
3.8
M
116
431 VH
NC = 359
65 L
NC = 33
67 L
946 M
5.7
6.78
1.5
7.0
MIN
R016-17
12921
2.5
L
92
247 VH
NC = 206
21 VL
NC = 11
152 H
845 H
6.5
0.4
5.9
MIN
RO16-18
12922
2.4
L
91
232 VH
NC = 193
17 VL
NC = 9
88 H
675 H
6.2
0.6
4.8
MIN
RO16-19
12923
1.1
L
69
144 VH
NC = 120
24 VL
NC = 12
25 L
284 M
5.6
6.88
0.5
2.2
MIN
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Sample ID
Field ID
K
%
Mg
%
Ca
%
Na
%
H
%
NON
ppm Rate
S
ppm Rate
Zn
ppm Rate
Mn
ppm Rate
Fe
ppm Rate
Cu
ppm Rate
B
ppm Rate
SS
ms/cm Rate
RO16-16
2.4
8.0
67.6
21.4
R016-17
0.9
21.5
71.6
6.8
RO16-18
0.9
15.3
70.3
12.5
RO16-19
2.8
9.5
64.5
22.7
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: �ri� me G�N�
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by: WaypolntAnalytical Virginia, Inc.
Pauric McGroary

Page 2 of 3
Report Number: 17-020-0621
Account Number: 46525.
Send To: Synagro Central LLC/ Lumberton
Mary Brewer
- 284 Boger Road - -
Mocksville NC 27028
Date Received: 01/20/2017
Date Of Report: 01/23/2017
I
J
WaY oint.
ANALYTICAL
Every acre... Every year. "T.
Farm ID: R016
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Grower: Campen Farms/ Lumberton
SOIL FERTILITY RECOMMENDATIONS
Nitrogen
Phosphate
Potash
Magnesium
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Sample ID
Intended Crop
Yield Goal
Lime
N
P205.
K20
Mg
S
Zn
Mn
Fe
Cu
B
Field ID
Tons/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
lb/A
Ib/A
Ib/A
Ib/A
Ib/A
R016-16 -
Adjust pH to 6.0
0
0.8'
13
RO 16-16
Bermuda, Coastal
5-
0.8
75
0
406
13
RO 16-17
Bermuda, Coastal
5
0.0
75
0
498
0
RO 16-17
Adjust pH to 6.0
0
0.0 -
0
RO 16-18
Bermuda, Coastal
5
0.0
75
0
495
0
R0 16-18
Adjust pH to 6.0
0
0.0 -,
0
R016-19
Adjust pH to 6.0
0
0.8
55
RO 16-19
Bermuda, Coastal
5
0.8
75
0
447
55
Comments:
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." M
Our reports and letters are for the exclusive and: confidential use of our clients,, and may not be reproduced in whole or part, nor may any reference be made to the �Gt�i6 +'rc GIN
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Pauric McGroary

Page 3 of 3
Report Number: 17-020-0621
Account Number: 46525 Waypoint 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
Send To: Synagro Central LLC/ Lumberton ANALYTICAL www.waypointanalytical.com
Mary Brewer "Every acre... Every year."rn, Grower: Campen Farms/ Lumberton
284 Boger Road
Mocksville NC 27028
Farm ID: R016
Sample(s) : RO 16-19 Crop: Adjust pH to 6.0
Apply dolomitic lime to raise pH and improve the magnesium level.
If dolomitic lime is not used, apply required magnesium with magnesium oxide. Epsom Salts, K-Mag or Sul-PO-Mag.
Sample(s) : RO 16-17,RO 16-18,1110 16-19 Crop: Bermuda, Coastal
Apply additional 65 pounds of nitrogen after every cutting and harvest of hay.
The recommended potash is the total pounds/acre needed to achieve the specified yield goal. Apply 1/2 or 1/3 (100-150 pounds) of the total at the first application in
spring or fall. Application of the remaining should be determined by the yield achieved after the first cutting and the moisture condition. If in drought condition and yield
is low the following applications should be reduced or eliminated.
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports'and letters are for the exclusive and confidential use of our clients„ a and may not be reproduced in whole or part, nor may any reference be made to the 1 Ate« me V�
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Pauric McGroary

Page 1 of 1
Report Number: 18-033-0526
Account Number: 46525
Send To: Synagro Central LLC/ Lumberton
Mary Brewer
284 Boger Road
Mocksvillb NC 27028
Date Received: 02/02/2018
Waypoint0
ANALYTICAL
"Every acre... Every year. ">x,
Date Of Analysis: 02/05/2018
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Grower: Airport
Farm ID/Name: RO-17
SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
Date Of Report: 02/07/2018
OM
W/V
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
Field ID
Number
°
/0
Soil
lbs/A
M3
K
Mg
Ca
Na
Soil
Buffer
H
Rate
Class
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
PH
Index
meq/100g
meq/100g
1
01213
3.3
107
568 VH
99 M
125 H
772 M
19 VL
5.8
6.81
1.2
6.4
M
IMIN
NC = 473
NC = 51
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
soluble Salts
Sample ID
Field ID
K
Mg
Ca
Na
H
NO, N
S
Zn
Mn
Fe
Cu
B
SS
%
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ms/cm Rate
1
4.0
16.3
60.3
1.3
18.8
23 M
39.4 VH
18 M
214 VH
6.6 VH
0.4 L
0.13 VL
NC = 48
NC = 985.0
NC = 113
NC = 430.0
Values on this report represent the plant available nutrients in the
soil. Rating after each value: VL (Very Low), L (Low), M (Medium),
H (High), VH (Very High). ENR - Estimated Nitrogen Release.
C.E.C. - Cation Exchange Capacity.
Date Received: 02/02/2018
Date Of Report: 02/07/2018
Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
(pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by: Pox" m� G eo"r
Salts ms/cm x 640 = ppm. Analysis prepared by: Waypoint Analytical Virginia, Inc.
SOIL FERTILITY RECOMMENDATIONS
Pauric McGroary
Nitrogen
Phosphate
Potash
Magnesium
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Sample ID
Intended Crop
Yield Goal
Lime
N
P205
K20
Mg
S
Zn
Mn
Fe
Cu
B
Field ID
Tons/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
1
Adjust pH to 6.0
0
0.8
0
2
0
Comments:
"The recommendatioris are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made."
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY17-SL034453
1�ULTU
'�wdc Predictive
Client:
Chad Hayes
Advisor:
1�,GR
273 Pete Strickland Rd
Soil Report
Mehlich-3 Extraction
Cerro Gordo,
NC 28430
~
fin$
Sampled County:
Robeson
•F°' 1 Links to Helpful Information
UNON 1�
Sampled: 05/16/2017
Received: 05/23/2017
Farm: co17-Allen
Completed: 06/02/2017
Client ID: 464046
Advisor ID:
Sample ID: co172
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre) N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Soybean
0.0 0 40
110
0 0
10
0
0 0
Note: 3
2-Soybean
0.0 0 40
-110
0 0
$
0
0 0
Note: 3 Note:
Test Results [units - WN in g/cm3; CEC and Na in meq/100 crrr3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P-1 K-1 Ca% Mg%
S-1 Mn-I
Mn-All Mn-AI2 Zn-I
Zn-AI
Cu-1 Na ESP
SS-1 NO3-N
1.31 1.26 8.1 80 1.6 6.1
44 17 73 6
31 21
22 22
73
73
54 0.1
1
Sample ID: c0173
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre) N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Soybean
0.8 0 0
110
0 0
10
0
0 0
Note: 3
2-Soybean
0.0 0 0
110
0 0
$
0
0 0
Note: 3 Note:
Test Results [units - WN in g/cm3; CEC and Na in meq/100 crrr3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P-1 _ K-1 Ca% Mg%
S-1 Mn-1
Mn-All Mn-AI2
Zn-1
Zn-Al
Cu-I Na ESP SS-1 NO3-N
1.67 1.11 9.1 74 2.3 5.7
105 17 68 6
51 18
21 21
103
103
100 0.1
1
Sample ID: co174
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre) N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Soybean
0.0 0 0
90
0 0
10
0
0 0
Note: 3
2-Soybean
0.0 0 0
90
0 0
$
0
0 0
Note: 3 Note:
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/daft
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P-1 K-1 Ca% Mg%
S-1 Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
1.43 1.24 9.5 84 1.5 6.2
157 26 71 12
54 27
23 ' 23
153
153
230 0.1
1
North Carolina
Tobacco Trust Fund Commission
Reprogramming of the laboratory -information -management system that makes this report possible is
being funded through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.neagr.gov/agronomi/ Report No. FY17-SLO34453
Chad Hayes Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS% % CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on
Ca% % CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I copper index
ESP' exchangeable sodium percent
Fertilizer
HM% percent humic matter
Recommendations for field crops or other large areas are. listed separately for each nutrient to be added (in units of
K-1 potassium index
Ib/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20 potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should.be > 50. If they
Mg% % CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is,recommended, 0-0-22 (11.5% Mg) is
MIN mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn manganese
only on reports for greenhouse soil or problem samples.
Mn-A11 Mn-availability index for crop 1Mn-AI2
Mn-availability index for crop 2
Mn-I manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
M-0 mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
N nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N nitrate nitrogen
_
ORG organic soil class
--Recnmmendations
forsmall areas, such as tiome lawnslgardens, are listed -in units of1b11000 sgft-lf you—canoffind-
�p=t— - --currenfsoif pH
the exactfertilizer grade recommended on the report, visit www.ncapr.povlapronomi/obnart4.htn*fsFind information that
P-1 phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205 phosphate
S-1 sulfur index
Test Results
SS -I soluble salt index
W/V weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil. and its degree of acidity. The
Zn-AI zinc availability index
remaining 16 [P-1, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routine)
Zn-I zinc index
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.goylagronomiluyrst.htm

Page 1 of 2
Report Number: 18-033-0518
Account Number:46525
Send To: Synagro Central LLC/ Lumberton
Mary Brewer
284 Boger Road
Mocksville NC 27028
Waypoint
ANALYTICAL
'Every acre... Every year.
Farm ID/Name: RO-20
SOIL ANALYSIS REPORT
Date Received: 02/02/2018 Date Of Analysis: 02/05/2018 Date Of Report: 02/07/2018
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Grower: R G Hammonds
Analytical Method(s): • Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
OM
WN
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
o �°
Soil
Ibs1A
M3.
K
Mg
Ca
Na
Soil
Buffer
H
Field ID
Number
Rate
Class
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
pH
Index
meq/100g
meq/100g
3
01193
3.4
109
555 VH
106 M
129 H
743 M
18 VL
5.8
6.81
1.2
6.3
MIN
M
NC = 462
NC = 54
4
01195
3.4
[�_�
108
559 VH
106 M
124 H
790 M
19 VL
5.7
6.79
1.4
6.7
M
NC = 466
NC = 54
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Sample ID
Field ID-
K
Mg
Ca
Na
H
NO, N
S
Zn
Mn
Fe
Cu
B
SS
%
%
%
%
%
ppm Rate
ppm Rate.
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ms/cm
Rate
3
4.3
17.1
59.0
1.2
19.0
17 M
38.7 VH
18 M
216 VH
8.7 VH
0.5 L
0.13
VL
NC=35
NC=967.5
NC=113
NC=435.0
4
4.1
15.4
59.0
1.2
20.9
18 M
39.6 VH
19 M
211 VH
8.8 VH
0.6 M
0.13
VL
NC = 37
NC = 990.0
NC = 119
NC = 440.0
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meg1100g maximum of thirty days after testing.
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by:
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by: WaypointAnalytical Virginia, Inc.
Pauric McGroary

Page 2 of 2
Report Number: 18-033-0518
Account Number: 46525
Send To: Synagro Central LLC/ Lumberton
Mary Brewer
284 Boger Road
Mocksville. NC 27028
Date Received: 02/02/2018
Date Of Report: 02/07/2018
S i
WaypointANALYTICAL
"Every acre... Every year. "ram
Farm ID/Name: RO-20
SOIL FERTILITY RECOMMENDATIONS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Grower: R G Hammonds
Nitrogen
Phosphate
Potash
Magnesium
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Sample ID
Intended Crop
Yield Goal
Lime
N
P205
K20
Mg
S
Zn
Mn
Fe
Cu
B
Field ID
Tons/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
3
Adjust pH to 6.0
0
0.8
0
2
0
4
Adjust pH to 6.0
0
0.8
0
2
0
Comments:
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." �p M
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Pauric McGroary

Page 1 of 2
Report Number: 17-363-0506
Account Number: 46789
Send To: Synagro Central LLC/ Dunn
Mary Brewer
284 Boger Road
Mocksville NC 27028
WaypA
NALYTICAL
'Every acre ... Every year. "rM
SOIL ANALYSIS REPORT
Date Received: 12/29/2017 Date Of Analysis: 01/02/2018 Date Of Report: 01/02/2018
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Grower: Carhell Locklear
Analytical Method(s): SMP Buffer pH Mehlich 3 Loss On Ignition Water pH
OM
W/V
ENR
IPhosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Field ID
Lab
Number
o �0
Rate
Soil
Class
Ibs/A
M3
ppm Rate
ppm Rate
ppm Rate
K
ppm Rate
Mg
ppm Rate
Ca
ppm Rate
Na
ppm Rate
Soil
pH
Buffer
Index
H
meq/100g
meq/100g
R0281
09886
3.3
M
104
173 VH
NC = 144
147 H
NC = 75
130 M
1158 M
6.2
1.0
8.3
MIN
R028 3
09887
2.1
LH
86
150 VH
NC = 125
62 L
NC = 32
35 L
388 L
4.9
6.74
1.9
4.3
Sample ID
-Field ID
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble salts
K
%
Mg
%
Ca
%
Na
%
H
%
NO3 N
ppm Rate
S
ppm Rate
Zn
ppm Rate
Mn
ppm Rate
Fe
ppm Rate
Cu
ppm Rate
B
ppm Rate
SS
ms/cm Rate
R028 1
4.5
13.1
69.8
12.0
R028 3
3.7
6.8r
1 45.1
44.2
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pobnds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by; �puri� m� Gad
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble v
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysts prepared by: WaypolntAnalytical Virginia, Inc.
Pauric McGroary

Page 2 of 2
Report Number: 17-363-0506
Account Number:46789
Send To: Synagro Central LLC/ Dunn
Mary Brewer
284 Boger Road
Mocksville NC 27028
Date Received: 12/29/2017
Date Of Report: 01/02/2018
Waypoint0
ANALYTICAL
"Every acre... Every year. ".
SOIL FERTILITY RECOMMENDATIONS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Grower: Carhell Locklear
Nitrogen
Phosphate
Potash
Magnesium
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Sample ID
Intended Crop
Yield Goal
Lime
N
P205
K20
Mg
S
Zn
Mn
Fe
Cu
B
Field ID
Tons/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
lb/A.
R028 1
Adjust pH to 6.0
0
0.0
0
R028 3
Adjust pH to 6.0
0 •
2.0
17
Comments:
Sample(s) : R028 3 Crop: Adjust pH to 6.5
Apply dolomitic lime to raise pH and improve the magnesium level.
If dolomitic lime is not used, apply required magnesium with magnesium oxide. Epsom Salts, K-Mag or Sul-PO-Mag.
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ `� and may not be reproduced in whole or part, nor may any reference be made to the 1 Aw« tM
"c 60w
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Pauric McGroary

Page 1 of 2
Report Number: 18-033-0517
Account Number:46525
Send To: Synagro Central LLC/ Lumberton
Mary Brewer
284 Boger Road
Mocksville NC 27028
Waypoin0 -
t
ANALYTICAL
'Every acre... Every year.
Farm ID/Name: RO-39
SOIL ANALYSIS REPORT
Date Received: 02/02/2018 Date Of Analysis: 02/05/2018 Date Of Report: 02/07/2018
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Grower: Patrick Bullard
Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
OM
WN
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
Field ID
Number
r �°
Soil
lbs/A
M3
K
Mg
Ca
Na
Soil
Buffer
H
Rate
Class
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
pH
index
meq/100g
meq/100g
4
01191
2.6
93
253 ' VH
178 VH
112 M
900 H
22 VL
6.6
0.4
6.4
M
MIN
NC=211
NC=91
9
01192
2.8H97
239 VH
170 VH
112 H
831 M
20 VL
6.6
0.4
6.0
M
NC = 199
NC = 87
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble salts
Sample ID
Field ID
K
Mg
Ca
Na
I H
NO3 N
S
Zn
Mn
Fe
Cu
B
SS
%
%
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ms/cm Rate
4
7.1
14.6
70.3
1.$
6.3
9 VL
6.7 H
17 M
163 VH
1.4 M
0.4 L
0.11 VL
NC=19
NC=167.5
NC=106
NC=70.0
9
7.3
15.6
69.3
1.4
6.7
8 VL
7.0 H
16 M
173 VH
1.3 M
0.4 L
0.17 VL
NC=17
NC=175.0
NC=100
NC=65.0
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by:
C
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble
.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by: Waypoint Analytical Virginia, Inc.
Pauric McGroary

Page 2 of 2
Report Number: 18-033-0517
Account Number: 46525
Send To: Synagro Central LLC/ Lumberton
Mary Brewer
284 Boger Road
Mocksville NC 27028
Date Received: 02/02/2018
Date Of Report: 02/07/2018
o
Waypoint�
ANALYTICAL
Every acre... Every year. ",,,,
Farm ID/Name: RO-39
SOIL FERTILITY RECOMMENDATIONS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Grower: Patrick Bullard
Nitrogen
Phosphate
Potash
Magnesium
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Sample ID
Intended Crop
Yield Goal
Lime-
N
P205
K20
Mg
S
Zn
Mn
Fe
Cu
B
Field ID
Tons/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
4
Adjust pH to 6.0
0
0.0
0
2
0
9
Adjust pH to 6.0
0
0.0
0
2
0
Comments:
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." M
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Pauric McGroary

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY18-SL004179
r.ULTrja �
Predictive
Client:
Patrick Bullard
Advisor:
Chad Hayes
4147 Prospect Rd. / PO Box 1262
273 Pete Strickland Rd
y
F
S o i I Ike po rt
Mehlich-3 Extraction
Pembroke, NC 28372
Cerro Gordo, NC 28430
H�
Sampled County: Robeson
�-D�s�1.
Links to Helpful Information
Sampled: Not Provided
Received: 09/08/2017
Farm: Ro 39
Completed: 09/19/2017
Client ID: 260315
Advisor ID: 464046
Sample ID: Ro399
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre) N P206
K20 Mg S
Mn
Zn
Cu B
Information
Lime History:
1 -Bermuda hay/past., M
0.6 180-220 0
200 25 0.
0
0
0 0
Note: 12
2-Bermuda hay/past., M
0.0 180-220 0
200 $ 0
0
0
0 0
Note: 12 Note:
Test Results [units -W/V in g/cO; CEC and Na in meq/100 cO; NO3-N in mg/dO]:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH
P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2
Zn-I
Zn-Al
Cu-I Na ESP • SS-1 NO3-N
0.36 1.26
4.1 66 1.4 5.5 1
190 15 55 9 -
29 73 61 61
213
213
178 0.1 2
North Carolina
Tobacco Trust Fund Commission
Reprogramming of the laboratory -information -management system that makes this report possible is
being funded through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.neagr.gov/agronomi/ Report No. FYiu-5L004179
Patrick Bullard Page 2 of 2' 1
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations I Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings,where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer ,
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 60. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
Mn-AI1
manganese
Mn-availability index for crop 1
only on reports for greenhouse soil or problem samples.
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
M-0
mineral -organic soil class
notations appear on the soil report, refer to. $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations forsmall areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft .-If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.n6agr.povlagronomilobpart4.htmVfsFnd information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P206
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
Zn-I
zinc availability index
zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-I, Zn-AI, Cu-1, S-1, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.govlagronomiluvrst.htm