NC0026051_Permit renewal application_20051107

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NPDES FORM 2A APPLICATION OVERVIEW
APPLICATION OVERVIEW
BASIC APPLICATION INFORMATION:
A.lent works
that discharges effluent to surface waters of the United States must also answer questions A.9 through A. 12.
B.
C.Certification. All applicants must complete Part C (Certification).
SUPPLEMENTAL APPLICATION INFORMATION:
D.
1.
2.
3.
E.
1.
2.
3.
F.
1.
2.
a.
b.
c.
G.
ALL APPLICANTS MUST COMPLETE PART C (CERTIFICATION)
Page 1 of 22EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Cape Fear
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
FORM
2A
NPDES
Combined Sewer Systems. A treatment works that has a combined sewer system must complete Part G (Combined Sewer
Systems).
Industrial User Discharges and RCRA/CERCLA Wastes. A treatment works that accepts process wastewater from any
significant industrial users (SIUs) or receives RCRA or CERCLA wastes must complete Part F (Industrial User Discharges
and RCRA/CERCLA Wastes). SIUs are defined as:
All industrial users subject to Categorical Pretreatment Standards under 40 Code of Federal Regulations (CFR) 403.6 and
40 CFR Chapter I, Subchapter N (see instructions); and
Any other industrial user that:
Discharges an average of 25,000 gallons per day or more of process wastewater to the treatment works (with certain
exclusions); or
Contributes a process wastestream that makes up 5 percent or more of the average dry weather hydraulic or organic
capacity of the treatment plant; or
Is designated as an SIU by the control authority.
Toxicity Testing Data. A treatment works that meets one or more of the following criteria must complete Part E (Toxicity Testing
Data):
Has a design flow rate greater than or equal to 1 mgd,
Is required to have a pretreatment program (or has one in place), or
Is otherwise required by the permitting authority to submit results of toxicity testing.
-
Form 2A has been developed in a modular format and consists of a “Basic Application Information” packet
and a “Supplemental Application Information” packet. The Basic Application Information packet is divided
into two parts. All applicants must complete Parts A and C. Applicants with a design flow greater than or
equal to 0.1 mgd must also complete Part B. Some applicants must also complete the Supplemental
Application Information packet. The following items explain which parts of Form 2A you must complete.
Basic Application Information for all Applicants. All applicants must complete questions A.1 through A.8. A tre;
fVe design flowsAdditional Application Information for Applicants with a Design Flow > 0.1 mgd. All treatment wqiks
greater than or equal to 0.1 million gallons per day must complete questions B.1 through B.6. xf
•\\\
Expanded Effluent Testing Data. A treatment works that discharges effluent to surface waters o?the'lkiited Slates and meets
one or more of the following criteria must complete Part D (Expanded Effluent Testing Data):
Has a design flow rate greater than or equal to Imgd,
Is required to have a pretreatment program (or has one in place), or
Is otherwise required by the permitting authority to provide the information.
1
BASIC APPLICATION INFORMATION
PART A. BASIC APPLICATION INFORMATION FOR ALL APPLICANTS:
All treatment works must complete questions A.1 through A.8 of this Basic Application Information Packet.
A.1. Facility Information.
Facility Name Triangle Wastewater Treatment Plant
Mailing Address 5926 NC Hwy 55 East
Durham, NC 27713
Contact Person Adrienne Fancher
Title Project Manager
Telephone Number [phone]
Facility Address 5926 NC Hwy 55 East
(not P.O. Box)Durham. NC 27713
A.2. Applicant Information. If the applicant is different from the above, provide the following:
Applicant Name Chuck Hill
Mailing Address 120 East Parrish Street, Suite 110
Durham, NC 27701
Contact Person Chuck Hill
Title Utility Division Manager
Telephone Number [phone]
Is the applicant the owner or operator (or both) of the treatment works?
□ operator
Indicate whether correspondence regarding this permit should be directed to the facility or the applicant.
□ facility 0 applicant
NPDES NC 0026051 PSD
UIC Other Collections WQCS00038
RCRA Other Stormwater NCG 110054
Name Type of Collection System OwnershipPopulation Served
Durham County Sanitary Durham County6000
City of DurhamCity of Durham Sanitary3000
Total population served 9000
Page 2 of 22EPA Form 3510-2A (Rev. 1 -99). Replaces EPA forms 7550-6 & 7550-22.
A.3. Existing Environmental Permits. Provide the permit number of any existing environmental permits that have been issued to the treatment works
(include state-issued permits).
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Cape Fear
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
KI owner
A.4. Collection System Information. Provide information on municipalities and areas served by the facility. Provide the name and population of each
entity and, if known, provide information on the type of collection system (combined vs. separate) and its ownership (municipal, private, etc.).
1
A.5. Indian Country.
a.
[3 No
b.
Yes E No
A.6.
Design flow rate 12.a.mgd
Two Years Ago Last Year This Year
b.Annual average daily flow rate 4.762 3.839 4.120
Maximum daily flow ratec.19.431 9.846 8.200
A.7. Collection System. Indicate the type(s) of collection system(s) used by the treatment plant. Check all that apply. Also estimate the percent
100 %
%
A.8. Discharges and Other Disposal Methods.
Does the treatment works discharge effluent to waters of the U.S.?E Yes Noa.
If yes, list how many of each of the following types of discharge points the treatment works uses:
Discharges of treated effluent 1 (ONE)
ii.Discharges of untreated or partially treated effluent
iii.Combined sewer overflow points
iv.Constructed emergency overflows (prior to the headworks)
Otherv.
b.
0 No
If yes, provide the following for each surface impoundment:
Location:
mgd
Does the treatment works land-apply treated wastewater? Yes I3 Noc.
If yes, provide the following for each land application site:
Location:
Number of acres:
mgd
intermittent?Is land application
d.
Yes 0 No
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.Page 3 of 22
contribution (by miles) of each.
E Separate sanitary sewer
Does the treatment works discharge or transport treated or untreated wastewater to another
treatment works?
Annual average daily volume applied to site:
continuous or
Annual average daily volume discharge to surface impoundment(s)
Is discharge continuous or intermittent?
Is the treatment works located in Indian Country?
Yes
RIVER BASIN:
Cape Fear
PERMIT ACTION REQUESTED:
Renewal
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
Combined storm and sanitary sewer
Does the treatment works discharge effluent to basins, ponds, or other surface impoundments
that do not have outlets for discharge to waters of the U.S.? Yes
Does the treatment works discharge to a receiving water that is either in Indian Country or that is upstream from (and eventually flows
through) Indian Country?
Flow. Indicate the design flow rate of the treatment plant (i.e., the wastewater flow rate that the plant was built to handle). Also provide the
average daily flow rate and maximum daily flow rate for each of the last three years. Each year’s data must be based on a 12-month time period
with the 12 month of “this year" occurring no more than three months prior to this application submittal.
If transport is by a party other than the applicant, provide:
Transporter Name
Mailing Address
Contact Person
Title
Telephone Number (1
For each treatment works that receives this discharge, provide the following:
Name
Mailing Address
Contact Person
Title
Telephone Number (
If known, provide the NPDES permit number of the treatment works that receives this discharge
Provide the average daily flow rate from the treatment works into the receiving facility.mgd
e.
E] No□ Yes
If yes, provide the following for each disposal method:
Description of method (including location and size of site(s) if applicable):
□ intermittent?Is disposal through this method or
Page 4 of 22ERA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Annual daily volume disposed by this method:
□ continuous
Does the treatment works discharge or dispose of its wastewater in a manner not included
in A.8. through A.8.d above (e.g., underground percolation, well injection):
If yes, describe the mean(s) by which the wastewater from the treatment works is discharged or transported to the other treatment works
(e.g., tank truck, pipe).
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Cape Fear
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
r
WASTEWATER DISCHARGES:
A.9. Description of Outfall.
Outfall number 001a.
b.Location
Distance from shore (if applicable)NA ft.c.
d.Depth below surface (if applicable)NA ft.
Average daily flow rate 4.240 - based on A.6-b.e.mgd
f.Does this outfall have either an intermittent or a periodic discharge?□ Yes C3 No (gotoA.9.g.)
If yes, provide the following information:
Number f times per year discharge occurs:
Average duration of each discharge:
Average flow per discharge:mgd
Months in which discharge occurs:
Is outfall equipped with a diffuser?□ Yes 0 Nog-
A.10. Description of Receiving Waters.
Name of receiving water Northeast Creeka.
b.Name of watershed (if known)Cape Fear
United States Soil Conservation Service 14-digit watershed code (if known):not known
Name of State Management/River Basin (if known): Basin: 03-06-05c.
United States Geological Survey 8-digit hydrologic cataloging unit code (if known):not known
d.Critical low flow of receiving stream (if applicable)
cfsNAcfschronic NAacute
mg/l of CaCOsTotal hardness of receiving stream at critical low flow (if applicable): NAe.
Page 5 of 22ERA Form 3510-2A (Rev. 1-99). Replaces ERA forms 7550-6 & 7550-22.
RIVER BASIN:
Cape Fear
PERMIT ACTION REQUESTED:
Renewal
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
Durham, NC__________
(City or town, if applicable)
Durham
(County)
27713
(Zip Code)
78° 53' 50"
(Longitude)
35° 52' 51"
(Latitude)
NC
(State)
If you answered “Yes" to question A.8.a, complete questions A.9 through A.12 once for each outfall (including bypass points) through
which effluent is discharged. Do not include information on combined sewer overflows in this section. If you answered “No" to question
A-8.a, go to Part B. “Additional Application Information for Applicants with a Design Flow Greater than or Equal to 0.1 mgd.”
A.11. Description of Treatment
a.
El Advanced Describe:Tertiary Sand Filters
b.
Design BODS removal or Design CBOD5 removal 98 %
Design SS removal 97 %
Design P removal 95 %
Design N removal 93 %
Other Design Ammonia %
c.
Ultraviolet Disinfection (UV)
If disinfection is by chlorination is dechlorination used for this outfall?□ Yes □ No
Does the treatment plant have post aeration?13 Yes □ No
Outfall number:001
MAXIMUM DAILY VALUE AVERAGE DAILY VALUEPARAMETER
Value Units Value Units Number of Samples
pH (Minimum)6.00 s.u.
pH (Maximum)8.39 s.u.
Flow Rate 19.431 MGD 4.038 MGD 1719
Temperature (Winter)22.7 Deg C 13.7 Deg C 23
27.6 Deg C 21.7 Deg C 34
AVERAGE DAILY DISCHARGE
POLLUTANT ML/MDL
UnitsCone.Units Cone.
CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS
BODS mg/L 2 mg/L50mg/L 2.88 1171 ERA 405.1
CBOD5
FECAL COLIFORM 1155 9222D 1 Col/100 mL803012.09
TOTAL SUSPENDED SOLIDS (TSS)mg/L 1172 ERA 160.2 1 mg/L112mg/L 5.44
Page 6 of 22EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
A.12. Effluent Testing Information. All Applicants that discharge to waters of the US must provide effluent testing data for the following
parameters. Provide the indicated effluent testing required by the permitting authority for each outfall through which effluent is
discharged. Do not include information on combined sewer overflows in this section. All information reported must be based on data
collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of
40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. At a
minimum, effluent testing data must be based on at least three samples and must be no more than four and one-half years apart.
END OF PART A.
REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS
OF FORM 2A YOU MUST COMPLETE
What level of treatment are provided? Check all that apply.
□ Primary |3 Secondary
I3 Other.
Indicate the following removal rates (as applicable):
PERMIT ACTION REQUESTED:
Renewal
Number of
Samples
ANALYTICAL
METHOD
RIVER BASIN:
Cape Fear
BIOCHEMICAL OXYGEN
DEMAND (Report one)
Col/100
mL
Col/100
mL
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
Temperature (Summer)
* For pH please report a minimum and a maximum daily value
MAXIMUM DAILY
DISCHARGE
96
What type of disinfection is used for the effluent from this outfall? If disinfection varies by season, please describe:
BASIC APPLICATION INFORMATION
PART B.
B.1.
a.
c.
f.
B.3.
United Water Hydro Management LLCName:
2554 Lewisville Clemmons Road, Suite 304Mailing Address:
Clemmons. N.C 27012
[phone]Telephone Number:
The contract's Scope of Services is attached.Responsibilities of Contractor:
a.
none
b.
Page 7 of 22ERA Form 3510-2A (Rev. 1-99). Replaces ERA forms 7550-6 & 7550-22.
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Cape Fear
ADDITIONAL APPLICATION INFORMATION FOR APPLICANTS WITH A DESIGN FLOW GREATER THAN OR
EQUAL TO 0.1 MGD (100,000 gallons per day).
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
gpd
Briefly explain any steps underway or planned to minimize inflow and infiltration.
We are utilizing annual manhole inspections and quarterly high priority line inspections to identify areas to repair.
We are developing a specification for flow meters for the collection system to further identify l/l sources._______
Indicate whether the planned improvements or implementation schedule are required by local, State, or Federal agencies.
Yes No
Process Flow Diagram or Schematic. Provide a diagram showing the processes of the treatment plant, including all bypass piping and all
backup power sources or redunancy in the system. Also provide a water balance showing all treatment units, including disinfection (e.g.,
chlorination and dechlorination). The water balance must show daily average flow rates at influent and discharge points and approximate daily flow
rates between treatment units. Include a brief narrative description of the diagram.
B.4. Operation/Maintenance Performed by Contractor(s).
Are any operational or maintenance aspects (related to wastewater treatment and effluent quality) of the treatment works the responsibility of a
contractor? Yes No
If yes, list the name, address, telephone number, and status of each contractor and describe the contractor’s responsibilities (attach additional
pages if necessary).
B.2. Topographic Map. Attach to this application a topographic map of the area extending at least one mile beyond facility property boundaries. This
map must show the outline of the facility and the following information. (You may submit more than one map if one map does not show the entire
area.)
The area surrounding the treatment plant, including all unit processes.
b. The major pipes or other structures through which wastewater enters the treatment works and the pipes or other structures through which
treated wastewater is discharged from the treatment plant. Include outfalls from bypass piping, if applicable.
Each well where wastewater from the treatment plant is injected underground.
d. Wells, springs, other surface water bodies, and drinking water wells that are: 1) within 14 mile of the property boundaries of the treatment
works, and 2) listed in public record or otherwise known to the applicant.
e. Any areas where the sewage sludge produced by the treatment works is stored, treated, or disposed.
If the treatment works receives waste that is classified as hazardous under the Resource Conservation and Recovery Act (RCRA) by truck, rail,
or special pipe, show on the map where the hazardous waste enters the treatment works and where it is treated, stored, and/or disposed.
All applicants with a design flow rate > 0.1 mgd must answer questions B.1 through B.6. Ail others go to Part C (Certification).
Inflow and Infiltration. Estimate the average number of gallons per day that flow into the treatment works from inflow and/or infiltration.
500,000
B.5. Scheduled improvements and Schedules of Implementation. Provide information on any uncompleted implementation schedule or
uncompleted plans for improvements that will affect the wastewater treatment, effluent quality, or design capacity of the treatment works. If the
treatment works has several different implementation schedules or is planning several improvements, submit separate responses to question B.5
for each. (If none, go to question B.6.)
List the outfall number (assigned in question A.9) for each outfall that is covered by this implementation schedule.
If the answer to B.5.b is "Yes," briefly describe, including new maximum daily inflow rate (if applicable).c.
d.
applicable. Indicate dates as accurately as possible.
Schedule Actual Completion
Implementation Stage MM/DD/YYYY MM/DD/YYYY
- Begin Construction
- End Construction /
- Begin Discharge
- Attain Operational Level
Have appropriate permits/clearances concerning other Federal/State requirements been obtained?e.□ Yes □ No
Describe briefly:
B.6.
Outfall Number: 001
AVERAGE DAILY DISCHARGE
POLLUTANT ML/MDL
Cone.Units Cone.Units
11.8 mg/L .35 mg/L 1154 ERA 350.3 .1 mg/L
3.5 mg/L .331 mg/L SM4500-CI G474 .01 mg/L
DISSOLVED OXYGEN 13.96 mg/L 8.08 mg/L 1670 SM4500-0 G .05 mg/L
TOTAL NITROGEN (TN)122 mg/L 17.66 mg/L 270 ERA 353.2 0.5 mg/L
MERCURY-LOW LEVEL .00691 ug/L .002217 ug/L 108 ERA 1631 .001 ug/L
OIL and GREASE <2 mg/L <2 mg/L 3 ERA 413.1 2 mg/L
PHOSPHORUS (Total)3.8 mg/L .71 mg/L 351 4500P-E .1 mg/L
811 mg/L mg/L664 3 ERA 160.1 10 mg/L
OTHER
ERA Form 3510-2A (Rev. 1-99). Replaces ERA forms 7550-6 & 7550-22.Page 8 of 22
TOTAL DISSOLVED SOLIDS
(TDS)
CHLORINE (TOTAL
RESIDUAL, TRC)
END OF PART B.
REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS
OF FORM 2A YOU MUST COMPLETE
MAXIMUM DAILY
DISCHARGE
Number of
Samples
ANALYTICAL
METHOD
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Cape Fear
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS
AMMONIA (as N)
Provide dates imposed by any compliance schedule or any actual dates of completion for the implementation steps listed below, as
applicable. For improvements planned independently of local, State, or Federal agencies, indicate planned or actual completion dates, as
EFFLUENT TESTING DATA (GREATER THAN 0.1 MGD ONLY).
Applicants that discharge to waters of the US must provide effluent testing data for the following parameters. Provide the indicated
effluent testing required by the permitting authority for each outfall through which effluent is discharged. Do not include information
on combine sewer overflows in this section. All information reported must be based on data collected through analysis conducted
using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate
QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. At a minimum effluent testing data must be
based on at least three pollutant scans and must be no more than four and on-half years old.
r
BASIC APPLICATION INFORMATION
PART C. CERTIFICATION
ALL APPLICANTS MUST COMPLETE THE FOLLOWING CERTIFICATION.
Name and official title
Signature
Telephone number
Date signed
SEND COMPLETED FORMS TO:
27699-1617
Page 9 of 22EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
RIVER BASIN:
Cape Fear
NCDENR/ DWQ
Attn: NPDES Unit
1617 Mail Service Center
Raleigh, North Carolina
PERMIT ACTION REQUESTED:
Renewal
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who
manage the system or those persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment
for knowing violations.
Indicate which parts of Form 2A you have completed and are submitting:
0 Basic Application Information packet Supplemental Application Information packet:
0 Part D (Expanded Effluent Testing Data)
S Part E (Toxicity Testing: Biomonitoring Data)
El Part F (Industrial User Discharges and RCRA/CERCLA Wastes)
□ Part G (Combined Sewer Systems)
[phone],______________________________________________________________________________
U //
Upon request of the permitting authority, you must submit any other information necessary to assure wastewater treatment practices at the treatment
works or identify appropriate permitting requirements.
Chuck Hill, Utility Division Manager - Durham County
All applicants must complete the Certification Section. Refer to instructions to determine who is an officer for the purposes of this
certification. All applicants must complete all applicable sections of Form 2A, as explained in the Application Overview. Indicate below which
parts of Form 2A you have completed and are submitting. By signing this certification statement, applicants confirm that they have reviewed
Form 2A and have completed all sections that apply to the facility for which this application is submitted.
PERMIT ACTION REQUESTED:RIVER BASIN:
Renewal Cape Fear
SUPPLEMENTAL APPLICATION INFORMATION
PART D. EXPANDED EFFLUENT TESTING DATA
Refer to the directions on the cover page to determine whether this section applies to the treatment works.
Outfall number:001 - Results attached
MAXIMUM DAILY DISCHARGE
POLLUTANT ML/MDLCone.Units Mass Units Cone.Units Mass Units
METALS (TOTAL RECOVERABLE), CYANIDE, PHENOLS, AND HARDNESS.
ANTIMONY
ARSENIC
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
MERCURY
NICKEL
SELENIUM
SILVER
THALLIUM
ZINC
CYANIDE
HARDNESS (as CaCO3)
Use this space (or a separate sheet) to provide information on other metals requested by the permit writer
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.Page 10 of 22
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
Number
of
Samples
TOTAL PHENOLIC
COMPOUNDS
ANALYTICAL
METHOD
(Complete once for each outfall discharging effluent to waters of the United States.)
AVERAGE DAILY DISCHARGE
Effluent Testing: 1.0 mgd and Pretreatment Works. If the treatment works has a design flow greater than or equal to 1.0 mgd or it has (or is required
to have) a pretreatment program, or is otherwise required by the permitting authority to provide the data, then provide effluent testing data for the following
pollutants. Provide the indicated effluent testing information and any other information required by the permitting authority for each outfall through which
effluent is discharged. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected
through analyses conducted using 40 CFR Part 136 methods. In addition, these data must comply with QA/QC requirements of 40 CFR Part 136 and
other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. Indicate in the blank rows provided below
any data you may have on pollutants not specifically listed in this form. At a minimum, effluent testing data must be based on at least three pollutant
scans and must be no more than four and one-half years old.
FACILITY NAME AND PERMIT NUMBER:PERMIT ACTION REQUESTED:RIVER BASIN:
Triangle WWTP, NC0026051 Renewal Cape Fear
AVERAGE DAILY DISCHARGE
POLLUTANT ML/MDL
Cone.Units Mass Units Cone.Units Mass Units
VOLATILE ORGANIC COMPOUNDS
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOFORM
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
1,1-DICHLOROETHANE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
ETHYLBENZENE
METHYL BROMIDE
METHYL CHLORIDE
METHYLENE CHLORIDE
TOLUENE
Page 11 of 22EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Outfall number: 001 - Results attached (Complete once for each outfall discharging effluent to waters of the United States.)
MAXIMUM DAILY DISCHARGE
Number
of
Samples
CARBON
TETRACHLORIDE
ANALYTICAL
METHOD
TETRACHLORO­
ETHYLENE
1,3-DICHLORO-
PROPYLENE
TRANS-1.2-DICHLORO-
ETHYLENE
1,1-DICHLORO­
ETHYLENE
2-CHLOROETHYLVINYL
ETHER
DICHLOROBROMO­
METHANE
CHLORODIBROMO­
METHANE
1,1,2,2-TETRA-
CHLOROETHANE
PERMIT ACTION REQUESTED:RIVER BASIN:
Renewal Cape Fear
Outfall number: 001 - Results attached
AVERAGE DAILY DISCHARGE
POLLUTANT ML/MDLCone.Units Mass Units Cone.Units Mass Units
TRICHLOROETHYLENE
VINYL CHLORIDE
Use this space (or a separate sheet) to provide information on other volatile organic compounds requested by the permit writer
ACID-EXTRACTABLE COMPOUNDS
P-CHLORO-M-CRESOL
2-CHLOROPHENOL
2,4-DICHLOROPHENOL
2.4-DIMETHYLPHENOL
4,6-DINITRO-O-CRESOL
2,4-DINITROPHENOL
2-NITROPHENOL
4-NITROPHENOL
PENTACHLOROPHENOL
PHENOL
Use this space (or a separate sheet) to provide information on other acid-extractable compounds requested by the permit writer
BASE-NEUTRAL COMPOUNDS
ACENAPHTHENE
ACENAPHTHYLENE
ANTHRACENE
BENZIDINE
BENZO(A)ANTHRACENE
BENZO(A)PYRENE
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.Page 12 of 22
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
Number
of
Samples
ANALYTICAL
METHOD
2,4,6-
TRICHLOROPHENOL
1.1,2-
TRICHLOROETHANE
1.1,1-
TRICHLOROETHANE
(Complete once for each outfall discharging effluent to waters of the United States.)
MAXIMUM DAILY DISCHARGE
FACILITY NAME AND PERMIT NUMBER:PERMIT ACTION REQUESTED:RIVER BASIN:
Triangle WWTP, NC0026051 Renewal Cape Fear
Outfall number: 001 - Results attached
AVERAGE DAILY DISCHARGE
POLLUTANT ML/MDL
Cone.Units Mass Units Cone.Units Mass Units
BENZO(GHI)PERYLENE
CHRYSENE
DI-N-BUTYL PHTHALATE
DI-N-OCTYL PHTHALATE
1,2-DICHLOROBENZENE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
DIETHYL PHTHALATE
DIMETHYL PHTHALATE
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
Page 13 of 22EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Number
of
Samples
1,2-DIPHENYL-
HYDRAZINE
3,3-DICHLORO-
BENZIDINE
DIBENZO(A,H)
ANTHRACENE
4-CHLORPHENYL
PHENYL ETHER
4-BROMOPHENYL
PHENYL ETHER
2-CHLORO-
NAPHTHALENE
BUTYL BENZYL
PHTHALATE
BIS (2-CHLOROISO-
PROPYL) ETHER
BIS (2-ETHYLHEXYL)
PHTHALATE
BIS (2-CHLOROETHOXY)
METHANE
BIS (2-CHLOROETHYL)-
ETHER
BENZO(K)
FLUORANTHENE
3,4 BENZO­
FLUORANTHENE
ANALYTICAL
METHOD
(Complete once for each outfall discharging effluent to waters of the United States.)
MAXIMUM DAILY DISCHARGE
FACILITY NAME AND PERMIT NUMBER:PERMIT ACTION REQUESTED:RIVER BASIN:
Triangle WWTP, NC0026051 Renewal Cape Fear
Outfall number: 001 - Results attached (Complete once for each outfall discharging effluent to waters of the United States.)
MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE
POLLUTANT ML/MDLCone.Units Mass Units Cone.Units Mass Units
FLUORANTHENE
FLUORENE
HEXACHLOROBENZENE
HEXACHLOROETHANE
ISOPHORONE
NAPHTHALENE
NITROBENZENE
PHENANTHRENE
PYRENE
Use this space (or a separate sheet) to provide information on other pollutants (e.g., pesticides) requested by the permit writer
Page 14 of 22EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
I I I I I
Use this space (or a separate sheet) to provide information on other base-neutral compounds requested by the permit writer
END OF PART D.
REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS
OF FORM 2A YOU MUST COMPLETE
Number
of
Samples
N-NITROSODI-
METHYLAMINE
N-NITROSODI-
PHENYLAMINE
N-NITROSODI-N-
PROPYLAMINE
INDENO(1,2,3-CD)
PYRENE
HEXACHLORO­
BUTADIENE
HEXACHLOROCYCLO-
PENTADIENE
ANALYTICAL
METHOD
1,2,4-
TRICHLOROBENZENE
SUPPLEMENTAL APPLICATION INFORMATION
PART E. TOXICITY TESTING DATA
E.1.Required Tests.
[please see attached results.6 acute
Test number: Test number: Test number:
Test information.a.
Test Species & test method number
Age at initiation of test
Outfall number
Dates sample collected
Date test started
Duration
b. Give toxicity test methods followed.
Manual title
Edition number and year of publication
Page number(s)
Give the sample collection method(s) used. For multiple grab samples, indicate the number of grab samples used.c.
24-Hour composite
Grab
d.Indicate where the sample was taken in relation to disinfection. (Check all that apply for each.
Before disinfection
After disinfection
After dechlorination
Page 15 of 22EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Indicate the number of whole effluent toxicity tests conducted in the past four and one-half years.
,19 | chronic | 6 |
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Cape Fear
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
E.2. Individual Test Data. Complete the following chart for each whole effluent toxicity test conducted in the last four and one-half years. Allow one
column per test (where each species constitutes a test). Copy this page if more than three tests are being reported.
POTWs meeting one or more of the following criteria must provide the results of whole effluent toxicity tests for acute or chronic toxicity for each of the
facility's discharge points: 1) POTWs with a design flow rate greater than or equal to 1.0 mgd; 2) POTWs with a pretreatment program (orthose that are
required to have one under 40 CFR Part 403); or 3) POTWs required by the permitting authority to submit data for these parameters.
• At a minimum, these results must include quarterly testing for a 12-month period within the past 1 year using multiple species (minimum of two
species), or the results from four tests performed at least annually in the four and one-half years prior to the application, provided the results
show no appreciable toxicity, and testing for acute and/or chronic toxicity, depending on the range of receiving water dilution. Do not include
information on combined sewer overflows in this section. All information reported must be based on data collected through analysis conducted
using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC
requirements for standard methods for analytes not addressed by 40 CFR Part 136.
• In addition, submit the results of any other whole effluent toxicity tests from the past four and one-half years. If a whole effluent toxicity test
conducted during the past four and one-half years revealed toxicity, provide any information on the cause of the toxicity or any results of a
toxicity reduction evaluation, if one was conducted.
• If you have already submitted any of the information requested in Part E, you need not submit it again. Rather, provide the information
requested in question E.4 for previously submitted information. If EPA methods were not used, report the reasons for using alternate methods.
If test summaries are available that contain all of the information requested below, they may be submitted in place of Part E.
If no biomonitoring data is required, do not complete Part E. Refer to the Application Overview for directions on which other sections of the form to
complete.
|please see attached results)Test number:Test number:Test number:
Describe the point in the treatment process at which the sample was collected.e.
Sample was collected:
f.For each test, include whether the test was intended to assess chronic toxicity, acute toxicity, or both
Chronic toxicity
Acute toxicity
g. Provide the type of test performed.
Static
Static-renewal
Flow-through
h.Source of dilution water. If laboratory water, specify type; if receiving water, specify source.
Laboratory water
Receiving water
I.Type of dilution water. If salt water, specify "natural" or type of artificial sea salts or brine used.
Fresh water
Salt water
j-Give the percentage effluent used for all concentrations in the test series.
k. Parameters measured during the test. (State whether parameter meets test method specifications)
pH
Salinity
Temperature
Ammonia
Dissolved oxygen
I.Test Results.
Acute:
%%%
lc50
%%%95% C.I.
%%%Control percent survival
Other (describe)
Page 16 of 22EPA Form 3510-2A (Rev. 1 -99). Replaces EPA forms 7550-6 & 7550-22.
Percent survival in 100%
effluent
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Cape Fear
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
Chronic:
NOEC %%%
IC25 %%%
Control percent survival %%%
Other (describe)
Is reference toxicant data available?
I I I I I I
Other (describe)
□ Yes £3 No If yes, describe:
Date submitted:(MM/DD/YYYY)
Summary of results: (see instructions)
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.Page 17 of 22
________________________________________________________________
E.3. Toxicity Reduction Evaluation. Is the treatment works involved in a Toxicity Reduction Evaluation?
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Cape Fear
Was reference toxicant test within
acceptable bounds?
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
END OF PART E.
REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS
OF FORM 2A YOU MUST COMPLETE.
What date was reference toxicant test
run (MM/DD/YYYY)?
E.4. Summary of Submitted Biomonitoring Test Information. If you have submitted biomonitoring test information, or information regarding the
cause of toxicity, within the past four and one-half years, provide the dates the information was submitted to the permitting authority and a summary
of the results.
m. Quality Control/Quality Assurance.
SUPPLEMENTAL APPLICATION INFORMATION
PART F. INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES
F.l.
F.2.Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (ClUs). Provide the number of each of the following types of
industrial users that discharge to the treatment works.
Number of non-categorical SIUs.6a.
b.Number of CIUs.9
SIGNIFICANT INDUSTRIAL USER INFORMATION:
Name:Please see Addendum for details pertaining to the 15 SIUs for Questions F.3. through F.8.
Mailing Address:
F.4.Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge.
Principal product(s):
Raw material(s):
F.6.Flow Rate.
a.
C continuous or intermittent)
b.
C intermittent) gpdcontinuous or
Pretreatment Standards. Indicate whether the SIU is subject to the following:F.7.
Yes NoLocal limitsa.
Yes NoCategorical pretreatment standardsb.
If subject to categorical pretreatment standards, which category and subcategory?
Page 18 of 22EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
All treatment works receiving discharges from significant industrial users or which receive RCRA.CERCLA, or other remedial wastes must
complete part F.
GENERAL INFORMATION:
Pretreatment program. Does the treatment works have, or is subject to an approved pretreatment program?
0 Yes No
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Cape Fear
gpd
Non-process wastewater flow rate. Indicate the average daily volume of non-process wastewater flow discharged into the collection system
in gallons per day (gpd) and whether the discharge is continuous or intermittent.
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per
day (gpd) and whether the discharge is continuous or intermittent.
Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and
provide the information requested for each SIU.
F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU’s
discharge.
F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages
as necessary.
F.8.
F.10.
Amount Units
F.13. Waste Origin. Describe the site and type of facility at which the CERCLA/RCRA/or other remedial waste originates (or is excepted to origniate in
the next five years).
F.15. Waste Treatment.
a.
No
If yes, describe the treatment (provide information about the removal efficiency):
b.
Intermittent If intermittent, describe discharge schedule.
ERA Form 3510-2A (Rev. 1-99). Replaces ERA forms 7550-6 & 7550-22.Page 19 of 22
END OF PART F.
REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS
OF FORM 2A YOU MUST COMPLETE
Is the discharge (or will the discharge be) continuous or intermittent?
Continuous
Is this waste treated (or will be treated) prior to entering the treatment works?
Yes
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Cape Fear
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
CERCLA (SUPERFUND) WASTEWATER, RCRA REMEDIATION/CORRECTIVE ACTION
WASTEWATER, AND OTHER REMEDIAL ACTIVITY WASTEWATER:
F.14. Pollutants. List the hazardous constituents that are received (or are expected to be received). Include data on volume and concentration, if
known. (Attach additional sheets if necessary.)
F.12. Remediation Waste. Does the treatment works currently (or has it been notified that it will) receive waste from remedial activities?
Yes (complete F.13 through F.15.) EJ No
Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g.,
upsets, interference) at the treatment works in the past three years?
Yes No If yes, describe each episode.
RCRA HAZARDOUS WASTE RECEIVED BY TRUCK, RAIL, OR DEDICATED PIPELINE: ' “
F.9. RCRA Waste. Does the treatment works receive or has it in the past three years received RCRA hazardous waste by truck, rail or dedicated pipe?
Yes E| No (go to F.12)
Waste transport. Method by which RCRA waste is received (check all that apply):
Truck Rail Dedicated Pipe
F.11. Waste Description. Give ERA hazardous waste number and amount (volume or mass, specify units).
ERA Hazardous Waste Number
SUPPLEMENTAL APPLICATION INFORMATION
F.1.
Number of non-categorical SIUs.6a.
b.Number of CIUs.9
SIGNIFICANT INDUSTRIAL USER INFORMATION:
F.3.
Name:Cintas
Mailing Address: 1003 Twin Creeks Court
Durham. NC 27703
F.4.Industrial Processes. Describe all the industrial processes that affect or contribute to the Sill’s discharge.
Principal product(s): Laundered goods
F.6.
a.
55.419 continuous or
b.
intennittent) gpd (.continuous or
F.7.
Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages
as necessary.
Process wastewater flow rate. Indicate the average daily volume of process wastewater
discharge into the collection system in gallons per day (gpd) and whether the discharge is
continuous or intermittent.
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Cape Fear
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
Pretreatment program. Does the treatment works have, or is subject to an approved pretreatment program?
KI Yes No
F.2. Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (CIUs). Provide the number of each of the following types of
industrial users that discharge to the treatment works.
gpd (X continuous or intermittent)
Non-process wastewater flow rate. Indicate the average daily volume of non-process
wastewater flow discharged into the collection system in gallons per day (gpd) and
whether the discharge is continuous or intermittent.
PART F. INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES
All treatment works receiving discharges from significant industrial users or which receive RCRA,CERCLA, or other remedial wastes must
complete part F.
<.IM1MI IXf OKXl \ | |< >\ . . . , -A;../' • A '•/I •' '?
Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and
provide the information requested for each SIU.
Raw material(s): Water and detergents to clean garments, mats, and towels.
Flow Rate.
Industrial Laundry Facility - Washing, drying, and sorting of garments, mats, and shop towels.
F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU’s
discharge.
Pretreatment Standards. Indicate whether the SIU is subject to the following:
a. Local limits Yes I I No
b. Categorical pretreatment standards Q Yes M No
If subject to categorical pretreatment standards, which category and subcategory?
F.8.
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Cape Fear
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU
caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past
three years?
Yes No If yes, describe each episode.
None of the 15 industries detailed in Part F has caused or contributed to any problems at the
treatment works in the past three years,
SUPPLEMENTAL APPLICATION INFORMATION
F.2.
Number of non-categorical SIUs.6c.
d.Number of CIUs.9
SIGNIFICANT INDUSTRIAL USER INFORMATION:
Name:Cree
Mailing Address: 4600 Silicon Drive
Durham. NC 27703
F.4.Industrial Processes. Describe all the industrial processes that affect or contribute to the SID's discharge.
Semiconductor manufacturing
Principal product(s): Semiconductors for LCD (Liquid Crystal Display) and LED (Light Emitting
Diode
F.6.
C.
326.869 continuous or
d.
continuous or intermittent)
F.7.
a.
b.
469 A&B
Process wastewater flow rate. Indicate the average daily volume of process wastewater
discharge into the collection system in gallons per day (gpd) and whether the discharge is
continuous or intermittent.
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Cape Fear
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
gpd (X continuous or intermittent)
Non-process wastewater flow rate. Indicate the average daily volume of non-process
wastewater flow discharged into the collection system in gallons per day (gpd) and
whether the discharge is continuous or intermittent.
PART F. INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES
All treatment works receiving discharges from significant industrial users or which receive RCRA.CERCLA, or other remedial wastes must
complete part F.
(.FNERAL INFORMAI ION: ~ '. , . . 4 \ 7 7 = _ 7-
F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SID’s
discharge.
F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages
as necessary.
Raw material(s):Various etchants, photoresists, and strippers as well as some chemical compounds.
Flow Rate.
gpd C
Pretreatment Standards. Indicate whether the SIU is subject to the following:
Local limits [X] Yes | | No
Categorical pretreatment standards Yes Q No
If subject to categorical pretreatment standards, which category and subcategory?
Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and
provide the information requested for each SIU.
F.1. Pretreatment program. Does the treatment works have, or is subject to an approved pretreatment program?
Yes No
Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (CIUs). Provide the number of each of the following types of
industrial users that discharge to the treatment works.
SUPPLEMENTAL APPLICATION INFORMATION
F.l.
F.2.
6e.
f.9
as necessary.
Name:
F.4.
F.5.
F.6.
e.
continuous or intermittent)
F.7.
433.17
Number of non-categorical SIUs.
Number of CIUs.
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Cape Fear
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
Process wastewater flow rate. Indicate the average daily volume of process wastewater
discharge into the collection system in gallons per day (gpd) and whether the discharge is
continuous or intermittent.
Dupont
Mailing Address: PO Box 13999
Principal product(s): Electronics industry R&D
Raw material(s): Metallic powders, metal oxides, ceramic and glass, resin media, thinners, polymers,
monomers, inhibitors, nitric acid, sodium hydroxide, water________________________________
Flow Rate.
18.889 gpd (X continuous or intermittent)
f.Non-process wastewater flow rate. Indicate the average daily volume of non-process wastewater
flow discharged into the collection system in gallons per day (gpd) and whether the
discharge is continuous or intermittent.
gpd (.
Pretreatment Standards. Indicate whether the SIU is subject to the following:
a. Local limits KI Yes O No
b. Categorical pretreatment standards K Yes O No
If subject to categorical pretreatment standards, which category and subcategory?
Pretreatment program. Does the treatment works have, or is subject to an approved pretreatment program?
K Yes Q No
Number of Significant Industrial Users (SIUs) and Categorical industrial Users (CIUs). Provide the number of each of the following types of
industrial users that discharge to the treatment works.
Research Triangle Park, NC 27709
Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU’s discharge.
Customer service as well as R&D and limited scale up production for the electronics industry.
Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU’s
discharge.
SIGMF1CAM IMH STRI Al I SER l\FORMATIOX: ~ ............ _
Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F 8 and
provide the information requested for each SIU.
F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages
PART F, INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES
complete partF0*8 reCe‘Vin9 discharges from significant industrial users or which receive RCRA,CERCLA, or other remedial wastes must
SUPPLEMENTAL APPLICATION INFORMATION
PART F. INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES
F.2.
g. Number of non-categorical SIUs.6
h.Number of CIUs.9
SIGNIFICANT INDUSTRIAL USER INFORMATION:
Name:Eisai
Mailing Address: PQ Box 14505
Research Triangle Park, NC 27709
F.4.Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge.
Pharmaceutical Manufacturing and R&D
Principal product(s): Aciphex, Aricept
Raw material(s): Various reagents including acids, com starch, ethanol, mineral oil, and sodium
chloride present
F.6.Flow Rate.
g-
36.132 continuous or
h.
intermittent) gpd (.continuous or
F.7.
a.
b.
439 D & E
All treatment works receiving discharges from significant industrial users or which receive RCRA,CERCLA, or other remedial wastes must
complete part F.
GENERAL INFORMATION: “ ■... " ’ „ !
Process wastewater flow rate. Indicate the average daily volume of process wastewater
discharge into the collection system in gallons per day (gpd) and whether the discharge is
continuous or intermittent.
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Cape Fear
Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and
provide the information requested for each SIU.
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
gpd (X continuous or intermittent)
Non-process wastewater flow rate. Indicate the average daily volume of non-process
wastewater flow discharged into the collection system in gallons per day (gpd) and
whether the discharge is continuous or intermittent.
F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages
as necessary.
F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's
discharge.
Pretreatment Standards. Indicate whether the SIU is subject to the following:
Local limits Yes I I No
Categorical pretreatment standards KI Yes Q No
If subject to categorical pretreatment standards, which category and subcategory?
F.1. Pretreatment program. Does the treatment works have, or is subject to an approved pretreatment program?
K Yes No
Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (CIUs). Provide the number of each of the following types of
industrial users that discharge to the treatment works.
SUPPLEMENTAL APPLICATION INFORMATION
F.2.
Number of non-categorical SIUs.6i.
j-Number of CIUs.9
SIGNIFICANT INDUSTRIAL USER INFORMATION:
Name:GlaxoSmithKline
Mailing Address: PO Box 13398
Research Triangle Park, NC 27709
F.4.Industrial Processes. Describe all the industrial processes that affect or contribute to the Sill’s discharge.
Principal product(s): Pharmaceutical R&D
Raw material(s): Numerous organic and inorganic chemicals that vary based on current project.
GSKs waste management policies attempt to ensure no unauthorized drain disposals.
F.6.
306.048 continuous or
intermittent)continuous or
F.7.
a.
b.
439 E
Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and
provide the information requested for each SIU.
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Cape Fear
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
gpd (X continuous or intermittent)
j.Non-process wastewater flow rate. Indicate the average daily volume of non-process wastewater
flow discharged into the collection system in gallons per day (gpd) and whether the
discharge is continuous or intermittent.
Flow Rate.
i. Process wastewater flow rate. Indicate the average daily volume of process wastewater
discharge into the collection system in gallons per day (gpd) and whether the discharge is
continuous or intermittent.
PART F. INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES
All treatment works receiving discharges from significant industrial users or which receive RCRA,CERCLA, or other remedial wastes must
complete part F.
GENERAL INIORM \TK>\: F " ~ .
gpd (.
Pretreatment Standards. Indicate whether the SIU is subject to the following:
Local limits Yes I I No
Categorical pretreatment standards Yes O No
If subject to categorical pretreatment standards, which category and subcategory?
F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages
as necessary.
Pharmaceutical R&D-pilot plant for clinical trials and developing manufacturing procedures.
F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU’s
discharge.
F.1. Pretreatment program. Does the treatment works have, or is subject to an approved pretreatment program?
£<] Yes No
Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (CIUs). Provide the number of each of the following types of
industrial users that discharge to the treatment works.
SUPPLEMENTAL APPLICATION INFORMATION
F.l.
F.2.
k.Number of non-categorical SIUs.6
1.Number of CIUs.9
SIGNIFICANT INDUSTRIAL USER INFORMATION:
Name:IBM
Mailing Address: PO Box 12195
Research Triangle Park, NC 27709
F.4.Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge.
Light manufacturing/assembly of computer hardware products, refurbishment, and hardware and
Principal product(s): Assembly and development of PCs and servers, computer R&D
Raw material(s): Some reagents, computers, servers, etc.
F.6.
continuous or 182,433
intermittent)continuous or gpd (.
F.7.
Process wastewater flow rate. Indicate the average daily volume of process wastewater
discharge into the collection system in gallons per day (gpd) and whether the discharge is
continuous or intermittent.
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Cape Fear
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
Pretreatment program. Does the treatment works have, or is subject to an approved pretreatment program?
KI Yes No
Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (CIUs). Provide the number of each of the following types of
industrial users that discharge to the treatment works.
gpd (X continuous or intermittent)
l.Non-process wastewater flow rate. Indicate the average daily volume of non-process wastewater
flow discharged into the collection system in gallons per day (gpd) and whether the
discharge is continuous or intermittent.
Flow Rate.
k.
PART F. INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES
All treatment works receiving discharges from significant industrial users or which receive RCRA,CERCLA, or other remedial wastes must
complete part F.
(.IM RAI. INFORMA1 ION;
Pretreatment Standards. Indicate whether the SIU is subject to the following:
a. Local limits [X] Yes I I No
b. Categorical pretreatment standards Q Yes M No
If subject to categorical pretreatment standards, which category and subcategory?
Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and
provide the information requested for each SIU.
F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages
as necessary.
software development. Call centers for software/hardware support and human resources.
F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU’s
discharge.
SUPPLEMENTAL APPLICATION INFORMATION
m. Number of non-categorical SIUs.6
Number of CIUs.9n.
SIGNIFICANT INDUSTRIAL USER INFORMATION:
Name:JMC
Mailing Address: PO Box 13582
Research Triangle Park, NC 27709
F.4.Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge.
High purity chromium metal
Principal product(s): High Purity Chromium
Raw material(s): Chromium Anhydride, Sulfuric, Water. Aluminum foil. Sodium Hydroxide. Nitric
F.6.Flow Rate.
m.
continuous or X790
n.
intermittent)continuous or
F.7.
a.
413
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
Process wastewater flow rate. Indicate the average daily volume of process wastewater
discharge into the collection system in gallons per day (gpd) and whether the discharge is
continuous or intermittent.
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Cape Fear
gpd (continuous or X intermittent)
Non-process wastewater flow rate. Indicate the average daily volume of non-process
wastewater flow discharged into the collection system in gallons per day (gpd) and
whether the discharge is continuous or intermittent.
PART F, INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES
All treatment works receiving discharges from significant industrial users or which receive RCRA.CERCLA, or other remedial wastes must
complete part F.
GENERAL INFORMATION: S
F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages
as necessary.
F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's
discharge.
Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and
provide the information requested for each SIU.
gPd C
Pretreatment Standards. Indicate whether the SIU is subject to the following:
Local limits Yes | I No
b. Categorical pretreatment standards Yes I I No
If subject to categorical pretreatment standards, which category and subcategory?
F.l. Pretreatment program. Does the treatment works have, or is subject to an approved pretreatment program?
K Yes O No
F.2. Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (CIUs). Provide the number of each of the following types of
industrial users that discharge to the treatment works.
SUPPLEMENTAL APPLICATION INFORMATION
F.2.
Number of non-categorical SIUs.6o.
Number of CIUs.9P-
SIGNIFICANT INDUSTRIAL USER INFORMATION:
F.3.
Name:NC IDEA (MCNC)
Mailing Address: PO Box 12889
Research Triangle Park, NC 27709
F.4.Industrial Processes. Describe all the industrial processes that affect or contribute to the SID's discharge.
Semiconductor research and manufacturing
Principal product(s):Silicon wafers and other components related to semiconductor processing
F.6.
o.
56,030 continuous or
P-
intennittent)continuous or
F.7.
a.
b.
469.10
Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages
as necessary.
Process wastewater flow rate. Indicate the average daily volume of process wastewater
discharge into the collection system in gallons per day (gpd) and whether the discharge is
continuous or intermittent.
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Cape Fear
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
gpd (X continuous or intermittent)
Non-process wastewater flow rate. Indicate the average daily volume of non-process
wastewater flow discharged into the collection system in gallons per day (gpd) and
whether the discharge is continuous or intermittent.
F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SID’s
discharge.
Raw material(s): Wafers and various chemicals including acids, bases, solvents, and gases.
Flow Rate.
gpd C
Pretreatment Standards. Indicate whether the SIU is subject to the following:
Local limits M Yes I I No
Categorical pretreatment standards [3 Yes I I No
If subject to categorical pretreatment standards, which category and subcategory?
PART F, INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES
All treatment works receiving discharges from significant industrial users or which receive RCRA.CERCLA, or other remedial wastes must
complete part F.
GENERAL INFORMATION:
Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and
provide the information requested for each SIU.
F.1. Pretreatment program. Does the treatment works have, or is subject to an approved pretreatment program?
KI Yes No
Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (CIUs). Provide the number of each of the following types of
industrial users that discharge to the treatment works.
SUPPLEMENTAL APPLICATION INFORMATION
F.l.
Number of non-categorical SIUs.6q-
Number of CIUs.9r.
SIGNIFICANT INDUSTRIAL USER INFORMATION:
Name:Research Triangle Institute (RTI)
Mailing Address: PQ Box 12194
Research Triangle Park, NC 27709
F.4.Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge.
Conducts basic and applied research for clients. Principal areas include various sciences.
engineering, statistics, and survey research. Possible small amounts of chemical samples.
Principal product(s): Summary report of the results or methods developed.
F.6.
q.
73,160 X continuous or
intermittent)continuous or
F.7.
Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and
provide the information requested for each SIU.
.intermittent)
r.Non-process wastewater flow rate. Indicate the average daily volume of non-process wastewater
flow discharged into the collection system in gallons per day (gpd) and whether the
discharge is continuous or intermittent.
Process wastewater flow rate. Indicate the average daily volume of process wastewater
discharge into the collection system in gallons per day (gpd) and whether the discharge is
continuous or intermittent.
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Cape Fear
Raw material(s):Reagent chemicals and solvents depending on research. Usually less than 100 grams.
Flow Rate.
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
PART F. INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES
All treatment works receiving discharges from significant industrial users or which receive RCRA.CERCLA, or other remedial wastes must
complete part F.
--------------------gpd (.
Pretreatment Standards. Indicate whether the SIU is subject to the following:
a. Local limits Yes | | No
b. Categorical pretreatment standards Q Yes M No
If subject to categorical pretreatment standards, which category and subcategory?
F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's
discharge.
F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages
as necessary.
Pretreatment program. Does the treatment works have, or is subject to an approved pretreatment program?
K Yes No
F.2. Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (CIUs). Provide the number of each of the following types of
industrial users that discharge to the treatment works.
SUPPLEMENTAL APPLICATION INFORMATION
F.l.
Number of non-categorical SlUs.6s.
Number of CIUs.t.9
SIGNIFICANT INDUSTRIAL USER INFORMATION:
Name:SCM Metals
Mailing Address: PO Box 10166
Research Triangle Park. NC 27709
F.4.Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU’s discharge.
Principal product(s): Powdered Copper, Tin Powder. Brazing Paste, and Solder Paste.
F.6.
s.
14.496 continuous or
continuous or intermittent)
F.7.
a.
b.
471 J
Process wastewater flow rate. Indicate the average daily volume of process wastewater
discharge into the collection system in gallons per day (gpd) and whether the discharge is
continuous or intermittent.
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Cape Fear
Raw material(s): Copper and Tin and accompanying additives
Flow Rate.
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
gpd (X continuous or intermittent)
t.Non-process wastewater flow rate. Indicate the average daily volume of non-process wastewater
flow discharged into the collection system in gallons per day (gpd) and whether the
discharge is continuous or intermittent.
PART F. INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES
All treatment works receiving discharges from significant industrial users or which receive RCRA.CERCLA, or other remedial wastes must
complete part F.
gpd (.
Pretreatment Standards. Indicate whether the SIU is subject to the following:
Local limits Yes | | No
Categorical pretreatment standards [X] Yes O No
If subject to categorical pretreatment standards, which category and subcategory?
F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages
as necessary.
R&D and manufacturing of metal powders and brazing and solder pastes.
F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's
discharge.
Pretreatment program. Does the treatment works have, or is subject to an approved pretreatment program?
13 Yes Q No
F.2. Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (CIUs). Provide the number of each of the following types of
industrial users that discharge to the treatment works.
Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and
provide the information requested for each SIU.
SUPPLEMENTAL APPLICATION INFORMATION
F.2.
Number of non-categorical SIUs.6u.
Number of CIUs.9v.
SIGNIFICANT INDUSTRIAL USER INFORMATION:
Name:Sumitomo
Mailing Address: PO Box 13445
Research Triangle Park. NC 27709
F.4.Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU’s discharge.
Manufacture of fiber optic cable
Principal product(s): Fiber Optic Cable
F.6.
U.
13.825 continuous or
v.
continuous or intermittent)
F.7.
Process wastewater flow rate. Indicate the average daily volume of process wastewater
discharge into the collection system in gallons per day (gpd) and whether the discharge is
continuous or intermittent.
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Cape Fear
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
gpd (X continuous or intermittent)
Non-process wastewater flow rate. Indicate the average daily volume of non-process
wastewater flow discharged into the collection system in gallons per day (gpd) and
whether the discharge is continuous or intermittent.
PART F. INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES
All treatment works receiving discharges from significant industrial users or which receive RCRA,CERCLA, or other remedial wastes must
complete part F.
GENERAL INFORMATION: I
F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU’s
discharge.
F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages
as necessary.
Raw material(s): Plastics, acrylics, PVC. mineral oil based jelly and steel jacket tape.
Flow Rate.
gP1^ (.
Pretreatment Standards. Indicate whether the SIU is subject to the following:
a. Local limits Yes I I No
b. Categorical pretreatment standards Q Yes IXI No
If subject to categorical pretreatment standards, which category and subcategory?
Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and
provide the information requested for each SIU.
F.l. Pretreatment program. Does the treatment works have, or is subject to an approved pretreatment program?
KI Yes Q No
Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (CIUs). Provide the number of each of the following types of
industrial users that discharge to the treatment works.
SUPPLEMENTAL APPLICATION INFORMATION
PART F. INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES
F.2.
w. Number of non-categorical SIUs.6
Number of CIUs.9x.
SIGNIFICANT INDUSTRIAL USER INFORMATION:
Name:Litespec
Mailing Address: PO Box 13445
Research Triangle Park, NC 27709
F.4.Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge.
Permit owner certifies monthly that no process water is discharged.
Principal product(s): When active, optical fiber
Raw material(s): Silica&germanium tetrachloride, H, N, Ar, HF, He, Q. chlorine, tetra fluorocarbon
F.6.Flow Rate.
W.
0 continuous or
x.
continuous or intermittent) gpd C
F.7.
All treatment works receiving discharges from significant industrial users or which receive RCRA.CERCLA, or other remedial wastes must
complete part F.
GENERAL INFORMATION: ’ T
Process wastewater flow rate. Indicate the average daily volume of process wastewater
discharge into the collection system in gallons per day (gpd) and whether the discharge is
continuous or intermittent.
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Cape Fear
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
gpd (continuous or intermittent)
Non-process wastewater flow rate. Indicate the average daily volume of non-process
wastewater flow discharged into the collection system in gallons per day (gpd) and
whether the discharge is continuous or intermittent.
F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU’s
discharge.
F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages
as necessary.
Pretreatment Standards. Indicate whether the SIU is subject to the following:
a. Local limits Yes O No
b. Categorical pretreatment standards I I Yes M No
If subject to categorical pretreatment standards, which category and subcategory?
Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and
provide the information requested for each SIU.
F.1. Pretreatment program. Does the treatment works have, or is subject to an approved pretreatment program?
0 Yes No
Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (CIUs). Provide the number of each of the following types of
industrial users that discharge to the treatment works.
SUPPLEMENTAL APPLICATION INFORMATION
PART F. INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES
F.2.
y. Number of non-categorical SIUs.6
Number of CIUs.9z.
SIGNIFICANT INDUSTRIAL USER INFORMATION:
Name:Week Closure Systems
Mailing Address: PQ Box 12600
Research Triangle Park, NC 27709
F.4.Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU’s discharge.
Principal product(s): Hand held surgical instruments and disposable products
F.6.
y-
28,026 continuous or
z.
gpd (.intermittent)continuous or
F.7.
a.
b.
433
All treatment works receiving discharges from significant industrial users or which receive RCRA.CERCLA, or other remedial wastes must
complete part F.
<.i\ik\i i\i(>rxi \i k>\ ' '
Process wastewater flow rate. Indicate the average daily volume of process wastewater
discharge into the collection system in gallons per day (gpd) and whether the discharge is
continuous or intermittent.
RIVER BASIN:
Cape Fear
PERMIT ACTION REQUESTED:
Renewal
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
gpd (X continuous or intermittent)
Non-process wastewater flow rate. Indicate the average daily volume of non-process
wastewater flow discharged into the collection system in gallons per day (gpd) and
whether the discharge is continuous or intermittent.
F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages
as necessary.
Manufacture and repair hand held surgical instruments and disposable products.
F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU’s
discharge.
Raw material(s): Stainless steel, titanium, tantalum, and form plastic parts.
Flow Rate.
Pretreatment Standards. Indicate whether the SIU is subject to the following:
Local limits IXI Yes | I No
Categorical pretreatment standards Yes I I No
If subject to categorical pretreatment standards, which category and subcategory?
Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and
provide the information requested for each SIU.
F.1. Pretreatment program. Does the treatment works have, or is subject to an approved pretreatment program?
13 Yes Q No
Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (CIUs). Provide the number of each of the following types of
industrial users that discharge to the treatment works.
SUPPLEMENTAL APPLICATION INFORMATION
PART F. INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES
F.l.
aa. Number of non-categorical SIUs.6
bb. Number of CIUs.9
SIGNIFICANT INDUSTRIAL USER INFORMATION:
Name:Astro Pak
Mailing Address: 2410 Presidential Drive, Suite 114
Durham. NC 27703
F.4.Industrial Processes. Describe all the industrial processes that affect or contribute to the Sill's discharge.
Principal product(s): No products - cleaning and passivation of stainless steel equipment
Raw material(s): Various acids and bases used in cleaning - ie citric, ascorbic, and formic acids.
potassium hydroxide, hydrogen peroxide
F.6.Flow Rate.
aa.
continuous or X
bb.
intermittent)continuous or
F.7.
a.
433.17
Process wastewater flow rate. Indicate the average daily volume of process wastewater
discharge into the collection system in gallons per day (gpd) and whether the discharge is
continuous or intermittent.
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Cape Fear
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
Pretreatment program. Does the treatment works have, or is subject to an approved pretreatment program?
13 Yes | | No
F.2. Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (CIUs). Provide the number of each of the following types of
industrial users that discharge to the treatment works.
2100 per batch (continuous or X intermittent)
Non-process wastewater flow rate. Indicate the average daily volume of non-process
wastewater flow discharged into the collection system in gallons per day (gpd) and
whether the discharge is continuous or intermittent.
All treatment works receiving discharges from significant industrial users or which receive RCRA,CERCLA, or other remedial wastes must
complete part F.
Gl M R\L INFORMATIOV !
F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages
as necessary.
Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and
provide the information requested for each SIU.
Passivation and cleaning of stainless steel piping and equipment for the pharmaceutical industry
F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU’s
discharge.
gpd (■
Pretreatment Standards. Indicate whether the SIU is subject to the following:
Local limits 3 Yes I I No
b. Categorical pretreatment standards 3 Yes Q No
If subject to categorical pretreatment standards, which category and subcategory?
SUPPLEMENTAL APPLICATION INFORMATION
PART F. INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES
F.l.
cc. Number of non-categorical SIUs.6
dd. Number of CIUs.9
SIGNIFICANT INDUSTRIAL USER INFORMATION:
F.3.
Name:Town of Cary
Mailing Address: 400 James Jackson Avenue
Cary,NC 27513
Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge.F.4.
Principal product(s): Domestic and pharmaceutical wastewater
Raw material(s): N/A
F.6.Flow Rate.
CC.
continuous or 375,462
dd.
intermittent)continuous or gpd (.
F.7.
a.
Significant Industrial User information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages
as necessary.
Process wastewater flow rate. Indicate the average daily volume of process wastewater
discharge into the collection system in gallons per day (gpd) and whether the discharge is
continuous or intermittent.
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Cape Fear
FACILITY NAME AND PERMIT NUMBER:
Triangle WWTP, NC0026051
Pretreatment program. Does the treatment works have, or is subject to an approved pretreatment program?
13 Yes No
F.2. Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (CIUs). Provide the number of each of the following types of
industrial users that discharge to the treatment works.
gpd (X continuous or intermittent)
Non-process wastewater flow rate. Indicate the average daily volume of non-process
wastewater flow discharged into the collection system in gallons per day (gpd) and
whether the discharge is continuous or intermittent.
All treatment works receiving discharges from significant industrial users or which receive RCRA,CERCLA, or other remedial wastes must
complete part F.
GF.NLRAI INFORMA i l<>\: 1
Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and
provide the information requested for each SIU.
Town of Cary discharge that contains 2 pharmaceutical industries and domestic flow.
F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU’s
discharge.
Pretreatment Standards. Indicate whether the SIU is subject to the following:
Local limits Yes I I No
b. Categorical pretreatment standards O Yes 13 No
If subject to categorical pretreatment standards, which category and subcategory?
FACILITY NAME AND PERMIT NUMBER:PERMIT ACTION REQUESTED:RIVER BASIN:
SUPPLEMENTAL APPLICATION INFORMATION
PART G. COMBINED SEWER SYSTEMS
If the treatment works has a combined sewer system, complete Part G.
a.
b.
c.
a.
b.
c.
d.
e.
CSO OUTFALLS:
Complete questions G.3 through G.6 once for each CSO discharge point.
G.3. Description of Outfall.
Outfall numbera.
b.Location
(City or town, if applicable)(Zip Code)
(County)(State)
(Latitude)(Longitude)
Distance from shore (if applicable)ft.c.
Depth below surface (if applicable)d.ft.
Which of the following were monitored during the last year for this CSO?e.
Rainfall CSO pollutant concentrations CSO frequency
CSO flow volume Receiving water quality
f.How many storm events were monitored during the last year?
G.4.CSO Events.
Give the number of CSO events in the last year.a.
events (□ actual or approx.)
b.Give the average duration per CSO event.
(□ actual or approx.)hours
Page 20 of 22EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
G.2. System Diagram. Provide a diagram, either in the map provided in G.1 or on a separate drawing, of the combined sewer collection system that
includes the following information.
Location of major sewer trunk lines, both combined and separate sanitary.
Locations of points where separate sanitary sewers feed into the combined sewer system.
Locations of in-line and off-line storage structures.
Locations of flow-regulating devices.
Locations of pump stations.
G.1. System Map. Provide a map indicating the following: (may be included with Basic Application Information)
All CSO discharge points.
Sensitive use areas potentially affected by CSOs (e.g., beaches, drinking water supplies, shellfish beds, sensitive aquatic ecosystems, and
outstanding natural resource waters).
Waters that support threatened and endangered species potentially affected by CSOs.
FACILITY NAME AND PERMIT NUMBER:PERMIT ACTION REQUESTED:RIVER BASIN:
c.
d.
G.5. Description of Receiving Waters.
Name of receiving water:a.
b.Name of watershed/river/stream system:
United State Soil Conservation Service 14-digit watershed code (if known):
Name of State Management/River Basin:c.
United States Geological Survey 8-digit hydrologic cataloging unit code (if known):
Page 21 of 22ERA Form 3510-2A (Rev. 1-99). Replaces ERA forms 7550-6 & 7550-22.
END OF PART G.
REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS
OF FORM 2A YOU MUST COMPLETE.
Give the minimum rainfall that caused a CSO event in the last year
Inches of rainfall
Give the average volume per CSO event.
million gallons (□ actual or approx.)
G.6. CSO Operations.
Describe any known water quality impacts on the receiving water caused by this CSO (e.g., permanent or intermittent beach closings, permanent or
intermittent shell fish bed closings, fish kills, fish advisories, other recreational loss, or violation of any applicable State water quality standard).
Additional information, if provided, will appear on the following pages.
NPDES FORM 2A Additional Information
2/28/05
Date Sample Rcvd:2/9/05
Meritech Work Order #020905107 Sample: 05020802 Composite 2/8/05
Parameters Result Analysis Date Reporting Limit Method
Contact:
Client:
Tyrone Battle
Woodard & Curran
5926 NC Hwy 55
East Durham, NC 27“ 13
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
2/16/05
2/10/05
2/16/05
2/11/05
2/11/05
2/11/05
2/11/05
2/11/05
2/11/05
2/11/05
2/11/05
2/11/05
2/11/05
2/11/05
2/11/05
2/11/05
2/11/05
2/16/05
2/15/05
2/17/05
EPA 410.4
EPA 160.1
SM 4500FC
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 420.1
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
COD
Total Dissolved Solids
Fluoride
Aluminum, total
Antimony, total
Arsenic, total
Beryllium, total
Cadmium, total
Chromium, total
Copper, total
Lead, total
Molybdenum, total
Nickel, total
Selenium, total
Silver, total
Thallium, total
Zinc, total
Hardness, total
Phenol, total
EPA Method 625
Page 1 of 2
Report Date:
15 mg/1
10 mg/1
0.1 mg/1
0.050 mg/1
0.025 mg/1
0.010 mg/1
0.005 mg/1
0.002 mg/1
0.005 mg/1
0.002 mg/1
0.010 mg/1
0.005 mg/1
0.010 mg/1
0.010 mg/1
0.005 mg/1
0.020 mg/1
0.010 mg/1
0.662 mg eq CaCO3/l
0.010 mg/1
22 mg/1
317 mg/1
1.2 mg/1
< 0.050 mg/1
< 0.025 mg/1
< 0.010 mg/1
< 0.005 mg/1
< 0.002 mg/1
< 0.005 mg/1
0.005 mg/1
< 0.010 mg/1
0.051 mg/1
< 0.010 mg/1
< 0.010 mg/1
< 0.005 mg/1
< 0.020 mg/1
0.092 mg/1
76.2 mg eq CaCO3/l
0.015 mg/1
attached
2/28/05
Date Sample Rcvd:2/9/05
Meritech Work Order #020905108 Sample: 05020802 Composite 2/8/05
Parameters Result Analysis Date Reporting Limit Method
these data.
Contact:
Client:
2/16/05
2/18/05
2/19/05
2/17/05
EPA 413.1
EPA 335.2
Tyrone Bartie
Woodard & Curran
5926 NC Hw\- 55
East Durham, NC 27713
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
< 5 mg/1
< 0.005 mg/1
attached
attached
Oil & Grease
Cyanide, total
EPA Method 6230D
EPA 624+Acrolein+AcryEnitrile
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
5 mg/1
0.005 mg/1
I hereby certify' that 1 have reviewed and approve
Page 2 of 2
Report Date:
/ 7
Laboratory Representative
I
NPDES#
Client )Tel /
PO #
Attention j \t i f i ....Project# r ! r'\
Dalt?
(.) ■XI
(r-tj- (>(
-1XC/I < ■>
c I-
I
V
—i—
Comments:Method ol Shipment
-A*
| ] UPS
\(>□Fed Ex Relinquished by Dale Time I ii ne
[ I Hand Delivery X
Relinquished by Time Date 1 ime
L ] Other
Relinquished by Date Time Received al lab by Date I une
I une
I
ill these results be used tor fej'tilalor) purposes? \ cs
Received by
-"'Received byDale
« o(
Coots
'J u r/;
i
1
pH
OK?
Chlorine
OK?
MERITECH, Inc.
642 Tamco Road
Reidsville, NC 27320
tel. [phone]
fax. [phone]
T une
2
C’
G?
□
Dale
Lab Use Only
Iced?
Temp?
If Composite?
Date
2
Chain of Custody Record
Sample
LocatioiVIDW
Address /'( -I . 7
72l. X6-
(I c {'i.ru'i
y, J / —■
( (;/} ___________
,V A/ ■ A
r‘-
Person Taking Sample (Signature) / t ■ j.
Tests Required
A A ? A j ________
\/ v ./ s/ V
/•7,4 /J?'. AfZ' AI A? C'/.Ci ,(
Fax ' ■ • ‘/ ./ ''■;
I hereby certify' that I have reviewed and approve these data.
Laboratory Representative
Meritech ID#:
Analysis:
Analyst:
< 50.0 ug/L
< 10.0 ug/L
020905108TB
02/17/05
CAH
642 Tamco Road * Reidsville, NC 27320
[phone] Ph * [phone] Fax
MERITECH, INC.
Environmental Laboratories
A Division of Water Technology and Controls, Inc.
Parameter
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon Tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,2-Dibromoethane
1.1- Dichloroethane
1.2- Dichloroethane
1,4-Dichlorobenzene
1.2- Dichlorobenzene
1.3- Dichlorobenzene
1.1- Dichloroethene
trans-1,2-Dichloroethene
1.2- Dichloropropane
cis-l,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethyl benzene
Methylene chloride
1.1.2.2- Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1 -Trichloroethane
1.1.2- T richloroethane
Trichloroethene
Trichloro fluoromethane
Vinyl chloride
Additional Compounds
Acrolein
Acrylonitrile
EPA 624 VOLATILE ORGANICS
Result
<1.00 ug/L
< 1.00 ug/L
<1.00 ug/L
< 5.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 5.00 ug/L
< 5.00 ug/L
< 1.00 ug/L
< 5.00 ug/L
<1.00 ug/L
< 1.00 ug/L
<1.00 ug/L
<1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
<1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
<1.00 ug/L
< 1.00 ug/L
<1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
<1.00 ug/L
<5.00 ug/L
< 5.00 ug/L
Client: Woodard & Curran
Project: PPA
Client Sample ID: Trip Blank
Sample Collection: 02/08/05
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
Meritech ID#:
Analysis:
Analyst:
< 50.0 ug/L
< 10.0 ug/L
020905108
02/17/05
CAH
MERITECH, INC.
Environmental Laboratories
A Division of Water Technology and Controls, Inc.
Parameter
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon Tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,2-Dibromoethane
1.1- Dichloroethane
1.2- Dichloroethane
1,4-Dichlorobenzene
1.2- Dichlorobenzene
1.3- Dichlorobenzene
1.1- Dichloroethene
trans-1,2-Dichloroethene
1.2- Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-DichIoropropene
Ethyl benzene
Methylene chloride
1.1.2.2- Tetrachloroethane
Tetrachloroethene
Toluene
1.1.1- Trichloroethane
1.1.2- Trichloroethane
Trichloroethene
T richlorofluoromethane
Vinyl chloride
Additional Compounds
Acrolein
Acrylonitrile
EPA 624 VOLATILE ORGANICS
Result
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 5.00 ug/L
< 1.00 ug/L
<1.00 ug/L
<5.00 ug/L
< 5.00 ug/L
1.02 ug/L
< 5.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 5.00 ug/L
< 5.00 ug/L
Client: Woodard & Curran
Project: PPA
Client Sample ID: 05020803
Sample Collection: 02/08/05
642 Tamco Road * Reidsville, NC 27320
[phone] Ph * [phone] Fax
A Division of Water Technology and Controls, Inc.
EPA 625 SEMIVOLATILE ORGANICS
Parameter ResultResultParameter
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
Acenaphthene
Acenaphthylene
Anthracene
Benzidine
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Benzyl butyl phthalate
Bis(2-chloroethoxy)methane
Bis(2-chloroethyl)ether
Bis(2-chloroisopropyl)ether
Bis(2-ethylhexyl) phthalate
4-Bromophenyl phenyl ether
2-Chloronaphthalene
4-Chlorophenyl phenyl ether
Chrysene
Dibenzo(a,h)anthracene
1.2- Dichlorobenzene
1.3- Dichlorobenzene
1.4- Dichlorobenzene
3,3'-Dichlorobenzidine
Diethyl phthalate
Dimethyl phthalate
Di-n-butyl phthalate
2.4- Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octyl phthalate
1,2-Diphenylhydrazine
Client:
Project:
Client Sample ID:
Sample Collection:
4-Chloro-3-methylphenol
2-Chlorophenol
2.4- Dichlorophenol
2.4- Dimethylphenol
2.4- Dinitrophenol
4.6- Dinitro-2-methylphenol
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol
Phenol
2.4.6- Trichlorophenol
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
lndeno(l ,2,3-cd)pyrene
Isophorone
2-Methylnapthalene
Naphthalene
Nitrobenzene
N-Nitrosodimethylamine
N-Nitrosodi-n-propylamine
N-Nitrosodiphenylamine
Phenanthrene
Pyrene
1,2,4-TrichIorobenzene
Meritech ID#:
Analysis:
Extraction:
Analyst:
Dilution Factor:
<10 ug/L
< 10 ug/L
<10 ug/L
< 10 ug/L
<50 ug/L
<50 ug/L
< 10 ug/L
<50 ug/L
< 50 ug/L
< 10 ug/L
< 10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<50 ug/L
< 10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
< 10 ug/L
< 10 ug/L
<10 ug/L
Woodard & Curran
PPA
05020802
02/08/05
<10 ug/L
< 10 ug/L
< 10 ug/L
<50 ug/L
< 10 ug/L
<10 ug/L
< 10 ug/L
<10 ug/L
<10 ug/L
< 10 ug/L
< 10 ug/L
<10 ug/L
<10 ug/L
23.9 ug/L
<10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
< 10 ug/L
<10 ug/L
<10 ug/L
<50 ug/L
<10 ug/L
<10 ug/L
< 10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
020905107
02/17/05
02/14/05
CAH
1
642 Tamco Road * Reidsville, NC 27320
[phone] Ph * [phone] Fax
MERITECH, INC.
Environmental Laboratories
II
ERA 6230D - VOLATILE ANALYSIS
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
020905107
02/19/05
ESC
MERITECH, INC.
ENVIRONMENTAL LABORATORIES
A Division of Water Technology and Controls, Inc.
Parameter
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon Tetrachloride
Chlorobenzene
Chiorodibromomethane
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-ChlorotoIuene
1.2- Dibromo-3-chloropropane
1.2- Dichlorobenzene
1.3- Dichlorobenzene
1.4- Dichlorobenzene
Dichlorodifluoromethane
1.1- Dichloroethane
1.2- Dichloroethane
1,1 -Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1.2- DichIoropropane
1.3- Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Di-isopropyl ether
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
p-Isopropyltoluene
Methylene chloride
Methyl tert-butyl ether
Naphthalene
Result
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<5.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<5.0 ug/L
<5.0 ug/L
<5.0 ug/L
Result
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<5.0 ug/L
<1.0 ug/L
<3.0 ug/L
Client:
Project:
Client Sample ID: 05020803
Sample Collection: 02/08/05
Meritech ID#:
Analysis:
Analyst:
Parameter
n-Propylbenzene
Styrene
1.1.1.2- Tetrachioroethane
1.1.2.2- Tetrachloroethane
1.2.3- Trichlorobenzene
1.2.4- Trichlorobenzene
1,1,1 -Trichloroethane
1.1.2- Trichloroethane
Trichloroethene
Trichloroflouromethane
1.2.3- Trichloropropane
1.2.4- T rimethylbenzene
1.3.5- Trimethylbenzene
Toluene
Vinyl chloride
Xylenes, total
Woodard & Curran
PPA
642 Tamco Road * Reidsville, NC 27320
[phone] Ph * [phone] Fax
5/26/05
5/6/05Dare Sample Rcvd:
Meritech Work Order it 05060561 Sample: 05050602 Composite 5/5-6/05
Parameters Result Analysis Date Reporting Limit Method
Contact:
Client:
Tyrone Battle
Woodard & Curran
5926 NC Hw 55
East Durham. \C 2“~13
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
5/10/05
5/10/05
5/11/05
5/11/05
5/11/05
5/11/05
5/11/05
5/11/05
5/11/05
5/11/05
5/11/05
5/11/05
5/11/05
5/11/05
5/11/05
5/11/05
5/11/05
5/10/05
5/17/05
COD
Total Dissolved Solids
Fluoride
Aluminum, total
Antimony, total
Arsenic, total
Beryllium, total
Cadmium, total
Chromium, total
Copper, total
Lead, total
Molybdenum, total
Nickel, total
Selenium, total
Silver, total
Thallium, total
Zinc, total
Hardness, total
EPA Method 625
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
15 mg/1
10 mg/1
0.1 mg/1
0.050 mg/1
0.025 mg/1
0.010 mg/1
0.005 mg/1
0.002 mg/1
0.005 mg/1
0.002 mg/1
0.010 mg/1
0.005 mg/1
0.010 mg/1
0.010 mg/1
0.005 mg/1
0.020 mg/1
0.010 mg/1
0.662 mg eq CaCO3/l
EPA 410.4
EPA 160.1
SM 4500FC
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
Page 1 of 2
Report Date:
35 mg/1
420 mg/1
0.9 mg/1
0.309 mg/1
< 0.025 mg/1
< 0.010 mg/1
< 0.005 mg/1
< 0.002 mg/1
< 0.005 mg/1
0.011 mg/1
< 0.010 mg/1
0.043 mg/1
< 0.010 mg/1
< 0.010 mg/1
< 0.005 mg/1
< 0.020 mg/1
0.248 mg/1
77.3 mg eq CaCO3/l
attached
5/26/05
Dare Sample Rcvd:5/6/05
Meritech Work Order #05060562 Sample: 05050603 Grab 5/6/05
Parameters Result Analysis Date Reporting Limit Method
these data.
Contact:
Client:
Tyrone Battle
Woodard & Curran
5926 NC H\xy 55
East Durham, XC 27713
5/12/05
5/9/05
5/10/05
5/19/05
5/16/05
EPA 335.2
EPA 413.1
EPA 420.1
Cyanide, total
Oil & Grease
Phenol, total
EPA Method 6230D
EPA 624
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
0.005 mg/1
5 mg/1
0.010 mg/1
I hereby certify that I have reviewed and approve
Page 2 of 2
Report Date:
< 0.005 mg/1
< 5 mg/1
0.020 mg/1
attached
attached
Laboratory Representative
NPDES#
Client Tel
Fax
P.O #
Project #Attention:
If Composite?
Tests Required
2
2J
C'3 1121
1
/
Comments:
Lj Hand Delivery
Relinquished by:
Relinquished by Date'Time Date:Time.
lifiii...
Date
L
/
3E
Method of Shipment:
□ UPS
Q Fed Ex
# of
Cents.
PH: 336-342-4748
FAX: [phone]
EMAIL: [e-mail]
Date
2
Received at lab by:
Date:
Date:
Time
1
//>()
pH OK?
Cl 2 OKV
/yew 3-1,()g/
(W)52<2^3/
Will these results be used for regulatory purposes? Yes
Relinquished by:<7Date: / / Time:
Time:
Time
/ Tw
Time:
Add fess 1^0/227//-
'NrOAa- -_________
Person Taking Sample (Signature):
Tf^cztc Rnniiimrl
I of rA
Time
2
17
Lab Use Only
On
Ice?
/ 7Date / /
b/7/QS
Date- 7
Comp?
Grab?
7 D •
CU Other
22..
c.. t
di: ,
^4 o /zrM' C^r^-
//
^<2
642 Tamco Rd
Reidsville, NC
27320
MERITECH, INC.
ENVIRONMENTAL LABORATORIES
A Divtvon of Wutf't Technology and Controls, Inc
3
xZ
&■
J
/05/
277>D
77)-^ F /
(77_________
(T-rcd s________
Q] f 7t&05-/- '
I No_______I I_________
Revived by:
Received by:
Chain of Custody Record (COC)
Sample
Location/ID#
EPA 625 SEMIVOLATILE ORGANICS
Parameter Result Parameter Result
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
Acenaphthene
Acenaphthylene
Anthracene
Benzidine
Benzo(a)anthracene
Benzo(a)pyrene
3,4-Benzofluoroanthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Butyl benzyl phthalate
Bis(2-chloroethoxy)methane
Bis(2-chloroethyl)ether
Bis(2-chloroisopropyl)ether
Bis(2-ethylhexyl)phthalate
4-Bromophenyl phenyl ether
2-Chloronaphthalene
4-Chlorophenyl phenyl ether
Chrysene
Dibenzo(a,h)anthracene
1.2- DichIorobenzene
1.3- Dichlorobenzene
1.4- Dichlorobenzene
3,3'-Dichlorobenzidine
Diethyl phthalate
Dimethyl phthalate
Di-n-butyl phthalate
2.4- Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octyl phthalate
1,2-Diphenylhydrazine
Client:
Project:
Client Sample ID:
Sample Collection:
<10 ug/L
<10 ug/L
<10 ug/L
<50 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
< 10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
< 10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<50 ug/L
< 10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
< 10 ug/L
<10 ug/L
p-chloro-m-cresol
2-Chlorophenol
2.4- Dichlorophenol
2.4- Dimethylphenol
2.4- Dinitrophenol
4.6- Dinitro-o-cresol
2-NitrophenoI
4-Nitrophenol
Pentachlorophenol
Phenol
2.4.6- Trichlorophenol
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(l ,2,3-cd)pyrene
Isophorone
2-Methylnapthalene
Naphthalene
Nitrobenzene
N-Nitrosodimethylamine
N-Nitrosodi-n-propylamine
N-Nitrosodiphenylamine
Phenanthrene
Pyrene
1,2,4-Trichlorobenzene
Meritech ID#:
Analysis:
Extraction:
Analyst:
Dilution Factor:
05060561
05/17/05
05/09/05
CAH
1
<10 ug/L
<10 ug/L
< 10 ug/L
< 10 ug/L
<50 ug/L
< 10 ug/L
< 10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
< 10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
< 10 ug/L
< 50 ug/L
< 50 ug/L
<10 ug/L
<50 ug/L
<50 ug/L
< 10 ug/L
<10 ug/L
Woodard & Curran
NPDES PPA
05050602
05/05-06/05
MERITECH, INC.
Environmental Laboratories
A Division of Water Technology and Controls, Inc.
642 Tamco Road * Reidsville, NC 27320
[phone] Ph * [phone] Fax
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
< 50.0 ug/L
< 10.0 ug/L
05060562
05/16/05
CAH
642 Tamco Road * Reidsville, NC 27320
[phone] Ph * [phone] Fax
MERITECH, INC.
Environmental Laboratories
A Division of Water Technology and Controls, Inc.
Parameter
Benzene
Dichlorobromomethane
Bromoform
Methyl Bromide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Methyl Chloride
Chlorodibromomethane
1,2-Dibromoethane
1.1- Dichloroethane
1.2- Dichloroethane
1,4-Dichlorobenzene
1.2- Dichlorobenzene
1.3- Dichlorobenzene
1.1- Dichloroethylene
trans-1,2-Dichloroethylene
1.2- Dichloropropane
cis-1,3-Dichloropropylene
trans-1,3-Dichloropropylene
Ethyl benzene
Methylene chloride
1.1.2.2- Tetrachloroethane
Tetrachloroethylene
Toluene
1,1,1 -Trichloroethane
1.1.2- Trichloroethane
Trichloroethylene
T richlorofluoromethane
Vinyl chloride
Additional Compounds
Acrolein
Acrylonitrile
Meritech ID#:
Analysis:
Analyst:
Dilution Factor: 1
EPA 624 VOLATILE ORGANICS
Result
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
<5.00 ug/L
< 1.00 ug/L
<1.00 ug/L
< 5.00 ug/L
<5.00 ug/L
<1.00 ug/L
< 5.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
<1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
<1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 1.00 ug/L
< 5.00 ug/L
< 5.00 ug/L
Client: Woodard & Curran
Project: NPDES PPA
Client Sample ID: 05050503
Sample Collection: 05/06/05
EPA 6230D - VOLATILE ANALYSIS
A
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
05060562
05/19/05
ESC
MERITECH, INC.
ENVIRONMENTAL LABORATORIES
A Division of Water Technology and Controls. Inc
Parameter
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon Tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1.2- Dibromo-3-chloropropane
1.2- Dichlorobenzene
1.3- Dichlorobenzene
1.4- Dichlorobenzene
Dichlorodifluoromethane
1.1- Dichloroethane
1.2- Dichloroethane
1.1- Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1.2- Dichloropropane
1.3- Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Di-isopropyl ether
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
p-lsopropyltoluene
Methylene chloride
Methyl tert-butyl ether
Naphthalene
Result
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<5.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<5.0 ug/L
<5.0 ug/L
<5.0 ug/L
Result
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<1.0 ug/L
<5.0 ug/L
<1.0 ug/L
<3.0 ug/L
Parameter
n-Propylbenzene
Styrene
1.1.1.2- Tetrachloroethane
1.1.2.2- T etrachloroethane
1.2.3- Trichlorobenzene
1.2.4- Trichlorobenzene
1.1.1- Trichloroethane
1.1.2- Trichloroethane
Trichloroethene
Trichloroflouromethane
1.2.3- Trichloropropane
1.2.4- Trimethylbenzene
1.3.5- Trimethylbenzene
Toluene
Vinyl chloride
Xylenes, total
Meritech ID#:
Analysis:
Analyst:
Client: Woodard & Curran
Project: 6230D
Client Sample ID: 05050602
Sample Collection: 05/05/05
642 Tamco Road * Reidsville, NC 27320
[phone] Ph * [phone] Fax
Page 1 of 4
Laboratory Report
Work Order #:0508-00396
TR8827
Test Performed Method Results Qualifier
Test Performed Method Results Qualifier
No.
002
No.
001
Sample ID
Effluent
Sample ID
Effluent
- Prepared for —
Tyrone Battle
HMS/Triangle WWTP
5926 NC Hwy 55 East
Durham, NC 27713
ERA 624
EPA 624
ERA 624
EPA 624
EPA 624
EPA 624
EPA 624
EPA 624
EPA 335.2/335.3
EPA 420.1
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
Time Sampled
10:40
Time Sampled
10:20
<0.005 mg/L
<0.005# mg/L
20.1 mg/L
5.74 mg/L
73.8 mg/L
Cust. Code:
Cust. P.O.#:
Report Date:
Date Received:
NC/WW Cert. #: 067
NC/DW Cert. #: 37731
Sample Type
Grab
Sample Type
Composite
8/31/2005
8/9/2005
8/15/05
8/19/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/12/05
8/12/05
8/12/05
8/12/05
8/12/05
8/12/05
8/12/05
8/12/05
8/12/05
8/12/05
8/12/05
8/12/05
8/12/05
8/17/05
8/17/05
8/17/05
13:10
8:59
12:34
12:34
12:34
12:34
12:34
12:34
12:34
12:34
12:34
12:13
12:13
12:13
12:13
12:13
12:13
12:13
12:48
12:13
12:13
12:13
12:13
12:13
0:00
10:09
10:09
10:09
Condition
4 +/- 2 deg C
Condition
4+/- 2 deg C
Cyanide
Phenols w/chloroform extr.
Volatile TTOs by GC/MS
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Telephone: [phone]
Fax: [phone]
6701 Conference Drive
Raleigh, NC 27607
Date Sampled
8/8/2005
Date Sampled
8/9/2005
<50 ug/L
<50 ug/L
<5 ug/L
<5 ug/L
<5 ug/L
<10 ug/L
<5 ug/L
<5 ug/L
<0.003 mg/L
<0.005 mg/L
<0.002 mg/L
<0.005 mg/L
<0.010 mg/L
<0.010 mg/L
<0.005 mg/L
<0.2 ug/L
<0.010 mg/L
0.002 mg/L
<0.010 mg/L
<0.001 mg/L
0.075 mg/L
Matrix
WW
Antimony
Arsenic
Beryllium
Cadmium
Chromium
Copper
Lead
Mercury
Nickel
Selenium
Silver
Thallium
Zinc
TOTAL HARDNESS (WW)
Calcium
Magnesium
Total Hardness Calculation
Matrix
WW
o
o
WTEST
Analyzed
Date Time
Analyzed
Date Time
Project No.: 01
Project ID: Expanded Effluent Testing
Page 2 of 4
Laboratory Report
Work Order#: 0508-00396
Test Performed Method Results Qualifier
No.
002
Telephone: [phone]
Fax: [phone]
Sample ID
Effluent
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 624
EPA 624
EPA 624
EPA 624
EPA 624
EPA 624
EPA 624
EPA 624
EPA 624
EPA 624
EPA 624
EPA 624
EPA 624
EPA 624
EPA 624
EPA 624
EPA 624
EPA 624
EPA 624
EPA 624
EPA 624
Time Sampled
10:40
<10 ug/L
<10 ug/L
<10 ug/L
<50 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
Sample Type
Grab
NC/WW Cert. #: 067
NC/DW Cert. #: 37731
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
12:34
12:34
12:34
12:34
12:34
12:34
12:34
12:34
12:34
12:34
12:34
12:34
12:34
12:34
12:34
12:34
12:34
12:34
12:34
12:34
12:34
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1.1- Dichloroethane
1.2- Dichloroethane
1.1- Dichloroethene
trans-1,2-Dichloroethene
1.2- Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Methylene chloride
1.1.2.2- Tetrachloroethane
Tetrachloroethene
Toluene
1.1.1- Trichloroethane
1.1.2- Trichloroethane
Trichloroethene
Vinyl chloride
Semivolatile TTOs by 625
Acenaphthylene
Acenaphthene
Anthracene
Benzidine
Benzo(a)anthracene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
Benzo(g,h,i)perylene
Benzyl butyl phthalate
Bis(2-chloroethyl)ether
Bis(2-chloroethoxy)methane
Bis(2-chloroisopropyl)ether
Bis(2-ethylhexyl)phthalate
4-Bromophenyl phenyl ether
2-Chloronaphthalene
4-Chloro-3-methyl phenol
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Dibenzo(a,h)anthracene
Date Sampled
8/8/2005
3909 Beryl Road
Raleigh, NC 27607
<5 ug/L
<10 ug/L
<5 ug/L
<5 ug/L
<5 ug/L
<5 ug/L
<5 ug/L
<5 ug/L
<5 ug/L
<5 ug/L
<5 ug/L
<5 ug/L
<5 ug/L
<5 ug/L
<5 ug/L
<5 ug/L
<5 ug/L
<10 ug/L
<5 ug/L
<5 ug/L
<5 ug/L
Matrix
WW
Condition
4 +/- 2 deg C
o
o
TOoTEST
Analyzed
Date Time
Page 3 of 4
Laboratory Report
Work Order #:0508-00396
Test Performed Method Results Qualifier
No.
002
Telephone: [phone]
Fax: [phone]
Sample ID
Effluent
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
EPA 625
Time Sampled
10:40
Sample Type
Grab
NC/WW Cert. #: 067
NC/DW Cert. #: 37731
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
8/16/05
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
11:00
Condition
4 +/- 2 deg C
Di-n-butyl phthalate
3,3'-Dichlorobenzidine
1.2- Dichlorobenzene
1.3- Dichlorobenzene
1.4- Dichlorobenzene
2.4- Dichlorophenol
Diethyl phthalate
2.4- Dimethylphenol
Dimethyl phthalate
2.4- Dinitrophenol
2.4- Dinitrotoluene
2.6- Dinitrotoluene
Di-n-octyl phthalate
1,2-Diphenylhydrazine
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
lndeno(1,2,3-c,d)pyrene
Isophorone
2-Methyl-4,6-dinitrophenol
Naphthalene
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodi methylamine
N-Nitrosodiphenylamine
N-Nitrosodi-n-propylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1.2.4- Trichlorobenzene
2.4.6- Trichlorophenol
Extraction, 625 (A&B/N)
Date Sampled
8/8/2005
3909 Beryl Road
Raleigh, NC 27607
<10 ug/L
<20 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<50 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<50 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<20 ug/L
<20 ug/L
<30 ug/L
<10 ug/L
<10 ug/L
<10 ug/L
<20 ug/L
<10 ug/L
DONE
Matrix
WW
G
O
TMoTEST
#ANALYZED BY OXFORD LABORATORIES, INC., WILMINGTON, NC (NC/WW
CERT. #75; NC/DW CERT. #37721).
Analyzed
Date Time
Page 4 of 4
Laboratory Report
Work Order #:0508-00396
Reviewed by:
for Tritest, Inc.
NC/WWCert. #: 067
NC/DW Cert. #: 37731
Telephone: [phone]
Fax: [phone]
3909 Beryl Road
Raleigh, NC 27607
o
o
TOdTEST
Page 1 of 1
Laboratory Report
Work Order #:0508-55683
TRITES
Method Results Qualifier
SM 510 A-B <.005 mg/L 8:59
t
Reviewed by:
for Oxford Laboratory
Telephone: [phone]
Fax: [phone]
www.oxfordlaboratory.com
Sample ID
508-00396-002
Oust. Code:
Cust. P.O.#:
Report Date:
Date Received:
Sample Type
Grab
NC/WW Cert. #: 075
NC/DW Cert. #: 37721
8/19/2005
8/10/2005
Condition
4 +/- 2 deg C
No.
001 Date Sampled
8/8/2005
Time Sampled
10:40
Matrix
WW
— Prepared for —
Maryanne Sims
Tritest, Inc.
PO Box 33190
6701 Conference Drive
Raleigh, NC 27636
Test Performed
Phenol
Oxford Laboratory
1316 S. Fifth Street
Wilmington, NC 28401
Project No.: 001
Project ID: 508-00396-002
Analyzed
Date Time
8/19/05
Page 1 of 10508-00396Tritest W.O.
Chain of Custody
Bill Results To:
Expanded Effluent TestingProject Reference:
01
Sampled By:
Attn: Tyrone Battle
Fax: [phone]
Analysis RequestedStart Date
Sample Description
Smp #Start Time
001WWCEffluent
002'WGEffluent
?!TESl PICKUP
Received by (signature)Relinquished by (signatun
C
□ 4+2 C
[>j Temp:
Composite
or Grab
Antimony, Arsenic, Beryllium, Cadmium, Chromium, Copper, Lead,
Mercury, Nickel, Selenium, Silver, Thallium, Zinc, TOTAL HARDNESS
(WW), Calcium, Magnesium, Total Hardness Calculation, Metals Prep
Cyanide, Phenols w/chloroform extr., Volatile TTOs by GC/MS,
Semivolatile TTOs by 625, Extraction, 625 (A&B/N)
Report Results To:
HMS / Triangle WWTP
5926 NC Hwy 55 East
Durham, NC 27713
Triangle WWTP
5926 NC Hwy 55 East
Durham, NC 27713
O Standard Report Delivery
| | Rush Report Delivery (w/ surcharge)
Note: Rush projects are subject to prior approval by Lab
Requested Due Date:
Matrix
WW,DW,
SW, GW etc.
AW
c* tfifOtest
6701 Conference Drive, Raleigh, NC 27607
ph: [phone] fax: [phone]
NCWW Cert #67, NCDW Cert # 37731
Project Number:
Purchase Order #:
Stop Date
Stop Time
'2/t/o5
Date
Date
- O A
Date
Time
Time
I 4 US
Time
RelinquisRecTby (signature)
Relinquished by (signature
Received by-fsi^n^ture)
Received by (signature)
Attn: Tyrone Battle
Phone: [phone]
For Lab Use Only:
Temperatue at receipt:
SAMPLE PRESERVATION CHECK-IN SHEET
WO#:
CD TTS GC UPS
.Analysis Requested
Container Chlorine None HCL H2SO4 Na OH Thio OTHER
^/G ^/G None HCL/H2SO4 NaOH Thio OTHER
c/g None HCL HN03 OTHERThio<Na<
C/G Pos / neg None HCL HNO'3 NaOH Thio OTHER
C/G Pos / neg <HCL)None HN03 NaOH Thio OTHER
C/C^Pos / neg.None HCL H2SO4 HN03 NaOH othe;
C/G P/G Pos / neg None HCL H2SO4 HN03 NaOH Thio OTHER
C/G P/G Pos / neg None HCL H2SO4 HN03 NaOH Thio OTHER
C/G-P/G Pcs / neg None HCL H2SO4 HN03 NaOH Thio OTHER
C/G P/G Pos / neg None HCL H2SO4 HN03 NaOH Thio OTHER
C/G P/G Pos / neg None HCL H2SO4 HN03 NaOH Thio OTHER
C/G P/G Pos/neg None HCL H2SO4 HN03 ThioNaOH OTHER
C/G P/G Pos / neg None HCL H2SO4 HN03 NaOH Thio OTHER
C/G P/G Pos / neg None HCL H2SO4 HN03 NaOH Thio OTHER
C/G P/G Pos / neg None HCL H2SO4 HN03 NaOH Thio OTHER
C/G P/G Pos / neg None HCL H2SO4 HN03 NaOH Thio OTHER
C/G P/G Pos / neg None HCL H2SO4 HN03 NaOH Thio OTHER
C/G P/G Pos / neg None HCL H2SO4 HN03 NaOH Thio OTHER
C/G P/G Pos / neg None HCL H2SO4 HN03 OTHERNaOHThio
C/G P/G Pos / neg None HCL H2SO4 HN03 OTHEPNaOHThio
COMMENTS:'
Sample
No.
Sample
Type
Comp/
Grab
(jZF
/H2^O4
H2SO4
°C____
i USM
Time:
Checked in by:
Date:
Temp:
Route:7^
Preservative
g
TmiTesT
Pos / ^eg
Pos / nebCM
p/&
P//G)
FEDX |
Thio (
^ffis’03
(h/>'°3
H2SO4
Chemical & Environmental Technology, Inc.
ENVIRONMENTAL ANALYTICAL SERVICES
FINAL REPORT OF ANALYSES
REPORT DATE: 10/11/05
SAMPLE ID- EFFLUENT
1 ofPage 1 PROJECT NAME : NPDES RENEWAL
PQLANALYSISRESULT UNITSMETHODBY
<2 mg/L10/10/05 CJY 2OIL AND GREASE EPA413.1
estimated concentrations.
3772496;PUBLIC WATER SUPPLYNC DENR CERTIFICATIONS:DWQ
LABORATORY DIRECTOR
Shipping: 1 02-A Woodwinds Industrial Court • Cary, NC 27511P.O. Box 12298 • Research Triangle Park, NC 27709
ANALYSIS
DATE
SAMPLE MATRIX- WW
TIME SAMPLED- .17 5 0
RECEIVED BY- ALT
PQL = Practical Quantitation Limit
Results followed by the letter J are
IM
UNITED WATER
Attn: TYRONE BATTLE
5926 HWY 55 EAST
DURHAM, NC 27713-
SAMPLE NUMBER- 2.3 072 9
DATE SAMPLED- 10/03/05
DATE RECEIVED- 10/06/05 SAMPLER- TYRONE BATTLE
TIME RECEIVED- 1115 DELIVERED BY- JOSE CORRALES
Chemical & Environmental Technology, Inc.
ENVIRONMENTAL ANALYTICAL SERVICES
FINAL REPORT OF ANALYSES
REPORT DATE: 10/11/05
SAMPLE ID- EFFLUENT
1 ofPage 1 PROJECT NAME : NPDES RENEWAL
ANALYSIS BY RESULT UNITS PQLMETHOD
<2 mg/L10/10/05 CJYOIL AND GREASE 2EPA413.1
estimated concentrations.
NC DENR CERTIFICATIONS:37724DWQ96 ;PUBLIC WATER SUPPLY
LABORATORY DIRECTOR
P.O. Box 12298 • Research Triangle Park. NC 27709 Shipping: 102-A Woodwinds Industrial Court • Cary, NC 27511
SAMPLER- TYRONE BATTLE
DELIVERED BY- JOSE CORRALES
ANALYSIS
DATE
SAMPLE MATRIX- WW
TIME SAMPLED- 1520
RECEIVED BY- ALT
UNITED WATER
Attn: TYRONE BATTLE
5926 HWY 55 EAST
DURHAM, NC 27713-
PQL = Practical Quantitation Limit
Results followed by the letter J are
SAMPLE NUMBER- 2.3 0 73 0
DATE SAMPLED- 10/05/05
DATE RECEIVED- 10/06/05
TIME RECEIVED- 1115
Chemical & Environmental Technology, Inc.
ENVIRONMENTAL ANALYTICAL SERVICES
FINAL REPORT OF ANALYSES
REPORT DATE: 10/11/05
SAMPLE ID- EFFLUENT
1 ofPage 1 PROJECT NAME : NPDES RENEWAL
ANALYSIS METHOD RESULT UNITS PQLBY
<2 mg/L10/10/05 CJYOIL AND GREASE 2EPA413.1
NO DENR CERTIFICATIONS:37724DWQ96;PUBLIC WATER SUPPLY
LABORATORY DIRECTOR
Shipping: 1 02-A Woodwinds Industrial Court • Cary, NC 2751 1P.O. Box 12298 • Research Triangle Park, NC 27709
ANALYSIS
DATE
PQL = Practical Quantitation Limit
Results followed by the letter J are estimated concentrations.
SAMPLE MATRIX- WW
TIME SAMPLED- 0955
RECEIVED BY- ALT
UNITED WATER
Attn: TYRONE BATTLE
5926 HWY 55 EAST
DURHAM, NC 27713-
SAMPLE NUMBER- 2.3 0 731
DATE SAMPLED- 10/06/05
DATE RECEIVED- 10/06/05 SAMPLER- TYRONE BATTLE
TIME RECEIVED- 1115 DELIVERED BY- JOSE CORRALES
Chemical & Environmental Technology, Inc.
ENVIRONMENTAL ANALYTICAL SERVICES
FINAL REPORT OF ANALYSES
UNITED WATER
REPORT DATE: 10/11/05
SAMPLE ID- EFFLUENT
1 ofPage 1 PROJECT NAME : NPDES RENEWAL
PQLANALYSISRESULT UNITSMETHODBY
725 mg/L10/07/05 RWH 10TOTAL DISSOLVED SOLIDS EPA160.1
NC DENR CERTIFICATIONS:DWQ 96;37724PUBLIC WATER SUPPLY
LABORATORY DIRECTOR
P.O. Box 12298 • Research Triangle Park, NC 27709 Shipping: 102-A Woodwinds Industrial Court • Cary, NC 2751 1
SAMPLER- TYRONE BATTLE
DELIVERED BY- JOSE CORRALES
ANALYSIS
DATE
SAMPLE MATRIX- WW
TIME SAMPLED- 0318
RECEIVED BY- ALT
PQL = Practical Quantitation Limit
Results followed by the letter J are estimated concentrations.
Attn: TYRONE BATTLE
5926 HWY 55 EAST
DURHAM, NC 27713-
SAMPLE NUMBER- 230732
DATE SAMPLED- 10/05/05
DATE RECEIVED- 10/06/05
TIME RECEIVED- 1115
Chemical & Environmental Technology, Inc.
ENVIRONMENTAL ANALYTICAL SERVICES
FINAL REPORT OF ANALYSES
REPORT DATE: 10/11/05
SAMPLE ID- EFFLUENT
1 ofPage 1 PROJECT NAME : NPDES RENEWAL
ANALYSIS RESULT UNITS PQLMETHODBY
811 mg/L10/07/05 RWH 10TOTAL DISSOLVED SOLIDS EPA160.1
96;PUBLIC WATER SUPPLY 37724NC DENR CERTIFICATIONS:DWQ
LABORATORY DIRECTOR
Shipping: 102-A Woodwinds Industrial Court • Cary, NC 27511P.O. Box 12298 • Research Triangle Park, NC 27709
SAMPLER- TYRONE BATTLE
DELIVERED BY- JOSE CORRALES
ANALYSIS
DATE
SAMPLE MATRIX- WW
TIME SAMPLED- 0319
RECEIVED BY- ALT
PQL = Practical Quantitation Limit
Results followed by the letter J are estimated concentrations.
UNITED WATER
Attn: TYRONE BATTLE
5926 HWY 55 EAST
DURHAM, NC 27713-
SAMPLE NUMBER- 230733
DATE SAMPLED- 10/06/05
DATE RECEIVED- 10/06/05
TIME RECEIVED- 1115
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FINAL REPORT OF ANALYSES
REPORT DATE: 10/11/05
SAMPLE ID- EFF
1 ofPage 1 PROJECT NAME : TDS
ANALYSIS
PQLANALYSISBYRESULT UNITSMETHODDATE
10/07/05 RWH 457 mg/L 10TOTAL DISSOLVED SOLIDS EPA160.1
3772496;PUBLIC WATER SUPPLYNC DENR CERTIFICATIONS:DWQ
LABORATORY DIRECTOR
Shipping: 1 02-A Woodwinds Industrial Court • Cary, NC 27511P.O. Box 12298 • Research Triangle Park, NC 27709
SAMPLE MATRIX- WW
TIME SAMPLED- 0405
RECEIVED BY- ALT
PQL = Practical Quantitation Limit
Results followed by the letter J are estimated concentrations.
SAMPLER- AC
DELIVERED BY- JOSE CORRALES
UNITED WATER
Attn: TYRONE BATTLE
5926 HWY 55 EAST
DURHAM, NC 27713-
SAMPLE NUMBER- 2.3 0787
DATE SAMPLED- 10/07/05
DATE RECEIVED- 10/07/05
TIME RECEIVED- 1205
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