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HomeMy WebLinkAboutWQ0014868_More Information (Received)_20240718From:brent.collins emaresourcesinc.com To:Saunders, Erickson G; atucker@smithfield.com Cc:Thornburg, Nathaniel; Allen, Trent Subject:[External] RE: [ADDITIONAL INFORMATION REQUEST #1] WQ0014868 - Smithfield Fresh Meats Corp. Class B Residuals Program Renewal Application Date:Thursday, July 18, 2024 9:57:30 AM Attachments:LASC & Map Corrections.pdf 05.23.24 North Digester Total.PDF RLAP 06-16.pdf CAUTION: External email. Do not click links or open attachments unless verified. Report suspicious emails with the Report Message button located on your Outlook menu bar on the Home tab. Erick, I have made the following changes to the Smithfield Renewal: D. I have removed Tim Weaver as the backup ORC and added Roy Whitaker in his place. G. The analysis that was submitted with the renewal was an older analysis from when Smithfield was adding caustic to their process. That is no longer the case and I have included the most recent analysis. Q. I have added the property line and corresponding buffers to field SF03-06. In the past, we have submitted property line waivers for different jobs, but they were no accepted by the State. If in the future we are able to obtain and file both waivers, will they be honored? R. 1. The field has been split into 6A and 6B. The map has been updated and the LASCA form has been updated with the new acreages. 2. The map has been updated and the acreage has been updated on the LASC form. 3. The parcel in question is a power station. There is no place of assembly. A property line buffer has been added and the acreage has been updated on the LASC form. 4. The map for SF08-05 has been included. I must have had a file name issue when submitting the original. 5. The residence and corresponding buffer has been added to the map. The acreage has been updated on the LASC form. 6. The area has been added back to the map and the LASC form has been updated. I have included one PDF that includes the LASC form and all of the map corrections. I will wait to hear from you about the corrections, and will re-submit the complete package online once everything looks good. Please let me know if you have any questions about these changes. Thank you Brent Collins Director of Technical Services EMA Resources Inc. From: Saunders, Erickson G <Erickson.Saunders@deq.nc.gov> Sent: Thursday, June 20, 2024 4:32 PM To: atucker@smithfield.com; brent.collins emaresourcesinc.com <brent.collins@emaresourcesinc.com> Cc: Thornburg, Nathaniel <nathaniel.thornburg@deq.nc.gov>; Allen, Trent <trent.allen@deq.nc.gov>; Saunders, Erickson G <Erickson.Saunders@deq.nc.gov> Subject: [ADDITIONAL INFORMATION REQUEST #1] WQ0014868 - Smithfield Fresh Meats Corp. Class B Residuals Program Renewal Application Importance: High All, Division of Water Resources’ Central and Regional Office staff have reviewed the application package. However, the Division requires additional information before completing our review. Please address the items in the attached Additional Information Request #1 no later than the close of business on July 22, 2024. All revised and/or additional documentation shall be signed, sealed, and dated (where needed), with an electronic response submitted in a single PDF as an email attachment (document size permitting) or via the Non-Discharge online portal as “Additional Information”. Please do not resubmit documentation that has no outstanding comments or revisions (i.e., manufacturer’s information, product cut sheets, flow reduction request, etc.) Failure to provide the requested additional information on or before 5:00 PM ET on July 22, 2024, shall result in your application being returned as incomplete pursuant to 15A NCAC 02T .0107(e)(2). You may request a one-time 14-calendar day extension to this deadline following the instructions on the attached Deadline Extensions for Additional Information Requests Memo. If you have any questions regarding this email, please contact me at your convenience. Regards, Erick Saunders Environmental Engineer III Division of Water Resources – Non-Discharge Branch North Carolina Department of Environmental Quality Office: (919) 707-3659 erickson.saunders@deq.nc.gov Email correspondence to and from this address may be subject to the North Carolina Public Records Law and may be disclosed to third parties by an authorized state official. FORM: RLAP 06-16 Page 2 of 5 III. RESIDUALS LAND APPLICATION PROGRAM INFORMATION: 1. Residuals Processing Facility’s physical address: 15855 NC-87 City: Tarheel State: NC Zip: 28392 Coordinates: Latitude: 34○ 44′ 50″ Longitude: 78○ 48′ 17″ Datum: NAD83 Level of accuracy: Nearest Second Method of measurement: GPS 2. County where residuals land application program is headquartered: Bladen 3. List the Operator In Responsible Charge (ORC) and all Back-Up ORCs for the residuals land application program, their certification numbers, and their affiliations in the following table: Designation Name Affiliation Certification Number ORC Dwayne Russ Smithfield Fresh Meats Corp LA1004586 Back-Up ORC Roy Whitaker EMA Resources Inc. LA13283 Additional Back-Up ORCs (if applicable) If an ORC and at least one Back-Up ORC are not currently designated for this residuals land application program, provide the candidates’ names, affiliations, and an estimated time schedule for each candidate’s completion of the required training school and certification test: 4. Complete the following tables regarding management of the residuals land application program: a. Plant Available Nitrogen Summary: Determine the maximum plant available nitrogen (PAN) generated by all residuals source-generating facilities as currently certified and proposed for certification with this application and list the results in the following table: Maximum amount of residuals to be certified: 2050 dry tons per year. PAN Pounds of PAN per Dry Ton (Weighted Average) Pounds of PAN per Year Surface Incorporation or Injection Surface Incorporation or Injection First-Year 39.879 61.979 81752 127057 Five-Year Maximum Adjusted 50.429 72.529 103379 148684 b. Land Application Site Use Summary: Summarize information regarding the land application sites as currently certified and proposed for certification with this application: Category Use Acres Comments Crops Forest or Plantation 0 Row Crops 714.86 Hay/Pasture 217.06 Total: 931.92 Methods Surface 931.92 Incorporation or Injection 0 Total: 931.92 LAND APPLICATION SITE CERTIFICATION FORM: LASC 06-16 Page 1 Applicant's name: Smithfield Fresh Meats Land application sites currently certified: 1164.8 net acres and Total to be certified: 931.92 net acres. I. LAND APPLICATION SITE INFORMATION (See Instruction B): Status Codea Site/Field ID Landowner(s) Lessee(s) or Operator(s) Net Acres County Crop(s) Predominant Soil Series Nameb Mapping Unit or Rep. Slopec R/M SF03-01 Steve Dunham 19.4 Bladen Bermuda Lakeland LaB R/M SF03-02 Steve Dunham 11.41 Bladen Rye Grass Centenary Ce R/M SF03-03 Steve Dunham 22.39 Bladen Rye Grass Centenary Ce R/M SF03-04 Steve Dunham 16.34 Bladen Row Crop Wasda Wh R/M SF03-05 Steve Dunham 3.05 Bladen Bermuda Lakeland LaB R/M SF03-6A Steven Dunham 7.17 Bladen Bermuda Lakeland LaB R/M SF03-6B John Dunham 5.48 Bladen Bermuda Lakeland LaB R/M SF03-07 Steve Dunham 30.91 Bladen Bermuda Wickham WmB R/M SF07-01 Herring Family Trust 28.97 Bladen Bermuda Altavista Aa R/M SF07-03 Herring Family Trust 11.12 Bladen Fescue Altavista Aa R/M SF07-06 Herring Family Trust 17.53 Bladen Bermuda Wickhham WmB R/M SF07-08 Herring Family Trust 9.99 Bladen Bermuda Altavista Aa R/M SF07-09 Bonnie Meeker 18.83 Bladen Row Crop Wickham WmB R/M SF07-14 Bonnie Meeker 5.63 Bladen Bermuda Lakeland LaB R/M SF07-15 Bonnie Meeker 4.05 Bladen Bermuda Augusta At R/M SF10-01 Murdock Butler 38.86 Bladen Row Crop Norfolk NoA R/M SF10-02 Murdock Butler 33.2 Bladen Row Crop Autryville AuA R/M SF10-03 Murdock Butler 20.74 Bladen Row Crop Norfolk NoA R/M SF12-01 Hinton McCall King Jr 32.19 Bladen Row Crop Norfolk NoA R/M SF06-01 Vance Tyson 7.44 Cumberland Bermuda Autryville AuA R/M SF06-02 Vance Tyson 32.52 Cumberland Bermuda Autryville AuA LAND APPLICATION SITE CERTIFICATION FORM: LASC 06-16 Page 2 R/M SF06-03 Vance Tyson 67.68 Cumberland Row Crop Deloss De R/M SF06-04 Vance Tyson 31.89 Cumberland Row Crop Deloss De R/M SF06-05 Vance Tyson 29.31 Cumberland Row Crop Deloss De R/M SF06-06 Vance Tyson 72.72 Cumberland Row Crop Deloss De R/M SF06-07 Vance Tyson 71.96 Cumberland Row Crop Deloss De R/M SF08-01 McCall King Jr. 6.19 Robeson Row Crop Goldsboro GoA R/M SF08-02 McCall King Jr. 12.32 Robeson Row Crop Goldsboro GoA R/M SF08-03 McCall King Sr. 73.92 Robeson Row Crop Marlboro MaA R/M SF08-04 McCall King Sr. 61.69 Robeson Row Crop Norfolk NoA R/M SF08-05 McCall King Sr. 39.06 Robeson Row Crop Goldsboro GoA R/M SF08-06 McCall King Sr. 17.5 Robeson Row Crop Norfolk NoA R/M SF08-07 McCall King Sr. 26.65 Robeson Row Crop Goldsboro GoA R/M SF08-09 McCall King Sr. 43.81 Robeson Row Crop Coxville Co D SF09-01 Musselwhite Family Farm 36 Robeson D SF09-02 Musselwhite Family Farm 27.5 Robeson D SF09-03 Musselwhite Family Farm 9.5 Robeson D SF09-04 Musselwhite Family Farm 25 Robeson a Status Code for land application sites are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ T (Transferred) ♦ D (Deleted) b Soil Series Name (i.e. Appling, Cecil, etc.) c Mapping Unit must be consistent with those used in the County Soil Survey (i.e. for a 2-8% slope Cecil in Anson County the mapping unit is CeB2) " " " " " " " " " " ! ! ! ! ! ! !! ! ! 6B 6A NC CGIA, Maxar, Microsoft Smithfield Fresh Meats, Inc. Land Application Program SF03 Steven Dunham & John Dunham 2 WQ0014868 BC SCALE: PROJECT NO: DRAWN BY: FIGURE NO. ± !Well "Off Site Dwelling "On Site Dwelling Drain Buffer Field Boundary Pond 7/17/2024DATE: 1":440' Field Total Acres Applicable Acres 6A 10.71 7.17 6B 10.69 5.48 The compliance boundary is established either 250 ft from the residuals application area or 50 ft within the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. The review boundary for this site has been modified to allow for application up to 100 feet from on-site water supply well. [ [ [ [ [ [ [[ [ [ [ [ [ [ [ ! " " " " " " "" " " " 1 2 3 4 5 NC CGIA, Maxar, Microsoft Smithfield Fresh Meats, Inc. Land Application Program SF03 Steve Dunham 2 WQ0014868 BC SCALE: PROJECT NO: DRAWN BY: FIGURE NO. ± Buffer On-Site Dwelling "Off Site Dwelling !Well [[Fenceline Drain Field Boundary Pond Property Boundary 7/16/2024DATE: 1":660' Field Total Acres Applicable Acres 1 29.52 19.4 2 14.46 11.41 3 24.96 22.39 4 18.47 16.34 5 6.25 3.05 î " " " " " " " " " " " " " "" " " "" "" """" " " " " " !! ! ! ! ! ! !! ! ! ! !! ! ! ! ! ! ! ! ! !! ! NC CGIA, Maxar Smithfield Fresh Meats, Inc. Land Application Program SF06 Vance Tyson 2 WQ0014868 BC SCALE: PROJECT NO: DRAWN BY: FIGURE NO. ± !Well "On Site Dwelling "Off Site Dwelling î Church Cemetary Buffer Field Boundary Property Boundary 7/17/2024DATE: 1":440' 1 2 Field Total Acres Applicable Acres 1 14.83 7.44 2 45.44 32.52 The compliance boundary is established either 250 ft from the residuals application area or 50 ft within the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. The review boundary for this site has been modified to allow for application up to 100 feet from on-site water supply well. " " " " " " "" " ! 3 4 NC CGIA, Maxar, Microsoft Smithfield Fresh Meats, Inc. Land Application Program SF06 Vance Tyson 2 WQ0014868 BC SCALE: PROJECT NO: DRAWN BY: FIGURE NO. ± !Well "On Site Dwelling "Off Site Dwelling Drain Buffer Drain_Buffer7_Clip Field Boundary Property Boundary 7/17/2024DATE: 1":440' Field Total Acres Applicable Acres 3 72.6 67.68 4 38.15 31.89 The compliance boundary is established either 250 ft from the residuals application area or 50 ft within the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. The review boundary for this site has been modified to allow for application up to 100 feet from on-site water supply well. " " " " 4 7 NC CGIA, Maxar, Microsoft Smithfield Fresh Meats, Inc. Land Application Program SF06 Vance Tyson 2 WQ0014868 BC SCALE: PROJECT NO: DRAWN BY: FIGURE NO. ± !Well "On Site Dwelling "Off Site Dwelling Drain Buffer Field Boundary Property Boundary 7/17/2024DATE: 1":660' 6 5 Field Total Acres Applicable Acres 5 32.85 29.31 6 103.85 72.72 The compliance boundary is established either 250 ft from the residuals application area or 50 ft within the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! " " " NC CGIA, Maxar, Microsoft Smithfield Fresh Meats, Inc. Land Application Program SF08 McCall King Sr. 2 WQ0014868 BC SCALE: PROJECT NO: DRAWN BY: FIGURE NO. ± "Off Site Dwelling Drain !!!!!!Stream Buffer Field Boundary Property Boundary 7/17/2024DATE: 1":440' 5 Field Total Acres Applicable Acres 5 46.5 39.06 The compliance boundary is established either 250 ft from the residuals application area or 50 ft within the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! !! !! !! !! !!!!!!!!!!!!!!!!!! !!!! !! !! !! !! !! !! !! !! !! !!!!!! !! !!!!!! !! !! !! !! !! !! !! !! !! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! " " "" " " " "! 2 3 NC CGIA, Maxar, Microsoft Smithfield Fresh Meats, Inc. Land Application Program SF10 Murdock Butler 2 WQ0014868 BC SCALE: PROJECT NO: DRAWN BY: FIGURE NO. ± !Well "On Site Dwelling "Off Site Dwelling !!!!!!Stream Drain Pond Buffer Field Boundary Property Boundary 7/17/2024DATE: 1":440' Field Total Acres Applicable Acres 2 44.44 33.2 3 30.67 20.74 The compliance boundary is established either 250 ft from the residuals application area or 50 ft within the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. The review boundary for this site has been modified to allow for application up to 100 feet from on-site water supply well. " " " " " " " " " " " ! ! ! ! ! ! ! ! ! ! 1 NC CGIA, Maxar Smithfield Fresh Meats, Inc. Land Application Program SF12 McCall King Jr 2 WQ0014868 BC SCALE: PROJECT NO: DRAWN BY: FIGURE NO. ± !Well "Off Site Dwelling Drain Buffer Field Boundary Property Boundary 7/17/2024DATE: 1":440' Field Total Acres Applicable Acres 1 46.28 32.19 The compliance boundary is established either 250 ft from the residuals application area or 50 ft within the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. The review boundary for this site has been modified to allow for application up to 100 feet from on-site water supply well.   Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.   6/3/2024 EMA Resources Inc Mr. Brent Collins 755 Yadkinville Rd Mocksville, NC, 27028 Ref: Analytical Testing Lab Report Number: 24-145-0038 Client Project Description: Smithfield/ NC Dear Mr. Brent Collins: Waypoint Analytical, LLC. received sample(s) on 5/24/2024 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '~' symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as- received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Connie Cook Project Manager Page 1 of 8 Certification Summary Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date 02/28/202540750State ProgramAlabama 02/07/202588-0650State ProgramArkansas 06/30/20242904State ProgramCalifornia 06/30/2024E871157State Program - NELAPFlorida 11/14/2025C044State ProgramGeorgia 06/30/202404015State ProgramGeorgia 10/31/2024200078State Program - NELAPIllinois 06/30/202480215State ProgramKentucky 12/31/2024KY90047State ProgramKentucky 12/31/2024LA037State Program - NELAPLouisiana 06/30/202404015State Program - NELAPLouisiana 11/14/2025MSState ProgramMississippi 07/31/202447701State ProgramNorth Carolina 12/31/2024415State ProgramNorth Carolina 05/31/202568-03195State Program - NELAPPennsylvania 06/30/202484002State ProgramSouth Carolina 11/14/202502027State ProgramTennessee 09/30/2024T104704180State Program - NELAPTexas 06/30/202400106State ProgramVirginia 09/14/2024460181State Program - NELAPVirginia Page 1 of 1 00001/24-145-0038 Page 2 of 8 Report Number: Sample Summary Table Client Project Description: 24-145-0038 Smithfield/ NC Lab No Client Sample ID Matrix Date Collected Date Received 05/23/2024 09:30Solids 83440 Smithfield North Dig 05/24/2024 Page 3 of 8   Client: EMA Resources Inc CASE NARRATIVE Project: Smithfield/ NC Lab Report Number: 24-145-0038 Date: 5/31/2024 Metals Analysis Method 6010D Sample 83440 (Smithfield North Dig) Analyte: Calcium QC Batch No: L753101/L752701 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 83440 (Smithfield North Dig) Analyte: Sulfur QC Batch No: L753457/L752701 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 83440 (Smithfield North Dig) Analyte: Zinc QC Batch No: L753101/L752701 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 4 of 8 , REPORT OF ANALYSISReport Number : Project Information : NC 27028 24-145-0038 46245 EMA Resources Inc 755 Yadkinville Rd Mr. Brent Collins Mocksville Connie Cook Project Manager Received : 05/24/2024 Smithfield/ NC Report Date : 06/03/2024 Sample ID : Lab No : Sampled:Smithfield North Dig 83440 Matrix: 5/23/2024 9:30 Solids Test Results Units MDL MQL By Analytical Method Date / Time Analyzed DF 95.55 %0.010 0.010 Moisture 1 05/24/24 12:50 SW-DRYWTCAH 14700 mg/Kg - dry 360 2250 Ammonia Nitrogen 1 05/31/24 11:00 4500NH3C-2011JPJ <106 mg/Kg - dry 106 112 Nitrate+Nitrite-N 1 05/29/24 10:57 4500NO3F-2016JRZ 65400 mg/Kg - dry 9280Organic N 1 05/31/24 11:00 CALCULATION 7.7 s.u.pH 1 05/24/24 16:00 9045DCNB 4.45 %0.010 0.010 Total Solids 1 05/24/24 12:50 2540G-2011CJR 79.0 %0.010 0.010 Total Volatile Solids 1 05/24/24 12:50 2540G-2011CJR 80000 mg/Kg - dry 9280Total Kjeldahl Nitrogen 1 05/31/24 14:00 4500NORGD-2011ANH 20500 mg/Kg - dry 62.9 112 Phosphorus 1 05/30/24 04:15 6010DJTR 10600 mg/Kg - dry 104 112 Aluminum 1 05/30/24 04:15 6010DJTR <5.62 mg/Kg - dry 5.62 11.2 Arsenic 1 05/30/24 04:15 6010DJTR <1.12 mg/Kg - dry 1.12 2.25 Cadmium 1 05/30/24 04:15 6010DJTR 29900 mg/Kg - dry 870 1120 Calcium 1 05/30/24 04:15 6010DJTR 61.8 mg/Kg - dry 5.62 5.62 Chromium 1 05/30/24 04:15 6010DJTR 1940 mg/Kg - dry 6.74 11.2 Copper 1 05/30/24 04:15 6010DJTR 16200 mg/Kg - dry 192 225 Iron 1 05/30/24 04:15 6010DJTR 10.1 mg/Kg - dry 4.49 6.74 Lead 1 05/30/24 04:15 6010DJTR 2670 mg/Kg - dry 58.4 112 Magnesium 1 05/30/24 04:15 6010DJTR 625 mg/Kg - dry 7.87 11.2 Manganese 1 05/30/24 04:15 6010DJTR <0.443 mg/Kg - dry 0.443 3.66 Mercury 1 05/30/24 13:19 7471AFDS 18.0 mg/Kg - dry 3.37 5.62 Molybdenum 1 05/30/24 04:15 6010DJTR 63.4 mg/Kg - dry 3.37 5.62 Nickel 1 05/30/24 04:15 6010DJTR 4940 mg/Kg - dry 139 225 Potassium 1 05/30/24 04:15 6010DJTR Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 5 of 8 , REPORT OF ANALYSISReport Number : Project Information : NC 27028 24-145-0038 46245 EMA Resources Inc 755 Yadkinville Rd Mr. Brent Collins Mocksville Connie Cook Project Manager Received : 05/24/2024 Smithfield/ NC Report Date : 06/03/2024 Sample ID : Lab No : Sampled:Smithfield North Dig 83440 Matrix: 5/23/2024 9:30 Solids Test Results Units MDL MQL By Analytical Method Date / Time Analyzed DF <7.87 mg/Kg - dry 7.87 11.2 Selenium 1 05/30/24 04:15 6010DJTR 9060 mg/Kg - dry 292 562 Sodium 1 05/30/24 04:15 6010DJTR 3640 mg/Kg - dry 19.1 28.1 Zinc 1 05/30/24 04:15 6010DJTR 23400 mg/Kg - dry 584 1120 Sulfur 5 05/30/24 18:17 6010DJTR 2.83 Ratio 0.01 0.01 Sodium Absorption Ratio 1 05/30/24 04:15 CALCULATION Qualifiers/ Definitions Method Quantitation LimitMQLDilution FactorDF Page 6 of 8 Fed Ex UPS US Postal Client Lab Courier Other : Shipment Receipt Form Customer Number: Customer Name: Report Number:24-145-0038 EMA Resources Inc 46245 Shipping Method Shipping container/cooler uncompromised? Thermometer ID:TI211 Chain of Custody (COC) present?Yes No Yes No Not Present Yes No Not Present Yes No COC agrees with sample label(s)? Yes No COC properly completed Samples in proper containers? Sample containers intact? Sufficient sample volume for indicated test(s)? All samples received within holding time? Cooler temperature in compliance? Yes No Yes No Yes No Yes No Yes No Yes NoCooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. Yes No Yes No N/A Yes No N/A Yes No N/ASoil VOA method 5035 – compliance criteria met Water - Sample containers properly preserved Water - VOA vials free of headspace Yes No N/A Trip Blanks received with VOAs Low concentration EnCore samplers (48 hr) High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d) High concentration container (48 hr) Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Number of coolers/boxes received Yes No 1 Signature:Carleen Qualls Date & Time:05/24/2024 09:44:52 Special precautions or instructions included? Comments: Page 7 of 8 Page 8 of 8