WQ0014885_2017 Annual Land App Report_20180213

I
HARNETT COUNTY, NC
CLASS A RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0014885
2017 ANNUAL REPORT

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00014885 County Harnett Year 2017
Facility Name (as shown on permit) Harnett County Utilities Regional WTP PWS ID No. 00-076-84
Land Application Operator ' Synagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip PartA, and PartB and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A— Residuals Application Summary:
Total number of application fields in the permit: N/A
Total number of fields utilized for land application during the year: 3
Total amount of dry tons applied during the year for all application sites: 797.49
Total number of acres utilized for land application during the year: 159.1
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2017 with all conditions of the land application permit.(including but not limited to items
1-13 below) issued by the Division of Water Quality X YBS NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied_ to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .I 111 were complied with (applicable to 40 CFR Part 503
regulated facilities). I
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Divisionof Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knWthe
elief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, inclbility of fines and imprisonment for
knowing violations."
Steve Ward. Director of Public Utilitie/ �/% 311
8
PernFRM,
i type or tj� na r rm EBD$el 2018
ignature of Pr96E rer* 6ate/ Mgnature of Land Applier Date
(if different fridm Permittee) (if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

201.7 ANNUAL,,OPERATIONS SUMMARY - LAND APPLICATION
HARNETT-CO. UTILITIES-, NC'
,HARNETT CO. UTIL'.,'NC COH
REGIONAL W-TP LIQUID
DRY METRIC
MONTHNEAR
AMOUNT
UNIT
DRY TONS
UNIT.
TONS
January 2017
668,400.00
G
44.82
D
40.66
February 2017
'122,200.00
G
75.82
D
68.77
March 2017
514,600.00
G
23.61
-D
21.41
April 2017.
892,800.00,
G
40.96
D
37.15
May 2017
973,400.0 - 0
G
89.71
D
81.37
June 2017
855,600.00
G
78.85
D
71-52
July 20.17,
954,800.00
-G
88.00
D-
79.82..
August 2017
1,853,80.0-.00.
G
170.84.
D.
154.96
September 2017
502,200.00
G
43.97
D
39.89-
October 2017
= 1,14.7,000.00
G
100.44
D
91.10
November 2017
961'000.00
G
24.03
D'
21.81
December 2017
657,200.00
G
16.44
D
14.92
YEARLY TOTAL
11,098,1000.00
G
797.49.
D
723.38.
1/30/2018

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQOG14885: Laboratory
Facility Name: HARNETT CO. UTILITIES, NC Waypoint Analytical Virginia Inc.
NPDES# : NC0007684
or WQ# (residual only)
WWTP Name:, COH REGIONAL WTP
Residuals Analysis Data
Product Type WPL WPI, WPL WPL
Date Sampled (grab) or 03/16/17 05/23/17 07/20/17 11/20/17
Date Composited
Percent Solids 1.10 2.21 2.10 0.60
PARAMETERS (mg/kg dry weight)
Arsenic
7:67
<3
10.2
13
Cadmium
<2
<2
<2
<2.02
Mercury
<0.4
<0.4
<0.4
<0.4
Chromium
1:3.2
25.5
13.6
9.72
Copper
353
84.1
206
335
Lead
7.57
12.6
5.91
<5.06
Molybdenum
9.97
8.41
6.76
24
Nickel
5.72
_ 10.6
5.15
7.23
Selenium
<5
<5
<5
<5.06
Zinc
30.8
88.3
22.7
32
Total Phosphorus
1560
1950
1690
2120
TKN
9010
6760
10900
9840,
Ammonia -Nitrogen
.4500
<50
<50
<50
Nitrate and Nitrite
<2.14
<2.25
<2.27
<2.38-
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel
properly gathered
and evalugted the information" submitted. I am aware that there are
significant pen 'e for submitting
false, informa. n, incl 'ng
the poss'
ility of fines and imprisonment for knowing violations."
X Date
(SI TORE AOFPREPAR R)
DENR FORM RSSF (5/2003) Printed: Tuesday - January 30, 2018 at 14:15:17 for: 2037 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to -be analyzed than those required to be summarized on this form.
Permit Number: WQ0014885
Laboratory
Facility Name: HARNETT CO. UTILITIES,
NC
Waypoint Analytical Virginia Inc.
NPDES# : NC0007684
or WQ# (residual only)
WWTP Name: COH REGIONAL WTP
Residuals Analysis Data
Product Type WPL
WPL
WPL
WPL
Date Sampled (grab) or 03%16/17
05/23/17
07/20/17
11/20/17
Date Composited
Percent Solids 1.10
2.21
2.10
0.60
PARAMETERS (mg/kg dry weight)
Aluminum 125000
111000
105000
143000
Calcium 962
1440
2380
2580
Magnesium 524
536
388
875
'pH 5.30
5.52
6.13
7.57
Potassium 398
391
282
767
Sodium 920
545
288
2820
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluate,4the information submitted. I am aware that there are
significant p naKt f r ubmitting false infor at' , in the possibi ' of fines and imprisonment for knowing violations."
X`Date 1-5 5�al
(SIGITATURE OF P
NR - Data Not Reported or Data Not Requi
DENR FORM RSSF-B (7/2002) Printed: Tuesday - January 30, 2018 at 14:15:51 for: 2037 01

Page: 1 of 2
Report Number: 17-076-0203
Account Number: 46460
Wayp
oi nt
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
Submitted By: Will Varner
ANALYTICAL
www.waypointanalytical.com
Send To: Synagro Central LLC/ Harnett
Project; Harnett WTP
Mary Brewer
NC- Cert#257
County .
284 Boger Road
Mocksville , NC 27028
;
REPORT OF ANALYSIS
Date Sampled: 3/16/2017 14:45:00
Lab Number: 62899.
Date Received: 03/17/2017 00:00
Sample Id : Harnett WTP.
Date Reported: 03/24/2017
RESULT
RESULT
QUANTITATION
METHOD
Total Solids *
1.10.
11000
100.0
R D"-
03/17/2017 15:00 SM-2540G
Moisture *
98.89
' : 100.0
R D
03/17/2017 15;00 8M-2540G
Total Kjeldahl Nitrogen
-.0.90
9010
50.0 .
JM
03/20/2017 09:35 SM-4500-NH3C-TKN
Total Phosphorus
0.16
1560
100"
MOS
03/21/2017 13:21 6010C
Total Potassium
0.04
398
100
MOS
03/21/2017 13:21 - 6010C
Total Sulfur . :.
2.04
20400
100
MOS
03/21/2017 13.21 6010C
Total Calcium
0.10
-962
100
MOS
03/21/2017 13:21 6010C
Total Magnesium
0.05
524
100
MOS
03/21/2017 13:21 6010C
Total Sodium
0.09
920
1.00
MOS
03/21/2017 13:21 601ob
Total Iron
18300
100
MOS
.03/21/2017 13:21 6010C
Total.Aluminum
125000
1 100
MOS,
03/21/2017 13:21 6010C
Total Manganese
1230
5.00
JTR
03/23/2017 23:20 6010C.
Total Copper
353
5.00
MOS
03/21/2017 13:21 60.10C
Total Zinc
30.8
5.00
JTR
03/23/2017 23:20 6010C
Ammonia Nitrogen
0A5
.4500
50.0
JM
03/20/2017 09:35 SM-4500-NH3C
Organic N -
0.45
4510
•50.0
03/20/2017 09:35 CALCULATION
Nitrate+Nitrite-N
<2.14
2.14
SJB
03122/201712:43 4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet -basis.
Our reports and letters are for the exclusive and confidential use or our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements withoutobtaining ourprior written authorization.
Debbie Holt
Laboratory Supervisor

I\
1
Page: 2 of 2,
Report Number:- 17-076-0203'
Account Number: 46460
Waypoint
. 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-94.01 ° Fax [phone]
Submitted By: Wilf Varner
ANALYTICAL
www.waypointanalytical.com
Send To: Synagro Central LLC/ Harnett
Project : Harriett WTP
Mary Brewer
NC Cert#257
County
284 Boger Road
Mocksville , NC 27028
REPORT OFANALYS/S '
'Date Sampled: 3/16/2017 14:45:00 .
Lab Number : 62899.
Date Received: 03/17/2017 00:00
Sample Id : Harnett WTP
a
Date Reported: 03/24/2017
PARAMETER
RESULT RESULT QUANTITATION
Total Cadmium
<2,00 2.00 MOS
03/21/2017 13:21 6010C
Total Chromium
13.2 5.00 MOS
03/21/2017 13:21 6010C -
Total Nickel,
5.72 5.00 MOS
03/21/.2017 13:21 6010C
Total Lead .'
.. 7.57- 5.00 MO$
03/21/2017 13:21 6010C
' Total Arsenic
7.67 3.00 JTR
03/23/2l)17 23:20 6010C'
Total Mercury
<0.400 0.400'' SJB
03/22/2017 12:32 SW-7471 B
Total Selenium
<5.00 5.00 JTR
03/21/2017 13:21 6010C
PH (Standard'.Units) *
-5.30 ; 1.00 R D
03/21/2017 10:15 SW-9045D
Total Molybdenum
9.97 5.00 MOS
03/21/2017 13:21 6010E .
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters:are for the exclusive and confidential use of our clients, and maynotbe reproduced in whole or part nor may any reference be made
to the work, the results, or the company in any advertising, news
release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Laboratory Supervisor

Sodium Absorption Ratio Calculation (SAR)'
Product Code Product Name Sample Date Report Range Ratio
2037-01-WPL-NC HARNETT CO. UTIL., NC COH REGIONAL. 3/16/2017 3/1/2017-4/30/2017 0.6193
WTP LIQUID •
Na mg/I = (Na mg/kg x % Solids) =100 = (920 x 1:1000) =100 = 10.12
Ca mg/I = (Ca mg/kg x % Solids) =.100 = (962'x 1.1000) = 100 = 10.582
Mg mg/l = (mg mg/kg x'% Solids) _ 100 = (524 x 1'.1000) -= 100 = 5.764
Na meq = Na mg/1-= Molec.Wgt.Na = 10.12 = 23 = 0.44
Ca meq = Ca mg/1 = Molec.Wgt.Ca = 10.582 + 20 = 0.5291
Mg meq = Mg mg/1 = Molec.Wgt.Mg =5.764 + 12 = 0.480333
SAR = Na meq = SqrRoot[0.5 x (Ca meq + Mg meq)] = 0.44 = SgrRoot[0.5(0.5291+0.480333)] = 0.61934
Page 1
Printed: 1/30/2018
14:18

Page: 1 of 2
Report Number: 17-144-0202
Account Number: 46460 7621 Whitepine Road, Richmond; VA 23237 .
Waypoint Main 804-743-9401 *.Fax [phone]
ANALYTICAL www.waypointanalytical.com
Send To: Synagro Central LLC/ Harnett" Project :.Harnett
MaryBrewer
County
284 Boger Road
Mocksville , NC 27028
REPORT OF ANALYSIS Date.Sampled: 5/23/201713:30:0&
Lab Number: 64100 Date. Received: 05/24/2017 00:00
Sample Id : Harnett WTP Date Reported: 05/31/2017
Total -Solids *
2.21
22100
100.0
JM
05/24/2017 15:50
SM-2540G
' Moisture *
97.78
100.0
JM
05/24/2017 15:50
SM-2540G
Total Kjeldahl Nitrogen
0.68
6760
50.0
R D
05/25/2017.08.30
SM-4500-NH3C-TKN
Total'Phosphorus
0.20
1950
100
JTR
05/26/2017 23:52
6010C
Total Potassium
0:04
391
100
JTR
05/26/2017 23:52
60.10C
Total Sulfur
1.36:
13600
100
JTR
05/26/2017 23:52
6010C
Total Calcium
0.14
1440
100
JTR
05/26/2017 23:52
6010C
Total -Magnesium
0.05
.536
100
JTR
05/26/2017 23:52
6010C
Total Sodium
0.05
545
100
JTR
05/26/2017 23:52
6010C
Total Iron
16400
100
JTR
05/26/2017 23:52
6010C.
Total Aluminum.
111000
1000
JTR.
05/27/2017 00:06
6010C
Total Manganese
1550
5.00
JTR
05/26/2017 23:52
6010C
Total Copper
84.1
5.00
-JTR
05/26/2017 23:52
6010C
Total Zinc
88.3
5.00
JTR
05/26/2017 23:52
6010C
Ammonia Nitrogen
<50.0
50.0
R 0
05/25/2017 08:30
SM-4500-NH3C
Organic.N
6760
56.0
05/25/2017 08:30
CALCULATION
" Nitrate+Nitrite-N
<2.25
2.25
"SJB
05/25/2017 14:07
4500NOY-2011
All values are on a dry weight
basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
.
.
. . . .
P /
l C w
"Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in
whole or part, nbr may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining ourprior written authorization. ,
Pauric McGroary
Agronomist

Page: 2 of 2
Report Number: 17-144-0202
Account Number: 46460
Send -To: Synagro Central LLC/ Harnett
Mary Brewer
County
284 Boger Road
Mocksville , NC 27028
Lab Number: 64100
Sample Id : Harnett WTP
Waypoint
ANALYTICAL
Project : Harnett
REPORT OF ANALYSIS
Total Cadmium.,
<2.00
Total Chromium
25.5
Total Nickel
10.6
Total Lead
12.6
Total Arsenic
<3.00
Total Mercury
<0.400
Total Selenium
<5.00
pH (Standard Units) *
5.52
Total Molybdenum
8.41
Comments:
NC CERT#257
SULFUR AND ORGANIC NITROGEN NOT
FOR COMPLIANCE PURPOSES:
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Date Sampled: 5/23/2017 13:30:00
Date Received 05/214/2017 00:06
Date Reported:-05/31/2017
2.00
JTR
05/26/2017 23:52
6010C
5.00
JTR
05/30/201717:20
6010C
5.00
JTR
05/26/2017 23:52
6010C
5.00
JTR
05/26/2017 23:52
6010C
3.00
JTR
05/26/2017 23:5.2
6010C
0.406
SJB
05/26/20.1710:46
SW-7471B
5.00
JTR
05/26/2017 23:52
6010C
1.00
R D
05/25/2017.08:30
SW-9045D
5.00
JTR
05/26/201123:52
6010C
All values are on a dry weight basis except as.noted by asterisk: Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
PeWi4 X '�Owr
Pauric McGroary
Agronomist

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
2037-01-WPL-NC HARNETT CO. UTIL., NC COH. REGIONAL 5/23/2017 5/1/2017-8/3112017 0.4612
WTP LIQUID
Na mg/1= (Na mg%kg x % Solids) _ 100 = (545 x 2.2100) : 100=.12.0445
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (1440 x 2.2100) _ 100 = 31.824
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (536 x 2.2100) _ 100 = 11.8456
Na meq = Na mg/I = Molec.Wgt.Na = 12.0445 _ 23 = 0.523674
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 31.824 _ 20 = 1.5912
Mg meq = Mg mg/1= Molec.Wgt.Mg = 11.8456 = 12 = 0.987133
SAR = Na meq - SgrRoot[0.5 x (Ca meq + Mg meq)] = 0.523674 = SgrRoot[0.5(1.5912+0.987133)] = 0.461218
Printed: 1 /30/2018
Page 1 14:18

Page: 1 of 2
Report Number: 17-214-0207
Account Number: 46460
Submitted By: Will Varner
Send To:, Synagro Central LLC/ Harnett
Mary Brewer
County
284 Boger Road
Mocksville , NC 27028
Lab Number 55518
Sample Id : Harnett WTP
Way t
io
,v
-ANALYTICAL
Project: HarnettWTP
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Date Sampled: 7/20/2017 15:15:00
Date Received: 08/02/2017 00:00
Date Reported: 08/09/2017• .
Total Solids *
2.10
21000
100.0
BW 1
08/02/2017 14:30
' SM-2540G
Moisture *
97.'89
..100.0
BW1
08/02/2017 14:30
SM-2540G
Total Kjeldahl Nitrogen
1.09
10900
50.0
R D
08/03/2017 08:40
SM-4500-NH3C-TKN
Total. Phosphorus
0:17
1690
100
MOS
08/03/2017 14:30
6010C
Total Potassium
0.03 .
282
.100
MOS
08/03/2017 14:30
6010C
Total Sulfur
1.3.2
13200
100
MOS
•08/.03/2017 14:30
6010C
Total'Calcium
0.24
2380
100
MOS
08/03/2017 -14:30
6010C
Total Magnesium
0.04 ..
388 -
.100
MOS
08/03/2017 14:30
6010C
Total Sodium
0.03,
288
100
MOS
08/03/2017 14:30
6010C
Total Iron
11900
100
MOS
08/03/2017 14:30.'
6010C
Total Aluminum
105000
100
MOS
08/03/2017 14:30
6010C
Total Manganese
1310
5.00
MOS
08/03/2017 14:30
60100
Total Copper
206
5.00
MOS
0810312017,14:30
6010C
Total Zinc
22.7.
5.00
MOS
08/03/2017 14:30
6010C
Ammonia Nitrogen
<50.0
.50.0
R D
08/03/2017 08:40
SM-4500-NH3C
Organic N
109001.
50.0
08/03/2017 08:40
CALCULATION
Nitrate+Nitrite-N
<2.27
2.27
SJB
08/03/201714:14
4500NO317-2011
All values are on'a.dry weight basis except as noted
by asterisk. Detection
limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in
whole or part, nor may any reference be made
.
to the work, the results, or the company in any advertising,
news release, or otherpubfic announcements without obtaining ourprior written authorization.
Pauric McGroary
Agronomist

Page: 2 of 2 "
Report N umber: 17-214-0207
•
Account Number: 46460
Waypoint
7621 Whitepine Road, Richmond, VA 23237
Submitted By: Will Varner
Main 804-743-9401 "Fax [phone]
ANALYTICAL.
www.waypointanalytical.com - -
Send To: Sy-nagro" Central LLC/ Harnett
Project: Harnett WTP
Mary Brewer
County
284 Boger Road
Mocksville ,' NC 27028
REPORT OF ANALYSIS'
Date Sampled: 7/20/2017 15:15:00
lab Number: 55518
Date Received: 08/02/2017 00:00 .
Sample Id : Harnett WTP-
Date Reported: 08/00/2017
RESULT RESULT QUANTITATION
PARAMETER
.• •.
Total Cadmium
<2.00 2.00 MOS
08/03/2017 14:30 6010C
Total Chromium
13.6 5.00 MOS
08/03/2017 14:30 6010C
Total'Nickel
5.15 5.00 MOS
08/03/2017 14:30 6010C
Total Lead
__ 591 - 5.00 MOS
08/03/2017 14:30 6010C,
Total Arsenic
10.2 3.00 MOS
08/03/2017 141.30 6010C
Total Mercury
<0.400 0.400 SJB
08/04/2017 12:00 SW-7471 B
Total Selenium
<5.00 5.00 _ MOS
08/03/2017 14:30 • 601 OC'.
pH *
6.13 1.00 " R D
.08/03/2017 08:40 SW-9045D
Total Molybdenum
6.76 5.00 MOS
08/03/2017 14:30 6010C
Comments:.
NC CERT#257; SC CERT#9300 7001
' SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
`All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use, of our clients, and may not be.reproduced in whole or part, nor may any reference be made
_
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining ourprior written authorization.
Pauric McGroary
Agronomist _

r
Sodium.Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
2037-01-WPL-NC HARNETT CO. UTIL., NC COH REGIONAL - 7/20/2017 91112017-10/31/2017 0.2086
WTP LIQUID
Na mg/I = (Na mg/kg x % Solids) _ 100 = (288 x 2.1000) + 100 = 6.048
Ca mg/I = (Ca mg/kg x % Solids) = 100 (2380 x 2.1000) 100 = 49.98
Mg mg/I = (mg mg/kg x % Solids) 100 = (388 x 2.1000) = 100 = 8.148
Na meq = Na mg/I - Molec.Wgt.Na = 6.048 = 23 = 0.262957
Ca meq ;= Ca mg/I _ Molec.Wgt.Ca= 49.98 = 20 = 2.499
Mg meq = Mg mg/I + Molec.Wgt.Mg = 8.148 =12 = 0.679
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] =,0.262957 = SgrRoot[0.5(2.499+0.679)] = 0.208604
- r
Printed: 1/30/2018
Pagel 14:19

Page: i of 2
Report Number: 17-333-0207
Account Number: 46460
Submitted By: Will Varner
Send To: Synagro Central LLC/ Harnett.
Mary Brewer
County
284 Boger Road.
Mocksville , NC 27028
Lab Number: 57370 ,
Sample Id : -Harnett WTP .
WaypointANALYTICAL"
Project: Harnett WTP
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond,'.VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalyVca l.com
Date Sampled: 11/20/2017 10:35:00
Date Received: 11/29/2017 00:00
Date Reported: 12/07/2017
Total Solids *
0.60
6000
100.0
JM
11/29/2017 16:30
SM-2540G
Moisture *
99.39
100.0
JM
11/29/2017.16:3U
SM-2540G
Total Kjeldahl Nitrogen
0.98
9840 ,
50.0
JM
11/30/2017 08:00
SM-4500-NH3C-TKN
Total Phosphorus
0.21
2120
101
MOS
12/01/2017 13:34
6010C
Total. Potassium
0.08
767
101
MOS
12/01/2017 13:34
6010C
Total Sulfur
2.55
25500
101
MOS
12/01/2017 13:34
6010C
Total Calcium
0.26
2580""
101
MOS
12/01/2017 13:34
6010C
Total Magnesium
0.09
875
101
MOS
12/01/2017-13:34
=. 6010.0
Total Sodium
0.28
'2820
101
MOS
12/01/2017 13:34
6010C'
Total Iron
8380
101
MOS
12/01/2017 13:34
6010C
Total Aluminum
143000
101
MOS
12/01/201713:34
6010C
Total Manganese
806 ..
5.06
MOS -
12/04/2017 13:03
' 6010C
Total Copper '
335 -
.5.06
MOS
12/01/2017 13:34
6010C"
Total Zinc
32.0
5.06 "
MOS
12/04/2017 13:03
6010C
Ammonia Nitrogen
<50.0 _
50.0
R D
'11/30/2017 08:00
SM-4500-NH3C
Organic N
9840
50.0
11/30/2017 08:00
CALCULATION .
Nitrate+Nitrite-N .
<2.38
2.38
BW 1
12/07/2017 11:09
4500NO3F-2011
All values are on a dry weight basis except as noted
by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and,may
not be reproduced in
whole or pact nor may any reference be made
to the wod1, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Pauric McGroary
Agronomist

Page: 2 of 2`/
Report Number: 17-333-0207
Account Number: 46460
Waypo
7621 Whitepine Road, Richmond, VA 23237
i nt.�
Main 804-743-94'01 ° Fax [phone]
Submitted By:
y Will Varner
ANALYTICAL
www.waypointanalytical.com
Send To: Synagro Central LLC/ Harnett
Project : Harnett WTP
Mary Brewer.
County
284 Boger•Road
Mocksville , NC-27028
REPORT OFANALYSIS'
Date sampled: 11/20/2017 10:35:00
-Lab Number: 57370
Date Received: 11/29/2017 00:00
Sample Id : Harnett WTP
Date Reported: 12/07/2017
RESULT RESULT QUANTITATION LIMIT
ANALYST
ANALYSIS
METHODPARAMETER
Total Cadmium
<2.02 2.02 MOS
12/01/201713:34 6010C
Total Chromium .
9.72. 5.00 MPS
12/05/2017 16:06- .6010C '
Total Nickel
7.23 5.00 MOS -:
12/05/2017,16:06. 010C.
Total Lead
<5.06 "5.06 MOS
12/01/2017 13:34 6010C
Total Arsenic
13.0 3.04 • MOS
12/01/2017 13:34 6010C
Total Mercury
<0.400 0.400 MOS
12/06/20,17 15:11 SW-7471 B
Total Selenium
<5.06 5.06 MOS
12/01/2017 13:34 6010C
pH -*:.
7.57. - 1.00 JM
11/30/2017 08:00. SW-9045D
Total Molybdenum .
24ff 5.00 MOS
12/05/2017 16:06 6010C
Comments:
NC CERT#257; SC CERT#9300 7001
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
. ._
.
• ��« . imp 6ew•
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising,'news
release, or other public announcements without obtaining ourprior written authorization.
Pauric McGroary
Agronomist

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2037-01-WPL-NC HARNETT CO. UTIL., NC COH REGIONAL 11/20/2011 11/1/2017-12/3112017 0.9452
WTP LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (2820 x 0.6000) _ 100 = 16.92
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (2580 x 0.6000) _ 100 = 15.48
Mg mg/I = (mg mg/kgx % Solids) _ 100'-- (875 x 0.6000) — 100 = 5.25
Na meq = Na mg/I = Molec.Wgt.Na = 16.92 = 23 = 0.735652
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 15.48 _ 20 = 0.774
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 5.25 _ 12 = 0.4376
SAR = Na meq -= SgrRoot[0.5 x (Ca meq + Mg meq)] 0.735652 = SgrRoot[0.5(0.774+0.4375)] = 0.945205
Printed: 1/3012018
Page 1 14:19

ACILITY NAME: HARNETT CO. UTILITIES, NC
WNER: HARNETT. COUNTY
ITE #: NC HA OOX43 FIELD# : HA OOX43 0001
ESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: LAKELAND
PERMIT #: WQ0014885 ANNUAL DRY TONS APPLIED: 711.20
OPERATOR: HARNETT COUNTY CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 39.30 ACRES PERMITTED: 39.30
Page
Lune Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
- %
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
MONTH
Solids
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
Total
Per Acre
1/16/17
235,600.00 (G)
5994.911
1.62
0.405
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
41,700.p
6,130.00 p
10.80 p
10190
I BERMUDAGRASS
1/17/17
210,800.00 (G)
5363.868
1.62
0.362
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
41,700.p
6,130.00 p
10.80 p
10190
BERMUDAGRASS
1/31/17
217,000.00 (G)
5521.628
1.62
0.373
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
41,700.p
6,130.00 p
10.80 p
10190
BERMUDAGRASS
Jan-17
663,400.00 (G)
16,880.407
2/1/17
198,400.00 (G)
5048.346
1.62
0.341
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
41,700. p
6,130.00 p
10.80 p
10190
I BERMUDAGRASS
2/16/17
285,200.00 (G)
7256.997
1.62
0.490
HCUCOHV
MOIST
0-<I/2"
SUR
0.5
0.20
41,700. p
6,130.00 p
10.80 p
10190
I BERMUDAGRASS
2/17/17
217,000.00 (G)
5521.628
1.62
0.373
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
41,700.p
6,130.00 p
10.80 p
10190
I BERMUDAGRASS
2/27/17
235,600.00 (G)
5994.911
1.62
0.405
HCUCOHV
DRY
0-<1/2"
SUR
0.5
0.20
41,700.p
6,130.00 p
10.80 p
10190
I BERMUDAGRASS
2/28/17
186,000.00 (G)
4732.824
1.62
0.320
HCUCOHV
DRY
0-<1/2"
SUR
0.5
0.20
41,700.p
6,130.00 p
10.80 p
10190
BERMUDAGRASS
Feb-17
1,122,200.00 (G)
28,554.706
3/20/17
155,000.00 (G)
3944.020
1.10
0.181
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
9,010.0,p
4,500.00 p
2.14 p
3154
BERMUDAGRASS
3/21/17
192,200.00 (G)
4890.585
1.10
0.224
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
9,010.0,p
4,500.00 p
2.14 p
3154
BERMUDAGRASS
3/22/17
167,400.00 (G)
4259.542
1.10
0.195
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
9,010.0�p
4,500.00 p
2.14 p
3154
BERMUDAGRASS
Mar-17
514,600.00 (G)
13,094.147
4/3/17
248,000.00 (G)
6310.433
1.10
0.289
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
9,010.0-p
4,500.00 p
2.14 p
3114
BERMUDAGRASS
4/5/17
192,200.00 (G)
4890.585
1.10
0.224
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
9,010.0,p
4,500.00 p
2.14 p
3154
BERMUDAGRASS
4/19/17
229,400.00 (G)
5837.150
1.10
0.268
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
9,010.0,p
4,500.00 p
2.14 p
3154
BERMUDAGRASS
4/20/17
223,200.00 (G)
5679.389
1.10
0.261
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
9,010.0,p
4,500.00 p
2.14 p
3114
BERMUDAGRASS
Apr-17
892,800.00 (G)
22,717.557
5/25/17
297,600.00 (G)
7572.519
2.21
0.698
HCUCOHV
DRY
0-<1/2"
SUR
0.5
0.20
6,760.0,p
50.00 p
2.25 p
1379 I
BERMUDAGRASS
5/26/17
223,200.00 (G)
5679.389
2.21
0.523
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
6,760.0,p
50.00 p
2.25 p
1379
BERMUDAGRASS
May-17
520,800.00 (G)
13,251.908
6/6/17
260,400.00 (G)
6625.954
2.21
0.611
HCUCOHV
DRY
0-<1/2"
SUR
0.5
0.20
6,760.0,p
50.00 p
2.25 p
1379
BERMUDAGRASS
6/7/17
136,400.00 (G)
3470.738
2.21
0.320
HCUCOHV
DRY
0-<1/2"
SUR
0.5
0.20
6,760.0-p
50.00 p
2.25 p
1379
BERMUDAGRASS
6/22/17
260,400.00 (G)
6625.954
2.21
0.611
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
6,760.0,p
50.00 p
2.25 p
1379
BERMUDAGRASS
6/23/17
198,400.00 (G)
5048.346
2.21
0.465
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
6,760.0,p
50.00 p
2.25 p
1379
BERMUDAGRASS
Jut-17
855,600.00 (G)
21,770.992
7/19/17
297,600.00 (G)
7572.519
2.21
0.698
HCUCOHV
SUR
0.5
0.20
6,760.0-p
50.00 p
2.25 p
1379 I
BERMUDAGRASS
7/20/17
173,600.00 (G)
4417.303
2.21
0.407
HCUCOHV
SUR
0.5
0.20
6,760.0-p
50.00 p
2.25 p
1379
BERMUDAGRASS
Jul-17
471,200.00 (G)
11,989.822
8/2/17
297,600.00 (G)
7572.519
2.21
0.698
HCUCOHV
SUR
0.5
0.20
6,760.0,p
50.00 p
2.25 p
1379 I
BERMUDAGRASS
8/3/17
173,600.00 (G)
4417.303
2.21
0.407
HCUCOHV
SUR
0.5
0.20
6,760.0-p
50.00 p
2.25 p
1379 Ij
BERMUDAGRASS
8/18/17
260,400.00 (G)
6625,954
2.21
0.611
HCUCOHV
SUR
0.5
0.20
6,760.0,p
50.00 p
2.25 p
1379
BERMUDAGRASS
8/21/17
148,800.00 (G)
3786.260
2.21
0.349
HCUCOHV
SUR
0.5
0.20
6,760.0-p
50.00 p
2.25 p
1379
BERMUDAGRASS
8/23/17
248,000.00 (G)
6310.433
2.21
0.582
HCUCOHV
SUR
0.5
0.20
6,760.0,p
50.00 p
2.25 p
1379
BERMUDAGRASS

CILITY NAME: HARNETT CO. UTILITIES, NC
INER: HARNETT COUNTY
'E #: NC HA OOX43 FIELD# : HA OOX43 0001
SIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: LAKELAND
PERMIT #: WQ0014885 ANNUAL DRY TONS APPLIED: 711.20
OPERATOR: HARNETT COUNTY CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 39.30 ACRES PERMITTED: 39.30
Page
Lime Applied
***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
ATE or
Per
-Residual
Dry, Wet,.,
Past 24
Method '
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
IONTH
Total
Per Acre
Solids
3/24/17
198,400.00 (G)
5048.346
2.21
0.465
HCUCOHV
SUR
0.5
0.20
6,760.0 p
50.00 p
2.25 p
1379
BERMUDAGRASS
3/25/17
210,800.00 (G)
5363.868
2.21
0.494
HCUCOI-N
SUR
0.5
0.20
6,760.0 p
50.00 p
2.25 p
1379
BERMUDAGRASS
3/28/17
179,800.00 (G)
4575.064
2.21
0.422
HCUCOHV
SUR
0.5
0.20
6,760.0 p
50.00 p
2.25 p
1379
BERMUDAGRASS
3/29/17
1-6,400.00 (G)
3470.738
2.21
0.320
HCUCOHV
SUR
0.5
0.20
6,760.0 p
50.00 p
2.25 p
1379
BERMUDAGRASS
A,ug-17
1,853,800.00 (G)
47,170.485
)/18/17
285,200.00 (G)
7256.997
2.10
0.635
HCUCOHV
SUR
0.5
0.20
10,900. p
50.00 p
2.27 p
2207
BERMUDAGRASS
)/19/17
217,000.00 (G).
5521.6281
2.10
0A84
HCUCOHV
SUR
0.5'
0.20
10,900. p
50.00 p
2.27 p
2207
'BERMUDAGRASS
Sep-17
502,200.00 (G)
12,778.625
10/2/17
260,400.00 (G)
6625.954
2.10
0.580
HCUCOHV
SUR
0.5
0.20
10,900. p
50.00 p
2.27 p
2207
BERMUDAGRASS
10/3/17
179,800.00 (G)
4575.064
2.10
0.401
HCUCOHV
SUR
0.5
0.20
10,900. p
50.00 p
2.27 p
2207
BERMUDAGRASS
0/17/17
235,600.00 (G)
5994.911
2.10
0.525
HCUCOHV
SUR
0.5
0.20
10,900. p
50.00 p
2.27 p
2207
BERMUDAGRASS
0/18/17
241,800.00 (G)
6152.672
2.10
0.539
HCUCOHV
SUR
. 0.5
0.20
10,900. p
50.00 p
2.27 p
2207
BERMUDAGRASS
0/31/17
229,400.00 (G)
5837.150
2.10
0.511
HCUCOHV
SUR
0.5
0.20
10,900. p
50.00 p
2.27 p
2207
BERMUDAGRASS
Oct-17
1,147,000.00 (G)
29,185.751
11/1/17
210,800.00 (G)
5363.868
0.60
0.134
HCUCOHV
SUR
0.5
0.20
9,840.0,p
50.00 p
_ 2.38 p
1995
I BERMUDAGRASS
1/16/17
291,400.00 (G)
7414.758
0.60
0.186
HCUCOHV
SUR
0.5
0.20
,9,840.0,p
50.00 p
2.38 p
1995
BERMUDAGRASS
1/17/17
223,200.00 (G)
5679.389
0.60
0.142
HCUCOHV
SUR
0.5
0.20
9,840.0-p
50.00 p
2.38 p
1995
BERMUDAGRASS
1/30/17
235,600.00 '(G)
5994.911
0.60
0.150
HCUCOHV
SUR
0.5
0.20
9,840.0-p
50.00 p
2.38 p
1995
BERMUDAGRASS
Nov-17
961,000.00 (G)
24,452.926
12/1/17
167,400.00 (G)
4259.542.
0.60
0.107
HCUCOHV
SUR
0.5
0.20
9,840.0,p
50.00 p
2.38 p
1995
BERMUDAGRASS
2/18/17
266,600.00 (G)
6783.715
0.60
0.170
HCUCOHV
SUR
0.5
0.20
9,840.0-p
50.00 p
2.38 p
1995
BERMUDAGRASS
2/19/17
223,200.00 (G)
5679.389
0.60
0.142
HCUCOHV
SUR
0.5
0.20
9,840.0-p
50.00 p
2.38 p
1995
BERMUDAGRMS .
Dec-17
657,200.00 (G)
16,722.646

.CILITY NAME: HARNETT CO. UTILITIES, NC
JNER: HARNETT COUNTY
'E #: NC HA OOX43 FIELD# : HA OOX43 0001
'.SIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: LAKELAND
PERMIT #: WQ0014885 ANNUAL DRY TONS APPLIED: 711.20
OPERATOR: HARNETT COUNTY CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 39.30 ACRES PERMITTED: 39.30
Page : 3
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner-
-- -
or Wet Tons (WT) (specify)
ova
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
ATE or
IONTH
Solids
per
Residual
Dry, Wet,
Past 24
Method -
zation
zation
TKN
Nitrogen
and
m
(pp )
Cro p
Total
Per Acre
iorai.vanons/ac:
'OTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
inual lbs/acre
117
0.259
0.072
0.742
6.174
0.417
0.016
0.351
0.337
0.181
2.056
67.74
emulative lbs/acre _
1.440
0.315
5.275
35.647
1.561
0.065 -
1.418
2.334
0.788
16.501
V.
mit PAN Limit (lbs/acre) 1st Crop/2nd Crop
{
° f;
c.
147
34
. J
_..{
Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 1 375.0
89.0
2500.0
J
UCOHWPL = HARNETT CO. UTIL., NC COH REGIONAL WTP LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
I/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate : Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
"ILITY NAME: HARNETT CO. UTILITIES, NC PREDOMINANT SOIL SERIES: GILEAD
NER: JAMES FARRAR PERMIT #: WQ0014885 ANNUAL DRY TONS APPLIED: 44.57
E #: NC HA OX124 FIELD# : HA OX124 0006 OPERATOR: JAMES FARRAR CATION EXCHANGE CAPACITY (NON-503):
3IDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 34.70 ACRES PERMITTED: 34.70
Page: 1
Line Applied ***
Date
Lbs/Ac
kTE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
Per Acre
:ONTH
7/5/17
297,600.00 (G)
8576.369
2.21
0.790
HCUCOHV
SUR
0.5
0.20
6,760.0 p
50.00 p
2.25 p
1379
I BERMUDAGRASS PASTURE
7/6/17
186,000.00 (G)
5360.231
2.21
0.494
HCUCOHV
SUR
0.5
0.20
6,760.0 p
50.00 p
2.25 p
1379
BERMUDAGRASS PASTURE
Jul-17
1 483,600.00 (G)
13,936.600
Total Gallons/Ac: 13,936.60
'OTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
nual lbs/acre
4
0.008
0.005
0.066
0.216
0.032
0.001
0.022
0.027
0.013
0.227
5.01
mulative lbs/acre
0.078
0.017
0.248
2.100
0.078
0.003
0.091
0.117
0.043
1.192
nit PAN Limit (lbs/acre) 1st Crop/2nd Crop
120
Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
,UCOHWPL = HARNETT CO. UTIL., NC COH REGIONAL WTP LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
UA = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

:�ILITY NAME: HARNETT CO. UTILITIES, NC
NER: CARL HAMILTON, JR.
E #: NC HA OX201 FIELD# : HA OX201 0004
SIDUAL SOURCE(S):* See list at bottom of report -
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: WAHEE FINE SANDY LOAM
PERMIT #: W00014885 ANNUAL DRY TONS APPLIED: 41.71
OPERATOR: CARL HAMILTON, JR. CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 85.10 ACRES PERMITTED: 85.10
Page
Lime Applied ***
Date
Lbs/Ac
kTE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
ode
Solids
Dry
Tons
per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
Per Acre
:ONTH
5/9/17
266,600.00 (G)
3132.785
2.21
0.289
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
6,760.0 p
50.00 p
2.25 p
1379
SOYBEANS
/10/17
18G,000.00 (G)
2185.664
2.21
0.201
HCUCOHV
MOIST
0-<1/2"
SUR
0.5
0.20
6,760.0 p
50.00 p
2.25 p
1379
SOYBEANS
4ay-17
1 452,600.00 (G)
5,318.449
Total Gallons/Ac: 5,318.45
'OTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
nuallbs/acre
1
0.003
0.002
0.025
0.082
0.012
<.001
0.008
0.010
0.005
0.087
1.91
mulative Ibs/acre
0.012
0.003
0.139
0.814
0.033
<.001
0.012
0.063
0.007
0.289
1`
nit PAN Limit (lbs/acre) Ist Crop/2nd Crop
`
�;
} ;
I
! 3 }
4L
{ 1
161
k }
k
lk
Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
to
1339.0
267.9
15.0 375.0
89.0
2500.0
}
:UCOHWPL = HARNETT CO. UTIL., NC COH REGIONAL WTP LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was, prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
YA = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

Summit Environmental Technologies, Inc.
3310'Win St.
tt{;�InC�tJfdEN9'ALY�r±t4L�c!_;;nte Cuyahoga Falls,'Ohio 44223
/Arralyttaffl LFi6arator't@S TEL: [phone] FAX. [phone]
Website: ham://wwwsettekcom
March 2% 2017.
Will Varner
-Synagro
284 Boger Rd.
Mocksville, NC 27028 .
TEL: [phone]
FAX: [phone]
RE: Harnett County
Dear Will Varner: - Order No.: 17031002
Summit Environmental Technologies, Inc. received 2 sample(s) on 3/17/2017 for the
analyses presented in the following report. ;
There were no problems, with the analytical eventsassociated with this report unless noted
in the Case Narrative.
.Quality control data is within laboratory defined or method specified acceptance limits .
except where noted..
If you have any questions'regarding these tests results, please feel free to call the
laboratory;
Sincerely; '
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223, -
Alabama 41600, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NEL•AC E87688, Georgia E87688, Idaho
' OH00923, Illinois 200061, Indiana C-OH-13, Kansas 510347, Kentucky (Underground Storage Tank) 3, Kentucky 9014.6, Louisiana 04061, Maryland
339, Massachusetts M-OPH923, Minnesota 409711, New Hampshire 2996, New Jersey OH006, New Yoik 11777, NortCarolina 39705 and 631, North
Dakota R-201, Ohio Drinking Water 4110, Ohio VAP CL0052, Oklahoma 9940, Oregon OH2O0001, Rhode Island LA000317, South Carolina 92016001,
Texas T104704466-11-5, Region 8 8TMS-L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581,
Washington C891, West Virginia 9957C
Page 1 of 41
Page 1 of 59

Summit Environmental Technologies, Inc. Case Narrative
SumMIT 3310 Win St.
FifVIROt4blEhl'rAL'IECHtZOLOG1ES, trtc. Cuyahoga Falls, Ohio 44223 WO#: 17031002
first, tical Lbharsfories TEL: [phone] FAX: [phone]
Website: hYR.-11vwiv.settek.com Date: 3/29/2017
CLIENT: Synagro
Project: Harnett County
WorkOrder Narrative:
17031002: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certif cations listed at the bottom of
the cover letter that may or, may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as' applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not certified."
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report -was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis.unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence QC Comments:
ccv l Oppb c0313/ 1106706: Analytical Comments for voc-mstr,npw(8260), Sample ccv l Oppb c0313/,
Batch ID R67087 : The VOC CCV (Batch R67087) exhibited high recovery for Acetone and low
recovery for Dichlorodifluoromethane; All samples were ND. All Method -Specified CCCs and SPCCs
exhibited control. DETL check shows adequate sensitivity.
LCS-26053 1107336: Analytical Comments for SVOC-BNA_TCLP(8270), Sample LCS-26053, Batch
ID 26053 : All surrogates failed to meet acceptance criteria. Recovery for all analytes were within
acceptance range.
Original
Page 2 of 41
Page 2 of 59

Summit Environmental Technologies, In SumMIT 3310 Win 8 Qualifiers and Acronyms
etSVIzONf�tEri1TAL Tt Gi .r�Lo�i_5, rMC. Cuyahoga Falls, Ohio 4421 WO#: .17031002
Aralyiieai Lahonlio ies TEL: [phone] FAX.- (330) 253-445
Website: htty.-1Avxnv.settekeo. Date:_ 3/29/2017
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
i
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
inManual integration was used to determine the area response.
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference. -
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD. was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits..
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLv1
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for.any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 41
Page 3 of 59

Summit Environmental Technologies, Inc.
Workorder
su
3310Win St.
Cuyahoga Falls, Ohio 44223
aul P Summary
Sample
E bVIROtJL1ENTAL �cCi'h10LlZG:25, INC.
Amilytical. Lsboraiprle
TEL: [phone] FAX.- [phone]
WO#: 17031002
Website:,l Q.-lAyimsettek.COm
29 Mar-17
CLIENT:
Synagro
Project:
Harnett County
Lab SamplelD Client Sample ID Tag No Date Collected
Date Received Matrix
17031002-001
North Harnett
3/16/2017 3:00:00 PM
3/17/2017 8:00:00 AM Sludge
17031002-002
Harnett WTP
3/16/2017 2:45:00 PM
3/17/2017 8:00:00 AM Sludge
Page 4 of 41
Page 4 of 59

SULMIMT
Summit Environmental Technologies, Inc.DATESREPORT
3310 Win St.
Ersviu0 N?404raL u FCHNouDGIES, WC.
Cuyahoga Falls, Ohio 44223
WO#: 17031002
q
A nall-WaHl Lebs AWDrIo5
TEL: [phone] FAX. [phone]
Website: htW.,11wwi4,.settelc.com
29 Mar-17
Client:
Synagro
Project:
Harnett County
Sample ID.
Client Sample ID Collection Date Matrix Test Name Leachate Date
Prep Date
Analysis Date
17031002-001A North Harnett 3/16/2017 3:00:00 PM Sludge Ignitability of Solids (SW-846: 1030)
3/23/2017 8:00:00 AM
pH (SW9045D)
3/22/2017 4:15:00 PM
Reactive Cyanide (9014/7.3.3.2)-Solid
3/22/2017 1:05:00 PM
Reactive Sulfide (9034)
.3/22/2017 1:05:00 PM
SVOC 8270 TCLP BNA List 3/20/2017 3:17:13 PM
3/21/2017 7:00:00 AM
3/22/2017.4:14:00 PM
SVOC SW-846: 8081-TCLP Pesticide,,3/20/2017 3:17:13 PM
3/21/2017 7`:30:00 AM
3/22/2017 3:26:00 PM
SVOC SW-846: 8151 Herbicides-TCL
3/21/2017 5:00:00 PM
3/23/2017 7:07:00 PM
TCLP Mercury Analysis (1311/7470) 3/20/2017 3:17:13 PM
3/21/2017 10:30:00 A
�R
3/21/2017 4:38:00 PM
TCLP Metals Analysis (6010) 3/20/2017 3:17:13 PM
3/21/2017 10:05:11 A
�R
3/24/2017 1:33:23 PM
VOC by GUMS (8260)-TCLP
3/21/2017 6:23:00 PM
17031002-002A
Harnett WTP 3/16/2017 2:45:00 PM Flashpoint Determination (1010)
3/20/201712:43:46 PM
Ignitabilityof Solids (SW-846: 1030)
3/23/2017 8:00:00 AM
pH (SW9045D)
3/22/2017 4:21:00 PM
Reactive Cyanide (9014/7.3.3.2)-Solid
3/22/2017 1:05:00 PM
Reactive Sulfide (9034) "
3/22/2017 1:05:00 PM
SVOC 8270 TCLP BNA List 3/20/2017 3:17:13 PM
3/21/2017 7:00:00 AM
3/22/2017 4:49:00 PM
SVOC SW-846: 8081-TCLP Pesticide., 3/20/2017 3:17:13 PM
3/21/2017 7:30:00 AM
3/22/2017 3:53:00 PM
SVOC SW-846: 8151 Herbicides-TCL
3/21/2017 5:00:00 PM
3/23/2017 7:40:00 PM
TCLP Mercury Analysis (1311/7470) 3/20/2017 3:17:13 PM
3/21/2017 10:30:00 A
3/21/2017 4:47:00 PM
TCLP Metals Analysis (6010) 3/20/2017 3:17:13 PM
3/21/2017 10:05:11 A
3/24/2017 1:33:23 PM
VOC by GUMS (8260)-TCLP
r�
3/21/2017 6:49:00 PM
Original
Page 5 of 41
Page 5 of 59

rnsu
rKVIRONh1EN'PA.LTECHNOLOGtr:S,tt_
Aralytical.Lsheraforles
SummitEnvironmentalTechnologies,Inc.
3310 Win St.
Cuyahoga Falls, Ohio44223
TEL: [phone] FAX: [phone]
Analytical Report
(base report)
WO#: 17031002
Website: hitp.Avxnv.settek.com
Date Reported: 3/29/2017
CLIENT:
Synagro
Tag Number:
Matrix:
SLUDGE
Collection Date:
3/16/2017 3:00:00 PM
Lab ID:
17031002-001A
Project:
Harnett County
Client Sample ID North Harnett
,
Analyses
Result
RL Qual
Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW7470A
SW7470A Analyst: ALJ
TCLP MERCURY ANALYSIS (1311/7470)
TCLP Mercury
ND
0.00200
mg/L
1
3/21/20174:38:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW6010C
SW3010A
Analyst: VVK
TCLP METALS ANALYSIS (6010)
TCLP Arsenic(As)
ND
0.500
mg/L
1
3/24/2017 1:33:23 PM
TCLP Barium(Ba)
ND
5.00
mg/L
1
3/24/2017 1:33:23 PM
TCLP Cadmium(Cd)
ND
0.100
mg/L
'1
3/24/2017 1:33:23 PM
TCLP Chromium(Cr)
ND
0.200
mg/L
1
3/24/2017 1:33:23 PM
TCLP Lead(Pb)
ND
0.500
mg/L
1
3/24/2017 1:33:23 PM
TCLP Selenium(Se)
ND
0.500
mg/L
1
3/24/2017 1:33:23 PM
TCLP Silver(Ag)
ND
0.500
mg/L
1
3/24/2017 1:33:23 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270C
SW3510C Analyst: CxA
SVOC 8270 TCLP BNA LIST
1,4-Dichlorobenzene
ND
0.0800
mg/L
2
3/22/2017 4:14:00 PM
2,4,5-Trichlorophenol
ND
0.200
mg/L
2
3/22/2017 4:14:00 PM
2,4,6-Trichlorophenol
ND
0.200
mg/L
2
3/22/2017 4:14:00 PM
2,4-Dinitrotoluene
ND
0.100
mg/L
2
3/22/2017 4:14:00 PM
Cresols, Total,
ND
4.00
mg/L
2
3/22/2017 4:14:00 PM
Hexachloro-1,3-butadiene
ND
0.100
mg/L
2
3/22/20174:14:00PM
Hexachlorobenzene
ND
0.100
mg/L
2
3/22/2017 4:14:00 PM
Hexachloroethane
ND
0.0800
mg/L
2
3/22/2017 4:14:00 PM
Nitrobenzene ,
ND
0.0800
mg/L
2
3/22/2017 4:14:00 PM
Pentachlorophenol
ND
0.200
mg/L
2
3/22/2017 4:14:00 PM
Pyridine
ND
0.200
mg/L
2
3/22/2017 4:14:00 PM
Surr: 2-Fluorophenol
72.4
10 - 109
%Rec
2
3/22/2017 4:14:00 PM
Surr: Phenol-d6
75.2
10 - 109
%Rec
2
3/22/2017 4:14:00 PM
Surr: Nitrobenzene-d5
84.2
19 - 120
%Rec.
2
3/22/2017 4:14:00 PM
Surr: 2,4,6-Tribromophenol
84.1
10 - 120
%Rec
2
3/22/2017 4:14:00 PM
Surr: 2-Fluorobiphenyl
82.1
22 -'117
%Rec
2
3/22/2017 4:14:00 PM
Surr: p-Terphenyl-d14
88.7
34 - 116
%Rec
2
3/22/2017 4:14:00 PM
Qualifiers: *
Value exceeds Maximum Contaminant Level.
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound Limit.
N
Tentatively identified compounds
ND
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit ,
P
Second column.confirmation exceeds
PL
Permit Limit Original
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 6 of 59

S U1
Summit Environmental Technologies, Inc.
3310Win St.
Analytical Report
V E IRONh1EW"AIGPt L=-!0LlGIES:Nq.
Cuyahoga Falls; Ohio 44223
(base report)
Arralyticsl Lzbaraiarie5
TEL: (330)
253-8211 FAX: [phone]
WO#: 17031002
Website: http:/hwww.settek.com
Date Reported: 3/29/2017
CLIENT: Synagro
Tag Number:
Matrix: SLUDGE
Collection Date:
3/16/2017 3:00:00 PM
Lab ID: 17031002-OOIA
Project: Harnett County
Client Sample ID North Harnett
Analyses Result
RL
Qual Units
DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8081A
SW3510C Analyst: JBN
SVOC SW-846: 8081-TCLP PESTICIDES
Chlordane, total .
ND
0.0100
mg/L
1 3/22/2017 3:26:00 PM
Toxaphene
ND
0.0200
mg/L
1 3/22/2017 3:26:00 PM
Endrin
ND
0.00100
mg/L
1 3/22/2017 3:26:00 PM
gamma-BHC
ND
0.00100
mg/L
1 3/22/2017 3:26:00 PM
Heptachlor
ND
0.00100
mg/L
1 3/22/2017 3:26:00 PM
Heptachlor epoxide
ND
0.00100
mg/L
1 3/22/2017 3:26:00 PM
Methoxychlor
ND
0.00100
mg/L
1 3/22/2017 3:26:00 PM
Surr: TCMX
67.9
10 - 119
%Rec
1 3/22/2017 3:26:00 PM
Surr: DCB
66.7
10 - 119
%Rec
1 3/22/2017 3:26:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8151A
SW8151A Analyst: JBN
SVOC SW-846: 8151 HERBICIDES-TCLP
2,4-D
ND
11.3
mg/L
1 3/23/2017 7:07:00 PM
2,4,5-TP
ND
11.3
mg/L
1 3/23/2017 7:07:00 PM
Surr: 2,4-Dichlorophenylacetic aci
84.3
20 - 140
%Rec
1 3/23/2017 7:07:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260B
Analyst: MES
VOC BY GC/MS (8260)-TCLP
1,1-Dichloroethene
ND
0.100
mg/L
1 3/21/2017 6:23:00 PM
1,2-Dichloroethane
ND
0.100
mg/L
1 3/21/2017 6:23:00 PM
MEK
5.82
2.00
mg/L
1 3/21/2017 6:23:00 PM
Benzene
ND
0.100
mg/L
1 3/21/2017 6:23:00 PM
Carbon tetrachloride
ND
0.100
mg/L
1 3/21/2017 6:23:00 PM
Chlorobenzene
ND
0.100
mg/L
1 3/21/2017 6:23:00 PM
Chloroform
ND
0.100
mg/L
1 3/21/2017 6:23:00 PM
Tetrachloroethene
ND
0.100
mg/L
1 3/21/2017 6:23:00 PM
Trichloroethene
ND
0.100
mg/L
1 3/21/2017 6:23:00 PM
Vinyl chloride
ND
0.200
mg/L '
1 3/21/2017 6:23:00 PM
Surr: 4-Bromofluorobenzene
98.9
70'- 130
%Rec
1 3/21/2017 6:23:00 PM
Surr: Dibromofluoromethane
97.9
70 - 130
%Rec
1 3/21/2017 6:23:00 PM
Surr: Toluene-d8
84.2
70 - 130
%Rec
1 3/21/2017 6:23:00 PM
Qualifiers: * Value exceeds Maximum Contaminant Level.
E Value above quantitation range
H Holding times for preparation or analysis exceeded
M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified compounds
ND Not Detected at the Reporting Limit
O RSD is greater than RSDlimit
P Second column Confirmation exceeds
PL Permit Limit
Original
R RPD outside accepted recovery limits
RL Reporting Detection Limit
Page 7 of 59

_ l
S' M'
Summit Environmental Technologies, Inc.
3310 Win St.
Analytical Report
ruviRommEwrAL1EC-PN5LGG:c5;WC.
Cuyahoga Falls, Ohio44223
(base report)
Arrai rtieal Lbharaiories
TEL: [phone] FA;E- [phone]
WO#: 17031002
Website: hM2://www.settekcom
Date Reported: 3/29/2017
CLIENT:
Synagro.
Tag Number:
Matrix:
SLUDGE
Collection Date:
3/16/2017 3:00:00 PM
Lab ED:
17031002-001A
Project:
Harnett County
Client Sample ID North Harnett
Analyses
Result RL Qual Units
DF Date Analyzed
RCI
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive ND
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability Non-flammable.
RCI
PH (SW9045D)
pH 7.6
RCI
REACTIVE SULFIDE (9034)
Sulfide, Reactive 90.0
0.500
Qualifiers:
* Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
P Second column confirmation exceeds
R RPD outside accepted recovery limits
25.0
SW9014
Analyst: MS
mg/Kg
1
3/22/2017 1:05:00 PM.
SW1030
Analyst: RMT
-1
3/23/2017 8:00:00 AM
SW9045D
- Analyst: DHC
s.u,@19.9C
1
'3/22/2017 4:15:00 PM
SW9034 '
Analyst: MS
mg/Kg
1
3/22/2017 1:05:00 PM
E Value above quantitation range.
M Manual Integrationused to determine area response
N Tentatively identified compounds
O RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 8 of 59

Summit Environmental Technologies, Inc.
3310 Win St. Analytical Report
re
rWVIR0Nh1EN`rAL TECHNOLOGIES. 4rtq, Cuyahoga Falls, Ohio 44223 (base report)
)
Araryf ral L borafories TEL: [phone] FAX. [phone] WO#: 17031002
Website: hW.-1Avwiv.settekcom Date Reported: 3/29/2017
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 3/16/2017 2:45:00 PM
Lab ID: 17031002-002A
Project: Harnett County
Client Sample ID Harnett WTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP MERCURY ANALYSIS (131117470)
TCLP Mercury ND
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP METALS ANALYSIS (6010)
TCLP Arsenic(As)
ND
TCLP Barium(Ba)
ND
TCLP Cadmium(Cd)
ND
TCLP Chromium(Cr)
ND
TCLP Lead(Pb)
ND
TCLP Selenium(Se)
ND
TCLP Silver(Ag)
ND
RCI
FLASHPOINT DETERMINATION (1010)
Flashpoint (140°F) >140
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SVOC 8270 TCLP BNA LIST
1,4-Dichlorobenzene
ND
2,4,5-Trichlorophenol
ND
2,4,6-Trichlorophenol
ND,
2,4-Dinitrotoluene
ND
Cresols, Total
ND
Hexachloro-1,3-butadiene
ND
Hexachlorobenzene
ND
Hexachloroethane
ND
Nitrobenzene
ND
Pentachlorophenol
ND
Pyridine
ND
Surr: 2-Fluorophenol
69.8
Surr: Phenol-d6
72.1
Surr: Nitrobenzene-d5
88.1
SW7470A SW7470A Analyst: ALJ
0.00200
mg/L
1
3/21/2017 4:47:00 PM
SW6010C
SW3010A Analyst: VVK
0.500
mg/L
1
3/24/2017 1:33:23 PM
5.00
mg/L
1
3/24/2017 1:33:23 PM
0.100
mg/L
1
3/24/2017 1:33:23 PM
0.200
mg/L
1
3/24/2017 1:33:23 PM
0.500,
mg/L
1
3/24/2017 1:33:23 PM
0.500
mg/L
1
3/24/2017 1:33:23 PM
0.500
mg/L
1
3/24/2017 1:33:23 PM
SW1010 Analyst: TAH
°F 1 3/20/2017 12:43:46 PM
SW82700 SW3510C Analyst: CxA
0.0800
mg/L
2
3/22/2017 4:49:00 PM
0.200
mg/L
2
3/22/2017 4:49:00 PM
0.200
mg/L
2
3/22/2017 4:49:00 PM
0.100
mg/L
2
3/22/2017 4:49:00 PM
4.00
mg/L
2
3/22/2017 4:49:00 PM
0.100
mg/L
2
3/22/2017 4:49:00 PM
0.100
mg/L
2
3/22/2017 4:49:00 PM
0.0800
mg/L
2
3/22/2017 4:49:00 PM
0.0800
mg/L
2
3/22/2017 4:49:00 PM
0.200
mg/L
2
3/22/2017 4:49:00 PM
0.200
mg/L
2
3/22/2017 4:49:00 PM
10 - 109
%Rec
2
3/22/2017 4:49:00 PM
10 - 109
%Rec
2
3/22/2017 4:49:00 PM
19 - 120
%Rec
2
3/22/2017 4:49:00 PM
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
P Second column confirmation exceeds
R RPD outside accepted recovery limits
E Value above quantitation range -
M Manual Integration used to determine area response
N Tentatively identified compounds
0 RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 9 of 59

sumfort
Summit Environmental Technologies, Inc. Analytical Report
3310 Win St.
c=i{'JIRONP,IEN'�kL=1 tirSLaG�cS,,rtc. Cuyahoga Falls, Ohio44223 (basereport)
Arrafyticsf L. horaiDrle5 TEL: [phone] FAX. [phone] WO#: 17031002
Website: hQ.*1A9ivw.settekcom Date Reported: 3/29/2017
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 3/16/2017 2:45:00 PM
Lab ID: 17031002-002A
Project: Harnett County
Client Sample ID Harnett WTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270C
SW3510C Analyst: CxA
SVOC 8270 TCLP BNA LIST
Surr: 2,4,6-Tribromophenol 56.3
10 - 120
%Rec
2 3/22/2017 4:49:00 PM
Surr: 2-Fluorobiphenyl 80.0
22 - 117
%Rec
2 3/22/2017 4:49:00 PM
Surr: p-Terphenyl-d14 95.0
34 - 116
%Rec
2 3/22/2017 4:49:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8081A
SW3510C Analyst: JBN
SVOC SW=846: 8081-TCLP PESTICIDES
Chlordane, total ND
0.0100
mg/L
1 3/22/2017 3:53:00 PM
Toxaphene ND
0.0200
mg/L
1 3/22/2017 3:53:00 PM
Endrin ND
0.00100
mg/L
1 3/22/2017 3:53:00 PM
gamma-BHC ND
0.00100
mg/L
1 3/22/2017 3:53:00 PM
Heptachlor ND
0.00100
mg/L
1 3/22/2017 3:53:00 PM
Heptachlor epoxide ND
0.00100
mg/L
1 3/22/2017 3:53:00 PM
Methoxychlor ND
0.00100
mg/L
1 3/22/2017 3:53:00 PM
Surr: TCMX 71.3
10 - 119
%Rec
1 3/22/2017 3:53:00 PM
Surr: DCB 73.5
10 - 119
%Rec
1 3/22/2017 3:53:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8151A
SW8151A Analyst: JBN
SVOC SW-846: 8151 HERBICIDES-TCLP
2,4-D ND
11.3
mg/L
1 3/23/2017 7:40:00 PM
2,4,5-TP ND
11.3
mg/L
1 3/23/2017 7:40:00 PM
Surr: 2,4-Dichlorophenylacetic ad 72.3
20 - 140
%Rec
1 3/23/2017 7:40:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260B
Analyst: MES
VOC BY GC/MS (8260)-TCLP
M-Dichloroethene ND
0.100
mg/L
1 3/21/2017 6:49:00 PM
1,2-Dichloroethane ND
0.100
mg/L
1 3/21/2017 6:49:00 PM
MEK ND
2.00
mg/L
1 3/21/2017 6:49:00 PM
Benzene ND
0.100
mg/L
1 3/21/2017 6:49:00 PM
Carbon tetrachloride ND
0.100
mg/L
1 3/21/2017 6:49:00 PM
Chlorobenzene ND
0.100
mg/L
1 3/21/2017 6:49:00 PM
Chloroform ND
0.100
mg/L
1 3/21/2017 6:49:00 PM
Tetrachlotoethene ND
0.100
mg/L
1 3/21/2017 6:49:00 PM
Qualifiers: * Value exceeds Maximum Contaminant Level.
E Value above quantitation range
H Holding times for preparation or analysis exceeded
M Manual Integration
used to determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified compounds
ND Not Detected at the Reporting Limit
0 RSD is greater than RSDlimit
P Second column confirmation exceeds
PL Permit Limit
Original
R RPD outside accepted recovery limits
RL Reporting Detection Limit
Page 10 of 59

Summit Environmental Technologies, Inc.MSUMM111 3310 Win St. Analytical Report
Ei 9RaNhlEtdTAL12CiJ 0L4Gt_S,9PtC. Cuyahoga Falls, Ohio44223 (basereport)
h.nzijrtisFrl Lsharaigrle4 TEL: [phone] FAX: [phone] WO#: 17031002
Website: hQ.1liviviv.settek.com Date Reported: 3/29/2017
CLIENT: Synagro
Tag Number:
Matrix: SLUDGE
Collection Date:
3/16/2017
2:45:00 PM
Lab ID: 17031002-002A
Project: Harnett County
Client Sample ID Harnett WTP
Analyses
Result
RL
Qual Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260B
Analyst: MES
VOC BY GC/MS (8260)-TCLP
Trichloroethene
ND
0.100
mg/L
1
3/21/2017 6:49:00 PM
Vinyl chloride
ND
0.200
mg/L
1
3/21/2017 6:49:00 PM
Surr: 4-Bromofluorobenzene
87.9'
70 - 130
%Rec
1
3/21/2017 6:49:00 PM
Surr: Dibromofluoromethane
97.9
70 - 130
%Rec
1
3/21/2017 6:49:00 PM
Sum Toluene-d8
83.8
70 - 130
%Rec
1
3/21/2017 6:49:00 PM
RCI
SW9014
Analyst: MS
REACTIVE CYANIDE (901417.3:3.2)-SOLID
Cyanide, Reactive
ND
0.500
mg/Kg
1
3/22/2017 1:05:00 PM
IGNITABILITY OF SOLIDS (SW-846: 1030)
SW1030
Analyst: RMT
Ignitability Non-flammable. 1 3/23/2017 8:00:00 AM
RCI SW9045D Analyst: DHC
PH (SW9045D)
pH 5.3 s.u.@19:2C 1 3/22/2017 4:21:00 PM
RCI SW9034 Analyst: MS
REACTIVE SULFIDE (9034)
Sulfide, Reactive 30.0 25:0 mg/Kg 1 3/22/2017 1:05:00 PM
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
P Second column confirmation exceeds
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
O RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 11 of 59

'
Summit Environmental Technologies,
10 Win SStt.
3310
QC SUMMARY REPORT
tray IRU;N roll. N I Al. o'LUH?4QLU0R:S. INC.
Cuyahoga Falls, Ohio 44223
WO#: 17031002
�6ndtlrN:c+�l CrTaaP �to,� f r
TEL: [phone]-FAX.• [phone]
Website: hW.-11www.se1tekcon:
29 Mar-17
Client:
Synagro
Project:
Harnett County
BatchID: 260.44
Sample ID 17031057-003AMS
SampType: MS
TestCode:: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 3/21/2017
RunNo: 67088
client ID: BatchQC
Batch ID: 26044
TestNo: SW6010C SW3010A
Analysis Date: 3/22/2017
SegNo: 1107257
knalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
2.37
0.500
2.000
0
119
70
130
TCLP Barium(Ba)
ND
5.00
2.000
0.2377
101
70
130
TCLP Cadmium(Cd)
2.16
0.100
2.000
0
108
70
130
TCLP Chromium(Cr)
2.00
0.200
2.000
0
99.9
70
130
TCLP Lead(Pb)
2.08
0.500
2.000
0
104
70
130
TCLP Selenium(Se)
2.48
0.500
2.000
0
124
70
130
TCLP Silver(Ag)
1.08
0.500
1.000
0
108
70
130
Sample ID 17031057-003AMSD
SampType: MSD
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 3/21/2017
RunNo: 67088
client ID: BatchQC
Batch ID: 26044-
TestNo: SW6010C SW3010A
Analysis Date: 3/22/2017
SegNo: 1107258
4nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
2.33
0.500
2.000 0 117
70
130
2.374 1.83
20
TCLP Barium(Ba)
ND
5.00
2.000 0.2377 97.3
70
130
0 0
20
TCLP Cadmium(Cd)
2.11
0.100
2.000 0 106
70
130
2.164 2.38
20
TCLP Chromium(Cr)
1.94
0.200
2.000 0 -97.0
70
130
1.998 2.89
20
TCLP Lead(Pb)
2.03
.0.500
2.000 0 102
70
130
2.078 2.29
20
TCLP Selenium(Se)
2.42
0.500
2.000 0 121
70
130
2.483 2.69
20
TCLP Silver(Ag)
1.05
0.500
1.000 0 105
70
130
1.083 2.90
20
Qualifiers:' *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
Original
MC
Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
0
RSA is greater than RSDlimit
P
Second column confim�ation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Page 12 of 41
Page 12 of 59

Summit Environmental Technologies, Inc.ffl . QC SUMMARY REPORT
S�, , NA MIT Win St.
tr vIKra+rttm:NIAl. I1-.0 T%1FJ t o1!:s, Jrgc. Cuyahoga Falls, Ohio44223 WO#: 17031002
<4rta?yPi.cal Laborstnrieg TEL: [phone] FAX- [phone]
Website: hup.-Mvwiv.settek conz 29 Mar-17
Client: Synagro
Project: Haniett County Batchll): 26044
iample ID MB-26044
SampType: MBLK
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 3/21/2017
RunNo: 67033
;lient ID: PBW
Batch ID: 26044
TestNo: SW6010C SW3010A
Analysis Date: 3/21/2017
SegNo: 1106632
\nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual _
TCLP Arsenic(As)
ND
0.500
TCLP Barium(Ba)
ND
5.00
TCLP Cadmium(Cd)
ND
0.100
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pb)
ND
0.500
TCLP Selenium(Se)
ND
0.500
TCLP Silver(Ag)
ND
0.500
Sample ID LCS-26044
SampType: LCS
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 3/2112017
RunNo: 67033
client ID: LCSW
Batch'ID: 26044
TestNo: SW6010C SW3010A
Analysis Date: 3/2112017
SegNo: 1106633
\nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
2.06
0.500
2.000
0
103
80
120
TCLP Barium(Ba)
ND
5.00
2.000
0
102
80
120
TCLP Cadmium(Cd)
1..98
0.100
2.000-
0
98.9
80
120
TCLP Chromium(Cr)
1.99
0.200
2.000
0
99.6
80
120
TCLP Lead(Pb)
1.96
0.500
2.000
0
98.0
80
120
TCLP Selenium(Se)
1.98
0.500
2.000
0
98.8
80
120
TCLP Silver(Ag)
1.02
0.500
1.000
0
102
80
120
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column conPrmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 13 of 41
Page 13 of 59

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
sual-ally 3310 Win St.
tMW I HVIN TA I., N IAl. I GJINULUCnU:S, ir(C. Cuyahoga Falls, Ohio 44223 WO#: 17031002
11,.ralyf1.caf Lzborwories TEL: [phone] FAX. [phone]
Website: hap:/hviviv.settek.com 29 Mar-17
Client:. Synagro
Project: Harnett County BatchID: 26052
Sample ID mb-26052
SampType: mblk
TestCode: telp-svoc-cpe Units: mg/L
Prep Date: 3/21/2b
RunNo: 67143
Client ID: PBW
Batch ID: 26052
TestNo: SW8081A SW3510C
Analysis Date: 3/22/2017
SegNo: 1107621
Analyte
Result
PQL SPK value SPK.Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, total
ND
0.00500 -
Toxaphene
ND
0.0100
Endrin
ND
0.000500
gamma-BHC
ND-
0.000500
Heptachlor.
ND
0.000500
Heptachlor epoxide
ND
0.000500
Methoxychlor
ND
OA00500
Surr: TCMX
6.06
10.00 60.6 10 119
Surr: DCB
7.58
10.00 75.8 10 119
Sample ID Ics-26052
SampType: Ics
TestCode: tclp-svoc-cpe Units: mg/L
Prep Date: _ 3/21/2017
RunNo: 67143
Client ID: LCSW
Batch.ID: 26052
TestNo: SW8081A SW3510C
Analysis Date: 312212017
SegNo: 1107622
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Endrin
0.00361
0.000500
0.00500
0
72.2
20
157
gamma-BHC
0.00301
0.000500
0.00500
0
60.2
22
137
Heptachlor
0.00350
0.000500
0.00500
0
70.1
24
121
Heptachlor epoxide
0.00363
0.000500
0.00500
0
72.6
27
152
Methoxychlor
0.00354
0.000500
0.00500
0
70.8
10
199
Surr: TCMX
6.05
10.00
60.5
10
119
Surr: DCB
7.60
10.00
76.0
10
119
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding tunes for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Jntegration used to.determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 14 of 41
Page 14 of 59

•
Summit Environmental Technologies, Inc.
3310 i�Vin St.
QC SUMMARY -REPORT
cra%11KVzNrnt;NIAl. Iht"uULDJILS,lrtc.
Cuyahoga Falls, Ohio44223
.
WO#: 17031002
F1 Tdt4dt.paP C>xhpr�tarle5 TEL: [phone] FAY.- [phone]
Website: httn:/Awww.settekcom
29 Mar-17
Client:
Synagro
Project:
Harnett County
BatehID: 26052
Sample ID 17031002-001ams
SampType: ms
TestCode: tclp-svoc-cpe Units: mg/L
Prep Date: 3/21/2017
RunNo: 67143
Client -ID: North Harnett
Batch ID: 26052
TestNo: SW8081A SW3510C
Analysis Date: 3/22/2017
SegNo: 1107623
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
0.00861
0.00100
0.0100
0
86.1
20 _
157
gamma-BHC
0.00729
0.00100
0.0100
0
72.9
22
137
Heptachlor
0.00862
0.00100
0.0100
0
86.2
24
121
Heptachlor epoxide
0.00889
0.00100
0.0100
0
88.9
27
152
Methoxychlor
0.00920
0.00100
0.0100.
0
92.0
10
199
Surr: TCMX
15.3
20.00
76.4
10
119
Surr: DCB
13.4
20.00
66.8
10
119
Sample ID 17031002-001amsd
SampType: msd
TestCode: tclp-svoc-cpe Units: mg/L
Prep Date: 3/21/2017
RunNo: 67143
Client ID: North Harnett
Batch ID: 26052
TestNo: SW8081A SW3510C
Analysis Date: 3/22/2017
SegNo: 1107624
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val '
%RPD RPDLimit Qual
Endrin
0.00998
0.00100
0.0100
0
99.8
20
157
0.00861
14.8
30
gamma-BHC
0.00852
0.00100
0.0100
0
85.2
22
137
0.00729
15.5
30
Heptachlor
0.00997
0.00100
0.0100
0
99.7
24
121
0.00862
14.5
30
Heptachlor epoxide
0.0101
0.00100
0.0100
0
101
27
152
0.00889
12.8
30
Methoxychlor
0.00989
o'Aio0
0.0100
0
98.9
10
199
0.00920
7.25
30
Surr: TCMX
19.6
20.00
98.2
10 •
119
0
Surr: DCB
18.0
20.00
90.0
10
119
0
Qualifiers: k Value exceeds Maximum Contaminant Level. B. Analyte detected in the associated Method Blank E Value above quantitation range
H . Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original.
P 'Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 15 of 41
Page 15 of 59

MSUIASummit
R 17-
Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
LNNIH �°N6UaNIai., Uhi:KNULUUJ1'S:INC
Cuyahoga Falls, Ohio44223
Vd0#: 17031002
Analyll.ral Lfiihnr�ia,-lei
TEL: [phone] FAX. [phone]
Website: http✓hvivw.settelccom
29 Mar-17
Client:
Synagro .
Project:
Harnett County
BatchED: 26053
iample ID MB-26053
SampType: MBLK
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 3/21/2017
RunNo: 67126
:lient ID: PBW
Batch ID: 26053
TestNo: SW8270C SW3510C
Analysis Date: 3122/2017
SegNo: 1107335
analyte
Result
PQL SPK value SPK Ref Val
%REC . Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
ND
0.o20o
2,4,5-Trichlorophenol
ND
0.0500
2,4,6-Trichlorophenol
ND
0.0500
2,4-Dinitrotoluene
ND
0.0100
o-Cresol"
ND
0.0500
m/p-Cresol(s)
ND
D.0500
Cresols, Total
ND
1.00
Hexachloro-1,3-butadiene
ND
0.00400
Hexachlorobenzene
ND
0.0100 -
Hexachloroethane
ND
0.0200
Nitrobenzene
ND
0.0200
Pentachlorophenol
ND
0.0500
Pyridine
ND
0.0500
Surr: 2-Fluorophenol
0.420
0.5000
84.1
10
109
Surr: Phenol-d6
D.420
0.5000
84.0
10
109
Surr: Nitrobenzene-d5
0.458
0.5000
91.5
19,
120
Surr. 2,4,6-Tribromophenol
0.612
0.5000
122
10
120
Surr:2-Fluorobiphenyl
0.402
0.5000
80.4
22
117
Surr: p-Terphenyl-d14
0.508
0.5000
102
34
116
S
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 16 of 41
Page 16 of 59

Summit Environmental Technol.
3310 Win SSt.
QC SUMMARY REPORT
10
trW(HVPJr,1hN IAI. a t +:actacaLstai: H, INC. Cuyahoga Falls, Ohio 44223 WO#: 17031002
_ .+'1!-r:dyNcal Cala4�,rato,r1e6 TEL: [phone] FAX: [phone]
Website: hQ.-1Avww.sette1ccom 29 Mar-17
Client: Synagro
Project: Harnett County BatchID: 26053
Sample ID LCS-26053
SampType: LCS
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 3/21/2017
RunNo: 67126
Arent ID` LCSW
Batch ID: 26053
TestNo: SW8270C SW3510C
Analysis Date: 3/22/2017
SegNo: 1107336
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Hight-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.176
0.0200
0.2000
0
-.87.9
19.1
126
2,4,5-Trichlorophenol
0.235
0.0500
0.2000
-0
118
11.7 -
151
2,4,6-Trichlorophenol
0.225
0.0500
0.2000
0
113
12.4
150
2,4-Dinitrotoluene
0.232
0.0100
0.2000
0
116
20.6
140
o-Cresol
0.197
0.0500
0.2000
0
98.4
13.8
137
m/p-Cresol(s)
0.195
0.0500
0.2000
0
97.4
10
134
Cresols, Total
ND
1.00
0.4000
0
97.9
10
129
Hexachloro=1,3-butadiene
0.177
0.00400
0.2000
0
88.5
14.7
137
Hexachlorobenzene
0.197
0.0100
0.2000
0
98.4
12
139
Hexachloroethane
0.178
0.0200
0.2000
0
89.1
14.8
132
Nitrobenzene
0.183.
0.0200
0.2000
0
91.7
15.6
.138
Pentachlorophenol
0.172
0.0500
0.2000
0
85.8.
10
156,
Pyridine
0.0837
0.0500
0.2000
0
41.8
10
126
Surr: 2-Fluorophenol
0.00220
0.5000
0.440
10
147 S
Surr: Phenol-d6
0.00290 .
0.5000
0.580
10
140 S
Surr: Nitrobenzene-d5
0.0110
0.5000
2.20
10
169 S
Surr: 2,4,6-Tribromophenol
0.00330
0.5000
0'.660
10
185 S
Surr: 2-Fluorobiphenyl
0.00370
0.5000
0.740
10
169 S
Surr: p-Terphenyl-d14
0.00610
0.5000
1.22
10
179 S
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte, detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 17 "of 41
Page 17 of 59

Summit Environmental Technologies, Inc.zu
} 3310 Win St.
QC SUMMARY REPORT
t"1191HUNNINN IAL a a;tHT,tFat..t GI3 :S, JKC.
Cuyahoga.Falls, Ohio 44223
WO#: 17031002
R4. a4-,2icaf L:,^iaongfurio� TEL: [phone] FAX. [phone]
•
Website: hM.-Ilwww.settelc.com
29 Mar-17
Client: Synagro
Project: Harnett, County
BatchID: 26053
Sample ID 17030724-001AMS SampType: MS
TestCode: SVOC-BNA T Units: mg/L•
Prep Date:
3/21/2017 RunNo: 67126
Client ID:" BatchQC Batch ID: 26053
TestNo: SW8270C SW3510C
Analysis Date:
3/2212017 SegNo: 1107338
Analyte Result
PQL
SPK value SPK Ref Val
%REC
Lowl-imit Highl-imit RPD Ref Val %RPD - RPDLimit Qual
1,4-Dichlorobenzene 0.343
0.0800
0.4000 0
85.7
29
112 "
2,4,5-Trichlorophenol 0.418
0.200
0.4000 0
105
53
-1.23
2,4,6-Trichlorophenol 0.406
0.200
0.4000 0
102
50
125,
2,4-Dinitrotoluene 0.390
0.0400
0.4000 0
97.6
57
128
o-Cresol 0.380
0.200.
0.4000 0
95.1
30
117
m/p-Cresol(s) 0.398,
0.200
0.4000 0
99.4
29
110
Cresols, Total ND
4.00
0.8000 0
97.2
20
125
Hexachloro-1,3-butadiene 0.339
0.0160
0.4000 0
84.8
22
124
Hexachlorobenzene 0.336
0.0400
0.4000 0
84.0
53
125
Hexachloroethane 0.397
0.0800
0.4000 0
99.2
21
115
Nitrobenzene 0.388
0.0800
0.4000, 0
97.0
45
121
Pentachlorophenol 0.365
0.200
0.4000 0
91.3
-35
138
Pyridine ND
0.200
0.4000 0
10.1
10
126 mQMR
Surr: 2-Fluorophen6l 0.810
1.000
81.0
10
147
Surr: Phenol-d6 0.818
1.000
81.8
10
140
Surr: Nitrobenzene-d5 0.901
1.000
90.1
-10
169
Surr: 2,4,6-Tribromophenol 0.991
1.000
99.1
10
185
Surr. 2-Fluorobiphenyl 0.775
-1.000
77.5
10
169
Surr: p-Terphenyl-d14 0.829
1.000
82.9
10
179
Qualifiers: Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E Value above quantitation range
H Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M Manual Integration used to determine
Original
MC Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
O RSD is greater than RSDlimit
P Second column confirmation exceeds
PL Permit Limit
R RPD outside acceptedrecovery limits 'Page 18 of 41
Page 18 of 59

survanklir Summit Environmental Technologies, Inc.QC SUMMARY REPORT
3310 Win St.
r=ravIHUINtlIL-N IAI. I1.t;H?,JULdti:]lzS, JKC. Cuyahoga Falls, Ohio 44223 WO#: 17031002
AnalYfl-a t Lrrboratn,r+e5 TEL: [phone] FAX.•. [phone]
Website: http://www.setie1cconz' 29 Mar-17
Client: Synagro
Project: Harnett County BatehID: 26053
§ample ID 17030724-001AMSD
SampType:-MSD
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 3/21/2017 °
RunNo: 67126
Dlient ID: BatchQC
Batch ID: 26053
TestNo: SW8270C SW3510C
Analysis Date: 3/22/2017
SegNo: 1107339
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-init , Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.295
0.0800
0.4000
0
73.8
29
112
0.3428
14.9
30
2,4,5-Trichlorophenol
0.368
0.200
0.4000
0
91.9
53
123
.0.4184
.12.9
30
2,4,6-Trichlorophenol
0.343
0.200
0.4000
0
85.8
50
125
0.4064
16.9
30
2,4-Dinitrotoluene
0.349
0.0400
0.4000
0
87.2
57
128
0.3904
11.3
30 '
6-Cresol
0.330
0.200
0.4000
0
82.6
30`
117
0.3804
14.1
30
mlp-Cresols)
0.335 -
0.200
0.4000
0
83.8
- 29
110
0.3976
17.0
30
.Cresols, Total
ND
4.00
.0.8000
0
83.2
20
125
-0
0
30
Hexachloro-1,3-butadiene
0.292
0.0160
0.4000
0
72.9
22
124
0.3392
15.1
30
Hexachlorobenzene
0.280
0.0400
0.4000
0
70.1
53
125
0.3360
18.0
30
Hexachloroethane
0.316
0.0800
0.4000.
0
79.1
21
115
0.3968
22.5
30
Nitrobenzene
0.329
0.0800
0.4000
0
82.3
45
121
0.3880
16.4
30
Pentachlorophenol
0.336
0.200
0.4000
0
84.1
35
138
0.3652
8.21
30
Pyridine
ND
0.200
0.4000
0
21.7
10
126
0
0
30
Surr: 2-Fluorophenol
0.735
1.000
73.5
10
147
0
Surr: Phenol-d6
0.745
1.000
74.5
10
140
0
Surr: Nitrobenzene-d5
0.777
1.000
77.7
10
169
0
Surr: 2,4,6=Tribromophenol
0.886
1.000
88.6
10
185 -
0
Surr: 2-Fluorobiphenyl
0.718
1.000
71.8
10
169
0
Surr: p-Terphenyl-d14
0.768
1.000
76.8
10
179
0
R
Qnalifrers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 19 of 41
Page 19 of 59

1
Summit Environmental Technologies, Inc.
�` QC SUMMARY REPORT
13310 Win St.
tr,W1K ENFo11:w I Al, I hi:HNUL GIt "s, JNQ Cuyahoga Falls, Ohio 44223 WO#: 17031002
Plr..WyfI.=f t.ahprfofie 5 TEL: [phone] FAX.- [phone] =
Website: http:/Avww.settelc.com 29 Mar-17
Client: Synagro
Project: Harnett County BatchID: 26055
Sample ID MB-26055
SampType: MBLK
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 3/21/2017
RunNo: 67061
Client ID: PBW
Batch ID: 26055
TestNo: SW7470A SW7470A
Analysis Date:. 3/21/2017
SegNo: 1106194
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury - ND 0.00200
Sample ID LCS-26055
SampType: LCS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 3/21/2017
RunNo: 67061
Client ID: LCSW
Batch ID: 26055
TestNo: SW7470A SW7470A
Analysis Date: 3/21/2017
SegNo: 1106195
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00401 0.00200 0.00400 0 100 80 120
Sample ID 17031057-003AMS
SampType: MS
TestCode: HG TCLP(74 Units: PPM.
Prep Date: 3/21/2017
RunNo: 67061
Client ID:- • Batch=
Batch ID: 26056
TestNo: SW7470A SW7470A
Analysis Date: 3/21/2017
SegNo: 1106210
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref.Val
%RPD RPDLimit Qual
TCLP Mercury 0.00446 0.00200 0.00400 0 112 75 125
Sample ID 17031057-003AMSD
SampType: MSD
TestCode: HG TCLP(74 Units: PPM
Prep Date:. 3121/2017
RunNo: 67061
Client ID: BatchQC
Batch ID: 26055
TestNo: SW7470A SW7470A
Analysis Date: 3/21/2017
SegNo: 1106211
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual.
TCLP Mercury 0.00446 0.00200
0.00400 0 - 112 75
125
0.00446 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E .
Value above quantitation range
H Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M
Manual Integration used to determine
Original
MC Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits Page 20 of41
Page 20 of 59

Summit Environmental Technologies, Inc.IT 3310 Win St. QC SUMMARY REPORT
r
tca%-IKUWMLN' 1,11, 11:VHNUL0CW:S, JNC. Cuyahoga Falls, Ohio 44223 WO#: 17031002
n1,�ra14r16c+3P LeTbprgtoFicy TEL: [phone] FAX.- [phone]
Website: ho.-Ilwww.settelccom 29 Mar_17
Client: Synagro
Project: Harnett County BatchID: 26055
ample ID 17031057-003AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 3/21/2017
RunNo: 67061
3ient ID: BatchQC
Batch ID: 26055
TestNo: SW7470A SW7470A
Analysis Date: 3/21/2017
SegNo: 1106211
,nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers:
'k Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded 7 Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 21 of 41
Page 21 of 59

l \
l
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SURIPAUT
3310 Win St.
LNVIKQ!NM+:NIAl. ra:M1:MULUUI.�:S:INC. Cuyahoga Falls, Ohio44223
WO#: 17031002
A'4ttat4l•cai C:Ttao.r,9tarir6 TEL: [phone] FAX.- [phone] -
Website: htty.-Mvivw.settekconr 29 Mat•-17
Client: Synagro•
Project: Haniett County BatchID: 26090
Sample ID mb-26090
SampType: mblk
TestCode: telp-svoc-her Units: mg/L
Prep Date: 3/21/2017
RunNo: 67188
Client ID: PBW
Batch ID: 26090
TestNo: SW8151A SW8151A
Analysis Date: 3/23/2017
SegNo: 1108188
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
2,4-D ND 1.00 0 0
2,4,5-TP ND 0.500 0 0
Surr: DCAA 401 500.0 80.3 20 140
Sample ID Ics-26090
SampType: Ics
TestCode: telp-svoc-her Units: mg/L
Prep Date: 3/21/2017
RunNo: 67188
Client ID: LCSW
Batch ID: 26090
TestNo: SW8151A SW8151A
Analysis Date: 3/23/2017
SegNo: 11081B9
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
ND 1.00
0.500
0 78.8
62.6
125
2,4,5-TP
ND 0.500
0.500
0 78.6
52.5
128
Surr: DCAA
421
500.0
84.2
20
140
Sample ID 17031000-001ams
SampType: ms
TestCode: tclp-svoc-her Units: mg/L
Prep Date: 3/21/2017
RunNo: 67188
Client ID: BatchQC
Batch ID: 26090
TestNo: SW8151A SW8151A
Analysis Date: 3/23/2017
SegNo: 1108190.
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D ND 1.00 0.500 0 75.6 37 105
2,4,5-TP ND 0.500 0.500 0.00801 74.4 38 106
Surr: DCAA 369 500.0 73.8 20 140
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded 7 Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 22 of 41
Page 22 of 59

summn-
3310 Win St. Summit Environmental Technologies, Inc.
QC SUMMARY REPORT
tr4A-1HVNro11,N IAA i hi;.aeWot.vth-S, JKC. Cuyahoga Falls, Ohio 44223 WO#: 17031002
Anzt1y,�ll:cs/ Lixbor,91Dd1E'� TEL: [phone] FAX. [phone]
Website: http.-Mvrviv.settelccom 29 Mar-17
Client: Synagro
Project: Harnett County BatchID: 26090
Sample ID 17031000-001amsd
SampType: msd
TestCode: telp-svoc-her Units: mg/L
Prep Date: 3/21/2017
RunNo: 67188
Client ID: BatchQC
Batch ID: 26090
TestNo: SW8151A SW8151A
Analysis Date: 3/23/2017
SegNo: 1108191
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
.%RPD RPDLimit Qual
2,4-D
ND
1.00 0.500 0
84.5
37
105
0 0 • 30 .
2;4,5-TP
ND-
0.500 0.500 0.00801
84.4
38
106
0 0 30
Surr: DCAA
466
500.0
93.2
20
140
0
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit 'Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 23 of 41
Page 23 of 59

Sumn:il Environmental Technologies, Inc. QC SUMMARY REPORT
sulu"IMINg- 3310 Win St.
�rsvltsv rrrnaN IAI. r L� roatULttt3l�s; 3n;c. Cuyahoga Falls, Ohio 44223 WO#: 17031002
A nalyldcal LaborwarieS TEL: [phone] FAX.- [phone]
Website: hitp://wiviv.settek.con: 29 Mar-17
Client: Synagro
Project: Harnett County BatchID: 26090
Sample ID 17031000-001ams
SampType: ms
TestCode: tclp-svoc-her
Units: mg/L
Prep Date:
3/2112017
Client ID: BatchQC
Batch ID: 26090
TestNo: SW8151A
SW8151A
Analysis Date:
3/23/2017
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit •HighLimit RPD Fief Val
2,4-D
ND
11.3 0.500
0
75.6. 37
105
2,4,5-TP
ND
11.3 0.500
0
76.0 38
106
Sample ID 17031000-001amsd SampType: msd
Client ID: BatchQC Batch ID: 26090
Analyte Result
2,4-D ND
2,4,5-TP ND
TestCode: tclp-svoc-her- Units: mg/L
TestNo: SW8151A SW8151A
PQL SPK value . SPK Ref Val
11.3 .0.500 0
11.3 0.500 0
Prep Date: 3/21/2017
Analysis Date: 3/2312017
%REC
Lowl-imit
HighLimit
RPD Ref Val
84.5
37
105
0
86.0
38
106
0
RunNo: 67188
SegNo: 1108894
%RPD- RPDLimit Qual
RunNo: 67188
SegNo: 1108895
%RPD RPDLimit Qual
0 30
0 30
Qualifiers: * Value exceeds Maximum Contaminant Level. . B Analyte detected in the associated Method Blank B Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine Original
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 24 of 41
Page 24 of 59

7 Summit Environmental Technologies,
3310 QC SUMMARY REPORT
10 Win SStt.
L70'1xwNr41:N IPIL 4 9-4;H?41LQ,Li11: i, JKC. Cuyahoga Falls, Ohio 44223 WO#: 17031002
:1,.r, tijrll:caf L�2aaY9ioti�s TEL: [phone] FAX. [phone]
Website: ho.-Ilitnvw.setteh.com 29 Mar-17
Client: Synagro
Project: Harnett County BatcliID: R66976
Sample ID LCS-R66976
SampType: LCS
TestCode: FlashPt S(10 Units: °F
Prep Date:
RunNo: 66976
Client ID: LCSS
Batch ID: -R66976
TestNo: SW1010
Analysis Date: 3/20/2017
SegNo: 1104679
Analyte
Result
PQL SPK value ..SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Flashpoint (140°F) 84.0 77.00 0: 109 100 110
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 25 of 41
Page 25 of 59

�SuntntitEnvironrnentalTechnolo0WinSt.
3310 Win St. -
1. �,7 U i .LV� 1
QC SUMMARY REPORT
�rsti Ix4i Pa m N N 11, R �a; t�d4U LUS irW �; arty .
Cuyahoga Falls, Ohio 44223
WO#: 17031002
_
dt.+t3l�lh�:af Laiatarato*iaF
TEL: [phone] FAX.- [phone]
,
Website: hQ.-1Mww.settek.com
29 Mar-17
Client:
Synagro
Project:
Harnett County
BatchID: R67087
'ample 113 Ics 10ppb L-0313
SampType: LCS
TestCode: voc-instr np Units: mgiL
Prep Date:
RunNo: 67087
,lient ID: LCSW
Batch ID: R67087
TestNo: SW8260B
Analysis Date: 3/21/2017
SegNo: 1106707
\nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0,00956
0.00500
0.0100
0
95.6
71
138
Benzene
0.00961
0.00500
0.0100
0
96.1
75
137
Chlorobenzene
0.00965
0.00500
0.0100
0
96.5
77
132
Trichloroethene
0.0107
0.00500
0.0100
0
107
64
119 .
Surr: 4-Bromofluorobenzene
57.5
-
50.00
115 "
70
130
Surr: Dibromofluoromethane
50.0-
50.00
100
70
130
Surr: Toluene-d8
54.7
50.00
109
70
130
Sample ID mblk
SampType: MBLK
TestCode: voc-mstr np " Units: mg/L
Prep Date:
RunNo: 67087
Client ID: PBW
Batch ID: R67087
TestNo: SW82608
Analysis Date: 3/21/2017
SegNo: 1106709
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
ND 0.00500
1,2-Dichloroethane
ND 0.00500
MEK
ND 0.0250
Benzene
ND 0.00500
Carbon tetrachloride
ND 0.00500
Chlorobenzene
ND 0.00500
Chloroform
ND 0.00500
Tetrachloroethene .
ND 0.00500
Trichloroethene
ND 0.00500
Vinyl chloride
ND 0.00200
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
7
Analyte detected below quantitation limits
M
Manual Integration used to determine
Original
MC
Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits Page 26 of 41
Page 26 of 59

suvIMIT
i
SununitEnvironinental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
tc','1KU srm:NIAI, Ia:r:rsraoLot3tts,svtG.
Cuyahoga Falls, Ohio44223
WO#: 17031002
Atrt�ll,tl,cFr! LrrbAPstvrFeS
TEL: [phone] FAX. • [phone]
Website: hup✓/rviviv.sette&.cons
29 Mar-17
Client:
Synagro
Project:
Harnett County
BatchID: R67087
Sample ID mbik
SampType: MBLK
TestCode: voc-mstr np Units: mg/L
Prep Date:
RunNo: 67087
Client ID: PBW
Batch ID: R67087
- TestNo: SW8260B
Analysis Date: 3/21/2017
SegNo: 1106709
Analyte
Result
PQL SPK value SPK Ref Val,
%REC Lowl-imit Hight-imit RPD Ref Val.
%RPD RPDLimit Qual
Surr:4-Bromofluorobenzene 43.5 50.00 86.9 70 130
Surr: Dibromofluoromethane 51.2 50.00 103 70 130
Surr: Toluene-d8 _ 45.1 50.00 90.2 70 130
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded 7 Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit
Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 27 of 41
Page 27 of 59

Summit Environmental Technologies,. QC SUMMARY REPORT
331010 Win SStt.
7,WI iUNtAGN IN. M 1:CH dULUCn!:5, JN . Cuyahoga Falls, Ohio 44223 WO#: 17031002
Atr?4yff,cal L.Tboratl7fie r, TEL: [phone] FAX: [phone] .
Website: ham://w1vw.setle1cconz 29 Mar-17
Client: Synagro
Project: Harnett County BatchID: R67087
Sample ID 17031002-002ams
SampType: MS
TestCode: tclp-voc-mstr Units: mg/L
Prep Dater
RunNo: 67087
;lient ID: Harnett WTP
Batch ID: R67087
TestNo: SW8260B
Analysis Date: 3/21/2017
SegNo: 1106727
analyte
Result
PQL SPK value SPK Ref Val -
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.235
0.00100
0.250
0
931.8
39.9
160
1,2-Dichloroethane
0.258
0.00100
0.250
0
103
42.5
157
MEK
1.69
0.00600
1.25
0.271
114
16.6
227
Benzene
0.242
0.00100
0.250
0
96.8
38.1
155
Carbon tetrachloride
0.260
0.00100
0.250
0
104
40.8
162
Chlorobenzene
0.256
0.00100
0.250
0
102
35.7
168
Chloroform
0.248•
0.00100
0.250
0.
99.4
18.3
199
Tetrachloroethene
0.257
0.00100
0.250
0
103
10
261
Trichloroethene
0.260
0.00100
0.250
0
104
23.8
175
Vinyl chloride
0.234
0.00100
0.250
0
93.6
10
165
Surr:4-Bromofluorobenzene
2670
2500
107
84.6
130
Surr: Dibromofluoromethane
2470
2500
98.7
71.4
127
Surr: Toluene-d8
2480
2500
99.3
74.6
127
'ample ID 17031002-002amsd
SampType: MSD
TestCode: tclp-voc-mstr Units: mg/L
Prep Date:
RunNo: 67087
Nent ID: Harnett WTP
Batch ID: R67087
TestNo: SW8260B
Analysis Date: 3/21/2017
SegNo: 1106.728
\nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.264 0.00100
0.250 0 105
39.9
160
0.235 11.6
25
1,2-Dichloroethane
0.278 0.00100
0.250 - 0 111
42.5
157
0.258 7.09
25
MEK
1.84 0.00500
1.25 0.271 126 -
16.6
227
1.69 8.35
25
Benzene
0.270, 0.00100
0.250 0 108
38.1
155
0.242 10.8
25
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
Original
MC
Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R.
RPD outside accepted -recovery limits
page 28 of 41
Page 28 of 59

Summit Environmental Technologies, Inc. Sum Mur 3310 Win St. QC SUMMARY REPORT
tr;NIKUNW.NIM. or.+:aatacautszaWs,are Cuyahoga Falls, Ohio44223 WO#: 17031002 .
_ 61 4di� ltc+3P Lr%a,ratgrFe r . , TEL: [phone] FAX.• [phone]
•Website: h9a.-Mvivw.setteIccom 29-Mar-1 7
Client: Synagro
Project: Harnett County BatchID: R67087
Sample ID 17031002-002amsd
SampType: MSD
TestCode: telp-voc-mstr Units: mg/L
Prep Date:
RunNo: 67087
Client ID: Harnett WTP
Batch ID: R67087
TestNo: SW8260B
Analysis Date: 3/21/2017
SegNo: 1106728
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Carbon tetrachloride
0.276
0.00100
0.250
0
111
= 40.8
162
0.260
5.96
25
Chlorobenzene
0.262
0.00100
0.250
0
105
35.7
168
0.256
2.32
25
Chloroform
0.280
0.00100
0.250
0
112
18.3
199
0.248
11.7
25
Tetrachloroethene
0.270
0.00100
0.250
0
108
10
261
0.257
5.12
25
Trichloroethene
0.270..
0.00100
0.250
0
108
23.8
175
0.260
3.77
25
Vinyl chloride
0.253
0.00100
0.250
0
101
- 10
165
0.234
7.80
25
Surr:4-Bromofluorobenzene
2700
2500
108
84.6
130
0
25
Surr: Dibromofluoromethane
2470
2500
98.9
71.4
127
0
25
Surr: Toluene-d8
2630
2500
105
74.6
127
0
25
Qualifiers: + Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit. .
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank E Value above quantitation range
J Analyte detected below quantitation limits M Manual Integration used to determine
ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
PL Permit Limit R RPD outside accepted recovery limits Page 29 of 41
Page 29 of 59

fflr Summit Environmental Technologies, Inc. QC- SUMMARY REPORT
cs ,
r .i +' 3310 Win St.
LMO1KVtNTOUNIR[.AI.i;HNOLrJuR:S;NC. Cuyahoga Falls, Ohio44223 WO#: 17031002
Analyrtt:caf CabpraParip, TEL: [phone] FAX. [phone]
Website: http:/hvww.settek.com 29 Mar-17
Client: Synagro
Project: Harnett County BatchID: R67102
Sample ID MB-R67102
SampType: MBLK
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo; 67102
Client ID: PBW
Batch ID: R67102
TestNo: SW9014
Analysis Date: 312212017.'
SegNo: 1106956
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive ND 0.500
Sample ID LCS-R67102
SampType: LCS
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 67102
Client ID: LCSW
Batch ID: R67102
TestNo: SW9014
Analysis Date: 312212017
SegNo: 1106957
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref. Val
%RPD RPDLimit Qual
Cyanide, Reactive 0.990 0.500 1.000 0 99.0 85 115
Sample ID 17030887-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 67102
Client ID: Batch=
Batch ID: R67102
TestNo: SW9014
Analysis Date:- 3/22/2017
SegNo: 1106969
Analyte
Result
PQL SPK value - SPK Ref Val .
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 1.03 0.500 1.000 0 103 81.3 118
Sample ID 17030887-001AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 67102
Client ID: BatchQC
Batch ID: R67102
TestNo: SW9014
Analysis Date: 3/22/2017
SegNo: 1106960
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
0.990 0.500
1.000 0 99.0 81.3
118
1.027 3.67 5
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B Analyte.detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M
Manual Integration used to determine
Original
MC
Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
0
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits Page 30 of 41
Page 30 of 59

�" Summit Environmental Technologies,lnc. QC SUMMARY REPORT
, _ 3310 Win St.
trav1KVNrntNIAI. rti:HNraLoJt..s, xfqw. Cuyahoga Falls, Ohio 44223 WO#: 17031002
_ Agz4 4'tdcml tabo,"wries 'TEL: [phone] FAX.- [phone]
Website: httP://www.settek.coni 29 Mar-17
Client: Synagro
Project: Harnett'County BatchID: R67102.
Sample ID. 17030887-001AMSD
SampType: MSD
TestCode:-Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 67102 .
Client ID: BatchQC
Batch ID: R67102
TestNo: SW9014
Analysis Date: 3/2212017
SegNo: 1106660
Analyte
Result
PQL SPK value SPK Ref Val.
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: k Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL . Permit Limit R RPD outside accepted recovery limits Page 31 of 41
Page 31 of 59

Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
'- M%-IRVIrlr ry AI, r r.rttlUW10t 5, JrqC.
Cuyahoga Falls, Ohio 44223
WO#: 17031002
_
'r+�16'lir ta�arafo�ies TEL: [phone] FAX.• [phone]
Website: hgp.-Mviviv.settelccom
29 Mar-17
'Client:
Synagro
Project:
Harnett County
BatchID: R67104
Sample ID 17031002-002ADUP
SampType: DUP
TestCode: pH_S(9045D) Units: s.u.@19.2C
Prep Date:
RunNo: 67104
Client ID: Harnett WTP
Batch ID: R67104
TestNo: SW9045D
Analysis Date: 3/22/2017
SegNo: 1107199
Analyte
Result
PQL SPK value . SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 5.3
5.3 0 10
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 32 of 41
Page 32 of 59

Surd
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
cc;:vlxU+rtUn:NIAL.Ibt;Ht�IULUG]1-S,t�
Cuyahoga Falls, Ohio44223
WO#: 17031002
Atgzr 4Vf&ca=P �aborr�tprfvF
TEL: [phone] FAX.- [phone]
Website: http:/fivivw.settelc.com/hvivw.settelc.com
29 Mar-17
Client:
Synagro
Project:
Harnett County
BatchID: R67104
Sample ID LCS-R67104
SampType: LCS
TestCode: pH_NPW(450 Units: s.u.@20.4C
Prep Date:
RunNo: 67104
Client ID: LCSW
Batch ID: R67104
TestNo: SW9045D
Analysis Date: 3/22/2017
SegNo: 1106987
Analyte
Result
. PQL SPK value SPK Ref Val, %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 100 98.6 101.4
Sample ID 17030887-001ADUP
SampType: DUP
TestCode: pH_NPW(450 Units: s.u.@21.3C
Prep Date:
RunNo: 67104
Client ID: BatchQC
Batch ID: R67104
TestNo: SW9045D
Analysis Date: 3/22/2017
SegNo: ,1106989
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit ' HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 8.2 8.1 0.2 5
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 33 of 41
Page 33 of 59

Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
Lr"viRUIN rnr;N i Al, I3;V ?4fJLUU-'S, INC. Cuyahoga Falls, Ohio 44223 WO#: 17031002
A>,z4aWhIcal b3borgwriou TEL: [phone] FAX.- [phone]
Website: httn://wivii,.settelc.com 29 Mar-17
Client: Synagro
Project: Harnett County BatchlD: R67115
Sample ID MB-R67115
SampType: MBLK
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 67115
Client ID: PBW
Batch ID: R67115
TestNo: SW9034
Analysis Date: 3/22/2017
SegNo:, 1107143
Analyte
Result
. PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Sulfide, Reactive ND 25.0
Sample ID LCS-R67115
SampType: LCS
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 67115
ClienYlD: - LCSW
Batch ID: R67115
TestNo: SW9034
Analysis Date: 312212017
SegNo: 1107144
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit 'Qual
Sulfide, Reactive 2040 25.0 2000 0 102 85 115
Sample ID 17030887-001AMS
SampType: MS
TestCode: Sulfide,React- Units: mg/L
Prep Date:
RunNo:.67115
Client ID: BatchQC
Batch ID: R67115
TestNo: SW9034
Analysis Date: 3/22/2017
SegNo: 1107145
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD - RPDLimit Qual
Sulfide, Reactive 2100 25.0 2000 0 105 75 125 H
Sample ID 11030887-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/L
Prep Date:
-RunNo: 67115
Client ID: BatchQC
Batch ID: R67115
TestNo: SW9034
Analysis Date: 3/22/2017
SegNo: 1107146
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
2040 25.0
2000 0 102 75
125
2100 2.90 30' H
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit Original
P
Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits Page 34 of 41.
Page 34 of 59

Summil Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
er'%'ltcVNrni;NIOU.a.rA.JMrJttl't:S,INC. Cuyahoga Falls, Ohio44223 Wo#: 17031002
A4rraitrt1.caP Caba.r9lade,5 TEL: [phone] FAX.- [phone]
Website: ht .-Mvivw.settek.com 29 Mar--"17
Client, Synagro _
Project: Harnett: County BatchID: R6711.5
Sample ID 17030887-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg1L
Prep Date:
RunNo: 671.15
Client ID: BatchQC
Batch ID: R67115
TestNo: SW9034
Analysis Date: 3/22/2017
SegNo: 1107146
Analyte
Result
PQL . SPK value SPK Ref Val .
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit, Qual
Qualifiers: ;k Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds. PL Permit Limit R RPD outside accepted recovery limits Page 35 of 41
Page 35 of 59

s
Suninzit Environmental Technologies, Inc. QC SUMMARY REPORT
y ti 3310 Win St.
LNVIKVaNTONNJAI. IJAMNULt IES,JRU. Cuyahoga Falls, Ohio44223 WO#: 17031002
Anaiyflc.8t LaborstoFles TEL: [phone] FAX- [phone]
Website: httI?:/hvivw.settelcconi 29-Mar-17
Client: Synagro
Project: Harnett County BatchID: R67135
Sample ID 17030870-001ADUP SampType: DUP TestCode: Ignitability_S Units: Prep Date: RunNo: 67135
Client ID: BatchQC Batch ID: R67135 TestNo: SW1030 Analysis Date: 3/23/2017 SegNo: 1107505
Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD- RPDLJmit Qual
Ignitability Jon -flammable. 0 0 20
Sample ID 17030870-001ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 67135.
:lient ID: BatchQC
Batch ID: R67135
TestNo: SW1030
Analysis Date: 3/23/2017
SegNo: 1107606
%nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability Jon -flammable. 0 0 20
Sample ID 1.7030870-002ADUP SampType: DUP TestCode: Ignitability_S Units: Prep Date:_. RunNo: 67135
Client ID: BatchQC Batch ID: R67135 TestNo: SW1030 Analysis Date: 3/23/2017 SegNo: 1107508
Analyte Result PQL SPK value • SPK Ref Val %REC LowLJmit HighLimit RPD Ref Val %RPD RPDLimit Qual
Ignitability not propagate. 0 0 20
Sample ID 17030870-002ATRIP
SampType: DUP
TestCode:- Ignitability_S Units:
Prep Date:
RunNo: 67135
'lient ID: BatchQC
Batch ID: R67135
TestNo: SW1030
Analysis Date: 3/23/2017
SegNo: 1107509
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability not propagate. 0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E ' Value above quantitation range
H Holding times for preparation or analysis exceeded 7 Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 36 of 41
Page 36 of 59

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
' � L�1 3310 Win St.
tr:%'It6UNh1uNIA[.IhCHNULdUI—IS,Jrtw+. Cuyahoga Falls, Ohio44223 WO#: 17031002
r4.r, i/Ui1,rr?P C:zba,rcatJlrle� TEL: [phone] FAX. [phone]
Website: hM.-Ilivivw.settelccom 29 Mar-17
Client: Synagro
Project: Harnett County BatchID: R67135
Sample ID 17030870-002ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 67135
Client ID: BatchQC
Batch ID: R67135
TestNo: SW1030
Analysis Date: 3/2312017
SegNo: 1107509
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sample ID 17031000-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 67135
Client ID: BatchQC
Batch ID: R67135
TestNo: SW1030
Analysis Date: 3/23/2017
SegNo: 1107511
Analyte
Result
PQL SPK value SPK Ref Val
%REC . LowLimit_ HighLimit RPD -Ref Val
.%RPD -RPDLimit Qual
Ignitability Jon -flammable. 0 0 20
Sample ID 17031000-001ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep'Date:
RunNo: 67135
Client ID: BatchQC
Batch ID: R67135
TestNo: SW1030
Analysis Date: 3/2312017
SegNo:, 1107512
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD 'RPDLimit Qua]
Ignitability Ion -flammable. 0 0 20
Sample ID 17031002-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 67135
Client ID: North Harnett
Batch ID: R67135
TestNo: SW1030
Analysis Date: 3/23/2017
SegNo: 1107514
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability Jon -flammable. 0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 37 of 41
Page 37 of 59

F � ;
SunsmitEnvironmentalTechnologies, Inc .
3310 Win St.
QC SUMMARY AI�tT REPORT
�C 1. �,7 U Lr1L�1� i .lt 1
tr "1HU!NUnaN mr, r 1.UH?4Uk.tt1311:S; INC.
Cuyahoga Falls, Ohio 44223
WO#: 17031002
Ana?yAra•P
TEL: [phone] FAX- (330)'253-4489
Website: hgp:/hvww.seuek.conz
29 Mar-17
Client:
Synagro
Project:
Harnett County
BatchED: R67135
Sample ID-17031002-001ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 67135
Client ID: North Harnett ,
Batch ID: R67135
TestNo: SW1030
Analysis Date: 3/23/2017
SegNo: 1107515
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitabil[ty Ion -flammable. 0 0 20
Sample ID 17031002-002ADUP
SampType:. DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 67135
Client ID: Harnett WTP
Batch ID: R67135
TestNo: SW1030
Analysis Date: 3/23/2017
SegNo: 1107517
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit -RPD Ref Val
%RPD RPDLimit Qual .
Ignitability Ion -flammable. 0 0 20
Sample ID 17031002-002ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:-
RunNo: 67135
Client ID: Harnett WTP
Batch ID: R67135
TestNo: SW1030
Analysis Date: 3/23/2017
SegNo: 1107518
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Ignitability Ion -flammable. 0 0 20
Sample ID 17031077-002ADUP
SampType: DUP
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo: 67135
Client ID: BatchQC
Batch ID: R67135
t TestNo: SW1030
Analysis Date: 3/23/2017
SegNo: 1107520
Analyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Ignitability 4.64 4.780 2.97 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 38 of 41
Page 38 of 59

k ' ' Summit Environmental Technologies, Inc. QC SUMMARY REPORT
kf� I I - 3310 Win St.
cr;:lgRUN rnt:NIALIh'.HRULUUR:S:JKC Cuyahoga Falls, Ohio44223 WO#: 17031002
_ Ar3lyltcaS Catto,rstorles TEL: [phone] FAX. [phone]
Website: http://www.settefc.com _ 29 Mar-17
Client: Synagro
Project: Harnett County BatchID: R67135
Sample ID 17031077-002ADUP
SampType: DUP
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo: 67135
;Inert ID: BatchQC
Batch ID: R67135
TestNo: SW1030
Analysis Date: 3/23/2017
SegNo: 1107520
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Sample ID 17031077-002ATRIP
SampType: DUP
TestCode: Ignitability _S Units: mm/sec
Prep Date:
RunNo: 67735
;Inert ID: BatchQC
Batch ID: R67135
TestNo: SW1030
Analysis Date: 3/23/2017
SegNo: 1107621
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability 4.98 4.780 4.10 20
Sample ID 17031077-003ADUP
SampType: DUP
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo: 67135
client ID: BatchQC
Batch ID: R67135-
TestNo: SW1030
Analysis'Date: 3/23/2017
SegNo: 1107523
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability 9.54 10.02 4.91 20
3ample.I1) 17031077-003ATRIP
SampType: DUP
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo: 67135
;Inert ID: BatchQC
Batch ID: R67135
TestNo: SW1030
Analysis Date: 3/23/2017
SegNo: 1107524
%nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability 8.47 10.02 16.8 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value.is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 39 of 41
Page 39 of 59

,ITsurnSummit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
L-MVIKVmNrolIMIA[.17;aHNULFJCnL:S,JKC Cuyahoga Falls, Ohio44223 WO#: 17031002
AnalyUc.7f Lsbor oolo6 TEL: [phone] FAX: [phone]
Website: http:/hviviv.settek.con: 29 Mar-17
Client: Synagro
Project: Harnett County _ BatchID: R67135.
"Sample ID 17031208-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 67135
Client ID: BatchQC
Batch ID: R67135
TestNo: SW1030
Analysis, Date: 3/23/2017
SegNo: 1107526
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighUrnit RPD Ref Val..
%RPD RPDLimit, Qual
Ignitability ]on -flammable. 0 0 20
Sample ID 17031208-001ATRIP
SampType: DUP
TestCode: Ignitabilify_S Units:
Prep Date:
RunNo: 67135
Client ID: BatchQC
Batch ID: R67135
TestNo: SW1030
Analysis Date: 3/23/2017
SegNo: 1107527
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Ignitability ]on -flammable. 0 0 20
Sample ID 17031210-001ADUP
SampType: DUP
TestCode: Ignitability_S •Units:
Prep Date:
RunNo: 67135
Client ID: BatchQC
Batch ID: R67135
TestNo: SW1030
Analysis Date: 3/23/2017
SegNo: 1107529
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit 'RPD Ref Val
.%RPD RPDLimit Qual
Ignitability ]on -flammable. 0 0 20 .
Sample ID .17031210-001ATRIP
SampType: DUP
TestCode: 1' n[tabllity_S Units:
Prep Date:
RunN6: 67135
Client ID: BatchQC
Batch ID: R67135
TestNo: SW1030
Analysis Date: 3/23/2017
SegNo: 1107530
Analyte
Result
PQL SPK value SPK Ref Val
%REC 'LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability Ion -flammable. 0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value.above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than•RSDlimit Original
P Second column confirmation exceeds PL Permit Limit' R RPD outside accepted recovery limits Page 40 of 41
Page 40 of 59

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
t 3310 Win St.
cr.'A-IKV,NrA1.NIAL. I4:-HNULOG U:S�,INC. Cuyahoga Falls, Ohio44223 WO#: 17031002
Aram yfli sf LzbpratnrleS TEL: [phone] FAX-.• [phone]
Website: htty.Ilww1i,.settelceom 29 Mar-17
Client: Synagro
Project: Harnett County
BatchID: R67135
Sample ID 17031210-001ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 67135
Client ID: BatchQC
Batch ID: R67135
TestNo: SW1030
Analysis Date: 3/23/2017
SegNo: 1107530
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit- Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit.. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 41 of 41
Page 41 of 59

1
`
AC-QACOC338 RexO
Lfreadva Vowwoorts
i U 1MIT
Analysis Request I. Chain - of Custody.
ENYINDNMEN7AI. �EGMN6tGli1�8,,tNC.
For SUjIMI1ti ttviranmCntal'i-110alogie4Isto.'uS®only
3310 win Sir
atwh- ao rwly Ohlo 44223
aoa s�a•aaao
Page Cf, SET No.
ClientNama
Prvj t dent' �aaticn
S na ro
n;.rnC
UM!
`
Clicni Addscas°
Project Addms
Client Mene "
Report Tn
336-909-8;627
Will Varner.
a to s . F
' nt Fallo.its � x >n Client v«t
Potl
ete umber
u N ,
�
_
Contaet Person
TWS IQ
Facility ll3
Will Varner
Client Email Address
Reporting Rcquiretdents
�
"p
wwerner na ro.com
Q d if for Ohio VAP
Sampled By..
Q d if for Drinking Water Dampllance
03
`�
(D
•
.YIrIVI
Varner
J
Q if Other.
U -
a .
•
.IA
..Lri
.a
r'

N
4—
O
(V
_ _ DC-7 EPlociivC Dafe: O7174no 0)
Ruv to M
n
Summit Environmental Technologies, Inc.
Cooler Receipt Form
Initials of person inspecting cooler and samples:
Chant.
Order Number,
hate Received
Time Received: 12;UQ> Date cooler(s) opened and samples inspeoted,�.3h [I n
Number of Coolersisoxes:
{� N/A
Shippe FED EX PS
DHL Airborne Us Postal' Walk-in Pickup Other.
Packaging:
Peanut° 8ubbte Wra Paper Foam None Other.
Tape on cooleribox
Q N NIA
N !A
Custody . Seals Intact
Y ;
C-O•C in ppl stir
0 N NIA
Ice �/ - Blue ice
present I absent I melted N/A
Sample Temperature IR Gun gjgg2045 CF t`l, °C 1 • °C NIA
Radiological Testing Instrument serial # 5127 Y N !A
(see page 2 for scan results)
-Use I sheet per sample for Radiological Testing., If sample is HOT, the Radiological Safety Officer must be notified
Immediately.
C-O-C filled out properly
N N/A
Samples in separate bags
Y N NIA
Sample containers Intact`
Y N NIA
`If no, fist broken sample(s):
Sample label(s) complete (ID• date, etc.)
L.3
N
NIA
Labels) agree with C-O-C
N
NIA
Correct containers used
Y•
N
NIA
Sufficient sample received
Y
N
NIA
Samples received within holding time
N
Bubbles absent frorn 40 mL vials"
Y
N
N!A
Samples with bubbles <6mm arc acceptabte. Indicate bubble size if>6mm.
Was client contacted about samples
Y N
Will client send new samples
Y N
Client contact:
Date/Tirrme:
Logged in by;
Comments.,
Page 1 of 2
Page 43 of 59

North carclina• wastewatcrlcrpl:n Walter Laboratory Certificatiarr
C01ifi6d Parametem Usti lg
1-- tm Name 8umm,If Cnvlroninenlal Tecnmi )loLjiv*,
Inc.
Certiucatr N•ror,hUr G37
Andreas: 33 tC by n Street
�� f �' _ • ,'. +a
l
Effm- - uu Giaie: 3fit7.017
Cuyahoga Falls. Ott AQ23-
txpiral ca DatE +2r3112U"if
•
�a1�¢tL¢5l+tirrrnalament 2!:+r`2017
The abgea nmad JpAurziory, hI,^4np dJly net. the recparr..mr rna n1 'I SA NCAC 2H.t)snq• .a 15=rcfrycarl,f,Ld far lrv,: rammurment a1 the:36rdmeem5 I,Slec Lclutr
'
'
-•---- - CERTIFIED KRJtifu7EYER5 - —
-
INORGANIC
fiEvlL*UE, SUSPENDED-
EOD
S1.1.2S40 O'•109 . - 7 Vtiou"jtis+r-
SRA 02 t9 U'•2C01 (Aqua irti9)
rd1 S]M. TOTAL
G.l=I.(1r tDE
Sh1 2840- B-1097 ;Aqw rio
SV4-846 905G n (iNqueou>)
S L It -.A
EPA:+00 -7, Rrv. 4A.. 1694 (Agt,eyil si
�rvt.x20G•19rJ7_iPticr�etu p-
ti+N-346GO10D(A4uoAt+ct
FLUORIDE '
9MIFATE-
EPA "CO.U. R(,V: 2.1. 1933 (AquuOue,)
EPA, amwl:l, Rev 2.1. 1093 ,tm1 ogu,1
SWM46 AMP tAQuapm%)
$L'1.M1-0C 90r{i.A. {fir}ueoaJsl
I G1v IrrtiB I �I Tv
51A. FIDE
SVJ-A+iO 163;)(Non-k1uaom)'
SAf446 9-334 1nr.,ner us}
INORGANIC', F13F• JOLS .-
METAL .
EPA 420.1 Rev 1978 4Ag1jjY.vt8F
TC1,r-rtL7 LS
.
PVIT?DGEN IaITWTE
SS+S'-G4€m131i(Iulhnirue4)
EPA 300.0. Rev Z 1.1993 (P.queoll.r:}
ALUMINUM
t1
Eth),94fj hOSG A f.P.quecs sJ
EPA 200.7. RCV: 4.4. 19.N (Aqua:+„!)
NITROGCN,NERITE
$4V 14G4Ut0t5.{Aqueuus;
EI•+A30J 0 r]ev. 2.1, 1S93 lAgsleotis)
EPA 200.8, 11ey„5.4.. 19:'4 fAqumv5)
' S'x -BAC. d79f, A 1Aqucous)
S'I�d-b4$•sl(Fc�U (i [tE�1000•LS)
h11 e�Gt;f W, NG3 * fti'C
AMINIONY
i;P.4300:0.Rev-2.1, 1093 :Acaeous)
EPA 200,7,-Rev.4,4, 1004 (Aqueeusl
SIN-546 9065 A (Aglutous)
'SIN-E46 a6l0 0 (Aclraou-s�
NITftx;i--N ID.TAL'KJEL'DAH.
,EPA 2Ci(; , R64, G;4,-C9QX (ftje4vz j
sr�rc'45a1) %IvrJ B 107 (.r.-rp1 460G N113 Q-19071 fAquecus)
S104-s4e r•020 B InglnocuU)-
aL rSttiREASL-
ARSEMIC
EPJ51IiK4 14(m. E (A queoum)
Et'A 2—CUT, T?5v. 4.4,19It1 (1tru--uus;
Hleq.W 90T1 0 (Non-AtI thous]
4vVrF;A* yfiit7T0 0 (AgLopaits) .
t`I`r
EPA 200.8, Rev. e.41 1994 (Aqueous).
--sve-8 .6 win 0 (Non-Aqueaus,
SINr746 fi0238 (Aquecusl
PHOM'K.MOS.70TAL
MI21t• M
EIIA200.7_ Ray. c 4 (iR,1A)(Aqueous}
EPA 20.0.7 Rev.4.4. '199M(4tytt-mis)
5NJ•04G GD'0 Lr i;AUueous)
S%V-841 sal n (�Ajuuou:sl
RESIMJF..:630LVED 180 G+
ZPA.200:8. Rum5.4.•d5174 (Aq.rmm1.K)
SIA 2540 C-1957?Aquecus)
M-340 GM0 B (P.gimet,ua)
Th,;c®rCrlicotan rgtreS rt,4,raanccetan aLujxdllle mmi:yAumim9mp1`Ly.'!Amn. rad RpVDonCd-•nethcdn1c.'nF.I)-ijw*Iwary ptrftrrtrdrl'm nrt'EY8IWHIIr+Rnamr+:.s La0.Y.z:od1:!& mSut71Pr11fjrluil pena9in,.GmeUG+Jecer:!�nviat; I9ranh�+rJiocs ai acl I,�r11),h 15A Nr A0 2H E-F67
r-
W
CD to
c- 4-
4- O
O
0) �
t7) M(ISM
a a

North Carolina UWastawaxerfGroundwatar [Axoratory Gerf7 lCatlatl
Codified Parameters Us ingl'
Leh hJtam-:unmiit Cnvilnrimerrtmi Ttrcnnalo;ples; tic_
f
Cer[I11r�In NtpitlUQr G31
hn'clr�s8: 3ti10VJin 5t�ee1
_
ET(4TCtitaDale:-'9�112CY17
Cuy oya F;a%, CH 44238•
Ex�lrhhan37ro14�' 12;3112017
DaIePTI.astA(riemmp..IIt 2j'I"417
ThC anave R31YN7,9tmr 1rrM n rrinySO�Ir ertul'.ha ragljrFrnepL• c!'SA
NC/4 2H JOCO, z fmrehycgrtlti(t;16)r If+e n1: ILIfCVICIlI011ne LLnr:tium. !: aclnA tojow.
.CERTIFIFD.174RAIVETERS
EERY LUUM
ff':R2116 S, rev 5.4. 191,19 (p,qunous)
_--, ---- — - _ .-
C°,a.200.0, Ray. 5.4 M94 (Aqueous}'
SW"-M 6020 F3;Aquwr &)
S'eV dt4�i fi j201j°dF�I)uusl
I.ITHPIJ/,'
BORON
.Y�
GF I,' ^O�i.7, RC'✓. 4 4. ! 45A• (Af7 nrrim;)
EPA M.G, Rau. GA. 1994 (Aqueous)
SW-840 -301 C, rr ?rtl ueuca)
S+A'-84G 6020 B4A.ouou:tO
MAGNESIUM
CADMIUM
EPA200 7. t cv.4.4,. 1994 (Aqutaroa)
EPA 20C1 7:'Rcv. 4 A. 1'f 914fAquaqus)
Sti"J:$�di SGIC D (Aqueous)
SW446 601D D (Aq9eoi no
MAhi(G ANESE
LPA 200:8, Rev. &. C. 1Sti4 0,Aqueacts)
[Pay 200 7..Fii;V• 4A. 1094 (A•Itiepus;•-
SIAr,84e F302D F'. {A@ueCrrS)
SCN•.neG f 0 is 0;T{queau9j
;CJi-I IUM
r NIJA100.r7. Rev 54, Igg4tAquobL,:i'I
FPA 200 7; Red. 4.4. 1 K14 Jpqumfp:}
aVQ-$A$ tiL29 ci jAq(,u;Ju01
LAMPAID D {Aontmut s)
t4ERCURY
CHROMIUM TOTAL
3=PA ?45 . Rev- 3.U. IUV4 (AQ1soom"
• EPA ZP0.7, Rev A.Z. 3994 ft.: fauctus)
- :;�r1-M4ra ; 4;0.A iAge,cuu3)
- .
;kV-S4&'301GD•(hgnanot) ,
EPA, 1021 Fib+1un44r:5Y
EPA 200 8, P,ev 54 I pPia (Aqueous}
41Q7U1 f3:']F Nt1n7
sw-84.0 and 6 Kk uenus)
EP& 209-7. Rev. a a iss4 (AgLIWUS3
C CsALT
INV-848 601a Cr fAqLIP i?uS¢
OA 2CO.7. Rev, 4.-1. 899a ;ru+u(*.mN)
EPA 200.6. Rluu. 3.4. 094. (At(uanas)
SW84€r 8011) 0 {Arlueaus)
_ V.V-4145 0t120 6 (Agt eGus)
EPA 200.0, Rev. 8.a, IgPa iAuuuuusp
MCKEL
gW.840 13020 B (A4"peoz)
EPA 24W.y, rtar. 5.4. 1994 (Aquaaaris]
COPPER'
ZW h45 G020 0 (Aquenlasj
EPA 20-37.Mvl.4.4.1f194 [Awcoas)'
TIOTASSIutvl
b"A84G Oal 110 (Acluea�uc)
EPA. �'40.�, Rev '4t1;' 19n•1 (Acueaiaa)
EPA 200.8, Rev. 5.4, 1904 ;Aqueous)
Slfd-84$ 4)10 D {,Ayueausj.
SM.1.94: ,CO20 B (Agmenusl
S1aL:EG14Uft9
IF2tYtd
EPA 200.8, Ruv. 5.4, 1'194 (Aqueausl
CPA 2A0.1. )Zev. b d 19t14 (Aque�ar.}
SUV-t I IH5020 G fAqur_ousl
SW-3d'S E014 U (kciieOLIS)
51E Lt12
LEJ' n
EPA M.7; Ftev 4.,k'A IQ4 (Aqueous)
- _ F'PAZQf,-7. F'i2v.4.JY l�ly4 (AII1%476u6)
-. S'AV-m fiCJ1i.1 P (Agtaoouw
-
8VO-a4rj ao10D (AgI.ewW
EPA MR8 R0v 8.4, 15N IAgvoom,
�h15 ',rCRtflCr�l019,:ngLli(C:t I]I:fA+IR�LRM e:M1 3GGCIlI0ai1 111JaC'rl/3LS Vr:IrIGC
e�, sel,hrrth in 15,E rJCAC.2H NUJ(
jY( f0y+ utecf a3rrcvCd i-te7 mmiriyp•. E1110 RXIStEe0rp pefreit(r1:v+M nilnJa11:8n1q g.puip5c�, .L�ora(pnga alv.;ti7�_c �o.;�ni piyaglties, �(YJror de.Gnjrit2lidn •te i(dn�"in-�
-
IM
Lf7
TI- 4--,
0 0
CN dam'
N

North Carolln-a wa1Stewaterler€Tcllydvwatet Lahot�ljoty Ce-tfiCatfnm
Cert FFM Parametc-ra Listing
WbNamer SurnmatEnvvemm�l�l2t-echo gd�ey(Irt
R ae1111CF:Ita Vuntber
�5�
Addresm* 33.10 4NIrf (r; a1
ElTecti4e'Ga:e:
4?1f 417
fi;I/xlkit�z Falls, 0H c4223
Expifanon D?10
j2 31t�0iY
Ua1001LostAmenun'senC
T2-2(F17
" 'The a6nva R.?rrv7d latOrd;ary. L•cvwr, d,,:� mpy II'a iequiiemeM� cf 1uA FI CAC:,k'�@rY0
:- txrebfcerllrerl far IFnm9Y.-�Oter'ieP! o'I I};epamsclorF I:S:SC IkIUn•
CERTIFIED PARAMETERS
SA+,'•84G SU1U es (Ag6vso S)
FSTF.AC-:• ABLE PETk{'JLtura P3.YDR�CAR®GAIS'
8+3D;rJtu1,
MADEP, rolay 20De, V*c . t 1 (Aqueous)
PPA 700 7, Rev. �T_1,.T994:(Aglrrh)vs;
P1(jNHAt.i)Cf-NIATE�� VCILAT(LE, CJ[t;;Ar4]CS - -
54'u-C (l+.gtioouS}
SV,l kl48 k.015 INgJLuuS)
STRL]HTI:}tf
PES-CICIDES Ok(,JLN'Q.:14L0R1NE
EIIA 200-7, Rev_ 4.4, t954{AgwJ0u';I
EF.,Ni!3f}g .;Popnruus]
S>,':1-84fi-CSDIOQ{,1qu•'•nusl
S�Jd"8451a0.3'1Lrr'iutvr:cusj
.
tPA 204.(5, Iiev. 5-4- 1'359 iAqu[x)usi
4" OLVCI ILORI.YA7FQ kff'HI_NYLS iPCBsj -
SYtr-840 smzo B (Aqueous'
+
EPACU (fsgcr1rd.b
THALLIUMSV1-846W52
A (Aquecus) `
EPA2130.7. Rev 4.4; 1994 (A. -mom ]
PURGIMBL E,'ORGANIC$
�
oLV•846901 D
EPJkG24 iAqueau9)
�
�,
EPA 20(I U. Row S.A. 19fJ4 (ng4r6Gux)
EW-846 8?G'4 (3 dflquefJus{
�0
O
S l•$40'BOZ+J 6 {Aqueaps(
TOTAL ORGANIC HAHIJES
M
TIN
SW-345 9020 S. f�.RUewr]
a)�.
CPA 20R.7. Rcu. 4;d, 9 LL: (Aquecusl
SPH OJESEL RANGE OI�LiAi41C5
�
�
< SWIM dU1•D D (14cpacus) �. _
sw.8e18 8p151; {Ajllmjs)
-
0..
ca
VANAVIUAA •
r[ARVFi OLIRE RANGE. DRGA NIcr�
,
a
EPA, 200_8, Rev 5.4, W34 (Aqueaua)
SVfr-9�6 J;0 S.0 (IL�ueir(sj "
SW -ads Roza s (AqlegauS)
:VOLATILE PE I RuLlvV110 HYDROCARBONS
-Rev. 1.1 (n.que94:SJ
EPA:00.8,Rev.5-4, IFIM (Aquecus)
sw-84'6 m7ii ft (Aclucous)
OROAN(C
rUP ORGANICS
Slyd-8461311 (AjuEUas)
ADSOr;M15LEORGANIC HAI 117F5
EPA 1ET50. Rou> C. '1 997 4Aijiruuuu) ...
VASE NEUTRALFACID 11SRGANICS
EPA 62$ (Apmeau 'r
5'MS.L6.8270 D fAqueocrsj
CHf ORINATEDACID I•IffRL3ICIDEE
. _ .• 5'V�t•it�i&.g1 S1 ds rllt7uCuce�( - _
_
-
6HL+7RkATED P4E'VOLICS
tWV 161M, Rev A, VD97iAgUc0us;
. TI1K' ��erYiGcotio� agclu=AS mBtrtrance o' cn acrr,I7,Oblh q��4^.(y-3r,srrs;7ctt-EY�yrmn u pl SGfm'V[0'1"ICOLCtttdngy.:urrl rry115!.v-*ryy per`,onnincJ?n av,+,t:: tt;r -U r. 1_F?".. :r0cr ala-mv w sct;e& T:� Dail l:� 'Atl o dt ur de: urla-;alionfa
azArt rnuIn15.t,kit-Ac-2HW217 - - '
intfaarr
-

North Carolina. WagtowatorlGr+ tm d''%%pafer L-abordtor-u Gertificat'ron
Certified Para'neters Lisiiffg.
. • Lab Na ,6; • SLArfailH EnVimmrrentoI lechnc ogica, ln�
'. -
'Corlifiratc NumL-er-
AtJUtca9s - 331C.Jan5lre.t
Efiect3::,Gate 1T1:2317
Cuyahoga N, E, •DH 44223•
rr�'rf
�SrEill l�y}Ir GaIE' 1Z'31f?QY7 '
L�iC-)6f1 ".1Am*pnv1+llarL uir41201,5
The Ebuve ITOMM. I;t!]eritnrr iIdW'l5 duly ntt-,l 11•G ra:urwn'_m5 ar 15A. WCA'- iH C50r?. uWmrlol WLhe n5e;swreaant c3 ChC p•'rLrTY,'ICt9 I,rin:,FCcW
i_ -
-
�GRT[FEEA P'RALA.EtEwz
--_.
MROANIC
SILICA
_ .
sbE},
EPA 200.1. Rev.4 t S4J,34 (Aqueo6isl
SM 521U B 2001 iAquaws)
SV,1-4Z ,'GV10-0 rAqueoupj
:CHLORIDE
SULFATE
V144G ,300A (Ailuemr.'i)
EPA 3UU.U, Rhv. 2. 1 10r& (1+.queass;
COO
SitVIA46 905E A, (A9cleous)
SPA 522rrr,-199T (A qusnuE?
$3ILFICiE
f i 1JfYRl[5E
- 5W-846 f1934 lijLAU k1%)
FPA•3001A,ftev.2.1, 1N?; (Aquemm)
rd TAE,
SL'I-1346 il,155.. A (Aqrat)nt,s J
1'CLF' METALS.
IMGIRC:I1NI P14ENOLS '
5LY-i1Gtf 1311 ;.�.lueniis}
CO 0)
Lr)
C-rft420,1, Rey' 1918 rYj,1Vrw.$)
rLLtlM NU4.1
r 4—
NITROGEN,r;t'1iFrt
FPkZ00,7 Ruv.,:4.199.4(Agr�me,)
O O
EPA 300.1?. F.Gv. 2:1, 7SG (f quensxsp
$1N-04•fi iG =0 D (Agwr7r,$)
ti
',I,t4�-f
N]T (P.quetn 5i
EPA 200A. fig'. 5A. 1994 (Aqueous)
0) Q)
NITrtOGEtZ:hJITR?TE
GEE;
SVJ446t:•:J211;t![Aflucous}
- tm
EP;ti 300.0; Itet' Z:A. 1995 (Aqueous)
kwnT 614: '
0- M
5W-846 905G A flLqje+TusY
Ef=NegC:7, Rev. 4.4, 1.394 (/l4taeau5)
VRf{17GEW• hD3 fW D2
SW-846 G310 C lAcIuj.,cusl'
LPA 30O.3, Re'v.2.1, 40.3 Lf oausl
ERA,200.o-,, Rev. 54.'•O -I {AglFDU3)
5�L4� 346 €0.%A (AtVacot�)
;iV1-:o45 60i0 E (nqueougF
h'IT3tc?fzUN, TOTAL KJELDAHL
ARGENIC -
;i 1 a5t70 %Jarg E-19,97 (SL14500 NH3 D-107) 44quecus)
EPA.20U.:1, AaO n. 1:!gd, (Aque6luvi
OIL,? CREASE
' S!,N-040 0010 rD rAquaous)
EPA 133Ti4 Hcv- fi (Ayu.Gaus}
EPA 200,9. f ev. 5 a 191JA (Aqusouc)
SW.S46 9071 B (Non•Aq'ueaw5,
:$Ih-640 H0:.6 R (Aeror-•ous)
Pa4r_tSPf-10pus,'10I'AL
6htit LJ rJ
EPA 26a.1, tiro 4 A (,11,0) [Acuaric g)
CPA 2037.7. Rev. 4-4. 1494 (Agijodus
• SW,&46 Of! 10 CC (Aq.ucous)
S)14414-6 5-0 10 17. (Aru ioU s)
RESIDUE, QfSS�3,.VL [1 1F1n'C,:
Ef'!, 200.8. ticv. 5.4. 1994 (Aqurn(ts)
610 254 0 G-IP97 (hgtieutt5)
SW946 d020 a mggeatl5l
RESIDUE;. SWPENDED . '
DCRYLLIU(o1
S'Ad2540 [} 9037 (r•':ptseams)
EPA 200 8, r v ; e :994 (Argurrn.r.)
RGv'1l?L E: TCtTgL .
$W-845 6020 D (Aqueous(
8PA 2540 13-107 (A(ALrecus)
BORON
-fhi�rxyitaotorr_'qu:rim�nt;.x.otAa'uc.ep:tulbG4+Wryassuran:cp'o�ntm,+tF�,rftirnvweclrttNh�ir,Ic3y.asdseritsrarmrypc:i0rrryan�ecq._YvuranWzsaWP'��
" c5sna!10h.inIfANC:'1:211MO
- Ca'Joins:ri!s:+te�4hje.rctt:Jcctlanieah-d!nrdMPfUv,Ftic. rtpfraclia�
- �� - C,`�

North CaroMna WastewatarfGroundyvr ter Labora'tbry.Gerdificatiim:
Goitifiedl Pa Ameteis LlstEhg .
ta:hUinan Summit.En•1upnmuejntafTcahrnigrli 3.lr+c,
CctUFcalehtcm9Atr' 0 f
dttfii'tss�. 3310'WIn St vct
EP1eC. -e Dale:
Cuyatioga 1Fplk. CH 44223-
Ex}air lion Dsle I1.i i1!ZO'•7
t?41a of Last Aiiiwdmenl: 1114 2{316
11w obam wmcY tsto'aloiy, ll= nn dlke, n aM he ru :+rtrrri7s rA .1.5q M'.h�, iW I INII:1, iy �.QfCYrr
c�dilie_ Ier lha bu vu
_CERTiucc; 7ARAIVETERS
Lim 200.8.Rev, a4,1D94(Aqueo-us)
UW-04Gr9101)(P.uturrc5l
t^f tFAE 6U�U 6 i%tquacus}
MAGt•1ESi1Jk1
r,,zOnlftJr.t
EPA 7W.7, P-ev.4.4. 1(194',Agwxins}
FPA 7.110,7. F1au. 4A. 1994' (Aquaoue)
GrJ1uri (lq••14rnw)
$lh-RAfi60,.0IJ(Alwous) -
. MAM'GiANE5E.
-
26n.R. RAv 5"4,. 19144 (AgijWuS)
EPA 200,7.Row, A:A, t�VP4 fA:4u&yj5)
i`Y•n4li 600 G {A,qu�aus}nllj0
D IAg;LIE{::15j
CALC61Jiv1
Ed'K5 iQ7.$, F.eu. 54. 1Mj4 fA ue�aus}
EOA 250 ;, M,. 4.4. 1944*(A' queau%I
s1r+ AE riiQ2n rs i ogurXnls)
5VL1•645 010.0 (A,quaaus)
J0ER 0UF0f ,
CHROMIUM TOTAL
EPA 245.1. Rev.3A :1994 (Aq.vor )
WA 20D.7. Rev: 4.4_ 1994 '(Aquaati,;:)
uW--04f3!r47G'A, AauL'Ut18)
=PA 200 6. iiev.:+_4,1994 lAqucuusl
MrJt."Y'ODCNtR.+
a1a1-040 5020 B (i tjujeoS}
Efi/\ 208-7rRev.4'4 199� ti�tic:ecOLo} ,
COSALT
5yJ�4G.li(YIq (y;Aratioous)
EPA 2CO3. Rem-4.4, 10'[A (Agtteaw)
EPA 200 G, Rcv. &4. 1094 {Aqut:aos}
S4'd•E46 60101) (Aqueoug}
$1lJ-645 G020,3 {Agcr7u.)
1.17A2009 Rev 5,4,1d94 (Acu-QrA51
NICKEL
IM11-640 M20 H tAC-verus) _
EP.x20G.8, Rev. S f, 1�J44 (4gueXW
COPPEN
SV1=91G E020 6 (Agueau,l
EPA. 71'{1.7 .FGGv.,A.f, 7+J 34lApusacxs}
ROTASSIUM
S1lJ-$4$ t ©i G O 17t�tar�eusb
EPAa 23G.7, RW. A.A. 1094 (Aquepo6;
EPA 2}(ID 8 14ev 5.4, 1994 (Agijwtig)
S%N-U56010 D,(AqueauFj
S5,,V-H4fi ii020 9 JAquea4s)
SELENit-M
:fUN
EPA 2dC:4: kteu Sa, y �91 {�yueau5!
EPA 20J 7 • Far.u. 4A. ?SIM ikqut-cut)
SLN BaCt13ti20 Et P qUt-Oa=_; _,'
_; V�'•8.4fi 6010 a fA�uenus)
5I'Lb'�R"
r-
LJAD
EPA.200.7. ilea+ 4 A: fills (A.'quwous)
CPf4200.7 Rev. 4.4,.1994 (Aquenas)
St'1'�840 G010 D (rtyu�auei
SW-0415 CC 10 D iA4leo'u53
Ef A 200.E. Re'r, s,d•. 1 OU {Aqi iWL;Sj
EPA?�F0'�. r`cv.5. . 19-04 (AVuLmus)
SY1-44G'9420^0 (A44liOti3}
Ly-,946 fi02fl B (Aalucausj
SODL0;11+1
�ItN11Jdr1'
EPA 20fk7,-RtkW4.4•, t994 (Agtpe(kus1
EPA 209. 7. i2C:: 4 4, fD94 (A$utmus}
y1N .t:45 0010 a (Agsleo9ls}
'rhi%.CUridictiwi�,rgw+4�rtlaiitAn�ednn,vi-,5uWA-4ualit}•;t.tntre-vejuritarn.am- rinmrGvWsnrolhodaK,y.,:PAS:'nti:lH¢Iuryp�erf4rm8l7U•C918r3'unlicnS:+T�AY:*,
_.,sal fclt�s'dr. 15A MC'M' 2F111EC7,
Lc:.LIJl0.•:IC`lilh�ti{I�{eGt1oCJ41IP1?I'IJIIIf'SpiMiprxIQt`ef11LCdID:IP:ir'IM((�1h6rte.
i
0)
4—
�' O
LO 00
N

NOPTIT Carolina Wastew6tetlGroundw#tbr La.baratory cortfftat,16n
GDrtiffod Paramataps Listing
Lark K4imL: lurnmil Envimnownhil Tachnalogie.A, Inc
Cr-Jlif:C-AO NUM13U. 01
AddrAuss 32 10 Vj-h site -A.
Pfdcfiva Ogle I h.2-3 17
Exp;r nti an Dato 1WIP-017
Dite orl-ndAmortawent: I
wo
CERTIFIED P.kll.A.M-CTER.
RES] JUIDES.'ORGANOCIII.CRINE
EPA ZTJU.?. Kiev 4 4 '-,P,4 4ftieotis',.
LPA GOS ;AqUeMlfl;•
SVbV4(i-UQlO D+,'Aqusau5t'
M-W 6 1-406 T 11 (Atl uruon)
FPA ZOO.8, Rate- 5.4. 1004 (AciuL-Dur.)
"LYCHLIORMATED EliVMhNYl,% (F';B*)'
SAS!-84 6 6 DZJ it FJ(QLIO aUS)
ERA 608.(Amaim)
THAU.11,M4
SW-846 san A (A.(tn?OoL1s)
PPA 7.rO.7. RLJ. 4A. 143P4 (Ap,�orjs)
PLJRC'PAn -F. ORSkNICS
8VV-84& 80-10 D
E PIA 624 :Aqudmjsj
EPA M* 8. Fav 5.4. 1 kl'j4 (AqUOqLjC:)
SVV-816 UdO 13 iAqueckf-.4
.--7TAI. ORGANIC, RALIDES
TIN
SVM40 9026 B (Aqamnus.}
co
EPMOD1.7 JR
ITI I DIE5-=i RANGIF. OnGANIGS
EW-846 -5G10 D lfiquaaLis7
S%,V-84G 8W!'; C.fAmm-mig)
4-
0
Mi CAWONI: RANGE. QRGANFCS
co
I*PA 290.8. Rev. S .4. 1 r,494 i6queous)
Siq -446 RID16C (.AqLeaus}
k(LATILE PF b-WAOWDROCARSOMS
2114C,
WADEP, May.2q04, Ray. 1.1 (Aqueol.-5),
MV-1346 5920.8
0116ANIC
-VZLf,l ORGpAPjlCS
'%W-V3 5 131 -1 CAquacus;)
ADS6REIAEI;.E 019MI'1lf. HALIDES
EPA 16M..Rav C. 1997 I/lqL.aqlj" .I
SA4,RF NELIFRALIA.C-10 OR.GANICIS
EPA 625
S'67-8-6 877D [I kAfjijsuuE)
CHLORU.HATED ACID HFUMCIDES
SW-84B 91 5t A (A:j m:ratj*)
CIALIORINANED r'llr NOUCS
EFIA 1-M. Rev. A.
E;XTRA-0AMA PET-ROLFUM HYDPOGARBOM;
mAdEP, Mm� Rev. 1.1 Ortkieow,,y
NONHALOGC?4A7W'VO-LATItE, ORW%IjfCS
S1a -846 66.15 C i.A94JaMd.)
Aal l0r.h in 1 SA NCAC PH DRU7
0)
U')
4-
0
a)
tm
cu
12-

North Carolina Wastewaief)Grour➢dwai ter Laboratory Certificattan
Certified Paramot.ors misting
Lao )dame: S)fimrn11En'riranrrsentaITech nblogi=, IRr-
Address: 33 10 Win Strecl
Gvjahoga Fait, OH .44i23-
Tho.aixwe naroterl lsuer};pr •, homq duty mQl thr, mqun .rents at 15A WAG 211.01100. Is
herebyei.0iiAd (br the measumnon;of Iha pordrnetar hoed be.ox
CIERTIF QeC FARA$M'T5KS..
tidG+f2GhF�JC
SILICA
BOO
EPA 200-7, Ruv,. 4 A,1.194 (Aqueous)
SPA 5E70 B 20Ca1 (+lqusiuus}
�Iw•fl4Gt�:c o s+queous}
Cl1LORI Q E
SULMTE
SIN-846 Ss.66'A (Aquevu3)
CFJt 300.0, Rev 7. I, 103 (,aqua.,ug)
COD'
SW-5d8 f!r)5f'A (aquootis)
Ski 5220 C-1 M7 (Aq ueou!;)
S4A-FI7E
FLJJ0Itl'DE
51°r-g4g C(k;4.(Aqu;3wu:s}
EPA 300-0, Rev,2.1. 1903(,Aquwww
METAL
SNl-E48206 A(agdeoua)
TCLPMEi'ALS
INOF CAWIC I- 6EU'3? S
M-9461311 tAqueous)
CPA,420,1,. Rev. 1978
ALUMINUM
NITROGEN, hll"I`MTE
C!PAt 20G-7. ?et•. 4.4. 1994 (Aqueous)
EPA.90it,n, Rev 2.1. 1t=93.{Aqu,;ous)
59d-946 Fin 10P(Agvebus)
SW-W905) A(Mueaus)
EPA 200.8, Rev. $ 4, 1994 (Aq'.reous)
NITRQ(i ;LN!, Mr BETE
S%V;04630200 (Aquecus)
EPA•300.0'. Rev.2.1, 1993 (Aqueous)
ANTONQNY
SA;V,846.9056 A (Aquecyis;
EPA M.7, R.ov. 4-4.1954 IAquEbusp
NITROGEN. NO + NO
Wb 84G:G010 D (Aqueaus)
CPIA OD0.0, Rev, 2,1 1,993 (Aqueous)
EP.A200.8'Rxv. 5.4, TW fARpueouS)
SW-640 2-356 A (Aque'ous)
SW-846 MO B (Aqueous)
NIi'-:t'33EN, TOTAL KJELDAHL
APSENIC
Shl 4500 Norg fi1997 ('SM 4500 N113 E7-1997) (Aqueous)
EPA-2 W.7; Rev 4.4. i.%d ft4geeouS)
OIL u GREA5E
SW7a4b' S jjC D (Aqueaus)
Er --A 9Sb4-Rov. 8 (Aque ua)
EPA 2,OM Roy. SA. 1994 (Aqueous)
$W-14E 0271 B (Non-Actucous}
SK-845 6G20 B (Aque ous)
PHOSWORUS, TOTAL
BARIUM
CPA2107.7, €tev 4.4 (1954) (AgUeatls)
PPA 20n..7, Rev. 4,4,1994 (A�ue,c,us)
BV'1-E4060SQ Difiqut3ous)
SW-84Q* 601.0ID(Aquku5)
RE81DUE, DIS800ur2 318i7 i;
EFA 200 R, Rev 5 4.1994 (fq6eeus)
SM 2540 C-1997 {Rqu4-Jaus)
. SW 94136LI70 S (AgtIe6u9)
RESUME, SUSPENDED
BEJ3 /( I,OI;tf�i
Sh+ 2r 0 D-1 W (Aqueous),
EPA 200.8, Rov. 5.4, 1994(Aqueous)
P'ESIEJJIIFa, IUTAL
SUV-84c6U20g:(Acueous)
5L4, 2540 s-11307 (Aqueous1
30RON
Corti:icate NLsrbar:
631
=ifective IR9:--
-A!1?2016
Expisatbi Carr.
12J3ii2016
Date 0( LaS1-,Ainendment:
11M/2M -
This. oerdiWlor: requims malrler,rt, ur rrn a mPlAebl-quiVitj 2ssurams pnp(n, uCa ff. pprfai,Gj rnethodology in.d ealie-,ctory W.ftoriai8riqu un ctiarr9tan, samples .Lnn&A'gr�m nre,subjeet to c-vl pw^zt iru ;ndtnr decarilicak;on tnrdnT�a':Acn;
35 set kali III 15.A. N AC 2H. C807
O)
L0
4-
O
O
Ln.
0)
t�
f6

North Carolina WastewateriGroundwatur Laboratory Cerjjfl:ztian
Cqrtified Param&ers'Llsffing
L;t , 4 Noma: Summ if Enwronlll&M Tec�rinloqles, Inc.
&triji4-
Addro—s: 3'j f 0 win Streei
r-UNUNU 15FAW 111/201'S
Cttyahmp FMs, rxr 44223.
DatEcif UwAmoffdmort:
TbTabnve irismrolaboratcr!j, havii)g, duly rnul We rerivIfemr-Ar.t4im
IbA N6:ACZ-11.60100, is herenycerii6m forv,crrcmurmemoriie rwormtess listed Lmlaw
ERTIFIED FARAJAIETERS
[:PA 2baz, ReV. 5A, t:994 (AqLlF91MF.)
0010 D UAqyeuus)
SW-846 6620 B.(JALI�UL-OUS]
MAC INE81UN
'CADMIUM
EPA*90rt ", Rev.-4 k IM (Acroepusj
EPA 2110.7, Rov. 4.4. T9�4-(Aqu0oLl8)-
SW-M OD 0 D (Aq uecusl
SVO-846 6010 D (AV4rjus)
14ANGANESE
EPA 200.8. Rev. 5.4, 19.9* JAqdeclus.)
EPA.20Q.T, Rev-4.6, 1994 JAquacus)
SIV-U46 6020 S' (AQueousl
SW-8413- 8010 D (Aqueous)
'CALCIUM
EPA 2 DG.49, Kiev, BN (Aqueous)
EPA 200.7; Rev.,4-4. 1994 (Aqw.mm)
SW-W 002.08 (Aqutmus)
S01-840 1301.0 D (Aci;j6ous)
MERCURY
Of 1R0fy1jL1;'vj, TOTAL
EFiA 249 -, r.,.v. 3.0, 1wil fAqunus)
(0 0)
EPA 211n 7. Virjv, 4.4, 1991. (Aquaou G)
SVV-1�46 1470 A (Aqueous)
L0
MV-11.46 6010 0 {Aqueous}
EPA 1631 L iAqueousj
4—
4— 0
0
EPA 2600.8, R0, 5.4, 1094 (A-Quimm)
MOLYBDENUM
00
sw-f;46 U020 B 'Aqueous)
EPA 2013-7. Reu. C41,1994 ftucaus),
W LID
a)
ff-Z)BALT'
(Aqueous)
0)
M M
EPA 200.7. Rev. -t4
EPA 200.8.. Rev.- 5,4, 1SO4.(Aqueau-s)
[L
SMC14656010 D (Aqueous)
SW446 PrOAD 6 (AqL,1-uus)
EPA 100,3, RpV -5A, I S94 fftrealus)
NIO KE'L
MV8413 - 602.0 S. (Aqueo'LlS,1
EPA 21 C(DA, Rov . . 5-41, 199A (Aqueous)
tbP-PER ---
SW-180 60.20 LA. (Aqueous)
EPA.21M.T. Rc;V, 4.4,1994 (Aqueous}.
POTA, '�Si UPA
SVV-z3466rJ10 13 ;Aquewm)
EPA 20',1.7, Rev. 4A, IQ94 (r%9L2ccuj)
EPA 2010.8, Ray. 6.4. MQ4 tAqucmus)
SW -MG 60 M 17 (Aqwous)
S6W-Z48 CO20 8 (Aqueous)
Sr=Lr=N1UM
IRON
I*FA ZOM, Rev. S. 4. 1 E04 (..Aqueous)
EPA 2DU. 'Rev 4.4, 19:94 (AqtjpDijs)
$VV- B�Cv -15NO S (Aquomki
PV,W 6010 D (Aqueous)
SILVER
L r-A D
EPA PM.7; Rev. 4.4, 1 894 (A qu*,.utl
EPA 209 7. Rov. 4-A, 19 94, (Aqueoun)
M446 '60 10 b (Aqueous)
SV&P-46 6 ' 010 D (Aque-oluQ
EPA:200,-.8, Rtv. E,4, 1-994 (Aucous)
EPA 2W.B, Rov 6.4,1994 (Aquicour,)
SVI-84 13*020 -8 lAcl ugoual
S1!'I-846 602 a � (Aqueoue.)
SOOMM
LITHIUM
EPA:200.7, Ray. 4.4, TS94'(Aquer3j.-s)
EPA 2010.7, Rev 4A, i 994'(AqLaL-nu,,)
.15VVA8-Ki 100.16D (Ac;ufjuuE,
mq-.1'res malmanco ;LTvn awpptmb*q;04ym5traw-- polrom, use vtawaml mAlmr1clogy, and satis6lay prvi
tpr1rcmatze on evalualjvvml:m cfva piamllim ondw decemri6Wji rix jillizzmns
as set Tonn I!i i %k Jjr—lAr: 2FLaW�,

North"CaroHma WastrevpaterlGround 2tO r..abomtctry Cartifca'tipri
Certified Pararlleters-U;ffng
Lab' Narle. Surnmlt Envircinnier6621 lechnoldgies, Inc Cerdifrcate NOMbor 531
I^xoklr�3s: 3310 Win Street Fffe-mlve Data: 1!'IJ2O16
Guyahagof Falts. 01,11 4422S- E>iF. Acin Dale: 1 13412C}16
Data of Last Argerldmell: 1 kfdr2difr
The .ab:)rue nanren Irinuratory, having Cute mattte mqui*manly 4l UA NGAG 2H 611M, i& heiabycertrrieif far to meusur-encril Crlhe!p3i:EtieItjrs lislu d be'ow
CERTIFIED PARAWF,TERS
STRONTIUM
EPA213117, fWv. 4-4. 191}4 (Ag"ouy)
SYN-846 B010 D (,Aquncus}
EPA 2001. Rr<•r,. 55.4, 1 U42 fAquen=)
WV-846 6-= 5 (Atlueolis)
THALLIUM
-EPA 2B0 ; Rev: 4.4. ty;=4 q;Aqueous)
&OV-84613010 D (Aiktra mIS)
EPA-2OO-8, Rev.5,4, 1.904 (AgUeau )
SVV-8456020 6 r,A4UOOusj
TIN
EPA 2L10.7, R.V. 4 4 19,1M, (Aqueou8p
SW-846 601013. Mquer3w)
VANADIUM
EF'A i0b.f3, Ftav "4, 19 4 �k uouus)
SAS-8466020,8,(AquimusY
.ZINC
FPA 2CO.8: Rev. 5A 1 PW (,equaous)
SVV-846'6020 B (Aqueous)
ORGANIC
TCLiu ORG�1PlIL'9
rpW4 461311 (Aqueous}
AUSORBABI 5'OROANIC HALIDES
EPA.1650, Rev. C, T.QV (Aqu(ia.%)
BASE NELI-FRAWACID, OriG14NICS
EPA 629114000f)t
SW-fs16827o b (Aquoaus)
CHLORINATED ACID HERSIGIDES
,•SU4-84frM51 A('Aqueous)
CHLORMTED PHENOLICS
EVA-169, Irv. IA.1 "7 (Aquec,us)
EXTR",CTA131-5 PETROLEOL'I HYl3ROGARBONS .
PdAIDEP, May-2004, Reu • 1 (A.gL1equsp
tj0NHAt00ENATFb Vt 3U,-, I E, ORGANICS
-Slff-&5-8015 G (Aqueoars).
3�GSTIClOE$; !7RC.,ANCCNLORIWE
=PA:I KS'(A'gneon)
S4'w.9a� 8081 D (,4qucous}
POLYCHWHINAtEd BIPHEPSYL.S (PrAL-)
EP, 08 (Aquaou,)
SVV-846 B0B2A (Aqueous)
PU:RGr-ABLE, ORGANICS
KP,A MA (A,queousl
SW, '11.4 � 82M R (Agraeous)
TOTAL (Y12GM41C HALIDES
$1M1dnA46 90220 0 (AgUocius)
TRH DIESELRANGE. ORGANICS
SL' r84a 8016 G (Aqueou:)
TPH GASOLINEPAPlGE.ORCAl11CS
SbAt'-flit 8915 C-(Aqueous)
VOLATIttPETROLEUM HYDRt7CAIlSONS
MA011P. May20(ld, Rev•1.1 (ftmuus)
(his cerlificMiunrequiresmsiriinr".*ropacmptamequalii!rtKtirancspruyram,usecrarpnrvr),ymaPiCtlologr.and•Zotu"aryraf5prenanmostlocwlUnaltiasarilloreeceilifiaMurlGurulracllnrs
W 4MI fnr4i 1.116. A W A 0 2H Of)D7,
4--
O
m
N
a0)
c1s
0)
LO
4-
0
N
L0
O
ca
i0-

R%"tY coopr!..
iMI('I11:AL ', RIA!AN
�. JAY 7.:111<It�R 1:1�
February 7; 2017
Gal
N'is. Meegan €)ougherty
5-Vmmif Ertyironrnental Techrtatoeiies, InG,
3310 Win Street
Cuyahoga Falls, OH 44223
Subject, NO V!?' IiGW LC Scxgy-flay Parameter -Meth6d Decertification Recommendation,
Zinc s EPA 200.7'and SW-846 6010 D
Oear Ms. Qc: uaherty:
The remedial Proflclanc,yr Testing .I;PT? result(s) for Me t?e€ow Parameter Methad(s) reported icy 'your
iaboratory For the North Carolin''a V11astewated Groundwater Laboratory Certification (NC V IGW LC)
perforrnanee evaluation viaslwere unacceptable and a sixthday Parameter method decertificabon will be
recommended. The results reported and the trtie values asAhey app2a.r in our records are as fall^,ti�'s_
Siu )r ParamQter Method UnitsRep�tied True 1:zcepianc� I 'PerformanceVatue Vatu RWoe
"fP 16-313 f=PA01501 lL 60C 496 421-569
S.1dU-ii4a rj+J.10 © rJ;� Nf;t kwpiable
EPA. 2aa_7)
Or-4201OC 1. , r pg,L 1660 f400 1190-1610 NotAcce table
S.r1-8�6601t7-D P !
''i tvdtten Carrectne iu;l n Report (Cl+R i for each unacceptable result will be required prior to reissuing cedricatidn,,
This is to notify you that the Laboratory Genii cation Branch of the North Carolina Diuision of Water
ResJu'rces, Water Scienues Section, is ronsfdering recommending a parameter method(s)
decertification to the Environmental Program Super'visur. The recornmendation .concerns tine above
menti•oned' Violation(s). This is not a decertification; it is 2 notification of our intent to consider
decertiftcatsari. Yc'u will be informed in a separatd communication if decertification is issued. '
Contact me immedii teia, at (919) 733-39G8 Pxt 251 if your records do not agree with ours or if you have
ttuas#lobs. -
Sncerety,
Todd Crawford
Technical' Assistance & Compliance Specialist
NO WVV?1-3W Laboratory Certi€icatirn :Sranch
A02i truant "
cc* Gana Uailerwhite, Jason Smith ivraster Ftln #601
IsMOr $daces ScC110fl
%V,1346votorA!rob ic" ;atoLAuntuiy CerlifrGaiIrm bf�ncl,
'bi7r4aii'er.i=1iaa-1- k'a
i=rrne•n:g-739.5:U.h'.Pn.i ;d�'�-;•'T!-G�:y
hi!cm I t4a1,t3ry n� ocda6a�ddloe i .�shwree-r utir-ems..;at�r rs: E}7-9p I�b6rdE�Pr-c ii �rlun-bmnrh
.. r k,uces-rlal�`�iater-sc,eltCas-horn
Page 10 of 16
Page 53 of 59

'V L7,
February 7, 2017
631
Jugs Mes'gan Dougherty
Summit Environmental Teehnoloyies, inc.
3310 Win Street
Cuyahoga Fails, OH 44223
R11?Y C(-)?-)11E
S, .1AY Z.,\1kIFiR..MaAT%
Subject; NC 'VAIVIMY LG- 8fxt-y-1 ay P�t6meter Method Decertificadort Recommendation_
Seleriiurn — EPA 200.7 and SOI-54� 6010 0
Doar farts- Gatighertyr_
Tho remedial Proficiency Testing PT) resultSSj for tho'befp%r Parerneter Mathad(s) reocrted by, yo-.-ir
laboratory for the Nurth C'arolino Wasteewaterl Groundwater Laboratory Certification (NC V°ortiftilrGW, LC
performance evalu3lion was,twere unacceptable and a sixty+ -day+ parameter method deceftif[cat:on r.vill be
reo mmended. The results reported and the, true values as they appear in our records are -as fell: vs:
Study Parameter't a hod
WP16-3B EPA20'0-71
SW-846 15010 D
092.o16G'1 1 EPA 20G,71
S %r-846 6010 D
!nits _ reported Trite F,Uceptance
Vatue Vatua Rar e
pg.eL I 520 442 376-50
t
VgJIL 47C j 4t3b
for each unacoeptat-le r esull
'Pl r€wmanr e
Not Arx ptable
326-444 1 Not Acce�table
'iUr w reissuirig cer"Ific.alkrv..
This is to notifyyou that the Laboratory Certification Branch of the North Cwollna Division of Wai9=r
Resources, Water Sciences Section, is considering recirininending a parameter Method(s)
decertification to Fhe Emironrnentol Prwgram �3upcntisor.. Thd- rec-ari mendolion concern; the above
mentioned violationl,s}- This is not a decertification, it is. a notification of our infent to consider
clacertifioation. You will be informed in a separate communication if decertification is issued.
Contact me irnmediatefy at (919.) 733�39G,8 ext. 251 if your records do not agree with ours or f you have
questions, '
8incerely,
Todd Craw ord
Technical Assistanc Corgi pliance S;erdlist
NO Vit'' /11:3'W Laboratory Ceftificati.on Branch
Altm,.-hmelhl
oe: Cana sattomwdie. J_r on Smith, rlasler Rig *63
4Vlmr Sdenms'weftr
RIC La4axaxiy Cartil'ieatiurr Bni!r I
LC-4$x'• 414C5 R >-Iy Pro"^ "4D;r:a
Inlerrai•hE?n:fi,��t�tc.=auu!:ir,ou�fdiv3elans!uesrgsesstwrcxe!watr.:-rssaurcE :isr:ih•.air-se�nccs•Ituale-pagzit�bpl�tttY-[er<irica'it�t�ran�h
R I
Page 11 of 16
Page 54 of 59

1TT� +i
a
r S
February 7, 2017
631
Nls. Pildegan Dopollerty
Stlmmii Enuironrriental Tetihriologies', fnc_-
3310 Win Street
Cuyahoga Falls, OFi 44223
ROY COOPER
,•tIC1-1E.1L S RL-b'tK
'; JAY f1MMEIt-MA''
Subject: NO V'tW1GIN 1 C Sixty -Day Pararr titer ?Aei;:t d Decartificatidn Redommendation:
Nickel — EPA 200.7 and SW-84.6 6010 D
Gear Ms. Dougherty -
Tine rergedial Pcofaciency Tasting (PT) result(s) for the beicti4r Pararnt ter �+1ethcd(s) reported by yo1�r
laboratoify far the NoAll Carolina Wastewater, Groundwater Lab6taitory Certification (NC: VitV*'J'IG V.LC)
performance evaluation wasIviere unacceptable and a sixty-day. Qamn"Ieter. meth6d decertifieatian will ELF
recommended, The res'taits reported and the true values as they appear in our reoords are as follovts:
FSludy
Value
EPA 1r1+P..9 6-3i3 71
pgfl. 1 ta�6 I 918
_.r 6}1+1-646 601 El D
_ ERA 200.71 � i
Parametea- Melttad l Units eparts
Value
'805-'1030
t}92Gi6C1 US+-846 60'0 D +L '1620 '1360 1 1200-152.0
_ S1_
'� u i;llen Corrcctrva iofl,Report �GARi for eacii unacccpja*1 C resutt't1111 GC
'Performance I
Not Acceptable
Not At-Oepiab.le ;
10 re9ssu.ng cerificatior5
This is to natify you That the Laboratory Certification Branch of the North Carolina Divisioi'1 of Water
Resource6,, Water 56ences SaeuliDn, is considering recommending a pafamei tsT method(s)
decertification to.the Environmental Pi"Qgram Supervisor. Th6 rec.ummendation concerns the above
menti6nved violationts}. This is not. a decertification; it is a notification of our intent to consider
decertification. You will he informed in a separate coil) inunication if deeertificaEion is issued.
Contact me lm' media#ely at [phone] ext, 251 if your records do not agree with ours or d you ha-ve
questlans.
Sincerely.
Todd Ceayvford
Technical, AssistEince & Co pa Specialist
PAC VAN!(! -'UV Laboratory Q..artificatian Branch
kitachment
V�' Dona wbIt� whiie,•Jason Smith, Master 1=dfo;C•. 1
Water SOLSIcay Se;.ilual
14CVhGo' aD.'IG: L-�'t.ri.rLaboraiory�trt 4]t6ijnSi4iict
r$zJ V.JCor R;n{:'3.t•_=Zi.!d,•3
LGidll�'1 �`�ai.;iy �rc:+ri•=�' - !,'iJrl4:Fd:.apa,. ;i'r
.iPnri r ii•79q.�c.nrry'gfuu^diriziva�A7mar-rg�yurcas:rra!er-resources- atdr'n'ate r-sciffl tj-•t!IJITK-yk '14 3ra[d•i[cal;'G!r irsi^j
Page 12 of 16
Page 55 of 59

IG - LOPIC f
i
Ill'1#;w Q.
•
- �--= � - �
Siorr:i•sr�e� GLti1�.Y�tl ls;' -
Final Report
• hieiltaa-lyPital)G.r 5{1��►�J.It;unl3"nv(t[!}
�
- .
1z
P.:;suh Ainlyrsusi
L'nJls 1•'rll]e
A=pt.
iYtn:ia�s
6'!aluati411
.. .
Iron- re '
mw tic PL 1360
1
1150 to
155L)
0 �� A cceptahir
LIViki PL•113?-2-C.NW 1m1.I F,PA'd;
lArxlystti^K{M:.lyrla'Jsre ?It::,^,7� 74
,
❑ i ��'cntart+
kt�knikurs.Pretumt:•[6r• a. I. b:U• c.6J75. d•rl '
262,
0;L'• 'Ells'_•^(e•1L-1r._I_R.'•?y "
1AimItsl Li;r raI?sis 1]n7„• `I}jt- iyI;d
E•
�] l%ielLlikA•rt:
t �citt�!lO l i7;lffife[ar- a ! !a rl. r tJ t1.3, tf t%
Mat Qdm-5i A!n''!- '
I n"0 ity,'L I11{+
MG tC'
,1.J7 15�ia• 1Ls:,k
12 s0
1
] C:}O f PE 1137�27'rIL- Li' I,li:in;l fy3
EM3111Btl7.'r f:rt'dEt:':7 - !
dNn!Iy9tsVFiAriI-,nJa M to 261i..59-19
-
Ean[uatirrq Farl:r,ete+
t a[ya;lt;nal. Mu
140 uji(L 122
Al to 144
? 52 AcDuplabie .
1']tr]rPE'6°,i-1ik?1L Lo+1,Rah'J337
Ll3tuctiureCr,'faria- [
EFatt:Gtt,7ni'arsmPtar•-n:fJ.t!9a3 L:-a.l+;iJ,
• j,lalsir4'KJh.�a.1;�L-.rxs+••:BGta"-+$-ttl ,
���`efunrar,
-_ .
Kid, 0. Ni
".
i(1�fr u111• �iilf
504111
t i
3 fa3 . `vtlr 3rre �fabt�
- .. 11u5.-PFIlT-'-13FfL.L,,'I 17:1-g
Erat..etrur.fSiu:�d-;
.
F-rn!Urr[If:3d'Lfi2'r>PiFr-r1:1.id'ri
'hnu:F'it�"�' �i.,.1,csLnee:?9inz:?�i9
❑5�aiuttfr.',T
.h.157Y5.
ntl.fl3t;5.ai;a"tt]5!
.r7ilsmllm, S4`'
St-J �Q!l: '%lam
JIt1 tiI .1L�4
3.53 I+ni trtit:liJllu:(1
. - 1149(PL113I:,ZQML-Ut L]LY,'WD
l:��iUa!JI!ti Cr72fr7l)
-
..-
:hn2lYsla'1:'huglgsss^>•�u:. Jku.drb7<.
�5'S�^•a:�.'y
.cra!t,Gt!urt l�nn:mefer-S7!1, L:J. c•.rt�G�, d:J.
SiNd., r y,
1_sl
13 to 21MI
. y to ^?StiCj7i¢?'•IE
ISO! I'I']�3c.2'7AL• LtA.1743r:F3E
I vciu hall C +
" -rAni:5;�1:Y1?i AnJ: .IS mete llt:C Q3-lc.
�fft[1rli[It'P
-
�Yei:.$ltaa r�@rn 1718[er-tit L:U.ii,.it3 ,1iF, .
i hal3ium,'[7+'
52C• uc1E 548
^1•sli -0 H-1
'2.35 1ct 5pc�i c ,
. .1L1 , PI7 �J�,=- OhfL• tF,; I�t•\faisgsli
Foa�ir.r!iu71 [:,-1L'- :: • '
F,,•:i�uc•:rerz Fq rtl:nPlcP - X2. G�-i}.•1� ,, '
01i"SNIA& AlmlpmISc
17J!WI!a-V
r•:7(tj,ll,tf.J33ri .. .
44? tc, 1f85
001 3ci c r sl lc
' ' , t17Sf1'C7'-a: �C'S�i...nr t 9?v��3•L
...fid'nttrai,n,� I::�fFr� • 1
-
, -- ,rr,,.1?ha:1`7:7 hn51�fi°=U-r. 7Cif--n,;-7B
�l�tT.11lr+[a^I"
Gi•�r9:i?lb;it"rzril"ICirr-�]•1, J:fi, c.t7.]f�, i[:ij .
F1D•!1-2dfli
}YrIS•i i.'!I }y@16+3$
Ptsrdie 83 of l'P
Page 13 of 16' '
Page 56 of 59

SIGMA-ALOF7[CH flftTC)
Xahod,XPA 200.7 5"(1998)' (Cointhawl
Ana. yti:
Date 2U103.1ir-I 9
Vimad-um, *v I -'
11 li7, i I'LL I's
Zh3c, Zr
1 `901PET 1 MANI lin
!drklyTA V K IF 7,. ..-p -E 3 L. � I s. zVlr4. 18.7 5
Al
I QW. FS11 32.201 L - L at LIVUNVI:lj
P;.,Ln- 20
MuLlinA: LPt
AMAYW
Antimony, Sh
1005 i I-E I 032--'01,11L - 119t I-RA3DII 311
AA-wilic. i's
U110.1 PRIM-2-OMI.. ],.r I
KOEYl)[Ulll, 31"" ' Plill
3r.3 G 05. 17
. '"T16-M
ccmdvc.,d
Final Rl:p-rrt
RosAl Mstgn.%
oeoept.
i_!Jsz, valuo
Whiduv.
209 tigiL 21'
184 V) 2411 -11.73
I.3till wg!L mqn
1 CrU 0 1 r;
1ABO
IX)li
I ('.L^ra:cdn,--•1, Lei 14.v.0 g:,)
05
421 CjI;4
9.35 N`oi. Acceptable
-v VO. I U 2 LiM. 9-r- - u. I . b: R. v, fi. 05, hl .1)
,1IJ91jgVL 4 03
.112 In 4�1_i
2.3D Acl:UFWhlQ
- I
Evirdum.o* Pure-mr,r r . u. r,.,.;b u,
Volul;fql'i .
;,,. 0. Cil 7 1 . Li; r j �, I i'l?, -
At ktpl
z.
C:e.O.; Vj 239
'271 liff,'L 7GE.
•(153 079
f,,.'o
£.QlLzliah
--SIB 11, Klli
1 16
L'Wil-.1111un Crlvr5� I
frGlVirm Flof l 1 luui r ].I
ug.l '234
ILI,-3 cr) M
-1-?l
El
a, d.c.
533 Up
12 1 01�.)
1640 ..
197t4529 WP16.311
pagm 44 a f 1 '6
Page 14 of 16
Page 57 of 59

ERA 92016CI 2009 TNI Evaluation, Final Comp.lete Repo
A Vt'al.eis Corll�dang
4`�
f
Moogan l7oughm-ty
Quality Maitager
Summit Enw Technologies Inc
3310 Win St..
El'fA ID:
EIIIA C,`r[1Storr ar Number
,4genCy.ILt
CdHG0,3?3
379.16t11
Cuyahoga Falls, OH 44223
{330;i 253.821 T
._,__
1-1
.1➢ida
rlatl llgnpAteoptanra
Une LmitEvluat.ian-
VVP Traco,Welsfs ecaff500, foffi 792016cli smdv b•ata, � n4Tatlrtg _ f-rrn..s,•r-r_- s
-
J=A-Analy
...1U[};J
Aluminl:.m py4.
1B•70
--6D - Z_2
�h.,u7
Nat R.nponnr
199+J
114
1C05
Antunn^y I1g;L
be3
452 0M,
NuLR-fporl c
5$I;
43
-fh
1010
Awitlio Ngtl.
194
154-204
NotPcins;erl
1t+M.
11.9
I615
:©nnum IlCI+L
lialrl
larpr]-Z5,. 510
Nf.rR.ep-irmr,
2illa
95.4
11]Z(]
6eryll,um t117 L
Z9.4
78.n - Iri
Nat. Meportrl
tla,$
Ei.L7fi
• 1R�7$
9mm� �g;t,
•270
e499
H.1=I-1'1Gp
9'ntAzmpft,,+Ii::
Cr.,n, i9ro
I1112.'201C
5.38
gfift
.524
L9:rwMiguneo
'D39
4iiUrri•mn Ng;l.
�25
0G1 -ap9'
NCO. I edwf.t r
415
17,9
1Ct97
^-hrryr-ta:m pg+L
697
662-802.
}kdd2r_T/rr_ic
654
31.3
i GSLv
4.017ak Ls-L
1?•G:1
72.2-S'ITFi
WA Ri_-poTioe
Bee
40.p
1U55
nry�ar JgA
4'4
412-aTG
4nl Rrnr.r7 rt
1070
I= utl'1
3340
?U(1-3a-;0
10:pme Qci
33�U
1frG-
1.Ut5
Lea N ,1•
272
2 ,
231 -315
:17-263;
Halka=parson
274
2C2
14.5
1.. t2,
1090
Marvjirnsp pglL
..r_
..._
IKi
tftF.A -uJ
VolF-prv:ej
'.38
"no'Wic.Hrl
NrrL
1620
13f30
1203-1520
.41luG4pS'Y,i
trA:;).. -1fj1
9CS7L'207fF
4.39
1340
64.9
l•InC!Vq.,lstrnr
1'IrU
..115dF'
Sd,aln:nn pgrL
47C
:30r)
't rbgA,
htCnx t:epin!jn
r•«.>c.: t.c„
yw-'2.2:7v3
3. r.
377
20:A
Vrad Finlr runn'r
Sipfrr pryrt
3'S;
312-a77
NO'Hi r'ogei
3Gra
-1 ,1
11 iliU
Stran:wrn 1
purl_
3 K;
gal - n.32
flol Rrp rfcxf
'•83
2 t:§
11{i5'
rhallitstr llr}+L
31
2G2-3 9
Rbt6ta,pcted
3U8
17.9
11N,.r Y
V:nceG,ur.1 _ .. 1.•g:L
054
55,3- 752
slim FOAnnar-
�,I
e45
272
1,t1 t,iafvle, oqarc inducn?Li'Tt PRA'; ii21-A nrcrmlilnrion Lab Catle 1919-L7' Page 5 of 21} �/ L
,'L,r- 1G3r Tnhre. I, ounlnln Pkawy-'301den. CC) 8G403.300 312.0192 �••3.aa.431_ 45e r fax 3u i 4,1 0159 • vfvAvc,fA.g0.carn Proleri:r raxNlr>c-
CO l)
N— LO
4--
O O
L17 00
L0
O N

E. RA 092016 C1 2009 TN Evaluation Final Complete Report
A Watprs. Company
Meogan Dbughiddy
Quartty MaOger
Sutumit E.nv Tech hoWgies fint
331 a Win St.
EPA ID;
ERA Customer Nurnbur:
Abbdipy I D-
Cuyahoga Falls, OM 44223-.
25:5-8211
T141rI
Q'O'ru
-',sj,;noo
I;je:HaPpnnv
AvCu,,jjjarr4v
L Ils
P:is 51udy
y W'Iy4t Name
I 1 Davlallc0
VWIracomwors (Cat# 5Do'-kPfff0320f6CI) Study
.
LI!Ln 14cju— 10-'010
CO G)
LO
4— 4—
0 0
(D 0)
LO
(1)
CY) tm
C13 Co
o n
AC PnalyL-3-S ark, !'YLI,jrJ,d in ER.kWVI:A-.qr;vrocttz;1.00 L'Ib Coda: IS,39-01 OF 24
1E,1941 Table Mountain Pkkvy - Golden. COAM03 - 600.37.2.D'127 -'3IjI3.,Qi.;,A64 -- fox 303.421.01'&q
rri projam j. - C-9--m1ec1

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
_ Facility Name: Harnett County WTP WQ Permit Number: W00014885
WWTP Name: Hamett County Regional WTP NPDES,Number: 00-016-84
Monitoring Period: From ' 01/01/17 To 4/30/17
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved' and alternative performed:
Class A: Fecal Coliform Testing
Alt. 1/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No, Prior Test). Alt. 5/Process to Further Reduce Pathogens Alt.. 6.(Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly- Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
It applicable to alternative perlormen l lass
A or l lass i5 complete the ionowing monitorin
aam:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
_ of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10to the 6th
CFU
MPN/g
Coliform
power per gram
of total solids
CFU/g
CFU
1000 MPN per gram of
200
200
CFU/g
0
4/yr
Grab
9222D
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform.)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: - N/A
Option/Alt. 1
Option/Alt. 2
Option/Alt: 3 Option/Alt; 4 .
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake) _
Option/Alt. 5
Option/Alt. 6
Option/Alt. 'T Option/Alt. 8
. (14-Day Aerobic)
(Alk Stabilization).
(Drying — Stable) (Drying —Unstable) _
Option/Alt. 9
Option/Alt. 10
(Iriiection)
(Incorporation)
No vector attraction reduction alternatives were performed _
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC -02T. 1106 and the vector attraction.
reduction requirement. in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this -statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false• certification including fine and imprisonment."
Allan Rex O'Briant, WTP Superintendent
Pre d title pe o t) Land Applief Name and Title (if applicable) (type or print)
47griature of Prepder* Date Signature of Land Applier (if applicable)' Date
*Preparer is defined in 40 CFR/art503.9(i) and 15A NCAC 2T.1102 (26)

Cameron Testing Services, Inc. Laboratory Report
Synagro _ v 170458
Harnett WTP e. = Yes
_ Sample Information
W. Varier r M5 - = 03116/17 � of C. Cameron
An4lyses and Results
170458 01
i r Fec, COIIfoRTt•S
200 MPNfg 10
03/17/17
MAJ.
Gr TS (%}
1.00% o.ot
03/17/17
02 :.h-b#
i r Fec. Colifortn-S
<20p MPN/g 10
03/17/17
sWa,°
pr TS (%)
0.900% % o.ol
03/17/17
Report
Review
Lab Director I Date
NC DENR#654
NG PHHS #37799
US EPA #NC01918
03/16117
9223 - MPN
2540 G TS
9223 - MPN
2540 G -TS
219 S. Steele Str.
Sanford NC 27330
919-208-4240
[e-mail]

219 S. Steele Str. i
Sanford, NC 2733a Cat71et'On T@S'�Iilg Sel'VICi'S, Inc. Chain of Custod v
ph.,.,A• n1a_9nn-Alan - NC WW/GW Cert. #664 NC PHHS Cert# 37799 US EPA NCO1918 Page i of
ra1;1a�any}
h"'r* ��
4 {
k�� llj�vr,i
). ;ICantal.ctsg
k, s
All
asst c
{ }
S`/na r0
J ,7
11Vill Varner
284 Boger Rd.
�mait^!
�
POW 917
R
"�y,
,�xt
i
-rs» �_2
vwamer s na ro.comy
@ Y 9
33fi-909-8627
f FiIt,�1��
`F ti L
Q'v' L.�
A y
SampleyT� )p
ti; � w Nr t� r
i+i �{ y 51r`'
�'�
� ��/y ��r �,
biseS. .li }a..:f+r,'i
,ti .rn ,.. �,.�._ •t
rrsrr�_7�i
-14� I ¢�
s
�
�,; ��
G s R
�9*
iif.
V�t� k�
:. �e ixe a6
..
Mocksville NC-27-028
�/-y� �y y1" (jam( /) / /y//�)
`-%! ",7,0 / j 1
�'�/`_
Name.�v✓�1��� Signature:
M i � ..rr.l7 J . � � .-. ,.,
;t�J`.5 V, �.� •- �r .�',h.�
.i 1.�r �,.IjY i;�, d..+r'i-' JJ'I.,r1Y,:
1 r. ti� .:.,.. r� ,.,I.
Sample 1D
.xµ`{. 1 - �.i{'. (A ��;14
C.R ._. vn r. ...«�a5'yJi:-'1
�iti'i `'Iv'.�J�.-if..1�3
rrtSa Pie�I.nor,•m
o I—
r
�..-u.'.'.II"+(alp.
�.
Q
E i
o
V �
x ?
n
� �
(
�q.;,:-.•�.,
i I
I o
N Ir
�- i m �
- X .
i 'y
i n�
r �
_tom' "] wl
_m
H o
o
! +Y.Y 2iY M J:. 7_ra f 'I.^ =n�:u 15u,'. rckt:::�h° a n,.., ...:7 ti„'t
,.�„ jyy , ,• � e>;.:a
d7T i 4r kke..v rt-0 Ci
Preservatives (U)npresenred� H(C)� t
fi2(S}O4 F�(N)03; (Na)T14o' f
a ..
JSM,ci�" •cy
��, 111•Fj �:'
e�rIs
l�rn G 110
- "--
I I
!
- _[
-e-Bap-Br�fi -Test
QS 1
1
-
T 5 a fSh 44PIL11
3
-
.... �:,:, - r... _.� r. ,.._... ..
�y z (y y'.+�'t":';II{IiTQ�II•yIIP
J\i liirJl... U�.�.�1',ftiO!ai?t+Y.;�ri"fvtGi'..�iG-
,. ., :.>.r .-,+�. �,,:. .. .-,y,:�..:
IIF.F.�,,J..��v�,.. �.. ..!-r,.:r_.ae-.s-
•:n .,ar%rw-s�S4„`a'•'-•^...•n-.,.. r+:,•:.tj�.�
---r :::=::
1";••-3+7,;-'"�c:
�`:^�:
s.Rw
b
.9iiJ
V-.: r_=.-,- d:,:. r.:-.....a^�-cr
r'�, `'.,'3 e�.IVC`L+�.>:..,.�sf:'
w�KiY,:'k%S�v.
w'
- ➢: ='�•L
�_'�"''•Swh;,;,.e�
,.7''y'. .. ,.e..�..ac
4-- u:-
ti
rig � 'ti3 'h!``: :'.1+"
_.�'. f.,P',`#a Y�1 I .5"RT5>,:�.
:Et, D..af I.T�'
t(. .k...,
Rush work will require prior approval. Additional charges will apply

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Harnett County WTP WQ Permit Number:
WWTP Name: Harnett County Regional WTP NPDES Number: _
Monitoring Period: From 5/01/17 To 6/30/17
WQ0014885
00-076-84
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1100 - Please indicate level achieved and alternative performed:
Class A: Fecal Coliform Testing
Alt. l/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
11 Up plWa VIC
Parameter
LU a1L01114L1V.0 PCIAU1111VU t-
Allowable Level in Sludge
4[ J to Ul a..laaa L �.vw icw
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2xl0 to the 6th
CFU
CFU/g
Coliform
power per gram
of total solids
CFU/g
CFU
1000 MPN per gram of
106
106
CFU/g
0
4/yr
Grab
9222D
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: - N/A
0ption/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.) — See Tab #1
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Allan Rex O'Briant, WTP Superintendent
—71 Land Applier Name and Title (if applicable) (type or print)
gnature of Preparer* Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CF Part 503.9(r) and 15A NCAC 2T.1102 (26)
Date

Cameron Testing Services, Inc.
Laboratory Report
NC DENR #654
NC PHHS #37799
US EPA #NC01918
a4�lie .°
'S na ro
y
olgi
170847
_ - EE m, i
c
Harnett WTP
v , iy
atc
ves
LIMIT.
Sample Information
_
il 76ar
f;z�sarnpfed>
W. Varner �3atsr
05l23l17 �Ff`eceiv"e'
S. Bullard ,' ; 05123/17
u 0-1
Analyses and. Results
170847 01 Harnett VVTP-1 Singe Gr
Fec. Conform-S'
<106 MPNIg 10
05/23117
ERP
9223 - MPN
swdoe Gr
TS (%)
1.69% 0.01
05/23117
ERP
2540'G -TS
02 Harnett WTP-2 nano. Gr
Fec. Coliform-S
106 MPNIg 10
05/23/17
ERP
9223 - MPN
snudoe Gr
TS (%)
1.69% % mo1
05/23117,
ERP
2540 G TS
Report f7S/3f�r'? _ Review
Lab Director Date
919-208-4240
219 S. Stecle Str.
chrisCca
Sanford NC '1.7330 merontesGngco�

219 S. Steele Str.
Sanford, NC 27330
2nQ 4240
Cameron, Testing Services, Inc. Chain of Custody
NC WW/GW Cert. #654 NC PHHS Cert# 37799 US EPA NC01918 Page of
Phone. 919-
Coirpaiiy: Synagro
Email
[e-mail]
CTS lab use only
_
— - - —
-- -- - -
Win Varner
-
�'� `M2'
_ --- -
336-909-8627
— ---
Sample Temp i
Pre,_
rc�
'A ddfe9s•-(City, 284 Boger Rd.
Fax
- Arrive: I - — -
- -- -- -----
-- -
- - --
.--
S:fate, Zip)
Mocksville, NC 27028
:Notes:
Due: I--
_—
p:^--,
r
-- ,
.
Regulatory Rush j
(Y/N) (YIN)
G'olEectetl: Name:. ((-
Signetur-
-Sam,ple.:lnfarmation
Number o . bottles
Requested Ar►al<ysis;,.
x
'-'
Z
@ O n. - �,
�-°
�.
°'
Preservatives: (U)npreserved, H(C)I,
ID
Sample ID
}!cj
a is a
"'
H2(S}04, H N o3, Na Thiosulfate, Na Q H,
(} ( ) ( )
0 i= 0 C9
o
=
m of r r
o
Other (X}, Indicate
-
c
3-17
o
-Rel:in: ti` lied,:
Received:
Date/Time':: -
Rush work will require prior approval. Additional charges will apply

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Harnett County WTP WQ Permit Number: WQ0014885
WWTP Name: Harnett County Regional WTP NPDES Number: 00-076-84
Monitoring Period: From 07/01/17 To 09/30/17
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A: Fecal Coliform Testing
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (C1ass.A only) indicate "Process to Further Reduce Pathogens".
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
74.. .. (Place A nr f]o Rl r nWo *hn fnllnwina mnnifnrina dnfn-
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytica
Excee-
of
Type
Techniqu,
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6h
CFU
CFU/g
Coliform
power per gram of
total solids
CFU/g
CFU
1000 MPN per gram of total
<81.8
<85.7
CFU/g
0
4/yr
Grab
9222D
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: _ N/A
0ption/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
Optioabiln/Alt. 6
Option/Alt. 7 Option%Alt. 8
(14=Day Aerobic)
(Alk Stization)
(Drying — Stable) (Drying- Unstable)
Option/Alt. 9
option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1 t06 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment"
Land Applier Name and Title (if applicable) (type or print)
*Prepares is defined in
bate Signature of Land Applier (if applicable)
Part 503.9(r) and 15A NCAC 2T.1102 (26)
Date

Cameron Testing Services, Inc. , Laboraltory Report
Synagro
,`- GTS p'►�c
Harnett VVTP
i�FRe�ii�ai�a
Sample Information
W. ti rrtor y 15a eE�} 071/91/7
� Rec�Tved
Y1
Analyses and Results
NG DENR#554
RG PHHS #37799
US EPA #NC4T910
171206
. Yes
M. SfPri8 071`E 9117
171205 01 Gkctc er Far. GOGPOrm-S
<81,8 htpn eg 10
0711W7
ERP
9223 - MPN
axe Gr TS (%+)
2,20% % 6.61
07124117
ERP
25.40 G -TS
42 Or FeC. Cbiirorrh-S
<35-7 MPNki 10
07119117
ERR
9223 - MPN
Gr TS (?A6)
2.1 4%
07124117
ERP
2540 Q -TS
Report
Reviewj/_f
Lab Qiret ,or Date
20 S; SWId Str, 919LZQ84240
5anfardNC 2F330 cfrri�i!u�nsermrt, stingy; cwn

.219 S. Steele Sir. Cameron Testing Services- Inc. Chain of Custody
SanFord, CSC 27330
Phone: 91S-208-4244 C.MIGWCen.::4654 NO-PHHS Oert g 37799'US EPA ;N001918 page —Of
G tpang: Email, -- — - CTS lib us-G on.IY
Contact:. r Phone, Sampre Temp Praj.
Address (City, - -- - -- - Fax: Arrlue:
State. zip) — -- • -- - • - - - - -- --
Notes'. Due..
Prolpd. R?gulafary Flush
o9leCted; Namii: V '+L• [f �I! �,'^` SfgRR �r ��
Sample JF forMatlon I uMber-of bottles Requestedi Arnalysis--- - _
na v CL -0, A j t ms Preservatives; (U)npresenred, .H(C)i, CTS Lab
SaMpJt? JD 15 o a ,? 0 C7 a M2(p)G4, H(N)t33, (Na)Thlosultate, N2(0)H.', 11
C)th:er{X),.Jndicate
f q "
R lin i&hed; Receive Patelrime
Rudd work will require prior approval. additional charges will apply

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Harnett County WTP WQ Permit Number
WWTP Name: Harnett County Regional WTP NPDES Number
Monitoring. Period: From 10/01/17 To 12/31/17
WQ0014885
00-076-84
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A: Fecal Coliform Testing
Alt. 1/A (time/temp)
Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying
Anaerobic Digestion
Composting Aerobic Digestion
Tf annlicable to alternative performed (Class A or Class B) comnlete the following monitorinLy data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytica
Excee-
of
Type
Techniquf
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the
CFU
CFU/g
Coliform
power per gram of
total solids
CFU/g
CFU
1000 MPN per gram of total
<118
<118
CFU/g
0
4/yr
Grab
9222D
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: - N/A
Option/Alt. 1
Option/Alt. 2
(VS reduction)
(40-day bench)
Option/Alt. 5
Option/Mt. 6
(14-Day Aerobic)
(Alk Stabilization)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate, statement)
Option/Mt. 3
Option/Alt. 4
(3 0-day bench)
(Spec. 02 uptake)
Option/Mt. 7
Option/Mt. 8
(Drying — Stable)
(Drying — Unstable)
No vector attraction reduction alternatives were performed
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment." '
Allan Rex O'Briant, WTP Superintendent
Prepa n tiM,-�in Land Applier Name and Title (if applicable) (type'or print)
a e of Prep er* Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CF art 503.9(r) and 15A NCAC 2T.1102 (26) .
Date

Cameron Testing Services, Inc.' Laboratory Report DENR#654
NC PHHS #37799
US EPA#NC01918
Synagro G it o �. 111792
roe Harnett WTP-'Class A Yes
Sample Information
e ar W. Varner 14' f 10/25/17 irkeceluea M. Sims DafeT ; 10125/17
Analyses and Results
�� f.,��, � ai�',i,'Y�_�� � h�� �����0' ,p"�`t.,N-� s`f�l'—'�-19s �� {��fr-3 '��c-G --3� z. 3 ��'.,I cr�_`�ir .� `1 y�-Q� � �-�£, -•.•i � ♦ �� +I
--�{'.. "ice � �f � �_+i �. ii �/ A ���: -�^ t z� 4li.C.;,� .^.K? L •h +.47 3� k I�.I+7 �� t.SRKi�x=�Q�iid�.�J` 1
as��,. p a. b1D` �� ,_ �=•eS,�kYt�t .��E;a.'� `fir 'x'�naty ''� j r �r+�.tReSnit,�"� r+�uG "� d'���� ea`�`'a. T �=r ,. � •s-�,;:�.�:;
^�tf�.�:tiX�
0.�•��
171792 01 Harnett.WTP 1 Studgo Gr Fea Coliform s <118 MFN19 10 10/25/17 ERP 9223 - MPN
sludge Gr TS (°/a) 1.52% 0.01 10/25/17 ERP 2540 G TS
02 Harnett W fP 2 sludge • Gr Fea, Coliform=S <118 MPNIg 10 10/25/17 ERP .9223 - MPN
Sludge Gr TS (%) 1.53% 0.01 10/25117 ERP 2540 G -TS

i
219 S. Steele Sir. Cameron Testing Services,. Inc.
Sanford, NO 27330 NC WW/GW Cert. #654 NC.PHHS Cert# 37799.US EPA NCO1918
Chain of Custody
Page of
Phone 9i9 iuu-424u
sd
liRY
Email'L>}
,
FR.Ni J'{tk
U
lry'lll ���i II
o
.k1p T-h pt y�4 Yyj+ 'VY'ly I -ail
I
ttf.A.
t il� I(;
Synagro
P�
[e-mail]
as= aCL ple Temp
lair
f� tact:
Will Varner
pr
336-909-8627
's,f`�;l',
r
La`}) .SaH
'��(tiy�J Ws
J
r
J.
{i
Rd. Boger 284
4,0iS!=.Ti.=•ci�„
fY =� xz �
l ill 1, )r,�pv
9
�"
,
i LnYr�"S
w;PyF;;
;
Mocksville, NC 27028Mot
n tQ�eCt yr:=n{�JZCi��
lr�t!_
k3R�rua,g.�,'.��s
it/�i'�nn
Ilr!TEt ln.ti7'c! kilt
+` 'et Name: Signature
F i, rin]wTy4. _
P:+-i :. .C'{! o "t 'l' EnT_w= .'wT 1 '-^_Ri✓f..,q+,ry,�Y - r+� �I^lyp'jo 4yA.,. V'v'4'�L �LkR. t' t�}`F. • yr I )✓'V:.. lk.l 1��.}r{ yfi� It
�a�.l} .�. `. C ,,,, •.-sm,-'• •V' ('On i -%w' ^' . r` ..b" ..mot.`. .�:+Jf .-_ . ,) '-a.. .r_ t'i : e'.z,. . �7F'iF:.. -.'c �, { e J -Mkt !a3 "& f�C 'C ' Y
'm stiY.a e V5 ,H. E�. t... y, u1'�![. ..f. •"fA''1\,i - ,1. .iy .ety ,� f, Y_�u ,�L-:� ec:. FI' Ei' .1'.; i ;2'w'C+. l It'd
.'?gy�?y57,rP.-,�!'. •.. �� .,.� E�>.7..,.'��7 �I�.jb_�c�,:.�t�ja�Samn e�lnforina�`io'�n�,:.�-<.;:_,.� �,�_.,.:,.�,�, �„_ .a z,� � �'Request�e oa �u� r ;)� x %: Kn
y '11Y,_ik t%f!S I Jr1
�, �,,-�, �, �!x.�-. �u � ,a,f, I:v�
_ ,. �;?�,,>r�� C
,(".Sr. J- Nai-�}N� u`�,:I^.)'1:_4i.Mii.lm.n.4.__ fLe• ...._�.�,�✓-.+,.v..uY:JrS;A:Y.-:'�K:-.-- w.i.� !Y.a - ..i :.1....1'J. -v[
9�'l.�cv J�j,�. �£..11 1iY, �h, �$" _
X I z m O w N, -. Preservatnres (U}n'preserved `H(C}(}"'
N Q- M •}� fl1 �j Clf m 2 L -� r it 3i7
} o �. U a H2(S)04 }H(N}Q3, (NajThtosulfate, Na(Q)11;Dd}
Sample 1®
j
p o m —' o I Other (Xis fndEcate rl p FRS' Ny l� �1 E
G] H (9 j o T
U r L 7
I I = ( 8 I L
!
I
�
!1iI'
I
pa-,y..-.. -.. ..5.tr •wv -'�-" ��
l5uhq. F!'•^%�.... s ay,�(,s?,,:.
Ijlshp yY7 's~`'� I Y 'C i yfj FP..1i -,.F X'�i'-�T .!�' � �4
jn:. �
. .•,tt>>-k-<.nk s I'.>7t".:.�ri���: �'yi4 +a,r._ft? 7'i�.: b'�`;'{ 7 a.1- CkfL i4 yr_f ?tglrr
ruEk..;,.k}I3'
�-.a s�•' : �.".�= ��C Receiu,�di. A.�..::aa:t, .w $'%-=��p'-J.i,'rrs�+'"�m") �".n [,LI!.� Ir(-. :lv._
in#, ... 1.✓�h&GfN./ .�f)T �`Mi:'il ...I..,a ,5a ,l,c..._
Rush work will require prior approval. Additional charges will apply