WQ0006101_2017 Annual Land Application_20180222

A
CITY OF DUNN, NC
RESIDUALS LAND APPLICATION, PROGRAM
Permit No. WQ0006101 .
2017 ANNUAL REPORT

City of Dunn, NC
Residuals Land Application Program
2017 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. , Annual Residual Sampling-Summary'Forms, Residuals Analyses,
& SAR Calculation Pages
3. Annual Land Application Field Summary Forms
` 4. TCLP, Analyses
.5. Pathogen Reduction/Vector Attraction Reduction
6. Soil pH & Lime Application Records

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00006101 County Ham ett Year 2017
Facility Name (as shown on permit) Dunn WWTP & Citvof Dunn WTP NPDES No. NC0043176, 03-43-010
Land Application Operator Synagro Phone# ,[phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. HNO, skip Part A, and PartB and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: 13
Total number of fields utilized for land application during the year: 8
Total amount of dry tons applied during the year for all -application sites: 308.19
Total number of acres utilized for land application during the year: 154.6
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2017 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other -monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .I 105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best o y e e and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false informati , i 1 the possibility of fines and imprisonment for
knowing violations."
1•(euschc�'
City Manager
Permittee Name and Title (type or print)
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

2017 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION
DUNN, NC
DUNN, NC WWTP`'AEROBICALLY DIGESTED LIQUID
DRY METRIC
MONTHNEAR
AMOUNT UNIT
DRY TONS
UNIT "
TONS
May 2017
719,200.00 G
' 82.48
D
74.80
-September._20.1,7_ . _. '
_46.5,0.00:.00 G.
51..39..
__. D_
_ 46.61_.
November 2017
390,600.00 G
43.17
D
39.15
YEARLY TOTAL
1,574,800.00 G
177,.04
D
160.56
DUNN,'NC WTP LIQUID
DRY METRIC
MONTHNEAR
AMOUNT UNIT
DRY TONS
UNIT
TONS
April 2017
576,600.00 G
59.63
D
54:09
September 2017
756,400.'00 G
43.84
D
39.77
November 201.7
477,400.00. G
27.68 ,
D '
25.10
YEARLY TOTAL.
1,810,.400.00 G
131.15
D
118.96

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this -form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be.analyzed than those required to be summarized on this form.
Permit Number: WQ0006101
Facility Name: DUNN, NC
NPDES# : NCO043176
or WQ# (residual.only)
WWTP-Name: DUNN WWTP
Residuals Analysis Data
Product Type AEDLIQ AEDLIQ
Date Sampled (grab) or 03/02/17 08/31/17
Date Composited
Percent Solids 2.75 2.65
PARAMETERS (mg/kg dry weight)
Arsenic
<5. 63
. 7.61
Cadmium
<2
<2
Mercury
<0.679
0.513
Chromium
30.3
23.1
Copper
225
256
Lead
34.2
44.5
Molybdenum
<6.12
7.8
Nickel
15.1
.14
Selenium
<5
<5
Zinc
314
444
Total Phosphorus
19300.
24500
TKN
64900
5980.0
Ammonia -Nitrogen
4710
13200
Nitrate and Nitrite
<139
1710
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant. penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(SIGNATURE OF P
ARER)
Date 91I et
DENR FORM RSSF (5/2003)
Printed; Friday - February 9 2018 at 09:48:34 for: 2188 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to: be analyzed than those required to be summarized on this form
Permit Number: WQ0006101 .
Facility Name: DUNN, NC
NPDES# : NCO043176
or WQ# (residual only)
WWTP Name: DUNN WWTP
Residuals Analysis Data
Product Type - I
AEDLIQ
AEDLIQ
Date Sampled (grab), or 03/02/17
08/31/17
Date Composited
Percent Solids
2.75
2.65
PARAMETERS (mg/kg dry weight)
-
Aluminum
12900
8980
Calcium
7370
9300
Magnesium
3720
3570
pH
6.37
7.03
Potassium
6040
6160
Sodium
1400
1450
Laboratory.
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Xi�'°QJ Date
(SIGNATURE OF PREPARER)
NR - Data Not Reported or Data Not Required
DENR FORM RSSF-B (7/2002) Printed: Friday - February 9, 2018 at 09:49:13 for: 2188 01

Page: 1 of 2
Report Number: 17=062-0206
•
Account Number: 46789
Way
7621 Whitepine Road, Richmond; VA 23237
-point..
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www.waypointanalytical.coriv
Send To: Synagro Central LLC/ Dunn
Project: Dunn.WWTP
Mary Brewer
NC Cert#257
284 Boger Road
Mocksville , NC 27028 "
REPORT OFANALYSIS
Date sampled:'3/2/2017 11:00:00
Lab Number: 62676-
Date Received:. 03/03/2017 00:00
Sample Id: Dunn WWTP
Date Reported: 03/13/2017
PARAMETER
RESULT
RESULT
QUANTITATION
Total Solids *
- 2.75 .
27500
100.0
R D
03/03/2017 14:45
SM-2540G--
'Moisture *
'97.24
100.0
R D
.03/03/2017 14:45
SM-254013
Total Kjeldahl Nitrogen
8.49
64900
: 50.0
JM
03/07/2017 13:35
SM-4500-NH3C-TKN
Total Phosphorus
1.93
19300
100
JTR
03/09/2017 22:01.
6010C'-
Total Potassium
0.60
6040
1000
JTR
03/09/2017 22:06
601 OC
Total Sulfur
0.79
7890
100
-JTR
03/09/2017 22:01
6010C
Total Calcium
0.74
7370
.100
JTR
03/09/2017-22:01
6010C
Total Magnesium
0.37
3720
100
JTR
03/09/2017 22:01
6010C
Total Sodium
0.14
1400"
100
JTR
03/09/2017 22:01
6010C .
" Total Iron
19400
100
JTR
03/09/2017 22:01
6010C
Total Aluminum
12900
100
JTR
03/09/2017 22:01
6010C
Total Manganese
203
5.00'
JTR
08/09/2017 22:01
60106
Total -Copper,
225
5.00
JTR
03/09/2017 22:01
6010C
Total Zinc
314.
5.00
JTR
03/09/20.17 22:01
6010C
Ammonia Nitrogen
0.47 .
4710
• 50.0
'JM
03/08/2,017 09:50
SM-4500-NH3C
Organic N
6.02
60190.'
50.0
03/07/2017 13:35
CALCULATION
Nitrate+Nitrite-N
139
-.89
SJB
03/07/2017 10:51
4500NO3F-2011 -•
All.values are on a dry weight basis except as noted by asterisk. Detection limit.on all N series is on a wet basis.
,
Our reports and letters are for the exclusive and confidential use of our clients, and may not be re rmay reference be made oduced in whole or part, nor
P Y P Y any
to the work, -the results, or the company in any.advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Laboratory Supervisor

Page: 2 of 2
Report Number: 17-062-0206
Account Number: 46789
Send To: Synagro Central LLC/ Dunn
Mary Brewer
284 Boger Road
Mocksville, NC 27028
Lab Number: 62676
Sample Id: Dunn WWTP
a
Wa Y-po
ANALYTICAL
Project: Dunn WWTP
NC Cert#257
REPORT -OF ANALYSIS
-Total Cadmium
<2.00
2.00
Total Chromium
30.3
5.00
Total Nickel
15.1
-5.00
Total Lead
34.2
5.00
Total Arsenic
5.63
3.00
Total Mercury
0.679,
0.400,
Total Selenium
<5.00.
5.00
pH (Standard Units.)
6.37
1.00
Total -Molybdenum
6.12
-5.00
Comments:
SULFUR AND ORGANIC NITROGEN NOT
FOR COMPLIANCE PURPOSES.
7621,Whitepind Road; Richmond, VA 23231
Main 804-743-94011 Fax [phone]
www.waypointanalytical.com
Date Sampled: 8/2/2017 11:00:00
Date Received: 03103/2017 00:00
Date Reported: 03/13/201.7
JTR
03/09/2017 22:01
601 OCI
JTR
03110120 1.7 13;09
601 OC
JTR
03/09/2017 22:01
6010C
JTR
03/09/2017 22:01
601 OC
JTR
03/10/2017 13:09
6010C
SJB
03/06/2017 14:56
SW-7471 B,
_JTR.
03/10/2017 13:09
601 OC
im
03/06/2017 09:30
SW-90450
JTR-'.
03/09/2017 22:01
6010C,
-All values -are on a dry weight -basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor May any reference be made
to the work, the results, or the company in any advertising,
rtising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Laboratory Supervisor

Sodium -Absorption Ratio Calculation (SAR)
Product Code Product Name , Sample Date Report Range Ratio
2188-01-AEDLIQ-NC . DUNN, NC WWTP•AEROBICALLY DIGESTED 3/2/2017 11112017-8/31/2017 0.5480
LIQUID
Na-mg/I = (Na mg/kg x % Solids) =.100 = (1400 x 2.7500) _ 100 = 38.5
Ca mg/I = (Ca mg/kg x % Solids) _ 100- (7370 x 2.7500) = 100 = 202.675
Mg mg/I = (mg mg/kg x % Solids) = 100 = (3720 x 2.7500) _ 100 = 102.3
Na meq = Na mg/I = Molec.Wgt.Na = 38.5 _ 23 = 1.67391
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 202.675 = 20 = 10.1338
Mg meq = Mg mg/I = Molec.Wgt.Mg 102.3 -= 12 = 8.525
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.67391 _ SgrRoot[0.5(10.1338+8.525)] = 0.548033
Printed: 2/9/2018
Page 1 09:52

Page: 1 of 2-
Report Number: 17-244-0208
Account Number: 46789 "
Submitted By: Chad Hayes
Send To: Synagro Central,LLC/ Dunn
Mary Brewer
284 Boger Road
Mocksville , NC 27028
'Lab Number 55937
Sample Id : Dunn WWTP
Waypoint,
ANALYTICAL
Project: Dunn WWTP
REPORT OF ANALYSIS
1621 Whitepine Road; Richmond, VA 23237
- Main 804-743-9401 ° Fax [phone]
www.waypoint-analytical.com
Date Sampled:.8/31/2017.11:00:00
Date Received: 09/01/2017 00:00
Date Reported: 09/11/2017
Total Solids *
2.65
26500
100:0 ,
JM
06/01/2017 15:00
SM-254OG
Moisture*
97.34
100.0
JM
09/01/201715:00-
SM-2540G
Total Kjeldahl_Nitrogen
5.98
59800
50.0
JM
09/05/2017 1'0:35
SM-4500-NH3C-TKN
'Total Phosphorus
2.45
-24600 '
100
MOS
09/11/2017 14:58
6010C
Total Potassium
0.62
6160
100
MOS
09/11/20.17 14:58
- 6010C ;
Total Sulfur
0.94
9390
100
MOS
09/11/2017 14:58
6010C
Total Calcium
0.93
9300
100
MOS
09/11/2017 14:58
6010C
Total Magnesium
0.36
3570
100
MOS
09/11/2017 14:58
6010C
T6tal'Sodium
0.15
1450
100
MOS
09/11/2017 14:58
6010C
Total Iron
23100
100
MOS
09/11/2017 14:58,
6010C
Total Aluminum
8980
100
MOS
09/11/2017 14:58
6010C
Total Manganese
197
5.00
'.MOS
09/11/2017 14:58
6010C
Total Copper
256
5.00
MOS
09/11/2017 14:58
6010C
Total2inc
444
5.00 .
MOS-
09/11/2017 14:58
6010C
Ammonia Nitrogen.. .,
1.32
13200
50.0
JM
09/05/2017 10:35
SM-4500-NH3C
Organic N
4.66
46600
50.0
09/05/2017 10:35
CALCULATION
Nitrate+Nitrite-N _
1710
2.17'
SJB
09/08/2017 09:52
- 4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection
limit on all N series is on a wet basis.
1 A�CG
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining ourprior written authorization.
'Pauric McGroary
Agronomist

Page: 2 of 2
Report Number: 17-244-0208.
Account Number: 46789
Submitted By: Chad Hayes
Send To: Synagro Central LLC/ Dunn
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 55937
Sample Id : Dunn WWTP
Waypoint. 7621 Whitepine Road, Richmond, VA23237
Main 804443-9401 ° Fax [phone] .
ANALYTICAL www.waypointanalytical.com
Project -:.Dunn WWTP.
ANALYSIS.-.
Sampled: 8/31/2017 11:00:00
. Date Received: 09/01 /2017 00:00
Date Reported: 09/11/2017
Total Cadmium
<2.00
2.00 , -
MOS
09/11/2017 14:58
Total Chromium
23.1
5.00
MOS
09/11/2017 14:58
Total. Nickel
14.0 _
5.00.
MOS
09/11/2017 14:58'
Total Lead
44.5
5.00. ;
MOS
09/11/2017 14:58
Total Mercury
0.513
0.400
SJB
09/07/2017 16:18
Total Selenium
<5.00
6.00.
MOS
09/11/2017 14:58
pH *
7.03
1.00
JM=
09/05/2017'10:35
Total Volatile Solids
67.16 671600
100.0
JM
09/01/2017 15:00
Total Molybdenum
= 7.80
'5.00.
MOS
09/11/2017 14:58
Comments:
NC CERT#257, SC 'CERT#9300 70.01
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE -PURPOSES.' -
All values are on a dry weight basis except as noted by asterisk. Detection limit on'all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to -the work, the results, or the company in any advertising, news release, or other public announcements without obtaining ourprior written authorization.
6010C .
6010C
6010C
6010C
SW-7471 B
6010C.
SW-9045D
SM-2540G-
6010C
60wr
Pauric.McGroary
Agronomist

Sodium Absorption Ratio Calculation (SAR)
Product Code 'Product Name -, Sample Date Report Range Ratio
2188-01-AEDLIQ-NC DUNN, NC WWTP AEROBICALLY DIGESTED 8/31/2017 911/2017-12/3112017 0.5256
LIQUID
Na mg/I = (Na mg/kg x % Solids) + 100 = (1450x2.6500) + 100 = 38.425
Ca mg/I = (Ca mg/kg x % Solids) + 100 = (9300 x 2.6500) + 100 = 246.45
Mg mg/I = (mg mg/kg x % Solids) + 100 = (3570 x 2.6500) + 100 = 94.605
Na meq = Na mg/I + Molec.Wgt.Na = 38.425 _ 23 = 1.67065
Ca meq = Ca mg/I + Molec.Wgt.Ca = 246.45 + 20 = 12.3225
Mg meq = Mg mg/I + Molec.Wgt.Mg = 94.605 + 12 = 7.88375
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.67065 + SgrRoot[0.5(12.3225+7.88375)] = 0.525603
Printed: 2/9/2018
Page 1 09:52

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those -required to be summarized on this form.
Permit Number: WQ0006101
Facility Name: DUNN, NC
NPDES#:
or WQ# (residual•only)
WWTP Name: DUNN WTP
Residuals Analysis Data'
-
Product Type
WPL
WPL
Date Sampled (grab) or 03/02/17
08/31/17
Date Composited
Percent Solids.
2.48
1.39
PARAMETERS (mg/kg dry weight)
Arsenic
<3
11.6
Cadmium
<2
<2
Mercury
<0.4
<0.4 .
Chromium
101
78.5
Copper
37.8
24
Lead
25.8
10.2
Molybdenum
<5
<5 .
Nickel
14.9
6.63
Selenium
<5
<5
Zinc
67:6
42.5
Total Phosphorus
1820
1960
TKN
8840
7860
Ammonia -Nitrogen
2010
<50
Nitrate and Nitrite
<2.12
154
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system -
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant enaities for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X Date J 8
(SIGNATURE OF PREPARER)
DENR FORM RSSF (6/2003) Printed: Friday - February 9, 2018 at 09:48:46 for: 2188 02

i
ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0006101
Facility Name: DUNN, NC
NPDES# :-
or WQ# (residual only)
WWTP Name: DUNN WTP
Residuals Analysis Data
Product Type WPL WPL
Date Sampled (grab) or 03/02/17 08/31/17
Date Composited
Percent Solids 2. 48 1.39
PARAMETERS (mg/kg dry weight)
Aluminum
131000
95800
Calcium
1010
1140
Magnesium
1020
709
pH
5.50
6.24
Potassium
825
445
Sodium
610
865
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X� Date
(SIGNATURE OF PREPARER)-
NR - Data Not Reported or Data Not Required
DENR FORM RSSF-B (7/2002) Printed: Friday - February 9, 2018 at 09:49:24 for: 2188 02

Page: 1 of 2 .,
Report Number: 17-062-0205.
Account Number: 46789-
Waypoint.
7621 Whitepine Road, Richmond, VA 23237
Main 804443-9401 ° Fax [phone]
ANALYTICAL :
www.waypolntanalytical.com
" Send To: Synagro Central LLC/ Dunn
Project: Dunn WTP
Mary Brewer
NC Cert#257
284 Boger Road
- Mocksville., NC 27028
REPORT .OF.ANALYS/S
Date Sampled::3/2/2017 13:15:00
Lab Number':,. 62675
Date Received: 03/03/2017 00:00
Sample Id : Dunn WTP
Date Reported: 03/13/2017
RESULT
RESULT
QUANTITATION LIMIT
ANALYSIS
METHOD
" Total Solids *
2.48
24800
100.0
- R D
03/03/2017 14.45 SM-2540G
Moisture *
' 97.51
100.0
R D
03/03/2017 14:45 SM-2540G
Total Kjeldahl Nitrogen
0.88 ,
8840
50.0
JM
03/07/2017 13:35 SM-4500-NH3C-TKN
Total Phosphorus .
0.18
1820
100
JTR
03/09/201.7 21:52 601 OC .
Total Potassium
0.08
825
100 .
JTR
03109/2017 21:52,, 6010C
- - --Total Sulfur- - - =
1,27 --
12700
- . - - _-__ -.. _100_
_JTR
03/09/2017 21:52 . 601 OC"
Total Calcium
0.10
1010
_100-
JTR
03/09/2017 21:52 6010C,
Total Magnesium
0.10
1020"
100
JTR
03/09/2017 21:52 6010C
Total Sodium''
0.06'
610
100 ".
JTR .
03/09/2017 21:52 6010C
Total Iron
24300
100
JTR
03/09/2017 21:52 60100
Total Aluminum
131000
1000
JTR
03/09/2017 21:56 6010C
Total Manganese
732
5.00 .
JTR
03/09/2017 21:52 6010C ,
Total Copper.
37.8
5.00
JTR
03/09/2017 21:52 5010C
Total Zinc
67.6
5.00
JTR
03/09/2017 21:52 601 OC
Ammonia Nitrogen
0.20
2010
50.0
JM
03/08/2017 09:50 SM-4500-NH3C
Organic N
0.68
6830
50.0
03/07/2017 13:35 CALCULATION
Nitrate+Nitrite-N
<2:12
2.12
SJB
03/07/201710:50 4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N
series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients and may not be"re roduced in whole or art nor may an reference be made
p Y. A p Y Y
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization,
Debbie Holt "
Laboratory Supervisor

Pager 2 of 2
Report Number: 17-062-0205
Account Number: 46789
Send -To: Synagro Central LLC/ Dunn
Mary Brewer
284 Boger, Road- -.
Mocksville , NC 27028
Lab Number.: 62675
Sample Id: Dunn WTP
Wa oint,�
Y ANALYTICAL •
Project:. Dunn WTP
NC. Cert#25 i
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Date -Sampled: 3/2/2017 13:15:00
Date Received: 03/0312017 00:00
Date Reported: 03/13/2017
Total Cadmium
<2.00
2.00
JTR
03/09/2017 21.52
Total Chromium
101
5.00
JTR .
03/10/2017 13:04
Total Nickel
14.9
5.00
JTR
.03/09/2017 21:52
Total Lead
25.8 -
5.00'
JTR
03/09/2017 21:52
Total Arsenic
<3.00
3.00
JTR
03/10/2017 13:04
"total Mercury
<0.400
0.400
SJB
03/06/2017 14:53
Total Selenium
<5.00
5.00
JTR
03/10/2017 13:04
pH -(Standard Units) *
5.50 -
1..00
JM
03/06/2017 09:30
Total Molybdenum
<5.00
5.00
JTR
03/09/2017 21:52
Comments: _
SULFUR AND ORGANIC NITROGEN' NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and' confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining ourprior written authorization.
601 OC
601 OC
601 OC
6010C
6010C .
SW-7471 B .
601 OC
SW-9045D
601 OC
Debbie Holt
Laboratory Supervisor

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample.Date Report Range Ratio
2188-02-WPL-NC DUNN, NC WTP LIQUID 3/2/2017 111/2017-8/31/2017 0.5074
Na mg/I = (Na mg/kg x % Solids) = 100 = (610 x 2.4800) _ 100 = 15.128
Ca mg/I = (Ca mg/kg z % Solids) _ 100 = (1010 x 2.4800) 100 = 25.048
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (1020 x 2.4800) _ 100 = 25.296
Na meq = Na mg/I _ Molec.Wgt.Na=•15.128 _ 23 = 0.657739
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 25.048 _ 20 = 1.2524
Mg meq = Mg mg/I,— Molec.Wgt.Mg = 25.296 = 12 = 2.108
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 0.657739 _ SgrRoot[0.5(1.2524+2.108)] = 0.507427
Painted: 2/9/2018
Page 1 09:53

Page: 1 of 2
'Report Number: 17-244-0209
Account Number: 46789
Waypoinip
7621 Whitepine Road, Richmond, VA 23237
Submitted By: Chad Hayes
Main 804-743-94010.. Fax [phone]
ANALYTICAL
wyvW.waypointanalytical.com
Send To: Synagro Central-LLC/I Dunn
?t6ject: Dunn WTP
-Mary Brewer
.2.84 Boger Road
Mocksville, NC 27028
-
REPORTOF ANALYSIS.
Date'Sampled: 8i3l/2017 11:45:00
Lab Number: 55938
Date Received: 09/01/2.0.17.00:00
Sample Id : Dunn WTP
Date Reported: 09/11/2017
RESULT
RESULT
QUANTITATION
LIMIT
ANALYSIS
(mg/kg)
(-g/kg*)
ANALYST
DATEITIME METHOD
Total Solids*,
1.39
13900
100.0
im
09/0.1/2017 15:00 SM-2540G
Moisture
98.60
100.0,
im
09/01/2017 15:00- SM-2540G
T6tal Kjeldahl Nitrogen
0.79
7860
50.0
JIM
09/05/2017 10:36 SIVI-4500-NH3C-TKN
Total Phosphorus
0.20
1960
100
MOS
09/11/20,17 15:02 '6010C
Total Potassium
0.04
445
100'
MOS
09/11/2017 15:02 60'1 OC
Total Sulfur
0.88
8750
100.
MOS
09/11/2017 15:02 6010C
Total Calcium
0.11
1940.
100
MOS
09/11/2017 15:02 6010C
Total Magnesium •
0.07
.709
100
MOS.
09/11/2017 15:02 6010.0
Tbtal Sodium
0.09
865
100
MOS
09/11/2017 15:02- 6010C
Total Iron
1.7600
100
MOS
09/11/2017 15:02 6010C
Total Aluminum
95800
100
MOS
09/11/2017 1 5`.02 6010C
Total Manganese'
1030
5.00
MOS
09/11/2017 15:02 6010C
Total Copper
24. . 0.
MOS •
09/11/2017 15:02 `6010C
Total Zinc -
42.5.
.5.00
MOS
09/11/2017 15:02 6010C
Ammonia, Nitrogen
<50.0
50.0
im
09/05/2017 10:35 :'SM-4500-NH3C
Organic N
7860,
50.0
09/05/2017 10-35 CALCULATION
Nitrate +N itrite-N
164
1.94
SJB-
09/08/2017 09:53 4500NO3F-2011
All values are on a,dry weight basis except as noted by asterisk., Detection limit on all N'series
is on a wet basis.
000f
powneo
Our reports a nd letters are for the exclusive and confidential us6
-of our clients, and may not be reproduced in whole orpart, nor may any reference be made
to the work the results, or the company in any advertising, news
release, or other public announcements without obtaining our prior written authorization.
Pauric McGroary'
Agronomist

Page: 2 of 2.
Report Number: 17-244-0209
Account Number: 46789
• -
Waypoint.-_.
7621 Whitepine Road, Richmond, VA 23237 _
Submitted By: Chad Hayes
Main 804-743-9401 ° Fax [phone]
ANALYTICAL "
www.waypoinianalytical.com
" Send To: Synagro Central LLC/ Dunn
Project : Dunn WTP-:
Mary Brewer
284 Boger Road
Mocksville , NC 27028
-"
REPORT- OF ANALYSIS _
' " 'Date Sampled: 8/31/2017 11:45,00'
Lab'Number': 55938
Date, Received: 09/01/2017 00:00
Sample Id: Dunn WTP--
Date Reported: 09/11/2017,,-
PARAMETER
RESULT RESULT QUANTITATION LIMIT
N .
ANALYSIS
DATE/TIMEMETHOD
Total Cadmium
<2,00 2.00 MOS
09/11/2017 15:02 6010C
Total Chromium
78.5 5.00 MOS
09/11/2017 15:02 6010C
Total Nickel
6.63 -5.00 MOS'
09/11/2017 15:02 6010C
Total Lead.
10.2 5.00 MOS-
09/11/2017 15:02 6010C
Total Mercury
<0.400 0.400 " SJB
09/07/201716:20 SW- 7471 B
Total Selenium "
<5.00 5.00. MOS
09/11/2017 15:02 6010C
pH*
. 6.24 1.00 JM
09/05/2017 10:35, SW-0045D
Total Volatile. Solids, -
. 28.57 285700 _ 100.0 JM
09/01/201715:00 SM-2540G
Totaf,Molybdenum
<5.00 ' _ 5.00 MOS -'
09/11/2017,16.02 6010C -
Comments:
NC CERT#257, SC CERT#9300 7001
SULFUR AND ORGANIC NITROGEN NOT FOR
COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit.on"all N series is on a wet basis.
imp 64W
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, orotherpublic announcements without obtaining ourprior written authorization.
Pauric McGroary
Agronomist

Sodium Absorption Ratio Calculation, (SAR)
Product Code Product Name Sample Date Report Range Ratio
2188-02-WPL-NC DUNN, NC WTP LIQUID 8/31/2017 91112017-12/31/2017 0.5820
Na mg/I = (Na mg/kg x % Solids): 100.= (865 x 1.3900) _ 100 = 12.0235
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (1140 x 1.3900) = 100 = 15.846
Mg mg/I = (mg mg/kg'x % Solids) _ 100 =. (709. x 1.3900) _ 100 = 9.8551
Na meq = Na mg/I _ Molec.Wgt.Na = 12.0235 _ 23 = 0.522761
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 15.846 = 20 = 0.7923
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 9.8551 _ 12 = 0.821258
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 0.522761 + SgrRoot[0.5(0.7923+0.821258)] = 0.582004
Printed: 2/9/2018
Page 1 09:53

FACILITY NAME: DUNN, NC
OWNER: HAROLD EDRIDGE
SITE #: NC CU 00034 FIELD# : CU 00034 0001
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GOLDSBORO
PERMIT #: W00006101 ANNUAL DRY TONS APPLIED: 12.21
OPERATOR: HAROLD ELDRIDGE CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 4.80 ACRES PERMITTED: 4.80
Page
Lune Applied
***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
,
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Solids
Per
Residual
Dry, Wet,
Past 24 -
Method
zation
zation
TKN
Nitrogen
and
(pp m )
Crop
p
Total
Per Acre
MONTH
"
11/22/17
68,200.00 (G)
14208.333
•2.65
1.570
DUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
59,800. p
13,200.00 p
1,710.00 p
22290
FESCUE
Nov-17
68,200.00 (G)
14,208.333
-
11/27/17
80,600.00 (G)
16791.6671
1.39
0.973
DUWPL
DRY
0-<1/2"
SUR
0.5
0.40
7,860.0 p
50.00 p
154.00 p
3323
FESCUE
Nov-17
80,600.00 (G)
16,791.667
I
1
1
Total Gallons/Ac: 31,000.00
As
Cd
Cr
Cu
Pb-
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
76
0.046
0.010
0.225
0.851
0.160
0.002
0.034
0.057
0.025
1.477
80.75
Cumulative lbs/acre
0.236
0.069
1.655
9.015
1 1:143
0.053
0.329
0.758
0.180
15.719
1'`•`; i
+
r n ;
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
;
(,
f
138
1f
{
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
r
$ i
1339.0
267.9
375.0
15.0 JI
89.0
2500.0
'
DUAEDL = DUNN, NC W WTP AEROBICALLY DIGESTED LIQUID
DUWPL = DUNN, NC WTP LIQUID
X Sliq Ll
0
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/lcg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

FACILITY NAME: DUNN, NC
JWNER: HAROLD EDRIDGE
SITE #: NC CU 00034 FIELD# : CU 00034 0002
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GOLDSBORO
PERMIT #: W00006101 ANNUAL DRY TONS APPLIED: 10.36
OPERATOR: HAROLD ELDRIDGE CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 4.00 ACRES PERMITTED: 4.00
Page
Lane Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Minei•-
or Wet Tons (WT) (specify)
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation.
TEN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
I1/22/17
12,400.00 (G)
3100.000
2.65
0.343
DUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
59,800. p
13,200.00 p
1,710.00 p
22290
FESCUE
Nov-17
12,400.00 (G)
3,100.000
11/27/17
136,400.00 (G)
34100.000
1.39
1.977
DUWPL
DRY
0-<1/2"
SUR
0.5
0.40
7,860.0 p
50.00 p
154.00 p
3323
I FESCUE .
11/28/17
18,600.00 (G)
4650.000
1.39
0.270
DUWPL
DRY
0-<I/2"
SUR
0.5
0.40
7,860.0 p
50.00 p
154.00 p
3323
FESCUE
Nov-17
-155,000.00 (G)
38,750.000
Total Gallons/Ac: '41,850.00
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annuallbs/acre
-
30
0.057
0.010
0.368
0.283
0.076
0.002
0.028
0.039
0.026
0.495 25.59
Cumulativelbs/acre
0.185
0.055
1.359
6.797
0.795
0.043
0.254
0.560
0.D8
11.587 FF
Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop
j ; • E
;
'�
138
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 r 375.0
89.0
2500.0
_
DUAEDL = DUNN, NC W WTP AEROBICALLY DIGESTED LIQUID
DUWPL = DUNN, NC WTP LIQUID
X �r�r
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system.designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

'ACILITY NAME: DUNN, NC
)WNER: HAROLD EDRIDGE
iITE #: NC CU 00034 FIELD# : CU 00034 0003
ZESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GOLDSBORO
PERMIT #: WQ0006101 ANNUAL DRY TONS APPLIED: 5.48
OPERATOR: HAROLD ELDRIDGE CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 4.30 ACRES PERMITTED: 4.30
Page
Lime Applied ***
Date -L
Lbs/Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
A lr
PP -
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
Per Acre
11/22/17
Nov-17
49,600.00 (G)
49,600.00 (G)
11534.884
1 11,534.884
2.65
1.275
DUAEDI
DRY
0-<1/2"
SUR 1
5.0
0.30
1 59,800. p
13,200.06-1
1,710.00 p
22290
SORGHUM/SUDAN PASTURE
Total
('a11 cM—
11 ewe oo
1
_
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
annual lbs/acre
0.019
0.005
0.059
0.653
0.113
0.001
0.020
0.036
0.013
1.132
62.46
208
umulative lbs/acre
0.256
0.073
1.682
9.143
1.158
0.055
0.344
0.828
0.191
16.005
`;Tw•`":
ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop
•✓ ,
=?
t_
239
: f
-D Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
;t
15.0 := 375.0
89.0
2500.0
)UAEDL = DUNN, NC W WTP AEROBICALLY DIGESTED LIQUID
X
V
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
k Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

?ACILITY NAME: DUNN, NC
OWNER: HAROLD EDRIDGE
31TE #: NC CU 00034 FIELD# : CU 00034 0004
ZESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: NORFOLK
PERMIT #: W00006101 ANNUAL DRY TONS APPLIED: 18.48
OPERATOR: HAROLD ELDRIDGE CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 6.20 ACRES PERMITTED: 6.20
Page
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner-,
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip. ' .
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Total
Solids '
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Per Acre
11/21/17
105,400.00 (G)
17000.000
2.65
1.879
DUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
59,800. p
13,200.00 p
1,710.00 p
22211
FESCUE
Nov-17
105,400.00 (G)
17,000.000
.11/28/17
117,800.00 (G)
19000.000
1.39
1.101
DUWPL
DRY
0-<1/2"
SUR
0.5
0.40
7,860.0 p
50.00 p
154.00 p
3323
FESCUE,
Nov-17
117,800.00 (G)
19,000.000
1
Total Gallons/Ac: 36,000.UU
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annuallbs/acre
-
91
0.054
0.012
0.260
1.015
0.190
0.003
0.040
0.067
0.030
1.762
96.37
Cumulative Ibs/acre
0.270
0.075
1.655
8.863
1.166
0.051
0.326
0.786
0.191
15.528
p ,;177
r r � �
t
n- ^� •
i, N
?ermit PAN Limit (Ibs/acre) 1st-Crop/2nd Crop
1
`'
g 1 °
1
120
t
I �
FD.Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
c` i
1339.0
267.9�
15.0
� ? 375.0
89.0
2500 0 !
DUAEDL = DUNN, NC W WTP AEROBICALLY DIGESTED LIQUID
DUWPL = DUNN, NC WTP LIQUID
X ( r
(SIGNATURE OF LAND APPLIER) DATE .
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME:. DUNN, NC PREDOMINANT SOIL SERIES: GOLDSBORO
OWNER: HAROLD EDRIDGE PERMIT #: WQ0006101 ANNUAL DRY TONS APPLIED: 24:32
SITE #: NC CU 00034 FIELD# : CU 00034 0005 OPERATOR: HAROLD ELDRIDGE CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 9.70 ACRES PERMITTED: 9.70
Page
Lime Applied
***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
ado
Tons
Cond. •
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre -
Solids
-
11/21/17
155,000.00 (G)
15979.381
2.65
1.766
DUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
59,800. p
13,200.00 p
1,710.00 p
22291
FESCUE
Nov-17
,155,000.00 (G)
15,979.381
11/28/17
124,000.00- (G)
12783.505
1.39
0.741
DUWPL
DRY
0-<1/2"
SUR
0.5
0.40
7,860.Op
50.00 p
154.00 p
3323
FESCUE
Nov-17
124,600.00 (G)
12,783.505
Total Gallons/Ac: - 28,762.89
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annual lbs/acre
84
0.044
0.010
0.198
0.940
0.172
0.002
0.035
0.059
0.025
1.631 89.43
Cumulative lbs/acre
0.244
0.072
1.613
9.263
1.261
0.052
0.320,
0.773
0.184
16.007
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
, S'
!
')
1i•�
4(
'1„
IF.
i '
E j
F' ;
i
-` i�I i�t 5 �)
138
.
j
l j
r
.f
s ", tl
FD Cumulative Pollutant LoadingRate Limit lbs/acre
( )
36.6
34.8
?
1339.0
267.9
15.0
g ",, 375.0
89.0
2500 0
_
i
(?ems
DUAEDL = DUNN, NC W WTP AEROBICALLY DIGESTED LIQUID
DUWPL = DUNN, NC WTP LIQUID
X - h
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for -submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent . p - ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injectioiuhcorporation 1.0
Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation. *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

FACILITY NAME: DUNN, NC
DWNER: HAROLD DIXON
SITE #: NC HA 00008 FIELD# : HA 00008 0008
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: NORFOLK
PERMIT #: W00006101 ANNUAL DRY TONS APPLIED: 29.32
OPERATOR: - HAROLD DIXON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 18.30 ACRES PERMITTED: 18.30
Page : 1
Lime Applied ***
Date
Lbs/Ac
allons. (G) or Cubic Yards (CY)
-
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual .'
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
m
(pp )
Cro p
MONTH
Total'
Per Acre
Solids
-
9/14/17
93,000.00 (G)
50.81.967
2.65
0.562
DUAEDL
MOIST
0-<1/2"
SUR
0.5
-0.30
59,800.p
13,200.00• p
1,710.00 p
22290
WHEAT
Sep-17
93,000.00 (G)
5,081.967
9/9/17 -
142,600.00 (G)
7792.350
1.39
0.452
DUWPL
MOIST
0-<I/2"
SUR
0.5
0.40
7,860.0 p
50.00 p
154.00 p
3323
I WHEAT
9/10/17
186,000.00 (G)
10163.934
1.39
0.589
DUWPL
MOIST
0-<I/2"
SUR
0.5
0.40
7,860.0 p
50.00 p
154.00 p
3323
WHEAT
Sep-17
328,600.00 (G)
17,956.284
Total Gallons/Ac: - 23,038.25
As
Cd
Cr
Cu
Pb-
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annual lbs/acre
32
0.033
0.006
0.189
0.337
0.071
0.001
0.019
0.030
0.016
0.587 31.60
Cumulative Ibs/acre
0.318
0.232
2.449
17.534
1.651
0.059
0.748
2.017
0.301
46.266
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
; _ 7
i
C t
12 5
f
;
FD Cumulative Pollutant LoadingRate Limit lbs/acre
( )
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
DUAEDL = DUNN, NC W WTP AEROBICALLY DIGESTED LIQUID
DUWPL = DUNN, NC WTP LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/lcg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

FACILITY NAME: DUNN, NC
)WNER: HAROLD DIXON
iITE #: NC HA 00008 FIELD# : HA 00068 0009
ZESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: NORFOLK
PERMIT #: W00006101 ANNUAL DRY TONS APPLIED: 65.90
OPERATOR: HAROLD DIXON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 22.20 ACRES PERMITTED: 22.20
Page
Lime Applied ***
Date
LWAc
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
oho
Tons
-
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
Total
Per Acre
9/14/17
167,400:00 (G)
7540.541
2.65
0.833
DUAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
59,800. p
13,200.00 p
1,710.00 p
22290
I BERMUDAGRASS,, COASTAL
9/15/17
204,600.00 (G)
9216.216
2.65
1.018
DUAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
59,800. p
13,200.00 p
1,710.00 p
22290
BERMUDAGRASS, COASTAL
Sep-17
372,000.00 (G)
16,756.757
9/8/17
272,800.00 (G)
12288.288
1.39
0.712
DUWPL
MOIST
0-<I/2"
SUR
0.5
0.40
7,860.0 p
50.00 p
154.00 p
3323
I BERMUDAGRASS, COASTAL
9/9/17
155,000.00 (G)
6981.982
1.39
0.405
DUWPL
MOIST
0-<1/2"
SUR
0.5
0.40
7,860.0 p
50.00 p
154.00 p
3323
BERMUDAGRASS, COASTAL
Sep-17
427,800.00 (G)
19,270.270
Total Gallons/Ac: 36,027.03
As
Cd
Cr
Cu
Pb
.Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annual lbs/acre
90
0.054
0.012
0.261
1.002
0.188
0.003
0.040
0.067
-0.030
1.739 95.11
Cumulative Ibs/acre
0.293
0.166
2.080
14.304
1.549
0.050
0.599
1.646
0.263
35.274
_
'ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop
1
'
y
'
3
( k
9
Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
;
1339.0
267.9
15.0
IFD
II
375.0
89.0
2500.0 1 u ayy
1
DUAEDL = DUNN, NC W WTP AEROBICALLY DIGESTED LIQUID
)UWPL = DUNN, NC WTP LIQUID
X q1 ilk
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent' p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
r. Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

FACILITY NAME: DUNN, NC
DWNER: CARL HAMILTON, JR.
SITE #: NC HA 00201 FIELD# : HA 00201 0004
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: WAHEE
PERMIT #: W00006101 ANNUAL DRY TONS APPLIED: 142.10"
OPERATOR: RONNIE HAMILTON, 7R. CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 85.10 ACRES PERMITTED: 85.10 "
Page
Lune Applied ***
Date
Lbs/Ac
allons (Q) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (VM (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
MONTH
Total
Per Acre
Solids
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
-
(ppm)
Crop -
4/17/17
186,000.00 (G)
2185.664
2.48
0.226
DUWPL
MOIST
0-<1/2"
SUR
0.5
0.40
8,840.0 p
2,010.00 p
2.12 p
3739
SOYBEANS
4/21/17
111,600.00 (G)
1311.398
2.48
0.136
DUWPL
MOIST
0-<1/2"
SUR
0.5
0.40
8,840.0 p
2,010.00 .p
2.12 p
3739
SOYBEANS
4/22/17
279,000.00 (G)
3278.496
2.48
0.339
DUWPL
MOIST
0-<I/2"
SUR
0.5
0.40
8,840.0 p
2,010.00 p
2.12 -p
3739
SOYBEANS
Apr-17
576,600.00 (G)
6,775.558
5/1/17
248,000.00. (G)
2914.219
2.75
0.334
DUAEDL
MOIST
0-<I/2"
SUR
0.5
0.30
64,900.p
4,710.00 p
139.00 p
20551 .I
SOYBEANS
5/3/17
49,600.00 (G)
582.844
2.15
0.067
DUAEDL
MOIST-
0-<1/2"
SUR-
0.5
0.30
64,900.p
4,710.00 p
139.00 p
20551
I SOYBEANS
5/4117
217,000.00 (G)
2549.941
2.75
0.292
DUAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
64,900. p
4,710.00 p
139.00 p
20551
I SOYBEANS
5/8117
167,400.00 (G)
1967.098
2.75-
0.226
DUAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
64,900. p
4,710.00 p
139.00 p
20551
SOYBEANS
5/11/17
37,200.00 (G)
437.133
2.75
0.050
DUAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
64,900. p
4,710.00 p
139.00 p
20551
SOYBEANS
May-17
719,200.00 (G)
1 8,451.235

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: " DUNN, NC PREDOMINANT SOIL SERIES: WADE
OWNER: CARL HAMILTON, JR. PERMIT #: WQ0006101 ANNUAL DRY TONS APPLIED: 142.10
SITE #: NC I -IA 00201 FIELD# : HA 00201 0004 OPERATOR: RONNIE HAMILTON, JR. CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 85.10 ACRES PERMITTED: 85.10
Page: 2
Lune Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24'
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
Total
Per Acre
TOTALS:
As
Cd
Cr -
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
45
0.015
0.007
0.200
0.489
0.102
0.002
0.019
0.050
0.017
0.703
39.96
Cumulativelbs/acre
0.168
0.071
1.150
6.753
1.391
0.037
0.169
0.743
0.128
12.302
+., ``
;y•°="'.j
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
f '
��
j, .
i
i
161
FD Cumulative Pollutant LoadingRate Limit Ibs/acre
( )
36.6
34.8
1339.0
267.9
15.0
375.0
89.0 2500.0
i
DUWPL = DUNN, NC WTP LIQUID
DUAEDL = DUNN, NC W WTP AEROBICALLY DIGESTED LIQUID
X Z _hq //-, 9
v
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

i i -
Summit Environmental Technologies, Inc.
3310 Win St.
-r;-r[RONMEtITA:LCuyahoga Falls, Ohio 44223
An.71yUcal Caiinmodes TEL:'[phone] FAK [phone],
Website: http://wlvw.setiek.com
March 15, 2017
Chad M. Hayes
Synagro
284 Boger Rd.
Mocksville, NC 27028. `
TEL: [phone]
FAX: [phone]
RE: 'Dunn WWTP
Dear Chad M. Hayes: Order No.: 17030217
Summit Environmental Technologies, Inc. received 1 sample(s) on 302017 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
'Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Alabama 41600, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E87688; Georgia E87688, Idaho
OH00923, Illinois 200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground'Stomge Tank) 3, Kentucky 90146, Louisiana 04061, .Maryland
339, Massachusetts M-OPH923, Minnesota 409711, New Hampshire 2996, New Jersey 011006, New York 11777, North Carolina 39705 and 631, North
Dakota R-201; Ohio Drinking Water 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon 0112O0001, Rhode Island LA000317; South Carolina 92016001,
Texas T104704466-11-5, Region 8 8TMS-L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581,
Washington C891, West Virginia 9957C .
Page 1 of 50 . .

- Szonmit Environmental Technologies, Inc. Case Narrative
3310 Win St.
r('iUIR0t4h1Eh1'rAL TSCV. 10LQQIF5, TZQ. Cuyahoga Falls, Ohio 44223 WO#: 17030211
Arralry cat Ubaratorie? TEL: [phone] FAX: [phone]
Website: hun.-Mviviv.settekcom Date: 3/15/2017
CLIENT: Synagro
Project: Dunn WWTP
WorkOrder Narrative:
17030217:.This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditation/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not certified."
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received". or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence QC Comments:
ccv 20ppb c0306/ 1096834: Analytical Comments for voc-MSTR npw(8260), Sample ccv 20ppb
c0306/, Batch ID R66502 : The VOC CCV (Batch R66502) exhibited slightly high (120.51/o) recovery
for Method -Specified CCC Vinyl chloride; All samples were ND for Vinyl chloride..All other Method -
'Specified CCCs and SPCCs exhibited control.
mb-25849 1098253: Analytical Comments for tclp-svoc-cpest tclp(8081), Sample mb-25849, Batch ID
25849 : The TCLP Pesticides Method Blank (Batch 25849) exhibited high recovery for Surrogate:
DCB; MB was ND for all analytes of interest.
lcs-25849 1098254: Analytical Comments for tclp-svoc-cpest_tclp(8081), Sample lcs-25849, Batch ID
25849 : The TCLP Pesticides 'LCS (Batch 25849) exhibited high recovery for Surrogate: DCB; All
Original
Page 2 of 50

Summit Environmental Technologies, Inc.
SM 3310 Win St. Case l� arra'tive
fibVln[�tdhlEhlA.Lht�3iPd4Ldri=s, iris. Cuyahoga Falls, Ohio 44223 WO#: 17030217
�rrai�Ffr`csl L.4haialur7e5 TEL: [phone] FAX.- (330) 25374489
Website: htto.1Mvw.settek.c6Date: 3/15/2017
n:
CLIENT: Synagro
Project: Dunn WWTP
other analytes of interest exhibited recoveries within acceptance limits.

Summit Environmental Technologies, In Qualifiers 'and Acronyms
3310 Win Sgam.
Umion
St�InC1N61Eh11h.L "s'> Gittit�Lrt>;lcs, INC. Cuyahoga Falls, Ohio 4422- WO#• 17030217
AnAly+deal Lzboratodez, TEL: [phone] FAX.• (330) 253-445
Website: http:Y/1vww.settekco: Date: 3/15/2017
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U
The compound was analyzed for but was not detected.
J
The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H
The hold time for sample preparation and/or analysis was exceeded.
D
The result is reported from a dilution. .
E
The result exceeded the linear range of the calibration or is estimated due to interference.
MC
The result is below the Minimum Compound Limit.
x
The result exceeds the Regulatory. Limit or Maximum Contamination Limit.
in
Manual integration was used to determine the area response.
N
The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P
The second column confirmation exceeded 25% difference.
C
The result has been confirmed by GC/MS.
X
The result was not confirmed when GC/MS Analysis was performed.
B/MB+
The analyte was detected in the associated blank.
G.
The ICB or CCB contained reportable amounts of analyte.
QC-/+
The CCV recovery failed low (-) or high (+).
R/QDR
The RPD was outside of accepted recovery limits.
QL-/+
The LCS or LCSD recovery failed low (-) or high (+).
QLR
The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+
The MS or MSD recovery failed low (-) or high (+).
QMR
The MS/MSD RPD was outside of accepted recovery limits.
QV-/+
The ICV recovery failed low (-) or high (+).
S
The spike result was outside of accepted recovery limits.
Z
Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected RL Reporting Limit
QC
Quality Control MDL Method Detection Limit
MB
Method Blank LOD Level ofDetection
LCS
Laboratory Control Sample LOQ Level of Quantitation
LCSD
Laboratory Control. Sample Duplicate, PQL Practical Quantitation Limit
QCS
Quality Control Sample CRQL Contract Required Quantitation Limit
DUP
Duplicate PL Permit Limit
MS
Matrix Spike RegLvl Regulatory Limit
MSD
Matrix Spike Duplicate MCL Maximum Contamination Limit
RPD
Relative Percent Different MinCL Minimum Compound Limit
ICV .
Initial Calibration Verification RA Reanalysis
ICB '
Initial Calibration Blank RE Reextraction
CCV
Continuing Calibration Verification TIC Tentatively Identified Compound
CCB
Continuing Calibration Blank RT Retention Time
PLC
Reporting Limit Check CF Calibration Factor '
DF
Dilution Factor RF Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported, data.
Original
Page 4 of 50

`
Summit Environmental Technologies, Inc.
a
WOPkOPCler
SU
3310'Win St.
Sal11PIe Summary
fitVIROtJIdENT�1L c3 P.`�SLzG ems; t�tr .
Cuyahoga Falls, Ohio 44223
Arralyticsf Laborafurwf s,
TEL: [phone] FAX.- [phone]
WO#: 17030217
Website:'htto://www.settek.com
15Mar-17
CLIENT:
Synagro
Project:
Dunn"WWTP
Lab SampleID Client Sample IDTag No Date Collected
Date Received Matrix'
17030217-601
Dunn WWTP
3/2/20 1111:00:00 AM
3/3/2017 1:40:00 PM Sludge

.,
Summit Environmental Technologies, Inc.
3310 Win St.
DATES REPORT
R!KVIR0NPAENTA aF,Cirl?J0L0G1E5,VC. Cuyahoga Falls, Ohio44223
Analy rzf Lzboralzmfes
TEL: [phone] FAX. [phone]
WO#: 17030217
Website: h1112.-Mvipiv.settekcom
15 Mar-17
Client:
Synagro
Project:
Drum WWTP
Sample ID
Client Sample ID
Collection Date Matrix Test Name Leachate Date
Prep Date Analysis Date
17030217-OOIA Dunn WWTP
3/2/2017 11:00:00 AM Sludge Ignitability of Solids (SW-846: 1036) .
3/8/2017 11:00:00 AM
pH (SW9045D)
3/10/2017 4:03:00 PM
Reactive Cyanide (9014/7.3.3.2)-Solid
3/6/2017 1-1:45:00 AM
Reactive Sulfide (9034)
3/6/2017 11:45:00 AM
SVOC 8270 TCLP BNA List 3/6/2017 5:29:57 PM
3/8/2017 8:30:00 AM 3/13/2017 4:46:00 PM
SVOC SW-846: 8081-TCLP Pesticide! 3/6/2017 5:29:57 PM
3/8/2017 7:00:00 AM 3/9/2017 5:09:00 PM
SVOC SW-846: 8151 Herbicides-TCL3/6/2017 5:29:57 PM
3/7/2017 10:30:00 AM" 3/10/2017 10:26:00 PM
TCLP Mercury Analysis (1311/7470) 3/6/2017 5:29:57 PM
3/7/2017 11:00:00 AM 3/7/2017 6:31:00 PM
TCLP Metals Analysis (60.10) 3/6/2017 5:29:57 PM
3/7/2017 9:50:48 AM 3/9/201710:09:47 AM
VOC by GUMS (8260)-TCLP
3/7/2017 11:51:60 PM
Original
Page 6 of 50

Summit
Environmental Technologies, Inc.
3310 Win St.
Analytical Report
t'KVIRONWW AL 120,Z0Lc.iz5, iilr.
Cuyahoga Falls, Ohio 44223
(base report)
Arras,-W .sl LaberaioR%;.
TEL: (330)
253-8211 FAX: [phone]
WO#: 17030217
Website: htty.-1Avwiv.settek-com
Date Reported: 3/15/2017
CLIENT: Synagro
Tag Number:
Matrix: SLUDGE
Collection Date:
3/2/2017 11:00:00 AM
Lab ID: 17030217-OOIA
Project: Dunn WWTP
Client Sample ED Dunn WWTP
Analyses Result
RL
Qual Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW7470A
SW7470A Analyst: ALJ
TCLP MERCURY ANALYSIS (1311/7470)
TCLP Mercury
ND
0.00200
mg/L
1
3/7/2017 6:31:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW6010C
SW3010A Analyst: VVK
TCLP METALS ANALYSIS (6010)
TCLP Arsenic(As)
ND
0.500
mg/L
1
3/9/2017 10:09:47 AM
TCLP Barium(Ba)
ND
5.00
mg/L
1
3/9/2017 10:09:47 AM
TCLP Cadmium(Cd)
ND
0.100
mg/L
1
3/9/2017 10:09:47 AM
TCLP Chromium(Cr)
ND
0.200
mg/L
1
3/9/2017 10:09:47 AM
TCLP Lead(Pb)
ND
0.500
mg/L
1
3/9/2017 10:09:47 AM
TCLP Selenium(Se)
ND
0.500
mg/L
1
3/9/2017 10:09:47 AM
TCLP Silver(Ag)
ND
0.500
mg/L
1
3/9/2017 10:09:47 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270C
SW3510C Analyst: CxA
SVOC 8270 TCLP BNA LIST
1,4-Dichlorobenzene
ND
0.0800
mg/L
2
3/13/2017 4:46:00 PM
2,4,5-Trichlorophenol
ND
0.200
mg/L
2
3/13/2017 4:46:00 PM `
2,4,6-Trichlorophenol
ND
0.200
mg/L
2
3/13/20,17 4:46:00 PM
2,4-Dinitrotoluene
ND
0.100
mg/L
2
3/13/2017 4:46:00, PM
Cresols, Total
ND
4.00
mg/L
2
3/13/2017 4:46:00 PM
Hexachloro-1,37butadiene
ND
0.100
mg/L
2
3113/2017 4:46:00 PM
Hexachlorobenzene
ND
0.100
mg/L
2
3/13/2017 4:46:00 PM
Hexachloroethane
• ND
0.0800
mg/L
2
3/13/2017 4:46:00 PM
Nitrobenzene
ND
0.0800
mg/L
2
3/13/2017 4:46:00 PM
Peritachlorophenol
ND
0.200
mg/L
2
3/13/2017 4:46:00 PM
Pyridine
ND
0.200
mg/L
2
3/13/2017 4:46:00 PM.
Surr: 2-Fluorophenol
63.0
10 - 109
%Rec
2
3/13/2017 4:46:00 PM
Surr. 0henol-d6
64.2
10'- 109
%Rec
2
3/13/2017 4:46:00 PM
Surr:-Nitrobenzene-d5
67.5
19 - 120
%Rec
2
3/13/2017 4:46:00 PM
Surr- 2,4,6-Tribromophenol
77.6
10 - 120
%Rec
2
3/13/2017 4:46:00 PM
Surr: 2-Flu6robiphenyl
62.9
22 - 117
%Rec
2
3/13/2017 4:46:00 PM
Surr: p-Terphenyl-d14 -
75.8
34- 116
%Rec
2
3/13/2017 4:46:00 PM
*
Qualifiers:
Value exceeds Maximum Contaminant Level.
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
M
Manual Integration used to determine area response .
MC
Value is below Minimum Compound Limit.
N
Tentatively identified compounds
ND -
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit Original
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 7 of 50

Summit Environmental Technologies, Inc. Analytical Report
SUM&WN'T 3310 Win St.
Fftt�IROhdhlEh'P,�.LT� ; Pvr3L G:LS; Wq. Cuyahoga Falls, Ohio44223 (base report)
AnAri- cal L3L;arajorj & TEL: [phone] FAX: [phone] WO#: 17030217_
Website: htR. Avww.settek.com Date Reported: 3/15/2017
.CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 3/2/2017 11:00:00 AM
Lab ID: 17030217-001A
Project: Dunn WWTP
Client Sample ID Dunn WWTP
Analyses Result RL "Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8081A
SW3510C Analyst: JBN
SVOC SW-846: 8081-TCLP PESTICIDES
Chlordane, total
ND
0.0100
mg/L "
1
3/9/2017 5:09:00 PM
Toxaphene
ND'
0.0200
mg/L
1
3/9/2017 5:09:00 PM
Endrin
ND
0.00100
mg/L
1
3/9/2017 5:09:00 PM
gamma-BHC
ND
0.00100
mg/L
1
3/9/2017 5:09:00 PM
Heptachlor
ND '
0.00100
mg/L
1
3/9/2017 5:09:00 PM
Heptachlor epoxide
ND
.0.00100
mg/L
1
3/9/2017 5:09:00 PM
Methoxychlor
ND
0.00100
mg/L
1
3/9/2017 5:09:00 PM
Surr: TCMX
73.7
10 - 119
%Rec
1
3/9/2017 5:09:00 PM
Surr: DCB
89.9
10 -'119
%Rec
1
3/9/2017 5:09:00 PM
TCLP HERBICIDES ANALYSIS (SW846 131118151)
SW8151A
SW8151A Analyst: JBN
SVOC SW-846: 8151 HERBICIDES-TCLP
2,4-D
ND
1.00
mgk
1
3/10/2017 10:26:00 PM
2,4,5-TP
ND
0.500
mg/L
1
'" 3/10/2017 10:26:00 PM
Surr: DCAA
75.8
.20 - 140
%Rec
1
3/10/2011 10:26:00 PM
TCLP METALS,,VOC, BNA, PEST, HERB -SOLID
SW8260B
Analyst: MES
VOC BY GC/MS (8260)-TCLP
M-Dichloroethene
ND
0.100
mg/L
1
3/7/2017 11:51:00 PM
1,2-Dichloroethane
ND
0:100'
mg/L
1
3/7/2017 11:51:00 PM
MEK
ND
2.00
mg/L
1
3/7/2017 11:51:00 PM
Benzene
ND
0.100
mg/L
1
3/7/2017 11:51:00 PM
Carbon tetrachloride
ND
0.100
mg/L
1
3/7/2017 11:51:00 PM
Chlorobenzene
ND
0.100
mg/L
1
3/7/2017 11:51:00 PM
Chloroform
ND
0.100
mg/L
1
3/7/2017 11:51:00 PM
Tetrachloroethene
ND
0.100
mg/L -
1
3/7/2017 11:51:00 PM
Trichloroethene
ND
0.100
mg/L
1
3/7/2017 11:51:00 PM
Vinyl chloride
ND
0.200 QC+
mg/L
1
3/7/2017 11:51:00 PM
Surr: 4-Bromofluorobenzene
97.2
70 - 130
%Rec
1
3/7/2017 11:51:00 PM
Surr: Dibromofluoromethane
96.0 "
70 - 130
%Rec
1
3/7/2017 11:51:00 PM
Surr: Toluene-d8
100
70 - 130
%Rec
1
3/7/2017 11:51:60 PM
*
Qualifiers:
Value exceeds Maximum Contaminant Level.
E
Value above quantitation range
H
Holding times'for preparation or analysis exceeded
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound Limit.
N
Tentatively identified compounds
ND
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit Original
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 8 of 50

F- Summit Environmental Technologies, Inc.
t
3310 Win St.
FKVIROtdhlEk'TALTEC3-!t OLQ-�IES; Tic. Cuydhoga Falls, Ohio 44223
i4nalytica l La-barator/rb TEL: [phone] FAX. • [phone]
Website: huDr/hvi4iv.settek.co7n
Analytical Report
(base report)
WO#: 17030217
Date Reported: 3/15/2017
CLIENT: Synagro
Tag Number:
Matrix: SLUDGE
Collection Date:
3/2/2017 11:00:00 AM
Lab ED: 17030217-001A
Project: Dunn WWTP
Client Sample ED Dunn WWT,P
Analyses- Result
RL Qual Units
DF Date Analyzed
RCI
SW9014-
Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive . ND
0.500 mg/Kg
1 3/6/2017 11:45:00 AM
IGNITABILITY OF SOLIDS (SW-846: 1030)
SW1030
Analyst: RMT
Ignitability Non-flammable.
1 3/8/2017 11:00:00 AM
RCI
SW9045D
Analyst: DHC
-PH (SW9045D),
y pH 6.5
l
s.u.@19.7C
1. 3/10/2017 4:03:00 PM
RCI
SW9034
Analyst: MS'
REACTIVE SULFIDE (9034)
Sulfide, Reactive ND
25.0 mg/Kg
1 3/6/2017 11:45:00 AM .
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below.Minimum Compound Limit.
ND, Not Detected at the Reporting Limit
P , Second column confirmation exceeds
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
O RSD is greater than RSDlimit
PL Peimit Limit Original,
RL Reporting Detection Limit
Page 9 of 50

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
Sul 4 e� IT- 3310 Win St.
L-r;v1H[rNro1NN 1Ah R W;51NUL1rJGR:a, JKC Cuyahoga Falls, Ohio 44223' WO#: 17030217
_, .. n1 r3i� tdcaP La1l,carfltQFle TEE: [phone] FAX.- [phone]
Website: h1tD:/Avww.setie1ccom IS Mar-17
Client: Synagro
Project: Dunn WWTP BatchED: 25824
Sample ID MB-25824
SampType: MBLK
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 3/7/2017
RunNo: 66446
Client ID: PBW
Batch ID: 25824
TestNo: SW6010C SW3010A
Analysis Date: 3/7/2017 .
SegNo: 1096699
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
ND
0.500
TCLP Barium(Ba)
ND
5.00
TCLP Cadmium(Cd)
ND
0.100
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pb)
ND
0.500
TCLP Selenium(Se)
ND
0.500
TCLP Silver(Ag)
ND,
0.500
Sample ID 'LCS-25824
SampType: LCS
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 3/7/2017
RunNo: 66446
Client ID: LCSW
Batch ID: 25824
TestNo: SW6010C SW3010A
Analysis Date: 3/7/2017 _
SegNo: 1096700'
Analyte .
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
1.98.
0.500
2.000
0
99.0
80
120
TCLP Barium(Ba)
ND
'5.00
2.000
0
102
80
120 .
TCLP Cadmium(Cd)
1.99
0.100
2.000 _
0
99.6
80
120
TCLP Chromium(Cr)
2.01
0.200
2.000
0
100
80
120
TCLP Lead(Pb)
2.00
0.500
2.000
0
99.8
80
120
TCLP-Selenium(Se)
1.99
0.500
2.000
0
99.7
80
120
TCLP Silver(Ag)
1.01
0.500
1.000
0
101
80
120
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound.Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page' 10 of 50
Original

s
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
t ' r 3310 Win St.
Fzrav1xrJ,Nr011;N 1A1. I W.; NULutti!:;a, rrvC. Cuyahoga Falls, Ohio 44223
+i:r,yi��li,�:a1 Ca?�pd.9fc�FieS WO#: 17030217
TEL: [phone] FAX [phone]
Website: http://lvivw.settelccom 15 Mar-17
Client: Synagro
Project: Dunn WWTP BatchID: 25839
Sample ID MB-25839
SampType: MBLK
TestCode:_HG TCLP(74 Units: PPM
Prep Date: 3/7/2017
RunNo: 66490
Client ID: PBW
Batch ID: 25839
TestNo: SW7470A SW7470A'
Analysis Date: 3/7/2017
SegNo: 1096547
Analyte
Result
PQL SPK value . SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury ND 0.0020D
Sample ID LCS-25839
SampType: LCS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 3/7/2017
RunNo: 66490
Client ID: LCSW
Batch ID: 25839
TestNo: SW7470A SW7470A
Analysis Date: 3/7/2017
SegNo: 1096548
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00411 0.00200 0.00400 0 103 80 120
Sample ID 17021496-008AMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 3/7/2017
RunNo: 66490
Client ID: BatchQC
Batch ID: 25839
TestNo: SW7470A SW7470A
Analysis Date: 3/7/2017
SegNo: 1096651
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00416 0.00200 0.00400 0 104 75 125
Sample ID 17021496-008AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 3/7/2017
RunNo: 66490
Client ID: BatchQC
Batch ID: 25839
TestNo: SW7470A SW7470A
Analysis Date: 3/7/2017
SegNo: 1096552
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00417 0.00200 0.00400 0 104 75 125 0.00416 0.240 20
Qualifiers: :k Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded 7 Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 11 of 50

1
a _ Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
ecwvlxVINtoll. NI.'161a:,L;H?,IULC07=S,arts. Cuyahoga Falls, Ohio44223 WO#: 17030217
4 ��tsrtt•cJ ? �rbaafratigy TEL: [phone] FAX.- [phone]
Websitei htty. 1wimsette1ccom 15 Mar-17
Client: Synagro
Sample ID 17021496-008AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 3/7/2017
RunNo: 66490
Client ID: Batch=
Batch ID: 25839
TestNo*. SW7470A . SW7470A
Analysis Date: 3/7/2017
SegNo: 1096552
Analyte -
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above, quantitation range
H Holding tunes for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC. Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit 'R RPD outside accepted recovery limits
Page 12 of 50

ffi
t•
S
Summit Environmental Technologies, St.
3310 10 Win St.
QC SUMMARY REPORT
Lw IHV!N MUNIALILuttitS,INC.
Cuyahoga Falls, Ohio44223
WO#: 17030217
Aylwf1fN,rmsf UxZ?ot,gXu fpn TEL: [phone] FAX. [phone]
Website: htto://lvww.settelr-coni
15 Mar-17
Client:
Synagro
Project:
Dunn WWTP
BatchID: 25848
Sample ID mb-25848
SampType: mblk-
TestCode: tclp-svoc-her Units: mg/L
Prep Date: 3/7/2017
RunNo: 66643
Client ID: PBW
Batch ID: 25848
TestNo: SW8151A SW8151A
Analysis Date: 3/10/2017
SegNo: 1099064
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D ND 1.00 0 0
2,4,5-TP ND 0.500 0 0
Surr: DCAA 320 500.0 64.0 20 140
Sample ID Ics-25848
SampType: Ics
TestCode: tclp-svoc-her Units: mg/L
Prep Date: 3/7/2017
RunNo: 66643
Client ID: LCSW
'Batch ID: 25848
TestNo: SW8151A SW8151A
Analysis Date: 3/10/2017
SegNo: 1099066
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
ND
1.00 0.500
0 80.3
62.6
125
2,4,5-TP
ND
0.500 0.500
0 79.6
52.5
128
Surr: DCAA
430
500.0
86.0
20
140
Sample ID 17030217-001ams
SampType: ms
TestCode: tclp-svoc-her Units: mg/L
Prep Date: W7/2017
RunNo: 66643
Client ID: 'Dunn WWTP
Batch ID: 25848
TestNo: SW8151A SW8151A
Analysis Date: 3/10/2017
SegNo: 1099066
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D ND 1.00 0.500 0 80.0 37 105
2,4,5-TP ND 0.500 0.500 0 78.9 38 106
Surr: DCAA 416 500.0 83.2 20 140
Qualifiers: * Value exceeds Maximum Contaminant Level. • B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 13 of 50

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUMMI"t 3310 Win St.
r czv�xc�r•�rnr:rn 4 a j;t7Hucal alC -s, ma. Cuyahoga Falls, Ohio 44223 Wo#: 17030217
nalyfll•caf C rbpr9lnrlF? TEL: [phone] FAX. [phone]
Website: httI2.1Avww.settelccon: 15-Mar-17
Client: Synagro
Project: Dunn WWTP BatchID: 25848
Sample ID 17030217-001amsd
SampType: msd
TestCode: tclp-svoc-her Units: mg/L
Prep Date: 3/7/2017
RunNo: 66643
Client ID: Dunn WWTP
Batch ID: 25848
TestNo: SW8151A SW8151A
Analysis Date: 3/10/2017
SegNo: 1099067
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D ND 1.00 0.500 0 75.9 37 105 0 0 30
2,4,5-TP ND 0.500 0.500 0 74.7 38 106 0 0 30
Surr: DCAA 393 500.0 78.6 20 140 0
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used -to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 14 of 50

SummitEnvironmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
Lr,%'IKVINrAH,NIAl. 9t;4.;H?4�JLUGILS,JKU.
Cuyahoga Falls, Ohio44223
WO#: 17030217
tX.n r1s�f�,caf C;rbofgta�te6 TEL: [phone] FAX [phone]
Websiter htto.-Mvww.settelcconz
15 Mar-17
Client:
Synagro
Project:
Dunn WWTP
BatchID: 25849
Sample ID mb-25849
SampType: mblk
TestCode: tclp-svoc-cpe Units: mg/L
Prep Date: 3/8/2017
RunNo: 66588
Client ID: PBW
Batch ID: 25849
TestNo: SW8081A SW3510C
Analysis Date: 3/9/2017
SegNo: 1098253
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, total
ND
0.00500
Toxaphene
ND
0.0100
Endrin
ND
0.000500 -
gamma-BHC
ND
0.000500
Heptachlor
ND
0.000600
Heptachlor epoxide
ND
0.000500
Methoxychlor
ND
0.000500 d
Surr: TCMX
8.23
10.00 82.3 10 119
Surr: DCB
11.9
10.00 119 10 119 S
Sample ID Ics-25849
SampType: Ics
TestCode: telp-svoc-cpe Units: mg/L.
Prep Date: 3/8/2017
RunNo: 66588
Client ID: LCSW
Batch ID: 25849
TestNo: SW8081A SW3510C
Analysis Date: 3/9/2017
SegNo: 1098254
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD'Ref Val
%RPD RPDLimit Qual
Endrin
0.00600 0.000500
0.00500' 0 -120
20
157
gamma-BHC
0.00426 0.000500
0.00500 0 85.3
22
137
Heptachlor
0.00553 0.000500
0.00500 0 111
24
121
Heptachlor epoxide
0.00565 0.000500
'0.00500 0 113
27
152
Methoxychlor
0.00608 0.000500
0.00500 0 122
10
199
Surr: TCMX
10.5
10.00 105
10
119
Surr: DCB
14.1
10.00 141
10
119 S
Qualifiers: *
Value.exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or analysis exceeded
J - Analyte detected below quantitation limits
M Manual Integration used to determine
Original
MC
Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
0 RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL Permit Limit
R RPD outside accepted recovery limits
Page 15 of 50

r
Summit Environmental Technologies, Inc. C SUMMARY REPORT
surafalur 3310 Win St. Q
t:rtvIKU'Nr41.N1AL as aaaltnD011.5,INC. Cuyahoga Falls, Ohio44223 WO#: 17030217
l.Kr3ilrtfcal C rbpt gir ,$es TEL:.[phone] FAX.- [phone]
Website: httv:lhvww.settelc.cons 15 Mar-17
Client: Synagro
Project: Dunn WWTP BatchID: 25849
Sample ID 17030215-001ams
SampType: ms
TestCode: telp-svoc-cpe Units: mg/L
Prep Date: 3/8/2017
RunNo: 66588
Client ID: BatchQC
Batch -ID: 25849
TestNo: SW8081A SW3510C
Analysis Date: 3/9/2017
SegNo: 1098255
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
0.0105
0.00100
0.0100
0
105
20
157
gamma-BHC
0.00712
0.00100
0.0100
0
71.2
22
137
Heptachlor
0.00878
0.00100
0.0100
0
87.8
24
121
Heptachlor epoxide
0.00969
.' 0.00100
0.0100
.0
96.9
27
152
Methoxychlor
0.0117
0.00100
0.0100
0
117
10
199
Surr: TCMX
12.0
20.00
60.0
10
119
Surr: DCB
22.3
20.00
112
10
119
Sample ID 17030215-001amsd,
SampType: msd
TestCode: tclp-svoc-cpe Units: mg/L
Prep Date: 3/8/2017
RunNo: 66588
Client ID: BatchQC
Batch ID: 25849
TestNo: SW8081A SW3510C
Analysis Date: 3/9/2017
SegNo: 1098256
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
0.00891
0.00100
0.0100
0
89.1
20
157
0.0105
16.7
30
gamma-BHC
0.00672
0.00100
0.0100
0
67.2
22
137
0.00712
5.78
30
Heptachlor
0.00825
0.00100
0.0100
0
82.5
24
121
0.00878
6.20
30
Heptachlor epoxide
0.00868 -
0.00100
0.0100
0
86.8
27
152
0.00969
10.9
30
Methoxychlor
0.00961
0.00100
0.0100
0
96.1
10
199
0.0117
19.9
30
Surr: TCMX
12.4
20.00
61.8
10
119
0
Surr: DCB
16.9
20.00
84.5
10
119
0
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 16 of 50

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
LNNINUIN6n:N IAI. Y bt;HW4LUU1!:S, INC Cuyahoga Falls, Ohio 44223 W09: 17030217
- Analyh affS Labaratorie r TEL: [phone] FAX.- [phone]
Website: hap:Mviviv.settekcom 15 Mar-17
Client: Synagro
Project: Dunn WWTP BatchID: 25878
Sample ID MB-25878
SampType: MBLK
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 3/8/2017
RunNo: 66688
'lient ID: PBW
Batch ID: 25878
TestNo: SW8270C SW3510C
Analysis Date: 311312017
SegNo: 1099749
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD"Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
ND
0.0200
2,4,5-Trichlorophenol
ND
0.0500
2,4,6-Trichlorophenol
ND
0.0500
2,4-Dinitrotoluene
ND
0.0100
Cresols, Total
ND
1.00
Hexachloro-1,3-butadiene
ND
0.00400
Hexachlorobenzene
ND
0.0100
Hexachloroethane
ND
0.0200
Nitrobenzene
ND
0.0200
Pentachlorophenol
ND
0.0500
Pyridine
ND
0.0500 ,
Surr: 2-Fluorophenol
0.335
0.5000
67.0
10
109
Surr: Phenol-d6
0.343
0.5000
68.6
10
109
Surr: Nitrobenzene-d5
0.376
0.5000
75.3
19
120
Surr: 2,4,6-Tribromophenol
0.457
0.5000
91.4
10
120
Surr:2-Fluorobiphenyl
0.350
0.5000
70.0
22
117
Surr: p-Terphenyl-d14
0.436
0.5000
87.2
34
116
Sample ID LCS-25878
SampType: LCS
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 3/8/2017
RunNo: 66688
Client ID:. LCSW
Batch ID: 25878
TestNo: SW8270C SW3510C
Analysis Date: 3/13/2017
SegNo: 1099750
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 17 of 50

SUMoftllmt
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
tr0lIKVNTA1.NIAl, RhC,HNULCUI-'S,INC.
Cuyahoga Falls, Ohio44223
WO#: 17030217
,tlnal(,Ili al tzborifvrfP-
TEL: [phone] FAX- [phone]
Website: http:/hvww.settek.com
15 Mar-17
Client:
Synagro
Project:
Dunn WWTP
BatchID: 25878
Sample ID LCS-25878
SampType: LCS
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 3/8/2017
RunNo: 66688
client ID: LCSW
Batch ID: 25878
TestNo: SW8270C SW3510C
Analysis Date: 3/13/2017
SegNo: 1099750
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.198
0.0200
0.2000
0
99.0
19.1
126
2,4,5-Trichlorophenol
0.257
0.0500
0.2000
0
128
11.7
151
2,4,6-Trichlorophenol
0.254
0.0500
0.2000
0
127
12.4
150
2,4-Dinitrotoluene
0.279
0.0100
0.2000
0
140
20.6
140
Cresols, Total
ND
1.00
0.4000 '
0
119
10
129
Hexachloro-1,3-butadiene
0.202
0.00400
0.2000
0
101
14.7
137
Hexachlorobenzene
0.215
0.0100
0.2000
0
107
12
139
Hexachloroethane
0.214
0.0200
0.2000
0
107
14.8
132
Nitrobenzene
0.233
0.0200
0.2000
0
116
15.6
138
Pentachlorophenol
0.201
0.0500
0.2000
0
101
10
156
Pyridine
0.0705
0.0500
0.2000
0
35.3
10
126
Surr: 2-Fluorophenol
0.454
0.5000
90.7
10
147
Surr: Phenol-d6
0.464
0.5000
92.7
10
140
Surr: Nitrobenzene-d5
0.480
0.5000
95.9
10
169
Surr: 2,4,6-Tribromophenol
0.590
0.5000
118
10
185
Surr: 2-Fluorobiphenyl
0.442
0.5000
88.4
10
169
Surr: p-Terphenyl-d14
0.495
0.5000
99.0
10
179
Sample ID 17030030-001AMS
SampType: MS
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 3/8/2017
RunNo: 66688
Client ID: BatchQC
Batch ID: 25878
TestNo: SW8270C SW3510C
Analysis Date: 3/13/2017
SegNo: 1099752
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank . E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 18 of 50

Sum, 7
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT -
!:r„VirVNr,14N1ALIrcear,�tiurr�t�s;JKC.
Cuyahoga Falls, Ohio44223
WO#: 17030217
IS,r,ail. U,car Laboralbrief,
TEL: [phone]_FAX.•.[phone] _
Website: http:/hvwwsettelccom
I5-Mar-17
Client:
Synagro
Project:.
Dunn WWTP
BatchID: 25878
Sample ID 17030030-001AMS
SampType: MS
TestCode: SVOC-BNA T Units: mg/L
Prep. Date: 3/8/2017
RunNo: 66688
Client ID: BatchQC
Batch ID: 25878
TestNo: SW8270C SW3510C
Analysis Date: 3/13/2017
SegNo: 1099752
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
.1,4;Dichlorobenzene
0.416
0.0800
0.4000 0
2,4,5-Trichloropheinol
0.501
0.200
0.4000 0
2,4,6-Trichlorophenol -
0.497
0.200
0.4000 0
2,4-Dinitrotoluene
.0.524
0.0400
0.4000 0
-Cresols, Total
ND
4.00
0.8000 0
Hezachloro-1,3-butadiene
0.393—
0.0160'
0.4000 0
Hexachlorobenzene
0.416
0.0400
0.4000 0
Hexachloroethane.-
0.458
0.0800
0.4000 0
Nitrobenzene
0.478
0.0800
0.4000 0
Pentachlorophenol
0.441
0.200
0.4000 0
Pyridine
ND
0.200
0:4000 0
Surr: 2-Fluorophenol
0.841
1.000
Surr: PhenoW6
0.856
1.000
Surr: Nitrobenzene-d5 ..
0.917
1.000
Surr: 2,4,6-Tribromophenol
1.04
1.000'
Surr. 2-Fluorobiphenyl
0.806
1.000
Surr: p-Terphenyl-d14
0.919
1.000
A04
29
112
125
53
123
124
- 50
125
131
57
128
119
20
125
98.2
22
124
104
53
125
115
21
.115
120
'45
121
110
35
138
21.3
10
126
84.1
10
147
85.6
10
140
91.7
10
169
104
10 _
1.85
..80.6
.10
91.9
10
179
S
S
Sample ID 17030030-001AMSD
SampType: MSD
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 3/8/2017
RunNo: 66688
Client ID: BatchQC.
Batch ID: 25878
TestNo: SW8270C SW3510C .
Analysis Date: 3/13/2017
SegNo: 1099753
Analyte
Result
PQL SPK value 'SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level. .
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Methoii Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
Page 19 of 50
E Value above quantitation range
M Manual Integration used to determine
O . RSD is greater than RSDlimit Original '
R RPD outside accepted recovery limits

,a Summit Environmental Technologies, Inc. QC SUMMARY REPORT
1 3310 Win St.
�rnitt4�r•Inu:NW.. iML"HWLQUIt-S, rho. Cuyahoga Falls, Ohio44223 WO#: 17030217
_. , na;ylFaaf Ctrbor furie.5 TEL: [phone] FAX.- [phone]
Website: httD://wtvw.settelc.com 15 Mar-17
Client: Synagro
Project: Dunn WWTP BatchID: 25878
Sample ID 17030030-001AMSD
SampType: MSD
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 3/8/2017
RunNo: 66688
Client ID: BatchQC
Batch ID: 25878
TestNo: SW8270C SW3510C
Analysis Date: 3/13/2017
SegNo: 1099753
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.368
0.0800
0.4000
0
92.1
29
112
0.4164
12.2 30
2,4,5-Trichlorophenol
0.438
0.200
0.4000
0
110
53
123
0.5008
13.4 30
2,4,6-Trichlorophenol
0.433
0.200
0.4000
0
108
50
125
0.4968
13.8 30
2,4-Dinitrotoluene
0.444
0.0400
0.4000
0
ill
57
128
0.5244
16.7 30
Cresols, Total
ND
4.00
0.8000
0
103
20
.125
0
0 30
Hexachloro-1,3-butadiene
0.345
0.0160
0.4000
0
86.2
22
124
0.3928
13.0 30
Hexachlorobenzene
0.370
0.0400
0.4000
0
92.6
53
125
0.4164
11.7 30
Hexachloroethane
0.391
0.0800
0.4000
0
97.8
21
115
0.4580
15.7 30
Nitrobenzene
0.413
0.0800
0.4000
0
103
45
121
0.4780
14.5 30
Pentachlorophenol
0.387
0.200
0.4000
0
96.7
35
138
0.4408
13.0 30
Pyridine
ND
0.200
0.4000
0
38.1
10
126
0
0, 30
Surr: 2-Fluorophenol
0.788
1.000
78.8
10
147
0
Surr: Phenol-d6
0.817
1.000
81.7
10
140
0
Surr: Nitrobenzene-d5
0.844
1.000
84.4
10
169
0
Surr: 2,4,6-Tribromophenol
0.959
1.000
95.9
10
185
0
Surr: 2-Fluorobiphenyl
0.762
1.000
76.2
10
169
0
Surr: p-Terphenyl-dl4
0.830
1.000
83.0
10
179
0
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit
P Second column confirmation exceeds PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
R
Original
Page 20 of 50

' 1
i
f Summit Environmental Technologies, Inc. QC SUMMARY REPORT
A u .f I ' . 3310 Win St.
�rsvikca r+rne;n IEII. a a:+ acracat utt�s, trig . Cuyahoga Falls, Ohio 44223 WO#: 17030217
ffl
i4rylyrtdc aP CnSargtarir s TEL: [phone] FXX." (330)" 253-4489
Website: http.-1Avtvw.sette1ccom 15 Mar-17
Client: Synagro
Project: Dunn WWTP BatchID: R66453
Sample ID MB-R66453
SampType: MBLK
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 66453
Client ID: PBS
Batch ID: R66453
TestNo: SW9014
Analysis Date: 3/6/2017
SegNo: 1095926
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive ND 0.500
Sample ID LCS-R66453
SampType: LCS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 66453
Client ID: LCSS
Batch ID: R66453
TestNo: SW9014
Analysis Date: 3/6/2017
SegNo: 1095926
Analyte
Result
PQL SPK value SPK Ref Val -
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 1.01 0.500 1.000 0 101 85 110
Sample ID 1702149&008AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 66453
Client ID: BatchQC
Batch ID: R66453
TestNo: SW9014
Analysis Date: 3/6/2017
SegNo: 1095928
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 1.07 0.500 1.000 0 107 81.6 122
Sample ID 17021495-008AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 66453
Client ID: BatchQC
Batch ID: R66453
TestNo: SW9014
Analysis Date: 3/6/2017
SegNo: 1095929
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
1.05 0.500
1.000 0 105 81.6
122
1.072 2.46 5
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H
MC
Holding times for preparation or analysis exceeded
Value is below Minimum Compound Limit.
J . Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
M
O
Manual Integration used to determine
RSD is greater than RSDlimit Original
P
Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits
Page 21 of 50

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
Sum, l 3310 Win St.
L-MIKU+N51I;N I A[. I i:cHwiLucut:S: In . Cuyahoga Falls, Ohio 44223 ,
Rlydtl2P:raP C:Ttia� wtc is WO#: 17030217
TEL: [phone] FAX-,[phone]
Website: http://ivivw.settelf.coni 15 Mai-17
Client: Synagro
Project: Dunn WWTP BatchED: R66453
Sample ID 17021495-OOSAMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 66453
Client ID: BatchQC-
Batch ID: R66453
TestNo: SW9014
Analysis Date: 3/6/2017
SegNo: 1095929
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua[
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 22 of 50

surdialut
Summit Environmental Technologies,Inc. QC SUMMARY REPORT
3310 Win St.
LMVIHU1NT,1I,N IAI. a t;%:HNULUG1.-S, INC. Cuyahoga Falls, Ohio 44223
fsr,8f4atf•GaP t ?Tbcarsforir TEL: [phone] FAX. [phone] WO#: 17030217
Website: http:/hvww.sette1ccom IS Mar-17
Client: Synagro
Project: Dunn WWTP BatchID: R66473
Sample ID MB-R66473
SampType: MBLK
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 66473
Client ID: PBS
Batch ID: R66473
TestNo: SW9034
Analysis Date: 3/6/2017
SegNo: 1096274
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Sulfide, Reactive ND 25.0
Sample ID LCS-R66473
SampType: LCS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 66473
Client ID: LCSS
Batch ID: R66473
TestNo: SW9034
Analysis Date: 3/6/2017
SegNo: 1096275
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 2100 25.0 2250 0 93.3 85 130115
Sample ID 17021495-OOBAMS
SampType: MS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 66473
Client ID: BatchQC
Batch ID: R66473
TestNo: SW9034
Analysis Date: 3/6/2017
SegNo: 1096276
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 2130 25.0 2250 0 94.7 80 120
Sample ID 17021495-OOBAMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/Kg
Prep Date-
RunNo: 66473
Client ID: BatchQC
Batch ID: R66473
TestNo: SW9034
Analysis Date: 3/6/2017
SegNo: 1096277
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Sulfide, Reactive 2140 25.0 2250 0 95.1 80 1 120 2130 0.468 30
Qualifiers: 1k Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 23 of 50

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
su—A-4101ir
3310 Win St.
I:MIxVaJ6tt.MIAl. Ilzu"diriLuGl1:S:INC. Cuyahoga Falls, Ohio44223
r6ttylyticat f r.Ttafsto�ie TEL: [phone] FAY. [phone] WO#: 17030217
Website: ht1pr/hvww.sette1ccon: 15=Mar-17
Client: Synagro
Project: Dunn WWTP BntchID: R66473
Sample ID 17021495-008AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/Kg
Prep Date: -
RunNo: 66473
client ID: BatchQC
Batch ID: R66473
TestNo: SW9034
Analysis Date: 3/6/2017
SegNo: 1096277
%nalyte
Result
. PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD . RPDUrnit Qual
Qualifiers: * • Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 24 of 50

Sununit Environmental Technologies, Inc. QC SUMMARY REPORT
sulaAMIT 3310 Win St.
eraVIRUINNUNJAI. or:ca1ryoLUU1!:6,trtc, Cuyahoga Falls, Ohio44223 WO#: 17030217
. l.nali{L'ca/ Lshar�torle TEL: [phone] FAX.- [phone]
Website: htty.-Mvivw.settek.coin IS Mm'-17
Client: Synagro
Project: Dunn WWTP BatchlD: R66500
Sample ID 17030215-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 66500
Client ID: BatchQC
Batch ID: R66500
TestNo: SW1030
Analysis Date: 3/8/2017
SegNo: 1096787
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability ]on -flammable. 0 0 20
Sample ID 17030215-001ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 66500
Client ID: BatchQC
Batch ID: R66500
TestNo: SW1030
Analysis Date: 3/8/2017
SegNo: 1096788
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Ignitability Ion -flammable. 0 0 20
Sample ID 17030217-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 66500
Client ID: Dunn WWTP
Batch ID: R66500
TestNo: SW1030
Analysis Date: 3/8/2017
SegNo: 1096790
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability Ion -flammable. 0 0 20
Sample ID
17030217-001ATRIP SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 66500.
Client ID:
Dunn WWTP Batch ID: R66500
TestNo: SW1030
Analysis Date: 3/8/2017
SegNo: 1096791
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability Ion -flammable. 0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 25 of 50

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
l'Y1 3310 Win St.
tr ixr�raou:NIAl. IW:HW0LL1U1!:6,INC. Cuyahoga Falls, Ohio44223
_ �Vr3IStPfcaP i_�tata,ralr�,�Ja4 WO#: 17030217
TEL: [phone] FAX.- [phone]
Website: hgp://ivww.setteh.com 15-Mm•-17
Client: Synagro
Project: Dunn WWTP BatchID: R66500
Sample ID 17030217-001ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 66500
Client ID: Dunn WWTP
Batch ID: R66500
TestNo: SW1030
Analysis Date: 3/8/2017
SegNo: 1096791
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sample ID 17030219-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 66500
Client ID: BatchQC
Batch ID: R66500
TestNo: SW1030
Analysis Date: 3/8/2017
SegNo: 1096793
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability Ion -flammable. 0 0 20
Sample ID 17030219-001ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 66500
Client ID: BatchQC
Batch ID: R66500
TestNo: SW1030
Analysis Date: 3/8/2017
SegNo: 1096794
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability Ion -flammable. 0 0 20
Sample ID 17030373-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 66500
Client ID: BatchQC
Batch ID: R66500
TestNo: SW1030
Analysis Date: 3/8/2017
SegNo: 1096796
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability Ion -flammable. 0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 26 of 50

_ Sunsmit Environmental Technol10 W Inc. (�C SUMMARY
UM � RY REPORT
surn I 3310 Win St. �Ll. �7 U l>lt i R �'� A l
tNVI+ QsNrnL•N IAI. I W-H74ULrjGU:S, JN,c. Cuyahoga Falls, Ohio 44223 WO#: 17030217
Aitalyticaf L bonispirlerr TEL: [phone] FAX. [phone]
Website: hQ./hvww.seitelccon: IS Mar-17
Client: Synagro.
Project:, Dunn WWTP BatchID: R66500
Sample ID 17630373-001ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 66500
Client ID:" BatchQC
Batch ID: R66500
TestNo: SW1030
Analysis Date: 3/8/2017
SegNo: 1096797
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighUmit RPD Ref Val
%RPD RPDLimit Qual
Ignitability Ion -flammable. 0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 27 of 50

"sl
1
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
Lr.vir Vr-JrnuN iAL a kt;HNcatrtU1!:S, W.C. Cuyahoga Falls, Ohio 44223
A6nall,16=1 Labp,r;: foric-5: TEL: [phone] FAX.- (330) 253=4489
WO#: 17030217
Website: http://wlvw.settelc.com
15-Mar-17 -
Client: Synagro
Project: Dunn WWTP
BatchlDi 1166502.
Sample ID Ics 20ppb L-0306
SampType: LCS
TestCode: voc-MSTR n Units: mg/L
Prep Date:
RunNo: 66502
Client ID: LCSW
Batch ID: R66502
TestNo: SW8260B
Analysis Date: 3/7/2017
SegNo: 1096835
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.0200
0.00500
0.0200
0
100
71
138
Benzene
0.0191
0.00500
0.0200
0
95.7
75
137
Chlorobenzene
0.0192
0.00500
0.0200
0
95.9
77
132
Trichloroethene
0.0196
0.00500
0.0200
0
97.8
64
119
Surr:4-Bromofluorobenzene
51.4
50.00
103
70
130
Surr: Dibromofluoromethane
49.4
50.00
98.8
70
130
Surr: Toluene-d8
51.1
50.00
102
70
130
Sample ID mblk
SampType: MBLK
TestCode_ voc-MSTR n Units: mg/L
Prep Date:
RunNo: 66502
Client ID: PBW
Batch ID: R66502
TestNo: SW8260B
Analysis Date: 3/7/2017 -
SegNo: 1096837
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
ND
0.00500
1,2-Dichloroethane
ND
0.00500
MEK
ND
0.0250
Benzene
ND
0.00500
Carbon tetrachloride
ND
0.00500
Chlorobenzene
ND
0.00500
Chloroform
ND
0.00500
Tetrachloroethene
ND
0.00500
Trichloroethene
ND
0.00500
Vinyl chloride
ND
0.00200 QC+
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit - Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 28 of 50

munimSummit Environmental Technologies, Inc. QC SUMMARY REPORT
s3310 Win St.
L'Cu+'IHWIMUNIAL 14a�9isfULUtilt S; art��. Cuyahoga Falls, Ohio 44223 WO#: 17030217
lot
k tt�RdcaP C:Tu�Qratnr es TEL: [phone] F- [phone]
Website: h11p.1Avww.sette1ccom 15-Mar-17•
Client: Synagro
Project: Dunn WWTP BatchID: R66502
Sample ID mblk
SampType: MBLK
TestCode: voc-MSTR n Units: mg/L
Prep Date:
RunNo: 66502
Client ID: PBW
Batch ID: R66502
TestNo: SW8260B
Analysis Date:_ 3/7/2017
SegNo: 1096837
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
48.9 50.00 97.9 70 - 130
50.8 50.00 102 70 130
50.1 50.00 100 70 130
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 29 of 50

Summit Environmental Technologies, Inc.
3310 Win St. QC SUMMARY REPORT
I Suramn XVIKVTJ I.,N IAl, 0I;UHRULStGIhs, N.C. Cuyahoga Falls, Ohio 44223 WO#: 17030217
F
Ana4dlml LTbor ilo ier TEL: [phone] FAX. [phone]
Website: http://wivw.settelc.com 15 Mar-17
Client: Synagro
Project: Dunn WWTP BatchID: R66502
'ample ID 17030217-001ams
SampType: MS
TestCode: tclp-voc-MST Units: mg/L
Prep Date:
RunNo: 66502
;lient ID: Dunn WWTP
Batch ID: R66502
TestNo: SW8260B
Analysis Date: 3/8/2017
SegNo: 1096853
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.174
0.0100
0.200
0
86.9
39.9
.160
1,2-Dichloroethane
0.170
0.0100
0.200
0
85.0
42.5
157
MEK
1.02.
0.0500
1.00
0
102
16.6
227
Benzene
0.190
0.0100
0.200 •
0
94.8
38.1
155
Carbon tetrachloride
0.188
0.0100
0.200
0
93.8
40.8
162
Chlorobenzene
0.200
0.0100
0.200
0
100
35.7
168
Chloroform
0.186
0.0100
0.200
0
93.2
18.3
199
Tetrachloroethene
0:197
0.0100
0.200
0
98.4
10
261
Trichloroethene
0.191
0.0100
0.200
0
95.3
23.8
175
Vinyl chloride
0.232
0.0100
0.200
0
116
10
165
Surr:4-Bromofluorobenzene
513
500.0
103
84.6
130
Surr: Dibromofluoromethane
478
500.0
95.5
71.4
127
Surr: Toluene-d8
510
500.0
102
74.6
127
QC+
Sample ID 17030217-001amsd
SampType: MSD
TestCode: tclp-voc-MST Units: mg/L
Prep Date:
RunNo: 66502
client ID: Dunn WWTP
Batch ID: R66502
TestNo: SW8260B
Analysis Date: 3/8/2017
SegNo: 1096854
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.177
0.0100
0.200
0
88.6
39.9
160
0.174
1.99
25
1,2-Dichloroethane
0.169
0.0100
0.200
0
84.4
42.5
157
0.170
0.590
25
MEK
1.01
0.0500
1.00
0
101
16.6
227
1.02
1.52
25
Benzene
0.186
0.0100
0.200
0
93.1
38.1
155
0.190
1.76
25
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded 7 Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 30 of 50

a Summit Environmental Technologies, Inc. QC SUMMARY REPORT
,S 1 3310 Win St.
tr,-VIHEJ;Nrni.NIALII.VHWJL4t33-�s,,111C. Cuyahoga Falls, Ohio44223
:lstad4df,cal Labprgfafip: TEL: [phone] FAX.- [phone] WO#: 17030217
Website: htty.-Mvivmsettelcconz 15-Mar-17
Client: Synagro
Project: Dunn WWTP BatchID: R66502
Sample ID 17030217-001amsd
SampType: MSD
TestCode: tclp-voc-MST Units: mg/L
Prep Date:
RunNo: 66502
Client ID: Dunn WWTP
Batch ID: R66502
TestNo: SW8260B
Analysis Date: 3/8/2017
SegNo: 1096854
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Carbon tetrachloride
0.182
0.0100
0.200
0
91.1
40.8
162
0.188
2.97
25
Chlorobenzene
0.189
0.0100
0.200
0
94.3
35.7
168
0.200
5.87
25
Chloroform
0.184
0.0100
0.200
0
92.2
18.3
199
0.186
1.08
25
Tetrachloroethene
0.180
0.0100
0.200
0
90.2
10
261
0.197
8.70
25
Trichloroethene
0.186
0.0100
0.200
0
92.8
23.8
175
0.191
2.66
25
Vinyl chloride
0.223
0.0100
0.200
0
112
10
165
0.232
3.91
25 QC+
Surr:4-Bromofluorobenzene
490
500.0
98.1
84.6
130
0
25
Surr: Dibromofluoromethane
486
500.0
97.3
71.4
127
0
25
Surr: Toluene-d8
512
500.0
102
74.6
127
0
25
Qualifiers: " Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding tines for preparation or analysis exceeded 7 Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 31 of 50

Summit Environmental Technologies, 1ne. QC SUMMARY REPORT
m";°� M 13310 LVin St.
Itz-VIRVINMUN JAL 1 9.Ck1ddOLUU1t:S, INC. Cuyahoga Falls, Ohio 44223 WO#: 17030217
ArWyLlcxl Laborall2rier TEL: [phone] FAX.- [phone]
Website: http://1vivw.settelccom IS Mar-17
Client: Synagro
Project: Dunn WWTP BatchID: R66612
Sample ID LCS-R66612
SampType: LCS
TestCode: pH_Oil(9045 Units: s.u.@19.6C
Prep Date:
RunNo: 66612
Client ID: LCSW
Batch ID: R66612
TestNo: SW9045D
Analysis Date: 3/10/2017
SegNo: 1098612
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 100 90 110
Sample ID 17030430-001ADUP
SampType: DUP
TestCode: pH_Oil(9045 Units: sm.@20.1C
Prep Date:
RunNo: 66612
Client ID: BatchQC
Batch ID: R66612
TestNo: SW9045D
Analysis Date: 3/10/2017
SegNo: 1098614
Analyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 5.8 0 0 5.8 0.7 10
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 32 of 50

rerswm imMe"MSummit Environmental Technologies, Inc. Analysis RequesllChain of Custody
3310 Win Street For Summit Environnlontal'Technologies, Inc, use only
Cuyahoga Falls, Ohio 44223 Tel: 330,253.8211. Fax: [phone] Page of SET No.
Company .Name (Please Print) Project Name EtinalytiClll parameters and Methoft
-70;Z
LJ/
Email
Report
Sampled lay _ Check if Oldo VA Samples ✓ U
'p Date Tune �'
A) # Sample Identification Colkecled CoRk".' 0
CD
W I b xe
�l
O
—n
01
CD
V,
Notes/Comments:.
/VC )�� 1t
�by:�,Tame Must be approved
in lab
Rush Requested By:.� by lab manager
white end yellowy pages should accomsa
pany mples toAnc laboratory. The client retains the pink page. Q /; Q
age 1 of 2

Efff:chra Dieu 91+1 An"
DC-7
Roe. 1$
Summit EnvizonImental "technologies, Inc.
Cooler Receipt Form
Initials of person inspecting cooler and samples—_� r
Client: SY.4 �
Order Number:
Date opened and samples inspected31
Date Received✓ T'trne Received;3�C}
ccoler(s)
Number of CoolerslBozes- -
NIA
- Shipper EO EX UPS OHL Airborne US Postal Walk-in Pickup Other. -
Packaging: Peanuts 131bbte Wr
Paper Foam None Other:
Tape on coolerlbox C 1 � N NIA
J
N
NJA
Custody Seals intact
,-Y--�
l Y 1 N
NIA
C-O-C in pl slit _
fce�L_ slue ice
- pr�esen, acbsent 1 mailed N.A
1
Sample Temperature IR•Gun#1®0! 2045g CF t0_v °C `t- !- -C
NIA
Radiological Testing Instrument serial #15127
Y N
N!
(see page 2 for scan results)
,,Use 1 street per sample for Radiological Testing.
if sample is tfo"r, tt;e Radiological Safety Officer must be notified
immediately.
C-O-C filled out property
N
NJA
Samples in separate bags •
N
NIA
containers intact`
�Y-�
� r _ N
NIA
-if no, list broken sample(s):. _
-�-�.
- ---- -
Sample label(s) cornpiete (tb, date, eta) -
N
NIA
Label(s) agree with C-O-C
N
N/A
Correct containers used
E yl N
NIA
Sufficient sample received
N
NIA
Samples received within holding time
CY N
Subbles absent from 40 nil- vials-
Y N
NIA
-Samples with bubbles -6mm are acceptable. Indicate k,j1)ble size if >6mm.
Was client contacted about samples Y
N
Will: client send new samples Y
N
Client contact:
bateliime:,,_, _
Logged in by: '
Comments:
--
Pa]e 1 of 2
N
v-
O
N
N
i)
n3
0-
Page 34 of 50 r.

North Carollina WatowatorlQvcjurldvvater Laboratbry-der0ficalloij,
Ofietiflied Parameters LfsflaU
L;1b N'tung Summit C-awlrbnm, en[d TL-.V(qoh>(jjt:-..,
Iris.
N-rialimir.
33 It Wfu Street
Cophoga Falls. Ot t 44Z23.
t),piraVca Date. 121,31i211.1y
DO, If Las[ Ammlament 2j2t2-u17
'RAMETr
V10 RGANT6
RESUM, SLISPENDLID
BOD
SM 2540 01907 tAumlorjsle'
91A a-Ml A uom,16)
I A
RES[OVE. TOTAL
01 E
Sht Z rC4B-199? OiQUA.nsf
SVV-846 9065 A (An mijaj
COE)t.l+a�_�151%.�,Row.
4A 104, (A.qojr"gt;i
"p57U220C-190 fAq.qc)Lt%,j,
FL IXIRIDE
S1JfLFAT1 E,
EPf, '31:D.11, Roo 2, 1. 100 fAqpGrjjj*)
EPA TJf J-U. Vw--2.1, 1993 (Acpyt,,okiqj
(Aqua uusj
5ULIFIM
CO
c:)
Lo
T—
4—
INGRC6ANIC PHENCILS
METAL
4—
0
0
F*f,,,. e4mi Pam. 1078 4Arpjr,-W.-qI.
TrW-reETALS
Lo -
-NIT-10GEN NITRATE-
SW-046 1311 (ALIgma u)4)
EPA 300 U. rev Z 1. 19112 (Aqueoll-R!
tm
tm
SOMO'SI056 A ?.Aquer6j
EPA 209.7. Rev. 4.4. 1954 (Atjuilxui5.!
(73
N I T fiO U. C 14, NO TRITE
SVV—VG GO 10 D fAqtjeovs:-
EVA 30D 0 Rev. 2.1, 150-3
EPA 206.8, Rev, $A,1924 fAqupal.,;,i
SV.1-848 MH;A:Aqucous5
NITROGEN, NO3 - N-C2
I. -PA 100:0. Rev. 1-1, 1093 P<Ulmusy
EPA 200.7, Ray.41,4,1994 (AqcmouaI
WAL R,1 6 Q056 A (Awrous)
SIN446 6-010 V fAqirna.us}
NITRO(IIN 1UTALiKJELQA1-I.
-EPA :Pf)o,& Rby, S.A. m4
SM e590 Norg B IR07 (&ltl 4500: NI-r� D-1997) fAziumTS)
SI.IV-046 11302C 6 (IVJL40005)
ARS E Nl:,
EIIA 1 U154 Roo. G (Aqueoij,-)
EPA 2M 1. Rev. 4.4.. 19D4 (!%cr;t:utj*;
Site-MAl'i q071 8 (Non-Aquoat4j
%YV-F A6 WID D (Mueoi m)
EPA 20011, Rul. 5.4 i t 994 (Aquuois)
-SkIM.45 qoZ!, r) (Nujn-Aqueauql
54V-fi4ei
P�&,se i-c �p km. 7rrml-
v%RI1;Ir4
F1,-8 200.7 Rev. 4 4 (IR-34) (Aqueous)
EVA2&.7 Rev.4.4, 1-9,CM(Af4d.nMIS3
SIV-84D. 911113 0 (klu Uou 5.1
RESIC-OF D16-3,01-VEID 1M C,
EPA LHO-6, RoN.S.4. 1444 (Aq.ciroitq
2540 C,-109NAqL1%iufi)
SW-94.0 CO20 B
7 flit ceftHicmar, "Vre&
me 10 knells,', 1 M NCAC; 2H.E-E,01

M (), rth Carolin,a Wa5tewaler/Groundmwr LaboratoryCertMitiixion
Ceirtifled Parameters Listing
Lab Name $i;jrlljjjjj ETIVITunmPrOsil TmAmologres, -nc- -
Address: 32• 10 Wirt Street
Cup.hogo r-ofb, OM 4*Q21.
tho UbNe nam" 13tumlary ortal 'ho saqLjrkmenhj
V 2H herehycAwrilieJ tot the njrmjwfLmcn; UJIME t1Al(1tlrwtc!r Adrld tAow.
1"RFRAMETERS
EERYLLILM',
EPA zm 8, r--wv 5.e. mm o,14arx9)
t , 0A 200A, * Rev. 5.d K494 (A%1[30u_-j
SWA40 60.20 B
8,16"40 61120.9 (Aqueum5l
LIT 11 UUM,
BORON
CPX00.7, R(!'V: 4 4, 1 Sqk- ift utg;rtz)
EPA 713C.6. Rev, 5.4. 199d (tocuorjus)
�'Ahi-34G 0301 C, D �i%queoj6)
SIN-8413 GM B (A que-oatj
MAGNEPSIUM
CADMIU KI
EPA 200 T W-v 4.4 1 90d J,Aq w--,vus)
EPA 2011 V. Rev. 4.4, 1 D,5),t J;%(juucus)
MANC/ANESE
r PA 20D.8, Rev. 6.4. ISIA epPALIWU.91)
ERA 290. ?. qev. 4.4, 10D4 (A-lijerjus',
SW,2415 604 U 1,1Avuec;w.i
SW,H' - (j 6019 D {Aqwcouq),
CA—, ' Uum
2 0
EPA 0. 0. Raw 51 .1 , 11 ci 1�44 gAq li oo us.1
MAt JA 0 50.10 D
MERCuRy
CHROMIUM TOTAL
EPA Rim: 3-0. 1994 (A01glogt)
EPA 2007,.ROV 4.4, IIAM rel-1prious)
V1-.F!4f> 7470A (AqLn"us)
� SYV -Z4&101DD(Aqnp.n,j�.) -
EPA U33211 F (Aokntims)
EVA 200 8, pp.0 q4 Inner lAqunows)
1602-5 13 (Aqu6rjus)
EPA,200.7, Rev. 4.4 Ic?.q.
Q Q00ALT
§1N-646 Aq usoi i&,,
r-PA 2.001.7. Rev. t.-j. 19 A Aouernas)
260-. NVY. 5.4. M14 (Aepjpn4s1
SW-84 6 0111)0 (Acluemis)
CO2-," B Aqopolts',
ERA P.MV, Rev. 5.4, 1 Nod iAuutouzq
I
MICKEL
EPA 2W,9, 1.79v. 5.4. 1991, (AqLjnlK.1
COPPER
$A-445 6 , 020 B Oqueous]
EPA 200,1. Hm. 4.A. '04 jP.,.ucroou:j
?SW-8413 49010 D
EPA1brj.-,, fle.L%l 4 4. 1994 (AcmnwN�
EPA 200 0, Rev. 5A, 1 D r14 -Aqtieows)
SV4-846 WiO D iAquooue)
U-1.9'M
IRUN
EPA'200.8, Rev, ri.A. 1904 (Aquacou3j
EPA.200.'1,Aev.4A UlTiA, (Aque,:stjq)
SW-8 41$ SQU B (Agucomi
2W-946
LEAD
EPA 2P,0.7, ReN Ckl 904 fAqU9VLf,,)
FTIA 200.7. Rov. 4.4, 1 4)9e (AqusGus)
aYV-&416 EU10 0 (Aqtpoourn
V04413 w; on [Aq l-(!CkkNj
EPA 24MS ROY 5A. 19N JALIPM1.10
Cr No ITI b P1
621:
111%Nctive Date:
1.11?2017
Expimhoa Mato.
12;SV20,17
D.-Of,LP',
-12 J'2 0 17
n;-,lm1Anru-o1rt,5 PfNfuff. Ulu cf a3pray*d rmftdOvigr', p;ir.1 ,;F.tjsteq0fy P��WflfftfflM till Mgt hmhn4 ffirP,�r
t%;,..�Itorthm 15ANf_.W,2H01jW SSIOZI'111 ILl infmc4irmr

North. Carolina WaslewalcrIGTOLind water Labdr*k .. Cdrtificatian
Car[vfed Parameters List)Itg .
Lc1DNante: Surnmal E:nUironnmt4V-cchnaagie0., Inc,
Ce11111�af>i:Numbe_r
031
AdsJress- 331u'cvin trwi
Ell I'och.mDa:e:
V11817 .
- Cklyami, a Fells, 6H 4422'.�-
Expifatlan Oak)
1213it2il47
UaI001Lt!alAmenalnenC
'2f2:2037
The abnva maa 1aWtWC"v, r.Mir d,,:e M0, u•-� tequirermms of 15A NCAC �rr:;wna .r
ngrebrcenlre ! for o-r+m�rsvfoe'�m. a Ire p nmclors LS;s r. p IUw
_
CERTIMED:P41RAMETERS---
5'u^i•8+7G GU2+J f3;Ftgr e)rf d)
pRTRACET.k0LI:LJ?A DROCAR©CJN,r_,' -- -
SC11)IU1:A
MADEP, N1aV 2fJD4. 9?(:v, 4 1 IAqueous)
1°FA'201J 7, Rev. 4-4, 1y34.{AgI,U,lr sl
NQNHA.f.C)(;r-NA-,EV .fOLATILr. kUARIC5
51h.-I'4ti fi(mn 17 (ltauru :.^-.
S1ht 4A k%01:51; IAgjeeus)
STRON T EIM
P ES-pC ID ES. OfiGAh Or IaLn- PINE
CPR 200-7, Rev- 4.4, L 994 (Ag l lam u•_)
EP.A r303 'Arpj v u,g)
tV-8413 .ti D 10 D {Aqu.=.m m i
sip -845 E9811 E (k4 VEmus)
EPA 200Jf ,.Rey. 5 a- 139,; AgUeaus;•
PS}L YtGI:fLORIgA'FC I f('HEN'i LS IPCRsJ
SW-P46 R320 a (Acueaus}
EPA C•08
THAILLIUM
9VJ--3r$'a0R2 A 114qu5:a5ls)'
5PAM0.7. Rtiv 4.4.:U54 (Acueousl
PUrlrjVAIILE. CRGR,UIC$
84V-846 6111 D D (Amt-ous) ,
EPA 624 fAquenuy)
EPA 200 f5, Rev 5.•4, 1004"fAglleou�)
51N-8�6 6?¢p (3 dF,girrs�us}
S11V846 02+18 (Aqueaas}
iC}TI;L C?T�Gd NiC, Hr1LIDE,S .
Tim
SVJ-8469020 9 (Aqueou,)
110A2003 Cr-,V. 44, 1004 (Aque¢u,l
TPH IMESEj RANGE ORGAMCS
SW-84ri G010 D (Aqueousj '
SW446 8-V15 C (A jauous)
br7 NhCHUc'A
17'ttGASC][ IJeE FiAM1iC'E. ORGANICS.
' EPA, 200-1i, Raga .5.4. W94 {A4ueaus4
SW-.84688r5 C fpgLjerrls}.
SM46 6020 13 (Agi)i?.5u j '
.'DLAITILE PLI ROLI;UM IAY'DR-Q1DA.'qBONq
ZINC,
i-A10y;70
04, --Rev. 1:1 ' (n.quepids)
.
EPA 200.8. Rm !i, it. 19514 IAW"OUS)
sw-84r 6070 n (k1urnu:s)
0110AN(C
YOLP ORGANICS
A $(1z!.€i,11,E4 E ORGANIC HAL 117FS •,
EPA 41350, Rou. C. '1997 04uuua}
SAGE INELITRAUACiO- ORGA:11C5.
EPA 625 iftieous}
E%N-846 8270 D (Aqueocts)
CKORINATED ACID I-ICRLIIGIOEE
."i1V-846 a I S1 A ri ,q dcnu: 4._
CH'LOAINATGL) P'4E'NOLICE
1hlS eErliGcatioi urrclu 45 rttscNtant:ed an acr,C{:;OtYI,� gl,tb'tyassrnrde 4tWrmn use ul 8ofrowLa'rteetursktln�y. am F9115ft1:43 y P t!orTmnceaq FVEhk*4t` LI;4sreltn.:ys s:e aut;err, yc,ll 4Jt3m3lGe� nn:ltur urcrllfa:etlonin• iRtrs�Yr-gas
a Frd rgtll', Irt 15r KICAC 21a 0237
O
CD LO
T— . 4-
0 O
M )`
1v CM
13 (1)
a.

North Carolina Wastewator/Gioundivaier Laboratory Certification
Certified Parameters Utft;1jq, .
LotsNmnt�n; SUM"14,Envsmnmental7ech6o!o9ica.Inc.
;i:ar{(Ilcat0Nufmlrer.; [i34
flfJJf[+85:, 33ra.Win; Streft
(/1 J! fr
v d!l
E(fecti.eCdate' iit:2fjii.
= tiu)nhaf�a 1=;rls, 0H a4«3•
-
Gxp'laare•n Date 12'31f^Ai.i
Dato of Last Arrm.14ltdil 1114J20U6
Thu *,uve mm" lowntni r Idw,q duly earl 11w ruclur3frtunL' of 15A r•1C4,` -,H
09W, r, mumvimrvfrd 16rtn0111m9uurcr,2n: al the p.)rEgMvip lzl6a ttQW.
•YC-1311F!E0 P,R_J4latET_E•TiS, '• __
—._
'
INORGANIC
SILICA--
fSOi}-
EPA 2011:7, PC%'. 4.4 1094 (Aqueou i1'
Sh1521❑ o 2001 j quco,.ls)
tivd=tSdfi'E010 iJ fFuqueoua}
ChELOKII�E
SULFATE
54V 046''305r A. (rtqun6ua)
EPA 30ti.u, Ftay. 7 1, 1005taqueats}
COD
M)IJ-045906E A (flgtlems+
fihJl � t lt3 (-109' {+�gvoau�t
SULFIDE
h'I tJORIDE
',^1-,nri, i13 (Agaieousl.
f PA 3Dp.t1, Rev. 2.1, i99 i (ACu?ctrsy
METAL
..
S:1-B46 R415BA p:gwrolrsy
5'CiF MEALS
ItdCJRf NIA PHEtiOLS -
SW-W 1311 !A.7uenuS}
(0
Lid '
Elh42D,1.Rev 19YF1fJ.ruen�s}
'\LLIN,11NUa1 -
4—
NITROGEN, NPPATr
;
,EF'A .2�6.1 t'uv: r.4 1914 (Agr,�nc }
4-
O
- O
EPA 30ITS}. Rf:v. 21, 19'-3 tAquontpsF
$W-OaGGO =0,0 {kq 4csj
d
M
MV-A 446:SDs;r A (A.queo1:5)
EPA.200A. l.w. 5.4. 1994.{Aqueoui j
0)
N
tJITi@bGEM,1VITR?TE
SVIr3d&6:12LI'f!btqueous'r
EPA 300.0. F?ev 2 1 1995 (Aqueous)
AN'7rr'JfOtdYCZ
SM46 905C A• ;Pfcrocous)
[-:P& 20C.7. Rev. 4.4. 1.3Q4 {r%Wuousl
V ITRp(, R N • NC13 + N 02
SW-34B 0010 C jAcluL`ou:.1
kPA MA Row. 2.1, L0.3 lAtiur:ausI
E-AL 206.7. Rev, 5 4. 1004 tAgtc=:gtrB+
W&B46_05C A {Agiuobm')
N'IT4t0Gt:re, TUrA.L KJELDAHL
ARSENIC
5614500 Nurg D-1937,,y1a 456•r, NH3 D-1a97i{Tittucousl
EPA 20C.2, Rkv,.4,r,. Md. {Aqucoual
01L 8 GREASE
Sb1r a4U C(j10•D rAquaour)
EPA 1IjB414ev. L+' (Aqujcans.i
EPA. 20Q 3. Rey. 5 4 1919(Aquocm)
SW.s417i g071 B (Non-Aqueuus;
S04445 CR fi R rtku.?ousl
P1105 PHORUS, I t7I'f.L,;
EARLLJm
EPA200.".Rav 44,(-�Kj4)(fcuaa�ls}
CPA 20i7.7,'Reh.4'd. jssa;kgu?tttrs
_ t^r•R4R �i010 D(Aqucous} -
- S11J-L+:O aJ!tl n tAcnnr�usl
-
RESIDUE. DISS7_VLM Ian f.-
EPh 240.8. Rev. 5A. 1.194 (Arjue,.nuq
_
Mv12ii40 G-1497 (Aq e.rnitcj
SV`W84a -M20 B (Aqurnu5j
RESIDUF;. MWENDED
OCRYLLlUttivl
_
S540 IY-183T (Aqueous)
EPA?(�A.�',i. Row "A 19JA JA4uec.is)
RMPE.'"AME. TOTAL
V*845'61025 D.(Aqueou5)
SM 2540 11-107 Mciuoous?
GCl to V '
- Thin rr,A11COtar rvqqu:n rrtan': v.t� tl e• uc.err•,ialo q(jajry 9Esvf l'44- P'oJMM. 11V? fry r1t) !tNM rn[:!Rai^Ie3Y. t;d §�tfsrrdcry� pCl'plm�:n.,ri c,).i vnlaatai s.�rclP�4u LJJuktllries:nir. ; �� p^, LI'.il Cerlell�B° C-dlnr t1rr.1•r571r iG'I r9riaff3 pia
tr. �:Icelh:en 11—NGAC 211007 � �
.

N0111.1 Camlona Wastewater,'GretindWhter Laborakory Geriffication;
Cedified ParAnietem Lj.sjFng
Fib Wo 11111 it Enm7i'll.uOntal Tedmmjq!�b. Irr-.
Coffiricalp oil
3310 Win Stf vat
Effertive Yala: IM21317
C.Uy1hO-3a-F-0E.QH 442231-
Eipf vian Dale:
oaia 3 r U-,1 Ametidmeni: '114-TC IIJ
the abawa namcd hmngduy iit-. vie'euverreMs V 15A NCAC.;,H 11HIn. I'
... .... - — -----
roretyetcairm: ]or thri rrNsbujeMmt o9Nmpi3rmc.ta* Ii5r.e4 idCw
I'P& 200.8. Rev. 6.4, 1QU4 (Aqueous)
Q)q ucrus)
ry1Al3N;:j51Ljm
CA ' rlmelum
ETIA M7. P.m A.4, 1994 yAqocax)
FPA2003, Rev. 4 A. 111,19 (A-q u a 0 U--)
i 1MV-846. 601 U TJ (Acplvot,;)
14�, 6.j401j (A.,,
FIA 266.1. pr,v 9'1, 7fJY4 (Aqjjp0j?s)
EPA 2aO..7. Roy, 44,
S16-fizill cif'.20 B (Apenu!r.)
8110-04C 17A10 0 lArruwjp,,'
CALCIUM
rPAMO.iS, Rp.v. 5 . .4. 1004 fAqti6aus)
EPA'2DET 7. NFu 4.4. Mie, (mciucausl
S45141451102171 5 (AqtfWl Ug)
G�iMli C) tO 13 (ALzuedus)
CHROMIUM T07A L
:PA-24U. Rev. 3A 19R4 (A(pwr3n)
11"A.203.7. Rey. 4.4. 1994 (Aquamrg)
811L!7-04G 7470A lkwuatis)
S-W-846-9010 D (Aciucaus) -
EPA 1$�1 t (A417i"'ous)
EPA 200 0. Rev. SA. 1994 (Pquuuusj
,WJ, Z14 0 6020 B (A4p6o
EPA M0.7, Rfv.. 4A - 199e. (f%a:UcoL-.)
CORIAL7
SW44B.6010 D (kricious)
EPA 200.7. Rov. 4.4. f D" A (Aqve0w)
EPA.= $. NY, SA.104 (AqLvrml
SWIM (i 6010 D Vkqumolj'a�
W-840 6020 B fAqutxwa)
i.-PA 200 8 ROV S.A. 104 (Aawepm[
NICkEL
EPAM.S. ROY. 5A-.'1504 (Aque-imai
0311PEPt
FPA71XF7 Rev. 4.d:.-1Q94.4Aqut3du-.5
SMI-84 6 6,310 D (AQLjqoUS
MV, 4A. 1994 (AqUe0j,$:
EPA �00,3 Rev 5.4, cgiJ4 (Aqueous}EPA20Q.T.
SkIV-846'6010 D (AqLj6OvS)
S1V-H4fi 602013 jAqueats)
51LE NIUM
Fix) 14
RP.U. 5 4. 1994 (Aq uaott5j
EPA Z107 H4Cht.4.-q.1994(AqU(-OLkS)
. -
T),,)20 9 {MuLaoug 'j
4 C 6OIDD (AqUeOLISJ
I LY E, R
LEAD
EPA: 200.7: Rev 4.4. fM'& (Ariu,6003)
EpK200.7 Rev 44, 1994.(ftipman .)
3�-�--640 r.010'D (Aqueousl
SVII-04C; 6010 D (AE2.ieorjs) I
EPA nO.8 4;w. 5.4. 19,04 (Aquequs )
SW
SW-340 EON 13 (Njvcout.).'
SODIUM
EPA M-7, Rev. 4A. 19 91, (AqvvuLQ
EPA 200.7. Rev. 4 4, f-004 (Aqueous)
W4442 5 0 10 D,(Aq;i"tm)
Thi; ogThwijam 'rq"-T5,)a3h%-.anrc cenn A-003plAiL -4•Wijy rrc� wm. umn. ri AMMV.Mg 11T1I1rdLv-rr2j. RnO Olmladary portwmail'OVI ev6lamficn zm'nP'z:r-. L.1.uisImw--zm
=s ccn forIndr, &a 7. f5riniewliDft.
0
(0 to
V- 4-
4- 0
0
LO rA
c1r)
CU 0)
0- , M
CL

North Curulinit Wastewater/G o.undwat8l' La.boratorytoritri6fim
CarViffed Parameters Usting
1 6 K41ol ;u..mmit Envimnrnr I-LilTdrhn8log¢es, Irby
Cgrl;kDte Mumbr7: 031
Addwss: CBI val sift"oE
EffCGliva De1e. 5)1Q317
GUYntfb la Fa ia, OH 44e23-
EXpira@inn Dak; 12�1C3997
Date Of L-ls1Amortament: ttill 1;..0.1G
The zbmvn inrmd iswsmlort, nawnp duly Met lfu feyttiremrrlh nI IrxA I CM, 2114FJJII, jr. nar?oy'"s'lirled r9T 11lonio2suforem1 m trw P.'S!.lr:P_ICr! I,swo Move.
STR(JNTIUM
frES1 ICitJES.:ORGANOCI,11 CORINE
_ EPA 2U0.7 Rrv. 4 4 104 rgqueomlr
L'F� t3UB ;Aqueous}
5D+t aats•b919 D{Avueotis;•
sw-,841311433T Lf (AnLWOUS)
ESA 200.8, P.ev. 5.4, 1994 Ikgtaeoun;
POLle'GpIUt*NATECJ SIPHI:NYI 1 (FCBs)
SkV-840 6DZU U Y(ClusouS)
ePA 6G8.f,Aggeaus)
THALI IUrat -
$U1-646. S0.02-A (Aquootj6)
hhA 707, Re1.•a.n. 14 L34 tiAquiuL[8)
PURCir-An.jr- crosAmcs
SW-846, 80,1 10 (Aepoott5)
EP'A 624 tiAgtlgnusl
EPA 2„tI S. F11w 5 A. 1 yf1j4.(Aqucous)
�4�1; 5 .FS' 75Q'E (Arftlnnl:s]
$W-846 0920F3(Agm-raf:)
'DT�yCt�F2 ,gN1,.I1ALl*JES ,
TIN
S�'J�S48 99217 8 {At1tle�as)
EPA200.7 Rev 4.z t°J34 (Agijofu3)
1'f'II blEbEi.RAN:; F.ORGANICS
EW-846 4C10 D tAqueous)
SW Lf4G f50! t C. [Aqt c pus)
VA1JARlE1f.1
TP14 CASOLINt t?AMs,E, CRe NFCS
CPA 1.00.9. Rrv.5.1. i9cI4IAqueoris)
SN-4413,PU16,C Agy:eaus).
U..4.84#i G'7ff03{Atlucclu;)
LOOL'yTILE I'ETTICteilPAi1Yt31# )CRRBQ.V'a
ZWC _
J'AADEF, t tny.70t14, Ruv.1.1 fPAuenl:sr.
EPA 201) J3, 1tcv. 5.4. f 54)4 (Attuet:fIsl
SYV-046 n2DB (Aq,fCous)
WIM14.Ef 131-1 (Aqueetts)
U R ADSEA HLE.L) IW AN I C HALIDES
EPA 1G.^,7S,.hfft i. ;!397 dAgi:omjq)
f1A4 NEtJTF1.4LbyCIJ OIiL;a5741L`a
EPA-625 {A'ruea.EFj
SynJ.Rc58�Ttltl {Ar�Uf?t}US). '-
_
CH ORIMATEDACIDI-IrRltlr.InES
CHLORINATED PH E NOLIC 3
EPA V353. Rov. A. t I't'r fAqurnue:;.
EMACTIAULE PETROLFUb1 HYDROCARf ONF—,
MADEP, P.1sy �.004. (rev. 1 J dr;tttieouSS
NoNHALoac A7WVDIATILF.CJRUi11IPC5
5411.6g63t1:5C IAqueatts)
,
Thre oenrrca',.�n aNCAf. M OMIr_eol �n uraFfaMd a;�alilyuypur�nW LY[gfarty .la. cl ajr.^.rnov. lip. hbNaloW. mrd i.^etl9,fory perlornorecm owalaelien 5W7 ry'em Letr_r amevale
xa1 frr-h Ir5.15ly NCAC :Iq t?Rn7 -
saki -d W mif rGnal.ums lltltO c e �r.:rralrrn lcr in acb,'im;
O O
Lo
4—
O O
O O
O �
0- CZ
iL

North Carolina ft-itewaterlGroundwi.ter Laboratory Certificattan
c- 0 nif fed Plarhnn ct&m Lasting
Lao Name: SiAmmit ErivIranmental Techricloglas. Im.
Address: 321 a Win struj
Gi0hogg Falls, OH 44M:-
i
Expiiradon Dmze: P-GI 6
Date of Lasi-Amendmar.t. ITAV21)iG
Tnoaw,m n3'aled labdr',ijnry, hwkiq duly mell ff* recImemm.s of 1,9A JUAG 2111:066,
Is hereby milifikorl (fir ine rneasurencm cA Iho prarra'a r; fisrmw, Wad. -
CERTIFIED PARAMETERS
SMICA
BOO
EPA 200.7, Roe: 41A. -1994 fAqueous)
SM 5210 B-2001 (Aqutmus)
SlIV-846 6'0: a D fAqueous)
CHLORIDE
SULrA7E
SIM-1346 40515 A (Aqueou F)
rz_P.A 311G.0, Rev Z.t, I%M (Aclarnw)
rQD1
SN-840 9063 A N. vomm!)
S14 5220 C-1 e797 (Aqueon)
FL.UQRIDP
F-PA.30.0-0, Rev. Mqumovs)
METAL
SW-1948 U066 A (A.q jemml
TCLPMETAtS
INOF4CANIC PHENOLS
W-046 1311 (Aqueous)'
CPA 420.1, Rev- 197$ (Aqueous)
ALIUMNUM -
NITROGEN, NITWE
CPA 2613-7. Rev. 4-4. 1-994 1,Aqumms)
CPA wo,'o, Rev 2.1. 1-993.(Aqueousl
S1vm545 60-10 D (Pwpeous)
SIALFA16 91056 A (Aqueous)
EPA 26b..s. Rpv J5.4, t994 (Aqueous)
NITROGEN, Mrl RITE
SW;246*6020.8
EPA-300.Ul ROV.2.1, 1993 (,� qucatjts)
ANT11MONY,
SlAt,846 0056 A (Aqu4uc-jss
E-PA 290.7, Rev. 4-4.
H.,M,oc,r--N M60, 4- NO2'
SVV1 846'.15010 U (Aquewn)
)EPA 100 0, Rev, 2.T 1-99.3:,Aqweous)
EPA 103.8; R.Y. 5. 4, 104 Aqueous)
SW-L'4r; R056 A (Aqueous)
W-13443 ,0020 B (Aqueous)
KIT-%0-3FN, 707AL KJELDAHL
ARSENIC
Shf, 46W Norg 8-191177 (W 4500 N113 D-1 997) (Aqjecqsj
EFA-2020. Rev 4. 1. 1.094 (AqUIEOUS)
OIL & GREAG5
SW�8413 601 � D (Aqwous)
EPA 1654 Re V. B (AqUenO
:EPA Z00,13 Rov. 5. 4, I.QU" (Aqueous}.
­M446 91" .71 B (Non-Aqticou5,L
SW-84 tV:9r.2-3 B (AquM)
PHOSPI-fMIS, TOTAL
BARIUM -
EPA 'A10.7, Rev 4.4 (1154301) (Aqueous)
EPA 2007, Rev. 4 4. IM (Aquecus)
SVIT64C 6010 D0'4WN3us)
SW-84Qvrw01 0 D (Aqueous)
M-SIDUE, DISSOL%UE) i,90 it
EPA 2018, RF,.v 5.4. 1894 (Kqyecws)
SM 2E40 C-19.97 (Aqueous)
RESMUE, -SUSPPINDED
BEWYLUM
SM. 25ito D-1 S9.7 (P.q uea*j)
EPA:200-18. HeY. 5-4,1994 (Aqueous , I.
RESIQUF, I UTAL
cAU -846 r)(20 13 �Ac4pays)
8M 2540 9-110T (Aqueous]
aORON
Pits certhc2eior) mc%uns n1almigant.,6.- uralflalry ["tab? clus1tY 3s'-wrtfre pKgNm, we *r;--prwmJ
as set lexth in itwk MAC 2H CE0 7
methcdolday.�mnd *Dftfrctory ppf1mirencu-m. evalmit'amssmplM 1A=x-qr-"r' &--stlbjjec'.-to c,vJ paltSfin, and -'or deumlicarion foria.'rickm
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North Carolina WastmaterlGr©unduvater Laboratory Certification
CelVUf d Parameters' Listing
Laib Noma:uwttrtrllt Env.ilnniti+yll(�0 Terhnnrrx�les, Inc.
Add 2ZiTO Win Streel
CultataD:t Fa115.OR 44JZ.
Th¢ stove uamrrt labunb:ry, , hauiny.kIUIy rnuttiresequiremearc of 16A NCAC M 0340, la hereoy centfied for vIQ rrV VUr=anr of :ae fP-trnet.r, lis:vd glow
CEPTIFIED FARAMETERS
EPA'200.8. Rev. 5.4, t994 filque117114s)
S4N"-84G601,'� D i,Aqueuus}
8101-1546 6620 8.(Acluecrvs)
MA0A'ESMI
'CADDARJI-A
EF'A 200.1, Rev. 4 4. 1 -z94,(Fi�ztepus}
EPA 2fiIG.7, Rev. 4.4, 19S4 (Aquoousl
%W-84C, 8310 D {?Aqueous)
SIN-846 5010 D (AgtjeoU5)
MANGANeSE
EPA 200.9, Fee. 5.4, 19.94 (Aqueous)
EPA'200.7, Rev. 4.., , i994 IAquacus)
5110-345 MOB (Aqueousl
SVU-0366010 D (Agrjeaus)
CALCIUM
01A 200.8, P,ev: 5•.4. i'9N i.Aqueous)
EPA Ei10,7. Rev.'4-4. 9S9d iArJw)us)
SVV-840 W20 13'(Aquamm)
SVa'-i14G_eO'C D (Agwaus)
MERCURY
OFR7titlU411'0TAL
EfiA.2451, rev, 3.0. 109f (Aqueous)
EPA 200.7. Mfiv. 44% 1994 (Aquaousal
.31U.046 T470.A'(A;queoue)
S%W1466010 D tAquepus)
li 3
FPA 1#31 ts }
EPA (Aqugor
EPA 200.8. ROV, 5.4, 144'(O\quaoU,.)
G,1t1t
%V-8415$0209 fAqueotus)
EPA 204.7; Rau..4 �4,1994 A(poob 35}
COBALT
S:V;0-?4G 6D10 D (aqueous)
EPA 200.7. Rev. 4.4 1994 (.+iquepus)
VA 200.8, Aev, 5.4.1;3 4.(Aqueous)
51irq,U46,30TO D Oqueaus)
Strbr-W 9D2013(AquRDusl
EPA. 20D.8. Rei 5.4. 1994 (Agttenits)
NICKEL
MV-840 662 EL (Aqueous)
EPA 2 MR, ReV. 5-4,. 199A (Aqu�oVs)
CLIPPER
SW-kg46 60120B.(A•qudoIts)
EPA 2D0.7, 110, 4.4, 1994 (Aqueous)
RQTriSSiUPh
MV4734G 6L110 D (Aoueoui;)
CPA 200 7, Rev. 4.4'r 1994 (I%quaausl
EPA 200.8, Rev_ E4, 1994 (ftroaus)
tW-646 60U D (Aqueous)
SW-'846 W-21D S (Aqueous)
SELL=N[UM
IRON
EPf'r2 .8..Pev. 5.4, 1594.{44ueau+s}
EPA 2D0,7.Rev 4.4,1D94 (Aqueous)
SYf $�6 6C2. f3'(Awwousl '
S01-E46 601-3 D (Aquanits)
S I Llf¢R
LC,4D
FPA 200.7, Rev. 4.4, 1994 (Rqurs.usl
EPA POP 7, Rov. 4.4, 1094• (Aqueous)
M-&16"6010 D.(Aqueausj
SW-946a 9r010 DQAgrj galM)"
EIPA:200.8, R_v. 5:4, 1.994 fAquonus)
EPA,:201f.N, Rev 6.4,19:94 ftutour,l
SVV446:15020-B (A4augoual
VJV-846 6029 � (Aqueous)
SOMM
LITH1Ufu1
EPA•204,7, Rev. 4.4, 1'99d'(Aquem:5)
ERA 2007, Rev 4.4,1994(Arluenusl
.WV-44E 150.16D (Acuaous;
Getlifirate Kraher•
631 .
Cf€uclive bate.
11112G16
Ek0dr9:kiorg Gn;e:
12?3112Uiia
Detp-af Last.Arnordmerlt:
19f+172D1a
This orrli�cre;n req;ilres nammmeu r-,'FA accapta5{ grr�ire assurenee rw*2r rm, USe olappmve*9 nathcxiolor4x ana satt;fxrcrk Dar$mt a cn oualuahcrr c
�;rrn�xa5.. Lat�or�;e'r `�-.4orr :abcat9rl ?v0 Nr,ialti�y,md-or tlarPr:l6caCi;yn f x inJrzcxns
as set Ton?] III I sr, -AU 2FLx0047, -
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Certified Parameters-MMing
Lab -Name. Strrnrnft Enrir(irinle dtaa 1'ecilnnlrgies, Ing
Aw�Clrrys: 3s10 Win ~Street
GLryahoga Elks, 01•1' 44223-
7lbe above mmrn tamorarory, having euy mat I,to mg0ramerlc 4l 18A NGAC 2H 080Q, le hereby eeRtPe6 `r tf..c merlsurencr,l cf 1hr •par ,melees lislrid be'vN
•CERTIFIED AARAMITTEMS
STROWIUM
tk200.7; Rew. 4.4, 1994 .Agj;vous)
MV-846.6010 ID (Aquamug
(_PA 200,9. Ro,r. r,,.4, 1 W4 (Aau®t,us)
SVb'-546 6Z1211.110,weaus)
THALLIUM
EP.A200.7, Rev..4.4. Ty54;'Aqueous)
S4VV-94d 6010 D (ftrenus)
EPA 200.8, Rev, .5,4, 1 V�4 (Agrreous)
S
M-845 020 6 (AquQr;us)
TM
EPA M.7, Rev. 4 4. 1;391 (Aqueous
}
S W-846 WO b f.Anuems)
VANADIUM
EPA200.B. Rest 5.4,1994 {+k4m4uus)
ZW-846 6020? £. gl1nzatrs I
ZINC
F_lPA moz. Rev. 5-4, 1 � (Aqueous)
SW-846 E020 B (AgUC-Dug)
ORGANIC
TCLP DRrAy1CS
$Vf B+F61':51i1 (Aqueou;}
AUSORBABLE ORGANIC HALIDES
EPA,'1650. Rev. O. 19n7 (AjuCO,A&
BASE N'ELr AUACIrt, ¢_ r-tc.' ,NIQS
EPA 625 (Aqumausf
SW-L48 8270 O (AqU®0us}
CHLOR114ATED ACID HERBICIDES
•S J-Wi.848r A (Aqueous)
CHL,1R(N&Tr=D PHENOUG$
1;i'-A 1665, Irv. A. 1 K? (Aquasaus)
EXTRACTABLE PETROLEGJMHYDROCA62RONR
f5iADEP, May 21304. Riau - I {L1:Ctilapus1
N•10NNA,tOGFNATFD VC31 A ILE, ORGANICS
SVI-845 aol 5 C (Aqueous).
PIES'iTICfbm;'ORGAdtiJCC HLC1RI?JE
FRA',BM51Aiqueaus)
SW-84$ 898:1 a (Xgtrsou3)
POLYCi IFLoR1NATEd•131PHfflNV:S (Pd8d)
EP.A,608 (Agrleauz )
SVV-846.8082 A {,Aqugtrygy
PUIZGEABLE.'ORGANICS.
EPA 62.4 (Aqueous)
TOTAL GRGM,NIC, HALIDES
s1M1,r-8rte 90�0 B'(0.quo0ur)
TRH DIESELRANG;F— ORGASSIIC•S
SW-846 8016 G (4.k4uGbrls)
TPH GAS:OLINF-RANCE 6RCANICS
SVV-846 BOib C-tAqueous)
VOLATILE PETROLEUM H''DROCAPiBONS
IAA OEF?. May 20U, Rw. i .1 • (aquuuus)
.Cer;ifrcale!I+umb@f. '
fi3.9
Fffrntivp Data:
1/1120/6
voratfan Dale:
12V 411 ra 1 F
Date of LastAm•ndnieni:
W02016.
Iht6CerltTid.11ecnrCgrrin?anigintan{>P-GrrndCl@ptdblCgteli'YiESLUiRSC2propram, use crnhflh'Wo.tjrlAt1C,]OtOgr,31dP.31�9�t1UYjt" rfFrntanS4iY1BWAIW&J9�993Y1�it^E:, ti;Iidmtafesar£sub(rttOGV�rRnaltl]3rSiUrOrdeCv'rlern,�UYt�rJritzi7Cllt113
s :e1 IOrN 11 16k NOA,G 211 C�i]G'.
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k, A 'S
� . JA V 7' VIlit EP MA N
February 7, 2017
631
Ms. Meegarl Dougherty
bqurrlmit Environmental Technollogies, Inn
3310 Win Street
Cuyahoga Falls, OH 44223
Gut,ject NO VW11GW LC Sfxty-Day Fet'- ia� '
am or Method Decatficatfun Rocommendation,
Zinc — SPA 200,7' and SW-8413 6010 D
Dear Ms. Diqucherty:
The remedial Proficioncy Testing (PT) result(s) for the b�61dw Par'ameter Tv]athqd(.$) reporled by V . ou r
-
15boratory for the North Carolirl'a Wastewater! Groundwater Laboratory Cf-rtificalron (NC
. . t VArVIGW LC;
performance evaluation. wastwere unacceptable and a wifibe'.
rewrrlmeodod. The ray (jlts rep6rted and the true values as -they appeiar in our records are as folio- ws-
Slv.dy P�rarneter Method units Reported I True Accepta.."Ce 'Perfirmiance
Value Value
EPA-200-71 IL 600 496
SIAI-846 5010 D 42 Not &
0 9 2 0 1 FD C 1 FPA 200.71 11 90-i 6­10 Not Atceplable
SA-V16 601:0 D pg.'L
i'97v_ritten r-di-le,;t4-e Action Report (CARI for each unacceptable result will be required prior 45 reissuing ceriricaiian,
This is .to notify you that the Laboratory Carfifi. cation Branch of the North Carolina Division of Water
Resources, Water Sciermes Serilbn, is considering reconirne'ding a pa - n rameter methodfs.)
decertification to the Environmental Program Supervisor_ The recornmendAtion. concerns the' abo'V.e.
mentioned Violation(s). This is not a decertification,, it Is a'nciflfiaz tlon of our . intent to consider
decertification. You will be inforrtied in a separate communication if decertification
fication is issued.
Contact me imi-aOdiat ly at (919) 7,33-3958 ext 251 -if your records do not agree wKh ours or it you have
Todd Crawford
Technical As. Specialist'' Assistance & Complianed Specialist'
No VRJ111-3VV Laboratory C2ri ffication �rancli
ALIWOmerit
cc' Dana 8-ailerwhite. Jason Smith, roaster File
Lt,A;Uoii C711f.i- R.zxid, H'Vi C� `2E-iira
Page 10 of 16
Page 44 of 50

f
February 7, 2017
631
IN13. Meagan Doughedy
Summit Environmental Technologie
s, ine.
3310 VVin Street
Cuyahoga Falls, OH 44223
k c)), (" oc.) lit :,.
�OICIIEAI- S. Kl-GA-.%
Subject: NO VV%fV/GVV LC. SIXVIvDaliPairameter Method Decer-rificaffon Recommendation,
Selenium - EPA 200.7 and SW-846 601O D
Dear Us -
The remedial Pr Oficienny Testing NPT) result(s) for tha below ParaTneter Me'thad(s) reported fay yoLir
laboratory for the North Garolins Wasteviateri Grouridwa-er ' Laboratory Ceriffication'(MC VMJIGW LCjI
performaxice evalualion -wastwere; unacc'eptabla and a sixty-dU—parameler method decertification will be
recommended.. The results reported a5d the true wilues. as they appear in our record's are as foliuvvs:
Study Paramater P.Ole-N:id
WP16-3B EPA 200.7i
D92015C-1 EPA 20.0.71
SV%1-846 m o b
n-7rbcrIVA,A,-ion Report (CA
—f— — PLcIRA
units I value I �az-,;, I —-Rwge
pO& 1 520 1 442 F73776-503
P91 ] 47c
3813 '1 326-444
required prii)r zu reissu;.ng
'Performance
Not Acceptable
Not Acceptable
This is try notify you that the Laboratory Gertillioation Branch of the North Garolifna Division of Wat&
Resources, Water . Sciences Section, is considering recornin ending a . pbrarriet=r . r-h et h od f S)
decertification to -the. Environmental Program �3wpt,-Niso'r, Tho'recommiendolian concern-s the -above
rne.rittoned violation''). This is not a 'clecertification; it is. a notification 6f 6,Li:r intar'lt-*tO C01119ider
clecertificatton. Youwillbe inf6rafed in a separate cornmunication if decertification is issued.
Contact me 733�-3
atefy at (.91908.e
jmrrie�dj9 t. 251- if yourrecords do not agree %tqth Ours or;
questions., .1 . .) : . . X if you have
Afto,limutil
cc:, Dana SaROI%vQ% Jssoti Srilith, Maslei Fill: "3-1
Todd Craveford
Technical Assjstanc� & Compliance Specialist
Nr, VWIIG'W Laboratory f-aOificatI--*n Branch
branch
-carfific.
Page 11 of 16
Page 45 of 50

February 7, 2017
1
631
k1s. Meeban DouOherty
sudinIft Erivironm-enial TeMnologjes, [lic-
3310 Win Street
Cuyahoga Falls, OP 44223
ROY COOPER
Nt I C 1-1 EA L N K 1: 13 A N
J A Y 71 N-IN-1 E R. M A %,
Subject NO. VVYVIOW LC -Sixty -pay Pararnoter Methfod.06cortification Recommendation:
Niaei - EPA 200J and 3'W-846 6010 D
D- ear Me;. Doughefty-
The rem�edia'l Profid=ncy 'I'ssfing (PT) resuic(s).for the below Pararn�+,er Methud(s) reported :by your
laboraiorry for the North Carolina Wastew
. ateri Groundwater Laboratory Ca0fication (NC V-jVV/GW LC)
pe-iformance evaluation wasMem unacceptable and azjxty-dlj meter method decertification
6ar") , n 11}e
recommended, The results reported and ffie true values as they appear in our records are as follows:
F—Sludy Pararnqtei Mi5th(ld
LPA 200,77
SW-645 601 11 0
EPA200.7)
6010
'A MilLen
loci! .un3ccen
I .
Value
Vol,
Acceptance
Range
805-103 Not Acceptp.bje
1200-1520 NOA Acceptable
prial to r0issungmrtk-rcalior.
This is to YfOt'ify - YOLI that the La4oraiory Certification Branch of the' North Oprolina Division of Wat-er
R'v-,$C�urces, MateF sciences Secl.lbn, is considering recommending � patametir method(g)
decertdiodfidn tQ the Environmental Program Supervisor. The racbmm'enclaiian 6bnc,,e=­
M.'s th6 abqije
meAcn-d r violaflon(s). This is not a decertification; 't- is a notification of akir intent to consider
clecertiffcation. You will be informed in a separate con'unun-leation if decertlficat16n' is"I s*sued.
Contact mp Immediately it [phone] ext, 251 if your records do rio' It agree viiih curs or d you Ila-,/a
questions.
Todd *Cr.m% lord
Technical Assistance & Compliance Specialist
NC V'AtV!GW Labora'lory q.?rtificatknr) Branch
csx. Dana Satfervkila, Jason Smith, Maefer File MI
"later 5171arCV5 secdO4
NC WRLv:a[r1Gs.Ldezzl.riat:ura:argfigrj.I &brf Branc-ti,
j I Ja o! yr Imo. F;
2
nqwwalar-rL Purccs-hv
Page 12 of 16
Page 46 of 50

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Page 13 of 16
Page 47 of 50

Sf G-MA -A L PRICH, iTC)
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'ribmmm. 711-
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Dale.2u16-cin-1 u
Van-ad.uw,'vl 2
Zb3c. 7r I
Antimony,, Sh'!
1005 i 1-1:10521MML - Ut
'VLllulvsL;P 'rZ ji)XuL; -'blik:12-7--
VA y
AXWni-. As
1AW-2plillie Ana vti
jDic, OR.1 7
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Page 14 of 16
Page 48 of 50

de 11111116
fj., F '09, TNI Evaluation Final Gbimplete Re, ort.
09:201 6,C1 20
�p
A MiWTS COMpanq
5yq-lf6
Mooph Doughwri - EPA ID.,
Quality Maiiager FJR I A Customer Number
�14 MIMI Lgnv 7-bohnoi4iffiv-, Inr Aybngy. I n;
3M'o win St'.
Cuphop Palls'. OH44223
(r;,O) 253-8211
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Quattty Manager ERA,& OHOUS22
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3310 V�jfj 91.
CuYa tfoig--, Falls, OR 44223
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Summit Environmental Technologies, Inc.
3310 Win St.
E:1•€1'IROt46fENTALSEt liNODS G!_S: mr- Cuyahoga Falls, Ohio44223
Anatlfreel Uboratur/es TEL: [phone] FAX- [phone]
Website: hQ.-Mviviv.settekcom
March 15, 2017
Chad M. Hayes
Synagro
284 Boger.Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Dunn WTP
Dear Chad M. Hayes: Order No.: 17030215
Summit Environmental Technologies, Inc. received 1 sample(s) on 3/3/2017 for the
analyses presented in the following report.
There were no problems with the analytical events associated with .this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Alabama 41600, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho
OH00923, Illinois 200061, Indiana C-011-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland
339, Massachusetts M-OPH923, Minnesota 409711, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North
Dakota R-201, Obio Drinking Water 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon OH2O0001, Rhode Island LA000317, South Carolina 92016001,
Texas T104704466-11-5, Region 8 8TMS-L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581,
Washington C891, West Virginia 9957C
Page 1 of 32
Page 1 of 50

Summit Environmental Technologies, Inc. Case Narrative
suwarAIT,
3310. Win St.
EiWIRONMEWALTECPWOLBmEs;3rtc_ Cuyahoga Falls, Ohio44223 WO#: 17030215
hrr.gIy ral Laberatork s TEL: [phone] FAX. [phone]
Website: http:/hvivw.settek.com Date: 3/15/2017
CLIENT: Synagro
Project: Dunn WTP
WorkOrder Narrative:
17030215: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable fonns as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies,,Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not'certified."
The information contained in this analytical report is the sole property of Summit Environmental
} 'Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence QC Comments:
ccv 20ppb c0306/ 1096834: Analytical Comments for voc-MSTR npw(8260), Sample ccv 20ppb
c0306/, Batch ID R66502 : The VOC CCV (Batch R66502) exhibited slightly high (120.5%) recovery
for Method -Specified CCC Vinyl chloride; All samples were ND for Vinyl chloride. All other Method -
Specified CCCs and SPCCs exhibited control.
mb-25849 1098253: Analytical Comments for telp-svoc-cpest_tclp(8081), Sample mb-25849, Batch ID
25849 : The TCLP Pesticides Method Blank (Batch 25849) exhibited high recovery for Surrogate:
DCB; MB was ND for all analytes of interest.
lcs-25849 1098254: Analytical Comments for telp-svoc-cpest_telp(8081), Sample les-25849, Batch ID
25849 : The TCLP Pesticides LCS (Batch 25849) exhibited high recovery for Surrogate: DCB; All
Original
Page 2 of 32
Page 2 of 50

Summit Environmental Technologies, Inc. N
SUMMIT 3310Win St.
Case Narrative
MVIRONMENHALIMPNOLO-mcs; nq. Cuyahoga Falls, Ohio.44223 W0#: 17030215
Arrar ,tical Laharaiories TEL: [phone] FAX: [phone]
Website: http.1Avww.settek.com Date: 3/15/2017
CLIENT: Synagro
Project: Dunn WTP ;
other analytes of interest exhibited recoveries within acceptance limits. ,

f
Summit Environmental Technologies, In
Qualifiers and Acronyms
3310 Win,
INVIRONb1Eb15'A.LCuyahoga Falls, Ohio442� WO#: 17030215
Analyffoal Lzboratorfas TEL: [phone] FAX.- (330) 253-446
Date: 3/15/2017
Website: hQ.-1Avww.settekco.
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers,
U
The compound was analyzed for but was not detected.
J
The.reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H
The hold time for sample preparation and/or analysis was exceeded.
D
The result is reported from a dilution.
E
The result exceeded the linear range of the calibration or is estimated due to interference.
MC
The result is below the Minimum Compound Limit.
*
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in
Manual integration was used to determine the area response.
N
The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P
The second column confirmation exceeded 25% difference.
C
The result has been confirmed by GC/MS.
X
The result was not confirmed when GC/MS Analysis was performed.
B/MB+
The analyte was detected in the associated blank.
G
The ICB or CCB contained reportable amounts of analyte.
QC-/+
The CCV recovery failed low (-) or high (+).
R/QDR
The RPD was outside of accepted recovery limits.
QL-/+
The LCS or LCSD recovery failed low (-) or high (+).
QLR
The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+
The MS or MSD recovery failed low (-) or high (+):
QMR
The MS/MSD RPD was outside of accepted recovery limits.
QV-/+
The ICV recovery failed low (-) or high (+).
S
The spike result was outside of accepted recovery limits.
Z
Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected RL Reporting Limit
QC
Quality Control MDL Method Detection Limit
MB
Method Blank LOD Level of Detection
LCS
Laboratory Control Sample LOQ Level of Quantitation
LCSD
Laboratory Control Sample Duplicate PQL Practical Quantitation Limit
QCS
Quality Control Sample CRQL Contract Required Quantitation Limit
DUP
Duplicate PL Permit Limit
MS
Matrix Spike RegLvl Regulatory Limit
MSD
Matrix Spike Duplicate MCL Maximum Contamination Limit
RPD
Relative Percent Different MinCL Minimum Compound Limit
ICV
Initial Calibration Verification RA Reanalysis
ICB
Initial Calibration Blank RE Reextraction
CCV
Continuing Calibration Verification TIC Tentatively Identified Compound
CCB
Continuing Calibration Blank RT Retention Time
RLC
Reporting Limit Check CF Calibration Factor
DF
Dilution Factor RF Response Factor
This list of Qualifiers and Acronyms reflects the most. commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this.
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 4 of 32
Page 4 of 50

11,,
Summit Environmental Technologies, Inc.
Workorder
•
,
SU"KAI
3310 Win St.
Sample Summary
FeWIRONMENUAL TECPNOLaGIIES, INC.
!Cuyahoga Falls, Ohio 44223
TEL: [phone]-I.FAX.- [phone]
WO#: 17030215.
Website: http://www.settekcom
15-Mar-I 7
CLIENT:
Synagro
Project:
Dunn WTP
Lab Sample][D Client gample'ID Tag No Date Collected
Date Received Matrix
17030215-001
Dunn WTP
.3/2/2017 1:15:00 PM
3/3/2017 1:40:00 PM Sludge
Page 5 of 32
Page 5 of -50

MIT.
Summit.Environmental Technologies, Inc:.,
3310 Win St.
DATES REPORT
ENIVIl OW01GNTfaL TfCH?Julov� —5,
3KC, Cuyahoga Falls, Ohio44223
WO#: 17030215
r na.
sy f.cal LibPragrifios
TEL: [phone] FAX.- [phone]
Website: httD://www.settekcom
15 Mar-17
Client:
Synagro
Project:
Dunn WTP
Sample ID
Client Sample ID
Collection Date Matrix Test Name Leachate Date
Prep Date Analysis Date
17030215-OOIA . Dunn WTP
3/2/2017 1:15:00 PM Sludge Ignitability of Solids (SW-846: 1030)
3/8/2017 11:00:00 AM
pH (SW9045D)
3/10/2017 4:00:00 PM
Reactive Cyanide (9014/7.3.3.2)-Solid
3/6/2017 11:45:00 AM
Reactive Sulfide (9034)
3/6/2017 11:45:00 AM
SVOC 8270 TCLP BNA List 3/6/2017 5:29:57 PM
3/8/2017 8:30:00 AM 3/13/2017 4:10:00 PM
SVOC SW-846: 8081-TCLP Pesticide! 3/6/2017 5:29:57 PM
3/8/2017 7:00:00 AM 3/9/2017 4:42:00 PM
SVOC SW-846: 8151 Herbicides-TCL3/6/2017 5:29:57 PM
3/7/2017 10:30:00 AM 3/10/2017 10:59:00 PM
TCLP Mercury Analysis (1311/7470) 3/6/2017 5:29:57 PM
3/7/2017 11:00:00 AM 3/7/2017 6:28:00 PM
TCLP Metals Analysis (6010) 3/6/2017 5:29:57 PM
3/7/2017 9:50:48 AM 3/9/2017 10:09:47 AM
VOC by GC/MS (8260)-TCLP
3/7/2017 11:17:00 PM
Original
Page 6 of 32
Page 6 of 50

Summit
Environmental Technologies, Inc.msummlur 3310 Win St.
Analytical Report
i Fbt�180NR9EN'fkL TE�flEdraLCticS; v,tr.
Cuyahoga Falls, Ohio 44223
(base report)
Araryffosl Lsharaiurle.,
TEL: (330)
253-8211 FAX: [phone]
WO#: 17030215
Website: hhW:/Avivw:settek.com
Date Reported: 3/15/2017
CLIENT: Synagro
Tag Number:
Matrix: SLUDGE
Collection Date:
3/2/2017 1:15:00 PM
Lab ID: 17030215-061A
Project: Dunn WTP
Client Sample ID Dunn WTP.
Analyses Result
RL
Qual Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW7470A
SW7470A Analyst: ALJ
TCLP MERCURY ANALYSIS (131117470)
TCLP Mercury
ND
0.00200
mg/U
1
3/7/2017 6:28:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW6010C
SW3010A Analyst: VVK
TCLP METALS ANALYSIS (6010)
%
TCLP Arsenic(As)
ND
0.500
mg/L
1
3/9/2017 10:09:47 AM
TCLP Barium(Ba)
ND
5.00
mg/L
1
3/9/2017 10:09:47 AM
TCLP Cadmium(Cd)
ND
0.100
mg/L
.1
3/9/2017 10:09:47 AM
— TCLP Chromium(Cr)
ND
0.200
mg/L
1
3/9/2017 10:09:47 AM
TCLP Lead(Pb)
ND
0.500
mg/L
1
3/9/2017 10:09:47 AM
TCLP Selenium(Se)
ND
0.500.
mg/L
1
3/9/2017 10:09:47 AM
TCLP Silver(Ag)
ND
0.500
mg/L
1.
3/9/2017 10:09:47 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270C
8W3510C Analyst: CxA
SVOC 8270 TCLP BNA LIST'
1,4-Dichlorobenzene
ND
0.0800
mg/L
2
3/13/201:7 4:10:00 PM
2,4,5-Trichlorophenol
ND
0.200
mg/L
2
3/13/2017 4:10:00 PM
2,4,6-Trichlorophenol
ND
0.200
mg/L
2
3/13/2017 4:10:00 PM
2,4-Dinitrotoluehe
ND
0.100
mg/L
2
3/13/2017 4:10:00 PM
Cresols, Total
ND
4.00
mg/L
2
3/13/2017 4:10:00 PM
Hekachloro-1,3-butadiene
ND
0.100
mg/L
2'
3/13/2017 4:10:00 PM
Hei achlorobenzene
ND
0:100
mg/L
2
3/13/2017 4:10:00 PM
Hexachloroethane
ND
0.0800
-mg/L.
2
3/13/2017 4:10:00 PM.
Nitrobenzene
ND
0.0800
mg/L '
2
3/13/2017 4:10:00 PM
Pentachlorophenol
ND
0.200
mg/L
2
3/13/2017 4:10:00 PM
Pyridine
ND
0.200
mg/L
2
3/13/2017 4:10:00 PM
Surr: 2-Fluorophenol
65.7
10 - 109
%Rec
2
3/13/2017 4:10:00 PM
Surr: Phenol-d6
68.0
10 - 109
%Rec
2
3/13/2017 4:10:00 PM
Surr: Nitrobenzene-d5
72.3
19 -.120
%Rec
2
3/13/2017 4:10:00 PM
Surr: 2,4,6-Tribromophenol
82.6
10 - 120
%Rec
2
3/13/2017 4:10:00 PM
Surr: 2-Fluorobiphenyl
68.6
•22 - 117
%Rec
2
3/13/2017 4:10:00 PM
Surr: p-TerphenylA14
80.5
34- 116
%Rec
2
3/13/2017 4:10:00 PM
Qualifiers: * �
Value exceeds Maximum Contaminant Level.
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
M •
Manual Integration used to determine area response
i MC
Value is below. Minimum Compound Limit.
N
Tentatively identified compounds
V ND
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit Original
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 7 of 50

Summit Environmental Technologies,.lnc. Analytical Report
S U SAN" 13310 Win St.
r.ifVIROtdHtEN'tALTECHtxOL .JeS, INC. Cuyahoga Falls, Ohio 44223 (base report)
ArtztyFicat Labaraior'ies TEL: [phone] FAX: [phone] WO#: 17030215
Website: htto://lvwiv.settek.com Date Reported: 3/15/2017
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 3/2/2017 1:15:00 PM
Lab ID: 17030215-OOIA
Project: Dunn WTP
Client Sample ID Dunn WTP '
Analyses Result. RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA; PEST, HERB -SOLID
SVOC SW-846: 8081-TCLP PESTICIDES
Chlordane, total
ND
Toxaphene
ND
Endrin
ND
gamma-BHC
ND
Heptachlor
ND
Heptachlor epoxide
ND
Methoxychlor
ND
Surr: TCMX
54.5
I Surr: DCB
80.6
SW8681A SW3510C Analyst: JBN
0.0100
mg/L
1
3/9/2017 4:42:00 PM
0.0200
mg/L
1
3/9/2017 4:42:00 PM
0.00100
mg/L
1.
3/9/2017 4:42:00 PM
0.00100
mg/L
1
3/9/2017 4:42:00 PM
0.00100
mg/L
1
3/9/2017 4:42:00 PM
0.00100
mg/L
1
3/9/2017 4:42:00 PM
0.00100
d mg/L
1
.3/9/2017 4:42:00 PM
10 - 119
%Rec
1
3/9/2017 4:42:00 PM
10 - 119
%Rec
1
3/912017 4:42:00 PM
TCLP HERBICIDES ANALYSIS (SW846 1311/8151)
SVOC SW-846: 8161 HERBICIDES-TCLP
2,4-D ND 1.00
2,4,5-TP ND 0.500
Surr: DCAA 78.0 • 20 - 140
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
VOC BY GC/MS (8260)-TCLP -
1,1-Dichloroethene
ND
1,2-Dichloroethane
ND
MEK
ND
Benzene
ND
Carbon tetrachloride
'ND
Chlorobenzene
ND
Chloroform
ND
Tetrachloroethene
ND
Trichloroethene
ND
Vinyl chloride
ND
Surr: 4-Bromofluorobenzene
97.1
Surr: Dibromofluoromethane
97.0
Surr: Toluene-d8
101
SW8151A SW8151A Analyst: JBN
mg/L 1 3/10/2017 10:59:00 PM
mg/L 1 3/10/2017 10:59:00 PM
%Rec 1 3/10/2017 10:59:00 PM
SW8260B
Analyst: MES
0.100
mg/L
1
3/7/2017 11:17:00 PM
0.100
mg/L
1 .
3/7/2017 11:17:00 PM
2.00
mg/L
1
3/7/2017 11:17:00 PM
0.100
mg/L
1.
3/7/2017 11:17:00 PM
0.100
mg/L
1
3/7/2017 11:17:00 PM
0.100
mg/L
1
3/7/201711:17:00 PM
0.100
mg/L
1
3/7/2017 11:17:00 PM
0.100
mg/L
1
3/7/2017 11:17:00 PM
0.100
mg/L
1
3/7/2017 11:17:00 PM
0.200
QC+ mg/L
1
3/7/2017 11:17:00 PM
70 - 130
%Rec
1
3/7/2017 11.:17:00 PM •
70 - 130
%Rec
1
3/7/2017 11:17:00 PM
70 - 130
%Rec
1
3/7/2017 11:17:00 PM
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit `
P Second column confirmation exceeds
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N . Tentatively identified compounds
O RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 8 of 50

Summit Environmental Technologies, Inc.
3310Win St.
RWIROhIMEh'I't�.L SECtttdrjLocic's; t^tc. Cuyahoga Falls, Ohio 44223
t3rra;lrt;cal Lahpraiotie& TEL: [phone] FAX. • [phone]
Website: htto://ivivw.settek.com
Analytical Report
(base report)
WO#: 17030215
Date Reported: 3/15/2017
CLIENT: Synagro
Tag Number:
Matrix: SLUDGE
Collection Date:
3/2/2017.1:15:00 PM
Lab ID: 17030215-OOIA
Project: Dunn WTP
Client Sample ID Dunn WTP
Analyses Result
RL Qual Units
DF Date Analyzed
RCI
SW9014
Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive ND
0.500 mg/Kg
1 3/6/2017 11:45:00 AM
IGNITABILITY OF SOLIDS (SW-846: 1030)
SW1030
Analyst: RMT
Ignitability Non-flammable.
1 3/8/2017 11:00:00 AM
RCI
SW9045D
Analyst: DHC
/ PH (SW9046D)
pH 5.8
s.u.@i9.6C
1 3/10/20174:00:00 PM
RCI
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)
Sulfide, Reactive ND
25.0 mg/Kg
1 3/6/2017 11:45:00 AM
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
P Second column confirmation exceeds
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
O RSD is greater than RSDlimit
PL'' Permit Limit Original
RL Reporting Detection Limit
Page 9 of 50

Summit Environmental Technologies,Inc. QC SUMMARY REPORT.
3310 Win SStt. ,
LNVIcE)TRLINIALI ;HWULU-M S,ANC. Cuyahoga Falls, Ohio44223 WO#: 17030215
A.191yRical LaboratofieB TEL: [phone] FAX.•.[phone]
Website: http.-Mvww.sette%com IS Mar-17
Client: Synagro
Project: Dunn WTP BatchID: 25824
Sample ID MB-25824
SampType: MBLK
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 3/7/2017
RunNo: 66446
client ID: PBW
Batch ID: 25824
TestNo: SW6010C SW3010A
Analysis Date: 3/7/2017
SegNo: 1096699
4nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighL]mit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
ND
0.500"
TCLP Barium(Ba)"
ND
5.00
TCLP Cadmium(Cd)
ND
0.100
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pb)
ND
0.500
TCLP Selenium(Se)
ND.-
0.500
TCLP Silver(Ag)
ND
0.500
Sample ID LCS-25824
SampType: LCS
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 3/7/2017
RunNo: 66446
;lient ID: LCSW
Batch ID: 25824
TestNo: SW6010C SW3010A -
Analysis Date: 3/7/2017
SegNo: 1096700
analyte .
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
TCLP Arsenic(As)
1.98
0.500
2.000
0
99.0
80
120
TCLP Barium(Ba)
ND
5.00
2.000
0
102
80
120
TCLP Cadmium(Cd)
1.99
0.100
2.000
0
99.6
80
120
TCLP Chromium(Cr)
2.01 "
0.200
2.000
0
100
80
120
TCLP Lead(Pb)
2.00
0.500
2.000
0
99.8• .
80
120
TCLP Selenium(Se)
1.99
0.500
2.000
0
99.7
80
120
TCLP Silver(Ag)
1.01
0.500
1.000
0
101
80
120
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 10 of 32
Page 10 of 50

a Summit Environmental Technologies, Inc. QC SUMMARY REPORT
Sunni 1T 3310 Win St.
trAlItKUTAMUN 1AL I1-.4;HNUWG1h5, 1KC. Cuyahoga Falls, Ohio 44223 WO#: 17030215
ArariVfl:caf Laboyptoriou TEL: [phone] FAX.- [phone]
Website: hap.-Mvivw.settelccom 15 Mar-17
Client: Synagro
Project: Dunn WTP BatchlD: 25839
Sample ID MB-25839
SampType: MBLK
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 3/7/2017
RunNo: 66490
Client ID: PBW
Batch ID: 25839
TestNo: SW7470A SW7470A
Analysis Date: 3/7/2017
SegNo: 1096547
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury ND 0.00200
Sample ID LCS-25839
SampType: LCS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 3/7/2017
RunNo: 66490
Client ID: LCSW
Batch ID: 25839
TestNo: SW7470A SW7470A
Analysis Date: 3/7/2017
SegNo: 1096548
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00411 0.00200 0.00400 0 103 80 120
Sample ID 17021496-008AMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 3/7/2017
RunNo: 66490
Client ID: BatchQC
Batch ID: 25839
TestNo: SW7470A SW7470A
Analysis Date: 3/7/2017
SegNo: 1096551
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00416 0.00200 0.00400 0 104 75 125
Sample ID 17021496-008AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 3/7/2017
Run No: 66490
Client ID: BatchQC
Batch ID: 25839
TestNo: SW7470A - SW7470A
Analysis Date: 3/7/2017
SegNo: 1096552
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00417 0.00200 0.00400 0 104 75 125 0.00416 0.240 ' 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P ; Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 11 of 32
Page 11 of 50

l et
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
m
LMN1HUNroll. NIAI.ua:��tal0LrJG11;s,W.C.
A'lnaly f� al Lagoa �turfes
Cuyahoga Falls, Ohio44223
TEL: [phone] FAX.- [phone]
WO#: -215
Website: http://www.settek.con:
I5-Ma
Alar-17
Client:
Synagro
-
Project:
Dunn WTP
BatchID: 25839
Sample ID 17021496-008AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 3/7/2017
RunNo: 66490
Client ID: BatchQC
Batch ID: •25839
TestNo: SW7470A SW7470A
Analysis Date: 3/7/2017
SegNo: 1096552
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Hight-imit RPD Ref Val
- %RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above-quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine Original
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 12 of 32
Page 12 of 50

r�
�
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
_
teNNIcVINT.lr:NIA[.o�t:�a-Gr,NWG1:a,IN..
Cuyahoga Falls, Ohio44223
WO#: 17030215
,+t.7aiw2i:cr�i LaTbc�P�taai�ia�
TEL: [phone] FAX.- [phone]
,
Website: hap.-Mvww.settekconr
IS Mar-17 .
Client:
Synagro
Project:
Dunn WTP-
BatchID: 25848
Sample ID mb-25848
SampType: mblk
-TestCode: tclp-svoc-her Units: mg/L
Prep Date: 3/7/2017
RunNo: 66643
Client ID: PBW
Batch ID: 25848
TestNo: SW8151A SW8151A
Analysis Date: 3/10/2017
SegNo: 1099064
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit ' HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D -ND 1.00 0 0
2,4,5-TP ND 0.500 0 0
Surr: DCAA 320 500.0 64.0 ' 20 140.
Sample ID les-25848
SampType: les
'TestCode: telp-svoc-her Units: mg/L
Prep Date:, 3/7/2017
RunNo: 66643
Client ID: LCSW
Batch ID: 25848
TestNo: SW8151A SW8151A
Analysis Date: 3/10/2017
SegNo: 1099065
Analyte
Result
PQL SPK value- SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
ND
1.00 0.500
0 -80.3
62.6.
125
2,4,5-TP
ND .
0.500 0.500-
0 79.6
-52.5
-128
Surr: DCAA
430
500.0
86.0
20
140
Sample ID 17630217-001ams
SampType: ins
TestCode: tclp-svoc-her Units: mg/L
Prep Date: 3/7/2017
RunNo: 66643
Client ID: BatchQC
Batch ID: 25848
TestNo: SW8151A SW8161A
Analysis Date: 3/10/2017
SegNo: 1099066
Analyte
Result'
PQL ,. SPK value SPK•Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
ND 1.00'
0.500' 0 80.0 37
105
2,4,5-TP
ND 0.500
0.500 0 78.9 - 38
106
Surr: DCAA
416
500.0 83.2 20
140
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H
MC
Holding times for preparation or analysis exceeded
Value is below Minimum Compound Limit.
J . Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
M
0
Manual Integration used to determine .
RSD is greater than RSDlimit Original
P
Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits Page 13 of 32
Page 13 of 50

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
surdraly 3310 Win St.
tNV1HVNro11.N LAI. o t:i:r WULrtGrtx, arew. Cuyahoga Falls, Ohio 44223
Anal final Labongrntrlo5 TEL: [phone] FAX. [phone] Wo#: 17030215
Website hQ.-11www.sette1c.con: 15 Mar-17
Client: Synagro
Project: Dunn WTP BatchID: 25848
Sample ID 17030217-001amsd
SampType: msd
TestCode: telp-svoc-her Units: mg/L
Prep Date: 3/7/2017
RunNo: 66643
Client ID: BatchQC
Batch ID: 25848
TestNo: SW8151A SW8151A
Analysis Date: 3/10/2017
SegNo: 1099067
Analyte
Result
PQL SPK value, SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDUrnit Qual
2,4-D ND
2,4,5-TP ND
Surr: DCAA- 393
1.00
0.500
Qualifiers: Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
0.500 0 75.9 37 105 0 0 30
0.500 0- 74.7 38 106 0 0 30
500.0 78.6 20 140 0
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit Original
R RPD outside accepted recovery limits Page 14 of 32
Page 14 of 50

Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
L-MVISVINrnr N IAI. I hCH acAs OILS, JKC.
AknaiylI.�P L'sbP ,qtD ieu
- Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
WO#: 17030215
Website: http://rvwiv.settelcconi//wwiv.settelcconi
15-Mat'-17
Client:
Synagro
Project:
Dunn WTP
BatchlD: 25849
Sample ID mb-25849
SampType: mblk
TestCode: tclp-svoc-cpe Units: mg/L
Prep Date: 3/8/2017
RunNo: 66588
Client ID: PBW
Batch ID: 25849
TestNo: SW8081A SW3510C
Analysis Date: 3/9/2017
SegNo: 1098253
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD. RPDLimit Qual
Chlordane, total
ND
0.00500
Toxaphene
ND
0.0100
Endrin
ND
0.000500
gamma=BHC
ND
0.000500
Heptachlor
ND
0.000500
Heptachlor epoxide
ND
0.000500
Methoxychlor
ND
0.000500 d
Surr: TCMX
8.23
10.00 82.3 10 119
Surr: DCB
11.9
10.00. 119 10 119 S
Sample ID Ics-25849-
SampType: Ics
TestCode: tclp-svoc-dpe Units: mg/L
Prep Date: 3/8/2017
RunNo: 66588
Client ID: LCSW
Batch ID: 25849
TestNo: SW8081A SW3510C
Analysis Date: 3/9/2017
SegNo: 1098264
Analyte
Result -
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
0.00600 0.000500
0.00500 0 120
20
157
gamma-BHC
0.00426 0.000500.
0.00500 0- 85.3
22
137
Heptachlor
0.00553 0.000500
0.00600 0 111
24
121
Heptachlor epoxide
0.00565 0.000500
0.00500 0- 113
27
152
'
Methoxychlor
0.00608 0.000500
0.00500 0 122.
10
199
Surr: TCMX
10.5
10.00 105
10
119.
Surr: DCB
14.1
10.00 141
10
119
S
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M
Manual Integration used to determine
Original
MC
Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
0
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits
Page 15 of 32
Page 15 of 50

r
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
trevlxr. Nto1UNI-Al-17apidaULSJ�i1�S;a�c. Cuyahoga Falls, Ohio44223 WO#: 17030215.
A1na;yllaaf tabongfo io5z TEL: [phone] FAX.- [phone]
Website: httn://wivw.sette1acom 15 Mar-17
Client: Synagro
Project: Dunn WTP BatchID: 25849
Sample ID 17030215-001ams
SampType: ms
TestCode: tclp-svoc-cpe Units: mg/L
Prep Date: 3/8/2017
RunNo: 66588
Client ID: Dunn WTP
Batch ID: 25849
TestNo: SW8081A SW3510C
Analysis Date: 3/9/2017
SegNo: 1098255
-Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit - RPD Ref Val
%RPD RPDLimit - Qual
Endrn
0.0105
0.00100
0.0100
0
105
20
157
gamma-BHC
0.00712
0.00100
0.0100
0
71.2
-22
137
Heptachlor
0.00878
0.00100
0.0100
0
87.8
24
121
Heptachlor epoxide
0.00969
0.00100
0.0100
0
96.9
27
152
Methoxychlor
0.0117
0.60100
0.0100
0
117
10
199'
Surr: TCMX
12.0
20.'00
60.0
10
119
Surr: DCB
22.3
20.00
112
10
119
Sample ID 17030215-001amsd
SampType: msd
TestCode: telp-svoc-cpe Units: mg/L
Prep Date: 3/8/2017
RunNo: 66588
Client ID: Dunn WTP
Batch ID: 25849
TestNo:•SW8081A SW3510C
Analysis Date: 3/9/2017
SegNo: 1098256
Analyte
Result
PQL SPK value SPK Ref Val.
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
0.00861
0.00100
0.0100
0
89.1
20
157
0.0105
16.7
30
gamma-BHC
0.00672
0.00100
0.0100
0
67.2
22
137
0.00712
5.78
30
Heptachlor
0.00825
0.00100
0.0100
0
82.5
24
121
0.00878
6.20
30
Heptachlor epoxide
0.00868
0.00100
0.0100
0
86.8
27
152
0.00969'
10.9
30
Methoxychlor
0.00961
0.00100
0.0100
0
96.1
10
199
0.0117
19.9
30
Surr: TCMX
12.4
-
20.00
61.8
10
119
0
Surr: DCB
16.9
20.00
84.5
10
119
0
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 16 of 32
Page 16 of 50

Sum,
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
tR%'1HVT-Jr.114NIAL I1.t;W4ULrJUR:'.i:, Irtc.
Cuyahoga Falls, Ohio44223
WO#: 17030215
_
.ekrt�tRy�tf;rxf Cra•kerp�rtiarlt?5
TEL: [phone] FAX. [phone]
Website: hup.-Ilwww.settek.conz
15 Mar-17
Client:
Synagro
Project:
Dunn WTP
BatchID: 25878
Sample ID MB-25878
SampType: MBLK
TestCode: SVOC-BNA T Units: mg1L
Prep Date: 3/8/2017
RunNo: 66688
Client ID: PBW
Batch ID: 25878
TestNo: SW8270C SW3510C
Analysis Date: - 3/13/2017
SegNo: 1099749
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit , RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
ND
0.0200
2,4,5-Trichlorophenol
ND
0.0500
2,4,6-Trichlorophenol
ND
0.0500
2,4-Dinitrotoluene
ND
0.0100
Cresols, Total
ND
1.00
Hexachloro-1,3-butadiene
ND
0.00400
Hexachlorobenzene
ND
0.0100
Hexachloroethane
ND
0.0200
Nitrobenzene
ND
0.0200
Pentachlorophenol
ND
0.0500
Pyridine
ND
0.0500
Surr: 2-Fluorophenol
0.335
Surr: Phenol-d6
0.343
Surr: Nitrobenzene-d5
: 0.376
Surr: 2,4,6-Tribromophenol
0.457
Surr: 2-Fluorobiphenyl_
0.350
Surr: p-Terphenyl-d14-
0.436
0.5000
67.0
10
109
0.5000
68.6
10
109
0.5000
75.3
19
120
0.5000
91.4
10
120
0.5000
70.0
22
117
0.5000
87.2
34
116
Sample ID LCS-25878
SampType: LCS
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 3/8/2017
RunNo: 66688
Client ID: LCSW
Batch ID: 25878
TestNo: SW8270C SW3510C
Analysis Date: 3/13/2017
SegNo:- 1099750
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits , Page 17 of 32
Page 17 of 50

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
summlir 3310 Win St.
tr HU'NTPUNIALI7aHWULUUR:'i7JKC. Cuyahoga Falls, Ohio44223 WO#: 17030215
AstdtyAaffi LHbo Wvriee TEL: [phone] FAX.- [phone]
Website: hgp.-1Avww.sette1c.com 15 Mar-17
Client: Synagro
Project: Dunn WTP BatchID: -25878
Sample ID LCS-25878
SampType: LCS
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 3/8/2017
RunNo: 66688
client ID: LCSW
Batch ID: 25878
TestNo: SW8270C SW3510C
Analysis Date: 3/13/2017
SegNo: 1099750
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.198,
0.0200
0.2000
0
99.0
19.1
126
2,4,5-Trichlorophenol
0.257
0.0500
0.2000
0
128
11.7
151
2,4,6-Trichlorophenol
0.254
0.0500
0.2000
0
127
12.4
150
2,4-Dinitrotoluene
0.279
0.0100
0.2000
0
140
20.6
140
Cresols, Total
ND
1.00
0.4000
0
119
10
129
Hexachloro-1,3-butadiene
0.202
0.00400
0.2000
0
101
14.7
137
Hexachlorobenzene
0.215
0.0100
0.2000
0
107
12
139
Hexachloroethane
0.214
0.0200
0.2000
0
107
14.8
132
Nitrobenzene
.0.233
0.0200
0.2000
0
116
15.6
138
Pentachlorophenol
0.201
0.0500
0.2000
0
101
10
156
Pyridine
0.0705
0.0500
0.2000
0
35.3 .
10
126
Surr: 2-Fluorophenol
0.454
0.5000
90.7
10
147
Surr: Phenol-d6
0.464
0.5000
92.7
10
140
Surr: Nitrobenzene-d5
0.480
0.5000
95.9
10
169
Surr: 2,4,6-Tribromophenol
0.590
0.5000
118
10
185
Surr: 2-Fluorobiphenyl
0.442
0.5000
88.4
10
169
Surr: p-Terphenyl-d14
0.495
0.5000
99.0
10
179
Sample ID 17030030-001AMS
SampType: MS
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 3/8/2017
RunNo: 66688
Client ID: BatchQC
Batch ID: 25878
TestNo: SW8270C SW3510C
Analysis Date: 3/13/2017
SegNo: 1099752
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL . Permit Limit R RPD outside accepted recovery limits Page 18 of 32
Page 18 of 50

SunrnaitEnvironmental Technologies, Inc. QC SUMMARY REPORT
. 3310 Win St.
trA-1KU+Nr01hN[A[.. I#:UH?4CJLtbU1--S, lriC. Cuyahoga Falls, Ohio 44223 WO#: 17030215
ArtdyflcaP Lar +�rglorieF - TEL: [phone] FAX.- [phone]
Website: http://lvlvw.settelc.com 15 Mar-17
Client: Synagro
Proiect: Dunn WTP BatchlD: 25878
Sample ID 17030030-001AMS
SampType: MS
TestCode: SVOC-BNA T Units: mg/L
Prep Dater 3/8/2017
RunNo: 66688
Nent ID: BatchQC
Batch ID: 25878
TestNo: SW8270C SW3510C
Analysis Date: 3/13/2017
SegNo: 1099752
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.416
D.0800
0.4000
• 0
104
29
112
2,4,5-Trichlorophenol
0.501
0.200
0.4000
0
125
53
123
2,4,6-Trichlorophenol
0.497
0.200
0.4000
0
124
50
125
2,4-Dinitrotoluene
0.524
0.0400.
0.4000
0
131
57
128
Cresols, Total
ND
4.00
0.8000
0
119
20
125
Hexachloro-1,3-butadiene
0.393
0.0160
0.4000
0'
98.2
22
124
Hexachlorobenzene
0.416
0.0400
0.4000
0
104
53
125
Hexachloroethane
0.458
0.0800
0.4000
0
115
21
115
Nitrobenzene
0.478
0.0800
0.4000
0
120
45
121
Pentachlorophenol
0.441
0.200
0.4000
0
110
35
138
Pyridine
ND
0.200
0.4000
0
21.3
10
126
Surr: 2-Fluorophenol
0.841
1.000
84.1
10
147
Surr: Phenol-d6
0.856
1.000
85.6
10
140
Surr: Nitrobenzene-d5
0.917
1.000
91.7
10
169
Surr: 2,4,6-Tribromophenol
1.04
1.000
104
10
185
Surr: 2-Fluorobiphenyl
0.806
1.000
80.6
10
169
Surr: p-Terphenyl-d14
0.919
1,000.
91.9
10
179
S
S
mQMR
Sample ID 17030030-001AMSD
SampType: MSD
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 3/8/2017
RunNo: 66688
Client ID: BatchQC
Batch ID: 25878
TestNo: SW8270C SW3510C
Analysis Date: 311312017
SegNo: 1099753
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: '� Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound. Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 19 of 32
Page 19 of 50

_
v
Sunnnit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
t,-VOIHlIN51N,N'IA[,Ih4;HNQL4i91!:S,JMC.
Cuyahoga Falls, Ohio44223
WO#: 17030215
AnzrSl.R of Latlprotpriog
TEL: [phone] FAX.- [phone]
Website: http:/11vivw.sette1ccom
15-Mar-17
Client:
Synagro
Project:
Dunn WTP
BatchID: 25878
Sample ID 17030030-001AMSD
SampType: MSD
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 3/8/2017
RunNo: 66688
Client ID: BatchQC
Batch ID: 25878
TestNo: SW8270C SW3510C
Analysis Date: 3/13/2017
SegNo: 1099753
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobehzene
0.368
0.0800.
0.4000
0
92.1
29
112
0.4164
12.2
30.
2,4,5-Trichlorophenol
-0.438
0.200
0.4000
0
110
53
' 123
0:5008
13.4
30
2,4,6-Trichlorophenol
0.433
0.200
0.4600
0
108
50
125
0.4968
13.8
30
2,4-Dinitrotoluene
0.444
0.0400
0.4000
0
111
57
128
0.5244
16.7
30
Cresols, Total
ND
4.00
0.8000
0
103
20
125
0
0
30
Hexachloro-1,3-butadiene
.0.345
0.0160
0.4000
0
86.2
22
124
0.3928
13.0
30
Hexachlorobenzene
0.370
0.0400
0.4000
0
92.6
53
125
0.4164
11.7
30
Hexachloroethane
0.391
0.0800
0.4000
0
97.8
21
115
0.4580
15.7
30
Nitrobenzene
0.413
0.0800
0.4000
0
103
45
121
0.4780
14.5
30
Pentachlorophenol
0.387
0.200
0.4000
0
96.7
35
138
0.4408
13.0
.30
Pyridine
ND
0.200
0.4000
0
38.1
10
126
0
0
30 R
Surr: 2-Fluorophenol
0.788
1.000
78.8
10
147
0
Surr: Phenol-d6
0.817
1.000
81.7
10
140
0
Surr: Nitrobenzene-d5
0.844
1.000
84.4
10
169
0
Surr: 2,4,6-Tribromophenol
0.959
1.000
95.9
10
185
0
Surr: 2-Fluorobiphenyl
0.762
1.000
76.2
10
169
0
Surr: p-Terphenyl-d14
0.830
1.000
83.0
10
179
0
Qualifiers: k Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 20 of 32
Page 20 of 50

0
SUMIAlat
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
trVOWITOOMN ini. ! ht;HNULUUt;a, ARC.
Cuyahoga Falls, Ohio 44223
WO#: 1Z030215
Anatlffl,raP La7bor fur ie4
TEL: [phone] FAX- [phone]
Website: hgp.-1Avww.sette%com
15 Mar-17
Client:
Synagro
Project:
Dunn WTP
BatchID: R66453
Sample ID MB-R66453
SampType: MBLK
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 66453
Client ID:. PBS
Batch ID: R66453
TestNo: SW9014
Analysis Date: 3/6/2017
SegNo: 1095925
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive ND 0.500
Sample ID LCS-R66453
SampType: LCS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 66453
Client ID: LCSS
Batch ID: R66453
TestNo: SW9014
Analysis Date: 3/6/2017-
SegNo: 1095926
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 1.01 0.500 1.000 0 101 85 110
Sample ID 17021495-008AMS
SampType: MS
TestCode: Cyanide,Rea. Units: mg/Kg
Prep Date:
RunNo: •66453
Client ID: BatchQC
Batch ID: R66453
`TestNo: SW9014
Analysis Date: 3/6/2017
SegNo: 1095928
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit ' Qual
Cyanide, Reactive 1.07 0.500 1.000 0 107 81.6 122
Sample ID 17021495-008AMSD
' SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 66453
Client ID: BatchQC
Batch ID: R66453
TestNo: SW9014
Analysis Date: 3/6/2017
SegNo: 1095929
Analyte
Result
PQL • SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
1.05 • 0.500
1.000 0 105 81.6
122
1.072 2.46 5
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
7 Analyte detected below quantitation limits
M
Manual Integration used to determine
Original
MC
Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits Page 21 of 32
Page 21 of 50

suriVINI
_ Summit Environmental Technologies, Inc. QC SUMMARY REPORT
N T 3310 Win St.
crrwIKVINril:. N �U. Y I;UIITMLUUIt�S, INC. Cuyahoga Falls, Ohio 44223 WO#• 17030215
11.rwfAluaf LP:rbP.ratvrie;� TEL: [phone] FAX.- [phone]
Website: http://www.settek com 15 Mar-17
Client: Synagro
Project: Dunn WTP BatchID: R66453
Sample ID 17021495-008AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 66453
Client ID: BatchQC
Batch ID: R66453
TestNo: SW9014
Analysis Date: 3/6/2017
SegNo: 1096929
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: :k Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 22 of 32
Page 22 of 50

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
frsuramllz
3310 Win St.
tr"IRUIN 1`0UNIAl. A9;4;HNULrJla1�'S,INC. Cuyahoga Falls, Ohio44223 WO#: 17030215
dlr rlt ll.cAP C tanrstn€te.$ TEL: [phone] FAX.- [phone]
97ebsite: httD://1vww.sette7ccom IS Mar-17
Client: Synagro
Project: Dunn WTP BatchID: R66473
Sample ID MB-R66473
SampType: MBLK
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 66473
Client ID: PBS
Batch ID: R66473
TestNo: SW9034
Analysis Date: 3/6/2017
SegNo: 1096274
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive ND 25.0
Sample ID LCS-R66473
SampType: LCS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 66473
Client ID: LCSS
Batch ID: R66473
TestNo: SW9034
Analysis Date: 3/6/2017
SegNo: 1096275
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 2100 25.0 2250 0 93.3 85 130115
Sample ID 17021496-008AMS
SampType: MS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 66473
Client ID: BatchQC
Batch ID: R66473
TestNo: SW9034
Analysis Date: 3/6/2017
SegNo: 1096276
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 2130 25.0 2250 0 94.7 80 120
Sample ID_ 17021496-008AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo:. 66473
Client ID: BatchQC
Batch ID: R66473
TestNo: SW9034
Analysis Date: 3/6/2017
SegNo: 1096277
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Sulfide, Reactive
2140 25.0
2250 0 95.1 80
120
2130 0.468 30
Qualifiers: k
Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M
Manual Integration used to determine
Original
MC
Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits Page 23 of 32
Page 23 of 50

i
S
f - SunsmitEnvironmentalTechnologies, t. QC SUMMARY REPORT
' �a r. 3310 Win St.
erati�lac�rar�ia N���- akt &%BISltStC31WS, are. Cuyahoga Falls, Ohio44223
WO#: 17030215
A nzr?yUcat Laboraivrie5 TEL: [phone] FAX.- (330)'253-4489
Website: http.-1Avww.settekcom 15 Mar-17
Client: Synagro
Project: Dunn WTP BatchID: R66473
Sample ID 17021495-006AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/Kg
Prep Date: -
RunNo: 66473
Client ID: BatchQC
Batch ID: R66473
TestNo: SW9034
Analysis Date: 3/6/2017
SegNo.- 1096277 -
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit . Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above, quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 24 of 32
Page 24 of 50

1 t, SummitEnviroramentalTechnologies;.Inc. QC SUMMARY REPORT
3310 Win St. l,� SUMMARY i 1
LNVIRPn IAL Y 1;CHurJLUG15,1rqC Cuyahoga Falls, Ohio 44223
&,,,3i4,16gHT LzZ;or�ta[l�s TEL: [phone] FAX. [phone] WO#: 17030215
Website: hQ.1Avww.settelc.con: 15-Mar-17
Client: Synagro
Project: Dunn WTP BatchID: R66500
Sample ID 17030215-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 66500
Client ID: Dunn WTP -
Batch ID: R66500
TestNo: SW1030
Analysis Date: 3/8/2017
SegNo: 1096787
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability ]on -flammable. 0 0 20
Sample ID 17030215-001ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 66500
Client ID: Dunn WTP
Batch ID: R66600
TestNo: SW1030
Analysis Date: 318/2017
SegNo: 1096788
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability Jon -flammable. 0 0 20
Sample ID .17030217-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo:. 66500
Client ID: BatchQC
Batch ID: R66500
TestNo:'SW1030
Analysis Date: 3/8/2017
SegNo: 1096790
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability Ion -flammable. 0 ' 0 20
Sample ID 17030217-001ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 66500
Client ID: BatchQC
Batch ID: R66500
TestNo: SW1030
Analysis Date: 3/8/2017
SegNo: 1096791
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability Ion -flammable. 0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine Original
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 25 of 32
Page 25 of 50

I
M9
sua#114101-
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
LNV1HIJTaG1i.NJAI. IW;HZ4ULCFin1:!i,AMC.
Cuyahoga Falls, Ohio44223
WO# 17030215
tinaljl2Lgif C�rkrcrr�toare5
TEL: [phone] FAX-[phone]
Website: hgp://wivw.settelccon:
15-Mar-17
Client:
Synagro
Project:
Dunn WTP
BatchID: R66500
Sample ID 17030217-001ATRIP
SampType: DUP
TestCode: Ignitability_S- Units:
Prep Date:
RunNo: 66500
Client ID: BatchQC
Batch ID: R66500
TestNo: SW1030
Analysis Date: 3/8/2017
SegNo: 1096791
Analyte-
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
.Sample ID 170302197001ADUP
SampType: DUP
TestCode: Ignitability_S Units:.
Prep Date:
RunNo: 66500
Client ID: BatchQC
Batch ID: R66500
TestNo: SW1030
Analysis Date: 3/8/2017
SegNo: 1096793
Analyte
Result
PQL - SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability Ion -flammable. 0 0 20
Sample ID 17030219-001ATRIP
SampType: DUP _
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 66500 - .
Client ID: BatchQC
Batch ID: R66500
TestNo: SW1030
Analysis Date. 3/8/2017
SegNo: 1096794 -
Analyte
Result
PQL SPK.value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability Ion -flammable. 0 0 20
Sample ID 17030373-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 66500
Client ID: BatchQC
Batch ID: R66500
TestNo: SW1030
Analysis Date: 3/8/2017
SegNo: 1096796
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit " Qual
Ignitability Ion -flammable. 0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 26 of 32
Page 26 of 50

Summit Environmental Technologies, S.
3310 QC SUMMARY REPORT
/0 Win Stt.
�cs41FC[7WfA�:NIR69ttidBd-04LUiil ,mt,:� CzryahogaFalls, Ohio 44223
_. A6 tal�Phcr�f.C�iaaratafies WO#: 17030215
TEL: [phone] FAX. [phone]
Client: Synagro
Project: Dunn WTP
BatchID: R66500
Sample ID 17030373-001ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 66500
Client ID: BatchQC
Batch ID: R66500
TestNo: SW1030
Analysis Date: 3/8/2017
SegNo: 1096797
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
.%RPD RPDLimit Qual
Ignitability Ion -flammable. 0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine Original
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 27 of 32
Page 27 of 50

sumforr
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
LPN IRUIN T IAI. Cuyahoga Falls, Ohio 44223
e' nalyN=1 iaborafvfiv,� TEL: [phone] FAX- [phone]•
WO#: 17030215
Websitd: htp.-Mvww.sette&.cony
15 Mar-17
Client:
Synagro
Project:
Dunn WTP
BatchED: R66502
Sample ID les 20ppb L-0306
SampType: LCS
TestCode: voc-MSTR_n Units: mg/L
Prep Date:
RunNo: 66502
Client ID: LCSW
Batch ID: R66502
TestNo: SW8260B
Analysis Date: 3/7/2017
SegNo: 1096835
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowL"imit HighLimit RPD Ref Val
%RPD RPDLimit . Qual
1,1-Dichloroethene
0.0200
0.00500
0.0200
0
100
71
138
Benzene
0.0191
0.00500
0.0200
0
95.7
75
137
Chlorobenzene
0.0192
0.00500
0.0200
0
95.9
77
132
Trichloroethene
0.0196
0.00500
0.0200
0
97.8
.64
119
" Surr: 4-Bromofluorobenzene
51.4
50.00
103
.70
130 "
Surr: Dibromofluoromethane
49.4
50.00
98.8
70
130
Surr: Toluene-d8
51.1
50.00
102
70
130
Sample ID mblk
SampType: MBLK
TestCode: voc-MSTR n Units: mg/L
Prep Date:
RunNo: 66502
aient ID: PBW
Batch ID: R66502
TestNo SW8260B
Analysis Date: '31712017
SegNo: 1096837
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit. HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
ND 0.00500
1,2-Dichloroethane
ND 0.00500
MEK
ND 0.0250
Benzene
ND - 0.00500
Carbon tetrachloride
ND 0.00500
Chlorobenzene
ND 0.00500
Chloroform
ND 0.00500
Tetrachloroethene
ND 0.00500
Trichloroethene
ND 0.00500
Vinyl chloride
ND 0.00200
QC+
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
Original
MC
Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
O'
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Page 28 of 32
Page 28 of 50

Zkommu
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
=MVItiU NTAUN I AL I bXHNUUJU1.�s, JmC.
Cuyahoga Falls, Ohio 44223
WO#: 17030215
11rWil oSS
TEL: [phone] FAX. [phone]
Website:,htty:/hvwwsette%com
15 Mar-17
Client:
Synagro
Project:
Dunn WTP
BatchID:. R66502.
Sample ID mblk
SampType: MBLK
TestCode: voc-MSTR_n Units: mg/L
Prep Date:
RunNo: 66502
Client ID: PBW
Batch ID: R66502
TestNo: SW8260B
Analysis Date: 3/7/2017
SegNo: 1096837
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val :
%RPD RPDLimit - Qual
Surr:4-Bromofluorobenzene
48.9
50.00
97.9
70
130
Surr: Dibromofluoromethane
50.8
50.00
102
70
130
Surr: Toluene-d8
50.1
50.00
100
70
130
Qualifiers: k Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit -
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit Original
R RPD outside accepted recovery limits Page 29 of 32
Page 29 of 50

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
sumfill ar 3310 Win St.
crV,'1KQ,NG1:N [Al. a W:H?4ULrJGR;5, 1KC. Cuyahoga Falls, Ohio 44223 WO#: 17030215
,+ rwl,krttmf Lrrlao,ratprie6z TEL: [phone] FAX. [phone]
Website: htty.-Mvwiv.settelccom 15 Mat-17
Client: Synagro
Project: Dunn WTP BatchID: R66502
Sample ID 17030217-001ams
SampType: MS
TestCode: tcip-voc-MST Units: mg/L
Prep Date:
RunNo: 66502
Client ID: BatchQC
Batch ID: R66502
TestNo: SW8260B
Analysis Date: 3/8/2017
SegNo: 1096853
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.174
0.0100
0.200
0.
86.9
.39.9
160
1,2-Dichloroethane
0.170
0.0100
0.200
0
85.0
42.5
157
MEK
1.02
0.0500
1.00
0
102
16.6
227
Benzene
0.190
0.0100
0.200
0
94.8
38.1
155
Carbon tetrachloride
0.188
0.0100
0.200
0
93.8
40.8
162
Chlorobenzene
0.200
0.0100
0.200
0
100
35.7
168
Chloroform
0.186
0.0100
0.200
0
93.2
18.3
199
Tetrachloroethene
0.197
0.0100
0.200
0
98.4
10
261
Trichloroethene
0.191
0.0100
0.200
0
95.3 -
23.8
175
Vinyl chloride
0.232
0.0100
0.200
0
116
10
165 QC+
Surr:4-Bromofluorobenzene
513
500.0
103
84.6
130
Surr: Dibromofluoromethane
478
500.0
95.5
71.4
127
Surr: Toluene-d8
510
500.0
102
74.6
127
Sample ID 17030217-001amsd.
SampType: MSD
TestCode: tclp-voc-MST Units: mg/L
Prep Date:
RunNo: 66502
Client ID: BatchQC
Batch ID: R66602
TestNo: SW8260B
Analysis Date: 3/8/2017
SegNo: 1096854
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.177
0.0100
0.200
0
88.6
39.9
160
0.174
1.99
25
1,2-Dichloroethane
0.169
0.0100
0.200
0
84.4.
42.5
157
0.170
0.590
25
MEK
1.01
0.0500
1.00
0
101
16.6
227
1.02 .. ,
1.52
25
Benzene
0.186
0.0100
0.200
0
93.1
38.1
155
0.190
1.76
25
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND . Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 30 of 32
Page 30 of 50

Summit Environmental Technologies, Inc. QC'SUMMARY REPORT
summur
3310 Win St.
Cuyahoga Falls, Ohio 44223 WO#: 17030215
__ dtstytlFlfca! Lsr2ze�.r41Q, iE? TEL: [phone] FAX.- [phone]
Website: hfW.1Av1vw.settek.com 15 Mar-17
Client: Synagro
Project: " Dunn WTP BatchID: R66502
Sample ID 17030217-001amsd
SampType: MSD
TestCode: telp-voc-MST Units: mglL.
Prep Date:
RunNo: 66502
client ID: BatchQC
Batch ID: R66502
TestNo: SW8260B
Analysis Date: 3/8/2017
SegNo: 1096854
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit , RPD Ref Val
%RP.D RPDLimit Qual
Carbon tetrachloride
0.182
0.01.00
0.200
0
91.1
40.8
162
0.188
2.97
25
Chlorobenzene
0.189
0.0100
0.200
0
94.3
35.7
168
0.200
5.87
25
Chloroform
0.184
0.0100
0.200"
0
92.2
18.3
199
0.186
1.08
25
Tetrachloroethene
0.180
0.0100
0.200
0
90.2
10
261
0.197
8.70
25
Trichloroethene
0.186
0.0100
0.200
0
92.8
23.8
175
0.191
2.66
25
Vinyl chloride
0.223
0.0100
0.200
0
112
10
165
0.232
3.91
25 QC+
Surr:4-Bromofluorobenzene
490
500.0
98.1
84.6
130
0
25
Surr: Dibromofluoromethane
486
_
500.0
97.3
71.4
127
0
25
Surr: Toluene-d8
512
500.0
102
74.6
127
0
25
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E . Value above quantitation range.
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds " PL Permit Limit R RPD outside accepted recovery limits Page 31 of 32
Page 31 of 50

Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
'
LNA11HPINTPIUNI.'4h97:GRINU*WGII:s,INC. Cuyahoga Falls, Ohio44223 WO#: 17030215
Anzdj,,H f Laborwta,riau TEL: [phone] FAX. [phone]
Website: hQ.-11ivww.sette1r com 15-Mar-17
Client: Synagro
Project: Dunn WTP BatchID: A66612
Sample ID LCS-R66612
SampType: LCS
TestCode: pH_011(9045 Units: s.u.@19.6C
Prep Date: _.
RunNo: '66612
Client ID: LCSW
Batch ID: R66612
TestNo: SW9045D
Analysis Date: 3/10/2017
SegNo: 1098612
Analyte
Result
PQL SPK value SPK Ref Val %REC
-LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
PH 7.q t.0 u 1uu au - Ilu
Sample ID 17030430-001ADUP
SampType: DUP
TestCode: pH_011(9045 Units: sx.@20.1C
Prep Date:
RunNo: 66612
Client ID: BatchQC
Batch ID: R66612
TestNo: SW9045D
Analysis Date: 3/10/2017
SegNo: 1098614
Analyte
Result
PQL SPK value SPK Ref Val. %REC
LowLimit HighLimit RPD Ref Val
%RPD ' RPDLimit Qual
PH 5.8 0 0
5.8 0.7 10
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for -preparation or analysis exceeded 7 Analyte detected below quantitation limits M Manual Integration used to determine Original
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O 'RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 32 of 32
Page 32 of 50

Sninm t:Environmental Technologies, Inc. nalysiS RequesWhain Of Custody
MOrpon 3310 Win Street Iror Summit Environmental Technologies, Inc. use only
Cuyahoga Falls, Ohio 44223, Tel: 330.253,8211 Fax: 330.253.448page of SET No.
Company -Name (Please Print)..
Project Name
Comp ny ddre s
roject Ad ress
a s
Ile
W. U t..� [ r.��
� to
1
C ' at P ne o.
Report to .
6&
a 4 . -
C ent Fag'No. Flease Fax Results ✓
PO#.
cm tt
Cllent Entail- Please Email Results ✓
QuoteNo.
. Cj1%A
.a
'd
Gontn •L P - n
-
;:
ar -
mpled G
Clieck if 01i10 VAP samples ✓ ©
0
o
t.
r
#,
F
Sample Itlenfificatlon
Date
Collected
Time
Collected
Analytical Parameters and Medwas,
Ld
z L.
While and yellow pages should nc.00ntpany Samples to the laoorawry.. nu cuent reimna u.0 pum m— � Q g `} �} v
f2

N
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N
-- Rev. 16 EffouM- Date. OAtans 0)
Rev, (a
�1
Summit. ]Environmental Technologies, Inc,
Cooler Receipt Forth
Initials of person Inspecting cooler and sample
Client S��ii�
Order Number._
Late fteceiv
Time Received: i8�� bate cooler(s) opened and samples Inspected?
Number of CoolarsBoxes:
I NIA
Shipper.- 6i3 EX UPS
DHL Airborne US Postal Walk-in Pickup Other.
Packaging:
Peanuts( Bubble Wr Paper Foam None Other
Tape on cooledbox:
(� N NIA
�--�
Custody Seaats intact
Y N NIA
C-Q-C in E stla
(y ) N NIA
Ice Blue lea
�presen absent ! melted NIA
Sample Temperature I Gun #t16a, 2LQ459 CF b . o °C - -C NIA
Radiological Testing Instrument serial # 53 127 Y N N!
{see page 2 for scan results}
"Use 1 sheet per sample for Radiological Testing. If sample is HOT, the Radiological Safety Officer must be'notified
immediately.
C•O-C filled out properly
N NIA
Samples in separate bags
N NIA
Sample containers intact`
N NIA
*If no, fist broken sample{s}:
Sample label(s) complete {11), date, eta)
N
NIA
Label(s) agree with C-O-C
�
'
`L-
N
N/A
Correct containers used
—1/��
N
NIA
Sufficient sample received
N
N/A
Samples received within holding time
-
N
Bubbles absent from 40 mL vials"
Y
N
NIA
"Samples with bubbles �6mm are acceptable, Indicate bubble size if>6mm,
Was client contacted about samples
Y N
Will client send new samples
Y ,, N
Cient contact
Date/Time:
Logged in by:
Comments:
Page I oft
Page 34 of 50

North Laboratory Certification
Opp ifi6d f ara-rieteTs Usfing
La1., Nning Summll E-,thIr©nmeiilal Tech,loltxijiea:Inc,
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Lab Nme SalRnurl[nvi;flnmerltal:T(!rnncilogieF, nr__
CartHlc lr,'rVtFtllUPi. fi31
Address! M Q Win Street
Lt uN tine Dale: 1 it2CP17
Cuyahoga r-a%.,OH (4228-
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NITROGEN. A't" HATF=
:EPP, 2- 7 RLY. 4 4. 1994 (Agt,onee)
EPA 3004, Riev. 2:1, 19I 3 fAquantis}
$' t-0416 DG' 0 D.;Age:Spcil
S441446 50:•ti A (Ae L ep.e)
EPA 200A. !vise 5.4. 1994 {Aqueous)
NIVloGiEu, kITr,!TE
uVd 3af c:r2u [! USnucauc)
EIIA300.0,Rev 71_IU93(AqueouS)
ANITINIO.NY
4ts1.846 W% A fAcroavus)
EPA, 2GC:7, Ras. 4.4, 1'0144 (r4vUeous)
'4rrRoGF14. NO3-I4O2'
S4`r-846 601t7C IrtquUbus;
I, PA 390.0. -?ev. 2.1, IgA:1 (iirumusl
EPh.200:F,,, IZry; 5 4. 10@4 Ihqu_nu3)'
SME, A {Afpueov�l
SUl-54b 60i
WTPi GI,04.' TOTAL fKJ.L-LDAHL
ARSENIC. '
$tLi o500 Varf1 B-1.397 ,SM AKG NFra IO-1597} (Aqueous)
EPA 200.3, :tar,', -e 4. 1Tr0+;i�quP.01)sI
OILY CREASE
S'A,-Z4C 6010•D (Aquavus)
EPA 156a* ItDv. b (PyuFuus)
EPA200.8. Re'1..5.4. 19194 CAqu5cvs)
S'N.r46 9071 B (Norio %q:reows;
SSN•Sidt3.�rl1J[5R {Mpgqua) ..
Pd�iC1Sf?F7CE:US, fCa)'iyl: -
- OAriIIJT.P
-
EPA200.7,RpW 4A(79jr4)(,At;ueaej9;
CPA 20;7,9. Rm. a 4. 1M.4 (AtppMigs
.S1,1I4C1MIGD'(Aq.utoua)
S+iJ-E)6icr11CTI1;ArreaOUs) '
Rt-SlDUE., DfSS-).VEfl ina C.EPA
200.'8. 1iay. 5.4, 1904 (Aylir.,nusl
31%12&40 C=1}97;Agrrnutrs)
SI+' .a4d'9020 R (Atlurm m) '
RESIDUE, $USRE, NOED
flERY LLIUNI
uM:2S4'O.D-9991 (7sgtre4re5)
SETA 200' . lluy 5.4`, 199 G fAque m)
"
RCv1Df E. TCiTAL
�r/.SAGGU72I1f3(Aqueou5l
RrA 25 G P-9Sg7 (,(Wcaus)
GU♦,SX:y
-rhi"e ce'Ti.iaamtl mqurm rltanl:N-xr, U' d-• uc:ep;u7le quidrl aESumnoL p'nym. wo rf ripL:.uved me'haicic3Y.;gt!d s�tfif:.th;ry pc'�Orn'fiFl.rf UrLvvW;raW7 a,�rnP�og LY]Oi$::ri pre �41)jP,� ry Gt'.rl C�tId111L'°_. ^d�nr rin-.rrJ'ir.�7i[+I fAri0rr3Glia:-
Ct4 sa:lnlhrn i.,r'+NCAC 2H+10C•1
C.0 O
4-
4-• O
O
00
CID
N N
� O
CO
0-
I

North CarofFna 1^lasteataWnGrourldWhter Laboratory..CeNificatii
Certified Parametars Listing
tnil :UfttatIII
Qprbkmiehiem:)er Oil
331Q'Alin Stttlat
E'it�c;ivi DaIC: tJkl2fiE?
4U/.ahCrOa FsIIF.6H 44223-
Expimlian,Dale: ' Ill3f720t7
i74tio 3r Ust Atli wifrrieit,L• ttfaJ2Otfi
•
1hB:16asc n:.rtSx{kb0•aloiy, hGvng r!:i•fnN_;the e��xrfrrr;5[-0ISu.MG7l2:JF•I ItIt117,:SrdjtBRjtOdiGe_Ief1harr�iaSiJf=11Er1[r�°1AcperAO:rlar3lib'.2i
b^_`aN
---
.cmimD. PARAMETERS
IiPk 200.8, rev. 5, 4. 1904 (Aqueova)--
S1N-84fr"(it}2U E1 •(raquacua)
MAGNESIUM
CAf'PItLYC.: - -• _
EPA U0.7, P.m 4.4. 1994-
FPA• 200.7, Rev. 4 A, T;g9A tAqueaue3
SIV340' 60,1 LI D f r':q:ri ous)
MA 40AN ES E
G'A2CSfi.fi-f•7AH.54.'7'4yd'{Aq�.isT;}ftSi
EPA 00,7.Rev. 4:4.:5rE-0•fh liocxr)
S!,641&r, Gf120 a (A,queaun)
-KW-fltt w;070 D jAq;ueaus)
_
CA5YC6U(v1
EPA.20.8.Reu.'5'4. HM4IAqueous)
EPA 2tlD 7, Rfru 4.4„ lQ9f'(ligueauSl
S4Y$4E r070 Ft fAqut lis)
SUl'-445 4)010 a (A.quenus)
h9EkCVP{y
CHi1OMIUNI TOTAL
F-PA-245.1_ Rev. 3.0 19g4 (Afjmeousf -
0
�p
CPA 200.7. Rev. 4,4: t-D94 (Aqueous)
GVJ=046 7470 A lAq;xnus)
� 4—
SW-246 HID b (P qunaus)
EP'A 101 t iHuauous)
— O
=PA2004.Rm'SA.19,IA(Aqueuus(
MIOLYODCNUM
L • 0
c,761 840 G020 B (rlq}teous)
EPA 2d9.7, keu_ 4.4. 1336 ACL-VroM)
O O -
(108gL7
SVd E4G F@Btl I� (1vaUaoUs)'
p)
EPA 20:7. RCv. 4.5,16i4 (A
EPA �y0.8. Rcv, s.4.10114 (AqueUu.G
0-
SW-94 G KI0 D (Aqueoug) .
SylJ.R48 Ti020:8.y'Agoag441S)
LPA 2,90 8 Rev 6,4,1914 f,Ac;u_aau3I
NUGEf
�,'Jl.G4G 0C2 7 h! {ncsagcv5)
EPA MA. Rmt. t-4.1004 (Aquamal
43PPER"
$elf y tC E02D E (Aqu-eau t .
'F(°t+ fXP 7 Rev. 4.-4.ISM dAtpreatt5)
POTASSIUM
SIAI-846 6010 -ro JAQuoous)
EPik Z-30-1. WW, :,4,199: (Aqueot6;
EPA 200 8 •Rev 5.4, IC194 (,Sf(nC,009}
m
Sth 84eGU;0•D f.AqueauEf
SIN-fl4f, ftOM 8 (,crJea4s}
SELENOM
NN
EPA, 2M.A.. Rpm S 4. 1994 (AqueauSl
EPA2ff3 7 P4?L?.4A. 1M (AquLaW)
- SIN RCG$OMS (AgUeoUEs .
SVd 846 6010 D (AquenuSJ
31L'v R"
LrAD
LPA2C0.7, hw.o 4 4. 1 OQ4 (Aqut znus)
CPA200.7 Rev 4.4, 1094 (Aq rP._'nus)
311'-845 6010 D (Aqueous(
S4'l-84(5 COW D (,%tx,teous)
EPA .Z00.@. Rev, 6.d. I f7S4 {Aqi u+iltrif
EPA r ;tD 8. C'ay. 5.4. MEN (Aqumfs)
-
NV1-a4G.0@2@ o (i4fj41KUtIS)
SIM-NG 5020 G ()t4UC!vusy
S'0DtY7('.1
Ll`N111?A
EPA 200-7. RftyA.4, 19W,'(Agve.UtiS)
EPA 20p.7. Rev.'4 4, f%4 (•Agaeou3)
SV4 43.8010 D.(Agstgoel8}
'Chia rAu?:cul:on •rqu•ro2 a'a�iR-Ftrt�^-d an rate plu�le gt,•nlgy?sst:rp {e pfC?]I'Srn. uw. rJ aporgmwi n'oihedck�gq. pn0 [:ausl:alary p�crlOfm.Bn:aw? ¢vs�wa:icn�m npk:;• L2:.vi:tica:es:fr�;UateLt
taff�l Ft:?A"u11w* arxi:bf 4pter:ifo---:o.1 firkf3:ttUre

N4 PUl rarolin2fWastdwa1eriGrourldwl Lter Laboratory Ocyrejrlcatfon
Certatiecl Pa.ramaters Usting.
I Z N9rne: 8U.'nmit EnunnnrticnLil Tacfi,nalogipe, Inc
Crlifcale IJklmber: 031
Address: r 101"A n slre5l
rMtvive Dr!e - i (7,2317
Cklyikha3a Fa'fs, OFF, 44$23-
Expimioll Dale: ' 1231t}099
- _� -- - - -- -- - - • - - - - - - - - � -
-
D1
, to of LOsI lkrnelmnrent: - 1lfdtill'I fr
- -
-
FNe atrwc -lam,d I abssJlorf, nawri� duly ntr! 11'e irywrenninls 01 IvA bICP.G }li UI9u- IG
mr?riS �Jldw_rl Sor Urc m�a.uet,•rrnl �: tlw aanmdcrs Lo.�Q L'Cdow.
�— --
CERTIFIED PARAMETERS.
STRONTIUM
IIG]DEi, ORGANOCI•ILri1:4NE
— ^— -- -- -
EPA2tIU.7 Ruv A 4 513:OqueotlS;•
EPA -GU iAgUeou }
_
SDY.Ndc,•t 010 D{Acuendso
5UJ^8A6&11oT 11 (Jiqueous)
EPA 2013.8, Rev.5.4. 1994 LAquemrj
PoLycH:ORMATEG 8IIAHhNYt.S
SAryF 6AC� fi01J 9� (�i�ryusOUs�
F-PA 608.(Acme iars)
THAL1.I(Jrv1
gyPA fat, sON2,A {,�t(moaus)
1^FAA t,M 7- RL J. A.A. MJ•L%4 (Aqueous;
$IJRGFAf3..1 . GRGANIC:S -
49W-1S41f 3011] 1 � IAclult : S)
EFIAS 624 !Aggenusl
EPA MI0 s. Rou r 4. 1 y 4 (Ag�nauF}
al°4',3f 0, L760 F (AIj1Ier] s)
,StN-946 0020 B IJlyuer,4r .)
70TAL OPGANIC HALIDES
TIN
SW-00.9G20 0 {Aqueairs]
(O
CD
LO
[ A 200.7 Pew 4 z t r r )
SO4 eAgiier;
rrI I PJIE;,�L PiAN ��, oRcnnlcs
4—
EW-946 6c1O D IAquecjus]
S1N-LA6 PD' ; C (Atleesus)
O
O
VANADIUM
TPH GA4.OLINC RANGE, ORGANICS
(D
dam'
LPA 200.$. Rev. 5+!• 1'E941Aquea4k5)
S:nj-ZIh.O P,31� C 44greakrs):
N
- :' SV'/•B46-GG20 ;3 {Itg41Cau5)
J
4'JLl�TII.E PESf7�l,m{11tiAItYdR'DCPRBJ.Vi^a
-
(>5
ZlNv
MADEP, pfay.2064, Rov. 1:1 fAguern:s}
CL
EPA 200-.l , Rov. 5.,4. 1 SE]h (PgUecUSj
Su'1-0d6 61320.13 (AquLrjus)
ORGAP41C
-
- FCLF UPoG�NICS - -
•
5 1311 CAqueaus),-
ADSOREIABLE LIK(jANIG HALIDES
EOA 1630.I;t3v %.1;a97 V%g1.amis)
P3A'-r NturRALIa.(:10. OiW.& IIC's
EPA626 (Aruee-e:j
- iW8cct877A 17 ttbjUeaus)
-
.
CI16ORINNTE0 ACID I•rFRIllrIDE!:
Sul'-0z0Ill 5o1 A %A:lumpuS) ,
CI ILORQNATED r H r NOLIC S
EF°A IM. Rov. A. AFJOY r;314u:na,l }
EXTRA'.'r+0'L=,I?ETR0LE'UM IIYDROCARBC]:dr,
TOADE P, Msy?.0 04, Rev. 1.1 iAquprnaSS
NONHALDC3Et.•;ATLI3 VOLATIpE, C)RO.kI,;FCS
SUV•♦afti,.l 0�01i OrlueTtl5)
-
ih•30pn[leaiian oaq�drt~•.rooi(IlelmrnF'anro;car;lallle avail"y�ytUran7 ei aly1na,�e nlBlNorlalocy. and SEtls'£�7xy 4n3rlUm�.�cra rn C?dlndIICR 9'..-m0eY 4nh rtlipn(eseie•stA�,P•d 4u a lit UUn3h`L5 sn4rorLe r'irancn+p•inf racUurs w "al fkInhi In 15A NCAC N ORUT . -

North Carolina Was towateriGrounc-1waiter Laboratory Cerfificatfan
C. ortifted Rarsmotm U61ing
Lan.NaMe,. Summit EtivIronmental Tech fioloyld-, fpc.'
Address: 32 10 Vin $traM
Guyaha#a Falls, OH 442231-
Thil awm nirtied howig duly 010 Ihf:mqujm-n M., sol W, -Slf,'AG211.0110. JE he-rr-"-4lfiPrl Or tie rReastirencer, of lhcj primetars b'Eze6bel.aw
CERTIFIED FAR AMEMRS
040Rl ANIC
SILICA
BOO
ERA 2017, 4.4. 1904 ffteatm)
SM 5210 8-20011 ftueaus),
SV1v=fIGCS 03'a D 4A� ueous)
OFILORIDE
SIJUATE
SIN-64173 0iD56A (Ar.1 uems)
-t, ig,93 (pqug,30,�)
coo
SN-940 1.4 VA (Aqu-eoms)
SIA 5Z2V C-IIS97 (4quew,-)
SULFIDE
FLUORIDE
SVV-646 �WA {AquO-N.5}
EPA 30.0-0., Rev, 2.1. 1 GS?3 (Aquamw
METAL
SW-1948 UNC, A (A.q-jemrs)
TCLP METAILS
INORCANIC P.HENOU�
M-1346 Utl fAqUeoqs)
[.PA 420.1 , Rev. I q7-S (4gIJEUH9)'
ALU PAINUM
NITROGEN, NITAA' F-
CPAs 2013.7, R6V.-A-A, i tr-44 (Aquetms)
15--PA 30�0, Relt 2-1, 1 993!(AquU0Us'-
'
SW-9461 905rD A (Aq Uemn)
EPA 2.6b:�. Rev.. 5.4, 1 R94 (Aqjeaus)
NITROGEN, Mr-l-RITE
6020.6 4.4,quecusl
EPA-,300.U; Rov.2.1,1993 (Aquoaus)
ANTOWNY
SIAF-846 90-66 A IlAquea,,4s)
EOA 209.7, Rev. 4-4,1994 fAqueousl
HRURIDGEN, 11,03, 1- NO2'
0-(A46ecub )
E P.A., 3M. 0, Rev. 2, T 1983 ,'Aq ueous)
ERA-1611.8' ; AcY. 5. 4, 1 9D4'(,44,uebu�)
SW-B40 D0513; -A (Aqueous)
S4h,'^-846 UPO B (Aqmous)
N IT!10G EN. 707AL XJELDAHL
ARSENIC
SPIT 000 Norg B-1097 (SIVI 4500 A1113 D-1 I 997)'(Aqjea,us)
EPA -2 00. 7, Rev 4 A. 1.994- (MUCRDUS)
OIL &GREAsrz-
SVir,8413%).10 D (AqUaout)
SPA 16S4.R ev. B (Aqueous)
r;PA 2.0(r UKov. 5.4,1.994-( . Aqueow)
SW44691171 B(Non,Aqucousi
sw-'846. U1123 B (AetrubW4
PHOSPFORUS, TOTAL
BAREUM
1-PXPJ00.7. kev. 4A (1934) (Aqueeus)
EPA-= - 7. Rev, 4 4,1994 (A,4uwas�
RESI 0 U E, D I S SOL'am iab a
EPA 20,349, Rpv $.4- 1 BRI (Aqaeaus)
-SIVI 040 b.-1997 (Aqaanusb
SVJ--84S 6071) A (AqULLCr M.
REtIDIPE, SUS43ENDED
F;P A 2 00.X, Rov 5.4, 1994. Q%queous)
PIESIQUE, IOTAL
SW-846 6b2C 8,Aaqeoug)
W 2540 9-19 . U7 (Aqueous]
a(?RON
Corti titer 'N oTbe f:
-=ffmC;H%re;DR1p
Fxpiraiisal7 Gaze.
Date a I Lasl -Ali j und-mm nt:
12S3V2G1;6
11 f4p-13T6
'rnm oertwam rtquims mail pn,:e*rjr;in ;fl;rP ptRb "-UVRIr' amljrgw-s PMCIPM, VSe methad0169Y.41nd `!Xfistdory pwfC7rl1l*r1q' im, em-alwILan samplem re 51.01*C.' C* c-0 peq;fflim; ;;nd.'or dem6fiention lr)r irfr�. i;cm
BE, set6ftll ill 1 '%4, NCAC 2H. 6201

R-orthCarollna'WastewaterdG'roandwater Laboratory Cartlrcation
CeTuFied Parametdrs 1_fsting
La.b Noma: Summit EnvIronmext@1TerhnnfWles, fnc.
rsddross: 2,;;iTO Winn Streel
Cttyah,o6e Falb, ON 44223•
Thu a brave nemeo labaatcry, rtaviny duly tnniilita.requlremrn a art i 5A N(;AC 2KG3CO3 Is heremy cemrkd for Ilia rrss:urmtent of ire. frrprneLT, hscrtl tuloiv
CERTIFIED PARANIETERS
EPA'200.6, R15v. 5A, tO94 fAquenus)
8w,r-r,46 6620 r1. fr W LE3,US3
`CACMIUM
EPA P00.7, Rov. e.4, 19IR4 (Aquoousj
S110-846 6010 D (AVe4US1 .
EPA 20U.B, Sev. 5.4, 19-94 (Aqudous),
SVM'-U463 S020 R•(Aqueous)
CALCIUM
EPA 2100.7, Rev.4-4. iSIM Oqunmm)
SIN-84 G 09' G D i ftmous)
CE fROMIUNt TOTAL
EPA 2()117: Rev. 4.4s, 1994 (rtguoousj
S%V-P.4560,1a 0 iAquepus,)
EPA 200.8% RGY,-BA, 1094 ,okoUaDus)
S7,V-84fi U020 E (Aqueous)
COBALT
EPA 206.7. Rev. 4.4 19E4 (Aqueous)
8 -846 st7 Tp D (Aqueous)
EPA, 200,S, Rev 6A. 1994 (Agrrentrs)
-SL'd-t54G't:i172(?I-",.(.�ryUe01t5) ,
COPPER
EPA.21M.T. Rev.4.4, T994 (Aqueous]
SkV.646 (K10 0 (Aqueoas)
EPA 200-8, Hay. E.4, f904 {,Aqueous)
SIN-84t 02D El (AquemE )
IRON
EPA20.7. Rev. 4.4.' IR94 (Agl.u:nus)
SNI-046 601'3 ,0 (Aquenrts)
LEAD
EPA 2007, Rev. ", 19t34• (Aqueous)
, wW-946 VA 0 D (Agworn)
EPA M.t1,,Rov- 6!4,1994 (Aqw-mus.)
srrI-846 6020 f3 (Aqueous)
LITHIUM
EPA 200.7, Rev 4,4,1994'(Aquenus)
S''A'-940 001C. D i,A.gveuus)
W 3NESIUM
EPA 20n. I,, R9Y, fi 4. 1 _94 (Af ueousj
Srh+1.$4CSGT0 D {A'yueuuz) -
Td6ANGA1,fESE
ERK2130.7, Rev:A4, 1994 t,Nquows)
SW-648.9710iD tAgy"us)
EPA, 2130,$, Rev, 5•.4. 4r'9ab•(Aqueous)
oY4'446'-002a B (Aquuuus)
MERCURY
EPA 245.1; Rev. 3'D_ 1�39r {A.quwus)
SIU'046a 7470.A .(A queouiY
EPA 1651 R (Aquaoud).
fUt4�]L.i'd31iE1'1 t164
EPA 204.7- Ray. AA. ISN (AoUenijr.]�
s�rw-1�G sG1a p(Aqueous)
EPA 200.8, Rev, 5,4,1994 f %queousj
S1, -'04G 302 'B (Fu,u*-uus)
t4li KEI
EPA 2C(0.A. RRV. 5 +1, 199d (AgUeolm)
SIhR•$d6 ob2GL4.(AgOeous)
POTASSIUM
EPA 200.7, Rev. 4.4'r 1094 (+',quocus)
SW-846 ,G046IG (Av7ueous)
SELL NIU&T
EPA $00,8: Rev. 5.4.1 n4. (.Agtfaaus)
$W-8�6 $C$20 S-(Aquuousi
SILVIER
FPAlrji)-7; ftev 4.4. 1894 (Aqumms).
Sw- 41516a1G D (Aqueous)
EPA:'ea3D.8, R_v. SA, 1.994 {h� ucous)
SOr1 Ci�M
EPA4204;7, RaY.4,4, 1'994'(Aqueous!
SW-846 6016 D (AcufJuu_;
Cnflificdle iYtsrh�r'
g37
Er(Mctive Data,
VWZU16
Exrlration Ga1e:
12,931t2uT1;
Date of LiISF AMan9meta:
1114P2016
Tnis mrllt6r rc;ra mpires mairz Inca ef;eat av^ceptnbr<yuMlyrasstrraml- W09rarm, use ofapparoH mullicaolopy, and e3tM .-t.l y r).;rtSf"V.s?em Walu311cncaroP�03. L:kLuara;ff,tdrwr--Nvb,ceiIac"A *1;i ti :v andMi-dererttiaaam fix in63c iris
as set Toner Ina 6k 2Fr.i ga7,
C4
v—
O
00
N
tf3
f1
CD
L0
4—
O
N
N
(B
0..

North GaralimaWastewaterIGroundvvstar.Laboratory Gartification
Certified Parameters- UsUng
LaL>Namu. StrmmftEnjir4nr.1e0;.jI Iechmoldgies, Inc
Address: 3310 Win utreet
!Gttyahaga: F klts, 011 4:4223-
CrnrlifrOaie Klumb0e
531
Ffrar,'.IIVp [sate:
2;1�201'6
Expiraton L7aie:•
1213V2D163
Data of Last Amendment
11iW2016
The above nanh�a Innoratory, having .cutir mU Ita regtdramenlc of 15A NCA0 2H OPM, i-. hoe8y certifiers :ar Iho measu a mml rI the •pkli pihGJU13 Iislcal be'oA
tERT1FrED PARANIF..7ER5
STRONTIUM
PESTICIDES;-;)RGANOOHLORINE
EPA 20G. i , Rev. ,-4, 19944 (Agveous)
E1'i4:l3GA'(RrtltPL�USJ
54^t-S4Q B010 D (Aquoous}
8VV.84$i gust 'e (AgUgaus)
EPA200.8, Rov—S.4, 1!N4: (Aqueous)
POL,YCIHfLOHINNIFED SIPHENAS (PC&)
S1*846 020 9 (Aqueous)
EPA 608 (Aqueous) .
THALLIUM
SVV-84s 8682 A {A,quPou.s1
EPA 200.7, Rev: d d, t P54;Aqueous)
PU"R LASI E,'ORGANICS• .
8%,V-6413 60]C) G9 (Ar lror�ilsj
CPS.62.1 JNJUMIS)
EPIC 200.8, Rev. 15A, 1.994 (Aqueous)
Stti.PAS A-'M P.' (e4 yeokls)
SVu-84ra 600 B (,4pueaus)
TOTAL o tCaAmr, HALIDES
T+N
SVLr &ds 9J7o E (a�{u3ous}
EPA 200.7. RBtl.4 4. 19rt: (Aqueous I
TRH C iErSEL MNGE, ORGANICS
SVV-0466010 D (Aquetatls)
SL^d-64F, 80150 (AAue0u_)
VANADIUM
TPH-GAS:0LINr=RAN- 0E 6RO-ANICS
EPA200.B, IRcv- 5.4, 1Sn4 (k4umus)
SW-84G B016 C-(Aqureaus)
ZW-8466020, B (Arptpqus)
VOLATILEE PETFSpLEUM (HYDROCARBONS
,ZINC
?AAOrEb, May20( 64, Rev. 1,1 (Art ums)
EPA 200.3, Rev. 5A, t L—�64 (Aqueous)
SVJ•846 GG20 B (,Aqueou5)
O RG,AN(C
TCLP ORG;A+t1CS
SW-M t31;1 (Au.ueou•s)
ADSORSASL.i ORGANIC HALIDES
EPA 1M, Rev. C, 107 (Aquea.1%
BASE NELtTRAUACIG. t lRGANICS
E9}A �,25 {Acjrl.=_oust .
SW-8d6 8270 D (AoUGGus)
CHLORINATED ACI3.HERBIC 0ES
S4l11-84fi 8151 A (Aqueous)
CHLORfNhTI=D PHENOLICS
EVA 1555, %,,. A,1997 (Aqueaus)
EKTRACTAS LE PE7ROLE(]i T HYDROCARBONS
WADER May 2004, Ri=_v ' 1 jAgLla ,usp
NONHALGGENATFIS VC)L, i IZE, ORGANICS
svv-F4sA015C(Agmc rs),
'ohs oerlrecilion requires merrJOnce pf,rr orrcptable quality xxstvev ca pmpram, use d a p4rroy mptjcbofog0. and eate°a_lury KoiScrenart n c/i gylfalua6��79ar tf PLa Labotat©rosaie nuhjr,(ladrol C^snal[ias to LrOfdeCEll4fn dGun fur rrlracllnrs
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JAY 7kM1LRMM,
February 7, 2017
6.31
Ms. Meegan Dougherty
"Ummit F=rlVfronMantal'Techno!ooies. Inn.
38 10 Win Street
Cuyahoga Falls,,OH 44223
Gubji;-ct; NO WV5flMVLr-,,3!x1y-r14y Para'm'ateir Ma . thod'Decetfication Recommendation,
Zinc - EPA 2CO, 7 and SVV-84 6 66*10 D
Dear MS, D.oughe'rty.
The reMeclial PrMcicnr-y'Testlng (PT) result(§) far the Vetayr Parameter Mathqdks) reported 'by your
laboratory for the Nurth'Garolln'a Wastewater) groundwater . Laboratory Certification (NC VMIGW W)
perforrnance evalueffonwashiere unacceptalafe anal a-iixtv-dav parameter mathod deaertifrcabon will b
recommended. The results reported and the true valLi6s as they appdat'ih our records are as follows:
—T
SiWy �.a ra. m 6 1 e r Us e-'., h ci d Units. 'Performarice
Value Rar-,ge
V%fP 1613B EPA20.0-71 Pq/1- 600 496' 421 -569 Not AQvptable
SlRwW 5010 0
EPA 200.71 pg,'L -7,360 400, 1190-1610 Not Accieptable'
SW-846 601:0 D
"IX-, �tten Co mcbve Action —Report (CARI fo,f each unacceplab[o result will W nequired prior
'his is t6 notify you, that the LabomtoTy Gerti&at'iort Branch of the North COrolina DiVision 'Of Water
Rr sources, . Water Sc;enues Section, is cortsfdering recomm.end.jng a parameter meftiod�s)
decertification to the' Env! ro ri mental 'Program 'Supervilsbi- The rec6mmenciRtlan.concerns 'the above
ff
menti^wPad violationfs). This is nova decertification-, it Is a'n6tj'.caj in of our'inte'nt to. consider
Fb
decertification. You will be informed in a separate communication if decertification is issued.
Gon;a,M me immedi�telje at (519) 7-33-39118 ext 251 your recards do not agreevvRh ours or if you have
Sincerely,
Todd Crawford
Technical Assistance &'Com'011ance Specialist
NO WWIGW Ulb.6ratorV Cartiffication �rahch
ca- Dana Savet'vehite, JasGn Smilh, dlv'rsler File # nill
Water 50u:ces sec*1011
Fi*�;,10'9�9-7,*J-'-Ii-A�i"-,,'t1 W--'1-92-62-0
Page 1,0 of 16
Page. 44 of 50

K A 'Vl rO F� R -M A IN
February 7, �01 7
631
10 s Mes-gan Dougherty
Summit Environmental Technologies, Inc.
33'1 0 Win 'Street
Cuyahoga Falls, OH 44223
Sutbject; NO VA?%1/MV LC Sixty -bay ,araP a
niater Method D.000ft-Ticatiori Recommendation,
SelenhAm ® EPA 2011.1 and SVV-846 8010. 0
dear Ms- Dotijberty:
The remedial Proficiency -resting fPT) result(s) for the below Parameter Math
ad(s) reported Fay yourlaboratory laboratory for the North Carolina. Wastewater/ ,Groundwater'Lgboratbry Cerlitic2tion (N . C VMfiGW LC)
performance evaluation wastwore,.inacceptable and a;:E�lxt . yd ly te r ri-�
_�a CE i a- th o d. de �cbif&�gafipn
will be
rewmrrendtd. The results reported P0 the true values as they appear. in our records are as follmvs:
-Study Parameter P.11eft Repofted True Acti§ptarze
d Units I 'PErfwmanGe
Vale Value
R-a—r-ge
EPA 200.7i
520 4,12 376-508 N6t; Acreptable
SW-646 601 1:) D
! PA 20G,z0b 71
092016LA1 S,Ar_at JG 386 326-444 Not Acceptable
I
Unyrective Action repiable reaull will be required prior to reissuing cenificalim,
This is to, notify you that the Laboratory Cortiflication. Branch of the- North Carolina Division of Watibr
R�ssourcesi` Water Sciences Seation", is considering recommending a 0arameter rti . efhod(s)
d6certification to ,he Environmental Program ;5up��Njs '' or, ThG recc­rnm&nd31ior1 wntems the above
meritfonmed violationt's)- This is not ai decertifiratl6n,. it is. a notification of our intent to consIdur
decertification. You will be informed in a s6parat "
a COMMUniCaElOn if decertiif�cation is issued.
Contact m6 irnmediatery at [phone] ext, 25.1- if your records do not agr"ee with ours or ef you have
questions,
Sincerely,
Todd Et'a+rt+fprr�
Technical Assist ' ance & Compliance Specialist
NC VVVIIGW LatiDratory C&tifinatidn 13.rancih
Ailtadirnoiil
-r--' DanO 48attG1%vMa, J­--Son Smitil, Maslen Fill 963-,
CailiflLu2i"aaRi a nch
%Ut I i Car.,111-
-j. Ne­r -0J6;r'
jr 44L :Fee
U
lnlerqd-
Page 11 of 16
Page 45 of 50

it.t) �r '3�. PER
�: � tit
4 ,^
February 1, 2017
Mk . Mjepn Dougnerty
oi6► imft Era'trironr drlial'f"a4ftiologitrs, fl'ac.'
3310 Win Street
Cayahop Fails, OH 44223
Subject; NOVsiV'VIGVV LC Sixty -Day Pararrieter 048'thod Decertification Recorn' mendation: ,
Mikel m EPA 200-7' and SW-84e 6010 G
Rear Ms, Dougherty
The rergediW 'fofci_alcy Testing (PT) result(s) for the below Pwarnoter iylethod(s) relac'rt6d by you-r
laboratory for the North GarDlina 'Nasiewateri Croundveatcr Laboratory Certification (NC- y'u'I+'J GW LC)
Pedormance evaluation veas/viero unacceptable and a sixty-day aaran'ieter method sLecert"ification rlrtll be
recommended, The res;Jits rebored -and the true value's as the appear in our records are as follows.
Ir I ttld + F'ararrsete= t�lethcd Ua,.S K=pert d rug 4cceptnnca
_ sY� Perfortr�anc� ;
Value V-3lue • Par�ge
let+P�t?-313 LPA 200.7,' +a r� r
_. BW-645 601 CI C ta9 I 1 55 �1 � 805- +��:� Not Acceptable '
EPA'1t3C3.71 Ng't- I �62� 1.C} t20�-ta�0 Not Acceptable
4}920i6CC1 + ! rl .s
--- I - _ SS+� -846 6010 ©...I
'He:llen C orrectrve. E+CiiOf+ Report (GAP,j for vacit un3 Cc l ��r0 .aaurt vrlr GC required prim ti) . Uissu.n3 ce M.—Irirrr
This is •to 610 ifs+.yazl that [he Laboratory Cartification Branch of tine Ndrth Carolina Division' of Wator
IRasctearces, Miter S6enoes Seclian, is considering recommending , a pararnetc•r rnethodfsj
d certlioation to: the Environmental Progret,' Supervisor- The recommendation concerrag t}ii} . above
rrie6tiened violation s). This is nat a decertification,` it is a notification, of our intent to consEder
rdeCert n. Y04 will be lnfd"rowed in a separate comintinication if decertification is issued.
Contact and immediately at (919) 733_3906 exL. 61 if S+ar.tf records db .rant adree with ours or if you have
questi6na-
Sincerely,
Todd Crawford
Teat ... aI Assiut Wce & Compliance ��eciali t
HC'�d1NIG"Af Laboratory Cartificati'on Sraneh
1�8l�efdr'rttrrr
C1ana S lk sv.'h:le, Jos xn Smith, Master do $C,31
Water sri6_+re ,. see,loa
_ P!C Vl;2s C=t;'�Ce�!G:��=hd:ri9r Laftoralcry C e li-f.:�ticv Srsrleh
! , ��Co�l"1 Yt=:J a.a J .rC';.' ••=J.i t' ii(.'IIi:C: -�1:
r,rrlrl jrr ncarr zlw�Bd,rrs iu� ticrier-r un€as.•al rresv }ryes Bald •r; �Clar-'S�IEIL 4' CItJIrIC—Oci{e ldl?�raCS�C �1[ LLa,ri-Y in.. v:'�
b
Page 12 of 16
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ERA 09120,1 KI 20-09, TNI Evaluation, Final Comp"Iete Report
A Weitug, Companq
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lIPfA ID -
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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Dunn WQ Permit Number: W00006101 .
WWTP Name: 'City of Dunn WWI? NPDES Number: NCO043176
Monitoring Period: From 01/01/2017 To 06/30/2017
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A(time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
it appucame to alternative periormea l lass
A or glass is com sere the ionowing monitoring
aata:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical .
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the oh
MPN
MPN/g
Coliform
power per gram
of total solids
CFU
<36400
<36600
<37500
CFU/g
0
Based on
grab
9222D -
Land App.
MF
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction) x
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Mt. 9
Option/A1t. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. Fain aware that there are significant penalties for false certification including fine and imprisonment."
Donrie Dukes Wastewater Treatment Plant Supervisor
Pr Name alid Title (type or p 'nt) Land Applier Name and Title (if applicable) (type or print)
..
Signature of Preparer* ate Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Cameron Testing Services, Inc. Laboratory Report NG DENR #654
NC F5HHS #37799
os US EPA #NCO191 8
...... .....
Synag ro ".7
MR.
ct
Dunn WWTP Yes
Sample Information
'
Fla M9141
C. Hayes 03102/17 iecegve¢k S. Bullard .03102/17
Analyses and Results
170363 01
170363 01
Slud& Gr Fec. Coliform-S. <37500
Mfg. 37500 03103/17 SB 9222D - MF
b
<36400
Mfg 36400
C
<36600
CFUIg 36600
d
<36400
CFUIg 36400
e
<36400
MID 36400
f
<36400
GFU/g 36400
9
<36600
CFUIg 36600
Geomean <36600
gludgc Gr TS N Z67%
0.01 03108117, - ERP 2540 G -TS
b
2.75%
0.01
G
2.73%
0.01,
d
2.75%
0.01
e
2.75%
0.01
f
2.75%
0.01
2.736/.
0.01
Report
Review
- 'WL�Ij
Lab Director Date
219 S. Stele Str, 919208-4240
Sanford NC 27330 c hds@camqon(est1ng.cqm

1
219 S- Steele Str.
Sanford, NC 27330
Phone:[phone]
Cameron Testing .Services, -Inc. .
NC WWIGW Cert.#654 NC PHHS Cert# 37799 US EPA NCO1918
Chain of Custody
Page - of
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284 Boger Rd.
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Mocksvi[le NC 27Q2$��
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Sample ID
E �-
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H2(S)04 H(N)03 (Na)Thiosulfatie Na(OjH
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Rush work.will require prior approval. Additional charges will apply

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: , City of Dunn WQ Permit Number: WQ0006101
�. WWTP Name: City of Dunn WWTP NPDES Number: NCO043176
Monitoring Period: From 07/01/2017 To 12/31/2017
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) .Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to. Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying • Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative pertormed c lass
A or u lass 1s coin sere me zouowing monitoring
aaia:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum. Units
dences
Analysis
Fecal
2x10 to the 6th
MPN
MPN/g
Coliform
power per gram
of total solids
<37500
<37600
<37600
CFU/g
.0
Based on
grab
9222D -
CFU
Land App.
MF
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR'503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Mt. 4
(VS reduction) x .(40-day bench) (30-day bench) (Spec. 02 uptake)
Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable)
Option/Alt. 9 Option/Alt. 10
(Injection) (Incorporation) No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check.the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met.
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Donrie Dukes Wastewater Treatment Plant Supervisor
Pre Name and Title ( or print)
Signature of Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Testing Services, Inc. Laboratory Report
NC DENR#654
Cameron
NC PHHS #37799
US EPA #NC01918
P
Synagro Ws:-iPr j
171454
ier�t
_ L
-. a
Dunn VMTP Regui;~ata.�t
Yes
Ev4rPr�a�et
Sample Information
E samples
C. Hayes to ' a 08/31/17 1 R WO.
M. Sims r>.bateNy 08/31/17
wW
�u�'k.�i-i'.y'^`k^1.o'•'i'...•u,.r.. .._...._
_
Analyses and Results
171454
01 a
Sludge Gr Fec. Coliform-S <37600
CFUIg
37600 08131/17 SB 9222D - MF
b
<37500
mig
37500
C
<37600
mig
37600
d
<37600
cFurg
37600
e
<37600
cr-urg
37600
f
<37600
OFU1g
37600
g
<37600
cFUtg
37600
Nmrnean <37600
171454
01 a
Sludge Gr iS (%j 2.66%
v,
o.oi 09/01/17 ERP 2540 G TS
b
2.67%
0,01
p
2.66%
%
0.01
d
2.66%
%
0.01
e
2.66%
4
0.01
f
2.66%
ti
0.01
9
2.66%
0.01
Report
Review
/
Lab Director
Date
919-208-4240
219 S. Steele St.
Sanford i�C 27330 chri.S&Rnlerontesting.afm

219 S. Steele Str-
Sanford, NO 27330
Phone:[phone]
Cameron Testing Services, Inc.
NO WW/GW Cert. #654 NO PHHS Cen # 37799 US EPA NCO1918
Chain of Custody
Page Of
C nr pony: `�
Email:
C2Pi`—
CTS lab use only
% ���� i�� ' n
Contact: C .vet, ►�iGw�cS _Phone:-
-
—
Sample Temp 1!
(C) _-- Prol
Address.! (City,
Fax:
Arrive:
State,,z0)
Notes:
Due:
Projects -Q-� (�
l�
Regulatory Rush
(YIN) (Y/N)
Collected: Name:
Signature:
Sample Information
Number of bottles
Requested Analysis
a) Cax
z
T N N
Preservatives: (U)npreserved, H(C)I,
CTS Lab
Sample ID
6 EE m
}
L7 o ii �"
H2(S)04, H(N)03, (Na)Thiosulfate, Na(0)H,
ID
d CJ
`
<- m v r
O
Other (X), Indicate
Relinquished:
Received
DatelTime
Rush work will require prior approval. Additional charges will apply

Black River Wastewater Treatment Plant
City of Dunn
2017
May 2017 Vector Attraction
Rec.—.77
Holding Tank—.66
.77 - .66 = 42.3%
77-(.77x.66)
August 2017 Vector Attraction
Rec.—.83
Holding Tank--.74
.83 - . 74 = 41.6 %
. 83 - (. 83 x.74)
November 2017 Vector Attraction
Rec. ---.79
Holding Tank -- .69
.79 -.69 = 41.7%
_.79 - (.79x .69)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) ,
Facility Name: City of Dunn WQ Permit Number: WQ0006101
WWTP Name: City of Dunn WTP NPDES Number: 03-43-010
Monitoring Period: From 01/01/2017 —,To 06/30/2017
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
It applicaDle to alternative pertormea Class
A or l:lass Is coin fete the ronowmR monitoring
aata:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum . Geo. Mean Maximum Units
dences
Analysis
Fecal,
2x10 to the 6'h
MPN
MPN/g
Coliform
power per gram
of total solids
-CFU
<35700
<40600
<45000
CFU/g
0
Based on'
grab
9222D -
Land App.
MF
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform) .
Vector Attraction Reduction (40 CFR'503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0ption/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) (Spec..02 uptake) _
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Mt. 8
(14-Day Aerobic)
(AlkStabilization)
(Drying —Stable) (Drying —Unstable) _
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation) .
No vector attraction reduction alternatives were performed x
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law; that the pathogen requirements in 40 CFR 503.32/15ANCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment
Pam Gibbons, Wastewater Treatment Plant Supervisor
Prep N and Title ( oa�r print)
0.
Signature of Preparer* , ate
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Cameron Testing Services, Inc.'
Laboratory Report
NC DENR#654
4
NC PHHS #37799
r-- - 7
., 4
w
F"
Synagroc,TPo�
-—F
x
y�
US EPA#NC01918
170362
Dunn WTP
'R2egu�a�a
.Ftr� �
Yes
Sample Information
`
x F
C. Hayes
y
03/02117eeved
S. BullardD_atez 3 03102J17
Analyses and Results
110362 01
3tudgc Or Fec. Coliform-S <40700
Mig 40700 03103/17 9222D - MF
b
<38600
cFur9 38600
C
<39800
CFuls 39800
d
<42700
cFurs 42700
e
<42600
cFulc 42600
f
<45000
crui9 46000
9
<35700
cruls 35700
Geomean e,40600
CFurg
170362 01 a
Sludge Gr TS 2.46%
aol 03/08/17 2640 G TS
b
2.59%u
0.01
c
2.51 %
0.01
d
2.34%
0.01.
e
2.35%
0.01
f
2.22%
0.01
5 '
2.80%
0,01
Report
Review
Lab Director Date
/'v v
219 S. Steele Str. 919-208-4240
Sanford NC 27330 [e-mail]

219 S. Steele Str.
Sanford, NC 27330
Phone: [phone]
Cameron Testing Services, Inc.
NC WWIGW Cert.#654 NC PHHS Cert037799 US EPA NOW918
Chain- of Custody
Page of
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+Company
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)=mail;
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_ ..:1 t:,9P .SSA::,., i ;_. -.
�;:., �- , , � fir, I Y1,31 1 elT�m
Rush work will require prior approval. Additional charges will apply

ANNUAL' PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Dunn WQ Permit Number: WQ0006101
WWTP Name: City of Dunn WTP _ NPDES Number: 03-43-010
Monitoring Period:
From 07/01/2017
To 12/31/2017
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp)
Alt. 4/D (No Prior Test)
Alt. 2B (Alk Treatment)
Alt. 5/Process to Further Reduce Pathogens
Alt. 3/C (Prior Testing)
Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed Ulass
A or Ulass ti coin fete the ronowmQ monnorm
aata: -
Parameter
Allowable Level in Sludge
Pathogen _ Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum' Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6th
MPN
-
MPN/9
Coliform
power per gram
of total solids
-
<69900,
<69900
<70900
CFU/g
0
Based on
grab
9222D -
CFU
Land App.
MF
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Mt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake) _
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable) _
Option/Alt: 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed x
CERTIFICATION STATEMENT (please check the appropriate -statement)
- "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that -the pathogen requirements in 40 CFR 503.32/15ANCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have ,
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Pam Gibbons. WastewaterTreatment Plant Supervisor
P=er e and Title (type or print) �� I 6
Signature of Preparer* Date
Land Applier Name and Title•(if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Cameron Testing Services, Inc.
Laboratory Report
NCDENR4654
NC PHHS #37799
US EPA #NC01918
Clte�it
Synagro�E'�`I'SiE�zoj
171455
Proecfi
Dunn WTP
Yes
Sample Information
'� ?
C u2ljfp ed ,
."
C. Hayes
08/31/17 Receteed M. Sims hate
08I31/17
,
Analyses and Results
171455 01
171455 01
a
b
C
d
e
f
9
sludge Gr Fee. Collform-S
<70400
cFU19
70400 08/31 /17 SB 9222D - MF
<6990,.0
CFur9
69900
<70900
cruig
70900
<$9904
CFu1g
69900
<69900
CFu19
69900
<69900
cFu1g
69900
<69900
Mig
69900
Geomeari
<69900
Sludge Gr TS {%)
1.42%
0.01 09/01/17 ERP 2540 G -TS
1.43%
0.01
1.41 %
0.01
1.43%
0.01
1.43%
0.01
1,43%
0.01
1.43%
0-01
Report
Review /0S//`7
Lab Director Date
219 S. Steele Str,
Sanford NC 27330
919-208-4240
Chris a,Camerontesting.coni

r-�
i
219 S. Steele Str. Cameron Testing Services, Inc.
Sanford, NC 27330
Phone: [phone] NC WW/GW Cert. #A654 NC PHHS Cert r 37799 US EPA NC0191a
Chain of Custody
Paqe of
company:
----Y�
Email:
r °tea., sy7��ru,�
_ CTS lab use only
y__�`T��._
Contact:
)�
Phone•
Sample Temp Pro'.
(C)
_
Add'r:_ess. (City,
_
-Fax:
-
Arrive:
State, Zip)
Notes:
—
—
Due: .
Project:
p —
Regulatory Rush
(Y/N) (YIN)
Collected:
Mama:
Signature:
Sample Information
Number of bottles
Requested Analysis
Sam le
ID
;✓
Cro7 15 � �
`m
Preservatives: (U)npreserved, H(C)i,
GTS Lab
p
d 1— 00 �
�
� m E 0 o. N
o
H2(8)04, H(N)03, (Na)Thiosulfate, Na(0)H,
ID
0
—
`` m v0 - r a
a,
Other (X), Indicate
Le
17
Ftelin0 u!shed:
Received Y
"47
Date/Time
--------
7
Rush work will require prior approval. Additional charges will apply

Agricultural Lime Application Log
Year: 2617
Project: City of Dunn
Field
(state -county -site -field code) .
Soil pH
Lime Requirement
(from soil analysis)
To
Applied
Date Applied
NC-CU-34-01
5.2
1.2 T/Ac.
Ordered*
NC-CU-34-02
6.4
O.OT/Ac.
NC-CU-34-03
4.9
0.9 T/Ac.
Ordered*
NC-CU-34-04
5.8
0.1 T/Ac.
Ordered*
NC-CU-34-05
5.6
0.3 T/Ac.
Ordered*
NC-HA-08-08
6.4
0 T/Ac.
NC-HA-08-09
6.3
0 T/Ac.
NC-HA-201-04
6.1
0 T/Ac.
*Lime to be spread once field, bond
itions improve

t
Page 1 of 2
Report Number: 17-363-0507
Account Number: 46789
Send To: Synagro Central LLC/ Dunn
Mary Brewer
284 Boger Road
Mocksville NC 27028
Waypoint
ANALYTICAL
"Every acre... Every year."Tm
SOIL ANALYSIS REPORT
r.e a _r....::. nainotoneQ n�+. of P nr?• n1/n9/9n9R
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Grower: Harold Eldridge
Analytical Method(s): SMP Buffer pH Mehlich 3 Loss On Ignition Water pH
OM
WN
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium.
pH
Acidity
C.E.0
Sample ID
Field ID
Lab
Number
%
Rate
Soil
Class
lbs/A
M3
ppm Rate
ppm Rate
ppm Rate
K
ppm Rate
Mg
ppm Rate
Ca
ppm Rate
. Na
ppm Rate
Soil
PH
Buffer
Index
H
megl100g
meq/100g
CU 34 1
CU 34 3
09888
09889
5.0
H
4.8
M
137
137
198 VH
NC = 165
250. VH
NC = 208
55 VL
NC = 28
171 VH
NC = 87
181 H
95 M
881 L
488 L
_T
5.2
4.9
6.62
6.64
3.1
2.9
9.2
6.6
MIN
MIN
CU 34 4
09890
2.9
M
M
102
239 VH
NC = 199
103 H
NC =
123 VH
408 L
5.8
6.85
0.8
4.1
lvll�N53
MIN
CU 34 5
Sample ID
Field ID
09891 4.1 124 219 VH -
M MIN NC = 182
Percent Base Saturation Nitrate Sulfur
Zinc
.66L
NC = 34
Manganese
123 H 593 M
Iron Copper
Boron
5.6 6.80 1.3
Soluble salts
SS
ms/cm Rate
5.5
K
Mg
%
Ca
%
Na
%
H
%
NO3 N
ppm Rate
S
ppm Rate
Zn
ppm Rate
Mn'
ppm Rate
Fe
ppm "Rate
. Cu
ppm Rate
B
ppm Rate
CU 34 1
1.5
16.4
47.9
33.7
CU 34 3
6.6
12.0
37.0
43.9
CU 34 4
6A
25.0
49.8
19.5
CU 34 5 _73.1
18.E
53.9
23.6
Values.oh this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per minion), iosrrA I nll
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm'(milll=mhos per centimeter), meq/100g maximum of thirty days after testing.
'H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble . Analysis prepared by: Waypoint Analytical Virginia, Inc.
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
by: Paµric
Pauric McGroary

Page 2 of 2
Report Number: 17-363-0507
Account Number: 46789 7621 Whitepine Road, Richmond, VA 23237
Waypoi nt." Main 804-743-9401 ° Fax [phone]
Send To: Synagro Central LLC/ Dunn ANALYTICAL www.waypointanalytical.com
Mary Brewer "Every acre... Every year.",A+ Grower: Harold Eldridge
284 Boger Road
Mocksville .NC 27028
Date Received: 12/29/2017
Date Of Reoort: 01/02/2018 SOIL FERTILITY RECOMMENDATIONS
Nitrogen
Phosphate
Potash
Magnesium
Sulfur -
Zinc
Manganese
Iron
Copper
Boron
Sample ID
Intended Crop
Yield Goal
Lime
N
P205
K20
Mg
S
Zn
Mn
Fe
Cu
B
Field ID
Tons/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
CU 34 1
Adjust pH to 6.0
0
2.5
0
CU343
Adjust pH to 6.0
0
2.5
"
0
CU 344
Adjust pH to 6.0
0
1.3
0
CU345
Adjust pH to 6.0
0
1.8
0
Comments:
Sample(s) : CU 34 3 Crop: Adjust pH to 6.5
-Apply dolomitic lime to raise pH and improve the magnesium level.
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." y�
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Pauric McGroary

Lime Recommendation Calculation
Using A&L.Soil Report
Soil pH 5.2
Target pH 6.0
Acidity 3.1
Lime Recommendation 1.2 tons per acre
Soil pH 5.2
Target pH 6.5
Acidity 12.0
Lime Recommendation 7.5 tons per acre

Lime Recommendation Calculation
Using A&L Soil Report
Soil pH
4.9
Target pH
6.0
Acidity
2.1
Lime Recommendation 0.9 tons per. acre
Soil pH
5.2
Target pH
6.5
Acidity
12.0 .
Lime Recommendation 7.5 tons per acre

Lime Recommendation Calculation
Using-A&L Soil.,Report
Soil pH
5.8
Target pH
6.0
Acidity
0.8
Lime Recommendation 0.1 tons per acre
Soil pH
5.2
Target pH
6.5
Acidity
12:0
Lime Recommendation 7.5.. tons per acre

Lime Recommendation Calculation
Using A&L Soil Report
Soil pH
5.6
Target pH
6.0
Acidity
1.3
Lime Recommendation.
0.3 tons per acre.
Soil pH
5.2
Target pH
6.5
Acidity
12.0
Lime Recommendation . 7.5 tons per acre

Page 1 of 1
Report Number: 18-036-0705
Account Number:46789
Send To: Synagro Central LLC/ Dunn
Mary Brewer
284 Boger Road
Mocksville NC 27028
Waypoint
ANALYTICAL
'Every acre... Every year."Tm
Farm ID/Name: CU-34
SOIL ANALYSIS REPORT
Date Received: 02/05/2018 Date Of Analvsis: 02/06/2018 Date Of Report: 02/07/2018
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 a Fax [phone]
www.waypointanalytical.com
Grower: Harold Eldridge
Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
OM
WN
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
%
Soil
M3
K
Mg
Ca
Na
Soil
Buffer
H
Field ID
Number
Rate
Class
Ibs/A
pprn Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
PH
Index
meq/100g
meq/100g
2
02652
3.0
103
260 VH
157 VH
157 VH
579 M
29 L
6.4
0.5
5.2
M
NC = 217
NC = 80
I MIN
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
soluble Salts
Sample ID
K
Mg
Ca
Na
H
NO, N
S
Zn
Mn
Fe
Cu
B
SS
Field ID
%
%
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ms/cm Rate
2
7.7
25.2
55.7
2.4
9.6
26 H
10.2 VH
9 L
262 VH
3.7 VH
0.6 M
0.1 VL
NC=54
NC=255.0
NC=56
NC=185.0
Values on this report represent the plant available nutrients in the
soil. Rating after each value: VL (Very Low), L (Low), M (Medium),
H (High), VH (Very High). ENR - Estimated Nitrogen Release.
C.E.C. - Cation Exchange Capacity.
Date Received: 02/05/2018
Date Of Rennrt. n2/n7/2018
Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
(pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum or thirty days after testing.
(milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: Waypoint Analytical Virginia, Inc.
Salts ms/cm x 640 = ppm.
SOIL FERTILITY RECOMMENDATIONS
6,W m° Nr
by: ppuri�
Pauric McGroary
Nitrogen
Phosphate
Potash
Magnesium
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Sample ID
Intended Crop
Yield Goal
Lime
N
P205
K20
Mg
S
Zn
Mn
Fe
Cu
B
Field ID
Tons/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
2
Adjust pH to 6.0
0
0.0
0
3
0
Comments:
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made."
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.

NCDA&CS Agronomic Division Phone: [phone] Website: www.neagr.gov/agronomi/
Report No. FY17-SLO14805
Predictive
- Client
- Chad Hayes
Advisor:
Harold Dixon
rGS,GllLTURF,u,A
C0
273 Pete Strickland Rd
PO Box 849
'I I Soil Report
Mehlich-3 Extraction
Cerro Gordo, NC 28430
Coats, NC 27521
Pti�'c
Sampled County : Harnett
1. Links to Helpful Information
tmn
Sampled: 11/09/2016
eD •�^
Received: 11/14/2016
Farm: HA-08
Completed: 12/06/2016
Client ID: 464046
Advisor ID: 358541
Sample ID: 08-08
Recommendations:
- Lime
Nutrients (lb/acre)
More
Crop
(tons/acre) N P205
K20 Mg S
Mn
Zn
Cu B
Information
Lime History:
1 -Small Grain (SG)
0.0 80-100 0
110 25 0
0
0
0 0
Note: 3
2-
Test Results [units - W/V in g/crrr3; CEC and Na in meq/100 carp; NO3-N in mglclo]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1 Ca% Mg%
S-1 Mn4 Mn-All Mn-AI2
Zn-1
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
0.32 1.37 6.6 88 0.8 6.4
367 17 82 5
34 126 80
245
245.
113 0.1 2
Sample ID: 08-09
Recommendations:
Lime
Nutrients (Iblacre)
More
Crop
(tons/acre) N P205
K20 Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Bermuda hay/past., M
0.0 180-220 0
170 0 0
0
0
0 0
Note: 12
2-
Test Results [units - W/V in g/crrP; CEC and Na in meq/100 cm3; NO3-N in mg/dO]:
Soil Class:
Mineral
HM% W/V . CEC BS% Ac pH
P-1 K-I _ Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2
Zn-1.
Zn-AI
Cu-I Na ESP
SS -I NO3-N
0.41 1.31 10.6 86 1.4 6.3
620 28 78 . - 7
46 148 101
565
565
276. 0.1 1
North Carolina
Tobacco Trust Fund Commission
Reprogramming of the laboratory -information -management system that makes this report possible is
being funded through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone] Website:
Chad Hayes
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000-sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rat(
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-1 and-P-1 values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs; SS-1 levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you.cannot find
the exact fertilizer grade recommended on the report, visit www•ncacir.aov/apronomi/obpart4.hnd information that
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizei
ort No. FY17-SLO14805
Page 2 of 2
Report Abbreviations
Ac
exchangeable.acidity
B
boron
BS%
% CEC occupied by basic cations
Ca%
% CEC occupied by calcium
GEC
cation exchange capacity
Cu-1
copper index
ESP
exchangeable sodium percent
HM%
percent humic matter
K-1
potassium index
K20
potash
Mg%
% CEC occupied by magnesium
MIN
mineral soil class
Mn
manganese
Mn-All
Mn-availability index for crop 1
Mn-AI2
Mn-availability index for crop 2
Mn-I
manganese index
M-O
mineral -organic soil class
N
Na
NO3-N
ORG
pH
P-1
P206
S-1
Test Results SS -I
W/V
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI
Zn-I
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-Al, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncapr.gov/agronomi/uvrst.htm
nitrogen
sodium
nitrate nitrogen
organic soil class
current soil pH
phosphorus index
phosphate
sulfur index
soluble salt index
weight per volume
zinc availability index
zinc index

Pagel of 2
Report Number: 17-090-0561
Account Number:46460
Send To: Synagro Central LLC/Harnett
Mary Brewer
County
284 Boger Road
Mocksville NC 27028
Waypoint
ANALYTICAL
"Every acre ... Every year. ".M
Date Received: 03/31/2017 Date Of Analysis: 04/03/2017
Farm ID: Ha-201
SOIL ANALYSIS REPORT
Date Of Report: 04/03/2017
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 a Fax [phone]
www.waypointanalytical.com
Grower: Hamilton/ Harnett
Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
OM
WN
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Field ID
Lab
Number
%
Rate.
Soil
Class
Ibs/A
M3
ppm Rate -
ppm Rate
ppm Rate
K
ppm Rate
Mg
ppm Rate
Ca
ppm Rate
Na
ppm Rate
Soil
pH
Buffer
Index
H
meq/100g
meq/100g
1
10526
1.8
L
79
80 H,
NC=67
151 VH
NC=77
141 H
554 M
10
VL
6.3
0.5
4.9
MIN
2
10527
2.5
L
93
46 M
NC = 38
155- VH
NC = 79
169 VH
540 M
10
VL
6.1
0.7
5.2
MIN
3
10528
1.9
L
82
58 H
NC = 48
132 VH
NC = 68
125 H
483 IVl
11
VL
6.1
0.6
4.4
MIN
4
10529
2.9
M
100
46 M
NC = 38
116 M
NC = 59
159 'VH
579 M
16
VL
6.1
0.7
5.3
MIN
Sample ID
Field ID
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
K
ova
Mg
%
Ca
%
Na
%
H
%
NO, N
ppm Rate
S
ppm Rate
Zn
ppm Rate
Mn
ppm Rate
Fe
ppm Rate
Cu
ppm Rate
B
ppm Rate
SS
ms/cm Rate
1
7.9
24.0
56.5
0.9
10.2
3 VL
NC=6
13.8 VH
NC=345.0
166 VH
NC=1038
200 VH
1.5 M
NC=75.0
0.4
L
0.09
VL
2
7.6
27.1
51.9
0.8
13.5
4 VL
NC=8
9.5 VH
NC=237.5
214 VH
NC=1338
152 VH
2.0 H
NC=100.0
0.3
VL
0.09
VL
3
7.7
23.7
54.9
1.1
13.6
3 VL
NC=6
8.9 VH
NC=222.5
166 VH
NC=1038
171 VH
1.2 M
NC=60.0
0.3
VL
0.08
VL
4
5.6
25.0
54.6
1.3
13.2
13 L
NC=27
3.8 H
NC=95.0
163 VH
NC=1019
150 VH
1.7 H
NC=65.0
0.4
L
0.12
VL
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g " maximum of thirty days after testing. by. Pwzc me 604,-r
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: WaypointAnalytical Virginia; Inc.
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
Pauric McGroary

Page 2 of 2
Report Number: 17-090-0561
Account Number: 46460
Send To: Synagro Central LLC/ Harnett
Mary Brewer
County
284 Boger Road
Mocksville NC 27028
Date Received: 03/31/2017
Date Of Report: 04/03/2017
WaypointANALYTICAL
"Every acre... Every year. "TM
Farm ID: Ha-201
SOIL FERTILITY RECOMMENDATIONS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Grower: Hamilton/ Harnett
Sample ID
Yield Goal
Lime
Nitrogen
Phosphate
Potash
Magnesium
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Field ID
Intended Crop
Tons/A
N
P205
K20
Mg
S
Zn
Mn
Fe
Cu
B
Ib/A
Ib/A
ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
1
Adjust pH to 6.0
0
0.0
0
0
0
1
Soybeans
45
0.0
15
30
33
0
18
0
0
0
0
0.5
2
Soybeans
45
0.8
15
30
33
0
17
0
0
0
0
1.0
2
Adjust pH to 6.0
0
0.0
0
0
0
3
-
Soybeans
45J_
0.8
15
30
33
0
18
0
0
0
0
1.0
3
Adjust pH to 6.0
0
0.0
0
0
0
�,4
Adjust pH to 6.0
0
0.0
0
0
0
4
—T-45
Soybeans
0.8
15
30
70
0
7
2.1
0
0
0
0.5
comments:
Sample(s) : 2,3,4 Crop: Soybeans
Boron recommendations are on a broadcast basis.
For best results apply 20-40# P205 and 20-30# K20 as a side placement application. Subtract from the amount recommended above then broadcast the rest if any.
Sample(s) : 4 Crop: Soybeans
Zinc should be side banded near the crops to be effective. Apply foliar for non -row crops.
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made."
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the - pcwR, or /4Nr
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Pauric McGroary