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Home My WebLink AboutNC0085359_Report_20241002ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 August 28, 2024 Keith Purgason Union County Public Works 8299 Kensington Drive Waxhaw, NC 28173 RE: Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Dear Keith Purgason: Enclosed are the analytical results for sample(s) received by the laboratory on August 07, 2024. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace National - Mt. Juliet • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte • Pace Analytical Services - Peachtree Corners, GA If you have any questions concerning this report, please feel free to contact me. Sincerely, Stephanie Knott stephanie.knott@pacelabs.com 704-977-0981 Project Manager Enclosures cc: Wyatt Howell, Union County Public Works Kevin Merrill REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 133 Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Pace Analytical Services National 12065 Lebanon Road, Mt. Juliet, TN 37122 Alabama Certification #: 40660 Alaska Certification 17-026 Arizona Certification #: AZ0612 Arkansas Certification #: 88-0469 California Certification #: 2932 Canada Certification #: 1461.01 Colorado Certification #: TN00003 Connecticut Certification #: PH-0197 DOD Certification: #1461.01 EPA# TN00003 Florida Certification #: E87487 Georgia DW Certification #: 923 Georgia Certification: NELAP Idaho Certification #: TN00003 Illinois Certification #: 200008 Indiana Certification #: C-TN-01 Iowa Certification #: 364 Kansas Certification #: E-10277 Kentucky UST Certification #: 16 Kentucky Certification #: 90010 Louisiana Certification #: A130792 Louisiana DW Certification #: LA180010 Maine Certification #: TN0002 Maryland Certification #: 324 Massachusetts Certification #: M-TNO03 Michigan Certification #: 9958 Minnesota Certification #: 047-999-395 Mississippi Certification #: TN00003 Missouri Certification #: 340 Montana Certification M CERT0086 Nebraska Certification #: NE-OS-15-05 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 CERTIFICATIONS Nevada Certification #: TN-03-2002-34 New Hampshire Certification #: 2975 New Jersey Certification #: TNO02 New Mexico DW Certification New York Certification #: 11742 North Carolina Aquatic Toxicity Certification #: 41 North Carolina Drinking Water Certification #: 21704 North Carolina Environmental Certificate #: 375 North Dakota Certification #: R-140 Ohio VAP Certification #: CL0069 Oklahoma Certification #: 9915 Oregon Certification #: TN200002 Pennsylvania Certification #: 68-02979 Rhode Island Certification #: LA000356 South Carolina Certification #: 84004 South Dakota Certification Tennessee DW/Chem/Micro Certification #: 2006 Texas Certification #: T 104704245-17-14 Texas Mold Certification #: LAB0152 USDA Soil Permit #: P330-15-00234 Utah Certification #: TN00003 Virginia Certification #: VT2006 Vermont Dept. of Health: ID# VT-2006 Virginia Certification #: 460132 Washington Certification #: C847 West Virginia Certification #: 233 Wisconsin Certification #: 998093910 Wyoming UST Certification #: via A21-A 2926.01 A21-A-ISO 17025 Certification #: 1461.01 A21-A-ISO 17025 Certification #: 1461.02 AIHA-LAP/LLC EMLAP Certification #:100789 South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 Virginia/VELAP Certification #: 460221 South Carolina Laboratory ID: 99030 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 Pace Analytical Services Peachtree Corners 110 Technology Pkwy, Peachtree Corners, GA 30092 North Carolina Certification #: 381 Florida DOH Certification #: E87315 South Carolina Certification #: 98011001 Georgia DW Inorganics Certification #: 812 Virginia Certification #: 460204 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: UC12-SEMI-AN & PPA-8/7-2024 92746299 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92746299003 UC12-INF EPA608.3 SEM 30 PASI-C EPA 200.7 Rev 4.4 1994 DBB1 1 PASI-A EPA 200.8 Rev 5.4 1994 CRW 13 PASI-A SM 2320B-2011 SMS 1 PASI-A SM 2540C-2015 AGM 1 PASI-A SM 2540D-2015 CMW1 1 PASI-A SM 521OB-2016 KPE 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 4 PASI-A EPA 350.1 Rev 2.0 1993 NCF 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 365.1 Rev 2.0 1993 Zip 1 PASI-A EPA420.4 Rev 1.0 1993 ARJ 1 PASI-A SM 5220D-2011 MDW 1 PASI-A 92746299004 UC12-INF EPA625.1 ICO 61 PASI-C EPA 624.1 SAS 37 PASI-C EPA 1664E MAB, MSJ 2 PAN SM 4500-CN-E-2016 AMB1 1 PASI-A 92746299007 UC12-EFF EPA608.3 SEM 30 PASI-C EPA 200.7 Rev 4.4 1994 DBB1 1 PASI-A EPA 200.8 Rev 5.4 1994 KRL 13 PASI-A EPA 625.1 ICO 61 PASI-C SM 2320B-2011 SMS 1 PASI-A SM 2540C-2015 AGM 1 PASI-A SM 2540D-2015 CMW1 1 PASI-A SM 521OB-2016 KPE 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 4 PASI-A EPA 350.1 Rev 2.0 1993 NCF 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 365.1 Rev 2.0 1993 Zip 1 PASI-A EPA420.4 Rev 1.0 1993 ARJ 1 PASI-A SM 5220D-2011 MDW 1 PASI-A 92746299008 UC12-EFF EPA624.1 SAS 37 PASI-C EPA 1664E MAB, MSJ 2 PAN SM 4500-CN-E-2016 AMB1 1 PASI-A 92746299009 UC12-FCE EPA 200.8 Rev 5.4 1994 CRW 13 PASI-A EPA 245.1 Rev 3.0 1994 KML 1 PASI-A SM 2540D-2015 CMW1 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Lab ID Sample ID Method Analysts Analytes Reported Laboratory SM 521OB-2016 KPE 1 PASI-A EPA 350.1 Rev 2.0 1993 NCF 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 CEM 1 PASI-A EPA 365.1 Rev 2.0 1993 Zip 1 PASI-A SM 5220D-2011 MDW 1 PASI-A 92746299010 UC12-FCE SM 4500-CN-E-2016 AMB1 1 PASI-A 92746299011 UC12-MLSS EPA608.3 SEM 30 PASI-C EPA 200.8 Rev 5.4 1994 CRW, KRL 13 PASI-A EPA 245.1 Rev 3.0 1994 KML 1 PASI-A EPA 625.1 ICO 61 PASI-C EPA 160.4 / SM2540B-2015 CMW1 2 PASI-A EPA 300.0 Rev 2.1 1993 CDC 4 PASI-A EPA 350.1 Rev 2.0 1993 NCF 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 365.1 Rev 2.0 1993 Zip 1 PASI-A 92746299012 UC12-MLSS EPA624.1 SAS 37 PASI-C SM 4500-CN-E-2016 AMB1 1 PASI-A 92746299013 UC12-RAS EPA 200.8 Rev 5.4 1994 CRW, KRL 13 PASI-A EPA 245.1 Rev 3.0 1994 KML 1 PASI-A EPA 160.4 / SM2540B-2015 CMW1 2 PASI-A EPA 350.1 Rev 2.0 1993 NCF 1 PASI-A EPA 365.1 Rev 2.0 1993 Zip 1 PASI-A SM 5220D-2011 MDW 1 PASI-A 92746299014 UC12-RAS SM 4500-CN-E-2016 AMB1 1 PASI-A 92746299015 UC12-WAS EPA 200.8 Rev 5.4 1994 CRW, KRL 13 PASI-A EPA 245.1 Rev 3.0 1994 KML 1 PASI-A EPA 160.4 / SM2540B-2015 CMW1 2 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 CEM 1 PASI-A EPA 365.1 Rev 2.0 1993 Zip 1 PASI-A 92746299016 UC12-WAS SM 4500-CN-E-2016 AMB1 1 PASI-A 92746299017 UC12-INFDIST EPA 200.8 Rev 5.4 1994 CRW, KRL 12 PASI-A EPA 245.1 Rev 3.0 1994 KML 1 PASI-A EPA 160.4 / SM2540B-2015 CMW1 2 PASI-A SM 521OB-2016 KPE 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 4 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: UC12-SEMI-AN & PPA-8/7-2024 92746299 Analytes Lab ID Sample ID Method Analysts Reported Laboratory EPA 350.1 Rev 2.0 1993 NCF 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 365.1 Rev 2.0 1993 Zip 1 PASI-A SM 5220D-2011 MDW 1 PASI-A 92746299018 UC12-INFDIST EPA608.3 SEM 30 PASI-C EPA 625.1 ICO 61 PASI-C EPA 624.1 SAS 37 PASI-C SM 4500-CN-E-2016 AMB1 1 PASI-A 92746299019 UC12-BFP-1-CAKE EPA 7471B VB 1 PASI-GA EPA 601OD DBB1 13 PASI-A SM 2540G-2011 CHC 1 PASI-C SW-846 KDF 1 PASI-C EPA 160.4 / SM2540B-2011 CMW1 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 MFO 3 PASI-A EPA 365.1 Rev 2.0 1993 NCF 1 PASI-A 92746299020 UC12-BFP-1-CAKE SW-846 CHC 1 PASI-C SM 4500-CN-E-2016 EGC 1 PASI-A 92746299021 UC12-BFP-1-FILT EPA 200.8 Rev 5.4 1994 CRW 13 PASI-A EPA 245.1 Rev 3.0 1994 KML 1 PASI-A SM 2540D-2015 AGM 1 PASI-A SM 521OB-2016 KPE 1 PASI-A EPA 350.1 Rev 2.0 1993 NCF 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 CEM 1 PASI-A EPA 365.1 Rev 2.0 1993 Zip 1 PASI-A SM 4500-CN-E-2016 AMB1 1 PASI-A SM 5220D-2011 MDW 1 PASI-A 92746299022 UC12-1_2 AER EPA 200.8 Rev 5.4 1994 CRW, KRL 13 PASI-A EPA 245.1 Rev 3.0 1994 KML 1 PASI-A EPA 160.4 / SM2540B-2015 CMW1 2 PASI-A 92746299023 UC12-1 2 AER SM 4500-CN-E-2016 AMB1 1 PASI-A 92746299024 UC12-5_6 AER EPA 200.8 Rev 5.4 1994 CRW, KRL 13 PASI-A EPA 245.1 Rev 3.0 1994 KML 1 PASI-A EPA 160.4 / SM2540B-2015 CMW1 2 PASI-A 92746299025 UC12-5 6AER SM4500-CN-E-2016 AMB1 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Analytes Lab ID Sample ID Method Analysts Reported Laboratory PAN = Pace National - Mt. Juliet PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte PASI-GA = Pace Analytical Services - Peachtree Corners, GA REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-INF Lab ID: 92746299003 Collected: 08/07/24 06:11 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 608 PCB Pest RVE Analytical Method: EPA 608.3 Preparation Method: EPA 608.3 Pace Analytical Services - Charlotte Aldrin ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 309-00-2 alpha-BHC ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 319-84-6 beta-BHC ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 319-85-7 delta-BHC ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 319-86-8 gamma-BHC (Lindane) ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 58-89-9 Chlordane (Technical) ND ug/L 0.83 10 08/08/24 00:59 08/08/24 13:37 57-74-9 alpha -Chlordane ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 5103-71-9 gamma -Chlordane ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 5103-74-2 4,4'-DDD ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 72-54-8 4,4'-DDE ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 72-55-9 4,4'-DDT ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 50-29-3 Dieldrin ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 60-57-1 Endosulfan I ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 959-98-8 Endosulfan II ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 33213-65-9 Endosulfan sulfate ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 1031-07-8 Endrin ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 72-20-8 Endrin aldehyde ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 7421-93-4 Heptachlor ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 76-44-8 L1 Heptachlor epoxide ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 1024-57-3 PCB-1016 (Aroclor 1016) ND ug/L 0.83 10 08/08/24 00:59 08/08/24 13:37 12674-11-2 PCB-1221 (Aroclor 1221) ND ug/L 0.83 10 08/08/24 00:59 08/08/24 13:37 11104-28-2 PCB-1232 (Aroclor 1232) ND ug/L 0.83 10 08/08/24 00:59 08/08/24 13:37 11141-16-5 PCB-1242 (Aroclor 1242) ND ug/L 0.83 10 08/08/24 00:59 08/08/24 13:37 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 0.83 10 08/08/24 00:59 08/08/24 13:37 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 0.83 10 08/08/24 00:59 08/08/24 13:37 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 0.83 10 08/08/24 00:59 08/08/24 13:37 11096-82-5 PCB, Total ND ug/L 0.83 10 08/08/24 00:59 08/08/24 13:37 1336-36-3 Toxaphene ND ug/L 0.83 10 08/08/24 00:59 08/08/24 13:37 8001-35-2 Surrogates Tetrachloro-m-xylene (S) 0 % 10-137 10 08/08/24 00:59 08/08/24 13:37 877-09-8 D3,S4 Decachlorobiphenyl (S) 0 % 19-200 10 08/08/24 00:59 08/08/24 13:37 2051-24-3 S4 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services -Asheville Hardness, Total(SM 2340B) 115000 ug/L 662 1 08/15/24 13:00 08/19/24 11:44 200.8 MET ICPMS Analytical Method: EPA 200.8 Rev 5.4 1994 Preparation Method: EPA 200.8 Rev 5.4 1994 Pace Analytical Services -Asheville Antimony ND ug/L 1.0 1 08/08/2412:30 08/09/2416:43 7440-36-0 Arsenic ND ug/L 1.0 1 08/08/2412:30 08/09/2416:43 7440-38-2 Beryllium ND ug/L 0.10 1 08/08/2412:30 08/09/2416:43 7440-41-7 Cadmium ND ug/L 0.10 1 08/08/2412:30 08/09/2416:43 7440-43-9 Chromium 1.1 ug/L 1.0 1 08/08/2412:30 08/09/2416:43 7440-47-3 Copper 21.0 ug/L 2.0 1 08/08/2412:30 08/09/2416:43 7440-50-8 Lead ND ug/L 1.0 1 08/08/2412:30 08/09/2416:43 7439-92-1 Molybdenum 1.1 ug/L 1.0 1 08/08/2412:30 08/09/2416:43 7439-98-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-INF Lab ID: 92746299003 Collected: 08/07/24 06:11 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.8 MET ICPMS Nickel Selenium Silver Thallium Zinc 2320B Alkalinity Alkalinity, Total as CaCO3 2540C Total Dissolved Solids Total Dissolved Solids 2540D Total Suspended Solids Total Suspended Solids 5210B cBOD, 5 day Carbonaceous BOD, 5 day 300.0 IC anions 48hr Chloride Nitrate as N Nitrate -Nitrite (as N) Nitrite as N 350.1 Ammonia Nitrogen, Ammonia 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 365.1 Phosphorus, Total Phosphorus 420.4 Phenolics, Total Phenolics, Total Recoverable Date: 08/28/2024 09:55 AM Analytical Method: EPA 200.8 Rev 5.4 1994 Preparation Method: EPA 200.8 Rev 5.4 1994 Pace Analytical Services -Asheville 2.2 ug/L 1.0 1 08/08/2412:30 08/09/2416:43 7440-02-0 ND ug/L 2.0 1 08/08/2412:30 08/09/2416:43 7782-49-2 ND ug/L 0.40 1 08/08/2412:30 08/09/2416:43 7440-22-4 ND ug/L 0.20 1 08/08/2412:30 08/09/2416:43 7440-28-0 118 ug/L 10.0 1 08/08/2412:30 08/09/2416:43 7440-66-6 Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville 253 mg/L 5.0 1 08/09/2415:17 Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville 263 mg/L 25.0 1 08/13/2411:52 Analytical Method: SM 2540D-2015 Pace Analytical Services -Asheville 210 mg/L 35.7 1 08/09/2413:16 Analytical Method: SM 521OB-2016 Pace Analytical Services -Asheville 158 mg/L 2.0 1 08/08/2414:06 08/13/2416:17 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville 45.3 mg/L 1.0 1 08/07/24 22:29 16887-00-6 ND mg/L 0.10 1 08/07/24 22:29 14797-55-8 ND mg/L 0.20 1 08/07/24 22:29 7727-37-9 ND mg/L 0.10 1 08/07/24 22:29 14797-65-0 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville 37.5 mg/L 0.60 6 08/21/2416:09 7664-41-7 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services -Asheville 49.5 mg/L 5.0 10 08/26/2418:34 08/27/2410:08 7727-37-9 Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville 5.9 mg/L 0.10 2 08/22/2418:08 08/23/2410:47 7723-14-0 Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993 Pace Analytical Services -Asheville M1,R1 0.038 mg/L 0.0050 1 08/24/2412:30 08/24/2415:16 64743-03-9 M1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-INF Lab ID: 92746299003 Collected: 08/07/24 06:11 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Pace Analytical Services -Asheville Chemical Oxygen Demand 687 mg/L 25.0 1 08/27/24 04:22 08/27/24 15:28 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-INF Lab ID: 92746299004 Collected: 08/07/24 05:22 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No 625 RVE Analytical Method: EPA 625.1 Preparation Method: EPA 625.1 Pace Analytical Services - Charlotte Acenaphthene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 83-32-9 Acenaphthylene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 208-96-8 Anthracene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 120-12-7 Benzo(a)anthracene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 56-55-3 Benzo(a)pyrene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 50-32-8 Benzo(b)fluoranthene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 205-99-2 Benzo(g,h,i)perylene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 191-24-2 Benzo(k)fluoranthene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 207-08-9 4-Bromophenylphenyl ether ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 101-55-3 Butylbenzylphthalate ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 85-68-7 4-ChIoro-3-methyl phenol ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 59-50-7 bis(2-Chloroethoxy)methane ND ug/L 50.0 5 08/08/24 00:54 08/08/24 21:05 111-91-1 bis(2-Chloroethyl) ether ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 111-44-4 2-Chloronaphthalene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 91-58-7 2-Chlorophenol ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 95-57-8 4-Chlorophenylphenyl ether ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 7005-72-3 Chrysene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 218-01-9 Dibenz(a,h)anthracene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 53-70-3 1,2-Dichlorobenzene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 95-50-1 1,3-Dichlorobenzene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 541-73-1 1,4-Dichlorobenzene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 106-46-7 3,3'-Dichlorobenzidine ND ug/L 50.0 5 08/08/24 00:54 08/08/24 21:05 91-94-1 2,4-Dichlorophenol ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 120-83-2 Diethylphthalate ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 84-66-2 2,4-Dimethylphenol ND ug/L 50.0 5 08/08/24 00:54 08/08/24 21:05 105-67-9 Dimethylphthalate ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 131-11-3 Di-n-butylphthalate ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/L 50.0 5 08/08/24 00:54 08/08/24 21:05 534-52-1 2,4-Dinitrophenol ND ug/L 250 5 08/08/24 00:54 08/08/24 21:05 51-28-5 2,4-Dinitrotoluene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 121-14-2 2,6-Dinitrotoluene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 606-20-2 Di-n-octylphthalate ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 117-81-7 Fluoranthene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 206-44-0 Fluorene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 86-73-7 Hexachloro-1,3-butadiene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 87-68-3 Hexachlorobenzene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 118-74-1 Hexachlorocyclopentadiene ND ug/L 50.0 5 08/08/24 00:54 08/08/24 21:05 77-47-4 Hexachloroethane ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 193-39-5 Isophorone ND ug/L 50.0 5 08/08/24 00:54 08/08/24 21:05 78-59-1 Naphthalene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 91-20-3 Nitrobenzene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 98-95-3 2-Nitrophenol ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 88-75-5 4-Nitrophenol ND ug/L 50.0 5 08/08/24 00:54 08/08/24 21:05 100-02-7 N-Nitrosodimethylamine ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 62-75-9 REPORT OF LABORATORY ANALYSIS Qual This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-INF Lab ID: 92746299004 Collected: 08/07/24 05:22 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 625 RVE Analytical Method: EPA 625.1 Preparation Method: EPA 625.1 Pace Analytical Services - Charlotte N-Nitroso-di-n-propylamine ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 621-64-7 N-Nitrosodiphenylamine ND ug/L 50.0 5 08/08/24 00:54 08/08/24 21:05 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 108-60-1 Pentachlorophenol ND ug/L 50.0 5 08/08/24 00:54 08/08/24 21:05 87-86-5 Phenanthrene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 85-01-8 Phenol ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 108-95-2 Pyrene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 129-00-0 1,2,4-Trichlorobenzene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 120-82-1 2,4,6-TrichIorophenol ND ug/L 50.0 5 08/08/24 00:54 08/08/24 21:05 88-06-2 Surrogates Nitrobenzene-d5 (S) 18 % 10-120 5 08/08/24 00:54 08/08/24 21:05 4165-60-0 D3 2-Fluorobiphenyl (S) 22 % 15-120 5 08/08/24 00:54 08/08/24 21:05 321-60-8 Terphenyl-d14 (S) 38 % 11-131 5 08/08/24 00:54 08/08/24 21:05 1718-51-0 Phenol-d6 (S) 17 % 10-120 5 08/08/24 00:54 08/08/24 21:05 13127-88-3 2-Fluorophenol (S) 16 % 10-120 5 08/08/24 00:54 08/08/24 21:05 367-12-4 2,4,6-Tribromophenol (S) 43 % 10-137 5 08/08/24 00:54 08/08/24 21:05 118-79-6 624 Volatile Organics Acrolein Analytical Method: EPA 624.1 Pace Analytical Services - Charlotte Acrolein ND ug/L 5.0 1 08/08/24 21:00 107-02-8 Acrylonitrile ND ug/L 5.0 1 08/08/24 21:00 107-13-1 Benzene ND ug/L 1.0 1 08/08/24 21:00 71-43-2 Bromodichloromethane ND ug/L 2.0 1 08/08/24 21:00 75-27-4 Bromoform ND ug/L 2.0 1 08/08/24 21:00 75-25-2 Bromomethane ND ug/L 2.0 1 08/08/24 21:00 74-83-9 Carbon tetrachloride ND ug/L 2.0 1 08/08/24 21:00 56-23-5 Chlorobenzene ND ug/L 2.0 1 08/08/24 21:00 108-90-7 Chloroethane ND ug/L 2.0 1 08/08/24 21:00 75-00-3 2-Chloroethylvinyl ether ND ug/L 5.0 1 08/08/24 21:00 110-75-8 Chloroform ND ug/L 2.0 1 08/08/24 21:00 67-66-3 Chloromethane ND ug/L 2.0 1 08/08/24 21:00 74-87-3 Dibromochloromethane ND ug/L 2.0 1 08/08/24 21:00 124-48-1 1,2-Dichlorobenzene ND ug/L 2.0 1 08/08/24 21:00 95-50-1 1,3-Dichlorobenzene ND ug/L 2.0 1 08/08/24 21:00 541-73-1 1,4-Dichlorobenzene ND ug/L 2.0 1 08/08/24 21:00 106-46-7 1,1-Dichloroethane ND ug/L 2.0 1 08/08/24 21:00 75-34-3 1,2-Dichloroethane ND ug/L 2.0 1 08/08/24 21:00 107-06-2 1,1-Dichloroethene ND ug/L 2.0 1 08/08/24 21:00 75-35-4 cis-1,2-Dichloroethene ND ug/L 2.0 1 08/08/24 21:00 156-59-2 trans-1,2-Dichloroethene ND ug/L 2.0 1 08/08/24 21:00 156-60-5 1,2-Dichloropropane ND ug/L 2.0 1 08/08/24 21:00 78-87-5 cis-1,3-Dichloropropene ND ug/L 2.0 1 08/08/24 21:00 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 2.0 1 08/08/24 21:00 10061-02-6 Ethylbenzene ND ug/L 1.0 1 08/08/24 21:00 100-41-4 Methylene Chloride ND ug/L 2.0 1 08/08/24 21:00 75-09-2 1,1,2,2-Tetrachloroethane ND ug/L 2.0 1 08/08/24 21:00 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-INF Lab ID: 92746299004 Collected: 08/07/24 05:22 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 624 Volatile Organics Acrolein Analytical Method: EPA 624.1 Pace Analytical Services - Charlotte Tetrachloroethene ND ug/L 2.0 1 08/08/24 21:00 127-18-4 Toluene 2.8 ug/L 1.0 1 08/08/24 21:00 108-88-3 1,1,1-Trichloroethane ND ug/L 2.0 1 08/08/24 21:00 71-55-6 1,1,2-Trichloroethane ND ug/L 2.0 1 08/08/24 21:00 79-00-5 Trichloroethene ND ug/L 2.0 1 08/08/24 21:00 79-01-6 Trichlorofluoromethane ND ug/L 2.0 1 08/08/24 21:00 75-69-4 Vinyl chloride ND ug/L 2.0 1 08/08/24 21:00 75-01-4 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 08/08/24 21:00 460-00-4 Toluene-d8 (S) 100 % 70-130 1 08/08/24 21:00 2037-26-5 1,2-Dichloroethane-d4 (S) 102 % 70-130 1 08/08/24 21:00 17060-07-0 Wet Chemistry 1664B Analytical Method: EPA 1664E Preparation Method: 1664B Pace National - Mt. Juliet Oil and Grease 17.5 mg/L 5.00 1 08/19/24 01:59 08/19/24 06:43 Total Petroleum Hydrocarbons ND mg/L 5.00 1 08/19/24 01:59 08/19/24 10:37 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND mg/L 0.0080 1 08/19/2417:07 08/20/2411:26 57-12-5 Date: 08/28/2024 09:55 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 12 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-EFF Lab ID: 92746299007 Collected: 08/07/24 06:06 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 608 PCB Pest RVE Analytical Method: EPA 608.3 Preparation Method: EPA 608.3 Pace Analytical Services - Charlotte Aldrin ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 309-00-2 alpha-BHC ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 319-84-6 beta-BHC ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 319-85-7 delta-BHC ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 319-86-8 gamma-BHC (Lindane) ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 58-89-9 Chlordane (Technical) ND ug/L 0.42 1 08/09/24 16:51 08/13/24 20:56 57-74-9 alpha -Chlordane ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 5103-71-9 gamma -Chlordane ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 5103-74-2 4,4'-DDD ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 72-54-8 4,4'-DDE ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 72-55-9 4,4'-DDT ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 50-29-3 Dieldrin ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 60-57-1 Endosulfan I ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 959-98-8 Endosulfan II ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 33213-65-9 Endosulfan sulfate ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 1031-07-8 Endrin ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 72-20-8 Endrin aldehyde ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 7421-93-4 Heptachlor ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 76-44-8 Heptachlor epoxide ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 1024-57-3 PCB-1016 (Aroclor 1016) ND ug/L 0.42 1 08/09/24 16:51 08/13/24 20:56 12674-11-2 PCB-1221 (Aroclor 1221) ND ug/L 0.42 1 08/09/24 16:51 08/13/24 20:56 11104-28-2 PCB-1232 (Aroclor 1232) ND ug/L 0.42 1 08/09/24 16:51 08/13/24 20:56 11141-16-5 PCB-1242 (Aroclor 1242) ND ug/L 0.42 1 08/09/24 16:51 08/13/24 20:56 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 0.42 1 08/09/24 16:51 08/13/24 20:56 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 0.42 1 08/09/24 16:51 08/13/24 20:56 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 0.42 1 08/09/24 16:51 08/13/24 20:56 11096-82-5 PCB, Total ND ug/L 0.42 1 08/09/24 16:51 08/13/24 20:56 1336-36-3 Toxaphene ND ug/L 0.42 1 08/09/24 16:51 08/13/24 20:56 8001-35-2 Surrogates Tetrachloro-m-xylene (S) 98 % 10-137 1 08/09/24 16:51 08/13/24 20:56 877-09-8 Decachlorobiphenyl (S) 150 % 19-200 1 08/09/24 16:51 08/13/24 20:56 2051-24-3 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services -Asheville Hardness, Total(SM 2340B) 109000 ug/L 662 1 08/15/24 13:00 08/19/24 11:47 200.8 MET ICPMS Analytical Method: EPA 200.8 Rev 5.4 1994 Preparation Method: EPA 200.8 Rev 5.4 1994 Pace Analytical Services -Asheville Antimony ND ug/L 1.0 1 08/10/24 13:45 08/12/24 00:15 7440-36-0 Arsenic ND ug/L 1.0 1 08/10/24 13:45 08/12/24 00:15 7440-38-2 Beryllium ND ug/L 0.10 1 08/10/24 13:45 08/12/24 00:15 7440-41-7 Cadmium ND ug/L 0.10 1 08/10/24 13:45 08/12/24 00:15 7440-43-9 Chromium ND ug/L 1.0 1 08/10/24 13:45 08/12/24 00:15 7440-47-3 Copper ND ug/L 2.0 1 08/10/24 13:45 08/12/24 00:15 7440-50-8 Lead ND ug/L 1.0 1 08/10/24 13:45 08/12/24 00:15 7439-92-1 Molybdenum ND ug/L 1.0 1 08/10/24 13:45 08/12/24 00:15 7439-98-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-EFF Lab ID: 92746299007 Collected: 08/07/24 06:06 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No 200.8 MET ICPMS Analytical Method: EPA 200.8 Rev 5.4 1994 Preparation Method: EPA 200.8 Rev 5.4 1994 Pace Analytical Services -Asheville Nickel 1.0 ug/L 1.0 1 08/10/24 13:45 08/12/24 00:15 7440-02-0 Selenium ND ug/L 2.0 1 08/10/24 13:45 08/12/24 00:15 7782-49-2 Silver ND ug/L 0.40 1 08/10/24 13:45 08/12/24 00:15 7440-22-4 Thallium ND ug/L 0.20 1 08/10/24 13:45 08/12/24 00:15 7440-28-0 Zinc 25.0 ug/L 10.0 1 08/10/24 13:45 08/12/24 00:15 7440-66-6 625 RVE Analytical Method: EPA 625.1 Preparation Method: EPA 625.1 Pace Analytical Services - Charlotte Acenaphthene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 83-32-9 Acenaphthylene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 208-96-8 Anthracene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 120-12-7 Benzo(a)anthracene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 56-55-3 Benzo(a)pyrene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 50-32-8 Benzo(b)fluoranthene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 205-99-2 Benzo(g,h,i)perylene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 191-24-2 Benzo(k)fluoranthene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 207-08-9 4-Bromophenylphenyl ether ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 101-55-3 Butylbenzylphthalate ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 85-68-7 4-ChIoro-3-methyl phenol ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 59-50-7 bis(2-Chloroethoxy)methane ND ug/L 8.3 1 08/08/24 00:54 08/08/24 21:30 111-91-1 bis(2-Chloroethyl) ether ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 111-44-4 2-Chloronaphthalene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 91-58-7 2-Chlorophenol ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 95-57-8 4-Chlorophenylphenyl ether ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 7005-72-3 Chrysene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 218-01-9 Dibenz(a,h)anthracene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 53-70-3 1,2-Dichlorobenzene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 95-50-1 1,3-Dichlorobenzene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 541-73-1 1,4-Dichlorobenzene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 106-46-7 3,3'-Dichlorobenzidine ND ug/L 8.3 1 08/08/24 00:54 08/08/24 21:30 91-94-1 2,4-Dichlorophenol ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 120-83-2 Diethylphthalate ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 84-66-2 2,4-Dimethylphenol ND ug/L 8.3 1 08/08/24 00:54 08/08/24 21:30 105-67-9 Dimethylphthalate ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 131-11-3 Di-n-butylphthalate ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/L 8.3 1 08/08/24 00:54 08/08/24 21:30 534-52-1 2,4-Dinitrophenol ND ug/L 41.7 1 08/08/24 00:54 08/08/24 21:30 51-28-5 2,4-Dinitrotoluene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 121-14-2 2,6-Dinitrotoluene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 606-20-2 Di-n-octylphthalate ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 117-81-7 Fluoranthene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 206-44-0 Fluorene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 86-73-7 Hexachloro-1,3-butadiene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 87-68-3 Hexachlorobenzene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 118-74-1 Hexachlorocyclopentadiene ND ug/L 8.3 1 08/08/24 00:54 08/08/24 21:30 77-47-4 REPORT OF LABORATORY ANALYSIS Qual This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-EFF Lab ID: 92746299007 Collected: 08/07/24 06:06 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 625 RVE Analytical Method: EPA 625.1 Preparation Method: EPA 625.1 Pace Analytical Services - Charlotte Hexachloroethane ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 193-39-5 Isophorone ND ug/L 8.3 1 08/08/24 00:54 08/08/24 21:30 78-59-1 Naphthalene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 91-20-3 Nitrobenzene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 98-95-3 2-Nitrophenol ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 88-75-5 4-Nitrophenol ND ug/L 8.3 1 08/08/24 00:54 08/08/24 21:30 100-02-7 N-Nitrosodimethylamine ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 62-75-9 N-Nitroso-di-n-propylamine ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 621-64-7 N-Nitrosodiphenylamine ND ug/L 8.3 1 08/08/24 00:54 08/08/24 21:30 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 108-60-1 Pentachlorophenol ND ug/L 8.3 1 08/08/24 00:54 08/08/24 21:30 87-86-5 Phenanthrene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 85-01-8 Phenol ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 108-95-2 Pyrene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 129-00-0 1,2,4-Trichlorobenzene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 120-82-1 2,4,6-TrichIorophenol ND ug/L 8.3 1 08/08/24 00:54 08/08/24 21:30 88-06-2 Surrogates Nitrobenzene-d5 (S) 18 % 10-120 1 08/08/24 00:54 08/08/24 21:30 4165-60-0 2-Fluorobiphenyl (S) 18 % 15-120 1 08/08/24 00:54 08/08/24 21:30 321-60-8 Terphenyl-d14 (S) 37 % 11-131 1 08/08/24 00:54 08/08/24 21:30 1718-51-0 Phenol-d6 (S) 15 % 10-120 1 08/08/24 00:54 08/08/24 21:30 13127-88-3 2-Fluorophenol (S) 16 % 10-120 1 08/08/24 00:54 08/08/24 21:30 367-12-4 2,4,6-Tribromophenol (S) 40 % 10-137 1 08/08/24 00:54 08/08/24 21:30 118-79-6 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 102 mg/L 5.0 1 08/09/24 15:26 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 296 mg/L 25.0 1 08/13/24 11:52 2540D Total Suspended Solids Analytical Method: SM 2540D-2015 Pace Analytical Services -Asheville Total Suspended Solids ND mg/L 2.5 1 08/09/24 13:16 5210B cBOD, 5 day Analytical Method: SM 521OB-2016 Pace Analytical Services -Asheville Carbonaceous BOD, 5 day ND mg/L 2.0 1 08/08/24 14:06 08/13/24 16:03 300.0 IC anions 48hr Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 44.9 mg/L 1.0 1 08/07/24 22:14 16887-00-6 Nitrate as N 8.2 mg/L 0.40 4 08/08/24 01:31 14797-55-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-EFF Lab ID: 92746299007 Collected: 08/07/24 06:06 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 300.0 IC anions 48hr Nitrate -Nitrite (as N) Nitrite as N 350.1 Ammonia Nitrogen, Ammonia 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 365.1 Phosphorus, Total Phosphorus 420.4 Phenolics, Total Phenolics, Total Recoverable 5220D COD Chemical Oxygen Demand Date: 08/28/2024 09:55 AM Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville 8.2 mg/L 0.80 4 08/08/24 01:31 7727-37-9 ND mg/L 0.10 1 08/07/24 22:14 14797-65-0 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville ND mg/L 0.10 1 08/21/2416:10 7664-41-7 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services -Asheville 1.5 mg/L 0.50 1 08/26/24 18:34 08/27/24 09:07 7727-37-9 M1 Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville 0.17 mg/L 0.050 1 08/22/2418:08 08/23/2410:52 7723-14-0 Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993 Pace Analytical Services -Asheville ND mg/L 0.0050 1 08/24/2412:30 08/24/2415:21 64743-03-9 Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Pace Analytical Services -Asheville ND mg/L 25.0 1 08/27/24 04:22 08/27/24 15:29 R1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 16 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-EFF Lab ID: 92746299008 Collected: 08/07/24 06:15 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 624 Volatile Organics Acrolein Acrolein Acrylonitrile Benzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane 2-Chloroethylvinyl ether Chloroform Chloromethane Dibromochloromethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene Methylene Chloride 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Vinyl chloride Surrogates 4-Bromofluorobenzene (S) Toluene-d8 (S) 1,2-Dichloroethane-d4 (S) Wet Chemistry 1664B Oil and Grease Total Petroleum Hydrocarbons Date: 08/28/2024 09:55 AM Analytical Method: EPA 624.1 Pace Analytical Services - Charlotte ND ug/L 5.0 1 08/08/24 21:18 107-02-8 ND ug/L 5.0 1 08/08/24 21:18 107-13-1 ND ug/L 1.0 1 08/08/24 21:18 71-43-2 ND ug/L 2.0 1 08/08/24 21:18 75-27-4 ND ug/L 2.0 1 08/08/24 21:18 75-25-2 ND ug/L 2.0 1 08/08/24 21:18 74-83-9 ND ug/L 2.0 1 08/08/24 21:18 56-23-5 ND ug/L 2.0 1 08/08/24 21:18 108-90-7 ND ug/L 2.0 1 08/08/24 21:18 75-00-3 ND ug/L 5.0 1 08/08/24 21:18 110-75-8 ND ug/L 2.0 1 08/08/24 21:18 67-66-3 ND ug/L 2.0 1 08/08/24 21:18 74-87-3 ND ug/L 2.0 1 08/08/24 21:18 124-48-1 ND ug/L 2.0 1 08/08/24 21:18 95-50-1 ND ug/L 2.0 1 08/08/24 21:18 541-73-1 ND ug/L 2.0 1 08/08/24 21:18 106-46-7 ND ug/L 2.0 1 08/08/24 21:18 75-34-3 ND ug/L 2.0 1 08/08/24 21:18 107-06-2 ND ug/L 2.0 1 08/08/24 21:18 75-35-4 ND ug/L 2.0 1 08/08/24 21:18 156-59-2 ND ug/L 2.0 1 08/08/24 21:18 156-60-5 ND ug/L 2.0 1 08/08/24 21:18 78-87-5 ND ug/L 2.0 1 08/08/24 21:18 10061-01-5 ND ug/L 2.0 1 08/08/24 21:18 10061-02-6 ND ug/L 1.0 1 08/08/24 21:18 100-41-4 ND ug/L 2.0 1 08/08/24 21:18 75-09-2 ND ug/L 2.0 1 08/08/24 21:18 79-34-5 ND ug/L 2.0 1 08/08/24 21:18 127-18-4 ND ug/L 1.0 1 08/08/24 21:18 108-88-3 ND ug/L 2.0 1 08/08/24 21:18 71-55-6 ND ug/L 2.0 1 08/08/24 21:18 79-00-5 ND ug/L 2.0 1 08/08/24 21:18 79-01-6 ND ug/L 2.0 1 08/08/24 21:18 75-69-4 ND ug/L 2.0 1 08/08/24 21:18 75-01-4 99 % 70-130 1 08/08/24 21:18 460-00-4 100 % 70-130 1 08/08/24 21:18 2037-26-5 101 % 70-130 1 08/08/24 21:18 17060-07-0 Analytical Method: EPA 1664E Preparation Method: 1664B Pace National - Mt. Juliet ND mg/L 5.00 1 08/19/24 01:59 08/19/24 06:43 ND mg/L 5.00 1 08/19/24 01:59 08/19/24 10:37 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 17 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-EFF Lab ID: 92746299008 Collected: 08/07/24 06:15 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND mg/L 0.0080 1 08/19/2417:07 08/20/2411:27 57-12-5 Date: 08/28/2024 09:55 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 18 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-FCE Lab ID: 92746299009 Collected: 08/07/24 06:09 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.8 MET ICPMS Analytical Method: EPA 200.8 Rev 5.4 1994 Preparation Method: EPA 200.8 Rev 5.4 1994 Pace Analytical Services -Asheville Antimony ND ug/L 1.0 1 08/08/2416:00 08/09/2413:54 7440-36-0 Arsenic ND ug/L 1.0 1 08/08/2416:00 08/09/2413:54 7440-38-2 Beryllium ND ug/L 0.10 1 08/08/2416:00 08/09/2413:54 7440-41-7 Cadmium ND ug/L 0.10 1 08/08/2416:00 08/09/2413:54 7440-43-9 Chromium ND ug/L 1.0 1 08/08/2416:00 08/09/2413:54 7440-47-3 Copper 2.1 ug/L 2.0 1 08/08/2416:00 08/09/2413:54 7440-50-8 Lead ND ug/L 1.0 1 08/08/2416:00 08/09/2413:54 7439-92-1 Molybdenum ND ug/L 1.0 1 08/08/2416:00 08/09/2413:54 7439-98-7 Nickel 1.1 ug/L 1.0 1 08/08/2416:00 08/09/2413:54 7440-02-0 Selenium ND ug/L 2.0 1 08/08/2416:00 08/09/2413:54 7782-49-2 Silver ND ug/L 0.40 1 08/08/2416:00 08/09/2413:54 7440-22-4 Thallium ND ug/L 0.20 1 08/08/2416:00 08/09/2413:54 7440-28-0 Zinc 28.2 ug/L 10.0 1 08/08/2416:00 08/09/2413:54 7440-66-6 245.1 Mercury Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994 Pace Analytical Services -Asheville Mercury ND ug/L 0.20 1 08/09/2419:27 08/12/2416:14 7439-97-6 2540D Total Suspended Solids Analytical Method: SM 2540D-2015 Pace Analytical Services -Asheville Total Suspended Solids 4.0 mg/L 2.5 1 08/09/24 13:17 5210B cBOD, 5 day Analytical Method: SM 521OB-2016 Pace Analytical Services -Asheville Carbonaceous BOD, 5 day ND mg/L 2.0 1 08/08/24 14:06 08/13/24 16:08 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia ND mg/L 0.10 1 08/21/24 16:11 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Kjeldahl, Total 2.0 mg/L 0.50 1 08/26/24 18:34 08/27/24 09:10 7727-37-9 353.2 Nitrogen, NO2/NO3 pres. Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, NO2 plus NO3 10.8 mg/L 0.40 10 08/22/24 03:28 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 0.32 mg/L 0.050 1 08/22/2418:08 08/23/2410:53 7723-14-0 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Pace Analytical Services -Asheville Chemical Oxygen Demand ND mg/L 25.0 1 08/27/24 04:22 08/27/24 15:29 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 19 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-FCE Lab ID: 92746299010 Collected: 08/07/24 06:05 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND mg/L 0.0080 1 08/19/2417:07 08/20/2411:28 57-12-5 Date: 08/28/2024 09:55 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 20 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-MLSS Lab ID: 92746299011 Collected: 08/07/24 04:09 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 608 PCB Pest RVE Analytical Method: EPA 608.3 Preparation Method: EPA 608.3 Pace Analytical Services - Charlotte Aldrin ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 309-00-2 alpha-BHC ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 319-84-6 beta-BHC ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 319-85-7 delta-BHC ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 319-86-8 gamma-BHC (Lindane) ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 58-89-9 Chlordane (Technical) ND ug/L 5.0 5 08/09/24 16:51 08/13/24 21:09 57-74-9 alpha -Chlordane ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 5103-71-9 gamma -Chlordane ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 5103-74-2 4,4'-DDD ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 72-54-8 4,4'-DDE ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 72-55-9 4,4'-DDT ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 50-29-3 Dieldrin ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 60-57-1 Endosulfan I ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 959-98-8 Endosulfan II ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 33213-65-9 Endosulfan sulfate ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 1031-07-8 Endrin ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 72-20-8 Endrin aldehyde ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 7421-93-4 Heptachlor ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 76-44-8 Heptachlor epoxide ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 1024-57-3 PCB-1016 (Aroclor 1016) ND ug/L 5.0 5 08/09/24 16:51 08/13/24 21:09 12674-11-2 PCB-1221 (Aroclor 1221) ND ug/L 5.0 5 08/09/24 16:51 08/13/24 21:09 11104-28-2 PCB-1232 (Aroclor 1232) ND ug/L 5.0 5 08/09/24 16:51 08/13/24 21:09 11141-16-5 PCB-1242 (Aroclor 1242) ND ug/L 5.0 5 08/09/24 16:51 08/13/24 21:09 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 5.0 5 08/09/24 16:51 08/13/24 21:09 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 5.0 5 08/09/24 16:51 08/13/24 21:09 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 5.0 5 08/09/24 16:51 08/13/24 21:09 11096-82-5 PCB, Total ND ug/L 5.0 5 08/09/24 16:51 08/13/24 21:09 1336-36-3 Toxaphene ND ug/L 5.0 5 08/09/24 16:51 08/13/24 21:09 8001-35-2 Surrogates Tetrachloro-m-xylene (S) 21 % 10-137 5 08/09/24 16:51 08/13/24 21:09 877-09-8 D3 Decachlorobiphenyl (S) 156 % 19-200 5 08/09/24 16:51 08/13/24 21:09 2051-24-3 200.8 MET ICPMS Analytical Method: EPA 200.8 Rev 5.4 1994 Preparation Method: EPA 200.8 Rev 5.4 1994 Pace Analytical Services -Asheville Antimony 2.0 ug/L 1.0 1 08/08/24 16:00 08/11/24 21:33 7440-36-0 Arsenic 8.3 ug/L 1.0 1 08/08/24 16:00 08/11/24 21:33 7440-38-2 Beryllium 1.0 ug/L 0.10 1 08/08/24 16:00 08/11/24 21:33 7440-41-7 Cadmium 1.6 ug/L 0.10 1 08/08/24 16:00 08/11/24 21:33 7440-43-9 Chromium 19.1 ug/L 1.0 1 08/08/24 16:00 08/11/24 21:33 7440-47-3 Copper 443 ug/L 10.0 5 08/08/24 16:00 08/09/2414:16 7440-50-8 M1 Lead 9.1 ug/L 1.0 1 08/08/24 16:00 08/11/24 21:33 7439-92-1 Molybdenum 9.0 ug/L 1.0 1 08/08/24 16:00 08/11/24 21:33 7439-98-7 Nickel 27.9 ug/L 1.0 1 08/08/24 16:00 08/11/24 21:33 7440-02-0 Selenium 6.8 ug/L 2.0 1 08/08/24 16:00 08/11/24 21:33 7782-49-2 Silver 3.5 ug/L 0.40 1 08/08/24 16:00 08/11/24 21:33 7440-22-4 Thallium ND ug/L 0.20 1 08/08/24 16:00 08/11/24 21:33 7440-28-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 21 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-MLSS Lab ID: 92746299011 Collected: 08/07/24 04:09 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.8 MET ICPMS Analytical Method: EPA 200.8 Rev 5.4 1994 Preparation Method: EPA 200.8 Rev 5.4 1994 Pace Analytical Services -Asheville Zinc 1720 ug/L 200 20 08/08/24 16:00 08/11/24 21:37 7440-66-6 M1 245.1 Mercury Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994 Pace Analytical Services -Asheville Mercury ND ug/L 0.20 1 08/09/2419:27 08/12/2416:22 7439-97-6 625 RVE Analytical Method: EPA 625.1 Preparation Method: EPA 625.1 Pace Analytical Services - Charlotte Acenaphthene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 83-32-9 Acenaphthylene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 208-96-8 Anthracene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 120-12-7 Benzo(a)anthracene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 56-55-3 Benzo(a)pyrene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 50-32-8 Benzo(b)fluoranthene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 205-99-2 Benzo(g,h,i)perylene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 191-24-2 Benzo(k)fluoranthene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 207-08-9 4-Bromophenylphenyl ether ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 101-55-3 Butylbenzylphthalate ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 85-68-7 4-Chloro-3-methyl phenol ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 59-50-7 bis(2-Chloroethoxy)methane ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:19 111-91-1 bis(2-Chloroethyl) ether ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 111-44-4 2-Chloronaphthalene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 91-58-7 2-Chlorophenol ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 95-57-8 4-Chlorophenylphenyl ether ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 7005-72-3 Chrysene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 218-01-9 Dibenz(a,h)anthracene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 53-70-3 1,2-Dichlorobenzene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 95-50-1 1,3-Dichlorobenzene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 541-73-1 1,4-Dichlorobenzene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 106-46-7 3,3'-Dichlorobenzidine ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:19 91-94-1 2,4-Dichlorophenol ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 120-83-2 Diethylphthalate ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 84-66-2 2,4-Dimethylphenol ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:19 105-67-9 Dimethylphthalate ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 131-11-3 Di-n-butylphthalate ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:19 534-52-1 2,4-Dinitrophenol ND ug/L 167 4 08/08/24 00:54 08/09/24 16:19 51-28-5 2,4-Dinitrotoluene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 121-14-2 2,6-Dinitrotoluene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 606-20-2 Di-n-octylphthalate ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 117-81-7 Fluoranthene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 206-44-0 Fluorene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 86-73-7 Hexachloro-1,3-butadiene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 87-68-3 Hexachlorobenzene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 118-74-1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 22 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-MLSS Lab ID: 92746299011 Collected: 08/07/24 04:09 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 625 RVE Analytical Method: EPA 625.1 Preparation Method: EPA 625.1 Pace Analytical Services - Charlotte Hexachlorocyclopentadiene ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:19 77-47-4 Hexachloroethane ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 193-39-5 Isophorone ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:19 78-59-1 Naphthalene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 91-20-3 Nitrobenzene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 98-95-3 2-Nitrophenol ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 88-75-5 4-Nitrophenol ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:19 100-02-7 N-Nitrosodimethylamine ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 62-75-9 N-Nitroso-di-n-propylamine ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 621-64-7 N-Nitrosodiphenylamine ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:19 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 108-60-1 Pentachlorophenol ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:19 87-86-5 Phenanthrene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 85-01-8 Phenol ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 108-95-2 Pyrene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 129-00-0 1,2,4-Trichlorobenzene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 120-82-1 2,4,6-TrichIorophenol ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:19 88-06-2 Surrogates Nitrobenzene-d5 (S) 23 % 10-120 4 08/08/24 00:54 08/09/24 16:19 4165-60-0 D3 2-Fluorobiphenyl (S) 19 % 15-120 4 08/08/24 00:54 08/09/24 16:19 321-60-8 Terphenyl-d14 (S) 40 % 11-131 4 08/08/24 00:54 08/09/24 16:19 1718-51-0 Phenol-d6 (S) 17 % 10-120 4 08/08/24 00:54 08/09/24 16:19 13127-88-3 2-Fluorophenol (S) 16 % 10-120 4 08/08/24 00:54 08/09/24 16:19 367-12-4 2,4,6-Tribromophenol (S) 31 % 10-137 4 08/08/24 00:54 08/09/24 16:19 118-79-6 2540D TSS/TVSS Analytical Method: EPA 160.4 / SM2540B-2015 Pace Analytical Services -Asheville Total Suspended Solids 3340 mg/L 250 1 08/13/24 21:28 Volatile Suspended Solids 2760 mg/L 250 1 08/13/24 21:28 300.0 IC anions 48hr Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 45.3 mg/L 1.0 1 08/07/24 22:00 16887-00-6 Nitrate as N 4.7 mg/L 0.20 2 08/08/24 01:03 14797-55-8 Nitrate -Nitrite (as N) 4.7 mg/L 0.40 2 08/08/24 01:03 7727-37-9 Nitrite as N ND mg/L 0.10 1 08/07/24 22:00 14797-65-0 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia 0.85 mg/L 0.10 1 08/21/24 16:13 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Kjeldahl, Total 234 mg/L 25.0 5 08/26/24 18:34 08/27/24 10:12 7727-37-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 23 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-MLSS Lab ID: 92746299011 Collected: 08/07/24 04:09 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 84.3 mg/L 1.0 20 08/22/2418:08 08/23/2410:55 7723-14-0 Date: 08/28/2024 09:55 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 24 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-MLSS Lab ID: 92746299012 Collected: 08/07/24 04:19 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 624 Volatile Organics Acrolein Acrolein Acrylonitrile Benzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane 2-Chloroethylvinyl ether Chloroform Chloromethane Dibromochloromethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene Methylene Chloride 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Vinyl chloride Surrogates 4-Bromofluorobenzene (S) Toluene-d8 (S) 1,2-Dichloroethane-d4 (S) 450OCNE Cyanide, Total Cyanide Date: 08/28/2024 09:55 AM Analytical Method: EPA 624.1 Pace Analytical Services - Charlotte ND ug/L 5.0 1 08/08/24 21:36 107-02-8 ND ug/L 5.0 1 08/08/24 21:36 107-13-1 ND ug/L 1.0 1 08/08/24 21:36 71-43-2 ND ug/L 2.0 1 08/08/24 21:36 75-27-4 ND ug/L 2.0 1 08/08/24 21:36 75-25-2 ND ug/L 2.0 1 08/08/24 21:36 74-83-9 ND ug/L 2.0 1 08/08/24 21:36 56-23-5 ND ug/L 2.0 1 08/08/24 21:36 108-90-7 ND ug/L 2.0 1 08/08/24 21:36 75-00-3 ND ug/L 5.0 1 08/08/24 21:36 110-75-8 ND ug/L 2.0 1 08/08/24 21:36 67-66-3 ND ug/L 2.0 1 08/08/24 21:36 74-87-3 ND ug/L 2.0 1 08/08/24 21:36 124-48-1 ND ug/L 2.0 1 08/08/24 21:36 95-50-1 ND ug/L 2.0 1 08/08/24 21:36 541-73-1 ND ug/L 2.0 1 08/08/24 21:36 106-46-7 ND ug/L 2.0 1 08/08/24 21:36 75-34-3 ND ug/L 2.0 1 08/08/24 21:36 107-06-2 ND ug/L 2.0 1 08/08/24 21:36 75-35-4 ND ug/L 2.0 1 08/08/24 21:36 156-59-2 ND ug/L 2.0 1 08/08/24 21:36 156-60-5 ND ug/L 2.0 1 08/08/24 21:36 78-87-5 ND ug/L 2.0 1 08/08/24 21:36 10061-01-5 ND ug/L 2.0 1 08/08/24 21:36 10061-02-6 ND ug/L 1.0 1 08/08/24 21:36 100-41-4 ND ug/L 2.0 1 08/08/24 21:36 75-09-2 ND ug/L 2.0 1 08/08/24 21:36 79-34-5 ND ug/L 2.0 1 08/08/24 21:36 127-18-4 ND ug/L 1.0 1 08/08/24 21:36 108-88-3 ND ug/L 2.0 1 08/08/24 21:36 71-55-6 ND ug/L 2.0 1 08/08/24 21:36 79-00-5 ND ug/L 2.0 1 08/08/24 21:36 79-01-6 ND ug/L 2.0 1 08/08/24 21:36 75-69-4 ND ug/L 2.0 1 08/08/24 21:36 75-01-4 100 % 70-130 1 08/08/24 21:36 460-00-4 98 % 70-130 1 08/08/24 21:36 2037-26-5 113 % 70-130 1 08/08/24 21:36 17060-07-0 Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville ND mg/L 0.0080 1 08/19/2417:07 08/20/2411:29 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 25 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-RAS Lab ID: 92746299013 Collected: 08/07/24 03:47 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.8 MET ICPMS Analytical Method: EPA 200.8 Rev 5.4 1994 Preparation Method: EPA 200.8 Rev 5.4 1994 Pace Analytical Services -Asheville Antimony 2.7 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:04 7440-36-0 Arsenic 12.1 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:04 7440-38-2 Beryllium 1.5 ug/L 0.10 1 08/08/24 16:00 08/11/24 22:04 7440-41-7 Cadmium 2.3 ug/L 0.10 1 08/08/24 16:00 08/11/24 22:04 7440-43-9 Chromium 32.4 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:04 7440-47-3 Copper 623 ug/L 10.0 5 08/08/24 16:00 08/09/2414:32 7440-50-8 Lead 14.0 ug/L 5.0 5 08/08/24 16:00 08/09/2414:32 7439-92-1 Molybdenum 12.9 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:04 7439-98-7 Nickel 41.8 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:04 7440-02-0 Selenium 10.6 ug/L 2.0 1 08/08/24 16:00 08/11/24 22:04 7782-49-2 Silver 4.9 ug/L 0.40 1 08/08/24 16:00 08/11/24 22:04 7440-22-4 Thallium ND ug/L 1.0 5 08/08/24 16:00 08/09/2414:32 7440-28-0 Zinc 2570 ug/L 200 20 08/08/24 16:00 08/11/24 22:07 7440-66-6 245.1 Mercury Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994 Pace Analytical Services -Asheville Mercury ND ug/L 0.20 1 08/09/2419:27 08/12/2416:29 7439-97-6 2540D TSS/TVSS Analytical Method: EPA 160.4 / SM2540B-2015 Pace Analytical Services -Asheville Total Suspended Solids 5070 mg/L 250 1 08/13/24 21:28 Volatile Suspended Solids 4050 mg/L 250 1 08/13/24 21:28 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia 1.6 mg/L 0.10 1 08/21/24 16:14 7664-41-7 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 94.4 mg/L 2.0 40 08/22/2418:08 08/23/2410:56 7723-14-0 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Pace Analytical Services -Asheville Chemical Oxygen Demand 6280 mg/L 250 1 08/27/24 04:22 08/27/24 15:29 Date: 08/28/2024 09:55 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. D3 Page 26 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-RAS Lab ID: 92746299014 Collected: 08/07/24 03:44 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND mg/L 0.0080 1 08/19/2417:07 08/20/2411:29 57-12-5 Date: 08/28/2024 09:55 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 27 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-WAS Lab ID: 92746299015 Collected: 08/07/24 03:48 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.8 MET ICPMS Antimony Arsenic Beryllium Cadmium Chromium Copper Lead Molybdenum Nickel Selenium Silver Thallium Zinc 245.1 Mercury Mercury 160.4 TVS and 2540B TS Total Solids Total Volatile Solids 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 353.2 Nitrogen, NO2/NO3 pres. Nitrogen, NO2 plus NO3 365.1 Phosphorus, Total Phosphorus Date: 08/28/2024 09:55 AM Analytical Method: EPA 200.8 Rev 5.4 1994 Preparation Method: EPA 200.8 Rev 5.4 1994 Pace Analytical Services -Asheville 2.9 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:11 7440-36-0 12.0 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:11 7440-38-2 1.4 ug/L 0.10 1 08/08/24 16:00 08/11/24 22:11 7440-41-7 2.3 ug/L 0.10 1 08/08/24 16:00 08/11/24 22:11 7440-43-9 28.7 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:11 7440-47-3 627 ug/L 10.0 5 08/08/24 16:00 08/09/2414:44 7440-50-8 13.9 ug/L 5.0 5 08/08/24 16:00 08/09/2414:44 7439-92-1 12.5 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:11 7439-98-7 41.1 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:11 7440-02-0 10.7 ug/L 2.0 1 08/08/24 16:00 08/11/24 22:11 7782-49-2 5.0 ug/L 0.40 1 08/08/24 16:00 08/11/24 22:11 7440-22-4 ND ug/L 1.0 5 08/08/24 16:00 08/09/2414:44 7440-28-0 2580 ug/L 200 20 08/08/24 16:00 08/11/24 22:15 7440-66-6 Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994 Pace Analytical Services -Asheville ND ug/L 0.20 1 08/09/2419:27 08/12/2416:31 7439-97-6 Analytical Method: EPA 160.4 / SM2540B-2015 Pace Analytical Services -Asheville 5570 mg/L 250 1 08/13/2418:55 4220 mg/L 250 1 08/13/2418:55 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services -Asheville 375 mg/L 25.0 5 08/26/2418:34 08/27/2410:13 7727-37-9 Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services -Asheville 2.3 mg/L 0.040 1 08/22/24 02:22 Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville 128 mg/L 2.0 40 08/22/2418:08 08/23/2410:58 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. D3 Page 28 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-WAS Lab ID: 92746299016 Collected: 08/07/24 03:44 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND mg/L 0.0080 1 08/19/2417:07 08/20/2411:30 57-12-5 Date: 08/28/2024 09:55 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 29 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-INFDIST Lab ID: 92746299017 Collected: 08/07/24 06:25 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.8 MET ICPMS Analytical Method: EPA 200.8 Rev 5.4 1994 Preparation Method: EPA 200.8 Rev 5.4 1994 Pace Analytical Services -Asheville Antimony 1.9 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:19 7440-36-0 Arsenic 6.6 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:19 7440-38-2 Beryllium 0.78 ug/L 0.10 1 08/08/24 16:00 08/11/24 22:19 7440-41-7 Cadmium 1.3 ug/L 0.10 1 08/08/24 16:00 08/11/24 22:19 7440-43-9 Chromium 16.6 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:19 7440-47-3 Copper 359 ug/L 10.0 5 08/08/24 16:00 08/09/2414:48 7440-50-8 Lead 7.5 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:19 7439-92-1 Nickel 23.1 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:19 7440-02-0 Selenium 5.9 ug/L 2.0 1 08/08/24 16:00 08/11/24 22:19 7782-49-2 Silver 4.3 ug/L 0.40 1 08/08/24 16:00 08/11/24 22:19 7440-22-4 Thallium ND ug/L 0.20 1 08/08/24 16:00 08/11/24 22:19 7440-28-0 Zinc 1470 ug/L 200 20 08/08/24 16:00 08/11/24 22:23 7440-66-6 245.1 Mercury Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994 Pace Analytical Services -Asheville Mercury ND ug/L 0.20 1 08/09/2419:27 08/12/2416:34 7439-97-6 2540D TSS/TVSS Analytical Method: EPA 160.4 / SM2540B-2015 Pace Analytical Services -Asheville Total Suspended Solids 2940 mg/L 357 1 08/09/24 13:38 Volatile Suspended Solids 2460 mg/L 357 1 08/09/24 13:38 5210B cBOD, 5 day Analytical Method: SM 521OB-2016 Pace Analytical Services -Asheville Carbonaceous BOD, 5 day 258 mg/L 2.0 1 08/08/24 14:06 08/13/24 16:21 300.0 IC anions 48hr Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 44.8 mg/L 1.0 1 08/08/24 08:58 16887-00-6 Nitrate as N 0.44 mg/L 0.10 1 08/08/24 08:58 14797-55-8 Nitrate -Nitrite (as N) 0.44 mg/L 0.20 1 08/08/24 08:58 7727-37-9 Nitrite as N ND mg/L 0.10 1 08/08/24 08:58 14797-65-0 M1 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia 18.6 mg/L 0.50 5 08/21/24 16:16 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Kjeldahl, Total 251 mg/L 25.0 5 08/26/24 18:34 08/27/24 10:14 7727-37-9 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 78.2 mg/L 1.0 20 08/22/2418:08 08/23/2410:59 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 30 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-INFDIST Lab ID: 92746299017 Collected: 08/07/24 06:25 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Pace Analytical Services -Asheville Chemical Oxygen Demand 3490 mg/L 250 1 08/27/24 04:22 08/27/24 15:29 Date: 08/28/2024 09:55 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 31 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-INFDIST Parameters ANALYTICAL RESULTS Lab ID: 92746299018 Collected: 08/07/24 06:28 Received: 08/07/24 11:41 Matrix: Water Results Units Report Limit DF Prepared Analyzed CAS No. Qual 608 PCB Pest RVE Analytical Method: EPA 608.3 Preparation Method: EPA 608.3 Pace Analytical Services - Charlotte Aldrin ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 309-00-2 alpha-BHC ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 319-84-6 beta-BHC ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 319-85-7 delta-BHC ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 319-86-8 gamma-BHC (Lindane) ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 58-89-9 Chlordane (Technical) ND ug/L 0.50 1 08/09/24 16:51 08/13/24 21:22 57-74-9 alpha -Chlordane ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 5103-71-9 gamma -Chlordane ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 5103-74-2 4,4'-DDD ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 72-54-8 4,4'-DDE ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 72-55-9 4,4'-DDT ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 50-29-3 Dieldrin ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 60-57-1 Endosulfan I ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 959-98-8 Endosulfan II ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 33213-65-9 Endosulfan sulfate ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 1031-07-8 Endrin ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 72-20-8 Endrin aldehyde ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 7421-93-4 Heptachlor ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 76-44-8 Heptachlor epoxide ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 1024-57-3 PCB-1016 (Aroclor 1016) ND ug/L 0.50 1 08/09/24 16:51 08/13/24 21:22 12674-11-2 PCB-1221 (Aroclor 1221) ND ug/L 0.50 1 08/09/24 16:51 08/13/24 21:22 11104-28-2 PCB-1232 (Aroclor 1232) ND ug/L 0.50 1 08/09/24 16:51 08/13/24 21:22 11141-16-5 PCB-1242 (Aroclor 1242) ND ug/L 0.50 1 08/09/24 16:51 08/13/24 21:22 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 0.50 1 08/09/24 16:51 08/13/24 21:22 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 0.50 1 08/09/24 16:51 08/13/24 21:22 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 0.50 1 08/09/24 16:51 08/13/24 21:22 11096-82-5 PCB, Total ND ug/L 0.50 1 08/09/24 16:51 08/13/24 21:22 1336-36-3 Toxaphene ND ug/L 0.50 1 08/09/24 16:51 08/13/24 21:22 8001-35-2 Surrogates Tetrachloro-m-xylene (S) 42 % 10-137 1 08/09/24 16:51 08/13/24 21:22 877-09-8 Decachlorobiphenyl (S) 55 % 19-200 1 08/09/24 16:51 08/13/24 21:22 2051-24-3 625 RVE Analytical Method: EPA 625.1 Preparation Method: EPA 625.1 Pace Analytical Services - Charlotte Acenaphthene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 83-32-9 Acenaphthylene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 208-96-8 Anthracene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 120-12-7 Benzo(a)anthracene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 56-55-3 Benzo(a)pyrene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 50-32-8 Benzo(b)fluoranthene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 205-99-2 Benzo(g,h,i)perylene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 191-24-2 Benzo(k)fluoranthene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 207-08-9 4-Bromophenylphenyl ether ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 101-55-3 Butylbenzylphthalate ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 85-68-7 4-Chloro-3-methyl phenol ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 59-50-7 bis(2-Chloroethoxy)methane ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:45 111-91-1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 32 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-INFDIST Lab ID: 92746299018 Collected: 08/07/24 06:28 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 625 RVE Analytical Method: EPA 625.1 Preparation Method: EPA 625.1 Pace Analytical Services - Charlotte bis(2-Chloroethyl) ether ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 111-44-4 2-Chloronaphthalene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 91-58-7 2-Chlorophenol ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 95-57-8 4-Chlorophenylphenyl ether ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 7005-72-3 Chrysene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 218-01-9 Dibenz(a,h)anthracene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 53-70-3 1,2-Dichlorobenzene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 95-50-1 1,3-Dichlorobenzene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 541-73-1 1,4-Dichlorobenzene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 106-46-7 3,3'-Dichlorobenzidine ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:45 91-94-1 2,4-Dichlorophenol ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 120-83-2 Diethylphthalate ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 84-66-2 2,4-Dimethylphenol ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:45 105-67-9 Dimethylphthalate ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 131-11-3 Di-n-butylphthalate ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:45 534-52-1 2,4-Dinitrophenol ND ug/L 167 4 08/08/24 00:54 08/09/24 16:45 51-28-5 2,4-Dinitrotoluene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 121-14-2 2,6-Dinitrotoluene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 606-20-2 Di-n-octylphthalate ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 117-81-7 Fluoranthene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 206-44-0 Fluorene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 86-73-7 Hexachloro-1,3-butadiene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 87-68-3 Hexachlorobenzene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 118-74-1 Hexachlorocyclopentadiene ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:45 77-47-4 Hexachloroethane ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 193-39-5 Isophorone ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:45 78-59-1 Naphthalene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 91-20-3 Nitrobenzene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 98-95-3 2-Nitrophenol ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 88-75-5 4-Nitrophenol ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:45 100-02-7 N-Nitrosodimethylamine ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 62-75-9 N-Nitroso-di-n-propylamine ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 621-64-7 N-Nitrosodiphenylamine ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:45 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 108-60-1 Pentachlorophenol ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:45 87-86-5 Phenanthrene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 85-01-8 Phenol ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 108-95-2 Pyrene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 129-00-0 1,2,4-Trichlorobenzene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 120-82-1 2,4,6-TrichIorophenol ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:45 88-06-2 Surrogates Nitrobenzene-d5 (S) 20 % 10-120 4 08/08/24 00:54 08/09/24 16:45 4165-60-0 D3 2-Fluorobiphenyl (S) 18 % 15-120 4 08/08/24 00:54 08/09/24 16:45 321-60-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 33 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-INFDIST Lab ID: 92746299018 Collected: 08/07/24 06:28 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 625 RVE Surrogates Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) 624 Volatile Organics Acrolein Acrolein Acrylonitrile Benzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane 2-Chloroethylvinyl ether Chloroform Chloromethane Dibromochloromethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene Methylene Chloride 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Vinyl chloride Surrogates 4-Bromofluorobenzene (S) Toluene-d8 (S) 1,2-Dichloroethane-d4 (S) Date: 08/28/2024 09:55 AM Analytical Method: EPA 625.1 Preparation Method: EPA 625.1 Pace Analytical Services - Charlotte 37 % 15 % 14 % 32 % Analytical Method: EPA 624.1 Pace Analytical Services - Charlotte ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 1.5 ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 99 % 98 % 107 % 11-131 4 08/08/24 00:54 08/09/24 16:45 1718-51-0 10-120 4 08/08/24 00:54 08/09/24 16:45 13127-88-3 10-120 4 08/08/24 00:54 08/09/24 16:45 367-12-4 10-137 4 08/08/24 00:54 08/09/24 16:45 118-79-6 5.0 1 08/08/24 21:54 107-02-8 5.0 1 08/08/24 21:54 107-13-1 1.0 1 08/08/24 21:54 71-43-2 2.0 1 08/08/24 21:54 75-27-4 2.0 1 08/08/24 21:54 75-25-2 2.0 1 08/08/24 21:54 74-83-9 2.0 1 08/08/24 21:54 56-23-5 2.0 1 08/08/24 21:54 108-90-7 2.0 1 08/08/24 21:54 75-00-3 5.0 1 08/08/24 21:54 110-75-8 2.0 1 08/08/24 21:54 67-66-3 2.0 1 08/08/24 21:54 74-87-3 2.0 1 08/08/24 21:54 124-48-1 2.0 1 08/08/24 21:54 95-50-1 2.0 1 08/08/24 21:54 541-73-1 2.0 1 08/08/24 21:54 106-46-7 2.0 1 08/08/24 21:54 75-34-3 2.0 1 08/08/24 21:54 107-06-2 2.0 1 08/08/24 21:54 75-35-4 2.0 1 08/08/24 21:54 156-59-2 2.0 1 08/08/24 21:54 156-60-5 2.0 1 08/08/24 21:54 78-87-5 2.0 1 08/08/24 21:54 10061-01-5 2.0 1 08/08/24 21:54 10061-02-6 1.0 1 08/08/24 21:54 100-41-4 2.0 1 08/08/24 21:54 75-09-2 2.0 1 08/08/24 21:54 79-34-5 2.0 1 08/08/24 21:54 127-18-4 1.0 1 08/08/24 21:54 108-88-3 2.0 1 08/08/24 21:54 71-55-6 2.0 1 08/08/24 21:54 79-00-5 2.0 1 08/08/24 21:54 79-01-6 2.0 1 08/08/24 21:54 75-69-4 2.0 1 08/08/24 21:54 75-01-4 70-130 1 70-130 1 70-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 08/08/24 21:54 460-00-4 08/08/24 21:54 2037-26-5 08/08/24 21:54 17060-07-0 Page 34 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-INFDIST Lab ID: 92746299018 Collected: 08/07/24 06:28 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND mg/L 0.0080 1 08/19/2417:07 08/20/2411:34 57-12-5 Date: 08/28/2024 09:55 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 35 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-BFP-1-CAKE Lab ID: 92746299019 Collected: 08/07/24 03:50 Received: 08/07/24 11:41 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 7471 Mercury Analytical Method: EPA 7471 B Preparation Method: EPA 7471 B Pace Analytical Services - Peachtree Corners, GA Mercury ND mg/kg 0.047 1 08/13/24 08:30 08/13/24 12:41 7439-97-6 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3050E Pace Analytical Services -Asheville Antimony ND mg/kg 11.7 1 08/13/24 15:49 08/15/24 01:26 7440-36-0 Arsenic ND mg/kg 11.7 1 08/13/24 15:49 08/15/24 01:26 7440-38-2 Beryllium ND mg/kg 0.47 1 08/13/24 15:49 08/15/24 01:26 7440-41-7 Cadmium 0.51 mg/kg 0.47 1 08/13/24 15:49 08/15/24 01:26 7440-43-9 Chromium 9.4 mg/kg 2.3 1 08/13/24 15:49 08/15/24 01:26 7440-47-3 Copper 135 mg/kg 23.4 1 08/13/24 15:49 08/15/24 01:26 7440-50-8 Lead ND mg/kg 4.7 1 08/13/24 15:49 08/15/24 01:26 7439-92-1 Molybdenum ND mg/kg 23.4 1 08/13/24 15:49 08/15/24 01:26 7439-98-7 Nickel 9.7 mg/kg 2.3 1 08/13/24 15:49 08/15/24 01:26 7440-02-0 Selenium 5.1 mg/kg 4.7 1 08/13/24 15:49 08/15/24 01:26 7782-49-2 Silver ND mg/kg 2.3 1 08/13/24 15:49 08/15/24 01:26 7440-22-4 Thallium ND mg/kg 4.7 1 08/13/24 15:49 08/15/24 01:26 7440-28-0 Zinc 528 mg/kg 4.7 1 08/13/24 15:49 08/15/24 01:26 7440-66-6 2540G Total Percent Solids Analytical Method: SM 2540G-2011 Pace Analytical Services - Charlotte Total Solids 16.7 % 0.10 1 08/08/24 18:08 Percent Moisture Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture 83.1 % 0.10 1 08/08/24 17:54 N2 160.4 Total Volatile Solids Total Volatile Solids 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 353.2 Nitrogen, NO2/NO3 Nitrogen, NO2 plus NO3 Nitrogen, Nitrate Nitrogen, Nitrite 365.1 Phosphorus, Total Phosphorus Date: 08/28/2024 09:55 AM Analytical Method: EPA 160.4 / SM254OB-2011 Pace Analytical Services -Asheville 779000 mg/kg 10000 1 08/14/2419:59 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services -Asheville 57600 mg/kg 2050 10 08/21/24 20:08 08/22/24 09:35 7727-37-9 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services -Asheville ND mg/kg 23.3 1 08/07/24 23:07 08/08/24 01:56 ND mg/kg 23.3 1 08/07/24 23:07 08/08/24 01:56 14797-55-8 ND mg/kg 23.3 1 08/07/24 23:07 08/08/24 01:56 14797-65-0 Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville 21900 mg/kg 251 50 08/12/24 20:16 08/13/24 19:05 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 36 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-BFP-1-CAKE Lab ID: 92746299020 Collected: 08/07/24 05:10 Received: 08/07/24 11:41 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture 83.1 % 0.10 1 08/23/24 15:48 N2 4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND mg/kg 1.5 1 08/14/2415:26 08/15/2411:02 57-12-5 Date: 08/28/2024 09:55 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 37 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-BFP-1-FILT Lab ID: 92746299021 Collected: 08/07/24 05:15 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.8 MET ICPMS Analytical Method: EPA 200.8 Rev 5.4 1994 Preparation Method: EPA 200.8 Rev 5.4 1994 Pace Analytical Services -Asheville Antimony ND ug/L 1.0 1 08/08/2416:00 08/09/2414:52 7440-36-0 Arsenic ND ug/L 1.0 1 08/08/2416:00 08/09/2414:52 7440-38-2 Beryllium ND ug/L 0.10 1 08/08/2416:00 08/09/2414:52 7440-41-7 Cadmium ND ug/L 0.10 1 08/08/2416:00 08/09/2414:52 7440-43-9 Chromium ND ug/L 1.0 1 08/08/2416:00 08/09/2414:52 7440-47-3 Copper 12.7 ug/L 2.0 1 08/08/2416:00 08/09/2414:52 7440-50-8 Lead ND ug/L 1.0 1 08/08/2416:00 08/09/2414:52 7439-92-1 Molybdenum ND ug/L 1.0 1 08/08/2416:00 08/09/2414:52 7439-98-7 Nickel 2.1 ug/L 1.0 1 08/08/2416:00 08/09/2414:52 7440-02-0 Selenium ND ug/L 2.0 1 08/08/2416:00 08/09/2414:52 7782-49-2 Silver ND ug/L 0.40 1 08/08/2416:00 08/09/2414:52 7440-22-4 Thallium ND ug/L 0.20 1 08/08/2416:00 08/09/2414:52 7440-28-0 Zinc 82.0 ug/L 10.0 1 08/08/2416:00 08/09/2414:52 7440-66-6 245.1 Mercury Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994 Pace Analytical Services -Asheville Mercury ND ug/L 0.20 1 08/09/2419:27 08/12/2416:36 7439-97-6 2540D Total Suspended Solids Analytical Method: SM 2540D-2015 Pace Analytical Services -Asheville Total Suspended Solids 26.2 mg/L 12.8 1 08/11/24 13:43 5210B cBOD, 5 day Analytical Method: SM 521OB-2016 Pace Analytical Services -Asheville Carbonaceous BOD, 5 day 3.5 mg/L 2.0 1 08/08/24 14:06 08/13/24 15:54 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia 0.29 mg/L 0.10 1 08/21/24 16:17 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Kjeldahl, Total 3.7 mg/L 0.50 1 08/26/24 18:34 08/27/24 09:17 7727-37-9 353.2 Nitrogen, NO2/NO3 pres. Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, NO2 plus NO3 7.4 mg/L 0.40 10 08/22/24 03:29 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 0.93 mg/L 0.050 1 08/22/2418:08 08/23/2411:01 7723-14-0 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND mg/L 0.0080 1 08/19/2417:07 08/20/2411:35 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 38 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-BFP-1-FILT Lab ID: 92746299021 Collected: 08/07/24 05:15 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Pace Analytical Services -Asheville Chemical Oxygen Demand 49.4 mg/L 25.0 1 08/27/24 04:22 08/27/24 15:30 Date: 08/28/2024 09:55 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 39 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-1_2 AER Lab ID: 92746299022 Collected: 08/07/24 04:06 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.8 MET ICPMS Antimony Arsenic Beryllium Cadmium Chromium Copper Lead Molybdenum Nickel Selenium Silver Thallium Zinc 245.1 Mercury Mercury 2540D TSS/TVSS Total Suspended Solids Volatile Suspended Solids Date: 08/28/2024 09:55 AM Analytical Method: EPA 200.8 Rev 5.4 1994 Preparation Method: EPA 200.8 Rev 5.4 1994 Pace Analytical Services -Asheville 2.1 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:27 7440-36-0 7.7 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:27 7440-38-2 0.91 ug/L 0.10 1 08/08/24 16:00 08/11/24 22:27 7440-41-7 1.5 ug/L 0.10 1 08/08/24 16:00 08/11/24 22:27 7440-43-9 19.1 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:27 7440-47-3 398 ug/L 10.0 5 08/08/24 16:00 08/09/2414:56 7440-50-8 8.3 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:27 7439-92-1 9.2 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:27 7439-98-7 26.2 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:27 7440-02-0 6.4 ug/L 2.0 1 08/08/24 16:00 08/11/24 22:27 7782-49-2 3.6 ug/L 0.40 1 08/08/24 16:00 08/11/24 22:27 7440-22-4 ND ug/L 0.20 1 08/08/24 16:00 08/11/24 22:27 7440-28-0 1600 ug/L 200 20 08/08/24 16:00 08/11/24 22:30 7440-66-6 Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994 Pace Analytical Services -Asheville ND ug/L 0.20 1 08/09/2419:27 08/12/2416:39 7439-97-6 Analytical Method: EPA 160.4 / SM2540B-2015 Pace Analytical Services -Asheville 3300 mg/L 250 1 08/09/2413:38 2680 mg/L 250 1 08/09/2413:38 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 40 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-1_2 AER Lab ID: 92746299023 Collected: 08/07/24 04:09 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND mg/L 0.0080 1 08/19/2417:07 08/20/2412:37 57-12-5 Date: 08/28/2024 09:55 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 41 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-5_6 AER Lab ID: 92746299024 Collected: 08/07/24 04:07 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.8 MET ICPMS Antimony Arsenic Beryllium Cadmium Chromium Copper Lead Molybdenum Nickel Selenium Silver Thallium Zinc 245.1 Mercury Mercury 2540D TSS/TVSS Total Suspended Solids Volatile Suspended Solids Date: 08/28/2024 09:55 AM Analytical Method: EPA 200.8 Rev 5.4 1994 Preparation Method: EPA 200.8 Rev 5.4 1994 Pace Analytical Services -Asheville 2.2 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:34 7440-36-0 8.3 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:34 7440-38-2 0.98 ug/L 0.10 1 08/08/24 16:00 08/11/24 22:34 7440-41-7 1.7 ug/L 0.10 1 08/08/24 16:00 08/11/24 22:34 7440-43-9 19.1 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:34 7440-47-3 434 ug/L 10.0 5 08/08/24 16:00 08/09/2415:00 7440-50-8 9.9 ug/L 5.0 5 08/08/24 16:00 08/09/2415:00 7439-92-1 9.4 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:34 7439-98-7 27.5 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:34 7440-02-0 7.1 ug/L 2.0 1 08/08/24 16:00 08/11/24 22:34 7782-49-2 4.4 ug/L 0.40 1 08/08/24 16:00 08/11/24 22:34 7440-22-4 ND ug/L 1.0 5 08/08/24 16:00 08/09/2415:00 7440-28-0 1750 ug/L 200 20 08/08/24 16:00 08/11/24 22:38 7440-66-6 Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994 Pace Analytical Services -Asheville ND ug/L 0.20 1 08/09/2419:27 08/12/2416:41 7439-97-6 Analytical Method: EPA 160.4 / SM2540B-2015 Pace Analytical Services -Asheville 3560 mg/L 250 1 08/09/2413:38 2910 mg/L 250 1 08/09/2413:38 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. D3 Page 42 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 Sample: UC12-5_6 AER Lab ID: 92746299025 Collected: 08/07/24 04:09 Received: 08/07/24 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND mg/L 0.0080 1 08/19/2417:07 08/20/2412:38 57-12-5 Date: 08/28/2024 09:55 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 43 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 875058 Analysis Method: EPA 7471 B QC Batch Method: EPA 7471 B Analysis Description: 7471 Mercury Laboratory: Pace Analytical Services - Peachtree Corners, GA Associated Lab Samples: 92746299019 METHOD BLANK: 4507441 Associated Lab Samples: 92746299019 Parameter Units Mercury mg/kg LABORATORY CONTROL SAMPLE: 4507442 Parameter Units Mercury mg/kg Matrix: Solid Blank Reporting Result Limit Analyzed Qualifiers ND 0.032 08/13/2412:04 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 0.33 0.32 98 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4507490 4507491 MS MSD 92746772002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Mercury mg/kg ND 0.33 0.32 0.34 0.34 104 104 75-125 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 44 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 874602 Analysis Method: EPA 245.1 Rev 3.0 1994 QC Batch Method: EPA 245.1 Rev 3.0 1994 Analysis Description: 245.1 Mercury Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92746299009,92746299011,92746299013,92746299015,92746299017,92746299021,92746299022, 92746299024 METHOD BLANK: 4505420 Matrix: Water Associated Lab Samples: 92746299009,92746299011,92746299013,92746299015,92746299017,92746299021,92746299022, 92746299024 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Mercury ug/L ND 0.20 08/12/2415:30 LABORATORY CONTROL SAMPLE: 4505421 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ug/L 2.5 2.5 102 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4505422 4505423 MS MSD 92745740003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Mercury ug/L ND 2.5 2.5 2.5 2.6 98 103 70-130 4 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4505424 4505425 MS MSD 92746299009 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Mercury ug/L ND 2.5 2.5 2.4 2.5 97 98 70-130 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 45 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 875840 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92746299003, 92746299007 METHOD BLANK: 4511481 Matrix: Water Associated Lab Samples: 92746299003, 92746299007 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Hardness, Total(SM 2340B) ug/L ND 662 08/19/24 10:27 LABORATORY CONTROL SAMPLE: 4511482 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Hardness, Total(SM 2340B) ug/L 33100 31700 96 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4511483 4511484 MS MSD 92746236001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Hardness, Total(SM 2340B) ug/L 87.6 33100 33100 121000 131000 101 132 70-130 8 mg/L MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4511485 4511486 MS MSD 92746788001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Hardness, Total(SM 2340B) ug/L 62.0 33100 33100 92100 93100 91 94 70-130 1 mg/L Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 46 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 874203 Analysis Method: EPA 200.8 Rev 5.4 1994 QC Batch Method: EPA 200.8 Rev 5.4 1994 Analysis Description: 200.8 MET Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92746299003 METHOD BLANK: 4503451 Associated Lab Samples: 92746299003 Parameter Units Antimony ug/L Arsenic ug/L Beryllium ug/L Cadmium ug/L Chromium ug/L Copper ug/L Lead ug/L Molybdenum ug/L Nickel ug/L Selenium ug/L Silver ug/L Thallium ug/L Zinc ug/L LABORATORY CONTROL SAMPLE: 4503452 Parameter Units Antimony ug/L Arsenic ug/L Beryllium ug/L Cadmium ug/L Chromium ug/L Copper ug/L Lead ug/L Molybdenum ug/L Nickel ug/L Selenium ug/L Silver ug/L Thallium ug/L Zinc ug/L Matrix: Water Blank Result Spike Conc. 50 50 50 50 50 50 50 50 50 50 25 25 50 ND ND ND ND ND ND ND ND ND ND ND ND ND Reporting Limit Analyzed Qualifiers 1.0 08/09/2415:44 1.0 08/09/2415:44 0.10 08/09/2415:44 0.10 08/09/2415:44 1.0 08/09/2415:44 2.0 08/09/2415:44 1.0 08/09/2415:44 1.0 08/09/2415:44 1.0 08/09/2415:44 2.0 08/09/2415:44 0.40 08/09/2415:44 0.20 08/09/2415:44 10.0 08/09/2415:44 LCS Result 52.5 50.7 55.3 52.7 52.5 53.6 51.8 51.4 53.3 51.2 26.4 26.7 51.7 LCS % Rec 105 101 111 105 105 107 104 103 107 102 106 107 103 % Rec Limits 85-115 85-115 85-115 85-115 85-115 85-115 85-115 85-115 85-115 85-115 85-115 85-115 85-115 Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4503453 4503454 MS MSD 92746001002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Antimony ug/L ND 50 50 53.1 53.2 105 106 70-130 0 Arsenic ug/L 1.9 50 50 52.8 53.4 102 103 70-130 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 47 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4503453 MS 92746001002 Spike Parameter Units Result Conc. MSD Spike Conc. 4503454 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Qual Beryllium ug/L ND 50 50 54.9 54.5 110 109 70-130 1 Cadmium ug/L ND 50 50 52.0 52.3 104 104 70-130 1 Chromium ug/L 3.7 50 50 56.4 56.3 105 105 70-130 0 Copper ug/L 13.9 50 50 65.2 65.6 103 103 70-130 1 Lead ug/L ND 50 50 52.8 53.1 104 105 70-130 1 Molybdenum ug/L 83.9 50 50 135 137 103 106 70-130 1 Nickel ug/L 14.4 50 50 66.9 67.1 105 105 70-130 0 Selenium ug/L ND 50 50 50.6 50.2 101 100 70-130 1 Silver ug/L ND 25 25 26.0 26.4 104 106 70-130 1 Thallium ug/L ND 25 25 27.0 27.0 108 108 70-130 0 Zinc ug/L ND 50 50 60.0 60.6 101 102 70-130 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 48 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 874279 Analysis Method: EPA 200.8 Rev 5.4 1994 QC Batch Method: EPA 200.8 Rev 5.4 1994 Analysis Description: 200.8 MET Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92746299009,92746299011,92746299013,92746299015,92746299017,92746299021,92746299022, 92746299024 METHOD BLANK: 4503846 Matrix: Water Associated Lab Samples: 92746299009,92746299011,92746299013,92746299015,92746299017,92746299021,92746299022, 92746299024 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Antimony ug/L ND 1.0 08/09/2413:46 Arsenic ug/L ND 1.0 08/09/2413:46 Beryllium ug/L ND 0.10 08/09/2413:46 Cadmium ug/L ND 0.10 08/09/2413:46 Chromium ug/L ND 1.0 08/09/2413:46 Copper ug/L ND 2.0 08/09/2413:46 Lead ug/L ND 1.0 08/09/2413:46 Molybdenum ug/L ND 1.0 08/09/2413:46 Nickel ug/L ND 1.0 08/09/2413:46 Selenium ug/L ND 2.0 08/09/2413:46 Silver ug/L ND 0.40 08/09/2413:46 Thallium ug/L ND 0.20 08/09/2413:46 Zinc ug/L ND 10.0 08/09/2413:46 LABORATORY CONTROL SAMPLE: Parameter 4503847 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Antimony ug/L 50 52.8 106 85-115 Arsenic ug/L 50 51.2 102 85-115 Beryllium ug/L 50 52.3 105 85-115 Cadmium ug/L 50 52.0 104 85-115 Chromium ug/L 50 51.4 103 85-115 Copper ug/L 50 52.5 105 85-115 Lead ug/L 50 49.9 100 85-115 Molybdenum ug/L 50 52.5 105 85-115 Nickel ug/L 50 51.7 103 85-115 Selenium ug/L 50 51.0 102 85-115 Silver ug/L 25 26.0 104 85-115 Thallium ug/L 25 25.8 103 85-115 Zinc ug/L 50 51.6 103 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4503860 4503861 MS MSD 92746299009 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Antimony ug/L ND 50 50 54.7 53.9 108 107 70-130 2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 49 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4503860 4503861 MS MSD 92746299009 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Arsenic ug/L ND 50 50 53.1 52.1 105 104 70-130 2 Beryllium ug/L ND 50 50 54.6 54.4 109 109 70-130 0 Cadmium ug/L ND 50 50 52.5 52.4 105 105 70-130 0 Chromium ug/L ND 50 50 53.7 53.3 107 106 70-130 1 Copper ug/L 2.1 50 50 55.4 55.3 106 106 70-130 0 Lead ug/L ND 50 50 52.2 51.9 104 104 70-130 1 Molybdenum ug/L ND 50 50 54.8 53.3 108 106 70-130 3 Nickel ug/L 1.1 50 50 54.1 54.3 106 106 70-130 0 Selenium ug/L ND 50 50 51.1 50.7 102 101 70-130 1 Silver ug/L ND 25 25 26.5 26.3 106 105 70-130 1 Thallium ug/L ND 25 25 27.4 27.1 110 108 70-130 1 Zinc ug/L 28.2 50 50 79.5 77.5 103 99 70-130 3 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4503862 4503863 MS MSD 92746299011 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Antimony ug/L 2.0 50 50 39.3 38.5 75 73 70-130 2 Arsenic ug/L 8.3 50 50 58.0 57.5 99 99 70-130 1 Beryllium ug/L 1.0 50 50 52.7 51.6 103 101 70-130 2 Cadmium ug/L 1.6 50 50 53.3 52.7 104 102 70-130 1 Chromium ug/L 19.1 50 50 72.5 70.3 107 102 70-130 3 Copper ug/L 443 50 50 471 462 56 38 70-130 2 M1 Lead ug/L 9.1 50 50 57.5 57.5 97 97 70-130 0 Molybdenum ug/L 9.0 50 50 51.3 50.6 85 83 70-130 1 Nickel ug/L 27.9 50 50 81.1 80.3 107 105 70-130 1 Selenium ug/L 6.8 50 50 51.4 49.7 89 86 70-130 3 Silver ug/L 3.5 25 25 29.8 29.6 105 104 70-130 1 Thallium ug/L ND 25 25 25.1 25.2 100 100 70-130 0 Zinc ug/L 1720 50 50 1790 1770 148 110 70-130 1 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 50 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 874647 Analysis Method: EPA 200.8 Rev 5.4 1994 QC Batch Method: EPA 200.8 Rev 5.4 1994 Analysis Description: 200.8 MET Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92746299007 METHOD BLANK: 4505705 Associated Lab Samples: 92746299007 Parameter Units Antimony ug/L Arsenic ug/L Beryllium ug/L Cadmium ug/L Chromium ug/L Copper ug/L Lead ug/L Molybdenum ug/L Nickel ug/L Selenium ug/L Silver ug/L Thallium ug/L Zinc ug/L LABORATORY CONTROL SAMPLE: 4505706 Parameter Units Antimony ug/L Arsenic ug/L Beryllium ug/L Cadmium ug/L Chromium ug/L Copper ug/L Lead ug/L Molybdenum ug/L Nickel ug/L Selenium ug/L Silver ug/L Thallium ug/L Zinc ug/L Matrix: Water Blank Result Spike Conc. 50 50 50 50 50 50 50 50 50 50 25 25 50 ND ND ND ND ND ND ND ND ND ND ND ND ND Reporting Limit Analyzed Qualifiers 1.0 08/11/24 23:29 1.0 08/11/24 23:29 0.10 08/11/24 23:29 0.10 08/11/24 23:29 1.0 08/11/24 23:29 2.0 08/11/24 23:29 1.0 08/11/24 23:29 1.0 08/11/24 23:29 1.0 08/11/24 23:29 2.0 08/11/24 23:29 0.40 08/11/24 23:29 0.20 08/11/24 23:29 10.0 08/11/24 23:29 LCS Result 50.4 48.0 52.9 51.7 52.2 53.3 50.5 49.4 52.9 49.1 25.8 26.1 50.0 LCS % Rec 101 96 106 103 104 107 101 99 106 98 103 105 100 % Rec Limits 85-115 85-115 85-115 85-115 85-115 85-115 85-115 85-115 85-115 85-115 85-115 85-115 85-115 Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4505707 4505708 MS MSD 92744458002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Antimony ug/L ND 50 50 48.7 49.8 97 99 70-130 2 Arsenic ug/L ND 50 50 48.5 49.9 97 99 70-130 3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 51 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4505707 MS 92744458002 Spike Parameter Units Result Conc. MSD Spike Conc. 4505708 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Qual Beryllium ug/L ND 50 50 48.3 49.8 97 100 70-130 3 Cadmium ug/L ND 50 50 46.0 46.8 92 93 70-130 2 Chromium ug/L 1.8 50 50 53.6 54.1 103 105 70-130 1 Copper ug/L ND 50 50 53.3 49.9 106 99 70-130 7 Lead ug/L ND 50 50 50.8 51.3 102 103 70-130 1 Molybdenum ug/L ND 50 50 50.9 52.1 101 104 70-130 2 Nickel ug/L 1.2 50 50 50.3 51.0 98 100 70-130 1 Selenium ug/L ND 50 50 44.9 45.8 89 91 70-130 2 Silver ug/L ND 25 25 23.3 23.6 93 94 70-130 1 Thallium ug/L ND 25 25 26.4 26.6 105 106 70-130 1 Zinc ug/L ND 50 50 54.0 52.8 95 92 70-130 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4505709 MS 92744458004 Spike Parameter Units Result Conc. MSD Spike Conc. 4505710 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Qual Antimony ug/L 1.1 50 50 50.3 48.8 98 95 70-130 3 Arsenic ug/L 1.1 50 50 50.0 48.1 98 94 70-130 4 Beryllium ug/L ND 50 50 52.5 51.0 105 102 70-130 3 Cadmium ug/L ND 50 50 50.3 49.4 100 99 70-130 2 Chromium ug/L 2.3 50 50 53.8 52.6 103 101 70-130 2 Copper ug/L ND 50 50 53.5 52.5 104 102 70-130 2 Lead ug/L ND 50 50 50.2 49.2 100 98 70-130 2 Molybdenum ug/L 3.9 50 50 53.6 52.6 99 97 70-130 2 Nickel ug/L 2.0 50 50 53.8 52.3 104 101 70-130 3 Selenium ug/L ND 50 50 47.8 47.0 95 94 70-130 2 Silver ug/L ND 25 25 25.4 24.8 102 99 70-130 3 Thallium ug/L ND 25 25 26.0 25.5 104 102 70-130 2 Zinc ug/L 303 50 50 360 362 114 117 70-130 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 52 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 875260 Analysis Method: EPA 6010D QC Batch Method: EPA 3050E Analysis Description: 6010 MET Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92746299019 METHOD BLANK: 4508545 Associated Lab Samples: 92746299019 Parameter Units Antimony mg/kg Arsenic mg/kg Beryllium mg/kg Cadmium mg/kg Chromium mg/kg Copper mg/kg Lead mg/kg Molybdenum mg/kg Nickel mg/kg Selenium mg/kg Silver mg/kg Thallium mg/kg Zinc mg/kg LABORATORY CONTROL SAMPLE: 4508546 Parameter Units Antimony mg/kg Arsenic mg/kg Beryllium mg/kg Cadmium mg/kg Chromium mg/kg Copper mg/kg Lead mg/kg Molybdenum mg/kg Nickel mg/kg Selenium mg/kg Silver mg/kg Thallium mg/kg Zinc mg/kg Matrix: Solid Blank Result Spike Conc. 50 50 50 50 50 50 50 50 50 50 25 50 50 ND ND ND ND ND ND ND ND ND ND ND ND ND Reporting Limit Analyzed Qualifiers 2.5 08/15/24 00:53 2.5 08/15/24 00:53 0.10 08/15/24 00:53 0.10 08/15/24 00:53 0.50 08/15/24 00:53 5.0 08/15/24 00:53 1.0 08/15/24 00:53 5.0 08/15/24 00:53 0.50 08/15/24 00:53 1.0 08/15/24 00:53 0.50 08/15/24 00:53 1.0 08/15/24 00:53 1.0 08/15/24 00:53 LCS Result 51.3 50.9 48.1 50.3 49.4 50.0 49.9 52.7 49.4 50.5 25.1 51.8 50.4 LCS % Rec 103 102 96 101 99 100 100 105 99 101 101 104 101 % Rec Limits 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4508547 4508548 MS MSD 92746020001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Antimony mg/kg ND 52.9 53.3 52.9 54.8 100 102 75-125 4 Arsenic mg/kg ND 52.9 53.3 53.4 54.9 100 102 75-125 3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 53 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4508547 MS 92746020001 Spike Parameter Units Result Conc. MSD Spike Conc. 4508548 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Qual Beryllium mg/kg ND 52.9 53.3 49.6 51.7 94 97 75-125 4 Cadmium mg/kg ND 52.9 53.3 51.5 53.4 97 100 75-125 3 Chromium mg/kg ND 52.9 53.3 50.4 52.5 95 98 75-125 4 Copper mg/kg ND 52.9 53.3 54.3 56.5 100 103 75-125 4 Lead mg/kg ND 52.9 53.3 51.2 52.8 96 99 75-125 3 Molybdenum mg/kg ND 52.9 53.3 53.8 55.9 102 105 75-125 4 Nickel mg/kg ND 52.9 53.3 51.2 53.1 96 99 75-125 4 Selenium mg/kg ND 52.9 53.3 54.5 55.9 103 104 75-125 3 Silver mg/kg ND 26.5 26.7 25.9 26.6 98 100 75-125 3 Thallium mg/kg ND 52.9 53.3 52.9 54.8 100 103 75-125 4 Zinc mg/kg 8.4 52.9 53.3 60.9 59.5 99 96 75-125 2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 54 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 874338 Analysis Method: EPA 624.1 QC Batch Method: EPA 624.1 Analysis Description: 624 MSV with Acrolein Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92746299004, 92746299008, 92746299012, 92746299018 METHOD BLANK: 4504162 Matrix: Water Associated Lab Samples: 92746299004, 92746299008, 92746299012, 92746299018 Blank Reporting Parameter Units Result Limit Analyzed 1,1,1-Trichloroethane ug/L ND 2.0 08/08/24 15:18 1,1,2,2-Tetrachloroethane ug/L ND 2.0 08/08/24 15:18 1,1,2-Trichloroethane ug/L ND 2.0 08/08/24 15:18 1,1-Dichloroethane ug/L ND 2.0 08/08/24 15:18 1,1-Dichloroethene ug/L ND 2.0 08/08/24 15:18 1,2-Dichlorobenzene ug/L ND 2.0 08/08/24 15:18 1,2-Dichloroethane ug/L ND 2.0 08/08/24 15:18 1,2-Dichloropropene ug/L ND 2.0 08/08/24 15:18 1,3-Dichlorobenzene ug/L ND 2.0 08/08/24 15:18 1,4-Dichlorobenzene ug/L ND 2.0 08/08/24 15:18 2-Chloroethylvinyl ether ug/L ND 5.0 08/08/24 15:18 Acrolein ug/L ND 5.0 08/08/24 15:18 Acrylonitrile ug/L ND 5.0 08/08/24 15:18 Benzene ug/L ND 1.0 08/08/24 15:18 Bromodichloromethane ug/L ND 2.0 08/08/24 15:18 Bromoform ug/L ND 2.0 08/08/24 15:18 Bromomethane ug/L ND 2.0 08/08/24 15:18 Carbon tetrachloride ug/L ND 2.0 08/08/24 15:18 Chlorobenzene ug/L ND 2.0 08/08/24 15:18 Chloroethane ug/L ND 2.0 08/08/24 15:18 Chloroform ug/L ND 2.0 08/08/24 15:18 Chloromethane ug/L ND 2.0 08/08/24 15:18 cis-1,2-Dichloroethene ug/L ND 2.0 08/08/24 15:18 cis-1,3-Dichloropropene ug/L ND 2.0 08/08/24 15:18 Dibromochloromethane ug/L ND 2.0 08/08/24 15:18 Ethylbenzene ug/L ND 1.0 08/08/24 15:18 Methylene Chloride ug/L ND 2.0 08/08/24 15:18 Tetrachloroethene ug/L ND 2.0 08/08/24 15:18 Toluene ug/L ND 1.0 08/08/24 15:18 trans-1,2-Dichloroethene ug/L ND 2.0 08/08/24 15:18 trans- 1,3-Dichloropropene ug/L ND 2.0 08/08/24 15:18 Trichloroethene ug/L ND 2.0 08/08/24 15:18 Trichlorofluoromethane ug/L ND 2.0 08/08/24 15:18 Vinyl chloride ug/L ND 2.0 08/08/24 15:18 1,2-Dichloroethane-d4 (S) % 104 70-130 08/08/24 15:18 4-Bromofluorobenzene (S) % 101 70-130 08/08/24 15:18 Toluene-d8 (S) % 99 70-130 08/08/24 15:18 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 55 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 LABORATORY CONTROL SAMPLE: Parameter 4504163 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1-Trichloroethane ug/L 20 23.4 117 70-130 1,1,2,2-Tetrachloroethane ug/L 20 21.9 109 70-130 1,1,2-Trichloroethane ug/L 20 23.1 116 70-130 1,1-Dichloroethane ug/L 20 22.7 114 70-130 1,1-Dichloroethene ug/L 20 23.2 116 69-131 1,2-Dichlorobenzene ug/L 20 23.4 117 70-130 1,2-Dichloroethane ug/L 20 23.2 116 70-130 1,2-Dichloropropane ug/L 20 22.9 115 70-130 1,3-Dichlorobenzene ug/L 20 22.9 115 70-130 1,4-Dichlorobenzene ug/L 20 23.4 117 70-130 2-Chloroethylvinyl ether ug/L 40 48.9 122 64-133 Acrolein ug/L 100 105 105 60-140 Acrylonitrile ug/L 100 111 111 70-130 Benzene ug/L 20 22.7 114 65-135 Bromodichloromethane ug/L 20 22.6 113 70-130 Bromoform ug/L 20 22.1 111 70-130 Bromomethane ug/L 20 20.0 100 41-148 Carbon tetrachloride ug/L 20 23.7 119 70-130 Chlorobenzene ug/L 20 22.2 111 70-130 Chloroethane ug/L 20 21.3 107 41-157 Chloroform ug/L 20 22.7 113 70-130 Chloromethane ug/L 20 22.6 113 59-141 cis-1,2-Dichloroethene ug/L 20 23.2 116 70-130 cis-1,3-Dichloropropene ug/L 20 23.2 116 70-130 Dibromochloromethane ug/L 20 23.2 116 70-130 Ethylbenzene ug/L 20 22.4 112 70-130 Methylene Chloride ug/L 20 22.1 110 62-130 Tetrachloroethene ug/L 20 21.9 109 70-130 Toluene ug/L 20 22.9 115 70-130 trans-1,2-Dichloroethene ug/L 20 24.0 120 70-130 trans- 1,3-Dichloropropene ug/L 20 23.8 119 70-130 Trichloroethene ug/L 20 22.7 114 70-130 Trichlorofluoromethane ug/L 20 20.8 104 57-130 Vinyl chloride ug/L 20 21.1 106 66-140 1,2-Dichloroethane-d4 (S) % 98 70-130 4-Bromofluorobenzene (S) % 99 70-130 Toluene-d8 (S) % 100 70-130 Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4504164 4504165 MS MSD 92745711001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 1,1,1-Trichloroethane ug/L ND 20 20 20.5 21.8 102 109 70-150 6 1,1,2,2-Tetrachloroethane ug/L ND 20 20 18.0 19.7 90 99 66-144 9 1,1,2-Trichloroethane ug/L ND 20 20 19.4 19.7 97 99 70-142 2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 56 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4504164 4504165 MS MSD 92745711001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 1,1-Dichloroethane ug/L ND 20 20 21.0 21.0 105 105 67-150 0 1,1-Dichloroethene ug/L ND 20 20 21.3 21.8 107 109 64-162 2 1,2-Dichlorobenzene ug/L ND 20 20 20.5 19.9 102 99 70-142 3 1,2-Dichloroethane ug/L ND 20 20 19.7 20.8 98 104 58-145 5 1,2-Dichloropropane ug/L ND 20 20 19.9 19.8 99 99 70-144 1 1,3-Dichlorobenzene ug/L ND 20 20 19.9 20.6 100 103 70-142 3 1,4-Dichlorobenzene ug/L ND 20 20 19.7 20.0 98 100 70-140 2 2-Chloroethylvinyl ether ug/L ND 40 40 39.7 42.5 99 106 10-211 7 Acrolein ug/L ND 100 100 19.4 16.4 19 16 40-160 17 M1 Acrylonitrile ug/L ND 100 100 79.7 98.1 80 98 59-155 21 Benzene ug/L ND 20 20 20.7 21.1 104 105 70-142 2 Bromodichloromethane ug/L ND 20 20 20.1 20.4 100 102 70-139 2 Bromoform ug/L ND 20 20 18.7 19.4 93 97 64-140 4 Bromomethane ug/L ND 20 20 14.8 15.6 74 78 28-192 5 Carbon tetrachloride ug/L ND 20 20 21.1 21.3 106 106 70-140 1 Chlorobenzene ug/L ND 20 20 19.3 20.0 97 100 70-141 3 Chloroethane ug/L ND 20 20 18.4 19.7 92 99 58-191 7 Chloroform ug/L ND 20 20 19.6 19.5 92 92 70-138 0 Chloromethane ug/L ND 20 20 19.0 19.9 95 100 43-162 5 cis-1,2-Dichloroethene ug/L ND 20 20 20.1 21.1 100 105 70-143 5 cis-1,3-Dichloropropene ug/L ND 20 20 19.6 19.9 98 100 68-151 2 Dibromochloromethane ug/L ND 20 20 19.7 20.1 98 100 70-144 2 Ethylbenzene ug/L ND 20 20 19.9 20.4 99 102 70-143 3 Methylene Chloride ug/L ND 20 20 18.6 19.5 93 98 70-144 5 Tetrachloroethene ug/L ND 20 20 18.3 19.2 92 96 70-143 5 Toluene ug/L ND 20 20 20.0 20.7 100 103 69-144 3 trans-1,2-Dichloroethene ug/L ND 20 20 20.4 22.0 102 110 70-151 8 trans- 1,3-Dichloropropene ug/L ND 20 20 20.3 20.9 101 105 70-139 3 Trichloroethene ug/L ND 20 20 20.5 20.4 102 102 70-142 0 Trichlorofluoromethane ug/L ND 20 20 19.0 19.8 95 99 62-146 4 Vinyl chloride ug/L ND 20 20 18.8 19.9 94 100 61-162 6 1,2-Dichloroethane-d4 (S) % 101 100 70-130 4-Bromofluorobenzene (S) % 99 100 70-130 Toluene-d8(S) % 99 97 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 57 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 874068 Analysis Method: EPA 608.3 QC Batch Method: EPA 608.3 Analysis Description: 608 PCB Pest Red Vol Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92746299003 METHOD BLANK: 4502871 Matrix: Water Associated Lab Samples: 92746299003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 4,4'-DDD ug/L ND 0.050 08/08/24 12:16 4,4'-DDE ug/L ND 0.050 08/08/24 12:16 4,4'-DDT ug/L ND 0.050 08/08/24 12:16 Aldrin ug/L ND 0.050 08/08/24 12:16 alpha-BHC ug/L ND 0.050 08/08/24 12:16 alpha -Chlordane ug/L ND 0.050 08/08/24 12:16 beta-BHC ug/L ND 0.050 08/08/24 12:16 Chlordane (Technical) ug/L ND 0.50 08/08/24 12:16 delta-BHC ug/L ND 0.050 08/08/24 12:16 Dieldrin ug/L ND 0.050 08/08/24 12:16 Endosulfan I ug/L ND 0.050 08/08/24 12:16 Endosulfan II ug/L ND 0.050 08/08/24 12:16 Endosulfan sulfate ug/L ND 0.050 08/08/24 12:16 Endrin ug/L ND 0.050 08/08/24 12:16 Endrin aldehyde ug/L ND 0.050 08/08/24 12:16 gamma-BHC (Lindane) ug/L ND 0.050 08/08/24 12:16 gamma -Chlordane ug/L ND 0.050 08/08/24 12:16 Heptachlor ug/L ND 0.050 08/08/24 12:16 Heptachlor epoxide ug/L ND 0.050 08/08/24 12:16 PCB-1016 (Aroclor 1016) ug/L ND 0.50 08/08/24 12:16 PCB-1221 (Aroclor 1221) ug/L ND 0.50 08/08/24 12:16 PCB-1232 (Aroclor 1232) ug/L ND 0.50 08/08/24 12:16 PCB-1242 (Aroclor 1242) ug/L ND 0.50 08/08/24 12:16 PCB-1248 (Aroclor 1248) ug/L ND 0.50 08/08/24 12:16 PCB-1254 (Aroclor 1254) ug/L ND 0.50 08/08/24 12:16 PCB-1260 (Aroclor 1260) ug/L ND 0.50 08/08/24 12:16 Toxaphene ug/L ND 0.50 08/08/24 12:16 Decachlorobiphenyl (S) % 146 19-200 08/08/24 12:16 Tetrachloro-m-xylene (S) % 78 10-137 08/08/24 12:16 LABORATORY CONTROL SAMPLE: 4502872 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 4,4'-DDD ug/L 0.25 0.32 127 31-141 4,4'-DDE ug/L 0.25 0.30 120 30-145 4,4'-DDT ug/L 0.25 0.29 117 25-160 Aldrin ug/L 0.25 0.26 102 42-135 alpha-BHC ug/L 0.25 0.30 119 37-140 alpha -Chlordane ug/L 0.25 0.31 122 45-140 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 58 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 LABORATORY CONTROL SAMPLE: 4502872 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers beta-BHC ug/L 0.25 0.30 121 38-147 delta-BHC ug/L 0.25 0.27 108 19-140 Dieldrin ug/L 0.25 0.30 120 36-146 Endosulfan I ug/L 0.25 0.31 122 45-153 Endosulfan II ug/L 0.25 0.33 134 38-155 Endosulfan sulfate ug/L 0.25 0.31 125 42-144 Endrin ug/L 0.25 0.31 122 33-147 Endrin aldehyde ug/L 0.25 0.33 133 33-153 gamma-BHC (Lindane) ug/L 0.25 0.29 117 32-140 gamma -Chlordane ug/L 0.25 0.33 132 45-140 Heptachlor ug/L 0.25 0.37 149 34-140 L1 Heptachlor epoxide ug/L 0.25 0.30 120 37-142 Decachlorobiphenyl (S) % 164 19-200 Tetrachloro-m-xylene (S) % 107 10-137 LABORATORY CONTROL SAMPLE: 4502873 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers PCB-1016 (Aroclor 1016) ug/L 5 5.8 116 50-140 PCB-1260 (Aroclor 1260) ug/L 5 5.6 112 42-140 Decachlorobiphenyl (S) % 145 19-200 Tetrachloro-m-xylene (S) % 129 10-137 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4502874 4502875 MS MSD 92745876001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 4,4'-DDD ug/L ND 0.5 0.5 0.55 0.61 109 121 31-141 10 4,4'-DDE ug/L ND 0.5 0.5 0.52 0.59 105 117 30-145 11 4,4'-DDT ug/L ND 0.5 0.5 0.52 0.59 105 118 25-160 12 Aldrin ug/L ND 0.5 0.5 0.47 0.56 94 112 42-140 18 alpha-BHC ug/L ND 0.5 0.5 0.50 0.58 101 116 37-140 14 alpha -Chlordane ug/L ND 0.5 0.5 0.53 0.59 107 118 45-140 10 beta-BHC ug/L ND 0.5 0.5 0.51 0.64 102 127 21-147 21 delta-BHC ug/L ND 0.5 0.5 0.45 0.50 90 99 19-140 10 Dieldrin ug/L ND 0.5 0.5 0.51 0.56 102 112 36-146 9 Endosulfan I ug/L ND 0.5 0.5 0.53 0.59 105 118 45-153 11 Endosulfan II ug/L ND 0.5 0.5 0.58 0.65 117 130 13-174 11 Endosulfan sulfate ug/L ND 0.5 0.5 0.54 0.61 108 122 26-144 12 Endrin ug/L ND 0.5 0.5 0.54 0.60 108 120 30-147 10 Endrin aldehyde ug/L ND 0.5 0.5 0.56 0.62 112 123 10-167 10 gamma-BHC (Lindane) ug/L ND 0.5 0.5 0.50 0.62 101 125 32-140 21 gamma -Chlordane ug/L ND 0.5 0.5 0.58 0.63 116 126 45-140 9 Heptachlor ug/L ND 0.5 0.5 0.69 0.71 139 142 34-140 3 MO Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 59 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4502874 4502875 MS MSD 92745876001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Heptachlor epoxide ug/L ND 0.5 0.5 0.51 0.56 102 112 37-142 9 Decachlorobiphenyl(S) % 136 155 19-200 Tetrachloro-m-xylene (S) % 90 166 10-137 SO MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4502876 4502877 MS MSD 92745711001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual PCB-1016 (Aroclor 1016) ug/L ND 10 10 11.3 11.7 113 117 50-140 4 PCB-1260 (Aroclor 1260) ug/L ND 10 10 11.5 11.7 115 117 42-140 2 Decachlorobiphenyl(S) % 144 135 19-200 Tetrachloro-m-xylene (S) % 112 105 10-137 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 60 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 874558 Analysis Method: EPA 608.3 QC Batch Method: EPA 608.3 Analysis Description: 608 PCB Pest Red Vol Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92746299007, 92746299011, 92746299018 METHOD BLANK: 4505262 Matrix: Associated Lab Samples: 92746299007, 92746299011, 92746299018 Blank Parameter Units Result Water Reporting Limit Analyzed 4,4'-DDD ug/L ND 0.050 08/13/24 22:55 4,4'-DDE ug/L ND 0.050 08/13/24 22:55 4,4'-DDT ug/L ND 0.050 08/13/24 22:55 Aldrin ug/L ND 0.050 08/13/24 22:55 alpha-BHC ug/L ND 0.050 08/13/24 22:55 alpha -Chlordane ug/L ND 0.050 08/13/24 22:55 beta-BHC ug/L ND 0.050 08/13/24 22:55 Chlordane (Technical) ug/L ND 0.50 08/13/24 22:55 delta-BHC ug/L ND 0.050 08/13/24 22:55 Dieldrin ug/L ND 0.050 08/13/24 22:55 Endosulfan I ug/L ND 0.050 08/13/24 22:55 Endosulfan II ug/L ND 0.050 08/13/24 22:55 Endosulfan sulfate ug/L ND 0.050 08/13/24 22:55 Endrin ug/L ND 0.050 08/13/24 22:55 Endrin aldehyde ug/L ND 0.050 08/13/24 22:55 gamma-BHC (Lindane) ug/L ND 0.050 08/13/24 22:55 gamma -Chlordane ug/L ND 0.050 08/13/24 22:55 Heptachlor ug/L ND 0.050 08/13/24 22:55 Heptachlor epoxide ug/L ND 0.050 08/13/24 22:55 PCB-1016 (Aroclor 1016) ug/L ND 0.50 08/13/24 22:55 PCB-1221 (Aroclor 1221) ug/L ND 0.50 08/13/24 22:55 PCB-1232 (Aroclor 1232) ug/L ND 0.50 08/13/24 22:55 PCB-1242 (Aroclor 1242) ug/L ND 0.50 08/13/24 22:55 PCB-1248 (Aroclor 1248) ug/L ND 0.50 08/13/24 22:55 PCB-1254 (Aroclor 1254) ug/L ND 0.50 08/13/24 22:55 PCB-1260 (Aroclor 1260) ug/L ND 0.50 08/13/24 22:55 Toxaphene ug/L ND 0.50 08/13/24 22:55 Decachlorobiphenyl (S) % 100 19-200 08/13/24 22:55 Tetrachloro-m-xylene (S) % 61 10-137 08/13/24 22:55 Qualifiers LABORATORY CONTROL SAMPLE: 4505263 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 4,4'-DDD ug/L 0.25 0.14 56 31-141 4,4'-DDE ug/L 0.25 0.14 57 30-145 4,4'-DDT ug/L 0.25 0.15 61 25-160 Aldrin ug/L 0.25 0.13 51 42-135 alpha-BHC ug/L 0.25 0.15 61 37-140 alpha -Chlordane ug/L 0.25 0.17 70 45-140 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 61 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 LABORATORY CONTROL SAMPLE: Parameter 4505263 Units Spike Conc. LCS LCS Result % Rec beta-BHC ug/L 0.25 0.15 delta-BHC ug/L 0.25 0.14 Dieldrin ug/L 0.25 0.14 Endosulfan I ug/L 0.25 0.15 Endosulfan II ug/L 0.25 0.16 Endosulfan sulfate ug/L 0.25 0.14 Endrin ug/L 0.25 0.15 Endrin aldehyde ug/L 0.25 0.16 gamma-BHC (Lindane) ug/L 0.25 0.15 gamma -Chlordane ug/L 0.25 0.18 Heptachlor ug/L 0.25 0.29 Heptachlor epoxide ug/L 0.25 0.14 Decachlorobiphenyl (S) % Tetrachloro-m-xylene (S) % % Rec Limits 61 38-147 57 19-140 55 36-146 60 45-153 65 38-155 55 42-144 60 33-147 66 33-153 59 32-140 72 45-140 115 34-140 57 37-142 87 19-200 63 10-137 Qualifiers LABORATORY CONTROL SAMPLE: 4505264 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers PCB-1016 (Aroclor 1016) ug/L 5 3.9 78 50-140 PCB-1260 (Aroclor 1260) ug/L 5 2.3 47 42-140 Decachlorobiphenyl (S) % 60 19-200 Tetrachloro-m-xylene (S) % 44 10-137 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4505265 4505266 MS MSD 92746528001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 4,4'-DDD ug/L ND 0.5 0.5 0.22 .0981 44 20 31-141 4,4'-DDE ug/L ND 0.5 0.5 0.28 0.10 55 20 30-145 4,4'-DDT ug/L ND 0.5 0.5 0.22 .096J 43 19 25-160 Aldrin ug/L ND 0.5 0.5 0.24 0.12 48 25 42-140 alpha-BHC ug/L ND 0.5 0.5 0.31 0.24 61 49 37-140 alpha -Chlordane ug/L ND 0.5 0.5 0.26 0.16 52 33 45-140 beta-BHC ug/L ND 0.5 0.5 0.34 0.24 68 48 21-147 delta-BHC ug/L ND 0.5 0.5 0.27 0.21 53 42 19-140 Dieldrin ug/L ND 0.5 0.5 0.20 0.10 40 21 36-146 Endosulfan I ug/L ND 0.5 0.5 0.22 0.13 44 26 45-153 Endosulfan II ug/L ND 0.5 0.5 0.26 0.19 52 39 13-174 Endosulfan sulfate ug/L ND 0.5 0.5 0.19 0.12 39 23 26-144 Endrin ug/L ND 0.5 0.5 0.22 0.12 43 23 30-147 Endrin aldehyde ug/L ND 0.5 0.5 0.15 0.13 30 26 10-167 gamma-BHC (Lindane) ug/L ND 0.5 0.5 0.28 0.20 55 40 32-140 gamma -Chlordane ug/L ND 0.5 0.5 0.25 0.17 50 34 45-140 Heptachlor ug/L ND 0.5 0.5 0.49 0.52 98 104 34-140 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the resul REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. M1 94 M1,R1 M1 63 M1,R1 23 46 M1,R1 34 24 63 M1,R1 53 M1,R1 29 49 M1,R1 59 M1,R1 16 33 37 M1,R1 6 Page 62 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4505265 4505266 MS MSD 92746528001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Heptachlor epoxide ug/L ND 0.5 0.5 0.22 0.13 45 27 37-142 50 M1,R1 Decachlorobiphenyl (S) % 0 0 19-200 SO Tetrachloro-m-xylene (S) % 25 33 10-137 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4505267 4505268 MS MSD 92746482001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual PCB-1016 (Aroclor 1016) ug/L ND 8.3 8.3 7.0 10.2 84 122 50-140 36 PCB-1260 (Aroclor 1260) ug/L ND 8.3 8.3 5.9 4.4 71 53 42-140 29 Decachlorobiphenyl (S) % 89 61 19-200 Tetrachloro-m-xylene (S) % 80 59 10-137 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 63 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 874069 Analysis Method: EPA 625.1 QC Batch Method: EPA 625.1 Analysis Description: 625 MSS Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92746299004, 92746299007, 92746299011, 92746299018 METHOD BLANK: 4502878 Matrix: Water Associated Lab Samples: 92746299004, 92746299007, 92746299011, 92746299018 Blank Reporting Parameter Units Result Limit Analyzed 1,2,4-Trichlorobenzene ug/L ND 5.0 08/08/24 12:20 1,2-Dichlorobenzene ug/L ND 5.0 08/08/24 12:20 1,3-Dichlorobenzene ug/L ND 5.0 08/08/24 12:20 1,4-Dichlorobenzene ug/L ND 5.0 08/08/24 12:20 2,2'-Oxybis(1-chloropropane) ug/L ND 5.0 08/08/24 12:20 2,4,6-Trichlorophenol ug/L ND 10.0 08/08/24 12:20 2,4-Dichlorophenol ug/L ND 5.0 08/08/24 12:20 2,4-Dimethylphenol ug/L ND 10.0 08/08/24 12:20 2,4-Dinitrophenol ug/L ND 50.0 08/08/24 12:20 2,4-Dinitrotoluene ug/L ND 5.0 08/08/24 12:20 2,6-Dinitrotoluene ug/L ND 5.0 08/08/24 12:20 2-Chloronaphthalene ug/L ND 5.0 08/08/24 12:20 2-Chlorophenol ug/L ND 5.0 08/08/24 12:20 2-Nitrophenol ug/L ND 5.0 08/08/24 12:20 3,3'-Dichlorobenzidine ug/L ND 10.0 08/08/24 12:20 4,6-Dinitro-2-methyl phenol ug/L ND 10.0 08/08/24 12:20 4-Bromophenylphenyl ether ug/L ND 5.0 08/08/24 12:20 4-ChIoro-3-methyl phenol ug/L ND 5.0 08/08/24 12:20 4-Chlorophenylphenyl ether ug/L ND 5.0 08/08/24 12:20 4-Nitrophenol ug/L ND 10.0 08/08/24 12:20 Acenaphthene ug/L ND 5.0 08/08/24 12:20 Acenaphthylene ug/L ND 5.0 08/08/24 12:20 Anthracene ug/L ND 5.0 08/08/24 12:20 Benzo(a)anthracene ug/L ND 5.0 08/08/24 12:20 Benzo(a)pyrene ug/L ND 5.0 08/08/24 12:20 Benzo(b)fluoranthene ug/L ND 5.0 08/08/24 12:20 Benzo(g,h,i)perylene ug/L ND 5.0 08/08/24 12:20 Benzo(k)fluoranthene ug/L ND 5.0 08/08/24 12:20 bis(2-Chloroethoxy)methane ug/L ND 10.0 08/08/24 12:20 bis(2-Chloroethyl) ether ug/L ND 5.0 08/08/24 12:20 bis(2-Ethylhexyl)phthalate ug/L ND 5.0 08/08/24 12:20 Butylbenzylphthalate ug/L ND 5.0 08/08/24 12:20 Chrysene ug/L ND 5.0 08/08/24 12:20 Di-n-butylphthalate ug/L ND 5.0 08/08/24 12:20 Di-n-octylphthalate ug/L ND 5.0 08/08/24 12:20 Dibenz(a,h)anthracene ug/L ND 5.0 08/08/24 12:20 Diethylphthalate ug/L ND 5.0 08/08/24 12:20 Dimethylphthalate ug/L ND 5.0 08/08/24 12:20 Fluoranthene ug/L ND 5.0 08/08/24 12:20 Fluorene ug/L ND 5.0 08/08/24 12:20 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 64 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 METHOD BLANK: 4502878 Matrix: Water Associated Lab Samples: 92746299004, 92746299007, 92746299011, 92746299018 Blank Reporting Parameter Units Result Limit Analyzed Hexachloro-1,3-butadiene ug/L ND 5.0 08/08/24 12:20 Hexachlorobenzene ug/L ND 5.0 08/08/24 12:20 Hexachlorocyclopentadiene ug/L ND 10.0 08/08/24 12:20 Hexachloroethane ug/L ND 5.0 08/08/24 12:20 Indeno(1,2,3-cd)pyrene ug/L ND 5.0 08/08/24 12:20 Isophorone ug/L ND 10.0 08/08/24 12:20 N-Nitroso-di-n-propylamine ug/L ND 5.0 08/08/24 12:20 N-Nitrosodimethylamine ug/L ND 5.0 08/08/24 12:20 N-Nitrosodiphenylamine ug/L ND 10.0 08/08/24 12:20 Naphthalene ug/L ND 5.0 08/08/24 12:20 Nitrobenzene ug/L ND 5.0 08/08/24 12:20 Pentachlorophenol ug/L ND 10.0 08/08/24 12:20 Phenanthrene ug/L ND 5.0 08/08/24 12:20 Phenol ug/L ND 5.0 08/08/24 12:20 Pyrene ug/L ND 5.0 08/08/24 12:20 2,4,6-Tribromophenol (S) % 83 10-137 08/08/24 12:20 2-Fluorobiphenyl (S) % 46 15-120 08/08/24 12:20 2-Fluorophenol(S) % 50 10-120 08/08/24 12:20 Nitrobenzene-d5 (S) % 59 10-120 08/08/24 12:20 Phenol-d6 (S) % 40 10-120 08/08/24 12:20 Terphenyl-d14 (S) % 75 11-131 08/08/24 12:20 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 4502879 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,2,4-Trichlorobenzene ug/L 50 33.2 66 44-142 1,2-Dichlorobenzene ug/L 50 31.5 63 32-129 1,3-Dichlorobenzene ug/L 50 30.8 62 1-172 1,4-Dichlorobenzene ug/L 50 31.0 62 20-124 2,2'-Oxybis(1-chloropropane) ug/L 50 50.9 102 36-166 2,4,6-Trichlorophenol ug/L 50 48.9 98 37-144 2,4-Dichlorophenol ug/L 50 44.5 89 1-191 2,4-Dimethylphenol ug/L 50 51.9 104 32-119 2,4-Dinitrophenol ug/L 250 304 122 1-181 2,4-Dinitrotoluene ug/L 50 52.3 105 39-139 2,6-Dinitrotoluene ug/L 50 49.5 99 50-158 2-Chloronaphthalene ug/L 50 41.4 83 60-118 2-Chlorophenol ug/L 50 43.0 86 23-134 2-Nitrophenol ug/L 50 49.4 99 29-182 3,3'-Dichlorobenzidine ug/L 100 100 100 1-262 4,6-Dinitro-2-methyl phenol ug/L 100 120 120 1-181 4-Bromophenylphenyl ether ug/L 50 50.5 101 53-127 4-Chloro-3-methylphenol ug/L 100 101 101 22-147 4-Chlorophenylphenyl ether ug/L 50 45.4 91 25-158 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 65 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 LABORATORY CONTROL SAMPLE: Parameter 4502879 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 4-Nitrophenol ug/L 250 162 65 1-132 Acenaphthene ug/L 50 44.6 89 47-145 Acenaphthylene ug/L 50 46.9 94 33-145 Anthracene ug/L 50 49.1 98 1-166 Benzo(a)anthracene ug/L 50 51.3 103 33-143 Benzo(a)pyrene ug/L 50 50.7 101 17-163 Benzo(b)fluoranthene ug/L 50 51.6 103 24-159 Benzo(g,h,i)perylene ug/L 50 53.4 107 1-219 Benzo(k)fluoranthene ug/L 50 49.6 99 11-162 bis(2-Chloroethoxy)methane ug/L 50 49.3 99 33-184 bis(2-Chloroethyl) ether ug/L 50 48.9 98 12-158 bis(2-Ethylhexyl)phthalate ug/L 50 54.0 108 8-158 Butylbenzylphthalate ug/L 50 57.5 115 1-152 Chrysene ug/L 50 48.9 98 17-168 Di-n-butylphthalate ug/L 50 50.4 101 1-118 Di-n-octylphthalate ug/L 50 57.5 115 4-146 Dibenz(a,h)anthracene ug/L 50 54.0 108 1-227 Diethylphthalate ug/L 50 48.1 96 1-114 Dimethylphthalate ug/L 50 48.8 98 1-112 Fluoranthene ug/L 50 48.3 97 26-137 Fluorene ug/L 50 46.3 93 59-121 Hexachloro-1,3-butadiene ug/L 50 31.1 62 24-116 Hexachlorobenzene ug/L 50 49.9 100 1-152 Hexachlorocyclopentadiene ug/L 50 36.5 73 25-150 Hexachloroethane ug/L 50 28.7 57 40-113 Indeno(1,2,3-cd)pyrene ug/L 50 52.2 104 1-171 Isophorone ug/L 50 49.6 99 21-196 N-Nitroso-di-n-propylamine ug/L 50 48.2 96 1-230 N-Nitrosodimethylamine ug/L 50 38.8 78 25-150 N-Nitrosodiphenylamine ug/L 50 48.6 97 25-150 Naphthalene ug/L 50 38.1 76 21-133 Nitrobenzene ug/L 50 44.9 90 35-180 Pentachlorophenol ug/L 100 117 117 14-176 Phenanthrene ug/L 50 49.1 98 54-120 Phenol ug/L 50 34.0 68 5-112 Pyrene ug/L 50 51.9 104 52-115 2,4,6-Tribromophenol (S) % 123 10-137 2-Fluorobiphenyl (S) % 86 15-120 2-Fluorophenol(S) % 71 10-120 Nitrobenzene-d5 (S) % 90 10-120 Phenol-d6 (S) % 56 10-120 Terphenyl-d14 (S) % 98 11-131 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 66 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4502880 4502881 MS MSD 35896202001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 1,2,4-Trichlorobenzene ug/L 1.71-1 100 100 41.1 39.9 41 40 44-142 3 M1 1,2-Dichlorobenzene ug/L 1.81-1 100 100 30.5 32.5 30 32 32-129 6 M1 1,3-Dichlorobenzene ug/L 1.61-1 100 100 26.0 28.6 26 29 1-172 9 1,4-Dichlorobenzene ug/L 1.71-1 100 100 27.4 30.4 27 30 20-124 10 2,2'-Oxybis(1-chloropropane) ug/L 1.21-1 100 100 84.6 75.2 85 75 36-166 12 2,4,6-TrichIorophenol ug/L 1.61-1 100 100 102 6.6J 102 7 37-144 M1 2,4-DichIorophenol ug/L 3.1J 100 100 118 31.5 115 28 1-191 116 R1 2,4-Dimethylphenol ug/L 1.71-1 100 100 100 84.1 100 84 32-119 18 2,4-Dinitrophenol ug/L 26.01-1 500 500 643 ND 129 1 1-181 2,4-Dinitrotoluene ug/L 1.61-1 100 100 115 93.6 115 94 39-139 20 2,6-Dinitrotoluene ug/L 1.71-1 100 100 112 96.0 112 96 50-158 15 2-Chloronaphthalene ug/L 1.7U 100 100 81.9 74.6 82 75 60-118 9 2-Chlorophenol ug/L 1.21-1 100 100 86.0 24.6 86 25 23-134 111 R1 2-Nitrophenol ug/L 1.4U 100 100 104 20.0 104 20 29-182 135 M1,R1 3,3'-Dichlorobenzidine ug/L 8.1U 200 200 155 177 77 89 1-262 14 4,6-Dinitro-2-methyl phenol ug/L 7.81-1 200 200 236 ND 118 6 1-181 4-Bromophenylphenyl ether ug/L 1.81-1 100 100 99.0 87.2 99 87 53-127 13 4-Chloro-3-methylphenol ug/L 3.31-1 200 200 193 135 97 68 22-147 35 R1 4-Chlorophenylphenyl ether ug/L 2.01-1 100 100 94.4 83.1 94 83 25-158 13 4-Nitrophenol ug/L 6.61-1 500 500 328 ND 66 0 1-132 M1 Acenaphthene ug/L 2.01-1 100 100 88.6 79.4 89 79 47-145 11 Acenaphthylene ug/L 2.01-1 100 100 92.8 82.5 93 82 33-145 12 Anthracene ug/L 2.31-1 100 100 97.2 85.2 97 85 1-166 13 Benzo(a)anthracene ug/L 2.71-1 100 100 99.5 86.0 99 86 33-143 15 Benzo(a)pyrene ug/L 2.81-1 100 100 102 86.7 102 87 17-163 16 Benzo(b)fluoranthene ug/L 2.61-1 100 100 99.2 84.3 99 84 24-159 16 Benzo(g,h,i)perylene ug/L 2.81-1 100 100 102 89.0 102 89 1-219 14 Benzo(k)fluoranthene ug/L 2.71-1 100 100 101 85.7 101 86 11-162 16 bis(2-Chloroethoxy)methane ug/L 1.81-1 100 100 95.9 82.8 96 83 33-184 15 bis(2-Chloroethyl) ether ug/L 1.91-1 100 100 90.5 78.3 91 78 12-158 14 bis(2-Ethylhexyl)phthalate ug/L 3.71-1 100 100 96.4 82.5 96 82 8-158 16 Butylbenzylphthalate ug/L 3.1U 100 100 99.4 83.7 99 84 1-152 17 Chrysene ug/L 2.81-1 100 100 97.5 83.2 98 83 17-168 16 Di-n-butylphthalate ug/L 2.21-1 100 100 101 88.8 101 89 1-118 12 Di-n-octylphthalate ug/L 3.91-1 100 100 105 89.6 105 90 4-146 16 Dibenz(a,h)anthracene ug/L 3.01-1 100 100 103 88.8 103 89 1-227 15 Diethylphthalate ug/L 2.01-1 100 100 99.9 86.7 100 87 1-114 14 Dimethylphthalate ug/L 2.1U 100 100 97.5 84.5 98 85 1-112 14 Fluoranthene ug/L 2.21-1 100 100 100 88.1 100 88 26-137 13 Fluorene ug/L 2.1U 100 100 94.5 83.3 94 83 59-121 13 Hexachloro-1,3-butadiene ug/L 1.81-1 100 100 24.9 27.8 25 28 24-116 11 Hexachlorobenzene ug/L 2.21-1 100 100 100 85.7 100 86 1-152 16 Hexachlorocyclopentadiene ug/L 1.61-1 100 100 53.5 46.6 54 47 25-150 14 Hexachloroethane ug/L 1.4U 100 100 17.7 21.4 18 21 40-113 19 M1 Indeno(1,2,3-cd)pyrene ug/L 2.91-1 100 100 101 86.2 101 86 1-171 16 Isophorone ug/L 1.71-1 100 100 104 90.0 104 90 21-196 14 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 67 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4502880 4502881 MS MSD 35896202001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual N-Nitroso-di-n-propylamine ug/L 1.31-1 100 100 95.8 84.5 96 84 1-230 13 N-Nitrosodimethylamine ug/L 1.91-1 100 100 79.5 70.0 80 70 25-150 13 N-Nitrosodiphenylamine ug/L 3.01-1 100 100 95.3 82.7 95 83 25-150 14 Naphthalene ug/L 2.1U 100 100 57.8 54.2 58 54 21-133 6 Nitrobenzene ug/L 1.91-1 100 100 96.9 85.0 97 85 35-180 13 Pentachlorophenol ug/L 3.81-1 200 200 222 ND 111 3 14-176 M1 Phenanthrene ug/L 2.01-1 100 100 95.6 83.7 96 84 54-120 13 Phenol ug/L 1.4U 100 100 60.4 29.6 60 30 5-112 69 R1 Pyrene ug/L 2.21-1 100 100 94.3 79.9 94 80 52-115 17 2,4,6-Tribromophenol (S) % 125 15 10-137 2-Fluorobiphenyl (S) % 82 75 15-120 2-Fluorophenol(S) % 69 8 10-120 SO Nitrobenzene-d5(S) % 102 89 10-120 Phenol-d6 (S) % 54 23 10-120 Terphenyl-d14 (S) % 96 82 11-131 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 68 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 874394 Analysis Method: SW-846 QC Batch Method: SW-846 Analysis Description: Dry Weight/Percent Moisture Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92746299019 SAMPLE DUPLICATE: 4504589 Parameter Percent Moisture SAMPLE DUPLICATE: 4504590 Parameter Percent Moisture 92745926003 Dup Units Result Result % 5.0 5.0 92746369001 Dup Units Result Result % 97.3 97.3 RPD Qualifiers 1 N2 RPD Qualifiers 0 N2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 69 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 877946 Analysis Method: SW-846 QC Batch Method: SW-846 Analysis Description: Dry Weight/Percent Moisture Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92746299020 SAMPLE DUPLICATE: 4522371 92748858001 Dup Parameter Units Result Result RPD Qualifiers Percent Moisture % 21.2 23.4 10 N2 SAMPLE DUPLICATE: 4522372 92749311007 Dup Parameter Units Result Result RPD Qualifiers Percent Moisture % 97.2 97.4 0 N2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 70 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 2344553 Analysis Method: EPA 1664B QC Batch Method: 1664A Analysis Description: Wet Chemistry 1664B Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92746299004, 92746299008 METHOD BLANK: R4108426-1 Matrix: Water Associated Lab Samples: 92746299004, 92746299008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.00 08/19/24 06:43 LABORATORY CONTROL SAMPLE & LCSD: R4108426-2 R4108426-3 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Oil and Grease mg/L 40.0 37.4 36.5 93.5 91.3 78.0-114 2.44 20 MATRIX SPIKE SAMPLE: R4108426-4 L1767324-01 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L ND 40.0 27.5 68.7 78.0-114 ML Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 71 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 2345741 Analysis Method: EPA 1664B QC Batch Method: 1664A Analysis Description: Wet Chemistry 1664B Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92746299004, 92746299008 METHOD BLANK: R4108519-1 Matrix: Water Associated Lab Samples: 92746299004, 92746299008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.00 08/19/24 10:37 LABORATORY CONTROL SAMPLE & LCSD: R4108519-2 R4108519-3 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Total Petroleum Hydrocarbons mg/L 20.0 18.5 17.6 92.5 88.0 64.0-132 4.99 34 MATRIX SPIKE SAMPLE: R4108519-4 L1767324-01 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 40.0 27.5 68.7 64.0-132 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 72 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 875150 Analysis Method: EPA 160.4 / SM2540B-2011 QC Batch Method: EPA 160.4 / SM2540B-2011 Analysis Description: 160.4 Total Volatile Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92746299019 SAMPLE DUPLICATE: 4507986 92746299019 Dup Parameter Units Result Result Total Volatile Solids mg/kg 779000 778000 RPD Qualifiers 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 73 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 875151 Analysis Method: EPA 160.4 / SM2540B-2015 QC Batch Method: EPA 160.4 / SM2540B-2015 Analysis Description: 160.4 TVS and 2540E TS Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92746299015 METHOD BLANK: 4507987 Associated Lab Samples: 92746299015 Parameter Units Total Solids mg/L LABORATORY CONTROL SAMPLE: 4507988 Parameter Units Total Solids mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 08/13/2418:54 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 500 546 109 90-110 SAMPLE DUPLICATE: 4507989 92746299015 Dup Parameter Units Result Result RPD Qualifiers Total Solids mg/L 5570 6090 9 Total Volatile Solids mg/L 4220 4690 11 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 74 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 874483 Analysis Method: SM 2320B-2011 QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92746299003, 92746299007 METHOD BLANK: 4505018 Matrix: Water Associated Lab Samples: 92746299003, 92746299007 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Alkalinity, Total as CaCO3 mg/L ND 5.0 08/09/24 12:50 LABORATORY CONTROL SAMPLE: 4505019 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 mg/L 50 52.8 106 80-120 LABORATORY CONTROL SAMPLE: 4505020 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 mg/L 50 53.3 107 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4505021 4505022 MS MSD 92746636001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Alkalinity, Total as CaCO3 mg/L 28.3 50 50 76.7 77.9 97 99 80-120 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4505023 4505024 MS MSD 92746636002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Alkalinity, Total as CaCO3 mg/L 29.7 50 50 79.9 78.8 100 98 80-120 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 75 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 874714 Analysis Method: SM 2540C-2015 QC Batch Method: SM 2540C-2015 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92746299003, 92746299007 METHOD BLANK: 4506205 Associated Lab Samples: 92746299003, 92746299007 Parameter Units Total Dissolved Solids mg/L LABORATORY CONTROL SAMPLE: 4506206 Parameter Units Total Dissolved Solids mg/L SAMPLE DUPLICATE: 4506208 Parameter Units Total Dissolved Solids mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 08/13/2411:50 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 256 102 90-110 92746245001 Dup Result Result RPD Qualifiers 40.0 41.0 2 SAMPLE DUPLICATE: 4506209 92746223001 Dup Parameter Units Result Result Total Dissolved Solids mg/L 92.0 88.0 RPD Qualifiers 4 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 76 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 874181 Analysis Method: EPA 160.4 / SM2540B-2015 QC Batch Method: EPA 160.4 / SM2540B-2015 Analysis Description: 2540D TSS/TVSS Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92746299017, 92746299022, 92746299024 METHOD BLANK: 4503289 Matrix: Water Associated Lab Samples: 92746299017, 92746299022, 92746299024 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 08/09/24 13:36 LABORATORY CONTROL SAMPLE: 4503290 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 246 98 90-110 SAMPLE DUPLICATE: 4505658 92745810002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 6720 6620 1 Volatile Suspended Solids mg/L 4120 4050 2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 77 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 875319 Analysis Method: EPA 160.4 / SM2540B-2015 QC Batch Method: EPA 160.4 / SM2540B-2015 Analysis Description: 2540D TSS/TVSS Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92746299011, 92746299013 METHOD BLANK: 4508922 Matrix: Water Associated Lab Samples: 92746299011, 92746299013 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 08/13/24 21:27 LABORATORY CONTROL SAMPLE: 4508923 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 270 108 90-110 SAMPLE DUPLICATE: 4509464 92746299011 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 3340 3480 4 Volatile Suspended Solids mg/L 2760 2850 3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 78 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 874445 Analysis Method: SM 2540D-2015 QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92746299003, 92746299007, 92746299009 METHOD BLANK: 4504943 Matrix: Water Associated Lab Samples: 92746299003, 92746299007, 92746299009 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 08/09/24 13:10 LABORATORY CONTROL SAMPLE: 4504944 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 252 101 90-110 SAMPLE DUPLICATE: 4505599 92746416001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 258 274 6 SAMPLE DUPLICATE: 4505600 92746042001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 42.7 49.5 15 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 79 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 874715 Analysis Method: SM 2540D-2015 QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92746299021 METHOD BLANK: 4506218 Associated Lab Samples: 92746299021 Parameter Units Total Suspended Solids mg/L LABORATORY CONTROL SAMPLE: 4506219 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 4506676 Parameter Units Total Suspended Solids mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 08/11/2413:40 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 240 96 90-110 92746736001 Dup Result Result RPD Qualifiers 120 110 9 SAMPLE DUPLICATE: 4506677 92746332001 Dup Parameter Units Result Result Total Suspended Solids mg/L 1170 1180 RPD Qualifiers 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 80 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 874215 Analysis Method: SM 521 OB-2016 QC Batch Method: SM 521OB-2016 Analysis Description: 5210E cASC, 5 day Final Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92746299003, 92746299007, 92746299009, 92746299017, 92746299021 METHOD BLANK: 4503477 Matrix: Water Associated Lab Samples: 92746299003, 92746299007, 92746299009, 92746299017, 92746299021 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Carbonaceous BOD, 5 day mg/L ND 2.0 08/13/24 15:40 LABORATORY CONTROL SAMPLE: 4503479 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Carbonaceous BOD, 5 day mg/L 198 211 106 84.6-115 SAMPLE DUPLICATE: 4503480 92746299021 Dup Parameter Units Result Result RPD Qualifiers Carbonaceous BOD, 5 day mg/L 3.5 3.5 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 81 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 874070 Analysis Method: EPA 300.0 Rev 2.1 1993 QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92746299003, 92746299007, 92746299011, 92746299017 METHOD BLANK: 4502882 Matrix: Water Associated Lab Samples: 92746299003, 92746299007, 92746299011, 92746299017 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride mg/L ND 1.0 08/07/24 19:32 Nitrate as N mg/L ND 0.10 08/07/24 19:32 Nitrate -Nitrite (as N) mg/L ND 0.20 08/07/24 19:32 Nitrite as N mg/L ND 0.10 08/07/24 19:32 LABORATORY CONTROL SAMPLE: 4502883 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride mg/L 50 51.9 104 90-110 Nitrate as N mg/L 2.5 2.5 100 90-110 Nitrate -Nitrite (as N) mg/L 5 5.2 103 90-110 Nitrite as N mg/L 2.5 2.7 106 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4502884 4502885 MS MSD 92746299017 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride mg/L 44.8 50 50 92.8 96.2 96 103 90-110 4 Nitrate as N mg/L 0.44 2.5 2.5 2.9 3.1 100 108 90-110 6 Nitrate -Nitrite (as N) mg/L 0.44 5 5 5.0 5.4 92 99 90-110 6 Nitrite as N mg/L ND 2.5 2.5 2.1 2.2 82 87 90-110 6 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 82 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 876972 Analysis Method: EPA 350.1 Rev 2.0 1993 QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92746299003, 92746299007, 92746299009, 92746299011, 92746299013, 92746299017, 92746299021 METHOD BLANK: 4517239 Matrix: Water Associated Lab Samples: 92746299003, 92746299007, 92746299009, 92746299011, 92746299013, 92746299017, 92746299021 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Ammonia mg/L ND 0.10 08/21/24 15:42 LABORATORY CONTROL SAMPLE: 4517240 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Ammonia mg/L 5 5.1 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4517241 4517242 MS MSD 92747947001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L ND 5 5 4.9 4.9 97 97 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4517243 4517244 MS MSD 92747948002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L 0.39 5 5 5.5 5.5 102 102 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 83 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 877196 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92746299019 METHOD BLANK: 4518114 Associated Lab Samples: 92746299019 Parameter Units Nitrogen, Kjeldahl, Total mg/kg LABORATORY CONTROL SAMPLE: 4518115 Parameter Units Nitrogen, Kjeldahl, Total mg/kg Matrix: Solid Blank Reporting Result Limit Analyzed Qualifiers ND 50.0 08/22/24 08:14 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 1000 1080 108 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4518116 4518117 MS MSD 92746351001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/kg 262 1130 1080 1530 1420 112 107 90-110 8 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 84 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 878258 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92746299003, 92746299007, 92746299009, 92746299011, 92746299015, 92746299017, 92746299021 METHOD BLANK: 4523605 Matrix: Water Associated Lab Samples: 92746299003, 92746299007, 92746299009, 92746299011, 92746299015, 92746299017, 92746299021 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg/L ND 0.50 08/27/24 09:01 LABORATORY CONTROL SAMPLE: 4523606 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg/L 10 10.5 105 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4523607 4523608 MS MSD 92746299003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 49.5 10 10 66.2 58.2 167 86 90-110 13 M1,R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4523609 4523610 MS MSD 92746299007 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 1.5 10 10 13.1 13.8 116 123 90-110 5 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 85 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 874090 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92746299019 METHOD BLANK: 4503069 Matrix: Solid Associated Lab Samples: 92746299019 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mg/kg ND 4.0 08/08/24 01:54 Nitrogen, Nitrite mg/kg ND 4.0 08/08/24 01:54 Nitrogen, NO2 plus NO3 mg/kg ND 4.0 08/08/24 01:54 LABORATORY CONTROL SAMPLE: 4503070 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/kg 15 15.6 104 90-110 Nitrogen, Nitrite mg/kg 10 10.3 103 90-110 Nitrogen, NO2 plus NO3 mg/kg 25 25.9 104 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4503071 4503072 MS MSD 92746369001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Nitrate mg/kg ND 548 541 564 534 103 99 90-110 5 Nitrogen, Nitrite mg/kg ND 363 359 383 365 105 102 90-110 5 Nitrogen, NO2 plus NO3 mg/kg ND 911 900 947 899 103 100 90-110 5 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 86 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 877081 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, preserved Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92746299009, 92746299015, 92746299021 METHOD BLANK: 4517733 Matrix: Water Associated Lab Samples: 92746299009, 92746299015, 92746299021 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, NO2 plus NO3 mg/L ND 0.040 08/22/24 03:27 LABORATORY CONTROL SAMPLE: 4517734 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mg/L 2.5 2.6 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4517735 4517736 MS MSD 92747195002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 0.35 2.5 2.5 2.8 2.8 98 97 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4517737 4517738 MS MSD 92747794001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 0.38 2.5 2.5 2.9 2.9 102 102 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 87 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 875011 Analysis Method: EPA 365.1 Rev 2.0 1993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92746299019 METHOD BLANK: 4507179 Associated Lab Samples: 92746299019 Parameter Units Phosphorus mg/kg LABORATORY CONTROL SAMPLE: 4507180 Parameter Units Phosphorus mg/kg Matrix: Solid Blank Reporting Result Limit Analyzed Qualifiers ND 1.0 08/13/2418:54 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 50 50.5 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4507181 4507182 MS MSD 92746020001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/kg 140 67.8 66.4 167 223 40 124 90-110 28 M1,R1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 88 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 877442 Analysis Method: EPA 365.1 Rev 2.0 1993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92746299003, 92746299007, 92746299009, 92746299011, 92746299013, 92746299015, 92746299017, 92746299021 METHOD BLANK: 4519659 Matrix: Water Associated Lab Samples: 92746299003, 92746299007, 92746299009, 92746299011, 92746299013, 92746299015, 92746299017, 92746299021 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/L ND 0.050 08/23/2410:42 LABORATORY CONTROL SAMPLE: 4519660 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg/L 2.5 2.5 98 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4519661 4519662 MS MSD 92748456001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L ND 2.5 2.5 2.5 2.4 98 96 90-110 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4519663 4519664 MS MSD 92748456002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L ND 2.5 2.5 2.4 2.4 95 96 90-110 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 89 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 877812 Analysis Method: EPA 420.4 Rev 1.0 1993 QC Batch Method: EPA 420.4 Rev 1.0 1993 Analysis Description: 420.4 Phenolics Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92746299003, 92746299007 METHOD BLANK: 4521561 Matrix: Water Associated Lab Samples: 92746299003, 92746299007 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phenolics, Total Recoverable mg/L ND 0.0050 08/24/24 15:19 LABORATORY CONTROL SAMPLE: 4521562 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phenolics, Total Recoverable mg/L 0.05 0.052 104 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4521563 4521564 MS MSD 92746299003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phenolics, Total Recoverable mg/L 0.038 0.05 0.05 0.092 0.094 108 113 90-110 3 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4521565 4521566 MS MSD 92746299007 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phenolics, Total Recoverable mg/L ND 0.05 0.05 0.060 0.059 110 108 90-110 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 90 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 875274 Analysis Method: SM 4500-CN-E-2016 QC Batch Method: SM 4500-CN-E-2016 Analysis Description: 450OCNE Cyanide, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92746299020 METHOD BLANK: 4508597 Associated Lab Samples: 92746299020 Parameter Units Cyanide mg/kg LABORATORY CONTROL SAMPLE: 4508598 Parameter Units Cyanide mg/kg Matrix: Solid Blank Reporting Result Limit Analyzed Qualifiers ND 0.22 08/15/2410:58 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 2.6 2.6 102 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4508599 4508600 MS MSD 92745383001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Cyanide mg/kg ND 3 3.3 3.0 3.1 98 94 80-120 5 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 91 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 876557 Analysis Method: SM 4500-CN-E-2016 QC Batch Method: SM 4500-CN-E-2016 Analysis Description: 450OCNE Cyanide, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92746299004,92746299008,92746299010,92746299012,92746299014,92746299016,92746299018, 92746299021,92746299023,92746299025 METHOD BLANK: 4515135 Matrix: Water Associated Lab Samples: 92746299004,92746299008,92746299010,92746299012,92746299014,92746299016,92746299018, 92746299021,92746299023,92746299025 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Cyanide mg/L ND 0.0080 08/20/2411:16 LABORATORY CONTROL SAMPLE: 4515136 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide mg/L 0.1 0.10 104 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4515137 4515138 MS MSD 92746735001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Cyanide mg/L ND 0.1 0.1 ND ND -1 0 80-120 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4515139 4515140 MS MSD 92746027001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Cyanide mg/L ND 0.1 0.1 ND ND 1 1 80-120 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 92 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 QC Batch: 878419 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92746299003, 92746299007, 92746299009, 92746299013, 92746299017, 92746299021 METHOD BLANK: 4524505 Matrix: Water Associated Lab Samples: 92746299003, 92746299007, 92746299009, 92746299013, 92746299017, 92746299021 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 08/27/24 15:28 LABORATORY CONTROL SAMPLE: 4524506 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 743 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4524507 4524508 MS MSD 92746299007 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L ND 100 100 108 115 104 110 90-110 6 R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4524509 4524510 MS MSD 92748569003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 26.9 100 100 126 126 99 99 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 93 of 133 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 aceo Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. SAMPLE QUALIFIERS Sample: 92746299008 Ill Wet Chemistry by Method 1664B - Total Oil&Grease is non -detect. Extract was not processed through silica gel. Sample: L1767324-01 Ill Wet Chemistry by Method 1664B - Total Oil&Grease is non -detect. Extract was not processed through silica gel. ANALYTE QUALIFIERS D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference. L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples may be biased high. MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. ML Matrix spike recovery and/or matrix spike duplicate recovery was below laboratory control limits. Result may be biased low. N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A complete list of accreditations/certifications is available upon request. R1 RPD value was outside control limits. SO Surrogate recovery outside laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 94 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: UC12-SEMI-AN & PPA-8/7-2024 Pace Project No.: 92746299 ANALYTE QUALIFIERS S4 Surrogate recovery not evaluated against control limits due to sample dilution. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 95 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: UC12-SEMI-AN & PPA-8/7-2024 92746299 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92746299003 UC12-INF EPA 608.3 874068 EPA 608.3 874161 92746299007 UC12-EFF EPA 608.3 874558 EPA 608.3 874980 92746299011 UC12-MLSS EPA 608.3 874558 EPA 608.3 874980 92746299018 UC12-INFDIST EPA 608.3 874558 EPA 608.3 874980 92746299019 UC12-BFP-1-CAKE EPA 7471 B 875058 EPA 7471 B 875147 92746299003 UC12-INF EPA 200.7 Rev 4.4 1994 875840 EPA 200.7 Rev 4.4 1994 875992 92746299007 UC12-EFF EPA 200.7 Rev 4.4 1994 875840 EPA 200.7 Rev 4.4 1994 875992 92746299019 UC12-BFP-1-CAKE EPA3050B 875260 EPA6010D 875409 92746299003 UC12-INF EPA 200.8 Rev 5.4 1994 874203 EPA 200.8 Rev 5.4 1994 874343 92746299007 UC12-EFF EPA 200.8 Rev 5.4 1994 874647 EPA 200.8 Rev 5.4 1994 874806 92746299009 UC12-FCE EPA 200.8 Rev 5.4 1994 874279 EPA 200.8 Rev 5.4 1994 874411 92746299011 UC12-MLSS EPA 200.8 Rev 5.4 1994 874279 EPA 200.8 Rev 5.4 1994 874411 92746299013 UC12-RAS EPA 200.8 Rev 5.4 1994 874279 EPA 200.8 Rev 5.4 1994 874411 92746299015 UC12-WAS EPA 200.8 Rev 5.4 1994 874279 EPA 200.8 Rev 5.4 1994 874411 92746299017 UC12-INFDIST EPA 200.8 Rev 5.4 1994 874279 EPA 200.8 Rev 5.4 1994 874411 92746299021 UC12-BFP-1-FILT EPA 200.8 Rev 5.4 1994 874279 EPA 200.8 Rev 5.4 1994 874411 92746299022 UC12-1 2 AER EPA 200.8 Rev 5.4 1994 874279 EPA 200.8 Rev 5.4 1994 874411 92746299024 UC12-5 6 AER EPA 200.8 Rev 5.4 1994 874279 EPA 200.8 Rev 5.4 1994 874411 92746299009 UC12-FCE EPA 245.1 Rev 3.0 1994 874602 EPA 245.1 Rev 3.0 1994 874717 92746299011 UC12-MLSS EPA 245.1 Rev 3.0 1994 874602 EPA 245.1 Rev 3.0 1994 874717 92746299013 UC12-RAS EPA 245.1 Rev 3.0 1994 874602 EPA 245.1 Rev 3.0 1994 874717 92746299015 UC12-WAS EPA 245.1 Rev 3.0 1994 874602 EPA 245.1 Rev 3.0 1994 874717 92746299017 UC12-INFDIST EPA 245.1 Rev 3.01994 874602 EPA 245.1 Rev 3.01994 874717 92746299021 UC12-BFP-1-FILT EPA 245.1 Rev 3.01994 874602 EPA 245.1 Rev 3.01994 874717 92746299022 UC12-1 2 AER EPA 245.1 Rev 3.0 1994 874602 EPA 245.1 Rev 3.0 1994 874717 92746299024 UC12-5 6 AER EPA 245.1 Rev 3.0 1994 874602 EPA 245.1 Rev 3.0 1994 874717 92746299004 UC12-INF EPA625.1 874069 EPA625.1 874165 92746299007 UC12-EFF EPA625.1 874069 EPA625.1 874165 92746299011 UC12-MLSS EPA625.1 874069 EPA625.1 874165 92746299018 UC12-INFDIST EPA625.1 874069 EPA625.1 874165 92746299004 UC12-INF EPA624.1 874338 92746299008 UC12-EFF EPA624.1 874338 92746299012 UC12-MLSS EPA624.1 874338 92746299018 UC12-INFDIST EPA624.1 874338 92746299019 UC12-BFP-1-CAKE SM 2540G-2011 875019 92746299019 UC12-BFP-1-CAKE SW-846 874394 92746299020 UC12-BFP-1-CAKE SW-846 877946 92746299004 UC12-INF 1664B 2344553 EPA 1664B 2344553 92746299004 UC12-INF 1664E 2345741 EPA 1664B 2345741 92746299008 UC12-EFF 1664B 2344553 EPA 1664B 2344553 Date: 08/28/2024 09:55 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 96 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: UC12-SEMI-AN & PPA-8/7-2024 92746299 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92746299008 UC12-EFF 1664B 2345741 EPA1664B 2345741 92746299019 UC12-BFP-1-CAKE EPA 160.4 / SM2540B- 875150 2011 92746299015 UC12-WAS EPA 160.4 / SM2540B- 875151 2015 92746299003 UC12-INF SM 2320B-2011 874483 92746299007 UC12-EFF SM 2320B-2011 874483 92746299003 UC12-INF SM 2540C-2015 874714 92746299007 UC12-EFF SM 2540C-2015 874714 92746299003 UC12-INF SM 2540D-2015 874445 92746299007 UC12-EFF SM 2540D-2015 874445 92746299009 UC12-FCE SM 2540D-2015 874445 92746299021 UC12-BFP-1-FILT SM 2540D-2015 874715 92746299011 UC12-MLSS EPA 160.4 / SM2540B- 875319 2015 92746299013 UC12-RAS EPA 160.4 / SM2540B- 875319 2015 92746299017 UC12-INFDIST EPA 160.4 / SM2540B- 874181 2015 92746299022 UC12-1 2 AER EPA 160.4 / SM2540B- 874181 2015 92746299024 UC12-5_6 AER EPA 160.4 / SM2540B- 874181 2015 92746299003 UC12-INF SM 5210B-2016 874215 SM 5210B-2016 874305 92746299007 UC12-EFF SM 5210B-2016 874215 SM 5210B-2016 874305 92746299009 UC12-FCE SM 5210B-2016 874215 SM 5210B-2016 874305 92746299017 UC12-INFDIST SM 5210B-2016 874215 SM 5210B-2016 874305 92746299021 UC12-BFP-1-FILT SM 5210B-2016 874215 SM 5210B-2016 874305 92746299003 UC12-INF EPA 300.0 Rev 2.1 1993 874070 92746299007 UC12-EFF EPA 300.0 Rev 2.1 1993 874070 92746299011 UC12-MLSS EPA 300.0 Rev 2.1 1993 874070 92746299017 UC12-INFDIST EPA 300.0 Rev 2.1 1993 874070 92746299003 UC12-INF EPA 350.1 Rev 2.0 1993 876972 92746299007 UC12-EFF EPA 350.1 Rev 2.0 1993 876972 92746299009 UC12-FCE EPA 350.1 Rev 2.0 1993 876972 92746299011 UC12-MLSS EPA 350.1 Rev 2.0 1993 876972 92746299013 UC12-RAS EPA 350.1 Rev 2.0 1993 876972 92746299017 UC12-INFDIST EPA 350.1 Rev 2.0 1993 876972 92746299021 UC12-BFP-1-FILT EPA 350.1 Rev 2.0 1993 876972 92746299019 UC12-BFP-1-CAKE EPA 351.2 Rev 2.0 1993 877196 EPA 351.2 Rev 2.0 1993 877406 92746299003 UC12-INF EPA 351.2 Rev 2.0 1993 878258 EPA 351.2 Rev 2.0 1993 878451 92746299007 UC12-EFF EPA 351.2 Rev 2.0 1993 878258 EPA 351.2 Rev 2.0 1993 878451 92746299009 UC12-FCE EPA 351.2 Rev 2.0 1993 878258 EPA 351.2 Rev 2.0 1993 878451 92746299011 UC12-MLSS EPA 351.2 Rev 2.0 1993 878258 EPA 351.2 Rev 2.0 1993 878451 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/28/2024 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 97 of 133 ceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: UC12-SEMI-AN & PPA-8/7-2024 92746299 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92746299015 UC12-WAS EPA 351.2 Rev 2.0 1993 878258 EPA 351.2 Rev 2.0 1993 878451 92746299017 UC12-INFDIST EPA 351.2 Rev 2.0 1993 878258 EPA 351.2 Rev 2.0 1993 878451 92746299021 UC12-BFP-1-FILT EPA 351.2 Rev 2.0 1993 878258 EPA 351.2 Rev 2.0 1993 878451 92746299019 UC12-BFP-1-CAKE EPA 353.2 Rev 2.0 1993 874090 EPA 353.2 Rev 2.0 1993 874097 92746299009 UC12-FCE EPA 353.2 Rev 2.0 1993 877081 92746299015 UC12-WAS EPA 353.2 Rev 2.0 1993 877081 92746299021 UC12-BFP-1-FILT EPA 353.2 Rev 2.0 1993 877081 92746299019 UC12-BFP-1-CAKE EPA 365.1 Rev 2.0 1993 875011 EPA 365.1 Rev 2.0 1993 875265 92746299003 UC12-INF EPA 365.1 Rev 2.0 1993 877442 EPA 365.1 Rev 2.0 1993 877667 92746299007 UC12-EFF EPA 365.1 Rev 2.0 1993 877442 EPA 365.1 Rev 2.0 1993 877667 92746299009 UC12-FCE EPA 365.1 Rev 2.0 1993 877442 EPA 365.1 Rev 2.0 1993 877667 92746299011 UC12-MLSS EPA 365.1 Rev 2.0 1993 877442 EPA 365.1 Rev 2.0 1993 877667 92746299013 UC12-RAS EPA 365.1 Rev 2.0 1993 877442 EPA 365.1 Rev 2.0 1993 877667 92746299015 UC12-WAS EPA 365.1 Rev 2.0 1993 877442 EPA 365.1 Rev 2.0 1993 877667 92746299017 UC12-INFDIST EPA 365.1 Rev 2.0 1993 877442 EPA 365.1 Rev 2.0 1993 877667 92746299021 UC12-BFP-1-FILT EPA 365.1 Rev 2.0 1993 877442 EPA 365.1 Rev 2.0 1993 877667 92746299003 UC12-INF EPA 420.4 Rev 1.0 1993 877812 EPA 420.4 Rev 1.0 1993 878086 92746299007 UC12-EFF EPA 420.4 Rev 1.0 1993 877812 EPA 420.4 Rev 1.0 1993 878086 92746299020 UC12-BFP-1-CAKE SM 4500-CN-E-2016 875274 SM 4500-CN-E-2016 875665 92746299004 UC12-INF SM 4500-CN-E-2016 876557 SM 4500-CN-E-2016 876700 92746299008 UC12-EFF SM 4500-CN-E-2016 876557 SM 4500-CN-E-2016 876700 92746299010 UC12-FCE SM 4500-CN-E-2016 876557 SM 4500-CN-E-2016 876700 92746299012 UC12-MLSS SM 4500-CN-E-2016 876557 SM 4500-CN-E-2016 876700 92746299014 UC12-RAS SM 4500-CN-E-2016 876557 SM 4500-CN-E-2016 876700 92746299016 UC12-WAS SM 4500-CN-E-2016 876557 SM 4500-CN-E-2016 876700 92746299018 UC12-INFDIST SM 4500-CN-E-2016 876557 SM 4500-CN-E-2016 876700 92746299021 UC12-BFP-1-FILT SM 4500-CN-E-2016 876557 SM 4500-CN-E-2016 876700 92746299023 UC12-1 2 AER SM 4500-CN-E-2016 876557 SM 4500-CN-E-2016 876700 92746299025 UC12-5 6 AER SM 4500-CN-E-2016 876557 SM 4500-CN-E-2016 876700 92746299003 UC12-INF SM 5220D-2011 878419 SM 5220D-2011 878442 92746299007 UC12-EFF SM 5220D-2011 878419 SM 5220D-2011 878442 92746299009 UC12-FCE SM 5220D-2011 878419 SM 5220D-2011 878442 92746299013 UC12-RAS SM 5220D-2011 878419 SM 5220D-2011 878442 92746299017 UC12-INFDIST SM 5220D-2011 878419 SM 5220D-2011 878442 92746299021 UC12-BFP-1-FILT SM 5220D-2011 878419 SM 5220D-2011 878442 Date: 08/28/2024 09:55 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 98 of 133 ,,,07 9800 Kincey Ave #100 WVff ; uLr4tz!ju I�Pace Huntersville, NC 28078 (704) 875-9092 EVENT TYPE: UC12. SEMI -AN 81712024 Proj. Mgr.: Stephanie Knot IIIuILIR. SEND REPORT 70: Keith Purgason 8299 Kensington Dr Waxhaw, NC 28173 keith.purgason@unioncountync.gov ActtNumlClient ID: North Carolina Wastewater Certification #,12 I + f I I Samp {Sign Namet: C 92746299 CLIENT: Union County Water Table#: FACILITY Twelve Mile Creek WRF, NCO085359 Profile/ Template: 16076 Print Name: Clean Hands Dirty Hands if ; p F A; ADDRESS: 8299 Kensington Drive, Waxhaw, NC 28173 Prelog! Bottle Ord. ID EZ 3143106 Sample Collection Data Sample Conlaine preservative Analyses Requested U) W o o Q r O w c) SAMPLE ID °' �; a Z 3 m(D N m-7 a W M Q w o n o W = a v CDN u�, v a LAB USE ONLY o I= m CD o --- o � m m � rn m c Q o v o �`+ � r> x , � � W � ti o M v ,s ca cn LAB SAMPLE ID 'C -OY W=� }. C1j q, a (3J E LLn O N 'cr 0 V. O %n O N M Q d O ;M- r 7 o V5 a to T Q CL c.0 r' [� t�P O L i [O C m 111 W O ~ 'm N [�7 co Cn CV CV 2 U1 N -- '� Q d 4 O U o N a W N to W W (� 04 N �n N , O O O E QI E E O E i= c4 .O O_ m C U Cn W z ('-] Q = O C� L(] W u'] ( (n Uj .0 o .^ 'C O Z a, W L a 6.1 d cn C7 Vi c O S C7 to —5 UJ CU M E E C° c O O o O 0 Z cn N b N U N [tl O [n O O UJ cn 7 cn Cf� cn a -� E E m z Y m O m U @_ cU o C7 R% U °a'1 CD d uJ 7 E QJ y, �/J 1 771 CA (M O F U [O 7_ S 2 Z 2 Z m a- _ d 5 J _j 2 -C 2f 7- O UC12-INF M 8/7/2024 I� N G GL 1 X X UC12-INF FIELD BLANK 8I712024 N G GL 1� X X vuZ Sample Temp at Collection: INF: °C EFF: °C Comments: SHIPPED ON WET ICE liy LL G SAMPLES Custody Seal Present: Custody Seat Number: 200.8 = Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,TI,Zn,Mo YES / NO Sample Temp at Receiving in Lab: INF: °C EFF: °C Sample T e Codes: Relinq ' by (Si to Received .. y (S'gnatu } . Date; Time: Q (Flow) Automatic Flow Pro orlloned Sample ) p p T (Time) = Automatic Time Proportioned Sample �� / `f U, Sample Temp of EFF Fecal Sample at Receiving in Lab ,C o Ref uished Sign�r . / e 'e' ed by (Signature : �i( '/ �-� Date: Time: (record only if collected): 0 H (Hand) =Hand Composite Sample G {Grab) = Grab Sample �-• -_ I !7�'-� �� I�< . • �/ I 'tL Zero Headspace & Teflon septa for YES NO NIA Relinquished by (Signature): Received by (Signature): Date: Time: VOAs: < Container Type Codes: A - Amber Glass P = Plastic Samples in Proper Containers: YES NO NIA m Relinquished by (Signature): Received by (Signature): Date: Time: GL = Clear Glass B = Bag TL = Teflon Lined Cap Chlorinated Samples De- YES NO NIA < Relinquished by (Signature): Received by (Signature): I Date: Time: Chlorinated: VOA = 40 ml Glass vial I age 99 of 133 9800 Kincey Ave #100 UC12 SEMI & 81712024 COC#: PAGE c of l 5 ace Huntersville, NC 28078 (704) 875.9092 EVENT TYPE: - -AN . - Pra � r Ste hanie Knott g p , I North Carolina Wastewater Certification #:12 SEND REPORT TO: Keith Purgason ActtNumlClient ID: Sam,fSign Name): CLIENT: Union County Water 8299 Kensington Dr Table#: _ no711pre FACILITY: Twelve Mile Creek WRF, NC0085359 Waxhaw, NC 28173 Profile/ Template: 16076 ADDRESS: 8299 Kensington Drive, Waxhaw, NC 28173 keith.purgason@unioncountync.gov Prelogl Bottle Ord. ID EZ 3143106 /j J�c_;T" If Sample Collection Data 3ample Containe Preservative Analyses Requested cn o H O Lu z U v 0 z } o a 3 O m o m r a w a a u _ Q ry a LAB USE ONLY SAMPLE ID �, O/ i-- £ o m o m a m N o M o M x N v o � M v M It � lu Cn Co LAB SAMPLE ID �, M o � _ ° a i= o U �' a) 3 cn Q T n E ry �, t., o ry ua o a v o e w Q a Lll o u7 M 0 M 2 co — Q n o o ry Q � r 0 r � f9 � C LU LL �- E r C N (n 2 L Ln K] CV a Ln N N 2 W H - U (n , N Z Q d d� �n - ay C o N ' ul W (7 N ,!j t'V F- O a Q 61 d d 61 d fp N o 0- C (� Q7 UJ M zT O Z � 0 l[] , C!) '� J C .2 O �! .0 a m ° U, C o Z ? 'L7 E E E E E E E c O O — z O 0 U) O N O m 0 O (1i c� cq (.f) cq i 0 s E m � Z X m O S a L U ot5 (a az5 U O W 2 W (n (17 U3 Cfl d UCQ M Z 2 Z 2 Z m c- d � J = Of l �d UC 24 81712024 8/7/2024 f N Q P 1 O o X X UC12-INF 816l2024 �� L{� 8/712024 Cb 817/2024 j N Q P 1 a X X 7J3 UC12-INF M 816/2024 �(� q7 8r712O24 0 81712024 dG N Q P 1 r X X UC12•INF VA 816/2024 oLq 8f712024 DGOt 8/712024 QG I1 N Q P 1 N X X U4 Sample Temp at Collection: INF: °C EFF: °C Comments: SHIPPED ON WET ICE 200,8= Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,TI,Zn,Mo �N SEMI-ANNUAL SAMPLES Custody Seal Present: YES /NO Custody Seal Number: Sample temp at Receiving in Lab: INF: °C EFF: °C Sample Type Codes: Q (Flow) =Automatic Flow Proportioned Sample p p T (Time) = Automatic Time Proportioned Sample Relinquish d by (Signat UCW � ,, �� R�lved by (S€�natur �� s�/ / D t : f 1 Time: Sample Temp of EFF Fecal Sample at Receiving in Lab °C o _ tipquished b �(Signafu�): , Rec ived by (Signature):. Date: Time: (record only if collected): 3> 0 H (Hand) = Hand Composite Sample G (Grab) = Grab Sample Zero Headspace & Teflon septa for YES NO NIA Relinbu€shed by (Signature): Received by (Signature): Date: Time: VOAs: Container Type Codes: A = Amber Glass P = Plastic Samples in Proper Containers: YES NO NIA o Relinquished by (Signature): Received by (Signature): Date: Time: GL = Clear Glass B = Bag TL = Tefon Lined Cap Chlorinated Samples De- YES NO NIA < Relinquished by (Signature): Received by (Signature): I Date: Time: Chlorinated: VOA = 40 ml Glass vial Pa e 100 of 133 9800 Kincey Ave #100 UC12 SEMI & 81712024 49ace COC#: PAGE r] of j Huntersville, NC 28078 704 875-9092 EVENT TYPE: - -AN - ( ) Proj. Mgr.: Stephanie Knott J i Sam b Sign Nam J _ r North Carolina Wastewater Certification #:12 SEND REPORT TO: Keith Purgason ActtidumlClient ID: CLIENT: Union County Water 8299 Kensington Dr Table#: r Print Name: FACILITY: Twelve Mile Creek WRF, NC0085359 Waxhaw, NC 28173 Profile/ Template: 16076 U ADDRESS.: 8299 Kensington Drive, Waxhaw, NC 28173 keith.purgason@unioncountync.gcv Prelog! Bottle Ord. ID EZ 3143106 L Sample Collection Data Sample Container Preservative Analyses Requested 00 c r LO H p Z W W Z U U o } m m Ci m-- Q w °o U o 0. eNp O o N LAB USE ONLY SAMPLE ID �, am E U m m p E m m W a� cn m o mo n on N v o o w m X N W CD F- W ti C; o m F- y -o CO LAB SAMPLE 1D vC DQT7 _m p-OC FC C QJn c4 ul CC mY] OY rU o CIA N Q O ID JO cE C d oU aQ-} cn coo' b L rN av OC- m m W W N N u, N W U.3 '.P E Q E Q E U) ) _ Li tom O cod O u7 o o c O r a_d N = ` C7 W a Wo Cn co U) Us O m O Z i 7 2 Z m mO [ > Y O d 00 Q �U] N G 0 3 v X XUCI2INF81712024 rVm,A �(�I� N G A 2 X XUC12-INF 8/6/2024 �� 817l2024 5�0C 81712024 ®[� N Q A 2 o X X �J3 UC12-INF p r"1 8/712024 0611 N G A 2 Q X X Jly UC12-INF 81712024 6 �q N G A 2 o X X U�C( UC12-INF ' 816/2024 �� 8/7/2024 040 � 817/2024 0111 N Q P 1 � X X UC12-INF �/� 8/6/2024 � �� 8/7/2024 (} �[ D� 8/7/2024 j j N Q P 2 o X X vJ� Uc12-INF 817/2024 l� 5 N G P 1 N X X pelt fT UC12-INF 8/6/2024 oG 8/7/2024 �[� b 8/7/2024 �4 (� N Q P 1 X X X X UC12-INF VOA 8/612024 81712024 gCtD 817/2024 N Q P 1 S X X X Ja?j UC12 INF L 8!6l2024 Q�� 8/712024 (j� 817I2024 Q� (f N Q P 1 N X I I I I I ,X X I I 1 °C �C Comments: SHIPPED ON WET ICE PPP PI '-6 _L 11 Custody Seal Present: Custody Seal Number: Sample Temp at Collection: WF: �. EFF: 200.8 = Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,TI,Zn,Mo NOX - 48hour hold YES / NO Sample Temp at Receiving in Lab: INF: °C EFF: °C Sample Type Codes: Relinqu' hed by i ture): UCW Received by (Si ature): Dale: _ Time: y Q (Flow) = Automatic Flow Proportioned Sample03 T (Tlme) = Automatic Time Proportioned Sample Sample Temp of EFF Fecal Sample at Receiving in Lab (record -C o Uinf(Uished y (Siigriatur`e)? / Rec ived by (Signature)- Date: Time: only if collected): H (Eland) = Hand Composite Sample G (Grab) = Grab Sample // �{" ��L �. � ��, f A Zero Headspace & Teflon septa for YES NO NIA Relinq ished by (Signature): Received by (Signature): Date: Time: VOAs-.er m CoContaiType Codes: A =Amber Glass P -Plastic Samples in Proper Containers: YES NO NIA Relinquished by (Signature): Received by (Signature): Date: Time: z GL = Clear Glass B = Bag TL = Teflon Lined Cap Chlorinated Samples De- YES NO N/A Relinquished by (Signature): Received by (Signature): Date: Time: Chlorinated: VOA = 40 ml Glass vial P ge 101 of 133 r 9800 Kincey Ave #100 UC12 SEMI & 8/712024 COC#: PAGE j,� of 5 �j I'a Huntersville, NC 28078 (704) 875-9092 EVENT TYPE: - -AN - Pro Mgr.: Stephanie Knott g p 4 Sam d y (Sign Name): Clean Hand: Dirty H North Carolina Wastewater Certification #:12 SEND REPORT TO: Keith Purgasor ActtNum/Client ID: CLIENT Union County Water 8299 Kensington Dr Table#: Print Name: Clean Hands Dirty Ha ds FACILITY: Twelve Mile Creek WRF, NCO085359 I Waxhaw, NC 28173 Profile/ Template: 16076 ADDRESS: 8299 Kensington Drive, Waxhaw, NC 28173 keilh.purgason@unioncountync.gov Prelog/ Bottle Ord. ID EZ 3143104 ywl`l A rf f x% Sample Collection Data Sample Container Preservative Analyses Requested L� o t- O W a U o } P m o ca (3 w M a 0 = a N O N N LAB USE ONLY SAMPLE ID a� E �, v a7 a3 m p) Cl) m c CC] n m N M o M x �„ W �, p W �, O c v v [n a cn LAB SAMPLE ID cp c '� O v m °� co Cf) m a a Ni n uN-1 o N in v 0 v o @ o N Q W LU O Z M- .'moo m" v w 7 T rri m a 'C m m W Q (6 �- ra co T H .� O O CR u7 N N N I— N C1 U O N W rtiN Lo N O O Q] G) CD al NUC a w C111 CO Cn !Q CO o .CW =2 d ` ` CJ} cN N : o E E ra co m o a O Z Cl) cv n U 0 n co � co w� 0 Z FU o Ucu o �� C) LLI 24 Cn Cn U) Cn o mz==ZZZ m 0. 5 2?q 8//2024 N G GL 1UC12-EFF X X FFFIELD BLANK 8712024 N G GL 1 . X X Sample Temp at Collection: WF: °C EFF: °C Comments: SHIPPED ON WET ICE EFF L�HG SAMPLES Custody Seal Present: Custody Seal Number: 200.8 = Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,TI,Zn,Mo YES / NO Sample Temp at Receiving in Lab: INF: °C EFF: °C � Sample Type Codes: Q (Flow) =Automatic Flow Proportioned Sample T (Time) = Automatic Time Proportioned Sample Relinq ' y ( re): UCW �.,.. Received by (Signs re): - � /�� _ Date: ell Time: Sample Temp of EFF Fecal Sample at Receiving in Lab (record ,C o uishe by,(SignaCura} ;. Received by (Signature): Date: Time: only if collected): Pu H (Hand) = Hand Composite Sample G (Grab) = Grab Sample /IZero rRe�linj�uished Headspace 8. TeFlon septa for YES NO NIA by (Signature): Received by (Signature): Date: Time: VOAs: c Container Type Codes: A = Amber Glass P = Plastic Samples in Proper Containers: YES NO NIA o Relinquished by (Signature): Received by (Signature): Date: Time: a < GL = Clear Glass B = Bag TL = Teflon Lined Cap Chlorinated Samples De- YES NO N/A Relinquished by (Signature): Received by (Signature): Date: Time: Chlorinated: I VOA = 40 ml Glass vial P ge 102 of 133 9800 Kincey Ave #100 UC12 SEMI & 8!7l2024 COC#: PAGE 5 of f 5 Huntersville, NC 28078 (704) 875-9092 EVENT TYPE: - -AN Proj- Mgr.: Stephanie Knott Sampl y ign N e North Carolina Wastewater Certification #:12 SEND REPORT TO: Keith Purgason ACtftm/Client ID: CLIENT: Union County Water 8299 Kensington Dr Table#: R Kt Name: u ��!�� CG��y FACILITY: Twelve Mile Creek WRF, MC0085359 Waxhaw, NC 28173 Profile! Template: 16076 — ADDRESS: 8299 Kensington Drive, Waxhaw, NC 28173 keith.purgason@unioncountync.gov Prelog! Bottle Ord. ID EZ 3143104 Sample Collection Data Sample Container Preservative Analyses Requested w O --- vwi I— O Z w W Z U U o m a m w� a U o v o Ln ci•, a LAB USE ONLY SAMPLE ID m ECd aUO o mCD cQnc m CD 0 co cm �, t0oQ}to) 1� S1/ °3 H-EC U T Cnm N [V co O G NN LLJ M O W C W �P LO m M W W cn_d E aQ C7 aU-) W U-3C'A LO ) - OCN LU O ocn_ O. Vj a n cli O 03 lAf/tl) On) .YGC6 miv a- m CV (n U `G Li m@ rLAB jA/D mccu E @O O C n n c� t ct5' d5 O �' p �MP�L�Ei fJ Cn co m OC4 2 Z R' :5 3 o X X dy— tJCtxEfF — — — — — UC12-EFF �!! 817/2024 N 0 A 2c:' X X oo UC12-EFF �`�' 81612024 07U3 817/2024 8/7/2024 ( ,� N Q A 2 Q X X UC12•EFF 81712024 Q(,VQZJ N G A 2 o X X CA� UC12-EFF $l712Q24 �Qp N G A 2 o X X UC12-EFF lf�i 81612024 p o 817l2024 OLD 8I7l2024 (�pD N Q P 1 X X u�� UC12-EFF 816l2024 07(13 012024 j 8l712024 �[)J� N Q P 2 o X X UC12-EFF 8f7l2024 �(9�� N G P 1 X X U�b UC12•EFF i 8I612024 G7U 817l2024 8l712024 �� N Q P 1 r X X X X �a� UC12•EFF 1 8/612024 07(�3 8/712024 (aU� 81712024 N Q P 1 N X X X UC12-EFF %l1`r/ 81612024 G-7& 3 81712024 j�j 817/2024 0(0 N 0 P 1 U X X X vJ-7 Comments: SHIPPED ON WET ICE Pl"A ZjANIFLt6 Custody Seal Present: Custody Seal Number: Sample Temp at Collection: INF: °C EFF: ,' °C 200.8 = Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,TI,Zn,Mo NOX - 48hour hold YES ! NO Sample Temp at Receiving in Lab: INF: °C EFF: °C Sample Type Codes: Reli �j�si by (S' at Receive by� 5-i rjatur �j�4�j;._.��z�/ Date; Time: � o Q (Flow) =Automatic Flow Proportioned Sample T (Time) = Automatic Time Proportioned Sample ,.,. �f Sample Temp of EFF Fecal Sample at Receiving in Lab (record °C Ret quisl ed by ISggnatute): / Received by (Signature): Date: Time: only if collected}: T H (Hand) = Hand Composite Sample G (Grab} = Grab Sample Zero Headspace & Teflon septa for YES NO NIA Relinqu shed by (Signature): Received by (Signature): Date: Time: VOAs Container Type Codes: A =Amber Glass P =Plastic Relinquished by (Signature): Received by {Signature}: Date: Time: Samples in Proper Containers: YES NO NIA o GL = Clear Glass B = Bag TL = Teflon Lined Cap Chlorinated Samples De- YES NO NIA < Relinquished by (Signature): I Received by (Signature): I Date: Time: Chlorinated: VOA = 40 ml Glass vial Page 103 of 133 9800 Kincey Ave #100 UC12 SEMI & 81712024 COC#: PAGE f _ of ace Huntersville, NC 28078 (704) 875-9092 EVENT TYPE: - -AN - Proj. Mgr.: Stephanie Knott Lx Sampl (Sig)pNape), 111 North Carolina Wastewater Certification #:12 SEND REPORT TO: Keith Purgason ActtNumlClient ID. CLIENT Union County Water 8299 Kensington Dr Table#: „� C P nt Name: FACILITY Twelve Mile Creek WRF, NCO085359 Waxhaw, NC 28173 Profilel Template: 16076 ADDRESS: 8299 Kensington Drive, Waxhaw, NC 28173 keith.purgason@unioncountync.gov Prelogl Bode Ord, ID EZ 3143104 Sample Collection Data 3ample Contairel Preservative Analyses Requested o T w LU O Uj Uj U z r O W N m o r o Q u�-� M Q CL c� � CM v N LAB USE ONLY SAMPLE ID _ E Q, m E CO � C!} w Q m m m o N ,ter, M X Vl o cn � W C. o CD CL g o LAB SAMPLE ID V, co d C ram. fd I.._ U �"� T (7 V] ^ N C N' e, O lQ �V Q uy O �"� N Q O N Md ` [n a E co C.. GOuD ti LLO lf] -0 O} Q1 � LLJR @ o u') CV Ln 47 N U) a. ID C= CL V i CN U u. N ! , (� N Qp om Q CL Q C- U47 J LLJ � O O Co E ` 'oN E E co E z O z cy c O M M O O O c s U) CD CO' oE 17 -6 ( 6 (S O w w m, oo Z 2--7 c) m U) cq U -t CD = ;E Z M 4 CL � N Q P 1 0 Q x x `7 UC12-EFF %VC— 8/612024 670 81712024 6b0� 817/2024 N Q P 1 a x _ x _ _ e, -7 UC12•EFF OC_ 81612024 0703 817/2024 OIkv! 817/2024 Q N Q P 1 X X Jv� UC12•EFF %/X_, 8/612024 6703 81712024 �� 817l2024 N Q P 1 n x x v�7 Sample Temp at Collection: NF: °C EFF: C} °C Comments: SHIPPED ON WET ICE EFF SEMI-ANNUAL SAMPLES Custody Seal Present: Custody Seal Number: ,� 200.8 = Sb,As,Be,Cd,Cr,Cu,Pb,N1,Se,Ag,TI,Zn,Mo YES 1 NO Temp Receiving in Lab: INF: °G EFF: °C Sample Type Codes: Relin h by (Sig re Receive by (Signature): // Date: Tjmej Sample at p P g y Q (Flow) = Automatic Flow Proportioned Sample T (Time) = Automatic Time Proportioned Sample ` 2 '1,/,) C- j 'f�7'�i j !! Sample Temp of EFF Fecal Sample at Receiving in Lab °C o Rel uished by Signatur ): 4 Received by (Signature): Date: Time: (record only if collected): 0 H (Hand) = Hand Composite Sample G (Grab) = Grab Sample Zero Headspace & Teflon septa for YES NO NIA Relinqu s ed by Signature): Received by (Signature): Date: Time: VOAs: a Container Type Codes: A -Amber Glass P =Plastic Samples in Proper Containers: YES NO N/A Relinquished by (Signature): Received by (Signature): Date: Time: Z GL = Clear Glass B = Bag TL = Teflon Lined Cap Chlorinated Samples De- YES NO NIA _< Relinquished by (Signature): Received by (Signature): Date: Time: Chlorinated: VOA = 40 mi &ass viai Pa e 104 of 133 9800 Kincev Ave #100 ^, r r� / Pace Huntersville, NC 28078 (704) 875-9092 EVENT TYPE: UC12 - SEMI -AN & - 81712024 Proj. Mgr.: Stephanie Knott ActtNumlClient ID: Sampled by (Sign Name): North Carolina Wastewater Certification #:12 SEND REPORT TO: Keith Purgason Table#: IP CLIENT: Union County Water 8299 Kensington Dr Profilel Template: 16076Name. ( P FACILITY: Twelve Mile Creek WRF, NCO085359Waxhaw, NC 28173 ul� AQQRESS: 8299 Kensington Drive, Waxhaw, NC 28173 keith,purgason@unloncountync.gov Prelog] Bottle Ord. ID l"lPo Sample Collection Data Sample Container Preservative Analyses Requested Uj F O W Z U o ? — p C� �0 o r o C1 Q w U', M Q w c Z [L U o W x d rr U =o N LAB USE ONLY SAMPLE ID a, E E a °' °' m o E m 00 0 o cn m o IX1 o m v o N,, M x� .�� w r, ^ o o Q m v� m� LAB SAMPLE 1D U U }, ` --- C'j NN " O w LC' 0 aVCDC 2Ny o w00 vLa`iJ' � -�ooa} E Q m W N 2 N 2 N n Cn N.` n a Q f W ~rt u] rn E C W Z co O O co O N 0 � O O COC7 � W � s OMw, � 2 n U wE c 0 i :E U M O O N a O O J) u 7 C Ocd 5Cn y� !2 24 817/2024 N T P 1 N X X U UC12-FCE (`-� 8I6l2024 Oda 8/712024 d �G� 8!7l2024 (}1pGq N T P 1 0 a X X UC12-FCE 81612024g 81712024 �8l712024 OIpO�[ N T P 1 a X X l/ UC12-FCE tom- 817/2024 ��5 N G P 1 Lo � UC12-FCE 8/612024 8912024 U V39 81712024 G� N T P i N X X UD�i UC12-FCE 8/612024 8!•712024 0b09 8l712024 6bU� N T P 1 X X UC12-FCE �'( 8/6/2024 817/2024 OW 81712024 �506� N T P 1 u' X X X UC12-FCE 816l2024 �� 8/712024 Obog 8/7/2024 d(�q N T P 1 X X UC12-FCE 8/612024 8/7/2024 8/712024 0 bt { N T P 1 N X X Comments: SHIPPED ON WET ICE Custody Seal Present: Custody Seal Number: Sample Temp at Collection: INF: °C EFF: °C 200.8 = Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,TI,Zn,Mo YES ! NO Sample Temp Receiving in Lab: WF: °C EFF: oC Sample Type Codes: Relinquished by (Signature : UCW Receive by (S'gryaturt. ;' e: Time- 7 at q (Flow) = Automatic Flow Proportioned Sample T (Time) = Automatic Time Proportioned Sample Sample Temp of EFF Fecal Sample at Receiving in Lab (record aC o R uished by,(Signtur ) " Recei ed by (Signature): ff Y.~ %7/- i Date: Time: only if collected): 0 H (Hand) = Hand Composite Sample G (Grab) = Grab Sample '',k / �- I tr . -ef-' Zero Headspace & Teflon septa for YES NO NIA Relin uished by (Signature): Received by (Signature): Date: Time: VOAs: < c Container Type Codes: A = Amber Glass P = Plastic Relinquished by (Signature): Received by (Signature): Date: Time: Samples in Proper Containers: YES NO NIA z GL = Clear Glass B - Bag TL = Teflon Lined Cap Chlorinated Samples De- YES NO NIA Relinquished by (Signature): Received by (Signature): Date: Time: Chlorinated: Lj VOA = 40 ml Glass vial I Pape 105 of 133 9800 Kincey Ave #100 UC12 & 817J2024 COC#: PAGE Q of S Pace Huntersville, NC 28078 704 875.9092 EVENT TYPE: -SEMI-AN ( } Proj. Mgr.; Stephanie Knott (� North Carolina Wastewater Certification #:12 SEND REPORT TO: Keith Purgason ACttNUm/Client ID. Sampled by Sign Name): i CLIENT: Union County Water 8299 Kensington Dr Table#: FACILITY: Twelve Mile Creek WRF, NCO085359 U Waxhaw, NC 28173 Profile/ Template: 16076 Print Name: ADDRESS: 8299 Kensington Drive, Waxhaw, NC 28173 keith.purgason@urioncounlync.gov Prelogl Bottle Ord. ID EZ 3143101 Sample Collection Data Sample Container Preservative Analyses Requested - cq w D H OLU W V U o 'O Z_ }i O �_ M r M C) C] N SAMPLE ID CD °; r E m m °� m N m o w a �' o a v LAB USE ONLY >✓ C Q7 O m C1 O m Cr1 M X N fn ' W rC M f� C1 M `7 cD qT -0 UJ LAB SAMPLE ID -C -U CU u7 W d 7. N .--. E tNfJ r N LO O N N m O r d O � C1 47 N (� O N d W O Z Lo [r7 O � O �C7 Co U5 O Q , cT ' O L t1 O tl�J _ .0 CO N m LJJ C W Q E Q � a � Q I— ~ fit _C � dJ N C'7 (n 2 C/'1 y' � CV � N � CJ] U UJ '.' d Q O �= � O N d W N �n W W � L � N N � ~ O � N Q 47 E, c CD o a C/z Cn y C O a C m CO c> U, m W m O= 0 c\j 1t7 0 uD Cn Cii U) J .� .[a O Z W d d c C7 O c -0 2 Lo E E CO E E ro E f9 m s E c O O — z O O Z co N O C. U N (o O m D O O O 7 W x E v Z m m U 7 �D _o C7 q5 C7 U O w 7 CU ([7 UJ CO Cn Cn Cn W F- U m O co Z 2 2 Z S Z C17 Cn [fJ -C d = Y O 2 J J Z W' O _2G24 � I�:89�2024'�i �4 I N T P 1 G X X X It UC12-MLSS 816/2024 (� �� ' g8/7/2024 r(v ` 89/2024 i; �U 9 N T P 1 N X X p[ UC12-MLSS 817/2024 `�J�� N G P 1 N X X 0 ('L UC12-MLSS cl 8/612024 Jyl� 8f712024 r,16 817/2024 -qo N r P 1 x x or( UC12-MLSS 81612024 ii �l 8/712024 (;110 3 817/2024 iUo9 N T P 1 r X x X X UC12-MLSS [, 816/2024 t)Yls; 8/7/2024 81712024 C ic! N T P 1 N X X x UC12-MLSS {j " 81712024 N G VO 3 X X 0( UC12-MLSS 8r712024 `{'¢ L A 2 o XTi UC12-MLSS % 816/2024 ):11 8/712024 ;_,:.ra $1712024 tNT A 2 X X J i� Comments: SHIPPED ON WET ICE Custody Seal Present: Custody Seal Number: Sample Temp at Collection: INF: °C EFF. °C 200.8 = Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,TI,Zn,Mo NOX • 48hour hold YES f NO Temp Receiving in Lab: INF: °C EFF: °C Sample Type Codes: Relinquished by (Signature): UCW eceive by (Signature): ,, Date- Time - Sample at Q = Automatic Flow Proportioned Sample (Flow) T (Time) = Automatic Time Proportioned Sample 7,4 ; Sample Temp of EFF Fecal Sample at Receiving in Lab (record °C 0 Relinquished by. (Sign to e): Recei ed by (Signature): Dat : Time: only if collected): 0 H (Hand) =Hand Composite Sample G (Grab) = Grab Sample / �n✓ 7 Zero Headspace & Teflon septa for YES NO NIA Relinquished by (Signature): Received by (Signature): Date: Time: VOAs: o Container Type Codes: A = Amber Glass P = Plastic Samples in Proper Containers: YES NO NIA Relinquished by (Signature): Received by (Signature): Date: Time: z GL =Clear Glass B =Bag TL = Teflon Lined Cap Chlorinated Samples De- YES NO NIA Relinquished by (Signature): Received by (Signature): Date: Time: Chlorinated: VOA = 40 ml Glass vial P ge 106 of 133 9800 Kincey Ave #100 UC12 SEMI & 81712024 Va COC#: PAGE of - -AN - �'� Huntersville, NC 28078 (704) 875-9092 EVENT TYPE: Proj. Mgr.: Stephanie Knott Sampled by (Sign Name: North Carolina Wastewater Certification #:12 SEND REPORT TO: Keith Purgason AGttNunn/Uent ID: CLIENT: Union County Water 8299 Kensington Dr Table#: m t Name: CPo FACILITY: Twelve Mile Creek WRF, NCO085359 Waxhaw, NC 28173 Profile/ Template: 16076 ADDRESS: 8299 Kensington Drive, Waxhaw, NC 28173 keith.purgason@Lnloncountync.gov Prelogl Bottle Ord. ID C e Sample Collection Data Sample Container Preservative Analyses Requested 0 0 Z w Z o m c �q Q w Q °- w n. v c a O N LAB USE ONLY SAMPLE ID (O E Q7 �' O E ?� °�° QJ m O O W m ' ry c,-i M X N N W �,.� o O V V -O V1 .a (!) LAB SAMPLE ID C C '� (� -0 O U Q7 U u: T CJ} O T rC N u7 N Ln O N N m O V O V O ia�i-.� m O N Q �- w O ? S`J O -C [� -O O co T Q C C N ch Q d c.o •— eTa O "� y7 tri aJ a C — m N m a w C W d E �" a~ .� �2 O N i.n U3 �r's N N "C U) ~ U T ' 'C �.' Q a Q p 'U in O N D_ w . N w w C7 N ti N N O P U O o O nwE o cn o .� o dO m oa � x o mfO o z O cry U N U w E E E E O O N o ci f U) c 7 Ea Yw U % 34'OWO U Co to U] Cn Uco 0 03 Z 7: 2 Z S Z In 2 d _5 2 cr 10 O o x x x UC12-RAS 81612024 1i{ g 817/2024 6343 817/2024 03LVj N H P 1 N X x (1 (3 UC12-RAS 8/712024 03`� I N G P 1 C X x �t� UC12-RAS 816l2024 f t�� 8f712024 0343 817/2024 G3y1 N H P 1 N CD x x 0(�J UC12-RAS 8/6/2024 MY 8/712024 0343 8/712024 03 Lj{ N H P 1 r X x UC 12-RAS 8/6/2024 ) t l 81712024 0 3 L13 8l712024 6� k j N H P 1 N x x UC12-RAS 8/6/2024 1110 81712024 634- 81712024 O�j�� N H P 1 r x X 1</ Comments: SHIPPED ON WET ICE Custody Seal Present: Custody Seal Number: Sample Temp at Collection: INF: �C EFF: °C 200.8 = Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,TI,Zn,Mo YES I NO Sample Temp at Receiving in Lab: iNF: °C EFF: aC Sample Type Codes: Relinquished by Signature : UCW Received by (Signature)• 7 ` l ` Date: J L Time: Q (Flow) = Automatic Flow Proportioned Sample ) p p T (Time) = Automatic Time Proportioned Sample 1 I 1 ]Date. ] r Sample Temp of EFF Fecal Sample at Receiving in Lab (record oC 0 quished by (Signature): ` 1 �'� Received by (Signature): /y ? Time: onlyif collected): 1 0 H Hand = Hard Composite Sample (Hand) p p G (Grab) = Grab Sample / ,- ` -/� ,t f �` ti. -' (ice Zero Headspace & Teflon septa for YES NO NIA Relinquished by (Si nature): Received by (Signature): Date: Time: VOAs: m Container Type Codes: A = Amber Glass P = Plastic Samples in Proper Containers: YES NO NIA Relinquished by (Signature): Received by (Signature): Date: Time: z GL = Clear Glass B = Bag TL = Teflon Lined Cap Chlorinated Samples De- YES NO NIA < Relinquished by (Signature): Received by (Signature): Date: Time: Chlorinated: VOA = 40 ml Glass vial Pli Ige 107 of 133 9a00 Kincey Ave #100 COC#: PAGE O of ` ace Huntersville, NC 28078 (704) 875.9092 EVENT TYPE: UC12 - SEMI -AN & - 81712024 Pro;. Mgr.: Stephanie Knott Sampled by (Sign Name): North Carolina Wastewater Certification #:12 SEND REPORT TO: Keith Purgason AcMum/Client ID: CLIENT: Union County Water 8299 Kensington Dr Table#: - z- ri erne: FACILITY: Twelve Mile Creek WRF, NCO085359 ) Waxhaw, NO 28173 Profile/ Template: 16076 ADDRESS: 8299 Kensington Drive, Waxhaw, NC 28173 keith.purgason@unioncountync.gov Prelogl Bottle Ord. ID aV.AyV_�' Ivu Sample Collection Data Sample Container Preservative Analyses Requested LU W p o r co 0 Z w Z U o SAMPLE ID °7 ° 'O " Z } m O m a m " ro'J w M `� �o w = rL N O a N N LAB USE ONLY E m a °J E OQ ' c u�i X N cn w M n O cln11 `* '� a U) CO LAB SAMPLE ID °1 Q 0- CD m E N ' CD N U'J M a� LO 0 Q U) 0VJ 7, N a Qm O '+a MQCM o cn Q CY QU d u'Nc;! isi m m w w E o E cN O fA � -' O ua' N w cn ucNo) E E E c E o — Lu O r E 7 ` = con v U P o 0abuj n ! i (n cn t oziQ 5 , O rJ/ 2G� f UC12-WAS 1612024 11 817/2024 3 3 8(712024 3 N H P 1 o X X X [ S UC12-WAS 8/612024 1 ! I' 81712024 0313 8/712024 o3�g N H P 1 N X X C l5 UC12-WAS 81712024 N G P 1 Lo r X X 0 �� UC12-WAS Taw 8/6/2024 I I �' 817/2024 C.3 8I7l2024 n3 L N H P 1 N X X O( S UC12-WAS 8I612024 I i 1 817/2024 C)3� 817/2024 v3�S N H P 1, X x UC12-WAS 8/612024 ) j I K 817024 ' 012024 3u{ N H P 1 Y X X X L/ Sample Temp at Collection: INF: °C EFF. °C Comments: SHIPPED ON WET ICE Custody Seal Present: Custody Seal Number: 200.8 = Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,TI,Zn,Mo YES / NO Sample Temp at Receiving in Lab: INF: °C EFF: °C Sample Type Codes: Relinquished by (Signature): UCW eived y, 5ignature :- i Datg: Time: �n 0 (Flow) = Automatic Flow Proportioned Sample T (Time) = Automatic Time Proportioned Sample �i�' '�Gca Sample Temp of EFF Fecal Sample at Receiving in Lab (record °C 0 Reli ished by (Signature}: l Red iv d by (Signaturer /" ` Date: Time: only if collected): H (Hand) = Hand Composite Sample G (Grab) = Grab Sample `-- 7 /I / Zero Headspace & Teflon septa for YES NO NIA Relinquished by (Signature): Received by (Signature): Date: Time: VOAs: Container Type Codes: A =Amber Glass P =Plastic Samples in Proper Containers: YES NO N/A m Relinquished by (Signature): Received by (Signature): Date: Time: z < GL =Clear Glass B =Bag TL = Teflon Lined Cap Chlorinated Samples De- YES NO NIA Relinquished by (Signature): Received by (Signature): Date: ELI Chlorinated: VOA = 40 ml Glass vial Pa 9800 Kincey Ave #100 COC#: PAGE I 1 of `ace Huntersville, NC 28078 (704) 875-9092 EVENT TYPE: UC12 - SEMI -AN & - 81712024 Proj. Mgr.: Stephanie KnotE l ` Sampled py Sin Name) - (((((( + North Carolina Wastewater Certification #:12 SEND REPORT TO: Keith Purgason ActtNum/Client ID: Table#: CLIENT: Union County Water 8299 Kensington Dr ini ame'. FACILITY: Twelve Mile Creek WRF, NCO085359 77 Waxhaw, NC 28173 Profile/ Template: 16076 ADDRESS- 8299 Kensington Drive, Waxhaw, NC 28173 keith.purgason@unioncountync.gov Prelogl Bottle Ord. ID EZ 3143105 Sample Collection Data Sample Container Preservative Analyses Requested _ w � O W Z U a ' r 3 m o L Q a, w N U CM N LAB USE ONLY SAMPLE ID a� E @ QD m _m °J E p 0 m N s 60 m O m O m v m N� M [+] X N "' 0 o `D i — W �;y n c o M CAP ~ [�O n -o 2 C/'1 a U) LAB SAMPLE ID Q ~ [� P U ?. C N � N Y7 O N CV m O � U O . O Q' N C6 O F N Lo (n Q d W O Z Y '0 M i O In a 'U co C cp Q O C. N Q Q t-- �D , 'C eti [O O "O 4) 7 �C d C CO W C d W F _0 Q H ~ _ T2 N_ CA rC fn tl'1 Y7 N 47 N L VJ J ' [o 'C. Q R Q to O vi aj O N d l!J N n w W C.'] CV ti y7 N N - 0 v, y E E E rL E a m E rL °� E E c c o U u7 w z c-3 O C) O0 w O O c.i Cl) n p O a u7 cn U] cn o act .S c o E Z W z Q �a d m , @ O 2 d o `o 2 L7 cn (� O cfl j _ a a o fr J� �� co ra M co co U) fn co M c� to O F- 0 m o 0 o m O Z Z" = -r M Z U 2 m z m O [m O cn u7 0. x E _ Y o U a —, co 2 Ks27 cc S o x x tUC12-INFDIST8/6/2024 0� 8/7/2024 r�A �tr L1 8/7/2024 objrN T P 1 N X x c9UG12-INFDIST 817/2024 ��2 N G P 1 N X x 0( O UC12-INFDIST 816/2024 8/712024 �Zi $l712024 ��'�� N T P 1 N x x v 1`7 UC12-INFDIST 8/6/2024 b� 817/2024 �j 8/712024 �� j N T P 1 X X x x r! UC12-INFDIST 4ro� 816/2024 817/2024 Z� 8/7/2024 �� N T P 1 n X X X V UC12-INFDIST l�Yl 817/2024 ��,� N G 0 3 X x UC12INFDIST 8(712024 �j� N G A 2 X X UC12-INFDIST $1712024 r0� OC 1 N G A 2 0> X x UC12ANFDIST IN'` 81612024 8/712024 ! �eti� 817/2024 j j� N T P i Q x x 0 [� UC12-INFDIST �TJI 8/6/2024 0(0 ( 81712024 OGtit 81712024 �G�,�j N T P 1 C x X 0(1 Comments: SHIPPED ON WET ICE Custody Seal Present: Custody Seal Number: Sample Temp at Collection: INF: °C EFF: 200.8 = Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,TI,Zn,Mo NOX - 48hour hold YES 1 NO Temp Receiving in Lab: INF: -C EFF: °C Sample Type Codes: Req ui edby (Si re}; UCW Received by (Signature}: ! Date: Time: . Sample at � Q (Flow) = Automatic Flow ProporEioned Sample T (Time) = Automatic Time Proportioned Sample Sample Temp of EFF Fecal Sample at Receiving in Lab (recordL_ oC ao o Re inquished by ( ignatu ): Received by (Signature): Date: Time: only if collected): H (Hand) = Hand Composite Sample G (Grab) =Grab Sample 1.1 (� Zero Headspace & Teflon septa for YES NO NIA Relinqui hed by (Signature): Received by (Signature): Date: Time: VOAs: o Container Type Codes: A = Amber Glass P = Plastic Relinquished by (Signature): Received by (Signature): Date: Time: Samples in Proper Containers: YES NO NIA z GL = Clear Glass B = Bag TL = Teflon Lined Cap Chlorinated Samples De- YES NO NIA < Relinquished by (Signature): Received by (Signature): Date: Pa Time: e 109 of 133 Chlorinated: VOA = 40 ml Glass vial 9800 Kincey Ave #100 UC12 SEMI & 81712024 �ace COC#: PAGE q of Huntersville, NC 28078 (704) 875-9092 EVENT TYPE: • -AN - Proj. Mgr.: Stephanie Knott l Sampled by Sign Namee))__, North Carolina Wastewater Certification #:12 SEND REPORT TO: Keith Purgason AottNum/Client ID: CLIENT: Union County Water 8299 Kensington Dr Table#: � Print Name: FACILITY: Twelve Mile Creek WRF, NCO085359 Waxhaw, NC 28173 Profile/ Template: 16076 ADDRESS: 8299 Kensington Drive, Waxhaw, NC 28173 keith.purgason@unioncountync.gov Prelogl Bottle Ord. ID 606r, —, I Sample Collection Data Sample Container Preservative Analyses Requested w o O W U O M o m `- 4 w M °a v W = N V C o v r N LAB USE ONLY SAMPLE !D m 1= E °' m u) m o m v N "' xo `„ "' r CD o r u> o LAB SAMPLE ID a ZI7 N (!) Q U] Ln N U) o N N m G V a C1 o V U O N d m Z y� _U_j" 0 -d r < CD N Q CAD o in cCS CD O) m m a CL d F- C C N O In U) [n � W H iA7 .� ¢ CZ d C] O N LL (7 r1 N N O N a a d 2 fn C Q_ C (6 O U UJC14 N L J C7 Q = Clj Q L17 fn i [n i co U O . C .ro C O z N ll.r L i U d `m N U N C -0 (fj fn fD }+ C 4] -t7 O E m E M E cv E co ca °' co t c a o — o Z O O Z cn cr O co C� N co O m 0 d o O co ul cn cA cn a a � E E = Z Y m o U _ m o r C? ou C7 ds U O� Ua ' m �� co c o cn co cn o U m z= x z= z m -c a d a z ^:'I", ,$ N H P 2 cm X X X ^. 8I612024 I i 817I2024 `; I 'J 8712024 r� _ 5U N H P 1 -CILUC12-BFP-1"CAKE N X X CiC� UC12-BFP-I-CAKE 817/2024 1�r1 Li N G P 1 r X X UC12-BFP-i-CAKE (� 8/6/2024 l i j I 012024 C i 1 5 81712Q24 J j j C% N H P 1 N X X 06 1-1C12-BFP-I-CAKE Lr^ 8/612024 } I i 1 B1712024 ;I 5 817/2024 N H P 1 C- X X 06 UC12-BFP-I-CAKE 8/612024 1 1 8/7/2024 C 1 , 817/2024 C} _ J v N H P 1 r X X X 0 — I—FFF 7—_ Comments: SHIPPED ON WET ICE Custody Seal Present: Custody Seal Number: Sample Temp at Collection: NF: °C EFF: °C 200.8 = Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,TI,Zn,Mo YES 1 NO Sample Temp at Receiving in Lab: INF: °C EFF: °C Sample Tvpe Codes: O (Flow) =Automatic Flaw Propo boned Sample T (Time) = Automatic Time Proportioned Sample Relinquished by (Signature): UCW _� . ec ived by (Signature]: �' I� r U /� P Date: �� '� Time: � t Sample Temp of EFF Fecal Sample at Receiving in Lab (record ,C o ReliJnquished by [Signature):. Receiv d by (Signature): Date: Time: only it collected): H (Hand) = Hand Composite Sample G (Grab) = Grab Sample L- �' r'� % r 1 %vu Zero Headspace & Teflon septa for YES NO NIA Relinq ished by (Signature): Received by (Signature): Date: Time: VOAs: c Container Type Codes: A =Amber Glass P = Plastic Samples in Proper Containers: YES NO N/A m Relinquished by (Signature): Received by (Signature): Date: Time: s < GL = Clear Glass B = Bag TL = Teflon Lined Cap Chlorinated Samples De- YES NO NIA Relinquished by (Signature): Received by (Signature): Date: I Time: Chlorinated: VOA = 40 ml Glass vial Pape 110 of 133 9800 Kincey Ave #100 Face COC#: PAGE of Huntersville, NC 28078 (704) 875-9092 EVENT TYPE: UC12 - SEMI -AN & - 8/712024 Proj. Mgr.: Stephanie Knott 3 Sampled by Sign Name): North Carolina Wastewater Certification #A2 SEND REPORT TO: Keith Purgason AcMum/Client ID: CLIENT: Union County Water 8299 Kensington Dr Table#: Print Name: FACILITY: Twelve Mile Creek WRF, NCO085359 I l Waxhaw, NC 28173 Profile/ Template: 46476 ADDRESS: 8299 Kensington Drive, Waxhaw, NC 28173 � keith.purgason@unioncounlync.gov Prelog/ Bottle Ord. ID Sample Collection Data Sample Container Preservative Analyses Requested cry w o r O W Z V CD °J a " Z 3 �a�i m CD m `- o Q CL � �' a- � L) W = z N U o a - c14 LAB USE ONLY SAMPLE ID °' [O CU E Q7 °' O °3 47 CD m O� co O m M M X W VJ p `D ~ L' M O O d `— cp p O LAB SAMPLE ID aD E ,N N u, NO N C) v C) v V Ln _ O 0 N Q O z N 'r' C t VI o °O CO O c (w'1 Q to `' CD O r U, m 'C l'll m N rC 61 d (� E fV � (p }C-, ~ H N .ro N O Cn ' N N Cn U J .� C z Q d n U O N a N N W w (,'J N 1 N N F_ O [Nf1 Q Q 2 aj n c '� a 'cc—o c j Lu <n Q Z Lo C7 va -o _c C a� a a C7 c f3] 2 V] 0 E m E E c > o E m 2 m E o L E m c o a � o z O 0 z cn c� O n U cv v O m o 0 o 0 M cn cry cn u7 a�i ro x E E m - Z X m� o CJ � z-2 m `o t C7 �f CJ w1 U p� w 2 a ro `O g Z� �j cn u7 cn UJ cn 0 H U m 7 Z S Z 2 z m 4 2>_ _j 2 > Of� RUj2n24f N G P 1 N x x UC12-BFP•1•FILT 817I2024 Cr 5 N G P 1 0 o X X UC12-BFP-1-FILT n 817/2024 jr- C N G P 1 0 Q X X UC12-BFP-I-FILT iln 8/7/2024 C�q N G P 1 r X x UC12-BFP-I-FILT rn 8I712024 Gf'y! 5 N G P 1 0 N X x UC12-13F13-I-FILT 81712024 L�j C N G P 1 N X x UC12•BFP•1-FILT 817024 o 5) 5 N G P 1 N X x UC12-BFP-I-FILT r^ 817/2024 p;+ S N G P 1 r X X x UC12-BFP-I-FILT C�^, 8/712024 ri)S N G P 1 X x v Comments: SHIPPED ON WET ICE Custody Seal Present: Custody Seal Number: Sample Temp at Collection: INF: °C EFF: °C 200.8 = Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,TI,Zn,Mo YES 1 NO Sample Temp at Receiving in Lab: INF: °C EFF: °C Sample Type Codes: Q (Flow) = Automatic Flow Proportioned Sample T (Time) = Automatic Time Proportioned Sample Relinquished by (Signature): UCW Received b (Signat a �Y r •� Date: �, Time: Sample Temp of EFF Fecal Sample at Receiving in Lab (record -rfcollected): °C o Relinquished by (Signature: Receive by (Signature): Date: Time: only H (Hand) = Hand Composite Sample G (Grab) - Grab Sample ! " AVlu'i 'fUw Zero Headspace & Teflon septa for YES NO N1A Relinquished by (Signature): Received by (Signature): Date: Time: VOAs: < Container Type Codes: A = Amber Glass P = Plastic Samples in Proper Containers: YES NO NIA m Relinquished by (Signature): Received by (Signature): Date: Time: z < GL = Clear Glass B = Bag TL = Teflon tined Cap Chlorinated Samples De- YES NO N/A Relinquished by (Signature): Received by (Signature): Date: Time: Chlorinated: VOA = 40 ml Glass vial Pa e 111 of 133 9800 Kincey Ave #100 UC12 SEMI & 81712024 COC#: PAGE of _ I�Face Huntersville, NC 28078 (704) 875.9092 EVENT TYPE: - -AN - Proj. Mgr.: Stephanie Knott t Sampled by (Sign Name): North Carolina Wastewater Certification #:12 SEND REPORT TO: Keith Purgason ACttNumlClient ID: CLIENT: Union County Water 8299 Kensington Dr Table#: Pri ame: FACILITY Twelve Mile Creek WRF, NCO085359 Waxhaw, NC 28173 Proftlel Template: 16076 ADDRESS: 8299 Kensington Drive, Waxhaw, NC 28173 Keith.purgason@unioncountync.gov Prelog! Bottle Ord. ID 11�- 66G� e �cgf'(C� Sample Collection Data 5ampie Container Preservative Analyses Requested LU w O Z w z U U o SAMPLE ID �, O Z } m 0 °' o �, m o w M a w co o • L o w a N G v ti N o LAB USE ONLY m E a� Q1 o EEi �? in a m a o Co 4 a v ro N� N Q o ep co ^- o M o CO o v3 LAB SAMPLE ID O1 � L4 0. E a Q Q. C .@ C N u7 a Cl) N "' N l(') O 11'1 N O fV C N H [n w Z N �"' Q fiJ O cm Q N d i ffl 7 H L v cv i--- 7 Q7 L1 Q7 w N E Cl"/ C C CO C'J O C14.T ct7 [A W '� ' ro _ z w -C N N w fll N S L/J N ti +n 6 E E E E m E °7 E p L F c o U 0 0 z o z p N 0 M c� N M O m Ln o 0 o Ln L; W m w s E E 5 Z m m ° 2 o U ou C7 CJ w Z U7 (n fn U} C7 1- U m z 2 2 Z 2 Z m �„ �„ 0. x o c} 0. 5_ 2 o o UC12.1 2 AER $1612024 817I2024 0 4068(712024 d(0 N T P i 0 o X X X UC12.1_2AER C7( 81612024 091t0 8f712024 0405 8l712024 04010 N T P 1 ry X X 0 -1,Z UC12.1_2AER 8/7/2024 DLl0q N G P 1 Lo X X �23 UC12-1_2 AER 816/2024 GLAI ro 8/712024 0 405 81712024 0 `i O( N T P 1 N X X VZZ 1 T L-L] Sample Temp at Collection: INF: °C EFF: °C Comments: SHIPPED ON WET ICE Custody Seat Present: Custody Seal Number- 200.8 = Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,TI,Zn,Mo YES /NO Sample Temp at Receiving in Lab: INF: °C EFF: 'C r— Sample Type Codes: Relinquished by (Signature : UCW Received by (Signature): i ��. Date: Time: n Q (Flow) = Automatic Flow Proportioned Sample T (Time) = Automatic Time Proportioned Sample �'� Sample Temp of EFF Fecal Sample at Receiving in Lab (record °C O Re wish d br (Signature):,, �'� Recei ed by (Sig tdrej: `'i! �! ' �- Date: Time: only if collected): 0 H (Hand) = Hand Composite Sample G (Grab) = Grab Sample " �_ '� } = L: `: lTv (� -tLl Zero Headspace & Teflon septa for YES NO NIA Relinquished by (Signature): Received by (Signature): Date: Time: VOAs: Container_Type Codes: A = Amber Glass P = Plastic Samples in Proper Containers: YES NO N/A rrnn Relinquished by (Signature): Received by (Signature): Date: Time: z GL =Clear Glass B =Bag TL = Teflon Lined Cap Chlorinated Samples De- YES NO WA < Relinquished by (Signature): Received by (Signature): Date: Time: Chlorinated: VOA = 40 ml Glass vial P ge 112 of 133 9800 Kincey Ave #106 COC#: PAGE of ace Huntersville, NC 28078 (704) 875-9092 EVENT TYPE: UC12 - SEMI -AN & - 817/2024 Proj. Mgr,; Stephanie Knott Sampled by (Sign Name): North Carolina Wastewater Certification #:12 SEND REPORT TO: Keith Purgason AottNum/Client ID: CLIENT: Union County Water 8299 Kensington Dr Table#; - not e' FACILITY: Twelve Mile Creek WRF, NCO085359 Waxhaw, NC 28173 Profile/ Template: 16076 ADDRESS: 8299 Kensington Drive, Waxhaw, NC 28173 keith.purgason@unioncourtync.gov Prelogl Bottle Ord. ID Sample Collection Data Sample Cont inerl Preservative Analyses Requested W o vi W u! U U - SAMPLE ID a m a L z } _FD CD N m o m CD a W �' a co v x = N p v N a LAB USE ONLY Q.1 a) N a_U5 o w m O cn m o m C G N �, ' N [bp H O o LAB SAMPLE ID -p7 -O 'a U aJ 61 j O 0 �, U] OJ f= CN N �!] N N O V 0 V V K] O O N < Uj O u'] C) O O 07 � ' [o G O C+C M Q Cl CD r Y'i tv O Cn m W W N F CL 2 H .� 0 N co 0 Cn u7 in N (n N N V1 }— Cn f6 "c y _ O .(n O N LGJ (n C7 N ~ y7 `r, to Q7 Q) d E (u E E co (n m C o N C U U) as tf] O Cn Cn cn = =c ,� S Z _C ° m O o z T: cn ` Qj o a EE (O (O M M M M L IC7 O O d 0 z N O M U N (U CO o 0 fl 0 co �i U) J 2 rc ` Y C J N @ 4i 4'S Q aJ m ��(/ /% 2`_ I Z 7 cn co Cn (n co 0 I-- C� M = S S Z m a O � 5 J S t 2 T. o r l U Cam- d N T P 1 0 o X X X UC12.5_6 AER 816/2024 C 817/2024 8/712024 & bj N T P 1 N X X bZ UC12-5_6AER 817I2024 C) N G P 1 r X X UZS UC12.5_6AER 81612024 U�iQs 81712024 0Lf0(4 8/7/2024 (7y U1 N. T P i N X X 2 Comments: SHIPPED ON WET ICE Custody Seal Present: Custody Seal Number: Sample Temp at Collection: INF °C EFF: °C 200.8 = Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,TI,Zn,Mo YES 1 NO Sample Temp at Receiving in Lab: INF: °C EFF: °C Sample Type Codes: Relinquished by (Signature): UCW Rec ived qy (Si nature,)': �� Date: Time: � Q (Flow) = Automatic Flow Proportioned Sample T (Time) = Automatic Time Proportioned Sample _ Sample Temp of EFF Fecal Sample at Receiving in Lab (record oC 0 el' uishrred by (Signat f e� / Recei ed by (Signature): /7 7 L! Date: Time: only if collected): H (Hand) = Nand Composite Sample G (Grab) =Grab Sample t, �� 1_� w�u Ei.T, k 1 Zero Headspace & Teflon septa for YES NO N/A Relinquf hed by (Signature): Received by (Signature): Date: Time: VOAs: < m Container Type Codes: A = Amber Glass P = Plastic Samples in Proper Containers: YES NO NIA Relinquished by (Signature): Received by (Signature): Date: Time: z GL = Clear Glass B = Bag TL = Teflon Lined Cap Chlorinated Samples De- YES NO< :E/A��] Relinquished by (Signature): Received by (Signature): Date: Time: Chlorinated: VOA = 40 ml Glass vial I Parle 113 of 133 11" O_ N @ m LA O O v rzv El o.. z a n ^7prD m r- � o- 1 3. a rti x VI n w z tn Ln n m a, mfD; 1 3 Qtc W o a - o .a = D4: 3 3 L N m m 'Cl c M <:3 rD n O D ❑T1[—f9D am a rbo - Z)w 0 � p ix "cr _ o y o a na c 'a Sr J .--.� ` El rD rrDD Z - In a +.l ro ti D cr �� rD !rt n 0❑ d U' -_- �D 1D $ rn 0 3 rn �+ s _� 3 .ar rD m GL .. q ro 4 2 u�l m v 3 a .� x rb _— n a " 41 0 3 a o v ❑ , a C m Z C 77, '34qro O O A s °- N -n ❑ ❑ r S ~ r�Y W \ W N� � C rn V o H C CT Z 0. v d 'wn' ❑❑ C. rt CD n N co CD rn v C W ❑ 1]❑ ❑ ❑ ❑ El El ❑ ❑ El ❑ P z❑ ❑ ta7t z z,z z a z o z o z z o 0 z 0 o z o z ❑ o z o -< I j a rD ❑� (n ❑ ❑ El ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ LA VI; d '7 rrD Z z n a z n a z� a z a z z n> z a z n z 'n z n z a El zEl� T. �y 3 r 1lj m o Q z (7 c rD M ❑ V W lf1 A W N F+ 0 i� Q (rryD. rn ❑ D 7t Q �- 0. o n ❑ v �' Da v d m v ari 3 c rt ,3.' 3 0 On cu G' '0 C m Q rD i0 y m � Z iA 7 1 3 Cr n ai 7 a 0 Elyam— • • CD 0 c m< j 1 �i/ J iv ro 3 m 0 3 D N o o C v a 3 a o a OV m r. ` O vi fl 7D D. N x p 01 7 0V C 4 n a ro .-r fn Eln�i O an 0--- - - --- n 5 ❑� C p m a ro n Z a u 7c rb !s n m' 3 ❑ _ N % ❑m n w 3 D I n ) O O r . .�j 5 � ❑ a � o O! a � N C A ID R Page 114 of 133 -n co { C7 iJ vs cn v (n p 0 w 0 !u m :-- n_ Q - m n CD 3 CD 3 m �^ �' J O l 3 1n 0 -., (n n -M cn cn cn n @ _ m _@ _ cn cn m 0 cn O a) m y cn ar Cn 3 m 5' 0 0 C) CD 0 k 3 3 3 m 3 3 3 n O C) M O a a 3 CD a -0 -0 cD _ 5 za M C7 pat O C7 s r 0- ujch rtln O (fi n Q- O N m ro W@ _ O _ � LL} (D mn 0 m 0 7 R O w y. a. 1D tp O .•' n p 3 O� a ,• N [SCD m. rN•+ — _ n a ro �' �=� y Omn �� cn CL rV) N tl v C 0 fU N [1 3 r+ < C 0 m CL co07 tn. n tnn 0 rt "* (D f C~ O J 3 @ N tl = O Q 0 CD N _ m (n s O n Vi pt zto oN 41 E3 o nn Q o m 0 teo al Q. m m at m y' a — N' m p7. m w n CL (D a O Q m a a m a as m o -0 0 fD �( cr (D tS �l CD (� C N - CD 5 0 ED 0 to m it a i m@ Vl ro ro m w — m — — N r^j �� (o in in n SD Cr �• m 0 y N 0. n z 3 4 J v_ v n Go 0 cn 0 Ld n. N• N p Z, m m 0 c ro n O (D C N N _ — O x m C a N tn N (c a N N C1 n ro CZ CD On C] EnfD n (0 j @ fD 3 3' m p O a O 3 Ca N O @ N (n 0] j r. G. 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Plastic Unptescrvcd{N/A) �' �. O a o e 'O -Cr, D w Si 3 m Cr n m o �p X a 4 a BPZU-500 rnL Plastic Unpreserved (N/A) m -i m k Cif `- 1 P1 •1 liter Plastic npreser" N p p x K — BP45-125 mL Plastrc H2SO4 (pH < 2) (0-) a CL ip CL i 4 I BP3N-2S0 mL plastic HNO3 (pH < 21 ', v N ID❑ M m IC BP4Z-125 mL Plasuc ZN acetate & NaOH 01 0 w n ❑ \ m p N N BP4& 125 ml Nam NaOH (PH a 12) (CI-J _ in A WGf U•Wlde•mouthed Glass jar Unpreserved r o E rd AG1U-1 liter Amber Unpreserved (N/A) (Cl.) U Y CL a O d LJ n a 7ZEZZ AG1H-1 liter Amber HCJ (pir< 21 s s c w rD � AG}U-250MLAmber VnprewvedJNJAJ'ILI] o c ro AG15.1 liter Amber H25O4 (pH < 2J H N ° ff AG35-250 mL Amber H25O4 (PH < 2) m OG54-40 mL Amber N14ACI (NJA)(Ck-) R ° -zz- OG91-1-40 mL VOA HOI N/A) VG9T-4C mi. VOA Na2S203 (N/A) 117111 -0 - e VG9U-40 mL VOA Unpieserved(NIA) n N K z DG9V-40 ml VOA Ii3PO4 IN/A) Li KP7U-50 mL Plastic Unpreserved IN/A) > N /D V/GK(3vtalsper kit)-VPH/Gaskit (NJA) j N ❑ a y SPST-125 mL Sterile Nastrc (N/A- lay) 7 C3 n 0 — '� O C O SPZT-250 mL Sterne plastic (N/A - lab) / BP3111-250 mL Plastrs INH212SO4 [93-9.7) AGOU-100 mL Amber Unpreserved(NJA)[CI-) VSGU-20 mL Scmullauoa vlats (NJAJ OG91)-40 mL Arn ber Unpreserved vial$ (N/A) QjTV ro M z C C z i 6 C O cn I N SU a_ tD fi 0 M Q o' 3 C 13 0 f4 0 tD rY Page 116 of 133 W, '`w ( L%. O c+ 0 4A N Q tO m �1 m a w M1t tom\ Y ILemA r � x a _ rp Cr n fl n N 0 N or X OZZZZZZ/ 8P4U-L 25 ml Plastic Unpreserved IN/Al (Cl.] Q s 3 N 3 3 a rb CO Im_ RL m h a D t7 SP3U•2SO mi. Plastic Unpreserved{NIA[ a °;, 6 a x n s• 1 0 > Q3 ra a M s �_ a- OP2U-SOO mL PlasOc Unpreserved )NIA) (Y) .^ „{ M sOe �'�� p. MC -- _ W 1}taeAl.u�unpraseRvedf N s = 0 3 :' rt. 2 � n a n N a? ERS-125 ml Plastic H25O4 (ptt < 2) [a-) o z a CL 4 n a 3 Q N 9P3N-250 ml plastic HNO3 [ pH S 7 } n`J ro M � 3 0 ` N m ro fo S OP4Z-125 ml PlaSUc ZN Acetate & NaOH (>9) L z = N a S xx n ❑ e q 3 �* O ro : m -� BP41S-125 mL Plastk NaOH [pH > 12) (LI-) o p ^61 N _ c _.. — — 'n LA yr• T n p p D _ — __ WGFU•Wide-mouthed Glass jar Unpreserved A 4b C rya su v � - is A - AG1U-1 filer Amber Unpreserved(NIA)[C,) N3 O �• 0 O m C y r t 0, 7 n AGSH-1 liter Amber H[I [pH c 2) { { !c rtl a �' 2 S L C r - AG3U-250ml.Ani Ur'.arvservedlNIA)ii m- �C -m m O � Z vi a AG15.1 liter amber H25O4 [pH c 21 - 3 m ;° by 0 o CL p - A(35-250 mL Amber H25O4 [pH < Z) CL zzzzzDG94-4O mL Amber NH4C1 (N/AI10.) ci• �• v s O _ 4 Q- DG9H-40 mL VOA HCI {NIA] 0 4 CA C ;M C _ VG9T-40 mL VOA Na251Oa NJ/A) n g rC CL w w VG9U.40 n,L VOA Unpreserved [1v/Al °: i m T DGSV-40 mL VOA H3PO4 (N/A) N ❑ y z C C - KP7U-50 mL Plastic Unpreserved (N/A) 4] 0 — - ,. - v i ((DD p' WGK (3 vials per kit)-VPH/Gas hi tJ d - -- O e1 p a m fo SPST-125 mL Sterile Plastic [N/A- lab) x iV Z c 2O 2 SP2T-250 mL Sterile Plastic [N/A -lab) - n c c m zz ZZZZZ7"lz BP3R 250 mL PIasLK (NH2)25O4 [7.3.9.l1 j O �--C AGOU•10C mL Amber Unpreserved (NIA) I0-1 21: - I USGU•20 mL Sctntillatlon vrals (N/A) 0 DG9U.40 mL Amber Unpreserved vials (NIA) Page 117 of 133 0 aceAnalytical Report of Analysis Pace Analytical LLC 1377 South Park Drive Kernersville, NC 27284 Attention: Stephanie Knott Project Name: UC12-SEMI-AN & PPA-8/7-2024 Project Number: 92746299 Lot Number:ZH15017 Date Completed:08/19/2024 08/20/2024 12:47 PM Approved and released by: Project Coordinator 1: Brooke Speers PCCRFO 24r ANSI National Accreditation Board qe0 A C C R E D I T E D TESTING LABORATORY The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC. Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 Tel:803-791-9700 Fax:803-791-9111 www.pacelabs.com Page 118 of 133 Page 1 of 16 PACE ANALYTICAL SERVICES, LLC SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative Pace Analytical LLC Lot Number: ZH15017 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Where sampling is conducted by the client, results relate to the accuracy of the information provided, and as the samples are received. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace") Laboratory Quality Manual, standard operating procedures (SOPS), and Pace policies. Any exceptions to the TNI standards, the Laboratory Quality Manual, SOPS or policies are qualified on the results page or discussed below. Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI scope of accreditation: E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7, Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320 B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal Coliform Colilert-18. If you have any questions regarding this report, please contact the Pace Project Manager listed on the cover page. Manual integration summaries are provided at the end of this report when applicable. Low Level Mercury Analysis The following sample was diluted 10x due to the nature of the sample matrix: ZH15017-001. The LOQ has been elevated to reflect the dilution. The sample did not stay brominated. Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 119 of 133 Page 2 of 16 PACE ANALYTICAL SERVICES, LLC Sample Summary Pace Analytical LLC Lot Number: ZH15017 Project Name: UC12-SEMI-AN & PPA-8/7-2024 Project Number: 92746299 Sample Number Sample ID Matrix Date Sampled Date Received 001 UC12-INF Aqueous 08/07/2024 0819 08/14/2024 002 UC12-INF FIELD BLANK Aqueous 08/07/2024 0819 08/14/2024 003 UC12-EFF Aqueous 08/07/2024 0803 08/14/2024 004 UC12-EFF FIELD BLANK Aqueous 08/07/2024 0803 08/14/2024 (4 samples) Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 120 of 133 Page 3 of 16 PACE ANALYTICAL SERVICES, LLC Detection Summary Pace Analytical LLC Lot Number: ZH15017 Project Name: UC12-SEMI-AN & PPA-8/7-2024 Project Number: 92746299 Sample Sample ID Matrix Parameter Method Result Q Units Page 001 UC12-INF Aqueous Mercury (CVAFS) 1631E 9.29 ng/L 5 003 UC12-EFF Aqueous Mercury (CVAFS) 1631E 0.734 ng/L 7 (2 detections) Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 121 of 133 Page 4 of 16 Mercury (CVAFS) Client: Pace Analytical LLC Laboratory ID:ZH15017-001 Description: UC12-INF Matrix: Aqueous Date Sampled:08/07/2024 0819 Project Name: UC12-SEMI-AN & PPA-8/7-2024 Date Received:08/14/2024 Project Number: 92746299 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 1631 E 10 08/17/2024 0443 KAJ 08/16/2024 1423 16441 Parameter Mercury (CVAFS) CAS Analytical Number Method Result Q LOQ Units Run 7439-97-6 1631 E 9.29 5.00 ng/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 5 of 16 Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 122 of 133 Mercury (CVAFS) Client: Pace Analytical LLC Laboratory ID:ZH15017-002 Description: UC12-INF FIELD BLANK Matrix: Aqueous Date Sampled:08/07/2024 0819 Project Name: UC12-SEMI-AN & PPA-8/7-2024 Date Received:08/14/2024 Project Number: 92746299 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 1631 E 1 08/17/2024 0449 KAJ 08/16/2024 1423 16441 Parameter Mercury (CVAFS) CAS Analytical Number Method Result Q LOQ Units Run 7439-97-6 1631E ND 0.500 ng/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 6 of 16 Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 123 of 133 Mercury (CVAFS) Client: Pace Analytical LLC Laboratory ID:ZH15017-003 Description: UC12-EFF Matrix: Aqueous Date Sampled:08/07/2024 0803 Project Name: UC12-SEMI-AN & PPA-8/7-2024 Date Received:08/14/2024 Project Number: 92746299 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 1631 E 1 08/17/2024 0454 KAJ 08/16/2024 1423 16441 Parameter Mercury (CVAFS) CAS Analytical Number Method Result Q LOQ Units Run 7439-97-6 1631E 0.734 0.500 ng/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 7 of 16 Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 124 of 133 Mercury (CVAFS) Client: Pace Analytical LLC Laboratory ID:ZH15017-004 Description: UC12-EFF FIELD BLANK Matrix: Aqueous Date Sampled:08/07/2024 0803 Project Name: UC12-SEMI-AN & PPA-8/7-2024 Date Received:08/14/2024 Project Number: 92746299 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 1631 E 1 08/17/2024 0511 KAJ 08/16/2024 1423 16441 Parameter Mercury (CVAFS) CAS Analytical Number Method Result Q LOQ Units Run 7439-97-6 1631E ND 0.500 ng/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 8 of 16 Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 125 of 133 QC Summary Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: ZH15017 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 126 of 133 Page 9 of 16 Mercury (CVAFS) - MB Sample ID: ZQ16441-001 Matrix: Aqueous Batch: 16441 Prep Method: Analytical Method: 1631 E Prep Date: 08/16/2024 1423 Parameter Result Q Dil LOQ Units Analysis Date Mercury (CVAFS) ND 1 0.500 ng/L 08/17/2024 0405 LOQ = Limit of Quantitation ND = Not detected at or above the LOQ = RSD is out of criteria N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 10 of 16 QC Data for Lot Number: ZH15017 Page 127 of 133 Mercury (CVAFS) - LCS Sample ID: ZQ16441-002 Matrix: Aqueous Batch: 16441 Prep Method: Analytical Method: 1631 E Prep Date: 08/16/2024 1423 Spike Amount Result %Rec Parameter (ng/L) (ng/L) Q Dil % Rec Limit Analysis Date Mercury (CVAFS) 5.00 4.93 1 99 75-125 08/17/2024 0416 LOQ = Limit of Quantitation ND = Not detected at or above the LOQ = RSD is out of criteria N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 11 of 16 QC Data for Lot Number: ZH15017 Page 128 of 133 Mercury (CVAFS) - MS Sample ID: ZH15017-003MS Matrix: Aqueous Batch: 16441 Prep Method: Analytical Method: 1631 E Prep Date: 08/16/2024 1423 Sample Spike Amount Amount Result %Rec Parameter (ng/L) (ng/L) (ng/L) Q Dil % Rec Limit Analysis Date Mercury (CVAFS) 0.734 5.00 5.50 1 95 71-125 08/17/2024 0500 LOQ = Limit of Quantitation ND = Not detected at or above the LOQ = RSD is out of criteria N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 12 of 16 QC Data for Lot Number: ZH15017 Page 129 of 133 Mercury (CVAFS) - MSD Sample ID: ZH15017-003MD Matrix: Aqueous Batch: 16441 Prep Method: Analytical Method: 1631 E Prep Date: 08/16/2024 1423 Sample Spike Amount Amount Result %Rec % RPD Parameter (ng/L) (ng/L) (ng/L) Q Dil % Rec % RPD Limit Limit Analysis Date Mercury (CVAFS) 0.734 5.00 5.30 1 91 3.7 71-125 24 08/17/2024 0505 LOQ = Limit of Quantitation ND = Not detected at or above the LOQ = RSD is out of criteria N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 13 of 16 QC Data for Lot Number: ZH15017 Page 130 of 133 Chain of Custody and Miscellaneous Documents Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 131 of 133 Page 14 of 16 PACE ANALYTICAL SERVICES, LLC L N C. X o fa z 5 Ca f� V fl L r— csl Cr] Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 15 of 16 Page 132 of 133 PACE ANALYTICAL SERVICES, LLC CCa?_Tit'w ENV- FRM-VOCAL-0286'M,Sampldls R,20rsipf,' CheckIst (SRC) Ettective Date- 812IM22 Sample Receipt Checklist (SRQ OKilt• PACK C4Dh' 11L5;;OACC11.}Yhbllt: i R ; 081' 5.024 - --- J-ar# ZH15011 memsalrecel t; Apace L ichr-rit 'I Jups 1'C;II.X U[tlwl: Yes No 1, wme cli_sf{xly ieaiq aresent an rlic cooler' YeSI.J. lNolt% NA Z. IfCUNM {'eab were 1'e5eni. ',�EA'e they inner and iuiLaolmci'r H SMp ID' MA Cirlclda- Ship ll)= _ . ntr-1 by Y_ Olds] temperature upon! Lweipt J I]el'ived (Owected} Tempe mi-e ][Pon ieceipt %sc4td Sinp-ov 0: A .. 34 /3.4 ac MA it%A 0(' NA iNA aC NA INA oC Itthod' ❑TeMeramm Blame JA¢awi 13 ouks IR Gun ID; 1 Elul { �slicrliurt Fr1 �tur. aC l: thod -Df c-olaur: I wet lcc Ic t Pacu 0 TirvTf-P r7None Ply3, Wm all coalcrs screwed at or bduw 6.OQ _a Lf no, vws Prof ecF 1+�i2 naeer norifi d? c [I lvc� Ut�t PM wis Notified Im. p4mir-1 t_~ana f f iltce-rt ee (eil'cle one). Yes l�ls of A 4- h tlrc rcmmn�l cumin's packingslip at Ulwd lu Il is fcnilr v, �-es No 5- 1F�'�rc pro}r�x cusiodj' �caridm'es {r�li,uluislrr�'uccri�ed) foUowe4i? Yes No -6- werc s-implt ll)s Ewd im the COC and all sanaple contai=57 o 7. P#No S. LU aUc(Minlcr label irfarmquoa UD, d3bc, tme) arrce witls the COG? 9. Welt tests to be nMU-Bled h5tcd an the COC? ❑�f Yrb EJh'.j 10. Did all seinpies arrive in the proper containers for cad trot mWor in g❑od cm litiatt (unbroken, lids on, etc.)? R Y�cNo ll- Was adequ�e samplevolaim available?Yes No 1 - Werc all smwilrs rc{-civcil within ".2 tlae holdinl7 Itiue of 43 ilolu& whichever ux5 &$T? DYes L]No 13- Watt Ssu4lt5 Mt'3 l KS WOMIt€d Re [-14-0i1kjSSiOl VC M9) QY 14- WmrVO — 8015G MdRSK-175 samples ftft ofbubbkc >°pea -size" ('ra"o iu NO1+1A rfiatnmr.r) m ntnr rkfthr. +CIA vlal�^ Yes No MA 15-WcrcallDRQ,'lncialihmrricntCana 1rRrcr6vcdx1M Hof<2? l' NO R 16. Wereall cyanide simples received air a pH ? 12 mid sulfide sin 1es received .2 ai °? 17- Wrrc all appLtcablc 1�lfIxMQ fCyaamdeiph ll 5,116 18.3 (; Q..=WL) !awpl s Oc W ❑�F� �N° � residual c}lls�tine'' U yes QTYa A 18- WDS dle :11tot�e ntjDAKE listed on ttr- containert1c1 Ir j1 xa Sirtuple purer v i¢u {Must Lr� c Meted foa' r lgs$lnple{s) ii1Colr1 ctlppa eservrd ar kith Tl aclspar -} Sallapia (s) xA- %vca'c reccMd incorrectly preserved and were act tA d ac conhi tgly in saulple rer-CN4 vridi NA rtxL cifcirek onC HM4. FINDS, HCL NFLOE 114kR SRC ' T1ue fprn elva*iau ifl orz thafr one preservative is uoeclerb please now in the comments L•ci w. '4A welt received with NiLbics �-6 nun id dimneter, Smlmples(s) T0a - . - - ..- - -- -- -. _-.— wera received rili th TRC > 0-5 TutJL ijf#19 is lio ) Md were adjusted actordhii i' in sample receh* with sodiva: dliosulrate (N,riO3) u0b Wyk ID- "4A COBU rents - Services, LLC PapIofI Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 16 of 16 Page 133 of 133