NC0085359_Supplemental DMR Info Attachment_20241001

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
August 28, 2024
Keith Purgason
Union County Public Works
8299 Kensington Drive
Waxhaw, NC 28173
RE: Project: UC12-SEMI-AN &PPA-8/7-2024
Pace Project No.: 92746299
Dear Keith Purgason:
Enclosed are the analytical results for sample(s)received by the laboratory on August 07, 2024. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National-Mt.Juliet
• Pace Analytical Services-Asheville
• Pace Analytical Services-Charlotte
• Pace Analytical Services- Peachtree Corners, GA
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Stephanie Knott
[e-mail]
704-977-0981
Project Manager
Enclosures
cc: Wyatt Howell, Union County Public Works
Kevin Merrill
�e AC f0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
9 without the written consent of Pace Analytical Services,LLC. Page 1 of 133
e

Pace Analytical Services,LLC
ace"
/� 9800 KinceyAve. Suite 100
/// G Huntersville,NC 28078
�!V [phone]
CERTIFICATIONS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Pace Analytical Services National
12065 Lebanon Road,Mt.Juliet,TN 37122 Nevada Certification#:TN-03-2002-34
Alabama Certification#:40660 New Hampshire Certification#: 2975
Alaska Certification 17-026 New Jersey Certification#:TNO02
Arizona Certification#:AZ0612 New Mexico DW Certification
Arkansas Certification#:88-0469 New York Certification#: 11742
California Certification#:2932 North Carolina Aquatic Toxicity Certification#:41
Canada Certification#: 1461.01 North Carolina Drinking Water Certification#:21704
Colorado Certification#:TN00003 North Carolina Environmental Certificate#:375
Connecticut Certification#:PH-0197 North Dakota Certification#:R-140
DOD Certification:#1461.01 Ohio VAP Certification#:CL0069
EPA#TN00003 Oklahoma Certification#:9915
Florida Certification#: E87487 Oregon Certification#:TN200002
Georgia DW Certification#:923 Pennsylvania Certification#:68-02979
Georgia Certification:NELAP Rhode Island Certification#:LA000356
Idaho Certification#:TN00003 South Carolina Certification#:84004
Illinois Certification#:200008 South Dakota Certification
Indiana Certification#:C-TN-01 Tennessee DW/Chem/Micro Certification#: 2006
Iowa Certification#:364 Texas Certification#:T 104704245-17-14
Kansas Certification#:E-10277 Texas Mold Certification#:LAB0152
Kentucky UST Certification#: 16 USDA Soil Permit#: P330-15-00234
Kentucky Certification#:90010 Utah Certification#:TN00003
Louisiana Certification#:A130792 Virginia Certification#:VT2006
Louisiana DW Certification#:LA180010 Vermont Dept.of Health: ID#VT-2006
Maine Certification#:TN0002 Virginia Certification#:460132
Maryland Certification#:324 Washington Certification#:C847
Massachusetts Certification#:M-TNO03 West Virginia Certification#:233
Michigan Certification#:9958 Wisconsin Certification#:998093910
Minnesota Certification#:047-999-395 Wyoming UST Certification#:via A21-A 2926.01
Mississippi Certification#:TN00003 A21-A-ISO 17025 Certification#: 1461.01
Missouri Certification#:340 A21-A-ISO 17025 Certification#: 1461.02
Montana Certification#:CERT0086 AIHA-LAP/LLC EMLAP Certification#:100789
Nebraska Certification#:NE-OS-15-05
Pace Analytical Services Charlotte
South Carolina Laboratory ID:99006 South Carolina Certification#:99006001
9800 Kincey Ave.Ste 100,Huntersville,NC 28078 South Carolina Drinking Water Cert.#:99006003
North Carolina Drinking Water Certification#:37706 Florida/NELAP Certification#: E87627
North Carolina Field Services Certification#:5342 Kentucky UST Certification#:84
North Carolina Wastewater Certification#: 12 Louisiana DoH Drinking Water#:LA029
South Carolina Laboratory ID:99006 Virginia/VELAP Certification#:460221
Pace Analytical Services Asheville
2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030
Florida/NELAP Certification#: E87648 South Carolina Certification#:99030001
North Carolina Drinking Water Certification#:37712 Virginia/VELAP Certification#:460222
North Carolina Wastewater Certification#:40
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners,GA 30092 North Carolina Certification#:381
Florida DOH Certification#:E87315 South Carolina Certification#:98011001
Georgia DW Inorganics Certification#:812 Virginia Certification#:460204
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services,LLC. Page 2 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92746299003 UC12-INF EPA608.3 SEM 30 PASI-C
EPA 200.7 Rev 4.4 1994 DBB1 1 PASI-A
EPA 200.8 Rev 5.4 1994 CRW 13 PASI-A
SM 2320B-2011 SMS 1 PASI-A
SM 2540C-2015 AGM 1 PASI-A
SM 2540D-2015 CMW1 1 PASI-A
SM 521OB-2016 KPE 1 PASI-A
EPA 300.0 Rev 2.1 1993 CDC 4 PASI-A
EPA 350.1 Rev 2.0 1993 NCF 1 PASI-A
EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A
EPA 365.1 Rev 2.0 1993 Zip 1 PASI-A
EPA420.4 Rev 1.0 1993 ARJ 1 PASI-A
SM 5220D-2011 MDW 1 PASI-A
92746299004 UC12-INF EPA625.1 ICO 61 PASI-C
EPA 624.1 SAS 37 PASI-C
EPA 1664E MAB, MSJ 2 PAN
SM 4500-CN-E-2016 AMB1 1 PASI-A
92746299007 UC12-EFF EPA608.3 SEM 30 PASI-C
EPA 200.7 Rev 4.4 1994 DBB1 1 PASI-A
EPA 200.8 Rev 5.4 1994 KRL 13 PASI-A
EPA 625.1 ICO 61 PASI-C
SM 2320B-2011 SMS 1 PASI-A
SM 2540C-2015 AGM 1 PASI-A
SM 2540D-2015 CMW1 1 PASI-A
SM 521OB-2016 KPE 1 PASI-A
EPA 300.0 Rev 2.1 1993 CDC 4 PASI-A
EPA 350.1 Rev 2.0 1993 NCF 1 PASI-A
EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A
EPA 365.1 Rev 2.0 1993 Zip 1 PASI-A
EPA420.4 Rev 1.0 1993 ARJ 1 PASI-A
SM 5220D-2011 MDW 1 PASI-A
92746299008 UC12-EFF EPA624.1 SAS 37 PASI-C
EPA 1664E MAB, MSJ 2 PAN
SM 4500-CN-E-2016 AMB1 1 PASI-A
92746299009 UC12-FCE EPA 200.8 Rev 5.4 1994 CRW 13 PASI-A
EPA 245.1 Rev 3.0 1994 KML 1 PASI-A
SM 2540D-2015 CMW1 1 PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 3 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
SM 521OB-2016 KPE 1 PASI-A
EPA 350.1 Rev 2.0 1993 NCF 1 PASI-A
EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A
EPA 353.2 Rev 2.0 1993 CEM 1 PASI-A
EPA 365.1 Rev 2.0 1993 Zip 1 PASI-A
SM 5220D-2011 MDW 1 PASI-A
92746299010 UC12-FCE SM 4500-CN-E-2016 AMB1 1 PASI-A
92746299011 UC12-MLSS EPA608.3 SEM 30 PASI-C
EPA 200.8 Rev 5.4 1994 CRW, KRL 13 PASI-A
EPA 245.1 Rev 3.0 1994 KML 1 PASI-A
EPA 625.1 ICO 61 PASI-C
EPA 160.4/SM2540B-2015 CMW1 2 PASI-A
EPA 300.0 Rev 2.1 1993 CDC 4 PASI-A
EPA 350.1 Rev 2.0 1993 NCF 1 PASI-A
EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A
EPA 365.1 Rev 2.0 1993 Zip 1 PASI-A
92746299012 UC12-MLSS EPA624.1 SAS 37 PASI-C
SM 4500-CN-E-2016 AMB1 1 PASI-A
92746299013 UC12-RAS EPA 200.8 Rev 5.4 1994 CRW, KRL 13 PASI-A
EPA 245.1 Rev 3.0 1994 KML 1 PASI-A
EPA 160.4/SM2540B-2015 CMW1 2 PASI-A
EPA 350.1 Rev 2.0 1993 NCF 1 PASI-A
EPA 365.1 Rev 2.0 1993 Zip 1 PASI-A
SM 5220D-2011 MDW 1 PASI-A
92746299014 UC12-RAS SM 4500-CN-E-2016 AMB1 1 PASI-A
92746299015 UC12-WAS EPA 200.8 Rev 5.4 1994 CRW, KRL 13 PASI-A
EPA 245.1 Rev 3.0 1994 KML 1 PASI-A
EPA 160.4/SM2540B-2015 CMW1 2 PASI-A
EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A
EPA 353.2 Rev 2.0 1993 CEM 1 PASI-A
EPA 365.1 Rev 2.0 1993 Zip 1 PASI-A
92746299016 UC12-WAS SM 4500-CN-E-2016 AMB1 1 PASI-A
92746299017 UC12-INFDIST EPA 200.8 Rev 5.4 1994 CRW, KRL 12 PASI-A
EPA 245.1 Rev 3.0 1994 KML 1 PASI-A
EPA 160.4/SM2540B-2015 CMW1 2 PASI-A
SM 521OB-2016 KPE 1 PASI-A
EPA 300.0 Rev 2.1 1993 CDC 4 PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 4 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
EPA 350.1 Rev 2.0 1993 NCF 1 PASI-A
EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A
EPA 365.1 Rev 2.0 1993 Zip 1 PASI-A
SM 5220D-2011 MDW 1 PASI-A
92746299018 UC12-INFDIST EPA608.3 SEM 30 PASI-C
EPA 625.1 ICO 61 PASI-C
EPA 624.1 SAS 37 PASI-C
SM 4500-CN-E-2016 AMB1 1 PASI-A
92746299019 UC12-BFP-1-CAKE EPA 7471B VB 1 PASI-GA
EPA 601OD DBB1 13 PASI-A
SM 2540G-2011 CHC 1 PASI-C
SW-846 KDF 1 PASI-C
EPA 160.4/SM2540B-2011 CMW1 1 PASI-A
EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A
EPA 353.2 Rev 2.0 1993 MFO 3 PASI-A
EPA 365.1 Rev 2.0 1993 NCF 1 PASI-A
92746299020 UC12-BFP-1-CAKE SW-846 CHC 1 PASI-C
SM 4500-CN-E-2016 EGC 1 PASI-A
92746299021 UC12-BFP-1-FILT EPA 200.8 Rev 5.4 1994 CRW 13 PASI-A
EPA 245.1 Rev 3.0 1994 KML 1 PASI-A
SM 2540D-2015 AGM 1 PASI-A
SM 521OB-2016 KPE 1 PASI-A
EPA 350.1 Rev 2.0 1993 NCF 1 PASI-A
EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A
EPA 353.2 Rev 2.0 1993 CEM 1 PASI-A
EPA 365.1 Rev 2.0 1993 Zip 1 PASI-A
SM 4500-CN-E-2016 AMB1 1 PASI-A
SM 5220D-2011 MDW 1 PASI-A
92746299022 UC12-1_2 AER EPA 200.8 Rev 5.4 1994 CRW, KRL 13 PASI-A
EPA 245.1 Rev 3.0 1994 KML 1 PASI-A
EPA 160.4/SM2540B-2015 CMW1 2 PASI-A
92746299023 UC12-1 2 AER SM 4500-CN-E-2016 AMB1 1 PASI-A
92746299024 UC12-5_6 AER EPA 200.8 Rev 5.4 1994 CRW, KRL 13 PASI-A
EPA 245.1 Rev 3.0 1994 KML 1 PASI-A
EPA 160.4/SM2540B-2015 CMW1 2 PASI-A
92746299025 UC12-5 6AER SM4500-CN-E-2016 AMB1 1 PASI-A
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services,LLC. Page 5 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
PAN=Pace National-Mt.Juliet
PASI-A=Pace Analytical Services-Asheville
PASI-C=Pace Analytical Services-Charlotte
PASI-GA=Pace Analytical Services-Peachtree Corners,GA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 6 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-INF Lab ID: 92746299003 Collected: 08/07/24 06:11 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
608 PCB Pest RVE Analytical Method: EPA 608.3 Preparation Method: EPA 608.3
Pace Analytical Services-Charlotte
Aldrin ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 309-00-2
alpha-BHC ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 319-84-6
beta-BHC ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 319-85-7
delta-BHC ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 319-86-8
gamma-BHC(Lindane) ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 58-89-9
Chlordane(Technical) ND ug/L 0.83 10 08/08/24 00:59 08/08/24 13:37 57-74-9
alpha-Chlordane ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 5103-71-9
gamma-Chlordane ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 5103-74-2
4,4'-DDD ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 72-54-8
4,4'-DDE ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 72-55-9
4,4'-DDT ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 50-29-3
Dieldrin ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 60-57-1
Endosulfan I ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 959-98-8
Endosulfan II ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 33213-65-9
Endosulfan sulfate ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 1031-07-8
Endrin ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 72-20-8
Endrin aldehyde ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 7421-93-4
Heptachlor ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 76-44-8 L1
Heptachlor epoxide ND ug/L 0.083 10 08/08/24 00:59 08/08/24 13:37 1024-57-3
PCB-1016(Aroclor 1016) ND ug/L 0.83 10 08/08/24 00:59 08/08/24 13:37 12674-11-2
PCB-1221 (Aroclor 1221) ND ug/L 0.83 10 08/08/24 00:59 08/08/24 13:37 11104-28-2
PCB-1232(Aroclor 1232) ND ug/L 0.83 10 08/08/24 00:59 08/08/24 13:37 11141-16-5
PCB-1242(Aroclor 1242) ND ug/L 0.83 10 08/08/24 00:59 08/08/24 13:37 53469-21-9
PCB-1248(Aroclor 1248) ND ug/L 0.83 10 08/08/24 00:59 08/08/24 13:37 12672-29-6
PCB-1254(Aroclor 1254) ND ug/L 0.83 10 08/08/24 00:59 08/08/24 13:37 11097-69-1
PCB-1260(Aroclor 1260) ND ug/L 0.83 10 08/08/24 00:59 08/08/24 13:37 11096-82-5
PCB,Total ND ug/L 0.83 10 08/08/24 00:59 08/08/24 13:37 1336-36-3
Toxaphene ND ug/L 0.83 10 08/08/24 00:59 08/08/24 13:37 8001-35-2
Surrogates
Tetrachloro-m-xylene(S) 0 % 10-137 10 08/08/24 00:59 08/08/24 13:37 877-09-8 D3,S4
Decachlorobiphenyl(S) 0 % 19-200 10 08/08/24 00:59 08/08/24 13:37 2051-24-3 S4
200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services-Asheville
Hardness,Total(SM 2340B) 115000 ug/L 662 1 08/15/24 13:00 08/19/24 11:44
200.8 MET ICPMS Analytical Method: EPA 200.8 Rev 5.4 1994 Preparation Method: EPA 200.8 Rev 5.4 1994
Pace Analytical Services-Asheville
Antimony ND ug/L 1.0 1 08/08/2412:30 08/09/2416:43 7440-36-0
Arsenic ND ug/L 1.0 1 08/08/2412:30 08/09/2416:43 7440-38-2
Beryllium ND ug/L 0.10 1 08/08/2412:30 08/09/2416:43 7440-41-7
Cadmium ND ug/L 0.10 1 08/08/2412:30 08/09/2416:43 7440-43-9
Chromium 1.1 ug/L 1.0 1 08/08/2412:30 08/09/2416:43 7440-47-3
Copper 21.0 ug/L 2.0 1 08/08/2412:30 08/09/2416:43 7440-50-8
Lead ND ug/L 1.0 1 08/08/2412:30 08/09/2416:43 7439-92-1
Molybdenum 1.1 ug/L 1.0 1 08/08/2412:30 08/09/2416:43 7439-98-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 7 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-INF Lab ID: 92746299003 Collected: 08/07/24 06:11 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.8 MET ICPMS Analytical Method: EPA 200.8 Rev 5.4 1994 Preparation Method: EPA 200.8 Rev 5.4 1994
Pace Analytical Services-Asheville
Nickel 2.2 ug/L 1.0 1 08/08/2412:30 08/09/2416:43 7440-02-0
Selenium ND ug/L 2.0 1 08/08/2412:30 08/09/2416:43 7782-49-2
Silver ND ug/L 0.40 1 08/08/2412:30 08/09/2416:43 7440-22-4
Thallium ND ug/L 0.20 1 08/08/2412:30 08/09/2416:43 7440-28-0
Zinc 118 ug/L 10.0 1 08/08/2412:30 08/09/2416:43 7440-66-6
2320B Alkalinity Analytical Method:SM 2320B-2011
Pace Analytical Services-Asheville
Alkalinity,Total as CaCO3 253 mg/L 5.0 1 08/09/24 15:17
2540C Total Dissolved Solids Analytical Method:SM 2540C-2015
Pace Analytical Services-Asheville
Total Dissolved Solids 263 mg/L 25.0 1 08/13/24 11:52
2540D Total Suspended Solids Analytical Method:SM 2540D-2015
Pace Analytical Services-Asheville
Total Suspended Solids 210 mg/L 35.7 1 08/09/24 13:16
5210B cBOD,5 day Analytical Method:SM 521OB-2016
Pace Analytical Services-Asheville
Carbonaceous BOD,5 day 158 mg/L 2.0 1 08/08/24 14:06 08/13/24 16:17
300.0 IC anions 48hr Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services-Asheville
Chloride 45.3 mg/L 1.0 1 08/07/24 22:29 16887-00-6
Nitrate as N ND mg/L 0.10 1 08/07/24 22:29 14797-55-8
Nitrate-Nitrite(as N) ND mg/L 0.20 1 08/07/24 22:29 7727-37-9
Nitrite as N ND mg/L 0.10 1 08/07/24 22:29 14797-65-0
350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen,Ammonia 37.5 mg/L 0.60 6 08/21/24 16:09 7664-41-7
351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen, Kjeldahl,Total 49.5 mg/L 5.0 10 08/26/24 18:34 08/27/24 10:08 7727-37-9 M1,R1
365.1 Phosphorus,Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services-Asheville
Phosphorus 5.9 mg/L 0.10 2 08/22/2418:08 08/23/2410:47 7723-14-0
420.4 Phenolics,Total Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993
Pace Analytical Services-Asheville
Phenolics,Total Recoverable 0.038 mg/L 0.0050 1 08/24/24 12:30 08/24/24 15:16 64743-03-9 M1
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 8 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-INF Lab ID: 92746299003 Collected: 08/07/24 06:11 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5220D COD Analytical Method:SM 5220D-2011 Preparation Method:SM 5220D-2011
Pace Analytical Services-Asheville
Chemical Oxygen Demand 687 mg/L 25.0 1 08/27/24 04:22 08/27/24 15:28
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 9 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-INF Lab ID: 92746299004 Collected: 08/07/24 05:22 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 RVE Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services-Charlotte
Acenaphthene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 83-32-9
Acenaphthylene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 208-96-8
Anthracene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 120-12-7
Benzo(a)anthracene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 56-55-3
Benzo(a)pyrene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 50-32-8
Benzo(b)fluoranthene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 205-99-2
Benzo(g,h,i)perylene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 191-24-2
Benzo(k)fluoranthene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 207-08-9
4-Bromophenylphenyl ether ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 101-55-3
Butylbenzylphthalate ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 85-68-7
4-ChIoro-3-m ethyl phenol ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 59-50-7
bis(2-Chloroethoxy)methane ND ug/L 50.0 5 08/08/24 00:54 08/08/24 21:05 111-91-1
bis(2-Chloroethyl)ether ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 111-44-4
2-Chloronaphthalene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 91-58-7
2-Chlorophenol ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 95-57-8
4-Chlorophenylphenyl ether ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 7005-72-3
Chrysene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 218-01-9
Dibenz(a,h)anthracene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 53-70-3
1,2-Dichlorobenzene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 95-50-1
1,3-Dichlorobenzene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 541-73-1
1,4-Dichlorobenzene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 106-46-7
3,3'-Dichlorobenzidine ND ug/L 50.0 5 08/08/24 00:54 08/08/24 21:05 91-94-1
2,4-Dichlorophenol ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 120-83-2
Diethylphthalate ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 84-66-2
2,4-Dimethylphenol ND ug/L 50.0 5 08/08/24 00:54 08/08/24 21:05 105-67-9
Dimethylphthalate ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 131-11-3
Di-n-butylphthalate ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 84-74-2
4,6-Dinitro-2-m ethyl phenol ND ug/L 50.0 5 08/08/24 00:54 08/08/24 21:05 534-52-1
2,4-Dinitrophenol ND ug/L 250 5 08/08/24 00:54 08/08/24 21:05 51-28-5
2,4-Dinitrotoluene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 121-14-2
2,6-Dinitrotoluene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 606-20-2
Di-n-octylphthalate ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 117-84-0
bis(2-Ethyl hexyl)phthalate ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 117-81-7
Fluoranthene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 206-44-0
Fluorene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 86-73-7
Hexachloro-1,3-butadiene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 87-68-3
Hexachlorobenzene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 118-74-1
Hexachlorocyclopentadiene ND ug/L 50.0 5 08/08/24 00:54 08/08/24 21:05 77-47-4
Hexachloroethane ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 67-72-1
Indeno(1,2,3-cd)pyrene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 193-39-5
Isophorone ND ug/L 50.0 5 08/08/24 00:54 08/08/24 21:05 78-59-1
Naphthalene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 91-20-3
Nitrobenzene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 98-95-3
2-Nitrophenol ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 88-75-5
4-Nitrophenol ND ug/L 50.0 5 08/08/24 00:54 08/08/24 21:05 100-02-7
N-Nitrosodimethylamine ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 62-75-9
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
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[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-INF Lab ID: 92746299004 Collected: 08/07/24 05:22 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 RVE Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services-Charlotte
N-Nitroso-di-n-propylamine ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 621-64-7
N-Nitrosodiphenylamine ND ug/L 50.0 5 08/08/24 00:54 08/08/24 21:05 86-30-6
2,2'-Oxybis(1-chloropropane) ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 108-60-1
Pentachlorophenol ND ug/L 50.0 5 08/08/24 00:54 08/08/24 21:05 87-86-5
Phenanthrene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 85-01-8
Phenol ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 108-95-2
Pyrene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 129-00-0
1,2,4-Trichlorobenzene ND ug/L 25.0 5 08/08/24 00:54 08/08/24 21:05 120-82-1
2,4,6-TrichIorophenol ND ug/L 50.0 5 08/08/24 00:54 08/08/24 21:05 88-06-2
Surrogates
Nitrobenzene-d5(S) 18 % 10-120 5 08/08/24 00:54 08/08/24 21:05 4165-60-0 D3
2-Fluorobiphenyl(S) 22 % 15-120 5 08/08/24 00:54 08/08/24 21:05 321-60-8
Terphenyl-d14(S) 38 % 11-131 5 08/08/24 00:54 08/08/24 21:05 1718-51-0
Phenol-d6(S) 17 % 10-120 5 08/08/24 00:54 08/08/24 21:05 13127-88-3
2-Fluorophenol(S) 16 % 10-120 5 08/08/24 00:54 08/08/24 21:05 367-12-4
2,4,6-Tribromophenol(S) 43 % 10-137 5 08/08/24 00:54 08/08/24 21:05 118-79-6
624 Volatile Organics Acrolein Analytical Method: EPA 624.1
Pace Analytical Services-Charlotte
Acrolein ND ug/L 5.0 1 08/08/24 21:00 107-02-8
Acrylonitrile ND ug/L 5.0 1 08/08/24 21:00 107-13-1
Benzene ND ug/L 1.0 1 08/08/24 21:00 71-43-2
Bromodichloromethane ND ug/L 2.0 1 08/08/24 21:00 75-27-4
Bromoform ND ug/L 2.0 1 08/08/24 21:00 75-25-2
Bromomethane ND ug/L 2.0 1 08/08/24 21:00 74-83-9
Carbon tetrachloride ND ug/L 2.0 1 08/08/24 21:00 56-23-5
Chlorobenzene ND ug/L 2.0 1 08/08/24 21:00 108-90-7
Chloroethane ND ug/L 2.0 1 08/08/24 21:00 75-00-3
2-Chloroethylvinyl ether ND ug/L 5.0 1 08/08/24 21:00 110-75-8
Chloroform ND ug/L 2.0 1 08/08/24 21:00 67-66-3
Chloromethane ND ug/L 2.0 1 08/08/24 21:00 74-87-3
Dibromochloromethane ND ug/L 2.0 1 08/08/24 21:00 124-48-1
1,2-Dichlorobenzene ND ug/L 2.0 1 08/08/24 21:00 95-50-1
1,3-Dichlorobenzene ND ug/L 2.0 1 08/08/24 21:00 541-73-1
1,4-Dichlorobenzene ND ug/L 2.0 1 08/08/24 21:00 106-46-7
1,1-Dichloroethane ND ug/L 2.0 1 08/08/24 21:00 75-34-3
1,2-Dichloroethane ND ug/L 2.0 1 08/08/24 21:00 107-06-2
1,1-Dichloroethene ND ug/L 2.0 1 08/08/24 21:00 75-35-4
cis-1,2-Dichloroethene ND ug/L 2.0 1 08/08/24 21:00 156-59-2
trans-1,2-Dichloroethene ND ug/L 2.0 1 08/08/24 21:00 156-60-5
1,2-Dichloropropane ND ug/L 2.0 1 08/08/24 21:00 78-87-5
cis-1,3-Dichloropropene ND ug/L 2.0 1 08/08/24 21:00 10061-01-5
trans-1,3-Dichloropropene ND ug/L 2.0 1 08/08/24 21:00 10061-02-6
Ethylbenzene ND ug/L 1.0 1 08/08/24 21:00 100-41-4
Methylene Chloride ND ug/L 2.0 1 08/08/24 21:00 75-09-2
1,1,2,2-Tetrachloroethane ND ug/L 2.0 1 08/08/24 21:00 79-34-5
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 11 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-INF Lab ID: 92746299004 Collected: 08/07/24 05:22 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
624 Volatile Organics Acrolein Analytical Method: EPA 624.1
Pace Analytical Services-Charlotte
Tetrachloroethene ND ug/L 2.0 1 08/08/24 21:00 127-18-4
Toluene 2.8 ug/L 1.0 1 08/08/24 21:00 108-88-3
1,1,1-Trichloroethane ND ug/L 2.0 1 08/08/24 21:00 71-55-6
1,1,2-Trichloroethane ND ug/L 2.0 1 08/08/24 21:00 79-00-5
Trichloroethene ND ug/L 2.0 1 08/08/24 21:00 79-01-6
Trichlorofluoromethane ND ug/L 2.0 1 08/08/24 21:00 75-69-4
Vinyl chloride ND ug/L 2.0 1 08/08/24 21:00 75-01-4
Surrogates
4-Bromofluorobenzene(S) 97 % 70-130 1 08/08/24 21:00 460-00-4
Toluene-d8(S) 100 % 70-130 1 08/08/24 21:00 2037-26-5
1,2-Dichloroethane-d4(S) 102 % 70-130 1 08/08/24 21:00 17060-07-0
Wet Chemistry 1664B Analytical Method: EPA 1664E Preparation Method: 1664B
Pace National-Mt.Juliet
Oil and Grease 17.5 mg/L 5.00 1 08/19/24 01:59 08/19/24 06:43
Total Petroleum Hydrocarbons ND mg/L 5.00 1 08/19/24 01:59 08/19/24 10:37
450OCNE Cyanide,Total Analytical Method:SM 4500-CN-E-2016 Preparation Method:SM 4500-CN-E-2016
Pace Analytical Services-Asheville
Cyanide ND mg/L 0.0080 1 08/19/2417:07 08/20/2411:26 57-12-5
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-EFF Lab ID: 92746299007 Collected: 08/07/24 06:06 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
608 PCB Pest RVE Analytical Method: EPA 608.3 Preparation Method: EPA 608.3
Pace Analytical Services-Charlotte
Aldrin ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 309-00-2
alpha-BHC ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 319-84-6
beta-BHC ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 319-85-7
delta-BHC ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 319-86-8
gamma-BHC(Lindane) ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 58-89-9
Chlordane(Technical) ND ug/L 0.42 1 08/09/24 16:51 08/13/24 20:56 57-74-9
alpha-Chlordane ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 5103-71-9
gamma-Chlordane ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 5103-74-2
4,4'-DDD ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 72-54-8
4,4'-DDE ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 72-55-9
4,4'-DDT ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 50-29-3
Dieldrin ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 60-57-1
Endosulfan I ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 959-98-8
Endosulfan II ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 33213-65-9
Endosulfan sulfate ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 1031-07-8
Endrin ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 72-20-8
Endrin aldehyde ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 7421-93-4
Heptachlor ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 76-44-8
Heptachlor epoxide ND ug/L 0.042 1 08/09/24 16:51 08/13/24 20:56 1024-57-3
PCB-1016(Aroclor 1016) ND ug/L 0.42 1 08/09/24 16:51 08/13/24 20:56 12674-11-2
PCB-1221 (Aroclor 1221) ND ug/L 0.42 1 08/09/24 16:51 08/13/24 20:56 11104-28-2
PCB-1232(Aroclor 1232) ND ug/L 0.42 1 08/09/24 16:51 08/13/24 20:56 11141-16-5
PCB-1242(Aroclor 1242) ND ug/L 0.42 1 08/09/24 16:51 08/13/24 20:56 53469-21-9
PCB-1248(Aroclor 1248) ND ug/L 0.42 1 08/09/24 16:51 08/13/24 20:56 12672-29-6
PCB-1254(Aroclor 1254) ND ug/L 0.42 1 08/09/24 16:51 08/13/24 20:56 11097-69-1
PCB-1260(Aroclor 1260) ND ug/L 0.42 1 08/09/24 16:51 08/13/24 20:56 11096-82-5
PCB,Total ND ug/L 0.42 1 08/09/24 16:51 08/13/24 20:56 1336-36-3
Toxaphene ND ug/L 0.42 1 08/09/24 16:51 08/13/24 20:56 8001-35-2
Surrogates
Tetrachloro-m-xylene(S) 98 % 10-137 1 08/09/24 16:51 08/13/24 20:56 877-09-8
Decachlorobiphenyl(S) 150 % 19-200 1 08/09/24 16:51 08/13/24 20:56 2051-24-3
200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services-Asheville
Hardness,Total(SM 2340B) 109000 ug/L 662 1 08/15/24 13:00 08/19/24 11:47
200.8 MET ICPMS Analytical Method: EPA 200.8 Rev 5.4 1994 Preparation Method: EPA 200.8 Rev 5.4 1994
Pace Analytical Services-Asheville
Antimony ND ug/L 1.0 1 08/10/24 13:45 08/12/24 00:15 7440-36-0
Arsenic ND ug/L 1.0 1 08/10/24 13:45 08/12/24 00:15 7440-38-2
Beryllium ND ug/L 0.10 1 08/10/24 13:45 08/12/24 00:15 7440-41-7
Cadmium ND ug/L 0.10 1 08/10/24 13:45 08/12/24 00:15 7440-43-9
Chromium ND ug/L 1.0 1 08/10/24 13:45 08/12/24 00:15 7440-47-3
Copper ND ug/L 2.0 1 08/10/24 13:45 08/12/24 00:15 7440-50-8
Lead ND ug/L 1.0 1 08/10/24 13:45 08/12/24 00:15 7439-92-1
Molybdenum ND ug/L 1.0 1 08/10/24 13:45 08/12/24 00:15 7439-98-7
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-EFF Lab ID: 92746299007 Collected: 08/07/24 06:06 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.8 MET ICPMS Analytical Method: EPA 200.8 Rev 5.4 1994 Preparation Method: EPA 200.8 Rev 5.4 1994
Pace Analytical Services-Asheville
Nickel 1.0 ug/L 1.0 1 08/10/24 13:45 08/12/24 00:15 7440-02-0
Selenium ND ug/L 2.0 1 08/10/24 13:45 08/12/24 00:15 7782-49-2
Silver ND ug/L 0.40 1 08/10/24 13:45 08/12/24 00:15 7440-22-4
Thallium ND ug/L 0.20 1 08/10/24 13:45 08/12/24 00:15 7440-28-0
Zinc 25.0 ug/L 10.0 1 08/10/24 13:45 08/12/24 00:15 7440-66-6
625 RVE Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services-Charlotte
Acenaphthene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 83-32-9
Acenaphthylene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 208-96-8
Anthracene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 120-12-7
Benzo(a)anthracene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 56-55-3
Benzo(a)pyrene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 50-32-8
Benzo(b)fluoranthene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 205-99-2
Benzo(g,h,i)perylene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 191-24-2
Benzo(k)fluoranthene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 207-08-9
4-Bromophenylphenyl ether ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 101-55-3
Butylbenzylphthalate ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 85-68-7
4-ChIoro-3-m ethyl phenol ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 59-50-7
bis(2-Chloroethoxy)methane ND ug/L 8.3 1 08/08/24 00:54 08/08/24 21:30 111-91-1
bis(2-Chloroethyl)ether ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 111-44-4
2-Chloronaphthalene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 91-58-7
2-Chlorophenol ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 95-57-8
4-Chlorophenylphenyl ether ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 7005-72-3
Chrysene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 218-01-9
Dibenz(a,h)anthracene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 53-70-3
1,2-Dichlorobenzene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 95-50-1
1,3-Dichlorobenzene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 541-73-1
1,4-Dichlorobenzene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 106-46-7
3,3'-Dichlorobenzidine ND ug/L 8.3 1 08/08/24 00:54 08/08/24 21:30 91-94-1
2,4-Dichlorophenol ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 120-83-2
Diethylphthalate ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 84-66-2
2,4-Dimethylphenol ND ug/L 8.3 1 08/08/24 00:54 08/08/24 21:30 105-67-9
Dimethylphthalate ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 131-11-3
Di-n-butylphthalate ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 84-74-2
4,6-Dinitro-2-m ethyl phenol ND ug/L 8.3 1 08/08/24 00:54 08/08/24 21:30 534-52-1
2,4-Dinitrophenol ND ug/L 41.7 1 08/08/24 00:54 08/08/24 21:30 51-28-5
2,4-Dinitrotoluene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 121-14-2
2,6-Dinitrotoluene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 606-20-2
Di-n-octylphthalate ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 117-84-0
bis(2-Ethyl hexyl)phthalate ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 117-81-7
Fluoranthene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 206-44-0
Fluorene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 86-73-7
Hexachloro-1,3-butadiene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 87-68-3
Hexachlorobenzene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 118-74-1
Hexachlorocyclopentadiene ND ug/L 8.3 1 08/08/24 00:54 08/08/24 21:30 77-47-4
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 14 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-EFF Lab ID: 92746299007 Collected: 08/07/24 06:06 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 RVE Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services-Charlotte
Hexachloroethane ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 67-72-1
Indeno(1,2,3-cd)pyrene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 193-39-5
Isophorone ND ug/L 8.3 1 08/08/24 00:54 08/08/24 21:30 78-59-1
Naphthalene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 91-20-3
Nitrobenzene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 98-95-3
2-Nitrophenol ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 88-75-5
4-Nitrophenol ND ug/L 8.3 1 08/08/24 00:54 08/08/24 21:30 100-02-7
N-Nitrosodimethylamine ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 62-75-9
N-Nitroso-di-n-propylamine ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 621-64-7
N-Nitrosodiphenylamine ND ug/L 8.3 1 08/08/24 00:54 08/08/24 21:30 86-30-6
2,2'-Oxybis(1-chloropropane) ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 108-60-1
Pentachlorophenol ND ug/L 8.3 1 08/08/24 00:54 08/08/24 21:30 87-86-5
Phenanthrene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 85-01-8
Phenol ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 108-95-2
Pyrene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 129-00-0
1,2,4-Trichlorobenzene ND ug/L 4.2 1 08/08/24 00:54 08/08/24 21:30 120-82-1
2,4,6-TrichIorophenol ND ug/L 8.3 1 08/08/24 00:54 08/08/24 21:30 88-06-2
Surrogates
Nitrobenzene-d5(S) 18 % 10-120 1 08/08/24 00:54 08/08/24 21:30 4165-60-0
2-Fluorobiphenyl(S) 18 % 15-120 1 08/08/24 00:54 08/08/24 21:30 321-60-8
Terphenyl-d14(S) 37 % 11-131 1 08/08/24 00:54 08/08/24 21:30 1718-51-0
Phenol-d6(S) 15 % 10-120 1 08/08/24 00:54 08/08/24 21:30 13127-88-3
2-Fluorophenol(S) 16 % 10-120 1 08/08/24 00:54 08/08/24 21:30 367-12-4
2,4,6-Tribromophenol(S) 40 % 10-137 1 08/08/24 00:54 08/08/24 21:30 118-79-6
2320B Alkalinity Analytical Method:SM 2320B-2011
Pace Analytical Services-Asheville
Alkalinity,Total as CaCO3 102 mg/L 5.0 1 08/09/24 15:26
2540C Total Dissolved Solids Analytical Method:SM 2540C-2015
Pace Analytical Services-Asheville
Total Dissolved Solids 296 mg/L 25.0 1 08/13/24 11:52
2540D Total Suspended Solids Analytical Method:SM 2540D-2015
Pace Analytical Services-Asheville
Total Suspended Solids ND mg/L 2.5 1 08/09/24 13:16
5210B cBOD,5 day Analytical Method:SM 521OB-2016
Pace Analytical Services-Asheville
Carbonaceous BOD,5 day ND mg/L 2.0 1 08/08/24 14:06 08/13/24 16:03
300.0 IC anions 48hr Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services-Asheville
Chloride 44.9 mg/L 1.0 1 08/07/24 22:14 16887-00-6
Nitrate as N 8.2 mg/L 0.40 4 08/08/24 01:31 14797-55-8
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 15 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-EFF Lab ID: 92746299007 Collected: 08/07/24 06:06 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
300.0 IC anions 48hr Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services-Asheville
Nitrate-Nitrite(as N) 8.2 mg/L 0.80 4 08/08/24 01:31 7727-37-9
Nitrite as N ND mg/L 0.10 1 08/07/24 22:14 14797-65-0
350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen,Ammonia ND mg/L 0.10 1 08/21/24 16:10 7664-41-7
351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen, Kjeldahl,Total 1.5 mg/L 0.50 1 08/26/24 18:34 08/27/24 09:07 7727-37-9 M1
365.1 Phosphorus,Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services-Asheville
Phosphorus 0.17 mg/L 0.050 1 08/22/2418:08 08/23/2410:52 7723-14-0
420.4 Phenolics,Total Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993
Pace Analytical Services-Asheville
Phenolics,Total Recoverable ND mg/L 0.0050 1 08/24/24 12:30 08/24/24 15:21 64743-03-9
5220D COD Analytical Method:SM 5220D-2011 Preparation Method:SM 5220D-2011
Pace Analytical Services-Asheville
Chemical Oxygen Demand ND mg/L 25.0 1 08/27/24 04:22 08/27/24 15:29 R1
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 16 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-EFF Lab ID: 92746299008 Collected: 08/07/24 06:15 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
624 Volatile Organics Acrolein Analytical Method: EPA 624.1
Pace Analytical Services-Charlotte
Acrolein ND ug/L 5.0 1 08/08/24 21:18 107-02-8
Acrylonitrile ND ug/L 5.0 1 08/08/24 21:18 107-13-1
Benzene ND ug/L 1.0 1 08/08/24 21:18 71-43-2
Bromodichloromethane ND ug/L 2.0 1 08/08/24 21:18 75-27-4
Bromoform ND ug/L 2.0 1 08/08/24 21:18 75-25-2
Bromomethane ND ug/L 2.0 1 08/08/24 21:18 74-83-9
Carbon tetrachloride ND ug/L 2.0 1 08/08/24 21:18 56-23-5
Chlorobenzene ND ug/L 2.0 1 08/08/24 21:18 108-90-7
Chloroethane ND ug/L 2.0 1 08/08/24 21:18 75-00-3
2-Chloroethylvinyl ether ND ug/L 5.0 1 08/08/24 21:18 110-75-8
Chloroform ND ug/L 2.0 1 08/08/24 21:18 67-66-3
Chloromethane ND ug/L 2.0 1 08/08/24 21:18 74-87-3
Dibromochloromethane ND ug/L 2.0 1 08/08/24 21:18 124-48-1
1,2-Dichlorobenzene ND ug/L 2.0 1 08/08/24 21:18 95-50-1
1,3-Dichlorobenzene ND ug/L 2.0 1 08/08/24 21:18 541-73-1
1,4-Dichlorobenzene ND ug/L 2.0 1 08/08/24 21:18 106-46-7
1,1-Dichloroethane ND ug/L 2.0 1 08/08/24 21:18 75-34-3
1,2-Dichloroethane ND ug/L 2.0 1 08/08/24 21:18 107-06-2
1,1-Dichloroethene ND ug/L 2.0 1 08/08/24 21:18 75-35-4
cis-1,2-Dichloroethene ND ug/L 2.0 1 08/08/24 21:18 156-59-2
trans-1,2-Dichloroethene ND ug/L 2.0 1 08/08/24 21:18 156-60-5
1,2-Dichloropropene ND ug/L 2.0 1 08/08/24 21:18 78-87-5
cis-1,3-Dichloropropene ND ug/L 2.0 1 08/08/24 21:18 10061-01-5
trans-1,3-Dichloropropene ND ug/L 2.0 1 08/08/24 21:18 10061-02-6
Ethylbenzene ND ug/L 1.0 1 08/08/24 21:18 100-41-4
Methylene Chloride ND ug/L 2.0 1 08/08/24 21:18 75-09-2
1,1,2,2-Tetrachloroethane ND ug/L 2.0 1 08/08/24 21:18 79-34-5
Tetrachloroethene ND ug/L 2.0 1 08/08/24 21:18 127-18-4
Toluene ND ug/L 1.0 1 08/08/24 21:18 108-88-3
1,1,1-Trichloroethane ND ug/L 2.0 1 08/08/24 21:18 71-55-6
1,1,2-Trichloroethane ND ug/L 2.0 1 08/08/24 21:18 79-00-5
Trichloroethene ND ug/L 2.0 1 08/08/24 21:18 79-01-6
Trichlorofluoromethane ND ug/L 2.0 1 08/08/24 21:18 75-69-4
Vinyl chloride ND ug/L 2.0 1 08/08/24 21:18 75-01-4
Surrogates
4-Bromofluorobenzene(S) 99 % 70-130 1 08/08/24 21:18 460-00-4
Toluene-d8(S) 100 % 70-130 1 08/08/24 21:18 2037-26-5
1,2-Dichloroethane-d4(S) 101 % 70-130 1 08/08/24 21:18 17060-07-0
Wet Chemistry 1664B Analytical Method: EPA 1664E Preparation Method: 1664B
Pace National-Mt.Juliet
Oil and Grease ND mg/L 5.00 1 08/19/24 01:59 08/19/24 06:43
Total Petroleum Hydrocarbons ND mg/L 5.00 1 08/19/24 01:59 08/19/24 10:37
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 17 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-EFF Lab ID: 92746299008 Collected: 08/07/24 06:15 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
450OCNE Cyanide,Total Analytical Method:SM 4500-CN-E-2016 Preparation Method:SM 4500-CN-E-2016
Pace Analytical Services-Asheville
Cyanide ND mg/L 0.0080 1 08/19/2417:07 08/20/2411:27 57-12-5
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 18 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-FCE Lab ID: 92746299009 Collected: 08/07/24 06:09 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.8 MET ICPMS Analytical Method: EPA 200.8 Rev 5.4 1994 Preparation Method: EPA 200.8 Rev 5.4 1994
Pace Analytical Services-Asheville
Antimony ND ug/L 1.0 1 08/08/2416:00 08/09/2413:54 7440-36-0
Arsenic ND ug/L 1.0 1 08/08/2416:00 08/09/2413:54 7440-38-2
Beryllium ND ug/L 0.10 1 08/08/2416:00 08/09/2413:54 7440-41-7
Cadmium ND ug/L 0.10 1 08/08/2416:00 08/09/2413:54 7440-43-9
Chromium ND ug/L 1.0 1 08/08/2416:00 08/09/2413:54 7440-47-3
Copper 2.1 ug/L 2.0 1 08/08/2416:00 08/09/2413:54 7440-50-8
Lead ND ug/L 1.0 1 08/08/2416:00 08/09/2413:54 7439-92-1
Molybdenum ND ug/L 1.0 1 08/08/2416:00 08/09/2413:54 7439-98-7
Nickel 1.1 ug/L 1.0 1 08/08/2416:00 08/09/2413:54 7440-02-0
Selenium ND ug/L 2.0 1 08/08/2416:00 08/09/2413:54 7782-49-2
Silver ND ug/L 0.40 1 08/08/2416:00 08/09/2413:54 7440-22-4
Thallium ND ug/L 0.20 1 08/08/2416:00 08/09/2413:54 7440-28-0
Zinc 28.2 ug/L 10.0 1 08/08/2416:00 08/09/2413:54 7440-66-6
245.1 Mercury Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994
Pace Analytical Services-Asheville
Mercury ND ug/L 0.20 1 08/09/2419:27 08/12/2416:14 7439-97-6
2540D Total Suspended Solids Analytical Method:SM 2540D-2015
Pace Analytical Services-Asheville
Total Suspended Solids 4.0 mg/L 2.5 1 08/09/24 13:17
5210B cBOD,5 day Analytical Method:SM 521OB-2016
Pace Analytical Services-Asheville
Carbonaceous BOD,5 day ND mg/L 2.0 1 08/08/24 14:06 08/13/24 16:08
350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen,Ammonia ND mg/L 0.10 1 08/21/24 16:11 7664-41-7
351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen, Kjeldahl,Total 2.0 mg/L 0.50 1 08/26/24 18:34 08/27/24 09:10 7727-37-9
353.2 Nitrogen,NO2/NO3 pres. Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen, NO2 plus NO3 10.8 mg/L 0.40 10 08/22/24 03:28
365.1 Phosphorus,Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services-Asheville
Phosphorus 0.32 mg/L 0.050 1 08/22/2418:08 08/23/2410:53 7723-14-0
5220D COD Analytical Method:SM 5220D-2011 Preparation Method:SM 5220D-2011
Pace Analytical Services-Asheville
Chemical Oxygen Demand ND mg/L 25.0 1 08/27/24 04:22 08/27/24 15:29
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 19 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-FCE Lab ID: 92746299010 Collected: 08/07/24 06:05 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
450OCNE Cyanide,Total Analytical Method:SM 4500-CN-E-2016 Preparation Method:SM 4500-CN-E-2016
Pace Analytical Services-Asheville
Cyanide ND mg/L 0.0080 1 08/19/2417:07 08/20/2411:28 57-12-5
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 20 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-MLSS Lab ID: 92746299011 Collected: 08/07/24 04:09 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
608 PCB Pest RVE Analytical Method: EPA 608.3 Preparation Method: EPA 608.3
Pace Analytical Services-Charlotte
Aldrin ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 309-00-2
alpha-BHC ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 319-84-6
beta-BHC ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 319-85-7
delta-BHC ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 319-86-8
gamma-BHC(Lindane) ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 58-89-9
Chlordane(Technical) ND ug/L 5.0 5 08/09/24 16:51 08/13/24 21:09 57-74-9
alpha-Chlordane ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 5103-71-9
gamma-Chlordane ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 5103-74-2
4,4'-DDD ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 72-54-8
4,4'-DDE ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 72-55-9
4,4'-DDT ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 50-29-3
Dieldrin ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 60-57-1
Endosulfan I ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 959-98-8
Endosulfan II ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 33213-65-9
Endosulfan sulfate ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 1031-07-8
Endrin ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 72-20-8
Endrin aldehyde ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 7421-93-4
Heptachlor ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 76-44-8
Heptachlor epoxide ND ug/L 0.50 5 08/09/24 16:51 08/13/24 21:09 1024-57-3
PCB-1016(Aroclor 1016) ND ug/L 5.0 5 08/09/24 16:51 08/13/24 21:09 12674-11-2
PCB-1221 (Aroclor 1221) ND ug/L 5.0 5 08/09/24 16:51 08/13/24 21:09 11104-28-2
PCB-1232(Aroclor 1232) ND ug/L 5.0 5 08/09/24 16:51 08/13/24 21:09 11141-16-5
PCB-1242(Aroclor 1242) ND ug/L 5.0 5 08/09/24 16:51 08/13/24 21:09 53469-21-9
PCB-1248(Aroclor 1248) ND ug/L 5.0 5 08/09/24 16:51 08/13/24 21:09 12672-29-6
PCB-1254(Aroclor 1254) ND ug/L 5.0 5 08/09/24 16:51 08/13/24 21:09 11097-69-1
PCB-1260(Aroclor 1260) ND ug/L 5.0 5 08/09/24 16:51 08/13/24 21:09 11096-82-5
PCB,Total ND ug/L 5.0 5 08/09/24 16:51 08/13/24 21:09 1336-36-3
Toxaphene ND ug/L 5.0 5 08/09/24 16:51 08/13/24 21:09 8001-35-2
Surrogates
Tetrachloro-m-xylene(S) 21 % 10-137 5 08/09/24 16:51 08/13/24 21:09 877-09-8 D3
Decachlorobiphenyl(S) 156 % 19-200 5 08/09/24 16:51 08/13/24 21:09 2051-24-3
200.8 MET ICPMS Analytical Method: EPA 200.8 Rev 5.4 1994 Preparation Method: EPA 200.8 Rev 5.4 1994
Pace Analytical Services-Asheville
Antimony 2.0 ug/L 1.0 1 08/08/24 16:00 08/11/24 21:33 7440-36-0
Arsenic 8.3 ug/L 1.0 1 08/08/24 16:00 08/11/24 21:33 7440-38-2
Beryllium 1.0 ug/L 0.10 1 08/08/24 16:00 08/11/24 21:33 7440-41-7
Cadmium 1.6 ug/L 0.10 1 08/08/24 16:00 08/11/24 21:33 7440-43-9
Chromium 19.1 ug/L 1.0 1 08/08/24 16:00 08/11/24 21:33 7440-47-3
Copper 443 ug/L 10.0 5 08/08/24 16:00 08/09/2414:16 7440-50-8 M1
Lead 9.1 ug/L 1.0 1 08/08/24 16:00 08/11/24 21:33 7439-92-1
Molybdenum 9.0 ug/L 1.0 1 08/08/24 16:00 08/11/24 21:33 7439-98-7
Nickel 27.9 ug/L 1.0 1 08/08/24 16:00 08/11/24 21:33 7440-02-0
Selenium 6.8 ug/L 2.0 1 08/08/24 16:00 08/11/24 21:33 7782-49-2
Silver 3.5 ug/L 0.40 1 08/08/24 16:00 08/11/24 21:33 7440-22-4
Thallium ND ug/L 0.20 1 08/08/24 16:00 08/11/24 21:33 7440-28-0
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 21 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-MLSS Lab ID: 92746299011 Collected: 08/07/24 04:09 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.8 MET ICPMS Analytical Method: EPA 200.8 Rev 5.4 1994 Preparation Method: EPA 200.8 Rev 5.4 1994
Pace Analytical Services-Asheville
Zinc 1720 ug/L 200 20 08/08/24 16:00 08/11/24 21:37 7440-66-6 M1
245.1 Mercury Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994
Pace Analytical Services-Asheville
Mercury ND ug/L 0.20 1 08/09/2419:27 08/12/2416:22 7439-97-6
625 RVE Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services-Charlotte
Acenaphthene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 83-32-9
Acenaphthylene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 208-96-8
Anthracene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 120-12-7
Benzo(a)anthracene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 56-55-3
Benzo(a)pyrene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 50-32-8
Benzo(b)fluoranthene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 205-99-2
Benzo(g,h,i)perylene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 191-24-2
Benzo(k)fluoranthene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 207-08-9
4-Bromophenylphenyl ether ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 101-55-3
Butylbenzylphthalate ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 85-68-7
4-Chloro-3-methyl phenol ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 59-50-7
bis(2-Chloroethoxy)methane ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:19 111-91-1
bis(2-Chloroethyl)ether ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 111-44-4
2-Chloronaphthalene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 91-58-7
2-Chlorophenol ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 95-57-8
4-Chlorophenylphenyl ether ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 7005-72-3
Chrysene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 218-01-9
Dibenz(a,h)anthracene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 53-70-3
1,2-Dichlorobenzene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 95-50-1
1,3-Dichlorobenzene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 541-73-1
1,4-Dichlorobenzene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 106-46-7
3,3'-Dichlorobenzidine ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:19 91-94-1
2,4-Dichlorophenol ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 120-83-2
Diethylphthalate ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 84-66-2
2,4-Dimethylphenol ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:19 105-67-9
Dimethylphthalate ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 131-11-3
Di-n-butylphthalate ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 84-74-2
4,6-Dinitro-2-methyl phenol ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:19 534-52-1
2,4-Dinitrophenol ND ug/L 167 4 08/08/24 00:54 08/09/24 16:19 51-28-5
2,4-Dinitrotoluene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 121-14-2
2,6-Dinitrotoluene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 606-20-2
Di-n-octylphthalate ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 117-84-0
bis(2-Ethyl hexyl)phthalate ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 117-81-7
Fluoranthene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 206-44-0
Fluorene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 86-73-7
Hexachloro-1,3-butadiene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 87-68-3
Hexachlorobenzene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 118-74-1
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 22 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-MLSS Lab ID: 92746299011 Collected: 08/07/24 04:09 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 RVE Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services-Charlotte
Hexachlorocyclopentadiene ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:19 77-47-4
Hexachloroethane ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 67-72-1
Indeno(1,2,3-cd)pyrene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 193-39-5
Isophorone ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:19 78-59-1
Naphthalene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 91-20-3
Nitrobenzene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 98-95-3
2-Nitrophenol ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 88-75-5
4-Nitrophenol ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:19 100-02-7
N-Nitrosodimethylamine ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 62-75-9
N-Nitroso-di-n-propylamine ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 621-64-7
N-Nitrosodiphenylamine ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:19 86-30-6
2,2'-Oxybis(1-chloropropane) ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 108-60-1
Pentachlorophenol ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:19 87-86-5
Phenanthrene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 85-01-8
Phenol ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 108-95-2
Pyrene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 129-00-0
1,2,4-Trichlorobenzene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:19 120-82-1
2,4,6-TrichIorophenol ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:19 88-06-2
Surrogates
Nitrobenzene-d5(S) 23 % 10-120 4 08/08/24 00:54 08/09/24 16:19 4165-60-0 D3
2-Fluorobiphenyl(S) 19 % 15-120 4 08/08/24 00:54 08/09/24 16:19 321-60-8
Terphenyl-d14(S) 40 % 11-131 4 08/08/24 00:54 08/09/24 16:19 1718-51-0
Phenol-d6(S) 17 % 10-120 4 08/08/24 00:54 08/09/24 16:19 13127-88-3
2-Fluorophenol(S) 16 % 10-120 4 08/08/24 00:54 08/09/24 16:19 367-12-4
2,4,6-Tribromophenol(S) 31 % 10-137 4 08/08/24 00:54 08/09/24 16:19 118-79-6
2540D TSS/TVSS Analytical Method: EPA 160.4/SM2540B-2015
Pace Analytical Services-Asheville
Total Suspended Solids 3340 mg/L 250 1 08/13/24 21:28
Volatile Suspended Solids 2760 mg/L 250 1 08/13/24 21:28
300.0 IC anions 48hr Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services-Asheville
Chloride 45.3 mg/L 1.0 1 08/07/24 22:00 16887-00-6
Nitrate as N 4.7 mg/L 0.20 2 08/08/24 01:03 14797-55-8
Nitrate-Nitrite(as N) 4.7 mg/L 0.40 2 08/08/24 01:03 7727-37-9
Nitrite as N ND mg/L 0.10 1 08/07/24 22:00 14797-65-0
350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen,Ammonia 0.85 mg/L 0.10 1 08/21/24 16:13 7664-41-7
351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen, Kjeldahl,Total 234 mg/L 25.0 5 08/26/24 18:34 08/27/24 10:12 7727-37-9
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 23 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-MLSS Lab ID: 92746299011 Collected: 08/07/24 04:09 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
365.1 Phosphorus,Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services-Asheville
Phosphorus 84.3 mg/L 1.0 20 08/22/2418:08 08/23/2410:55 7723-14-0
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 24 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-MLSS Lab ID: 92746299012 Collected: 08/07/24 04:19 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
624 Volatile Organics Acrolein Analytical Method: EPA 624.1
Pace Analytical Services-Charlotte
Acrolein ND ug/L 5.0 1 08/08/24 21:36 107-02-8
Acrylonitrile ND ug/L 5.0 1 08/08/24 21:36 107-13-1
Benzene ND ug/L 1.0 1 08/08/24 21:36 71-43-2
Bromodichloromethane ND ug/L 2.0 1 08/08/24 21:36 75-27-4
Bromoform ND ug/L 2.0 1 08/08/24 21:36 75-25-2
Bromomethane ND ug/L 2.0 1 08/08/24 21:36 74-83-9
Carbon tetrachloride ND ug/L 2.0 1 08/08/24 21:36 56-23-5
Chlorobenzene ND ug/L 2.0 1 08/08/24 21:36 108-90-7
Chloroethane ND ug/L 2.0 1 08/08/24 21:36 75-00-3
2-Chloroethylvinyl ether ND ug/L 5.0 1 08/08/24 21:36 110-75-8
Chloroform ND ug/L 2.0 1 08/08/24 21:36 67-66-3
Chloromethane ND ug/L 2.0 1 08/08/24 21:36 74-87-3
Dibromochloromethane ND ug/L 2.0 1 08/08/24 21:36 124-48-1
1,2-Dichlorobenzene ND ug/L 2.0 1 08/08/24 21:36 95-50-1
1,3-Dichlorobenzene ND ug/L 2.0 1 08/08/24 21:36 541-73-1
1,4-Dichlorobenzene ND ug/L 2.0 1 08/08/24 21:36 106-46-7
1,1-Dichloroethane ND ug/L 2.0 1 08/08/24 21:36 75-34-3
1,2-Dichloroethane ND ug/L 2.0 1 08/08/24 21:36 107-06-2
1,1-Dichloroethene ND ug/L 2.0 1 08/08/24 21:36 75-35-4
cis-1,2-Dichloroethene ND ug/L 2.0 1 08/08/24 21:36 156-59-2
trans-1,2-Dichloroethene ND ug/L 2.0 1 08/08/24 21:36 156-60-5
1,2-Dichloropropene ND ug/L 2.0 1 08/08/24 21:36 78-87-5
cis-1,3-Dichloropropene ND ug/L 2.0 1 08/08/24 21:36 10061-01-5
trans-1,3-Dichloropropene ND ug/L 2.0 1 08/08/24 21:36 10061-02-6
Ethylbenzene ND ug/L 1.0 1 08/08/24 21:36 100-41-4
Methylene Chloride ND ug/L 2.0 1 08/08/24 21:36 75-09-2
1,1,2,2-Tetrachloroethane ND ug/L 2.0 1 08/08/24 21:36 79-34-5
Tetrachloroethene ND ug/L 2.0 1 08/08/24 21:36 127-18-4
Toluene ND ug/L 1.0 1 08/08/24 21:36 108-88-3
1,1,1-Trichloroethane ND ug/L 2.0 1 08/08/24 21:36 71-55-6
1,1,2-Trichloroethane ND ug/L 2.0 1 08/08/24 21:36 79-00-5
Trichloroethene ND ug/L 2.0 1 08/08/24 21:36 79-01-6
Trichlorofluoromethane ND ug/L 2.0 1 08/08/24 21:36 75-69-4
Vinyl chloride ND ug/L 2.0 1 08/08/24 21:36 75-01-4
Surrogates
4-Bromofluorobenzene(S) 100 % 70-130 1 08/08/24 21:36 460-00-4
Toluene-d8(S) 98 % 70-130 1 08/08/24 21:36 2037-26-5
1,2-Dichloroethane-d4(S) 113 % 70-130 1 08/08/24 21:36 17060-07-0
450OCNE Cyanide,Total Analytical Method:SM 4500-CN-E-2016 Preparation Method:SM 4500-CN-E-2016
Pace Analytical Services-Asheville
Cyanide ND mg/L 0.0080 1 08/19/2417:07 08/20/2411:29 57-12-5
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 25 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-RAS Lab ID: 92746299013 Collected: 08/07/24 03:47 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.8 MET ICPMS Analytical Method: EPA 200.8 Rev 5.4 1994 Preparation Method: EPA 200.8 Rev 5.4 1994
Pace Analytical Services-Asheville
Antimony 2.7 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:04 7440-36-0
Arsenic 12.1 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:04 7440-38-2
Beryllium 1.5 ug/L 0.10 1 08/08/24 16:00 08/11/24 22:04 7440-41-7
Cadmium 2.3 ug/L 0.10 1 08/08/24 16:00 08/11/24 22:04 7440-43-9
Chromium 32.4 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:04 7440-47-3
Copper 623 ug/L 10.0 5 08/08/24 16:00 08/09/2414:32 7440-50-8
Lead 14.0 ug/L 5.0 5 08/08/24 16:00 08/09/2414:32 7439-92-1
Molybdenum 12.9 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:04 7439-98-7
Nickel 41.8 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:04 7440-02-0
Selenium 10.6 ug/L 2.0 1 08/08/24 16:00 08/11/24 22:04 7782-49-2
Silver 4.9 ug/L 0.40 1 08/08/24 16:00 08/11/24 22:04 7440-22-4
Thallium ND ug/L 1.0 5 08/08/24 16:00 08/09/2414:32 7440-28-0 D3
Zinc 2570 ug/L 200 20 08/08/24 16:00 08/11/24 22:07 7440-66-6
245.1 Mercury Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994
Pace Analytical Services-Asheville
Mercury ND ug/L 0.20 1 08/09/2419:27 08/12/2416:29 7439-97-6
2540D TSS/TVSS Analytical Method: EPA 160.4/SM2540B-2015
Pace Analytical Services-Asheville
Total Suspended Solids 5070 mg/L 250 1 08/13/24 21:28
Volatile Suspended Solids 4050 mg/L 250 1 08/13/24 21:28
350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen,Ammonia 1.6 mg/L 0.10 1 08/21/24 16:14 7664-41-7
365.1 Phosphorus,Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services-Asheville
Phosphorus 94.4 mg/L 2.0 40 08/22/2418:08 08/23/2410:56 7723-14-0
5220D COD Analytical Method:SM 5220D-2011 Preparation Method:SM 5220D-2011
Pace Analytical Services-Asheville
Chemical Oxygen Demand 6280 mg/L 250 1 08/27/24 04:22 08/27/24 15:29
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 26 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-RAS Lab ID: 92746299014 Collected: 08/07/24 03:44 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
450OCNE Cyanide,Total Analytical Method:SM 4500-CN-E-2016 Preparation Method:SM 4500-CN-E-2016
Pace Analytical Services-Asheville
Cyanide ND mg/L 0.0080 1 08/19/2417:07 08/20/2411:29 57-12-5
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 27 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-WAS Lab ID: 92746299015 Collected: 08/07/24 03:48 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.8 MET ICPMS Analytical Method: EPA 200.8 Rev 5.4 1994 Preparation Method: EPA 200.8 Rev 5.4 1994
Pace Analytical Services-Asheville
Antimony 2.9 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:11 7440-36-0
Arsenic 12.0 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:11 7440-38-2
Beryllium 1.4 ug/L 0.10 1 08/08/24 16:00 08/11/24 22:11 7440-41-7
Cadmium 2.3 ug/L 0.10 1 08/08/24 16:00 08/11/24 22:11 7440-43-9
Chromium 28.7 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:11 7440-47-3
Copper 627 ug/L 10.0 5 08/08/24 16:00 08/09/2414:44 7440-50-8
Lead 13.9 ug/L 5.0 5 08/08/24 16:00 08/09/2414:44 7439-92-1
Molybdenum 12.5 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:11 7439-98-7
Nickel 41.1 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:11 7440-02-0
Selenium 10.7 ug/L 2.0 1 08/08/24 16:00 08/11/24 22:11 7782-49-2
Silver 5.0 ug/L 0.40 1 08/08/24 16:00 08/11/24 22:11 7440-22-4
Thallium ND ug/L 1.0 5 08/08/24 16:00 08/09/2414:44 7440-28-0 D3
Zinc 2580 ug/L 200 20 08/08/24 16:00 08/11/24 22:15 7440-66-6
245.1 Mercury Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994
Pace Analytical Services-Asheville
Mercury ND ug/L 0.20 1 08/09/2419:27 08/12/2416:31 7439-97-6
160.4 TVS and 2540B TS Analytical Method: EPA 160.4/SM2540B-2015
Pace Analytical Services-Asheville
Total Solids 5570 mg/L 250 1 08/13/24 18:55
Total Volatile Solids 4220 mg/L 250 1 08/13/24 18:55
351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen, Kjeldahl,Total 375 mg/L 25.0 5 08/26/24 18:34 08/27/24 10:13 7727-37-9
353.2 Nitrogen,NO2/NO3 pres. Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen, NO2 plus NO3 2.3 mg/L 0.040 1 08/22/24 02:22
365.1 Phosphorus,Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services-Asheville
Phosphorus 128 mg/L 2.0 40 08/22/2418:08 08/23/2410:58 7723-14-0
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 28 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-WAS Lab ID: 92746299016 Collected: 08/07/24 03:44 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
450OCNE Cyanide,Total Analytical Method:SM 4500-CN-E-2016 Preparation Method:SM 4500-CN-E-2016
Pace Analytical Services-Asheville
Cyanide ND mg/L 0.0080 1 08/19/2417:07 08/20/2411:30 57-12-5
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 29 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-INFDIST Lab ID: 92746299017 Collected: 08/07/24 06:25 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.8 MET ICPMS Analytical Method: EPA 200.8 Rev 5.4 1994 Preparation Method: EPA 200.8 Rev 5.4 1994
Pace Analytical Services-Asheville
Antimony 1.9 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:19 7440-36-0
Arsenic 6.6 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:19 7440-38-2
Beryllium 0.78 ug/L 0.10 1 08/08/24 16:00 08/11/24 22:19 7440-41-7
Cadmium 1.3 ug/L 0.10 1 08/08/24 16:00 08/11/24 22:19 7440-43-9
Chromium 16.6 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:19 7440-47-3
Copper 359 ug/L 10.0 5 08/08/24 16:00 08/09/2414:48 7440-50-8
Lead 7.5 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:19 7439-92-1
Nickel 23.1 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:19 7440-02-0
Selenium 5.9 ug/L 2.0 1 08/08/24 16:00 08/11/24 22:19 7782-49-2
Silver 4.3 ug/L 0.40 1 08/08/24 16:00 08/11/24 22:19 7440-22-4
Thallium ND ug/L 0.20 1 08/08/24 16:00 08/11/24 22:19 7440-28-0
Zinc 1470 ug/L 200 20 08/08/24 16:00 08/11/24 22:23 7440-66-6
245.1 Mercury Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994
Pace Analytical Services-Asheville
Mercury ND ug/L 0.20 1 08/09/2419:27 08/12/2416:34 7439-97-6
2540D TSS/TVSS Analytical Method: EPA 160.4/SM2540B-2015
Pace Analytical Services-Asheville
Total Suspended Solids 2940 mg/L 357 1 08/09/24 13:38
Volatile Suspended Solids 2460 mg/L 357 1 08/09/24 13:38
5210B cBOD,5 day Analytical Method:SM 521OB-2016
Pace Analytical Services-Asheville
Carbonaceous BOD,5 day 258 mg/L 2.0 1 08/08/24 14:06 08/13/24 16:21
300.0 IC anions 48hr Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services-Asheville
Chloride 44.8 mg/L 1.0 1 08/08/24 08:58 16887-00-6
Nitrate as N 0.44 mg/L 0.10 1 08/08/24 08:58 14797-55-8
Nitrate-Nitrite(as N) 0.44 mg/L 0.20 1 08/08/24 08:58 7727-37-9
Nitrite as N ND mg/L 0.10 1 08/08/24 08:58 14797-65-0 M1
350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen,Ammonia 18.6 mg/L 0.50 5 08/21/24 16:16 7664-41-7
351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen, Kjeldahl,Total 251 mg/L 25.0 5 08/26/24 18:34 08/27/24 10:14 7727-37-9
365.1 Phosphorus,Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services-Asheville
Phosphorus 78.2 mg/L 1.0 20 08/22/2418:08 08/23/2410:59 7723-14-0
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 30 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-INFDIST Lab ID: 92746299017 Collected: 08/07/24 06:25 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5220D COD Analytical Method:SM 5220D-2011 Preparation Method:SM 5220D-2011
Pace Analytical Services-Asheville
Chemical Oxygen Demand 3490 mg/L 250 1 08/27/24 04:22 08/27/24 15:29
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 31 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-INFDIST Lab ID: 92746299018 Collected: 08/07/24 06:28 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
608 PCB Pest RVE Analytical Method: EPA 608.3 Preparation Method: EPA 608.3
Pace Analytical Services-Charlotte
Aldrin ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 309-00-2
alpha-BHC ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 319-84-6
beta-BHC ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 319-85-7
delta-BHC ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 319-86-8
gamma-BHC(Lindane) ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 58-89-9
Chlordane(Technical) ND ug/L 0.50 1 08/09/24 16:51 08/13/24 21:22 57-74-9
alpha-Chlordane ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 5103-71-9
gamma-Chlordane ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 5103-74-2
4,4'-DDD ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 72-54-8
4,4'-DDE ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 72-55-9
4,4'-DDT ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 50-29-3
Dieldrin ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 60-57-1
Endosulfan I ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 959-98-8
Endosulfan II ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 33213-65-9
Endosulfan sulfate ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 1031-07-8
Endrin ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 72-20-8
Endrin aldehyde ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 7421-93-4
Heptachlor ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 76-44-8
Heptachlor epoxide ND ug/L 0.050 1 08/09/24 16:51 08/13/24 21:22 1024-57-3
PCB-1016(Aroclor 1016) ND ug/L 0.50 1 08/09/24 16:51 08/13/24 21:22 12674-11-2
PCB-1221 (Aroclor 1221) ND ug/L 0.50 1 08/09/24 16:51 08/13/24 21:22 11104-28-2
PCB-1232(Aroclor 1232) ND ug/L 0.50 1 08/09/24 16:51 08/13/24 21:22 11141-16-5
PCB-1242(Aroclor 1242) ND ug/L 0.50 1 08/09/24 16:51 08/13/24 21:22 53469-21-9
PCB-1248(Aroclor 1248) ND ug/L 0.50 1 08/09/24 16:51 08/13/24 21:22 12672-29-6
PCB-1254(Aroclor 1254) ND ug/L 0.50 1 08/09/24 16:51 08/13/24 21:22 11097-69-1
PCB-1260(Aroclor 1260) ND ug/L 0.50 1 08/09/24 16:51 08/13/24 21:22 11096-82-5
PCB,Total ND ug/L 0.50 1 08/09/24 16:51 08/13/24 21:22 1336-36-3
Toxaphene ND ug/L 0.50 1 08/09/24 16:51 08/13/24 21:22 8001-35-2
Surrogates
Tetrachloro-m-xylene(S) 42 % 10-137 1 08/09/24 16:51 08/13/24 21:22 877-09-8
Decachlorobiphenyl(S) 55 % 19-200 1 08/09/24 16:51 08/13/24 21:22 2051-24-3
625 RVE Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services-Charlotte
Acenaphthene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 83-32-9
Acenaphthylene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 208-96-8
Anthracene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 120-12-7
Benzo(a)anthracene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 56-55-3
Benzo(a)pyrene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 50-32-8
Benzo(b)fluoranthene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 205-99-2
Benzo(g,h,i)perylene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 191-24-2
Benzo(k)fluoranthene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 207-08-9
4-Bromophenylphenyl ether ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 101-55-3
Butylbenzylphthalate ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 85-68-7
4-Chloro-3-methyl phenol ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 59-50-7
bis(2-Chloroethoxy)methane ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:45 111-91-1
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 32 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-INFDIST Lab ID: 92746299018 Collected: 08/07/24 06:28 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 RVE Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services-Charlotte
bis(2-Chloroethyl)ether ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 111-44-4
2-Chloronaphthalene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 91-58-7
2-Chlorophenol ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 95-57-8
4-Chlorophenylphenyl ether ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 7005-72-3
Chrysene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 218-01-9
Dibenz(a,h)anthracene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 53-70-3
1,2-Dichlorobenzene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 95-50-1
1,3-Dichlorobenzene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 541-73-1
1,4-Dichlorobenzene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 106-46-7
3,3'-Dichlorobenzidine ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:45 91-94-1
2,4-Dichlorophenol ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 120-83-2
Diethylphthalate ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 84-66-2
2,4-Dimethylphenol ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:45 105-67-9
Dimethylphthalate ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 131-11-3
Di-n-butylphthalate ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 84-74-2
4,6-Dinitro-2-m ethyl phenol ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:45 534-52-1
2,4-Dinitrophenol ND ug/L 167 4 08/08/24 00:54 08/09/24 16:45 51-28-5
2,4-Dinitrotoluene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 121-14-2
2,6-Dinitrotoluene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 606-20-2
Di-n-octylphthalate ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 117-84-0
bis(2-Ethyl hexyl)phthalate ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 117-81-7
Fluoranthene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 206-44-0
Fluorene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 86-73-7
Hexachloro-1,3-butadiene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 87-68-3
Hexachlorobenzene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 118-74-1
Hexachlorocyclopentadiene ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:45 77-47-4
Hexachloroethane ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 67-72-1
Indeno(1,2,3-cd)pyrene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 193-39-5
Isophorone ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:45 78-59-1
Naphthalene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 91-20-3
Nitrobenzene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 98-95-3
2-Nitrophenol ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 88-75-5
4-Nitrophenol ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:45 100-02-7
N-Nitrosodimethylamine ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 62-75-9
N-Nitroso-di-n-propylamine ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 621-64-7
N-Nitrosodiphenylamine ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:45 86-30-6
2,2'-Oxybis(1-chloropropane) ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 108-60-1
Pentachlorophenol ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:45 87-86-5
Phenanthrene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 85-01-8
Phenol ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 108-95-2
Pyrene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 129-00-0
1,2,4-Trichlorobenzene ND ug/L 16.7 4 08/08/24 00:54 08/09/24 16:45 120-82-1
2,4,6-TrichIorophenol ND ug/L 33.3 4 08/08/24 00:54 08/09/24 16:45 88-06-2
Surrogates
Nitrobenzene-d5(S) 20 % 10-120 4 08/08/24 00:54 08/09/24 16:45 4165-60-0 D3
2-Fluorobiphenyl(S) 18 % 15-120 4 08/08/24 00:54 08/09/24 16:45 321-60-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 33 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-INFDIST Lab ID: 92746299018 Collected: 08/07/24 06:28 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 RVE Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services-Charlotte
Surrogates
Terphenyl-d14(S) 37 % 11-131 4 08/08/24 00:54 08/09/24 16:45 1718-51-0
Phenol-d6(S) 15 % 10-120 4 08/08/24 00:54 08/09/24 16:45 13127-88-3
2-Fluorophenol(S) 14 % 10-120 4 08/08/24 00:54 08/09/24 16:45 367-12-4
2,4,6-Tribromophenol(S) 32 % 10-137 4 08/08/24 00:54 08/09/24 16:45 118-79-6
624 Volatile Organics Acrolein Analytical Method: EPA 624.1
Pace Analytical Services-Charlotte
Acrolein ND ug/L 5.0 1 08/08/24 21:54 107-02-8
Acrylonitrile ND ug/L 5.0 1 08/08/24 21:54 107-13-1
Benzene ND ug/L 1.0 1 08/08/24 21:54 71-43-2
Bromodichloromethane ND ug/L 2.0 1 08/08/24 21:54 75-27-4
Bromoform ND ug/L 2.0 1 08/08/24 21:54 75-25-2
Bromomethane ND ug/L 2.0 1 08/08/24 21:54 74-83-9
Carbon tetrachloride ND ug/L 2.0 1 08/08/24 21:54 56-23-5
Chlorobenzene ND ug/L 2.0 1 08/08/24 21:54 108-90-7
Chloroethane ND ug/L 2.0 1 08/08/24 21:54 75-00-3
2-Chloroethylvinyl ether ND ug/L 5.0 1 08/08/24 21:54 110-75-8
Chloroform ND ug/L 2.0 1 08/08/24 21:54 67-66-3
Chloromethane ND ug/L 2.0 1 08/08/24 21:54 74-87-3
Dibromochloromethane ND ug/L 2.0 1 08/08/24 21:54 124-48-1
1,2-Dichlorobenzene ND ug/L 2.0 1 08/08/24 21:54 95-50-1
1,3-Dichlorobenzene ND ug/L 2.0 1 08/08/24 21:54 541-73-1
1,4-Dichlorobenzene ND ug/L 2.0 1 08/08/24 21:54 106-46-7
1,1-Dichloroethane ND ug/L 2.0 1 08/08/24 21:54 75-34-3
1,2-Dichloroethane ND ug/L 2.0 1 08/08/24 21:54 107-06-2
1,1-Dichloroethene ND ug/L 2.0 1 08/08/24 21:54 75-35-4
cis-1,2-Dichloroethene ND ug/L 2.0 1 08/08/24 21:54 156-59-2
trans-1,2-Dichloroethene ND ug/L 2.0 1 08/08/24 21:54 156-60-5
1,2-Dichloropropane ND ug/L 2.0 1 08/08/24 21:54 78-87-5
cis-1,3-Dichloropropene ND ug/L 2.0 1 08/08/24 21:54 10061-01-5
trans-1,3-Dichloropropene ND ug/L 2.0 1 08/08/24 21:54 10061-02-6
Ethylbenzene ND ug/L 1.0 1 08/08/24 21:54 100-41-4
Methylene Chloride ND ug/L 2.0 1 08/08/24 21:54 75-09-2
1,1,2,2-Tetrachloroethane ND ug/L 2.0 1 08/08/24 21:54 79-34-5
Tetrachloroethene ND ug/L 2.0 1 08/08/24 21:54 127-18-4
Toluene 1.5 ug/L 1.0 1 08/08/24 21:54 108-88-3
1,1,1-Trichloroethane ND ug/L 2.0 1 08/08/24 21:54 71-55-6
1,1,2-Trichloroethane ND ug/L 2.0 1 08/08/24 21:54 79-00-5
Trichloroethene ND ug/L 2.0 1 08/08/24 21:54 79-01-6
Trichlorofluoromethane ND ug/L 2.0 1 08/08/24 21:54 75-69-4
Vinyl chloride ND ug/L 2.0 1 08/08/24 21:54 75-01-4
Surrogates
4-Bromofluorobenzene(S) 99 % 70-130 1 08/08/24 21:54 460-00-4
Toluene-d8(S) 98 % 70-130 1 08/08/24 21:54 2037-26-5
1,2-Dichloroethane-d4(S) 107 % 70-130 1 08/08/24 21:54 17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 34 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-INFDIST Lab ID: 92746299018 Collected: 08/07/24 06:28 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
450OCNE Cyanide,Total Analytical Method:SM 4500-CN-E-2016 Preparation Method:SM 4500-CN-E-2016
Pace Analytical Services-Asheville
Cyanide ND mg/L 0.0080 1 08/19/2417:07 08/20/2411:34 57-12-5
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 35 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-BFP-1-CAKE Lab ID: 92746299019 Collected: 08/07/24 03:50 Received: 08/07/24 11:41 Matrix: Solid
Results reported on a "dry weight"basis and are adjusted for percent moisture,sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
7471 Mercury Analytical Method: EPA 7471 B Preparation Method: EPA 7471 B
Pace Analytical Services-Peachtree Corners,GA
Mercury ND mg/kg 0.047 1 08/13/24 08:30 08/13/24 12:41 7439-97-6
6010 MET ICP Analytical Method: EPA 6010D Preparation Method:EPA 3050E
Pace Analytical Services-Asheville
Antimony ND mg/kg 11.7 1 08/13/24 15:49 08/15/24 01:26 7440-36-0
Arsenic ND mg/kg 11.7 1 08/13/24 15:49 08/15/24 01:26 7440-38-2
Beryllium ND mg/kg 0.47 1 08/13/24 15:49 08/15/24 01:26 7440-41-7
Cadmium 0.51 mg/kg 0.47 1 08/13/24 15:49 08/15/24 01:26 7440-43-9
Chromium 9.4 mg/kg 2.3 1 08/13/24 15:49 08/15/24 01:26 7440-47-3
Copper 135 mg/kg 23.4 1 08/13/24 15:49 08/15/24 01:26 7440-50-8
Lead ND mg/kg 4.7 1 08/13/24 15:49 08/15/24 01:26 7439-92-1
Molybdenum ND mg/kg 23.4 1 08/13/24 15:49 08/15/24 01:26 7439-98-7
Nickel 9.7 mg/kg 2.3 1 08/13/24 15:49 08/15/24 01:26 7440-02-0
Selenium 5.1 mg/kg 4.7 1 08/13/24 15:49 08/15/24 01:26 7782-49-2
Silver ND mg/kg 2.3 1 08/13/24 15:49 08/15/24 01:26 7440-22-4
Thallium ND mg/kg 4.7 1 08/13/24 15:49 08/15/24 01:26 7440-28-0
Zinc 528 mg/kg 4.7 1 08/13/24 15:49 08/15/24 01:26 7440-66-6
2540G Total Percent Solids Analytical Method:SM 2540G-2011
Pace Analytical Services-Charlotte
Total Solids 16.7 % 0.10 1 08/08/24 18:08
Percent Moisture Analytical Method:SW-846
Pace Analytical Services-Charlotte
Percent Moisture 83.1 % 0.10 1 08/08/24 17:54 N2
160.4 Total Volatile Solids Analytical Method: EPA 160.4/SM254OB-2011
Pace Analytical Services-Asheville
Total Volatile Solids 779000 mg/kg 10000 1 08/14/24 19:59
351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen, Kjeldahl,Total 57600 mg/kg 2050 10 08/21/24 20:08 08/22/24 09:35 7727-37-9
353.2 Nitrogen,NO2/NO3 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen, NO2 plus NO3 ND mg/kg 23.3 1 08/07/24 23:07 08/08/24 01:56
Nitrogen, Nitrate ND mg/kg 23.3 1 08/07/24 23:07 08/08/24 01:56 14797-55-8
Nitrogen, Nitrite ND mg/kg 23.3 1 08/07/24 23:07 08/08/24 01:56 14797-65-0
365.1 Phosphorus,Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services-Asheville
Phosphorus 21900 mg/kg 251 50 08/12/24 20:16 08/13/24 19:05 7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 36 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-BFP-1-CAKE Lab ID: 92746299020 Collected: 08/07/24 05:10 Received: 08/07/24 11:41 Matrix: Solid
Results reported on a "dry weight"basis and are adjusted for percent moisture,sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method:SW-846
Pace Analytical Services-Charlotte
Percent Moisture 83.1 % 0.10 1 08/23/24 15:48 N2
4500CNE Cyanide,Total Analytical Method:SM 4500-CN-E-2016 Preparation Method:SM 4500-CN-E-2016
Pace Analytical Services-Asheville
Cyanide ND mg/kg 1.5 1 08/14/2415:26 08/15/2411:02 57-12-5
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 37 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-BFP-1-FILT Lab ID: 92746299021 Collected: 08/07/24 05:15 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.8 MET ICPMS Analytical Method: EPA 200.8 Rev 5.4 1994 Preparation Method: EPA 200.8 Rev 5.4 1994
Pace Analytical Services-Asheville
Antimony ND ug/L 1.0 1 08/08/2416:00 08/09/2414:52 7440-36-0
Arsenic ND ug/L 1.0 1 08/08/2416:00 08/09/2414:52 7440-38-2
Beryllium ND ug/L 0.10 1 08/08/2416:00 08/09/2414:52 7440-41-7
Cadmium ND ug/L 0.10 1 08/08/2416:00 08/09/2414:52 7440-43-9
Chromium ND ug/L 1.0 1 08/08/2416:00 08/09/2414:52 7440-47-3
Copper 12.7 ug/L 2.0 1 08/08/2416:00 08/09/2414:52 7440-50-8
Lead ND ug/L 1.0 1 08/08/2416:00 08/09/2414:52 7439-92-1
Molybdenum ND ug/L 1.0 1 08/08/2416:00 08/09/2414:52 7439-98-7
Nickel 2.1 ug/L 1.0 1 08/08/2416:00 08/09/2414:52 7440-02-0
Selenium ND ug/L 2.0 1 08/08/2416:00 08/09/2414:52 7782-49-2
Silver ND ug/L 0.40 1 08/08/2416:00 08/09/2414:52 7440-22-4
Thallium ND ug/L 0.20 1 08/08/2416:00 08/09/2414:52 7440-28-0
Zinc 82.0 ug/L 10.0 1 08/08/2416:00 08/09/2414:52 7440-66-6
245.1 Mercury Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994
Pace Analytical Services-Asheville
Mercury ND ug/L 0.20 1 08/09/2419:27 08/12/2416:36 7439-97-6
2540D Total Suspended Solids Analytical Method:SM 2540D-2015
Pace Analytical Services-Asheville
Total Suspended Solids 26.2 mg/L 12.8 1 08/11/24 13:43
5210B cBOD,5 day Analytical Method:SM 521OB-2016
Pace Analytical Services-Asheville
Carbonaceous BOD,5 day 3.5 mg/L 2.0 1 08/08/24 14:06 08/13/24 15:54
350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen,Ammonia 0.29 mg/L 0.10 1 08/21/24 16:17 7664-41-7
351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen, Kjeldahl,Total 3.7 mg/L 0.50 1 08/26/24 18:34 08/27/24 09:17 7727-37-9
353.2 Nitrogen,NO2/NO3 pres. Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen, NO2 plus NO3 7.4 mg/L 0.40 10 08/22/24 03:29
365.1 Phosphorus,Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services-Asheville
Phosphorus 0.93 mg/L 0.050 1 08/22/2418:08 08/23/2411:01 7723-14-0
450OCNE Cyanide,Total Analytical Method:SM 4500-CN-E-2016 Preparation Method:SM 4500-CN-E-2016
Pace Analytical Services-Asheville
Cyanide ND mg/L 0.0080 1 08/19/2417:07 08/20/2411:35 57-12-5
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 38 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-BFP-1-FILT Lab ID: 92746299021 Collected: 08/07/24 05:15 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5220D COD Analytical Method:SM 5220D-2011 Preparation Method:SM 5220D-2011
Pace Analytical Services-Asheville
Chemical Oxygen Demand 49.4 mg/L 25.0 1 08/27/24 04:22 08/27/24 15:30
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 39 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-12 AER Lab ID: 92746299022 Collected: 08/07/24 04:06 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.8 MET ICPMS Analytical Method: EPA 200.8 Rev 5.4 1994 Preparation Method: EPA 200.8 Rev 5.4 1994
Pace Analytical Services-Asheville
Antimony 2.1 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:27 7440-36-0
Arsenic 7.7 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:27 7440-38-2
Beryllium 0.91 ug/L 0.10 1 08/08/24 16:00 08/11/24 22:27 7440-41-7
Cadmium 1.5 ug/L 0.10 1 08/08/24 16:00 08/11/24 22:27 7440-43-9
Chromium 19.1 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:27 7440-47-3
Copper 398 ug/L 10.0 5 08/08/24 16:00 08/09/2414:56 7440-50-8
Lead 8.3 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:27 7439-92-1
Molybdenum 9.2 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:27 7439-98-7
Nickel 26.2 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:27 7440-02-0
Selenium 6.4 ug/L 2.0 1 08/08/24 16:00 08/11/24 22:27 7782-49-2
Silver 3.6 ug/L 0.40 1 08/08/24 16:00 08/11/24 22:27 7440-22-4
Thallium ND ug/L 0.20 1 08/08/24 16:00 08/11/24 22:27 7440-28-0
Zinc 1600 ug/L 200 20 08/08/24 16:00 08/11/24 22:30 7440-66-6
245.1 Mercury Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994
Pace Analytical Services-Asheville
Mercury ND ug/L 0.20 1 08/09/2419:27 08/12/2416:39 7439-97-6
2540D TSS/TVSS Analytical Method: EPA 160.4/SM2540B-2015
Pace Analytical Services-Asheville
Total Suspended Solids 3300 mg/L 250 1 08/09/24 13:38
Volatile Suspended Solids 2680 mg/L 250 1 08/09/24 13:38
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 40 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-12 AER Lab ID: 92746299023 Collected: 08/07/24 04:09 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
450OCNE Cyanide,Total Analytical Method:SM 4500-CN-E-2016 Preparation Method:SM 4500-CN-E-2016
Pace Analytical Services-Asheville
Cyanide ND mg/L 0.0080 1 08/19/2417:07 08/20/2412:37 57-12-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 41 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-5_6 AER Lab ID: 92746299024 Collected: 08/07/24 04:07 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.8 MET ICPMS Analytical Method: EPA 200.8 Rev 5.4 1994 Preparation Method: EPA 200.8 Rev 5.4 1994
Pace Analytical Services-Asheville
Antimony 2.2 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:34 7440-36-0
Arsenic 8.3 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:34 7440-38-2
Beryllium 0.98 ug/L 0.10 1 08/08/24 16:00 08/11/24 22:34 7440-41-7
Cadmium 1.7 ug/L 0.10 1 08/08/24 16:00 08/11/24 22:34 7440-43-9
Chromium 19.1 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:34 7440-47-3
Copper 434 ug/L 10.0 5 08/08/24 16:00 08/09/2415:00 7440-50-8
Lead 9.9 ug/L 5.0 5 08/08/24 16:00 08/09/2415:00 7439-92-1
Molybdenum 9.4 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:34 7439-98-7
Nickel 27.5 ug/L 1.0 1 08/08/24 16:00 08/11/24 22:34 7440-02-0
Selenium 7.1 ug/L 2.0 1 08/08/24 16:00 08/11/24 22:34 7782-49-2
Silver 4.4 ug/L 0.40 1 08/08/24 16:00 08/11/24 22:34 7440-22-4
Thallium ND ug/L 1.0 5 08/08/24 16:00 08/09/2415:00 7440-28-0 D3
Zinc 1750 ug/L 200 20 08/08/24 16:00 08/11/24 22:38 7440-66-6
245.1 Mercury Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994
Pace Analytical Services-Asheville
Mercury ND ug/L 0.20 1 08/09/2419:27 08/12/2416:41 7439-97-6
2540D TSS/TVSS Analytical Method: EPA 160.4/SM2540B-2015
Pace Analytical Services-Asheville
Total Suspended Solids 3560 mg/L 250 1 08/09/24 13:38
Volatile Suspended Solids 2910 mg/L 250 1 08/09/24 13:38
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 42 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Sample: UC12-5_6 AER Lab ID: 92746299025 Collected: 08/07/24 04:09 Received: 08/07/24 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
450OCNE Cyanide,Total Analytical Method:SM 4500-CN-E-2016 Preparation Method:SM 4500-CN-E-2016
Pace Analytical Services-Asheville
Cyanide ND mg/L 0.0080 1 08/19/2417:07 08/20/2412:38 57-12-5
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 43 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 875058 Analysis Method: EPA 7471 B
QC Batch Method: EPA 7471 B Analysis Description: 7471 Mercury
Laboratory: Pace Analytical Services-Peachtree Corners,GA
Associated Lab Samples: 92746299019
METHOD BLANK: 4507441 Matrix: Solid
Associated Lab Samples: 92746299019
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/kg ND 0.032 08/13/2412:04
LABORATORY CONTROL SAMPLE: 4507442
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Mercury mg/kg 0.33 0.32 98 80-120
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4507490 4507491
MS MSD
92746772002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Mercury mg/kg ND 0.33 0.32 0.34 0.34 104 104 75-125 1
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 44 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 874602 Analysis Method: EPA 245.1 Rev 3.0 1994
QC Batch Method: EPA 245.1 Rev 3.0 1994 Analysis Description: 245.1 Mercury
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92746299009,92746299011,92746299013,92746299015,92746299017,92746299021,92746299022,
92746299024
METHOD BLANK: 4505420 Matrix: Water
Associated Lab Samples: 92746299009,92746299011,92746299013,92746299015,92746299017,92746299021,92746299022,
92746299024
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L ND 0.20 08/12/2415:30
LABORATORY CONTROL SAMPLE: 4505421
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Mercury ug/L 2.5 2.5 102 85-115
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4505422 4505423
MS MSD
92745740003 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Mercury ug/L ND 2.5 2.5 2.5 2.6 98 103 70-130 4
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4505424 4505425
MS MSD
92746299009 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Mercury ug/L ND 2.5 2.5 2.4 2.5 97 98 70-130 1
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 45 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 875840 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92746299003,92746299007
METHOD BLANK: 4511481 Matrix: Water
Associated Lab Samples: 92746299003,92746299007
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Hardness,Total(SM 2340B) ug/L ND 662 08/19/24 10:27
LABORATORY CONTROL SAMPLE: 4511482
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Hardness,Total(SM 2340B) ug/L 33100 31700 96 85-115
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4511483 4511484
MS MSD
92746236001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Hardness,Total(SM 2340B) ug/L 87.6 33100 33100 121000 131000 101 132 70-130 8
mg/L
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4511485 4511486
MS MSD
92746788001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Hardness,Total(SM 2340B) ug/L 62.0 33100 33100 92100 93100 91 94 70-130 1
mg/L
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 46 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 874203 Analysis Method: EPA 200.8 Rev 5.4 1994
QC Batch Method: EPA 200.8 Rev 5.4 1994 Analysis Description: 200.8 MET
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92746299003
METHOD BLANK: 4503451 Matrix: Water
Associated Lab Samples: 92746299003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Antimony ug/L ND 1.0 08/09/2415:44
Arsenic ug/L ND 1.0 08/09/2415:44
Beryllium ug/L ND 0.10 08/09/2415:44
Cadmium ug/L ND 0.10 08/09/2415:44
Chromium ug/L ND 1.0 08/09/2415:44
Copper ug/L ND 2.0 08/09/2415:44
Lead ug/L ND 1.0 08/09/2415:44
Molybdenum ug/L ND 1.0 08/09/2415:44
Nickel ug/L ND 1.0 08/09/2415:44
Selenium ug/L ND 2.0 08/09/2415:44
Silver ug/L ND 0.40 08/09/2415:44
Thallium ug/L ND 0.20 08/09/2415:44
Zinc ug/L ND 10.0 08/09/2415:44
LABORATORY CONTROL SAMPLE: 4503452
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Antimony ug/L 50 52.5 105 85-115
Arsenic ug/L 50 50.7 101 85-115
Beryllium ug/L 50 55.3 111 85-115
Cadmium ug/L 50 52.7 105 85-115
Chromium ug/L 50 52.5 105 85-115
Copper ug/L 50 53.6 107 85-115
Lead ug/L 50 51.8 104 85-115
Molybdenum ug/L 50 51.4 103 85-115
Nickel ug/L 50 53.3 107 85-115
Selenium ug/L 50 51.2 102 85-115
Silver ug/L 25 26.4 106 85-115
Thallium ug/L 25 26.7 107 85-115
Zinc ug/L 50 51.7 103 85-115
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4503453 4503454
MS MSD
92746001002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Antimony ug/L ND 50 50 53.1 53.2 105 106 70-130 0
Arsenic ug/L 1.9 50 50 52.8 53.4 102 103 70-130 1
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 47 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4503453 4503454
MS MSD
92746001002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Beryllium ug/L ND 50 50 54.9 54.5 110 109 70-130 1
Cadmium ug/L ND 50 50 52.0 52.3 104 104 70-130 1
Chromium ug/L 3.7 50 50 56.4 56.3 105 105 70-130 0
Copper ug/L 13.9 50 50 65.2 65.6 103 103 70-130 1
Lead ug/L ND 50 50 52.8 53.1 104 105 70-130 1
Molybdenum ug/L 83.9 50 50 135 137 103 106 70-130 1
Nickel ug/L 14.4 50 50 66.9 67.1 105 105 70-130 0
Selenium ug/L ND 50 50 50.6 50.2 101 100 70-130 1
Silver ug/L ND 25 25 26.0 26.4 104 106 70-130 1
Thallium ug/L ND 25 25 27.0 27.0 108 108 70-130 0
Zinc ug/L ND 50 50 60.0 60.6 101 102 70-130 1
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 48 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 874279 Analysis Method: EPA 200.8 Rev 5.4 1994
QC Batch Method: EPA 200.8 Rev 5.4 1994 Analysis Description: 200.8 MET
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92746299009,92746299011,92746299013,92746299015,92746299017,92746299021,92746299022,
92746299024
METHOD BLANK: 4503846 Matrix: Water
Associated Lab Samples: 92746299009,92746299011,92746299013,92746299015,92746299017,92746299021,92746299022,
92746299024
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Antimony ug/L ND 1.0 08/09/2413:46
Arsenic ug/L ND 1.0 08/09/2413:46
Beryllium ug/L ND 0.10 08/09/2413:46
Cadmium ug/L ND 0.10 08/09/2413:46
Chromium ug/L ND 1.0 08/09/2413:46
Copper ug/L ND 2.0 08/09/2413:46
Lead ug/L ND 1.0 08/09/2413:46
Molybdenum ug/L ND 1.0 08/09/2413:46
Nickel ug/L ND 1.0 08/09/2413:46
Selenium ug/L ND 2.0 08/09/2413:46
Silver ug/L ND 0.40 08/09/2413:46
Thallium ug/L ND 0.20 08/09/2413:46
Zinc ug/L ND 10.0 08/09/2413:46
LABORATORY CONTROL SAMPLE: 4503847
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Antimony ug/L 50 52.8 106 85-115
Arsenic ug/L 50 51.2 102 85-115
Beryllium ug/L 50 52.3 105 85-115
Cadmium ug/L 50 52.0 104 85-115
Chromium ug/L 50 51.4 103 85-115
Copper ug/L 50 52.5 105 85-115
Lead ug/L 50 49.9 100 85-115
Molybdenum ug/L 50 52.5 105 85-115
Nickel ug/L 50 51.7 103 85-115
Selenium ug/L 50 51.0 102 85-115
Silver ug/L 25 26.0 104 85-115
Thallium ug/L 25 25.8 103 85-115
Zinc ug/L 50 51.6 103 85-115
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4503860 4503861
MS MSD
92746299009 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Antimony ug/L ND 50 50 54.7 53.9 108 107 70-130 2
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 49 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4503860 4503861
MS MSD
92746299009 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Arsenic ug/L ND 50 50 53.1 52.1 105 104 70-130 2
Beryllium ug/L ND 50 50 54.6 54.4 109 109 70-130 0
Cadmium ug/L ND 50 50 52.5 52.4 105 105 70-130 0
Chromium ug/L ND 50 50 53.7 53.3 107 106 70-130 1
Copper ug/L 2.1 50 50 55.4 55.3 106 106 70-130 0
Lead ug/L ND 50 50 52.2 51.9 104 104 70-130 1
Molybdenum ug/L ND 50 50 54.8 53.3 108 106 70-130 3
Nickel ug/L 1.1 50 50 54.1 54.3 106 106 70-130 0
Selenium ug/L ND 50 50 51.1 50.7 102 101 70-130 1
Silver ug/L ND 25 25 26.5 26.3 106 105 70-130 1
Thallium ug/L ND 25 25 27.4 27.1 110 108 70-130 1
Zinc ug/L 28.2 50 50 79.5 77.5 103 99 70-130 3
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4503862 4503863
MS MSD
92746299011 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Antimony ug/L 2.0 50 50 39.3 38.5 75 73 70-130 2
Arsenic ug/L 8.3 50 50 58.0 57.5 99 99 70-130 1
Beryllium ug/L 1.0 50 50 52.7 51.6 103 101 70-130 2
Cadmium ug/L 1.6 50 50 53.3 52.7 104 102 70-130 1
Chromium ug/L 19.1 50 50 72.5 70.3 107 102 70-130 3
Copper ug/L 443 50 50 471 462 56 38 70-130 2 M1
Lead ug/L 9.1 50 50 57.5 57.5 97 97 70-130 0
Molybdenum ug/L 9.0 50 50 51.3 50.6 85 83 70-130 1
Nickel ug/L 27.9 50 50 81.1 80.3 107 105 70-130 1
Selenium ug/L 6.8 50 50 51.4 49.7 89 86 70-130 3
Silver ug/L 3.5 25 25 29.8 29.6 105 104 70-130 1
Thallium ug/L ND 25 25 25.1 25.2 100 100 70-130 0
Zinc ug/L 1720 50 50 1790 1770 148 110 70-130 1 M1
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 50 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 874647 Analysis Method: EPA 200.8 Rev 5.4 1994
QC Batch Method: EPA 200.8 Rev 5.4 1994 Analysis Description: 200.8 MET
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92746299007
METHOD BLANK: 4505705 Matrix: Water
Associated Lab Samples: 92746299007
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Antimony ug/L ND 1.0 08/11/24 23:29
Arsenic ug/L ND 1.0 08/11/24 23:29
Beryllium ug/L ND 0.10 08/11/24 23:29
Cadmium ug/L ND 0.10 08/11/24 23:29
Chromium ug/L ND 1.0 08/11/24 23:29
Copper ug/L ND 2.0 08/11/24 23:29
Lead ug/L ND 1.0 08/11/24 23:29
Molybdenum ug/L ND 1.0 08/11/24 23:29
Nickel ug/L ND 1.0 08/11/24 23:29
Selenium ug/L ND 2.0 08/11/24 23:29
Silver ug/L ND 0.40 08/11/24 23:29
Thallium ug/L ND 0.20 08/11/24 23:29
Zinc ug/L ND 10.0 08/11/24 23:29
LABORATORY CONTROL SAMPLE: 4505706
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Antimony ug/L 50 50.4 101 85-115
Arsenic ug/L 50 48.0 96 85-115
Beryllium ug/L 50 52.9 106 85-115
Cadmium ug/L 50 51.7 103 85-115
Chromium ug/L 50 52.2 104 85-115
Copper ug/L 50 53.3 107 85-115
Lead ug/L 50 50.5 101 85-115
Molybdenum ug/L 50 49.4 99 85-115
Nickel ug/L 50 52.9 106 85-115
Selenium ug/L 50 49.1 98 85-115
Silver ug/L 25 25.8 103 85-115
Thallium ug/L 25 26.1 105 85-115
Zinc ug/L 50 50.0 100 85-115
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4505707 4505708
MS MSD
92744458002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Antimony ug/L ND 50 50 48.7 49.8 97 99 70-130 2
Arsenic ug/L ND 50 50 48.5 49.9 97 99 70-130 3
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 51 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4505707 4505708
MS MSD
92744458002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Beryllium ug/L ND 50 50 48.3 49.8 97 100 70-130 3
Cadmium ug/L ND 50 50 46.0 46.8 92 93 70-130 2
Chromium ug/L 1.8 50 50 53.6 54.1 103 105 70-130 1
Copper ug/L ND 50 50 53.3 49.9 106 99 70-130 7
Lead ug/L ND 50 50 50.8 51.3 102 103 70-130 1
Molybdenum ug/L ND 50 50 50.9 52.1 101 104 70-130 2
Nickel ug/L 1.2 50 50 50.3 51.0 98 100 70-130 1
Selenium ug/L ND 50 50 44.9 45.8 89 91 70-130 2
Silver ug/L ND 25 25 23.3 23.6 93 94 70-130 1
Thallium ug/L ND 25 25 26.4 26.6 105 106 70-130 1
Zinc ug/L ND 50 50 54.0 52.8 95 92 70-130 2
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4505709 4505710
MS MSD
92744458004 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Antimony ug/L 1.1 50 50 50.3 48.8 98 95 70-130 3
Arsenic ug/L 1.1 50 50 50.0 48.1 98 94 70-130 4
Beryllium ug/L ND 50 50 52.5 51.0 105 102 70-130 3
Cadmium ug/L ND 50 50 50.3 49.4 100 99 70-130 2
Chromium ug/L 2.3 50 50 53.8 52.6 103 101 70-130 2
Copper ug/L ND 50 50 53.5 52.5 104 102 70-130 2
Lead ug/L ND 50 50 50.2 49.2 100 98 70-130 2
Molybdenum ug/L 3.9 50 50 53.6 52.6 99 97 70-130 2
Nickel ug/L 2.0 50 50 53.8 52.3 104 101 70-130 3
Selenium ug/L ND 50 50 47.8 47.0 95 94 70-130 2
Silver ug/L ND 25 25 25.4 24.8 102 99 70-130 3
Thallium ug/L ND 25 25 26.0 25.5 104 102 70-130 2
Zinc ug/L 303 50 50 360 362 114 117 70-130 0
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 52 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 875260 Analysis Method: EPA 6010D
QC Batch Method: EPA 3050E Analysis Description: 6010 MET
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92746299019
METHOD BLANK: 4508545 Matrix: Solid
Associated Lab Samples: 92746299019
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Antimony mg/kg ND 2.5 08/15/24 00:53
Arsenic mg/kg ND 2.5 08/15/24 00:53
Beryllium mg/kg ND 0.10 08/15/24 00:53
Cadmium mg/kg ND 0.10 08/15/24 00:53
Chromium mg/kg ND 0.50 08/15/24 00:53
Copper mg/kg ND 5.0 08/15/24 00:53
Lead mg/kg ND 1.0 08/15/24 00:53
Molybdenum mg/kg ND 5.0 08/15/24 00:53
Nickel mg/kg ND 0.50 08/15/24 00:53
Selenium mg/kg ND 1.0 08/15/24 00:53
Silver mg/kg ND 0.50 08/15/24 00:53
Thallium mg/kg ND 1.0 08/15/24 00:53
Zinc mg/kg ND 1.0 08/15/24 00:53
LABORATORY CONTROL SAMPLE: 4508546
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Antimony mg/kg 50 51.3 103 80-120
Arsenic mg/kg 50 50.9 102 80-120
Beryllium mg/kg 50 48.1 96 80-120
Cadmium mg/kg 50 50.3 101 80-120
Chromium mg/kg 50 49.4 99 80-120
Copper mg/kg 50 50.0 100 80-120
Lead mg/kg 50 49.9 100 80-120
Molybdenum mg/kg 50 52.7 105 80-120
Nickel mg/kg 50 49.4 99 80-120
Selenium mg/kg 50 50.5 101 80-120
Silver mg/kg 25 25.1 101 80-120
Thallium mg/kg 50 51.8 104 80-120
Zinc mg/kg 50 50.4 101 80-120
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4508547 4508548
MS MSD
92746020001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Antimony mg/kg ND 52.9 53.3 52.9 54.8 100 102 75-125 4
Arsenic mg/kg ND 52.9 53.3 53.4 54.9 100 102 75-125 3
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 53 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4508547 4508548
MS MSD
92746020001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Beryllium mg/kg ND 52.9 53.3 49.6 51.7 94 97 75-125 4
Cadmium mg/kg ND 52.9 53.3 51.5 53.4 97 100 75-125 3
Chromium mg/kg ND 52.9 53.3 50.4 52.5 95 98 75-125 4
Copper mg/kg ND 52.9 53.3 54.3 56.5 100 103 75-125 4
Lead mg/kg ND 52.9 53.3 51.2 52.8 96 99 75-125 3
Molybdenum mg/kg ND 52.9 53.3 53.8 55.9 102 105 75-125 4
Nickel mg/kg ND 52.9 53.3 51.2 53.1 96 99 75-125 4
Selenium mg/kg ND 52.9 53.3 54.5 55.9 103 104 75-125 3
Silver mg/kg ND 26.5 26.7 25.9 26.6 98 100 75-125 3
Thallium mg/kg ND 52.9 53.3 52.9 54.8 100 103 75-125 4
Zinc mg/kg 8.4 52.9 53.3 60.9 59.5 99 96 75-125 2
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 54 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 874338 Analysis Method: EPA 624.1
QC Batch Method: EPA 624.1 Analysis Description: 624 MSV with Acrolein
Laboratory: Pace Analytical Services-Charlotte
Associated Lab Samples: 92746299004,92746299008,92746299012,92746299018
METHOD BLANK: 4504162 Matrix: Water
Associated Lab Samples: 92746299004,92746299008,92746299012,92746299018
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,1,1-Trichloroethane ug/L ND 2.0 08/08/24 15:18
1,1,2,2-Tetrachloroethane ug/L ND 2.0 08/08/24 15:18
1,1,2-Trichloroethane ug/L ND 2.0 08/08/24 15:18
1,1-Dichloroethane ug/L ND 2.0 08/08/24 15:18
1,1-Dichloroethene ug/L ND 2.0 08/08/24 15:18
1,2-Dichlorobenzene ug/L ND 2.0 08/08/24 15:18
1,2-Dichloroethane ug/L ND 2.0 08/08/24 15:18
1,2-Dichloropropene ug/L ND 2.0 08/08/24 15:18
1,3-Dichlorobenzene ug/L ND 2.0 08/08/24 15:18
1,4-Dichlorobenzene ug/L ND 2.0 08/08/24 15:18
2-Chloroethylvinyl ether ug/L ND 5.0 08/08/24 15:18
Acrolein ug/L ND 5.0 08/08/24 15:18
Acrylonitrile ug/L ND 5.0 08/08/24 15:18
Benzene ug/L ND 1.0 08/08/24 15:18
Bromodichloromethane ug/L ND 2.0 08/08/24 15:18
Bromoform ug/L ND 2.0 08/08/24 15:18
Bromomethane ug/L ND 2.0 08/08/24 15:18
Carbon tetrachloride ug/L ND 2.0 08/08/24 15:18
Chlorobenzene ug/L ND 2.0 08/08/24 15:18
Chloroethane ug/L ND 2.0 08/08/24 15:18
Chloroform ug/L ND 2.0 08/08/24 15:18
Chloromethane ug/L ND 2.0 08/08/24 15:18
cis-1,2-Dichloroethene ug/L ND 2.0 08/08/24 15:18
cis-1,3-Dichloropropene ug/L ND 2.0 08/08/24 15:18
Dibromochloromethane ug/L ND 2.0 08/08/24 15:18
Ethylbenzene ug/L ND 1.0 08/08/24 15:18
Methylene Chloride ug/L ND 2.0 08/08/24 15:18
Tetrachloroethene ug/L ND 2.0 08/08/24 15:18
Toluene ug/L ND 1.0 08/08/24 15:18
trans-1,2-Dichloroethene ug/L ND 2.0 08/08/24 15:18
trans-1,3-Dichloropropene ug/L ND 2.0 08/08/24 15:18
Trichloroethene ug/L ND 2.0 08/08/24 15:18
Trichlorofluoromethane ug/L ND 2.0 08/08/24 15:18
Vinyl chloride ug/L ND 2.0 08/08/24 15:18
1,2-Dichloroethane-d4(S) % 104 70-130 08/08/24 15:18
4-Bromofluorobenzene(S) % 101 70-130 08/08/24 15:18
Toluene-d8(S) % 99 70-130 08/08/24 15:18
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 55 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
LABORATORY CONTROL SAMPLE: 4504163
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
1,1,1-Trichloroethane ug/L 20 23.4 117 70-130
1,1,2,2-Tetrachloroethane ug/L 20 21.9 109 70-130
1,1,2-Trichloroethane ug/L 20 23.1 116 70-130
1,1-Dichloroethane ug/L 20 22.7 114 70-130
1,1-Dichloroethene ug/L 20 23.2 116 69-131
1,2-Dichlorobenzene ug/L 20 23.4 117 70-130
1,2-Dichloroethane ug/L 20 23.2 116 70-130
1,2-Dichloropropane ug/L 20 22.9 115 70-130
1,3-Dichlorobenzene ug/L 20 22.9 115 70-130
1,4-Dichlorobenzene ug/L 20 23.4 117 70-130
2-Chloroethylvinyl ether ug/L 40 48.9 122 64-133
Acrolein ug/L 100 105 105 60-140
Acrylonitrile ug/L 100 111 111 70-130
Benzene ug/L 20 22.7 114 65-135
Bromodichloromethane ug/L 20 22.6 113 70-130
Bromoform ug/L 20 22.1 111 70-130
Bromomethane ug/L 20 20.0 100 41-148
Carbon tetrachloride ug/L 20 23.7 119 70-130
Chlorobenzene ug/L 20 22.2 111 70-130
Chloroethane ug/L 20 21.3 107 41-157
Chloroform ug/L 20 22.7 113 70-130
Chloromethane ug/L 20 22.6 113 59-141
cis-1,2-Dichloroethene ug/L 20 23.2 116 70-130
cis-1,3-Dichloropropene ug/L 20 23.2 116 70-130
Dibromochloromethane ug/L 20 23.2 116 70-130
Ethylbenzene ug/L 20 22.4 112 70-130
Methylene Chloride ug/L 20 22.1 110 62-130
Tetrachloroethene ug/L 20 21.9 109 70-130
Toluene ug/L 20 22.9 115 70-130
trans-1,2-Dichloroethene ug/L 20 24.0 120 70-130
trans-1,3-Dichloropropene ug/L 20 23.8 119 70-130
Trichloroethene ug/L 20 22.7 114 70-130
Trichlorofluoromethane ug/L 20 20.8 104 57-130
Vinyl chloride ug/L 20 21.1 106 66-140
1,2-Dichloroethane-d4(S) % 98 70-130
4-Bromofluorobenzene(S) % 99 70-130
Toluene-d8(S) % 100 70-130
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4504164 4504165
MS MSD
92745711001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
1,1,1-Trichloroethane ug/L ND 20 20 20.5 21.8 102 109 70-150 6
1,1,2,2-Tetrachloroethane ug/L ND 20 20 18.0 19.7 90 99 66-144 9
1,1,2-Trichloroethane ug/L ND 20 20 19.4 19.7 97 99 70-142 2
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 56 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4504164 4504165
MS MSD
92745711001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
1,1-Dichloroethane ug/L ND 20 20 21.0 21.0 105 105 67-150 0
1,1-Dichloroethene ug/L ND 20 20 21.3 21.8 107 109 64-162 2
1,2-Dichlorobenzene ug/L ND 20 20 20.5 19.9 102 99 70-142 3
1,2-Dichloroethane ug/L ND 20 20 19.7 20.8 98 104 58-145 5
1,2-Dichloropropane ug/L ND 20 20 19.9 19.8 99 99 70-144 1
1,3-Dichlorobenzene ug/L ND 20 20 19.9 20.6 100 103 70-142 3
1,4-Dichlorobenzene ug/L ND 20 20 19.7 20.0 98 100 70-140 2
2-Chloroethylvinyl ether ug/L ND 40 40 39.7 42.5 99 106 10-211 7
Acrolein ug/L ND 100 100 19.4 16.4 19 16 40-160 17 M1
Acrylonitrile ug/L ND 100 100 79.7 98.1 80 98 59-155 21
Benzene ug/L ND 20 20 20.7 21.1 104 105 70-142 2
Bromodichloromethane ug/L ND 20 20 20.1 20.4 100 102 70-139 2
Bromoform ug/L ND 20 20 18.7 19.4 93 97 64-140 4
Bromomethane ug/L ND 20 20 14.8 15.6 74 78 28-192 5
Carbon tetrachloride ug/L ND 20 20 21.1 21.3 106 106 70-140 1
Chlorobenzene ug/L ND 20 20 19.3 20.0 97 100 70-141 3
Chloroethane ug/L ND 20 20 18.4 19.7 92 99 58-191 7
Chloroform ug/L ND 20 20 19.6 19.5 92 92 70-138 0
Chloromethane ug/L ND 20 20 19.0 19.9 95 100 43-162 5
cis-1,2-Dichloroethene ug/L ND 20 20 20.1 21.1 100 105 70-143 5
cis-1,3-Dichloropropene ug/L ND 20 20 19.6 19.9 98 100 68-151 2
Dibromochloromethane ug/L ND 20 20 19.7 20.1 98 100 70-144 2
Ethylbenzene ug/L ND 20 20 19.9 20.4 99 102 70-143 3
Methylene Chloride ug/L ND 20 20 18.6 19.5 93 98 70-144 5
Tetrachloroethene ug/L ND 20 20 18.3 19.2 92 96 70-143 5
Toluene ug/L ND 20 20 20.0 20.7 100 103 69-144 3
trans-1,2-Dichloroethene ug/L ND 20 20 20.4 22.0 102 110 70-151 8
trans-1,3-Dichloropropene ug/L ND 20 20 20.3 20.9 101 105 70-139 3
Trichloroethene ug/L ND 20 20 20.5 20.4 102 102 70-142 0
Trichlorofluoromethane ug/L ND 20 20 19.0 19.8 95 99 62-146 4
Vinyl chloride ug/L ND 20 20 18.8 19.9 94 100 61-162 6
1,2-Dichloroethane-d4(S) % 101 100 70-130
4-Bromofluorobenzene(S) % 99 100 70-130
Toluene-d8(S) % 99 97 70-130
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 57 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 874068 Analysis Method: EPA 608.3
QC Batch Method: EPA 608.3 Analysis Description: 608 PCB Pest Red Vol
Laboratory: Pace Analytical Services-Charlotte
Associated Lab Samples: 92746299003
METHOD BLANK: 4502871 Matrix: Water
Associated Lab Samples: 92746299003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
4,4'-DDD ug/L ND 0.050 08/08/24 12:16
4,4'-DDE ug/L ND 0.050 08/08/24 12:16
4,4'-DDT ug/L ND 0.050 08/08/24 12:16
Aldrin ug/L ND 0.050 08/08/24 12:16
alpha-BHC ug/L ND 0.050 08/08/24 12:16
alpha-Chlordane ug/L ND 0.050 08/08/24 12:16
beta-BHC ug/L ND 0.050 08/08/24 12:16
Chlordane(Technical) ug/L ND 0.50 08/08/24 12:16
delta-BHC ug/L ND 0.050 08/08/24 12:16
Dieldrin ug/L ND 0.050 08/08/24 12:16
Endosulfan I ug/L ND 0.050 08/08/24 12:16
Endosulfan II ug/L ND 0.050 08/08/24 12:16
Endosulfan sulfate ug/L ND 0.050 08/08/24 12:16
Endrin ug/L ND 0.050 08/08/24 12:16
Endrin aldehyde ug/L ND 0.050 08/08/24 12:16
gamma-BHC(Lindane) ug/L ND 0.050 08/08/24 12:16
gamma-Chlordane ug/L ND 0.050 08/08/24 12:16
Heptachlor ug/L ND 0.050 08/08/24 12:16
Heptachlor epoxide ug/L ND 0.050 08/08/24 12:16
PCB-1016(Aroclor 1016) ug/L ND 0.50 08/08/24 12:16
PCB-1221 (Aroclor 1221) ug/L ND 0.50 08/08/24 12:16
PCB-1232(Aroclor 1232) ug/L ND 0.50 08/08/24 12:16
PCB-1242(Aroclor 1242) ug/L ND 0.50 08/08/24 12:16
PCB-1248(Aroclor 1248) ug/L ND 0.50 08/08/24 12:16
PCB-1254(Aroclor 1254) ug/L ND 0.50 08/08/24 12:16
PCB-1260(Aroclor 1260) ug/L ND 0.50 08/08/24 12:16
Toxaphene ug/L ND 0.50 08/08/24 12:16
Decachlorobiphenyl(S) % 146 19-200 08/08/24 12:16
Tetrachloro-m-xylene(S) % 78 10-137 08/08/24 12:16
LABORATORY CONTROL SAMPLE: 4502872
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
4,4'-DDD ug/L 0.25 0.32 127 31-141
4,4'-DDE ug/L 0.25 0.30 120 30-145
4,4'-DDT ug/L 0.25 0.29 117 25-160
Aldrin ug/L 0.25 0.26 102 42-135
alpha-BHC ug/L 0.25 0.30 119 37-140
alpha-Chlordane ug/L 0.25 0.31 122 45-140
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 58 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
LABORATORY CONTROL SAMPLE: 4502872
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
beta-BHC ug/L 0.25 0.30 121 38-147
delta-BHC ug/L 0.25 0.27 108 19-140
Dieldrin ug/L 0.25 0.30 120 36-146
Endosulfan I ug/L 0.25 0.31 122 45-153
Endosulfan II ug/L 0.25 0.33 134 38-155
Endosulfan sulfate ug/L 0.25 0.31 125 42-144
Endrin ug/L 0.25 0.31 122 33-147
Endrin aldehyde ug/L 0.25 0.33 133 33-153
gamma-BHC(Lindane) ug/L 0.25 0.29 117 32-140
gamma-Chlordane ug/L 0.25 0.33 132 45-140
Heptachlor ug/L 0.25 0.37 149 34-140 L1
Heptachlor epoxide ug/L 0.25 0.30 120 37-142
Decachlorobiphenyl(S) % 164 19-200
Tetrachloro-m-xylene(S) % 107 10-137
LABORATORY CONTROL SAMPLE: 4502873
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
PCB-1016(Aroclor 1016) ug/L 5 5.8 116 50-140
PCB-1260(Aroclor 1260) ug/L 5 5.6 112 42-140
Decachlorobiphenyl(S) % 145 19-200
Tetrachloro-m-xylene(S) % 129 10-137
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4502874 4502875
MS MSD
92745876001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
4,4'-DDD ug/L ND 0.5 0.5 0.55 0.61 109 121 31-141 10
4,4'-DDE ug/L ND 0.5 0.5 0.52 0.59 105 117 30-145 11
4,4'-DDT ug/L ND 0.5 0.5 0.52 0.59 105 118 25-160 12
Aldrin ug/L ND 0.5 0.5 0.47 0.56 94 112 42-140 18
alpha-BHC ug/L ND 0.5 0.5 0.50 0.58 101 116 37-140 14
alpha-Chlordane ug/L ND 0.5 0.5 0.53 0.59 107 118 45-140 10
beta-BHC ug/L ND 0.5 0.5 0.51 0.64 102 127 21-147 21
delta-BHC ug/L ND 0.5 0.5 0.45 0.50 90 99 19-140 10
Dieldrin ug/L ND 0.5 0.5 0.51 0.56 102 112 36-146 9
Endosulfan I ug/L ND 0.5 0.5 0.53 0.59 105 118 45-153 11
Endosulfan II ug/L ND 0.5 0.5 0.58 0.65 117 130 13-174 11
Endosulfan sulfate ug/L ND 0.5 0.5 0.54 0.61 108 122 26-144 12
Endrin ug/L ND 0.5 0.5 0.54 0.60 108 120 30-147 10
Endrin aldehyde ug/L ND 0.5 0.5 0.56 0.62 112 123 10-167 10
gamma-BHC(Lindane) ug/L ND 0.5 0.5 0.50 0.62 101 125 32-140 21
gamma-Chlordane ug/L ND 0.5 0.5 0.58 0.63 116 126 45-140 9
Heptachlor ug/L ND 0.5 0.5 0.69 0.71 139 142 34-140 3 MO
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 59 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4502874 4502875
MS MSD
92745876001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Heptachlor epoxide ug/L ND 0.5 0.5 0.51 0.56 102 112 37-142 9
Decachlorobiphenyl(S) % 136 155 19-200
Tetrachloro-m-xylene(S) % 90 166 10-137 SO
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4502876 4502877
MS MSD
92745711001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
PCB-1016(Aroclor 1016) ug/L ND 10 10 11.3 11.7 113 117 50-140 4
PCB-1260(Aroclor 1260) ug/L ND 10 10 11.5 11.7 115 117 42-140 2
Decachlorobiphenyl(S) % 144 135 19-200
Tetrachloro-m-xylene(S) % 112 105 10-137
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 60 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 874558 Analysis Method: EPA 608.3
QC Batch Method: EPA 608.3 Analysis Description: 608 PCB Pest Red Vol
Laboratory: Pace Analytical Services-Charlotte
Associated Lab Samples: 92746299007,92746299011,92746299018
METHOD BLANK: 4505262 Matrix: Water
Associated Lab Samples: 92746299007,92746299011,92746299018
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
4,4'-DDD ug/L ND 0.050 08/13/24 22:55
4,4'-DDE ug/L ND 0.050 08/13/24 22:55
4,4'-DDT ug/L ND 0.050 08/13/24 22:55
Aldrin ug/L ND 0.050 08/13/24 22:55
alpha-BHC ug/L ND 0.050 08/13/24 22:55
alpha-Chlordane ug/L ND 0.050 08/13/24 22:55
beta-BHC ug/L ND 0.050 08/13/24 22:55
Chlordane(Technical) ug/L ND 0.50 08/13/24 22:55
delta-BHC ug/L ND 0.050 08/13/24 22:55
Dieldrin ug/L ND 0.050 08/13/24 22:55
Endosulfan I ug/L ND 0.050 08/13/24 22:55
Endosulfan II ug/L ND 0.050 08/13/24 22:55
Endosulfan sulfate ug/L ND 0.050 08/13/24 22:55
Endrin ug/L ND 0.050 08/13/24 22:55
Endrin aldehyde ug/L ND 0.050 08/13/24 22:55
gamma-BHC(Lindane) ug/L ND 0.050 08/13/24 22:55
gamma-Chlordane ug/L ND 0.050 08/13/24 22:55
Heptachlor ug/L ND 0.050 08/13/24 22:55
Heptachlor epoxide ug/L ND 0.050 08/13/24 22:55
PCB-1016(Aroclor 1016) ug/L ND 0.50 08/13/24 22:55
PCB-1221 (Aroclor 1221) ug/L ND 0.50 08/13/24 22:55
PCB-1232(Aroclor 1232) ug/L ND 0.50 08/13/24 22:55
PCB-1242(Aroclor 1242) ug/L ND 0.50 08/13/24 22:55
PCB-1248(Aroclor 1248) ug/L ND 0.50 08/13/24 22:55
PCB-1254(Aroclor 1254) ug/L ND 0.50 08/13/24 22:55
PCB-1260(Aroclor 1260) ug/L ND 0.50 08/13/24 22:55
Toxaphene ug/L ND 0.50 08/13/24 22:55
Decachlorobiphenyl(S) % 100 19-200 08/13/24 22:55
Tetrachloro-m-xylene(S) % 61 10-137 08/13/24 22:55
LABORATORY CONTROL SAMPLE: 4505263
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
4,4'-DDD ug/L 0.25 0.14 56 31-141
4,4'-DDE ug/L 0.25 0.14 57 30-145
4,4'-DDT ug/L 0.25 0.15 61 25-160
Aldrin ug/L 0.25 0.13 51 42-135
alpha-BHC ug/L 0.25 0.15 61 37-140
alpha-Chlordane ug/L 0.25 0.17 70 45-140
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 61 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
LABORATORY CONTROL SAMPLE: 4505263
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
beta-BHC ug/L 0.25 0.15 61 38-147
delta-BHC ug/L 0.25 0.14 57 19-140
Dieldrin ug/L 0.25 0.14 55 36-146
Endosulfan I ug/L 0.25 0.15 60 45-153
Endosulfan II ug/L 0.25 0.16 65 38-155
Endosulfan sulfate ug/L 0.25 0.14 55 42-144
Endrin ug/L 0.25 0.15 60 33-147
Endrin aldehyde ug/L 0.25 0.16 66 33-153
gamma-BHC(Lindane) ug/L 0.25 0.15 59 32-140
gamma-Chlordane ug/L 0.25 0.18 72 45-140
Heptachlor ug/L 0.25 0.29 115 34-140
Heptachlor epoxide ug/L 0.25 0.14 57 37-142
Decachlorobiphenyl(S) % 87 19-200
Tetrachloro-m-xylene(S) % 63 10-137
LABORATORY CONTROL SAMPLE: 4505264
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
PCB-1016(Aroclor 1016) ug/L 5 3.9 78 50-140
PCB-1260(Aroclor 1260) ug/L 5 2.3 47 42-140
Decachlorobiphenyl(S) % 60 19-200
Tetrachloro-m-xylene(S) % 44 10-137
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4505265 4505266
MS MSD
92746528001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
4,4'-DDD ug/L ND 0.5 0.5 0.22 .0981 44 20 31-141 M1
4,4'-DDE ug/L ND 0.5 0.5 0.28 0.10 55 20 30-145 94 M1,R1
4,4'-DDT ug/L ND 0.5 0.5 0.22 .096J 43 19 25-160 M1
Aldrin ug/L ND 0.5 0.5 0.24 0.12 48 25 42-140 63 M1,R1
alpha-BHC ug/L ND 0.5 0.5 0.31 0.24 61 49 37-140 23
alpha-Chlordane ug/L ND 0.5 0.5 0.26 0.16 52 33 45-140 46 M1,R1
beta-BHC ug/L ND 0.5 0.5 0.34 0.24 68 48 21-147 34
delta-BHC ug/L ND 0.5 0.5 0.27 0.21 53 42 19-140 24
Dieldrin ug/L ND 0.5 0.5 0.20 0.10 40 21 36-146 63 M1,R1
Endosulfan I ug/L ND 0.5 0.5 0.22 0.13 44 26 45-153 53 M1,R1
Endosulfan II ug/L ND 0.5 0.5 0.26 0.19 52 39 13-174 29
Endosulfan sulfate ug/L ND 0.5 0.5 0.19 0.12 39 23 26-144 49 M1,R1
Endrin ug/L ND 0.5 0.5 0.22 0.12 43 23 30-147 59 M1,R1
Endrin aldehyde ug/L ND 0.5 0.5 0.15 0.13 30 26 10-167 16
gamma-BHC(Lindane) ug/L ND 0.5 0.5 0.28 0.20 55 40 32-140 33
gamma-Chlordane ug/L ND 0.5 0.5 0.25 0.17 50 34 45-140 37 M1,R1
Heptachlor ug/L ND 0.5 0.5 0.49 0.52 98 104 34-140 6
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 62 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4505265 4505266
MS MSD
92746528001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Heptachlor epoxide ug/L ND 0.5 0.5 0.22 0.13 45 27 37-142 50 M1,R1
Decachlorobiphenyl(S) % 0 0 19-200 SO
Tetrachloro-m-xylene(S) % 25 33 10-137
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4505267 4505268
MS MSD
92746482001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
PCB-1016(Aroclor 1016) ug/L ND 8.3 8.3 7.0 10.2 84 122 50-140 36
PCB-1260(Aroclor 1260) ug/L ND 8.3 8.3 5.9 4.4 71 53 42-140 29
Decachlorobiphenyl(S) % 89 61 19-200
Tetrachloro-m-xylene(S) % 80 59 10-137
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 63 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 874069 Analysis Method: EPA 625.1
QC Batch Method: EPA 625.1 Analysis Description: 625 MSS
Laboratory: Pace Analytical Services-Charlotte
Associated Lab Samples: 92746299004,92746299007,92746299011,92746299018
METHOD BLANK: 4502878 Matrix: Water
Associated Lab Samples: 92746299004,92746299007,92746299011,92746299018
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,2,4-Trichlorobenzene ug/L ND 5.0 08/08/24 12:20
1,2-Dichlorobenzene ug/L ND 5.0 08/08/24 12:20
1,3-Dichlorobenzene ug/L ND 5.0 08/08/24 12:20
1,4-Dichlorobenzene ug/L ND 5.0 08/08/24 12:20
2,2'-Oxybis(1-chloropropane) ug/L ND 5.0 08/08/24 12:20
2,4,6-Trichlorophenol ug/L ND 10.0 08/08/24 12:20
2,4-Dichlorophenol ug/L ND 5.0 08/08/24 12:20
2,4-Dimethylphenol ug/L ND 10.0 08/08/24 12:20
2,4-Dinitrophenol ug/L ND 50.0 08/08/24 12:20
2,4-Dinitrotoluene ug/L ND 5.0 08/08/24 12:20
2,6-Dinitrotoluene ug/L ND 5.0 08/08/24 12:20
2-Chloronaphthalene ug/L ND 5.0 08/08/24 12:20
2-Chlorophenol ug/L ND 5.0 08/08/24 12:20
2-Nitrophenol ug/L ND 5.0 08/08/24 12:20
3,3'-Dichlorobenzidine ug/L ND 10.0 08/08/24 12:20
4,6-Dinitro-2-m ethyl phenol ug/L ND 10.0 08/08/24 12:20
4-Bromophenylphenyl ether ug/L ND 5.0 08/08/24 12:20
4-ChIoro-3-m ethyl phenol ug/L ND 5.0 08/08/24 12:20
4-Chlorophenylphenyl ether ug/L ND 5.0 08/08/24 12:20
4-Nitrophenol ug/L ND 10.0 08/08/24 12:20
Acenaphthene ug/L ND 5.0 08/08/24 12:20
Acenaphthylene ug/L ND 5.0 08/08/24 12:20
Anthracene ug/L ND 5.0 08/08/24 12:20
Benzo(a)anthracene ug/L ND 5.0 08/08/24 12:20
Benzo(a)pyrene ug/L ND 5.0 08/08/24 12:20
Benzo(b)fluoranthene ug/L ND 5.0 08/08/24 12:20
Benzo(g,h,i)perylene ug/L ND 5.0 08/08/24 12:20
Benzo(k)fluoranthene ug/L ND 5.0 08/08/24 12:20
bis(2-Chloroethoxy)methane ug/L ND 10.0 08/08/24 12:20
bis(2-Chloroethyl)ether ug/L ND 5.0 08/08/24 12:20
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 08/08/24 12:20
Butylbenzylphthalate ug/L ND 5.0 08/08/24 12:20
Chrysene ug/L ND 5.0 08/08/24 12:20
Di-n-butylphthalate ug/L ND 5.0 08/08/24 12:20
Di-n-octylphthalate ug/L ND 5.0 08/08/24 12:20
Dibenz(a,h)anthracene ug/L ND 5.0 08/08/24 12:20
Diethylphthalate ug/L ND 5.0 08/08/24 12:20
Dimethylphthalate ug/L ND 5.0 08/08/24 12:20
Fluoranthene ug/L ND 5.0 08/08/24 12:20
Fluorene ug/L ND 5.0 08/08/24 12:20
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 64 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
METHOD BLANK: 4502878 Matrix: Water
Associated Lab Samples: 92746299004,92746299007,92746299011,92746299018
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Hexachloro-1,3-butadiene ug/L ND 5.0 08/08/24 12:20
Hexachlorobenzene ug/L ND 5.0 08/08/24 12:20
Hexachlorocyclopentadiene ug/L ND 10.0 08/08/24 12:20
Hexachloroethane ug/L ND 5.0 08/08/24 12:20
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 08/08/24 12:20
Isophorone ug/L ND 10.0 08/08/24 12:20
N-Nitroso-di-n-propylamine ug/L ND 5.0 08/08/24 12:20
N-Nitrosodimethylamine ug/L ND 5.0 08/08/24 12:20
N-Nitrosodiphenylamine ug/L ND 10.0 08/08/24 12:20
Naphthalene ug/L ND 5.0 08/08/24 12:20
Nitrobenzene ug/L ND 5.0 08/08/24 12:20
Pentachlorophenol ug/L ND 10.0 08/08/24 12:20
Phenanthrene ug/L ND 5.0 08/08/24 12:20
Phenol ug/L ND 5.0 08/08/24 12:20
Pyrene ug/L ND 5.0 08/08/24 12:20
2,4,6-Tribromophenol(S) % 83 10-137 08/08/24 12:20
2-Fluorobiphenyl(S) % 46 15-120 08/08/24 12:20
2-Fluorophenol(S) % 50 10-120 08/08/24 12:20
Nitrobenzene-d5(S) % 59 10-120 08/08/24 12:20
Phenol-d6(S) % 40 10-120 08/08/24 12:20
Terphenyl-d14(S) % 75 11-131 08/08/24 12:20
LABORATORY CONTROL SAMPLE: 4502879
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
1,2,4-Trichlorobenzene ug/L 50 33.2 66 44-142
1,2-Dichlorobenzene ug/L 50 31.5 63 32-129
1,3-Dichlorobenzene ug/L 50 30.8 62 1-172
1,4-Dichlorobenzene ug/L 50 31.0 62 20-124
2,2'-Oxybis(1-chloropropane) ug/L 50 50.9 102 36-166
2,4,6-Trichlorophenol ug/L 50 48.9 98 37-144
2,4-Dichlorophenol ug/L 50 44.5 89 1-191
2,4-Dimethylphenol ug/L 50 51.9 104 32-119
2,4-Dinitrophenol ug/L 250 304 122 1-181
2,4-Dinitrotoluene ug/L 50 52.3 105 39-139
2,6-Dinitrotoluene ug/L 50 49.5 99 50-158
2-Chloronaphthalene ug/L 50 41.4 83 60-118
2-Chlorophenol ug/L 50 43.0 86 23-134
2-Nitrophenol ug/L 50 49.4 99 29-182
3,3'-Dichlorobenzidine ug/L 100 100 100 1-262
4,6-Dinitro-2-m ethyl phenol ug/L 100 120 120 1-181
4-Bromophenylphenyl ether ug/L 50 50.5 101 53-127
4-Chloro-3-methylphenol ug/L 100 101 101 22-147
4-Chlorophenylphenyl ether ug/L 50 45.4 91 25-158
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 65 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
LABORATORY CONTROL SAMPLE: 4502879
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
4-Nitrophenol ug/L 250 162 65 1-132
Acenaphthene ug/L 50 44.6 89 47-145
Acenaphthylene ug/L 50 46.9 94 33-145
Anthracene ug/L 50 49.1 98 1-166
Benzo(a)anthracene ug/L 50 51.3 103 33-143
Benzo(a)pyrene ug/L 50 50.7 101 17-163
Benzo(b)fluoranthene ug/L 50 51.6 103 24-159
Benzo(g,h,i)perylene ug/L 50 53.4 107 1-219
Benzo(k)fluoranthene ug/L 50 49.6 99 11-162
bis(2-Chloroethoxy)methane ug/L 50 49.3 99 33-184
bis(2-Chloroethyl)ether ug/L 50 48.9 98 12-158
bis(2-Ethylhexyl)phthalate ug/L 50 54.0 108 8-158
Butylbenzylphthalate ug/L 50 57.5 115 1-152
Chrysene ug/L 50 48.9 98 17-168
Di-n-butylphthalate ug/L 50 50.4 101 1-118
Di-n-octylphthalate ug/L 50 57.5 115 4-146
Dibenz(a,h)anthracene ug/L 50 54.0 108 1-227
Diethylphthalate ug/L 50 48.1 96 1-114
Dimethylphthalate ug/L 50 48.8 98 1-112
Fluoranthene ug/L 50 48.3 97 26-137
Fluorene ug/L 50 46.3 93 59-121
Hexachloro-1,3-butadiene ug/L 50 31.1 62 24-116
Hexachlorobenzene ug/L 50 49.9 100 1-152
Hexachlorocyclopentadiene ug/L 50 36.5 73 25-150
Hexachloroethane ug/L 50 28.7 57 40-113
Indeno(1,2,3-cd)pyrene ug/L 50 52.2 104 1-171
Isophorone ug/L 50 49.6 99 21-196
N-Nitroso-di-n-propylamine ug/L 50 48.2 96 1-230
N-Nitrosodimethylamine ug/L 50 38.8 78 25-150
N-Nitrosodiphenylamine ug/L 50 48.6 97 25-150
Naphthalene ug/L 50 38.1 76 21-133
Nitrobenzene ug/L 50 44.9 90 35-180
Pentachlorophenol ug/L 100 117 117 14-176
Phenanthrene ug/L 50 49.1 98 54-120
Phenol ug/L 50 34.0 68 5-112
Pyrene ug/L 50 51.9 104 52-115
2,4,6-Tribromophenol(S) % 123 10-137
2-Fluorobiphenyl(S) % 86 15-120
2-Fluorophenol(S) % 71 10-120
Nitrobenzene-d5(S) % 90 10-120
Phenol-d6(S) % 56 10-120
Terphenyl-d14(S) % 98 11-131
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 66 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4502880 4502881
MS MSD
35896202001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
1,2,4-Trichlorobenzene ug/L 1.71-1 100 100 41.1 39.9 41 40 44-142 3 M1
1,2-Dichlorobenzene ug/L 1.81-1 100 100 30.5 32.5 30 32 32-129 6 M1
1,3-Dichlorobenzene ug/L 1.61-1 100 100 26.0 28.6 26 29 1-172 9
1,4-Dichlorobenzene ug/L 1.71-1 100 100 27.4 30.4 27 30 20-124 10
2,2'-Oxybis(1-chloropropane) ug/L 1.21-1 100 100 84.6 75.2 85 75 36-166 12
2,4,6-TrichIorophenol ug/L 1.61-1 100 100 102 6.6J 102 7 37-144 M1
2,4-DichIorophenol ug/L 3.1J 100 100 118 31.5 115 28 1-191 116 R1
2,4-Dimethylphenol ug/L 1.71-1 100 100 100 84.1 100 84 32-119 18
2,4-Dinitrophenol ug/L 26.01-1 500 500 643 ND 129 1 1-181
2,4-Dinitrotoluene ug/L 1.61-1 100 100 115 93.6 115 94 39-139 20
2,6-Dinitrotoluene ug/L 1.71-1 100 100 112 96.0 112 96 50-158 15
2-Chloronaphthalene ug/L 1.71-1 100 100 81.9 74.6 82 75 60-118 9
2-Chlorophenol ug/L 1.21-1 100 100 86.0 24.6 86 25 23-134 111 R1
2-Nitrophenol ug/L 1.4U 100 100 104 20.0 104 20 29-182 135 M1,R1
3,3'-Dichlorobenzidine ug/L 8.1U 200 200 155 177 77 89 1-262 14
4,6-Dinitro-2-m ethyl phenol ug/L 7.81-1 200 200 236 ND 118 6 1-181
4-Bromophenylphenyl ether ug/L 1.81-1 100 100 99.0 87.2 99 87 53-127 13
4-Chloro-3-methylphenol ug/L 3.31-1 200 200 193 135 97 68 22-147 35 R1
4-Chlorophenylphenyl ether ug/L 2.01-1 100 100 94.4 83.1 94 83 25-158 13
4-Nitrophenol ug/L 6.61-1 500 500 328 ND 66 0 1-132 M1
Acenaphthene ug/L 2.01-1 100 100 88.6 79.4 89 79 47-145 11
Acenaphthylene ug/L 2.01-1 100 100 92.8 82.5 93 82 33-145 12
Anthracene ug/L 2.31-1 100 100 97.2 85.2 97 85 1-166 13
Benzo(a)anthracene ug/L 2.71-1 100 100 99.5 86.0 99 86 33-143 15
Benzo(a)pyrene ug/L 2.81-1 100 100 102 86.7 102 87 17-163 16
Benzo(b)fluoranthene ug/L 2.61-1 100 100 99.2 84.3 99 84 24-159 16
Benzo(g,h,i)perylene ug/L 2.81-1 100 100 102 89.0 102 89 1-219 14
Benzo(k)fluoranthene ug/L 2.71-1 100 100 101 85.7 101 86 11-162 16
bis(2-Chloroethoxy)methane ug/L 1.81-1 100 100 95.9 82.8 96 83 33-184 15
bis(2-Chloroethyl)ether ug/L 1.91-1 100 100 90.5 78.3 91 78 12-158 14
bis(2-Ethylhexyl)phthalate ug/L 3.71-1 100 100 96.4 82.5 96 82 8-158 16
Butylbenzylphthalate ug/L 3.1U 100 100 99.4 83.7 99 84 1-152 17
Chrysene ug/L 2.81-1 100 100 97.5 83.2 98 83 17-168 16
Di-n-butylphthalate ug/L 2.21-1 100 100 101 88.8 101 89 1-118 12
Di-n-octylphthalate ug/L 3.91-1 100 100 105 89.6 105 90 4-146 16
Dibenz(a,h)anthracene ug/L 3.01-1 100 100 103 88.8 103 89 1-227 15
Diethylphthalate ug/L 2.01-1 100 100 99.9 86.7 100 87 1-114 14
Dimethylphthalate ug/L 2.1U 100 100 97.5 84.5 98 85 1-112 14
Fluoranthene ug/L 2.21-1 100 100 100 88.1 100 88 26-137 13
Fluorene ug/L 2.1U 100 100 94.5 83.3 94 83 59-121 13
Hexachloro-1,3-butadiene ug/L 1.81-1 100 100 24.9 27.8 25 28 24-116 11
Hexachlorobenzene ug/L 2.21-1 100 100 100 85.7 100 86 1-152 16
Hexachlorocyclopentadiene ug/L 1.61-1 100 100 53.5 46.6 54 47 25-150 14
Hexachloroethane ug/L 1.4U 100 100 17.7 21.4 18 21 40-113 19 M1
Indeno(1,2,3-cd)pyrene ug/L 2.91-1 100 100 101 86.2 101 86 1-171 16
Isophorone ug/L 1.71-1 100 100 104 90.0 104 90 21-196 14
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 67 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4502880 4502881
MS MSD
35896202001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
N-Nitroso-di-n-propylamine ug/L 1.31-1 100 100 95.8 84.5 96 84 1-230 13
N-Nitrosodimethylamine ug/L 1.91-1 100 100 79.5 70.0 80 70 25-150 13
N-Nitrosodiphenylamine ug/L 3.01-1 100 100 95.3 82.7 95 83 25-150 14
Naphthalene ug/L 2.1U 100 100 57.8 54.2 58 54 21-133 6
Nitrobenzene ug/L 1.91-1 100 100 96.9 85.0 97 85 35-180 13
Pentachlorophenol ug/L 3.81-1 200 200 222 ND 111 3 14-176 M1
Phenanthrene ug/L 2.01-1 100 100 95.6 83.7 96 84 54-120 13
Phenol ug/L 1.4U 100 100 60.4 29.6 60 30 5-112 69 R1
Pyrene ug/L 2.21-1 100 100 94.3 79.9 94 80 52-115 17
2,4,6-Tribromophenol(S) % 125 15 10-137
2-Fluorobiphenyl(S) % 82 75 15-120
2-Fluorophenol(S) % 69 8 10-120 SO
Nitrobenzene-d5(S) % 102 89 10-120
Phenol-d6(S) % 54 23 10-120
Terphenyl-d14(S) % 96 82 11-131
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 68 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 874394 Analysis Method: SW-846
QC Batch Method: SW-846 Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services-Charlotte
Associated Lab Samples: 92746299019
SAMPLE DUPLICATE: 4504589
92745926003 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 5.0 5.0 1 N2
SAMPLE DUPLICATE: 4504590
92746369001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 97.3 97.3 0 N2
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 69 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 877946 Analysis Method: SW-846
QC Batch Method: SW-846 Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services-Charlotte
Associated Lab Samples: 92746299020
SAMPLE DUPLICATE: 4522371
92748858001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 21.2 23.4 10 N2
SAMPLE DUPLICATE: 4522372
92749311007 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 97.2 97.4 0 N2
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 70 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 2344553 Analysis Method: EPA 1664B
QC Batch Method: 1664A Analysis Description: Wet Chemistry 1664E
Laboratory: Pace National-Mt.Juliet
Associated Lab Samples: 92746299004,92746299008
METHOD BLANK: R4108426-1 Matrix: Water
Associated Lab Samples: 92746299004,92746299008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L ND 5.00 08/19/24 06:43
LABORATORY CONTROL SAMPLE&LCSD: R4108426-2 R4108426-3
Spike LCS LCSD LCS LCSD %Rec Max
Parameter Units Conc. Result Result %Rec %Rec Limits RPD RPD Qualifiers
Oil and Grease mg/L 40.0 37.4 36.5 93.5 91.3 78.0-114 2.44 20
MATRIX SPIKE SAMPLE: R4108426-4
L1767324-01 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Oil and Grease mg/L ND 40.0 27.5 68.7 78.0-114 ML
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 71 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 2345741 Analysis Method: EPA 1664B
QC Batch Method: 1664A Analysis Description: Wet Chemistry 1664E
Laboratory: Pace National-Mt.Juliet
Associated Lab Samples: 92746299004,92746299008
METHOD BLANK: R4108519-1 Matrix: Water
Associated Lab Samples: 92746299004,92746299008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Petroleum Hydrocarbons mg/L ND 5.00 08/19/24 10:37
LABORATORY CONTROL SAMPLE&LCSD: R4108519-2 R4108519-3
Spike LCS LCSD LCS LCSD %Rec Max
Parameter Units Conc. Result Result %Rec %Rec Limits RPD RPD Qualifiers
Total Petroleum Hydrocarbons mg/L 20.0 18.5 17.6 92.5 88.0 64.0-132 4.99 34
MATRIX SPIKE SAMPLE: R4108519-4
L1767324-01 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Total Petroleum Hydrocarbons mg/L ND 40.0 27.5 68.7 64.0-132
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 72 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 875150 Analysis Method: EPA 160.4/SM2540B-2011
QC Batch Method: EPA 160.4/SM2540B-2011 Analysis Description: 160.4 Total Volatile Solids
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92746299019
SAMPLE DUPLICATE: 4507986
92746299019 Dup
Parameter Units Result Result RPD Qualifiers
Total Volatile Solids mg/kg 779000 778000 0
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 73 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 875151 Analysis Method: EPA 160.4/SM2540B-2015
QC Batch Method: EPA 160.4/SM2540B-2015 Analysis Description: 160.4 TVS and 2540E TS
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92746299015
METHOD BLANK: 4507987 Matrix: Water
Associated Lab Samples: 92746299015
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Solids mg/L ND 25.0 08/13/24 18:54
LABORATORY CONTROL SAMPLE: 4507988
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Total Solids mg/L 500 546 109 90-110
SAMPLE DUPLICATE: 4507989
92746299015 Dup
Parameter Units Result Result RPD Qualifiers
Total Solids mg/L 5570 6090 9
Total Volatile Solids mg/L 4220 4690 11
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 74 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 874483 Analysis Method: SM 2320B-2011
QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92746299003,92746299007
METHOD BLANK: 4505018 Matrix: Water
Associated Lab Samples: 92746299003,92746299007
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Alkalinity,Total as CaCO3 mg/L ND 5.0 08/09/24 12:50
LABORATORY CONTROL SAMPLE: 4505019
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Alkalinity,Total as CaCO3 mg/L 50 52.8 106 80-120
LABORATORY CONTROL SAMPLE: 4505020
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Alkalinity,Total as CaCO3 mg/L 50 53.3 107 80-120
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4505021 4505022
MS MSD
92746636001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Alkalinity,Total as CaCO3 mg/L 28.3 50 50 76.7 77.9 97 99 80-120 1
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4505023 4505024
MS MSD
92746636002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Alkalinity,Total as CaCO3 mg/L 29.7 50 50 79.9 78.8 100 98 80-120 1
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 75 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 874714 Analysis Method: SM 2540C-2015
QC Batch Method: SM 2540C-2015 Analysis Description: 2540C Total Dissolved Solids
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92746299003,92746299007
METHOD BLANK: 4506205 Matrix: Water
Associated Lab Samples: 92746299003,92746299007
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Dissolved Solids mg/L ND 25.0 08/13/24 11:50
LABORATORY CONTROL SAMPLE: 4506206
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Total Dissolved Solids mg/L 250 256 102 90-110
SAMPLE DUPLICATE: 4506208
92746245001 Dup
Parameter Units Result Result RPD Qualifiers
Total Dissolved Solids mg/L 40.0 41.0 2
SAMPLE DUPLICATE: 4506209
92746223001 Dup
Parameter Units Result Result RPD Qualifiers
Total Dissolved Solids mg/L 92.0 88.0 4
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 76 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 874181 Analysis Method: EPA 160.4/SM2540B-2015
QC Batch Method: EPA 160.4/SM2540B-2015 Analysis Description: 2540D TSS/TVSS
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92746299017,92746299022,92746299024
METHOD BLANK: 4503289 Matrix: Water
Associated Lab Samples: 92746299017,92746299022,92746299024
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 08/09/24 13:36
LABORATORY CONTROL SAMPLE: 4503290
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Total Suspended Solids mg/L 250 246 98 90-110
SAMPLE DUPLICATE: 4505658
92745810002 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 6720 6620 1
Volatile Suspended Solids mg/L 4120 4050 2
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 77 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 875319 Analysis Method: EPA 160.4/SM2540B-2015
QC Batch Method: EPA 160.4/SM2540B-2015 Analysis Description: 2540D TSS/TVSS
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92746299011,92746299013
METHOD BLANK: 4508922 Matrix: Water
Associated Lab Samples: 92746299011,92746299013
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 08/13/24 21:27
LABORATORY CONTROL SAMPLE: 4508923
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Total Suspended Solids mg/L 250 270 108 90-110
SAMPLE DUPLICATE: 4509464
92746299011 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 3340 3480 4
Volatile Suspended Solids mg/L 2760 2850 3
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 78 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 874445 Analysis Method: SM 2540D-2015
QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92746299003,92746299007,92746299009
METHOD BLANK: 4504943 Matrix: Water
Associated Lab Samples: 92746299003,92746299007,92746299009
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 08/09/24 13:10
LABORATORY CONTROL SAMPLE: 4504944
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Total Suspended Solids mg/L 250 252 101 90-110
SAMPLE DUPLICATE: 4505599
92746416001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 258 274 6
SAMPLE DUPLICATE: 4505600
92746042001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 42.7 49.5 15
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 79 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 874715 Analysis Method: SM 2540D-2015
QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92746299021
METHOD BLANK: 4506218 Matrix: Water
Associated Lab Samples: 92746299021
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 08/11/24 13:40
LABORATORY CONTROL SAMPLE: 4506219
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Total Suspended Solids mg/L 250 240 96 90-110
SAMPLE DUPLICATE: 4506676
92746736001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 120 110 9
SAMPLE DUPLICATE: 4506677
92746332001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 1170 1180 1
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 80 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 874215 Analysis Method: SM 521 OB-2016
QC Batch Method: SM 521OB-2016 Analysis Description: 5210E cASC,5 day Final
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92746299003,92746299007,92746299009,92746299017,92746299021
METHOD BLANK: 4503477 Matrix: Water
Associated Lab Samples: 92746299003,92746299007,92746299009,92746299017,92746299021
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Carbonaceous BOD,5 day mg/L ND 2.0 08/13/24 15:40
LABORATORY CONTROL SAMPLE: 4503479
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Carbonaceous BOD,5 day mg/L 198 211 106 84.6-115
SAMPLE DUPLICATE: 4503480
92746299021 Dup
Parameter Units Result Result RPD Qualifiers
Carbonaceous BOD,5 day mg/L 3.5 3.5 1
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 81 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 874070 Analysis Method: EPA 300.0 Rev 2.1 1993
QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92746299003,92746299007,92746299011,92746299017
METHOD BLANK: 4502882 Matrix: Water
Associated Lab Samples: 92746299003,92746299007,92746299011,92746299017
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chloride mg/L ND 1.0 08/07/24 19:32
Nitrate as N mg/L ND 0.10 08/07/24 19:32
Nitrate-Nitrite(as N) mg/L ND 0.20 08/07/24 19:32
Nitrite as N mg/L ND 0.10 08/07/24 19:32
LABORATORY CONTROL SAMPLE: 4502883
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Chloride mg/L 50 51.9 104 90-110
Nitrate as N mg/L 2.5 2.5 100 90-110
Nitrate-Nitrite(as N) mg/L 5 5.2 103 90-110
Nitrite as N mg/L 2.5 2.7 106 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4502884 4502885
MS MSD
92746299017 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Chloride mg/L 44.8 50 50 92.8 96.2 96 103 90-110 4
Nitrate as N mg/L 0.44 2.5 2.5 2.9 3.1 100 108 90-110 6
Nitrate-Nitrite(as N) mg/L 0.44 5 5 5.0 5.4 92 99 90-110 6
Nitrite as N mg/L ND 2.5 2.5 2.1 2.2 82 87 90-110 6 M1
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 82 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 876972 Analysis Method: EPA 350.1 Rev 2.0 1993
QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92746299003,92746299007,92746299009,92746299011,92746299013,92746299017,92746299021
METHOD BLANK: 4517239 Matrix: Water
Associated Lab Samples: 92746299003,92746299007,92746299009,92746299011,92746299013,92746299017,92746299021
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen,Ammonia mg/L ND 0.10 08/21/24 15:42
LABORATORY CONTROL SAMPLE: 4517240
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Nitrogen,Ammonia mg/L 5 5.1 101 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4517241 4517242
MS MSD
92747947001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Nitrogen,Ammonia mg/L ND 5 5 4.9 4.9 97 97 90-110 0
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4517243 4517244
MS MSD
92747948002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Nitrogen,Ammonia mg/L 0.39 5 5 5.5 5.5 102 102 90-110 0
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 83 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 877196 Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92746299019
METHOD BLANK: 4518114 Matrix: Solid
Associated Lab Samples: 92746299019
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Kjeldahl,Total mg/kg ND 50.0 08/22/24 08:14
LABORATORY CONTROL SAMPLE: 4518115
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Nitrogen, Kjeldahl,Total mg/kg 1000 1080 108 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4518116 4518117
MS MSD
92746351001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Nitrogen, Kjeldahl,Total mg/kg 262 1130 1080 1530 1420 112 107 90-110 8 M1
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 84 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 878258 Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92746299003,92746299007,92746299009,92746299011,92746299015,92746299017,92746299021
METHOD BLANK: 4523605 Matrix: Water
Associated Lab Samples: 92746299003,92746299007,92746299009,92746299011,92746299015,92746299017,92746299021
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Kjeldahl,Total mg/L ND 0.50 08/27/24 09:01
LABORATORY CONTROL SAMPLE: 4523606
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Nitrogen, Kjeldahl,Total mg/L 10 10.5 105 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4523607 4523608
MS MSD
92746299003 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Nitrogen, Kjeldahl,Total mg/L 49.5 10 10 66.2 58.2 167 86 90-110 13 M1,R1
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4523609 4523610
MS MSD
92746299007 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Nitrogen, Kjeldahl,Total mg/L 1.5 10 10 13.1 13.8 116 123 90-110 5 M1
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 85 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 874090 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate+Nitrite
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92746299019
METHOD BLANK: 4503069 Matrix: Solid
Associated Lab Samples: 92746299019
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Nitrate mg/kg ND 4.0 08/08/24 01:54
Nitrogen, Nitrite mg/kg ND 4.0 08/08/24 01:54
Nitrogen, NO2 plus NO3 mg/kg ND 4.0 08/08/24 01:54
LABORATORY CONTROL SAMPLE: 4503070
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Nitrogen, Nitrate mg/kg 15 15.6 104 90-110
Nitrogen, Nitrite mg/kg 10 10.3 103 90-110
Nitrogen, NO2 plus NO3 mg/kg 25 25.9 104 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4503071 4503072
MS MSD
92746369001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Nitrogen, Nitrate mg/kg ND 548 541 564 534 103 99 90-110 5
Nitrogen, Nitrite mg/kg ND 363 359 383 365 105 102 90-110 5
Nitrogen, NO2 plus NO3 mg/kg ND 911 900 947 899 103 100 90-110 5
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 86 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 877081 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate+Nitrite,preserved
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92746299009,92746299015,92746299021
METHOD BLANK: 4517733 Matrix: Water
Associated Lab Samples: 92746299009,92746299015,92746299021
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, NO2 plus NO3 mg/L ND 0.040 08/22/24 03:27
LABORATORY CONTROL SAMPLE: 4517734
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Nitrogen, NO2 plus NO3 mg/L 2.5 2.6 103 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4517735 4517736
MS MSD
92747195002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Nitrogen, NO2 plus NO3 mg/L 0.35 2.5 2.5 2.8 2.8 98 97 90-110 1
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4517737 4517738
MS MSD
92747794001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Nitrogen, NO2 plus NO3 mg/L 0.38 2.5 2.5 2.9 2.9 102 102 90-110 0
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 87 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 875011 Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus,Total
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92746299019
METHOD BLANK: 4507179 Matrix: Solid
Associated Lab Samples: 92746299019
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phosphorus mg/kg ND 1.0 08/13/2418:54
LABORATORY CONTROL SAMPLE: 4507180
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Phosphorus mg/kg 50 50.5 101 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4507181 4507182
MS MSD
92746020001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Phosphorus mg/kg 140 67.8 66.4 167 223 40 124 90-110 28 M1,R1
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 88 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 877442 Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus,Total
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92746299003,92746299007,92746299009,92746299011,92746299013,92746299015,92746299017,
92746299021
METHOD BLANK: 4519659 Matrix: Water
Associated Lab Samples: 92746299003,92746299007,92746299009,92746299011,92746299013,92746299015,92746299017,
92746299021
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phosphorus mg/L ND 0.050 08/23/2410:42
LABORATORY CONTROL SAMPLE: 4519660
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Phosphorus mg/L 2.5 2.5 98 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4519661 4519662
MS MSD
92748456001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Phosphorus mg/L ND 2.5 2.5 2.5 2.4 98 96 90-110 2
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4519663 4519664
MS MSD
92748456002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Phosphorus mg/L ND 2.5 2.5 2.4 2.4 95 96 90-110 1
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 89 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 877812 Analysis Method: EPA 420.4 Rev 1.0 1993
QC Batch Method: EPA 420.4 Rev 1.0 1993 Analysis Description: 420.4 Phenolics
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92746299003,92746299007
METHOD BLANK: 4521561 Matrix: Water
Associated Lab Samples: 92746299003,92746299007
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phenolics,Total Recoverable mg/L ND 0.0050 08/24/24 15:19
LABORATORY CONTROL SAMPLE: 4521562
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Phenolics,Total Recoverable mg/L 0.05 0.052 104 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4521563 4521564
MS MSD
92746299003 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Phenolics,Total Recoverable mg/L 0.038 0.05 0.05 0.092 0.094 108 113 90-110 3 M1
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4521565 4521566
MS MSD
92746299007 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Phenolics,Total Recoverable mg/L ND 0.05 0.05 0.060 0.059 110 108 90-110 1
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 875274 Analysis Method: SM 4500-CN-E-2016
QC Batch Method: SM 4500-CN-E-2016 Analysis Description: 450OCNE Cyanide,Total
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92746299020
METHOD BLANK: 4508597 Matrix: Solid
Associated Lab Samples: 92746299020
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Cyanide mg/kg ND 0.22 08/15/2410:58
LABORATORY CONTROL SAMPLE: 4508598
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Cyanide mg/kg 2.6 2.6 102 80-120
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4508599 4508600
MS MSD
92745383001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Cyanide mg/kg ND 3 3.3 3.0 3.1 98 94 80-120 5
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 91 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 876557 Analysis Method: SM 4500-CN-E-2016
QC Batch Method: SM 4500-CN-E-2016 Analysis Description: 450OCNE Cyanide,Total
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92746299004,92746299008,92746299010,92746299012,92746299014,92746299016,92746299018,
92746299021,92746299023,92746299025
METHOD BLANK: 4515135 Matrix: Water
Associated Lab Samples: 92746299004,92746299008,92746299010,92746299012,92746299014,92746299016,92746299018,
92746299021,92746299023,92746299025
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Cyanide mg/L ND 0.0080 08/20/2411:16
LABORATORY CONTROL SAMPLE: 4515136
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Cyanide mg/L 0.1 0.10 104 80-120
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4515137 4515138
MS MSD
92746735001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Cyanide mg/L ND 0.1 0.1 ND ND -1 0 80-120 M1
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4515139 4515140
MS MSD
92746027001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Cyanide mg/L ND 0.1 0.1 ND ND 1 1 80-120 M1
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 92 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
QC Batch: 878419 Analysis Method: SM 5220D-2011
QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92746299003,92746299007,92746299009,92746299013,92746299017,92746299021
METHOD BLANK: 4524505 Matrix: Water
Associated Lab Samples: 92746299003,92746299007,92746299009,92746299013,92746299017,92746299021
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chemical Oxygen Demand mg/L ND 25.0 08/27/24 15:28
LABORATORY CONTROL SAMPLE: 4524506
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 750 743 99 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4524507 4524508
MS MSD
92746299007 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Chemical Oxygen Demand mg/L ND 100 100 108 115 104 110 90-110 6 R1
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4524509 4524510
MS MSD
92748569003 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 26.9 100 100 126 126 99 99 90-110 0
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 93 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALIFIERS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
DEFINITIONS
DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot.
ND-Not Detected at or above adjusted reporting limit.
TNTC-Too Numerous To Count
J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL-Practical Quantitation Limit.
RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S-Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is
a combined concentration.
Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values.
LCS(D)-Laboratory Control Sample(Duplicate)
MS(D)-Matrix Spike(Duplicate)
DUP-Sample Duplicate
RPD-Relative Percent Difference
NC-Not Calculable.
SG-Silica Gel-Clean-Up
U-Indicates the compound was analyzed for,but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as
"Total"may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
SAMPLE QUALIFIERS
Sample:92746299008
Ill Wet Chemistry by Method 1664B-Total Oil&Grease is non-detect. Extract was not processed through silica gel.
Sample: L1767324-01
Ill Wet Chemistry by Method 1664B-Total Oil&Grease is non-detect. Extract was not processed through silica gel.
ANALYTE QUALIFIERS
D3 Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.
L1 Analyte recovery in the laboratory control sample(LCS)was above QC limits. Results for this analyte in associated
samples may be biased high.
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample(LCS)recovery.
ML Matrix spike recovery and/or matrix spike duplicate recovery was below laboratory control limits.Result may be biased
low.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply.A
complete list of accreditations/certifications is available upon request.
R1 RPD value was outside control limits.
SO Surrogate recovery outside laboratory control limits.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALIFIERS
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
ANALYTE QUALIFIERS
S4 Surrogate recovery not evaluated against control limits due to sample dilution.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92746299003 UC12-INF EPA 608.3 874068 EPA 608.3 874161
92746299007 UC12-EFF EPA 608.3 874558 EPA 608.3 874980
92746299011 UC12-MLSS EPA 608.3 874558 EPA 608.3 874980
92746299018 UC12-INFDIST EPA 608.3 874558 EPA 608.3 874980
92746299019 UC12-BFP-1-CAKE EPA 7471 B 875058 EPA 7471 B 875147
92746299003 UC12-INF EPA 200.7 Rev 4.4 1994 875840 EPA 200.7 Rev 4.4 1994 875992
92746299007 UC12-EFF EPA 200.7 Rev 4.4 1994 875840 EPA 200.7 Rev 4.4 1994 875992
92746299019 UC12-BFP-1-CAKE EPA3050B 875260 EPA6010D 875409
92746299003 UC12-INF EPA 200.8 Rev 5.4 1994 874203 EPA 200.8 Rev 5.4 1994 874343
92746299007 UC12-EFF EPA 200.8 Rev 5.4 1994 874647 EPA 200.8 Rev 5.4 1994 874806
92746299009 UC12-FCE EPA 200.8 Rev 5.4 1994 874279 EPA 200.8 Rev 5.4 1994 874411
92746299011 UC12-MLSS EPA 200.8 Rev 5.4 1994 874279 EPA 200.8 Rev 5.4 1994 874411
92746299013 UC12-RAS EPA 200.8 Rev 5.4 1994 874279 EPA 200.8 Rev 5.4 1994 874411
92746299015 UC12-WAS EPA 200.8 Rev 5.4 1994 874279 EPA 200.8 Rev 5.4 1994 874411
92746299017 UC12-INFDIST EPA 200.8 Rev 5.4 1994 874279 EPA 200.8 Rev 5.4 1994 874411
92746299021 UC12-BFP-1-FILT EPA 200.8 Rev 5.4 1994 874279 EPA 200.8 Rev 5.4 1994 874411
92746299022 UC12-1 2 AER EPA 200.8 Rev 5.4 1994 874279 EPA 200.8 Rev 5.4 1994 874411
92746299024 UC12-5 6 AER EPA 200.8 Rev 5.4 1994 874279 EPA 200.8 Rev 5.4 1994 874411
92746299009 UC12-FCE EPA 245.1 Rev 3.0 1994 874602 EPA 245.1 Rev 3.0 1994 874717
92746299011 UC12-MLSS EPA 245.1 Rev 3.01994 874602 EPA 245.1 Rev 3.01994 874717
92746299013 UC12-RAS EPA 245.1 Rev 3.0 1994 874602 EPA 245.1 Rev 3.0 1994 874717
92746299015 UC12-WAS EPA 245.1 Rev 3.0 1994 874602 EPA 245.1 Rev 3.0 1994 874717
92746299017 UC12-INFDIST EPA 245.1 Rev 3.01994 874602 EPA 245.1 Rev 3.01994 874717
92746299021 UC12-BFP-1-FILT EPA 245.1 Rev 3.01994 874602 EPA 245.1 Rev 3.01994 874717
92746299022 UC12-1 2 AER EPA 245.1 Rev 3.0 1994 874602 EPA 245.1 Rev 3.0 1994 874717
92746299024 UC12-5 6 AER EPA 245.1 Rev 3.0 1994 874602 EPA 245.1 Rev 3.0 1994 874717
92746299004 UC12-INF EPA625.1 874069 EPA625.1 874165
92746299007 UC12-EFF EPA625.1 874069 EPA625.1 874165
92746299011 UC12-MLSS EPA625.1 874069 EPA625.1 874165
92746299018 UC12-INFDIST EPA625.1 874069 EPA625.1 874165
92746299004 UC12-INF EPA624.1 874338
92746299008 UC12-EFF EPA624.1 874338
92746299012 UC12-MLSS EPA624.1 874338
92746299018 UC12-INFDIST EPA624.1 874338
92746299019 UC12-BFP-1-CAKE SM 2540G-2011 875019
92746299019 UC12-BFP-1-CAKE SW-846 874394
92746299020 UC12-BFP-1-CAKE SW-846 877946
92746299004 UC12-INF 1664B 2344553 EPA 1664B 2344553
92746299004 UC12-INF 1664E 2345741 EPA 1664B 2345741
92746299008 UC12-EFF 1664B 2344553 EPA 1664B 2344553
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92746299008 UC12-EFF 1664B 2345741 EPA1664B 2345741
92746299019 UC12-BFP-1-CAKE EPA 160.4/SM2540B- 875150
2011
92746299015 UC12-WAS EPA 160.4/SM2540B- 875151
2015
92746299003 UC12-INF SM 2320B-2011 874483
92746299007 UC12-EFF SM 2320B-2011 874483
92746299003 UC12-INF SM 2540C-2015 874714
92746299007 UC12-EFF SM 2540C-2015 874714
92746299003 UC12-INF SM 2540D-2015 874445
92746299007 UC12-EFF SM 2540D-2015 874445
92746299009 UC12-FCE SM 2540D-2015 874445
92746299021 UC12-BFP-1-FILT SM 2540D-2015 874715
92746299011 UC12-MLSS EPA 160.4/SM2540B- 875319
2015
92746299013 UC12-RAS EPA 160.4/SM2540B- 875319
2015
92746299017 UC12-INFDIST EPA 160.4/SM2540B- 874181
2015
92746299022 UC12-1 2 AER EPA 160.4/SM2540B- 874181
2015
92746299024 UC12-5_6 AER EPA 160.4/SM2540B- 874181
2015
92746299003 UC12-INF SM 5210B-2016 874215 SM 5210B-2016 874305
92746299007 UC12-EFF SM 5210B-2016 874215 SM 5210B-2016 874305
92746299009 UC12-FCE SM 5210B-2016 874215 SM 5210B-2016 874305
92746299017 UC12-INFDIST SM 5210B-2016 874215 SM 5210B-2016 874305
92746299021 UC12-BFP-1-FILT SM 5210B-2016 874215 SM 5210B-2016 874305
92746299003 UC12-INF EPA 300.0 Rev 2.1 1993 874070
92746299007 UC12-EFF EPA 300.0 Rev 2.1 1993 874070
92746299011 UC12-MLSS EPA 300.0 Rev 2.1 1993 874070
92746299017 UC12-INFDIST EPA 300.0 Rev 2.1 1993 874070
92746299003 UC12-INF EPA 350.1 Rev 2.0 1993 876972
92746299007 UC12-EFF EPA 350.1 Rev 2.0 1993 876972
92746299009 UC12-FCE EPA 350.1 Rev 2.0 1993 876972
92746299011 UC12-MLSS EPA 350.1 Rev 2.0 1993 876972
92746299013 UC12-RAS EPA 350.1 Rev 2.0 1993 876972
92746299017 UC12-INFDIST EPA 350.1 Rev 2.0 1993 876972
92746299021 UC12-BFP-1-FILT EPA 350.1 Rev 2.0 1993 876972
92746299019 UC12-BFP-1-CAKE EPA 351.2 Rev 2.0 1993 877196 EPA 351.2 Rev 2.0 1993 877406
92746299003 UC12-INF EPA 351.2 Rev 2.0 1993 878258 EPA 351.2 Rev 2.0 1993 878451
92746299007 UC12-EFF EPA 351.2 Rev 2.0 1993 878258 EPA 351.2 Rev 2.0 1993 878451
92746299009 UC12-FCE EPA 351.2 Rev 2.0 1993 878258 EPA 351.2 Rev 2.0 1993 878451
92746299011 UC12-MLSS EPA 351.2 Rev 2.0 1993 878258 EPA 351.2 Rev 2.0 1993 878451
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 97 of 133

Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: UC12-SEMI-AN&PPA-8/7-2024
Pace Project No.: 92746299
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92746299015 UC12-WAS EPA 351.2 Rev 2.0 1993 878258 EPA 351.2 Rev 2.0 1993 878451
92746299017 UC12-INFDIST EPA 351.2 Rev 2.0 1993 878258 EPA 351.2 Rev 2.0 1993 878451
92746299021 UC12-BFP-1-FILT EPA 351.2 Rev 2.0 1993 878258 EPA 351.2 Rev 2.0 1993 878451
92746299019 UC12-BFP-1-CAKE EPA 353.2 Rev 2.0 1993 874090 EPA 353.2 Rev 2.0 1993 874097
92746299009 UC12-FCE EPA 353.2 Rev 2.0 1993 877081
92746299015 UC12-WAS EPA 353.2 Rev 2.0 1993 877081
92746299021 UC12-BFP-1-FILT EPA 353.2 Rev 2.0 1993 877081
92746299019 UC12-BFP-1-CAKE EPA 365.1 Rev 2.0 1993 875011 EPA 365.1 Rev 2.0 1993 875265
92746299003 UC12-INF EPA 365.1 Rev 2.0 1993 877442 EPA 365.1 Rev 2.0 1993 877667
92746299007 UC12-EFF EPA 365.1 Rev 2.0 1993 877442 EPA 365.1 Rev 2.0 1993 877667
92746299009 UC12-FCE EPA 365.1 Rev 2.0 1993 877442 EPA 365.1 Rev 2.0 1993 877667
92746299011 UC12-MLSS EPA 365.1 Rev 2.0 1993 877442 EPA 365.1 Rev 2.0 1993 877667
92746299013 UC12-RAS EPA 365.1 Rev 2.0 1993 877442 EPA 365.1 Rev 2.0 1993 877667
92746299015 UC12-WAS EPA 365.1 Rev 2.0 1993 877442 EPA 365.1 Rev 2.0 1993 877667
92746299017 UC12-INFDIST EPA 365.1 Rev 2.0 1993 877442 EPA 365.1 Rev 2.0 1993 877667
92746299021 UC12-BFP-1-FILT EPA 365.1 Rev 2.0 1993 877442 EPA 365.1 Rev 2.0 1993 877667
92746299003 UC12-INF EPA 420.4 Rev 1.0 1993 877812 EPA 420.4 Rev 1.0 1993 878086
92746299007 UC12-EFF EPA 420.4 Rev 1.0 1993 877812 EPA 420.4 Rev 1.0 1993 878086
92746299020 UC12-BFP-1-CAKE SM 4500-CN-E-2016 875274 SM 4500-CN-E-2016 875665
92746299004 UC12-INF SM 4500-CN-E-2016 876557 SM 4500-CN-E-2016 876700
92746299008 UC12-EFF SM 4500-CN-E-2016 876557 SM 4500-CN-E-2016 876700
92746299010 UC12-FCE SM 4500-CN-E-2016 876557 SM 4500-CN-E-2016 876700
92746299012 UC12-MLSS SM 4500-CN-E-2016 876557 SM 4500-CN-E-2016 876700
92746299014 UC12-RAS SM 4500-CN-E-2016 876557 SM 4500-CN-E-2016 876700
92746299016 UC12-WAS SM 4500-CN-E-2016 876557 SM 4500-CN-E-2016 876700
92746299018 UC12-INFDIST SM 4500-CN-E-2016 876557 SM 4500-CN-E-2016 876700
92746299021 UC12-BFP-1-FILT SM 4500-CN-E-2016 876557 SM 4500-CN-E-2016 876700
92746299023 UC12-1 2 AER SM 4500-CN-E-2016 876557 SM 4500-CN-E-2016 876700
92746299025 UC12-5 6 AER SM 4500-CN-E-2016 876557 SM 4500-CN-E-2016 876700
92746299003 UC12-INF SM 5220D-2011 878419 SM 5220D-2011 878442
92746299007 UC12-EFF SM 5220D-2011 878419 SM 5220D-2011 878442
92746299009 UC12-FCE SM 5220D-2011 878419 SM 5220D-2011 878442
92746299013 UC12-RAS SM 5220D-2011 878419 SM 5220D-2011 878442
92746299017 UC12-INFDIST SM 5220D-2011 878419 SM 5220D-2011 878442
92746299021 UC12-BFP-1-FILT SM 5220D-2011 878419 SM 5220D-2011 878442
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:08/28/2024 09:55 AM without the written consent of Pace Analytical Services,LLC. Page 98 of 133

9800 Kincey Ave#100
COC#: IWI I VII'ff I I;I IU IIILIB IfI I4 I IbIIZ!JU
aCeHuntersville,INC 28078(704)875.9092 EVENT TYPE: UC12-SEMI-AN& -817/2024 Proj. Mgr.: Stephanie Knott North Carolina Wastewater Certification#:12 SEND REPORT TO: Keith Purgason ACttNum/Client ID: Samp�b (Sign N me):C 92746299
CLIENT: Union County Water 7 8299 Kensington Dr Table#:
FACILITY: Twelve Mile Creek WRF,NCO085359 I Waxhaw,NC 28173 Profile/Template: 16076 'Print Name:Clean Hands Dirty Hands
ADDRESS: 8299 Kensington Drive,Waxhaw,NC 28173 [e-mail] Prelogl Bottle Ord. ID EZ 3143106 ,; �Fir:� 1 f/ �ljL�
SampTi:Collectio­n_Dafa Sample Containe Preservative Analyses Requested
W
w
o cc O Z� o
CD N
a Q n = v o
SAMPLE ID °' Q) U } m m N m o w W o g o a � � � LAB USE ONLY
E m °' E m m . N `D o v o o LAB SAMPLE ID
Q O O 0 _ M X i W n O c�D U)
C C F- U T d N N N O O O (D N !L O 1A O O c" O Q �-
LU rn v o> co � a`� E u) N v v o n a c
:C -O C Q d _0 Q F- C cL to � In N I f/) LLl N M d U O Q N n. i � L � O >
m m lL W E O >. '� N (n � N N - Q fn O � I.L.1 F- N N O
E I— N c� Cn `L 6. p Vi N LU cnCD � to
a- n CL n. c- � a� -Q a �� U a> w c-� O = O � � � � � � .o C 0 � LLJ � CL = U7 �
E E E E E E E c — Z O cn O c� O o O cry cn U) M E m Z m m @ _ � o C� C! U w c
cn co Cn U) fn o F- U `° o :tto m Oz = _ ° = Z 0 m O cn > u7 > w Y E Y o dU a)5 J = t 0 0 O Of :�3 '
En 0 0
UC12-INF M 8/7/2024 N G GL 1 o X X vIL,
UC12-INF FIELD l
BLANK to 817/2024 N G GL 1 ,o X X
v�L
Comments: SHIPPED ON WET ICE Custody Seal Present: Custody Seal Number:
Sample Temp at Collection: INF: °C EFF: °C 200.8= Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,TI,Zn,Mo IIVi= LLHG SAMPLES YES 1 NO
Sample Type Codes: Relinq ' by(Si to Received by(S'gnatu ) Date; Time:
Sample Temp at Receiving in Lab: INF: °C EFF: °C � f
Q(Flow)=Automatic Flow Proportioned Sample G�
Sample Temp of EFF Fecal Sample at Receiving in Lab ,C o T(Time)=Automatic Time Proportioned Sample Reli� wished Si lna�r ./ e e' ed by(Signature: /—'Lj Date: Time:
(record only if collected): H(Hand)=Hand Composite Sample !7� -� / Yj I �t
Zero Headspace&Teflon septa for YES NO NIA 0 G(Grab)=Grab Sample Relinquished by(Signature): Received by(Signature): Date: Time:
VOAs: Container Type Codes:
Samples in Proper Containers: YES NO NIA m A=Amber Glass P=Plastic Relinquished by(Signature): Received by(Signature): Date: Time:
z GL=Clear Glass B=Bag
Chlorinated Samples De- YES NO NIA < TL=Teflon Lined Cap Relinquished by(Signature): Received by(Signature): Date: Time:
Chlorinated: VOA=40 ml Glass vial I qage 99 of 133

9800 Kincey Ave#100
ace Huntersville,NC 28078 704 875.9092 EVENT TYPE: UC12-SEMI-AN& -817/2024 COC#: PAGE of 1 5
( ) Proj. Mgr.: Stephanie Knott
North Carolina Wastewater Certification#:12 SEND REPORT TO: Keith Purgason AcUNum/Client ID: Sam
by,(Sign Name):
CLIENT: Union County Water 8299 Kensington Dr Table#: /�
FACILITY: Twelve Mile Creek WRF,NCO085359 Waxhaw,NC 28173 Profile/Template: 16076 rmt Name:
ADDRESS: 8299 Kensington Drive,Waxhaw,NC 28173 [e-mail] Prelogl Bottle Ord. ID EZ 3143106 , /t A-ti-;r" ))
Sample Collection Data "ample Containe Preservative Analyses Requested
cn
W
o H W U
o O Z o
3 o n z W U u�
} d o a vNO d v m C
wo
AB USE ONLY
SAMPLE ID m a) w
aNE nmE C-a n Ha U y m
2 (n L
co
ina
ca
LAB SAMPLE IDi 92 E M w M vm M x N o CO CO
Q 0 _
C
. 4)(n Od
L
04
C uy W U,m LLJW
CO Cl) LIJ N@ A Cn
O () , U
N N U) a) O co U) CO z LLJ -C a)n- ao o n ca U W h O n � 0 CD U W EE o n . E OoE E ° n c, O O m n c E a L ou .0
) ) ° 5 U W <n U i o m =
�j
0
0
It-
UC 4 8/7/2024 8/7/202 1 N Q P 1 o X X 0,93
UC12-INF 816/2024 dG q7 8/712024 8f7/2024 [ N Q P 1 o X X �203
UC12-INF �M 816/2024 0�q7 817/2024 Q 81712024 ob( I N Q P 1 X X 00�
UC12-INF VA 8/612024 Ob 8l7/2024 O&O� 8/7l2024 QG[1 N Q P 1 N X X U6
Comments: SHIPPED ON WET ICE Custody Seal Present: Custody Seal Number:
Sample Temp at Collection: INF: °C EFF: °C 200.8= Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,TI,Zn,Mo INF SEMI-ANNUAL SAMPLES YES /NO
Sample Type Codes: Relinquish d by(Signat UCW Rived by(Sinatur Dot : Time:
Sample Temp at Receiving in Lab: INF: °C EFF: °C
Q(Flow)=Automatic Flow Proportioned Sample "�� /i �l ��' ( �j
C',
Sample Temp of EFF Fecal Sample at Receiving in Lab oC o T(Time)=Automatic Time Proportioned Sample elinquished b�(Sigl Y: Rec ived by(Signature): Date: Time:
(record only if collected): H(Hand)=Hand Composite Sample l-
Zero Headspace&Teflon septa for YES NO NIA 0 G(Grab)=Grab Sample Relinquished by(Signature): Received by(Signature): Date: Time:
VOAs: < Container Type Codes:
En Samples in Proper Containers: YES NO NIA m A=Amber Glass P=Plastic Relinquished by(Signature): Received by(Signature): Date: Time:
z GL=Clear Glass B=Bag
Chlorinated Samples De- YES NO NIA TL=Teflon Lined Cap Relinquished by(Signature): Received by(Signature): Date: Time:
Chlorinated: VOA=40 ml Glass vial I I Pa e 100 of 133

9800 Kincey Ave#100
ace Huntersville,NC 28078 704 875.9092 EVENT TYPE: UG12-SEMI-AN& -8/7(2024 COC#: PAGE of 1
( ) Proj. Mgr.: Stephanie Knott
North Carolina Wastewater Certification#:12 SEND REPORT TO: Keith Purgason ActtNum/Client ID: Sam b Sign Nam Q):
CLIENT: Union County Water 71 8299 Kensington Dr Table#: r
FACILITY: Twelve Mile Creek WRF,NC0085359 Waxhaw,NC 28173 Profile/Template: 16076 Print Name:
ADDRESS: 8299 Kensington Drive,Waxhaw,NC 28173 [e-mail] Prelogl Bottle Ord. ID EZ 3143106 lj�✓t > rT� t
Sample Collection Data Sample Container Preservative Analyses Requested
U)
w
C F— W U
3 O z o
Z W U
d Z OO G <� CD N
O V — Q d V o
i, } o a m c� _ �+ v LAB USE ONLY
SAMPLE ID �, °' U m m v o ,� R w F- o F `D
cu E °' o ayEi � cn o mo 0 oo � C" X N w M r M v a to cn LAB SAMPLE ID
cn c m ~ U U 0 � e� cn c� o m 0 o � N Q O � �n � coo 0
N N O O CLZ Q L
C O d "O C n L]. �_ C N f/I u") N N N H N w C") d _0 O d N W ' 1 L N O O
m m w w E E °' F- ° N rn u = a o v N w c� in
Q7 N d N d (d co O O C Q (n .0 ,� '_ Z L N v1 O W C.7 (� N �_
fn C C O co V CV fn N C C W W a N O = Cn fD
E E E E E °� E E 12 c U z 0 U) 0 N O 0 U) cn c�i� E m Z s m a = a o (� C� U w E m �J(�
inCz rn cn in o i- U ° o o m Oz = = z S Z 00 ro O cn > cn > Y E Y o a J = r aS ozs 0 2 ( [�j 2l'1 1
o v
/A� �2- N G 0 3 v X X
UC12-INF 8/7/2024 N G A 2 F X X vac
UC12-INF 8/6/2024 d��7 8/7/2024 817/2024 N Q A 2 o X X �J3
UC12-INF 8/7/2024 0;11 N G A 2 a X X U0
UC12-INF 8/712024 C) �q N G A 2 o X X pJL�
UC12-INF 8/612024 oG�U� 8/7/2024 0( 0 8I7/2024 O4 11 N Q P 1 23 X X W�
UC12-INF V10A 8/6/2024 8/712024 Q 81712024 L N Q P 2 o X X
UC12-INF 8/7/2024 QSaz- N G P 1 N X X v0��
UC12-INF 81612024 817/2024 8/712024 N Q P 1 X X X X Uhl
UC12-INF u+r� 8/6/2024 ®��� 8/7/2024 C)(t0 8/7/2024 �� I N Q P 1 � X X X Ja?j
UC12-INF l 8/6/2024 Q��1 8/7/2024 (�o� 8(712024 Q� f N Q P 1 N X X X
Comments: SHIPPED ON WET ICE IM l'i'A J,'-1i�N`LC6 Custody Seal Present: Custody Seal Number:
Sample Temp at Collection: INF: °C EFF: °C 200.8= Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,TI,Zn,Mo NOX-48hour hold YES /NO
Sample Type Codes: Relinqui hed by i ure):UCW Received by(Si ature): Dale: Time:
Sample Temp at Receiving in Lab: INF: °C EFF: °C Q( ) p p /,= �� r-� � /
Flow =Automatic Flow Proportioned Sample
_ l
Sample Temp of EFF Fecal Sample at Receiving in Lab(record °C Co T(Time)=Automatic Time Proportioned Sample /I RelinQUished y(Siig nature�: / Rec ived by(Signature): y y j%7(}'y Date: Time:
only if collected): H(Hand)=Hand Composite Sample
Zero Headspace&Teflon septa for YES NO N/A 0 G(Grab)=Grab Sample Relinq is ed by(Signature): Received by(Signature): Date: Time:
VOAs: < Container Type Codes:
cn Samples in Proper Containers: YES NO NIA m A=Amber Glass P=Plastic Relinquished by(Signature): Received by(Signature): Date: Time:
z GL=Clear Glass B=Bag
Chlorinated Samples De- YES NO N/A TL=Teflon Lined Cap Relinquished by(Signature): Received by(Signature): Date: Time:
Chlorinated: VOA=40 ml Glass vial P ge 101 of 133

9800 Kincey Ave#100
�ace Huntersville,NC 28078(704)875.9092 EVENT TYPE: UC12-SEMI-AN& -81712024 Proj. Mgr.: Stephanie Knott
COC#: PAGE of
North Carolina Wastewater Certification#:12 SEND REPORT TO: Keith Purgason ACttNum/Client ID: Sam d y(Sign Name):Clean Handy Dirty Hap
HBa�fsT
CLIENT: Union County Water 8299 Kensington Dr Table#: 'r /f f�fj� / /..� �S_
FACILITY: Twelve Mile Creek WRF,NCO085359 Waxhaw,NC 28173 Profile/Template: 16076 Print Name:Clean Hands Dirty Ha ds
ADDRESS: 8299 Kensington Drive,Waxhaw,NC 28173 U [e-mail] Prelog/Bottle Ord. ID EZ 3143104 ji4 A1,11
Sample Collection Data Sample Container Preservative Analyses Requested
W
W U
O Z O
3 M z w r)
O O N
o z 3 (D a = o
SAMPLE ID °' �' d r m m N m CDW w o o a to v LAB USE ONLY
F E o cn o a 0 m M M x �„ `D W M o v v o cn LAB SAMPLE ID
C° 1- U V N o m ca o @ N Q O _ E cn O o M cOc O a
C (] d Q U N N O O lf") lC') O O O Q
LU cOJO M
� u-) N 04
n CD
c E N N U cz) ow in C14
UJ
M . 6l D r O d cN
pN
� Cn n CD n = n co
a n. o
ofl. O i[
E E E ) O n O [ c v7 o CD CD C� w c Z
) U � ° O o OZ O0O n n > Y E o CL :E O � 0n U W U ) m Z z m ZEJ = 0 a
�ti Z"7(f 1f/2lj
UC12-EFF 817/2024 3 N G GL 1 X X D /FFFIEID
BLANK 8/7/2024 /'��(�, N G GL 1 X X 001 _
Comments: SHIPPED ON WET ICE Custody Seal Present: Custody Seal Number:
Sample Temp at Collection: INF: °C EFF: °C 200.8= Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,TI,Zn,Mo EFF LLHG SAMPLES YES /NO
Sample Tvpe Codes: Relinq ' ed by 6e):U C W Received by(Signa re): Date: Time:
Sample Temp at Receiving in Lab: INF: °C EFF: °C
� Q(Flow)=Automatic Flow Proportioned Sample ,,.. L ji� r1 1. I I
Sample Temp of EFF Fecal Sample at Receiving in Lab(record ,C O T(Time)=Automatic Time Proportioned Sample Reli quishe by,SignaC re) Received by(Signature): r=i 7!i 1 Date: Time:
only if collected): H(Hand)=Hand Composite Sample � I � _" , �_//('/A
Zero Neadspace&Teflon septa for YES NO N/A G(Grab)=Grab Sample Relinquished by(Signature): Received by(Signature): Date: Time:
VOAs: Container Type Codes:
Samples in Proper Containers: YES NO NIA m A=Amber Glass P=Plastic Relinquished by(Signature): Received by(Signature): Date: Time:
z GL=Clear Glass B=Bag
Chlorinated Samples De- YES NO NIA TL=Teflon Lined Cap Relinquished by(Signature): Received by(Signature): Date: Time:
Chlorinated: VOA=40 ml Glass vial I I P ge 102 of 133

9800 Kincey Ave#100 I
Huntersville,NC 28078(704)875-9092 EVENT TYPE: UC12-SEMI-AN& -81712024 COC#: PAGE 5 of
��ace Proj. Mgr.: Stephanie Knott ;J
North Carolina Wastewater Certification#:12 SEND REPORT TO: Keith Purgason ActtNum/Client ID: Sampl y ign 1p;ne:
CLIENT: Union County Water 8299 Kensington Dr Table#:
FACILITY: Twelve Mile Creek WRF,NCO085359 Waxhaw,NC 28173 Profile/Template: 16076 P t Name:
_ ADDRESS: 8299 Kensington Drive,Waxhaw,NC 28173 \ [e-mail] Prelog/Bottle Ord. ID EZ 3143104 �1.�LT 666f
Sample Collection Data Sample Container Preservative Analyses Requested
cn
W
H W U
C cri O Z o
W
O C f) w = OCD
N
m o m w C, o � n LAB USE ONLY
SAMPLE ID _ °' °' M a) `" o �' o LAB SAMPLE ID
O E E a) U) O m m M c7 X N to w ch r` CD tD 2 to U)
N C M F U U >. fll rn N O O m (] O (D N Q O O vl t0 Ci c0 O �...
(U C 0 (U (n N d O E Lo u) N V at to O W Z ('�7 L -O O N (L L u-) 9 j
En _ "O Q O_ C ^2 LO lf) Lf) N I— fn N d U O Q L O
.0 CO W C E N_ VJ rL (/� T .� �- O O w W C7 1� N CN N O
m w E io n N W n
cn a� o w r> o o .� o z w a = U) to o
E E E E E °� a' E E U Z O O� O N O O M co U) co a�i @ E m Z a a3 ° 2 a _o O (7 > 2 > 7a
ca N A t9 to E L t9 O O O O Z N M U O CO O O co � co L -Y E = Y O U O J O L R'3 R'3 O
Cf) W In C0 W U H U m Z S 2 Z 2 Z co d CL J S OC
tiCt7£ff 3 c X — — —- X —
UC12-EFF �! 8f7/2024 �) N Q A 2 o X X JJ
UC12-EFF �� 8/6l2024 0703 81712024 0(o0 817/2024 INQ
A 2 o X X
UC12•EFF �� 8/712024 Q�j"P2(> A 2 o X X
UC12-EFF 8/7/2024 Q�) A 2 o X X
UC12-EFF /f(� 816/2024 0-70 81712024 6(,-5 81712024 COD P 1 X X u��
UC12•EFF 8/612024 ()7(,13 817/2024 �(}� 8/7/2024 0�/� P 2 o X XUC12-EFF 8,7/2024 0&1157 P 1 X X U�UC12-EFF 11IL 8/612024 0-1 8r7/2024 N12024 C)�� P 1 X X X X ValUC12-EFF f 8/612024 U7U3 8/712024 (PU' 817/2024 P 1 N X X X
UC12-EFF 'I!!(/ 81612024 G7G 8/712024 (,(dj�j 817/2024 0(0 N Q P 1 N X X X vJ�
Comments: SHIPPED ON WET ICE �f= tjf A 6Ai'jh Lc"j Custody Seal Present: Custody Seal Number:
Sample Temp at Collection: INF: °C EFF: - °C 200.8= Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,TI,Zn,Mo NOX-48hour hold YES I NO
Sample Type Codes: Rel�ii d by(S' atur Receive by(_Sigpp turgy / Date; Time:Sam Ie Tem at Receivin in Lab: INF' °C EFF: °C
p p g Q(Flow)=Automatic Flow Proportioned Sample �� � �x -/ 12 0
Sample Temp of EFF Fecal Sample at Receiving in Lab(record °C o T(Time)=Automatic Time Proportioned Sample Rel' quis ed by Pgnatufe):1.� Received by(Signature): 45 -�! Date: Time:
only if collected): H(Hand)=Hand Composite Sample �' l r Y
Zero Headspace&Teflon septa for YES NO NIA 0 G(Grab)=Grab Sample Relinquished by(Signature): Received by(Signature): Date: Time:
VOAs: < Container Type Codes:
c
Samples in Proper Containers: YES NO N/A o A=Amber Glass P=Plastic Relinquished by(Signature): Received by(Signature): Date: Time:
Z GL=Clear Glass B=Bag
Chlorinated Samples De YES NO N/A TL=Teflon Lined Cap Relinquished by(Signature): Received by(Signature): Date: TieChlorinated: VOA=40 ml Glass vialP03 of 133

r 9800 Kincey Ave#100
Huntersville,NC 28078 704 875-9092 EVENT TYPE: UC12-SEMI-AN& -81712024 COC#: PAGE I ' of 15
( ) Proj. Mgr.: Stephanie Knott U
North Carolina Wastewater Certification#:12 SEND REPORT TO: Keith Purgascn AcUNum/Client ID: Sampl (Sig Na e):
CLIENT: Union County Water 8299 Kensington Dr Table#: C
FACILITY: Twelve Mile Creek WRF,NCO085359 ® Waxhaw,NC 28173 Profile/Template: 16076 P nt Name:
ADDRESS: 8299 Kensington Drive,Waxhaw,NC 28173 [e-mail] Prelog/Bottle Ord. ID EZ 3143104 C_-Jw g-
Sample Collection Data 3ample Containe Preservative Analyses Requested
co
W
o .-- H W U
3 o o� O Z Z w U u-
V M O N
a�i —aoi m o a CL oo U = N
E .12
v LAB USE ONLY
SAMPLE ID a> m ac'i °' E CO a0 m v mo CD
w F oo
m a — o °' �? 0 00 m cc) M x ,,, w o v v cn LAB SAMPLE ID
N O Cn (U N O� O m 0 O N Q O N cn mi cD O M c�D � O 'O
C I— U U „y N N O O V n Z -a Q 'C to @ N
CM Ed n C tNf) t� N F— Cn LU N M C1 V O Q N n- , , V O >
C m m W w E @ 2 F- a`� m N CO U) U >. .O `- Ll O in N W v� W W C7 I� N cV
N d O (n Cn c N c (n 0 Cn Cn Cn - .� c Z W -o S Cn (]
a n CL n n a� - a '"o U a� w e O = O n o o a C; c n _ `�/// ,'
E E E E E °J E c _ Z O co O N O 0 o cn n cn aci 7 E m Z F6 m' m = o C7 C� U w E m ° Z ( -ll-&�
<v m m M M m _ L a o `o o O z CN M U M m 0 0 cn > co > Y E — Y o U V J m s o6 Ks O > a> > o
(n cn to co Cn O F- U Co Z 2 2 Z = Z CO 4 d J S of �
O
N Q P 1 o X X — — ----- �
UC12-EFF %/� 8/6/2024 6-A) 8/7/2024 Ob 8/712024 N Q P 1 o X X U✓�
UC12-EFF �/�� 816/2024 Q7U7j 817/2024 OWJ 8/7/2024 Q N Q P 1 X X w�
UC12-EFF -f//C, 8/6/2024 0703 8/7/2024 Q�� 8/7/2024 N Q P 1 N X X vi7
Comments: SHIPPED ON WET ICE Custody Seal Present: Custody Seal Number:
Sample Temp at Collection: NF: °C EFF: Cj ,� °C 200.8= Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,TI,Zn,Mo EFF SEMI-ANNUAL SAMPLES YES /NO
Sample Type Codes: [Relp- juished
4nqed
by(Sig re • Receive by(Signature): / ,. Date: TimeZc I
Sample Temp at Receiving in Lab: INF: °C EFF: °C D Q(Flow)=Automatic Flow Proportioned Sample �, �/ ��'�7 1 u l
Sample Temp of EFF Fecal Sample at Receiving in Lab °C o T(Time)=Automatic Time Proportioned Sample by(Signaturl): Received by(Signature): +S /%/ Date: Time:
(record only if collected): H(Hand)=Hand Composite SampleZero Headspace 8 Teflon septa for YES NO NIA M G(Grab)=Grab Sample by Signature): Received by(Signature): Date: Time:
VOAs: < Container Type Codes:
c
Samples in Proper Containers: YES NO N/A M A=Amber Glass P=Plastic Relinquished by(Signature): Received by(Signature): Date: Time:
Z GL=Clear Glass B=Bag
Chlorinated Samples De- YES NO NIA TL=Teflon Lined Cap Relinquished by(Signature): Received by(Signature): Date: Time:
Chlorinated: VOA=40 ml Glass vial I I I Page 104 of 133

9800 Kincey Ave#100
��a
�,e Huntersville,NC 28078 704 875-9092 EVENT TYPE: UC12-SEMI-AN& -8/7/2024 COC#: PAGE -7 of i
( ) Proj. Mgr.: Stephanie Knott l I
North Carolina Wastewater Certification#:12 SEND REPORT TO: Keith Purgason ActtNum/Client ID: Sampled by(Sign Name):
CLIENT: Union County Water 8299 Kensington Dr Table#:
FACILITY: Twelve Mile Creek WRF,NCO085359 l Waxhaw,NC 28173 Profile/Template: 16076 P Name: 1
ADDRESS 8299 Kensington Drive,Waxhaw,NC 28173 [e-mail] Prelogl Bottle Ord. ID
Sample Collection Data Sample Container Preservative Analyses Requested
LU
cn
~O Z o
m =
O � cmN
L) } m o m w w o v O n= LAB USE ONLY
SAMPLE ID m E o Co O mo o m ? M X N D w M r M N U) LAB SAMPLE ID
N O C @ H CUOEca7 Cn U >oU) O CD N Q O d?. N cO Co
U N N 17O - Oo
U) E o n O Q
m LJ G a LO (D T ~60) N O NW N N N
m W T c N
CDL.Li N W
N ( n i .0 W W
O d U) C W v = co
co O
n a 0 0 E -oE E E E ZO co O c", cn W � _
a c O c m o C C U w � CU
N>�
.oDN>
Z-7 a OO > U O O .� (D
U) co U) 0 H U 2 Z
(/
d 1:5: J II U 10 0 > 2 5_
17/2 24 0 h A 817/2024 6 b N T P 1 N X X U
0
UG12•FCE 8/6/2024 p(o 8/712024 0�0? 8/712024 QIpGq N T P 1 o X X
UC12-FCE �.(, 8/6/2024 g 8/7/2024 OW 8/712024 OI000( N T P 1 o X X V
UC12•FCE CL 817/2024 bb rJ5 N G P 1 X X 00
UC12-FCE 8/6/2024 8/712024 U VJ9 8/7/2024 bc( N T P 1 N X X UJ�
UC12-FCE 81612024 81712024 OW9 8/7/2024 010C)O� N T P 1 X X
UC12•FCE 816/2024 8/7/2024 WE 8/7/2024 0(009 N T P 1 X X X
UC12-FCE 8/6/2024 �� 8/7/2024 L909 817/2024 0(009 N T P 1 X X
UC12-FCE 81612024 8/7/2024 817/2024 0 b01� N T P 1 N X X
Comments: SHIPPED ON WET ICE Custody Seal Present: Custody Seal Number:
Sample Temp at Collection: INF: °C EFF: °C 200.8= Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,TI,Zn,Mo YES /NO
Sample Type Codes: Relinquished by(Signature:UCW Received by(Signature ,' Date: Time:
Sample Temp at Receiving in Lab: INF: °C EFF: °C F> O(Flow)=Automatic Flow Proportioned Sample
Sample Temp of EFF Fecal Sample at Receiving in Lab(record 0 T(Time)=Automatic Time Proportioned Sample R uished by(Sign It ) Received by(Signature): _ Date: Time:
only if collected): °C � H(Hand)=Hand Composite Sample ;�� �''' �/ — (:.: I t
Zero Headspace&Teflon septa for YES NO N/A 0 G(Grab)=Grab Sample Relinquished by(Signature): Received by(Signature): Date: Time:
VOAs: '< Container Type Codes:
a
Samples in Proper Containers: YES NO NIA Cl) A=Amber Glass P=Plastic Relinquished by(Signature): Received by(Signature): Date: Time:
Z GL=Clear Glass B=Bag
Chlorinated Samples De- YES NO N/A < TL=Teflon Lined Cap Relinquished by(Signature): Received by(Signature): Date: Time:
Chlorinated: J11 VOA=40 ml Glass vial I Pa e 105 of 133

9800 Kincey Ave#100
ace Huntersville,NC 28078 704 875.9092 EVENT TYPE: UC12-SEMI-AN& 81712024 COC#: PAGE Q of 1 S
( ) Proj. Mgr.: Stephanie Knott (� l
North Carolina Wastewater Certification#:12 SEND REPORT TO: Keith Purgason ActtNumlClient ID: Sampled by jSign Name):
CLIENT: Union County Water 8299 Kensington Dr Table#:
FACILITY: Twelve Mile Creek WRF,NCO085359 i Waxhaw,NC 28173 Profile/Template: 16076 Print Name:
ADDRESS: 8299 Kensington Drive,Waxhaw,NC 28173 [e-mail] Prelog(Bottle Ord. ID EZ 3143101
Sample Collection Data Sample Container Preservative Analyses Requested
co
w
r k— W U
O O o
O �� W O N
z 3 m x = o
} CO o a a � = N � LAB USE ONLY
SAMPLE ID m �, °' E m a m v o w "' � o D
i= o to 0 0 0 m M M X N N w M ti o v � LAB SAMPLE ID
v' 0 c ,a F U U >. � a7 ,n N — O m � o � N Q O _ � N � cD o �"� � 1-0 O
C O (li � C1 tfJ N N O O LO O �- Z t2") O 00 O Q L u7 (Q Q7
CD -p N (U >, N E ,n N v W M L N Cl >
a, o C n Q a .� o N N i— N 2 Q a c� oo a W i— N in N o
m m LU W E I— N M U) Cn U ,� -' a O rn N W cn w C.7 „ N cn
O_ C1 CL C1 CL Cn y 'C d 'co C) O w C`7 0 = 0 L0 Cn N U '0 C N W a C .D = U7 O
E E E E E 21 E E c z O O c� O o o m cn co Ta E v z m m ° _ o _o (7 (� U w
in C0 Cn cn in o i— U ° o o m 0 = = z = z m Om O cn > cn > 0- E _ Y o a- J = r au �zs O � � o
0
N T P 1 o X X X
UC12-MLSS 8/6/2024 8/712024 b q O� 8/712024 y U d N T P 1 N X X O[,r
UC12•MLSS t;f^ 81712024 y l q N G P 1 N X X (2
UC12-MLSS 8/6/2024 Jy/�i 8/7/2024 C,(c 817l2024 uyc- N T P 1 N X X O
UC12-MLSS 81612024 0 �� 8/712024 C (0`3 81712024 -1 N T P 1 �2 X X X X
UC12-MLSS ( 81612024 817/2024 817/2024 C'?crl N T P 1 N X X X
UC12•MLSS 8/7/2024 L, N G 0 3 X X 0(Z,
UC12-MLSS SR/2024 Dy4u N T A 2 o X X D 11
UC12"MLSS ( 816/2024 1 8/7/2024 i 8f112024 Cyr N T A 2 o X X of(
Comments: SHIPPED ON WET ICE Custody Seal Present: Custody Seal Number:
Sample Temp at Collection: INF: °C EFF: °C 200.8= Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,TI,Zn,Mo NOX- 48hour hold YES 1 NO
Sample Type Codes: Relinquished by(Signature):UCW Receive by(Signature):,, Date- Time:
Sample Temp at Receiving in Lab: INF: °C EFF: °C L
P P 9
Q(Flow)=Automatic Flow Proportioned Sample ; '�- �. ���
Sample Temp of EFF Fecal Sample at Receiving in Lab(record ,C o T(Time)=Automatic Time Proportioned Sample Relinquished by.(Sign to e): Received by(Signature): Date: Time:
Dory if collected): H(Hand)=Hand Composite Sample ` t' /l�n✓( L / e
Zero Headspace&Teflon septa for YES NO NIA 0 G(Grab)=Grab Sample Relinquished by(Signature): Received by(Signature): Date: Time:
VOAs: < Container Type Codes:
Samples in Proper Containers: YES NO NIA rn A=Amber Glass P=Plastic Relinquished by(Signature): Received by(Signature): Date: Time:
Z GL=Clear Glass B=Bag
Chlorinated Samples De- YES NO NIA < TL=Teflon Lined Cap Relinquished by(Signature): Received by(Signature): Date: P gem: of 133
Chlorinated: VOA=40 ml Glass vial I i

9800 Kincey Ave#100 I
UC12-SEMI-AN& •8f712024 COC#: PAGE of
ace Huntersville,NC 28078(704)875.9092 EVENT TYPE: Proj. Mgr.: Stephanie Knott
North Carolina Wastewater Certification#:12 SEND REPORT TO: Keith Purgason ActtNum/Client ID: Sampled by(Sign Name):
CLIENT: Union County Water \ 8299 Kensington Dr Table#:
FACILITY: Twelve Mile Creek WRF,NCO085359 Waxhaw,NC 28173 Profile/Template: 16076 t Name: /
ADDRESS: 8299 Kensington Drive,Waxhaw,NC 28173 �J [e-mail]— Prelogl Bottle Ord. ID aeo C Q
Sample Collection Data Sample Container Preservative Analyses Requested
cn
w
o 1 H W U
`n O Z CD3 W c� n
O ch C'7 t oG CV
r m o a a a, �_ = N LAB USE ONLY
SAMPLE ID a) °' �, E m a m v mo U, w "' F- o `o z'
Fo o a� a°'i cn o mo o m �N, ch x N ? w ,� M o cn LAB SAMPLE ID
<n c H U U �. a� n ^ N o m o m N Q O _ <n co o cn co o �
CIDc �n N N o o n o d z u' O a °' C) Q vi m 0
C d a c n n a t- .� cn "' N N g ~ cn llJ a Q N o CL N w N N o
n] m W w E M F N_ c'7 1 (/') 2 2 Cn U Y ,(O Cr O VJ N W in W (.7 r- N (n
QJ Ql @ C O I N , Z L N i Vl , `+ N
rn C g C O Cn V CJ (n C W d = Lo fD U
Q O_ a d CL D_ .O W CJ = N CID C O .0 O (' C cn .7
E E E E E °� E c U z O OW O N O C0 cn cn E v Z m fII _ `o C� C� U w 2
co O O O a cc] ( L 4' O O >• O
CID CIO !n Cn Cn H U (I] Z S S Z = Z CO J 2 �
0
jL X
o
UC12-RAS 816/2024 )<<8' 8!7/2024 0343 8f7/2024 03LAI N H P 1 N X X ()c3
UC12-RAS 8/7/2024 03�� N G P 1 X X ©j K
UC12-RAS 8/6/2024 It1 8/7/2024 0343 8f7/2024 G3�� N H P 1 N X X U(?j
UC12-RAS 8/6/2024 ttl 8/7/2024 o3143 8/7/2024 0'jL{1 N H P 1 X X
UC12-RAS 8/6/2024 AIX 8/7/2024 03'13 8/7/2024 63�1� N H P 1 X X
UC12-RAS 8/6/2024 f))0 8f712024 6343 8/7/2024 �3 L1� N H P 1 r X X
Comments: SHIPPED ON WET ICE Custody Seal Present: Custody Seal Number:
Sample Temp at Collection: INF: °C EFF: °C 200.8= Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,TI,Zn,Mo YES /NO
Sample Tvpe Codes: Re�n, sCW Received y(Signature)- Date: Time:
Sample Temp at Receiving in Lab: INF: °C EFF: °C
Q(Flow)=Automatic Flow Proportioned Sampleca
hed by Signature :U
Sample Temp of EFF Fecal Sample at Receiving in Lab(record o T(Time)=Automatic Time Proportioned Sample quished by(Signature): - / Receiv d by(Signature): }} � I`7 ?'�iN Date. Time:
only if collected): °C H(Hand)=Hand Composite Sample
Zero Headspace&Teflon septa for YES NO NIA 0 G(Grab)=Grab Sample Relinquished by(Si nature): Received by(Signature): Date: Time:
VOAs: < Container Type Codes:
Samples in Proper Containers: YES NO NIA m A=Amber Glass P=Plastic Relinquished by(Signature): Received by(Signature): Date: Time:
z GL=Clear Glass B=Bag
Chlorinated Samples De- < TL=Teflon Lined Cap Relinquished by(Signature): Received by(Signature): Date: Time:
Chlorinated: YES NO N/A VOA=40 ml Glass vial P ge 107 of 133

9800 Kincey Ave#100
ace Huntersville,NC 28078(704)875-9092 EVENT TYPE: UC12-SEMI-AN& -8f712024 Proj. Mgr.: Stephanie Knott COC#: PAGE O of I
North Carolina Wastewater Certification#:12 SEND REPORT TO: Keith Purgason ActtNum/Client ID: Sampled by(Sign Name):,
CLIENT: Union County Water 8299 Kensington Dr Table#:
FACILITY: Twelve Mile Creek WRF,NCO085359 Waxhaw, NC 28173 Profile/Template: 16076 ri ame:
ADDRESS: 8299 Kensington Drive,Waxhaw,NC 28173 [e-mail] Prelog/Bottle Ord. ID rz Avg l� livu
Sample Collection Data Sample Container Preservative Analyses R quested
co
w
U _o
Z 3 O M M w = �
CD N
Q
SAMPLE ID E m Co m m v mo w w CD CN v LAB USE ONLY
in a� E o o o mo p Co �N.., c-� X N W W �:, ^ o v v _a N LAB SAMPLE ID
0 C (D ~ U U T N V1 N O m 0 O N Q O In CO M tOD CO O i
@ C _d Q. ZE
to N N O O a Z 47 O (UCIR
O Q L
C d C Q C- Q C E Lo 47 U-) N H (n W N M Q. Z O Q N � ' L v _>
m m w W E T a (n N N g - Q N '- o d W g H N N o
ca a N to .° Z a L r w w C� N u
CD C N C O (n V' N � U) (n � CO W d 2 (n cC "O G
E E E E E a o E c U z 0 ChC-j 0 N O o O (n cn W � m E m z a m E _ � `o O C R Cl) w ' CU O
Cn W W Cn (n O U O O CO O = = Z = Z m m O (n Cn QL Y E = Y O 0-
J = L O2S RS O 5 T ( (lD
12-WAS 16/2 24 11 17/2024 03L13 8f7 2 24 D 3 N H P 1 o X X X (S
uclz•wns 8/6/2024 11 / �' 8/7/2024 D3`f3 8/7/2024 03`fg N H P 1 N X X
UC12-WAS 8/7/2024 N G P 1 X X
UC12-WAS 8/612024 1 1 1 Y 817/2024 C 3Lf 8/7/2024 C)3r{ N H P 1 N X X O(S
UC12-WAS 8/6/2024 i t (`a 817/2024 t)3'( 817/2024 u3g N H P 1 N X X
UC12-WAS $� ' 8/6/2024 f J l K 8f712024 �`J 8/712024 3� ) N H P 1 X X X
Comments: SHIPPED ON WET ICE Custody Seal Present: Custody Seal Number:
Sample Temp at Collection: INF: °C EFF: °C 200.8= Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,TI,Zn,Mo YES 1 NO
Sample Type Codes: Relinquished by(Signature):UCW eived y,Signature:- ° Dates: Time:
Sample Temp at Receiving in Lab: INF: °C EFF: °C ,
Q(Flow)=Automatic Flow Proportioned Sample � / ��� } �/' i
Sample Temp of EFF Fecal Sample at Receiving in Lab(record °C o T(Time)=Automatic Time Proportioned Sample Reli fished by(Signature): Receiv d by(Signature}: /-7 T Date: 1 Time:
only if collected): � H(Hand)=Hand Composite Sample `�( ^ i �� All
Zero Headspace 8 Teflon septa for YES NO NIA � G(Grab)=Grab Sample Relinqul§he by(Signature): Received by(Signature): Date: Time:
VOAs: < Container Type Codes:
Samples in Proper Containers: YES NO NIA m A=Amber Glass P=Plastic Relinquished by(Signature): Received by(Signature): Date: Time:
z GL=Clear Glass B=Bag
Chlorinated Samples De- YES NO NIA TL=Teflon Lined Cap Relinquished by(Signature): Received by(Signature): Date: Time:
Chlorinated: I j VOA=40 ml Glass vial I Page 108 of 133

9800 Kincey Ave#100
/ ace Huntersville,NC 28078(704)875-9092 EVENT TYPE: UC12-SEMI-AN& -81712024 Proj. Mgr.: Stephanie Knott
COC#: PAGE 1 1 of
`
North Carolina Wastewater Certification#:12 SEND REPORT TO: Keith Purgason ActtNum/Client ID: Sampled�v(Sin Name)
CLIENT: Union County Water 8299 Kensington Dr Table#: /` //'
Chi
FACILITY: Twelve Mile Creek WRF,NCO085359 Waxhaw,NC 28173 Profile/Template: 16076 nt ame:
_ADDRESS: 8299 Kensington Drive,Waxhaw,NC 28173 [e-mail] Prelog/Bottle Ord. ID EZ 3143105 1Y+ j
Sample Collection Data Sample Container Preservative Analyses Requested
W
J I W U
O co U Z o
3 = n Z w U ,�
O N
O cD
r �, Co o a . � = N n LAB USE ONLY
SAMPLE ID Q1 to
co Q) m v mo w F o o
a E a� E m N o LAB SAMPLE ID
E p cn o O 0 CO M M X N <n W ,,.� n can -a cn U
cn O c �° U U a a� <n ,� cv N CocD o -It co N d 0 co
u7 0 w — o Q r L `-
N [7 O W M CN d tl'Y N j
E d c n a a n t- c cn �" N N - rn ° Q n c� O o W N N o
CD m W W E E H N c7 fn 2 N �-. .O '_' d NO in N W u� W U` ti N vOi
C a� a n a co �_ n co W c> v = O 0 in N .o c �o 6 W a a v c -9 = cn `o = 2Z 1
E E E E E cu �' o E c U z 0 60 0 N 0 0 0 cn cn cry 'o E ,6 z m m = o o C7 C7 U W a 7(�
(p (p CO co cC E t m O O O O Z N (D U m O] O O cn > (.!) > L Y E = Y O U O J O L o6S '' O > O T
U) cn co (n O F— U m Z S S Z = Z cD U J S0 0 0 of
cD
o X X o f✓)
- O
UC12-INFDIST 8/6/2024 lJt051 8f1/2024 OL L1 8/712024 �G 2� N T P 1 N X X ((�I
UC12-INFDIST 817/2024 QLZ N G P 1 N X X Q O
UC12-INFDIST 8/6/2024 p S 8/7/2024 �Zl 8f7/2024 Q�Z� N T P 1 N X X v ��
UC12-INFDIST 816/2024 5_I 8/712024 b �t 8/7/2024 6��j N T P 1 � X X X X
UC12-INFDIST 11A 8/612024 C�71 8l7/2024 b� l 81712024 0�2� N T P 1 N X X X V
UC12-INFDIST IHYI 817/2024 UZD N G 0 3 X X U��
UC12-INFDIST �� 8/712024 �r��/� N G A 2 o X X .P(
UC12-INFDIST I 8/712024 N G A 2 o X x
UC12-INFDIST 8/612024 0(dj, 8/7/2024 8/7/2024 N T P 1 o X X
UC12-INFDIST y4v\ 1 8/612024 8/7/2024 ���1 8/7/2024 N T P 1 x X 00
Comments: SHIPPED ON WET ICE Custody Seal Present: Custody Seal Number:
Sample Temp at Collection: INF: °C EFF: 200.8= Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,TI,Zn,Mo NOX- 48hour hold YES /NO
Sample Type Codes: Reli ui ed.by(Si re):UCW Received by(Signature): ' Date: Time-
Sample Temp at Receiving in Lab: INF: °C EFF: IC % /� /) a J ��
Q(Flow)=Automatic Flow Proportioned Sample
ca
Sample Temp of EFF Fecal Sample at Receiving in Lab(record ,C O T(Time)=Automatic Time Proportioned Sample Re)inquished by(Signatu ):,) Received by(Signature): Date: Time:
only if collected): P H(Hand)=Hand Composite Sample I l
Zero Headspace&Teflon septa for YES NO N/A G(Grab)=Grab Sample Relinquished by(Signature): Received by(Signature): Date: Time:
VOAs: < Container Type Codes:
c
Samples in Proper Containers: YES NO NIA M A=Amber Glass P=Plastic Relinquished by(Signature): Received by(Signature): Date: Time:
Z GL=Clear Glass B=Bag
Chlorinated Samples De- YES NO N/A < TL=Teflon Lined Cap Relinquished by(Signature): Received by(Signature): Date: Pa Time:
of 133
Chlorinated: VOA=40 ml Glass vial

9800 Kincey Ave#100
ace COC#: PAGE q of
Huntersville,NC 28078(704)875-9092 EVENT TYPE: UC12•SEMI-AN 8 -81712024 Proj. Mgr.: Stephanie Knott I 1
North Carolina Wastewater Certification#:12 SEND REPORT TO: Keith Purgason ActtNum/Client ID: Sampled by Sign Name)/:_,
CLIENT: Union County Water 8299 Kensington Dr Table#-.
FACILITY: Twelve Mile Creek WRF,NCO085359 Waxhaw,NC 28173 Profile/Template: 16076 Print Name:
ADDRESS: 8299 Kensington Drive,Waxhaw,NC 28173 [e-mail] Prelog/Bottle Ord. ID Go-6r—I e I m
Sample Collection Data Sample Container Preservative Analyses Requested
co
W
c W U
M 0 z w U
O N
a z 3 a) Q = o
a) Q m o 00 7 w CL � U = N v LAB USE ONLY
a) N c W o o d 1.0
SAMPLE ID E a, o o m �_ o 0 o m v M M x N `n w ti cD v _� c�i� LAB SAMPLE ID
`� c m F U U ?. o t_n N O Co 0 0 N Q O _ cD o to o 'n
(D C_ - O a) n If) N N O O d Z l['1 O Q) W O Q L
cm -O Q) a) T Q) E 11') N V' V Lo O rL L -O u-� (Q a)
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00 y W y E tv c9 H a`) c N c7 Cn U '`. .� O. O N N W to W C.7 n N T
a a) a) In C a) C U VJ V N N U - C Z W N S (!) ca
cf)
a Q a n a -o Q. '@ U a) W c� O = 0 � o .c o a) W D_ U c N 0
E E E E E E E _ z 0 cn O N O o 0 crn cn cn E m z m _ o c� c) U W m iv
ca a3 is ca m m _C ca o 0 o O z cN ca CJ co m 0 0 U) > cn > L Y E = Y o U a) �a t -6 .6 0 > o >. o
co (n cn W Cn 0 H U m Z 2 = 7_ 2 Z [� Q_ 2 � J 2 0_
R(719094 Ili N H P 2 X X X
UC12-BFP•1-CAKE 8/6l2024 ) i 8/712024 ',I 8/7/2024 N H P 1 N X X �y f4
UC12-BFP-I-CAKE L r. 817l2024 7�r N G P 1 X X 0,�o
UC12-BFP-I-CAKE 8/6/2024 !i 1 i 8/7/2024 C l 817/2024 b j J C N H P 1 N X X 06
UC12-BFP-I-CAKE C-)r^ 8/612024 111 ) 81712024 Z%>1 S 81712024 N H P 1 X X 0(�
UC12-BFP-I-CAKE 816l2024 /i 1 8/712024 C )5 817/2024 N H P 1 Lo X X X /
U1
Comments: SHIPPED ON WET ICE Custody Seal Present: Custody Seal Number:
Sample Temp at Collection: NF: °C EFF: °C 200.8= Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,TI,Zn,Mo YES /NO
Sample Type Codes: Relinquished by(Si nature):UCW ec ived by(Signature): �' / ' Date: Tine:
Sample Temp at Receiving in Lab: INF: °C EFF: °C
Q(Flow)=Automatic Flow Proportioned Sample �� ;�j �' I f L
Sample Temp of EFF Fecal Sample at Receiving in Lab(record ,C o T(Time)=Automatic Time Proportioned Sample Relinquished by�Signatu e):, Receiv d by(Signature): Date: Time:
only if collected): H(Hand)=Hand Composite Sample
Zero Headspace&Teflon septa for YES NO N/A G(Grab)=Grab Sample lRelinqUished by(Signature): Received by(Signature): Date: Time:
VOAs: < Container Type Codes:
Samples in Proper Containers: YES NO NIA m A=Amber Glass P=Plastic Relinquished by(Signature): Received by(Signature): Date: Time:
z GL=Clear Glass B=Bag
Chlorinated Samples De- YES NO NIA < TL=Teflon Lined Cap Relinquished by(Signature): Received by(Signature): Date: Time:
Chlorinated: I VOA=40 ml Glass vial I I Pape 110 of 133

9800 Kincey Ave#100
COC#: PAGE of
ace Huntersville,NC 28078(704)875-9092 EVENT TYPE: UC12-SEMI-AN& -81712024 Proj. Mgr.: Stephanie Knott � 3 l
North Carolina Wastewater Certification#:12 SEND REPORT TO: Keith Purgason ACttNum/Client ID: Sampled by Sign Name):
CLIENT: Union County Water 8299 Kensington Dr Table#:
FACILITY: Twelve Mile Creek WRF,NCO085359 IT Waxhaw,NC 28173 Profile/Template: 16076 Print Name:
i
ADDRESS: 8299 Kensington Drive,Waxhaw,NC 28173 [e-mail] Prelog/Bottle Ord.ID ��{h e I '1��.r1••�c
Sample Collection Data Sample Container Preservative Analyses Requested
W
w
o .- H W U
O Z o
3 o U') z w c�
a Z 3 (D ¢
SAMPLE ID °' °-� r m CO N m o "' w o v o a v -1 LAB USE ONLY
E m a) - E a) m v ui o �- g -
co i•= a) E o o a) �? c mo o m r) �"� x N w M ^ o v -o cn cn LAB SAMPLE ID
C/) a) <n C14 o m O o N Q O E c c� � L �-
c y a u-j N N o o v d in o 00 o Q
a� v a) ca > a`� E u-) N v v o o Sri12
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m W E co is ~ `�) fn VJ U y N — a- O in N W v� W C) r N >, N
Q Q o- n. a. d - o_ � U a) w ch O = �n co 0 .c o a� °- ") C� c u) � O
E E E E E °' E E c - z 0 CO 0 N O o a cn cn cn a�i E z m m _ o `o C7 c7 U w
co co in co in U c° o o m Oz S S z = z CO m 0 cn > cn > d Y E - Y o a 5 J = U 0 O � � > Z
0
N G P 1 N X X
0
UC12-BFP-I-FILT G M 817/2024 C f 1 5 N G P 1 o X X
0
UC12-BFP-I-FILT L 'n 8/7/2024 Crl(7, N G P 1 o X X
UC12-BFP-I-FILT ^n 817/2024 C-Q i N G P 1 X X
UC12-BFP-I-FILT r 8/712024 fy 15 N G P 1 N X X
UC12-BFP-I-FILT (J 817/2024 L"yrj N G P 1 N X X
UC12-BFP-I-FILT 817/2024 0 N G P 1 X X
UC12-BFP-I-FILT G!^ 8/712024 p,, N G P 1 r X X X
UC12-BFP-I-FILT 8/7/2024 ujl N G P 1 C X X
IL
Comments: SHIPPED ON WET ICE Custody Seal Present: Custody Seal Number:
Sample Temp at Collection: INF: °C EFF: °C 200.8= Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,TI,Zn,Mo YES /NO
Sample Type Codes: Relinquished by(Signature):UCW Received b�'jSignat r Date: Time:
Sample Temp at Receiving in Lab: INF: °C EFF: °C ; � `'� �' � f^ / J1JQ(Flow)=Automatic Flow Proportioned Sample �:�� //�� /' �, �,
Sample Temp of EFF Fecal Sample at Receiving in Lab(record ,C 0 T(Time)=Automatic Time Proportioned Sample Relinquished by(Signature: Receive ,�-by(Signature): ,/7 IDaie: Time:
only if collected): T. H(Hand)=Hand Composite Sample J �, I (.� .vt L'( y iG—t (f vt ( 1-('
Zero Headspace&Teflon septa for YES NO N/A 0 G(Grab)=Grab Sample Relinquished by(Signature): Received by(Signature): Date: Time:
VOAs: < Container Type Codes:
Samples in Proper Containers: YES NO N/A " A=Amber Glass P=Plastic Relinquished by(Signature}: Received by(Signature): Date: Time:
z GL=Clear Glass B=Bag
Chlorinated Samples De- YES NO NIA < TL=Teflon Lined Cap Relinquished by(Signature): Received by(Signature): Date: Time:
Chlorinated: VOA=40 ml Glass vial Page 111 of 133

9800 Kincey Ave#100
ace Huntersville,NC 28078(704)875.9092 EVENT TYPE: UC12-SEMI-AN& -81712024 Proj. Mgr.: Stephanie Knott COC#: PAGE `1.1 of 1�
North Carolina Wastewater Certification#:12 SEND REPORT TO: Keith Purgason AcUNum/Client ID: Sampled by(Sign Name): _l
CLIENT: Union County Water - 8299 Kensington Dr Table#:
FACILITY: Twelve Mile Creek WRF,NCO085359 Waxhaw,NC 28173 Profile/Template: 16076 Pri ame: 1 L
ADDRESS: 8299 Kensington Drive,Waxhaw,NC 28173 [e-mail] Prelog/Bottle Ord. ID
Sample Collection Data Sample Container Preservative Analyses Requested
W
w
o w U
O z o
3 o u�-)
a z_ 3 Q < = o N
SAMPLE ID a' °�' } m m o m o w W o v o a v LAB USE ONLY
iE E o o °_E a° mo mo p m MLo X N n `D w M ^ o r v � LAB SAMPLE ID
c H U U i. a> fn c� •- o m o m N Q O cn co �p in o
CO C O 61 0- N N O O V a Z N O (U O p
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127
UC12-1 2 AER 8/6/2024 q\(0817I2024 0 8/712024 0& N T P 1 o X X X
UC12.1_2 AER 81612024 () -it b 8/712024 0 Li05 81712024 ti D10 N T P 1 N X X OZ Z
� X X �j23 UC12.1_2AER � 8/712024 O�Oq N G P 1
UC12.1_z AER 81612024 G 1-11 f0 8/712024 0 405 81712024 0�1 U 6N T P 1 N X X v22
I I I FFFI IL I I I
Comments: SHIPPED ON WET ICE Custody Seal Present: Custody Seal Number:
Sample Temp at Collection: INF: °C EFF: °C 200.8= Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,TI,Zn,Mo YES /NO
Sample Temp at Receiving in Lab: INF: °C EFF: °C
Sample Type Codes: Relinquished by(Signature:UCW Received by(Signature): Date: Time:
� %.
n Q(Flow)=Automatic Flow Proportioned Sample l�C /i 1 j l
Sample Temp of EFF Fecal Sample at Receiving in Lab(record ,C o T(Time)=Automatic Time Proportioned Sample ReViquishld b�r-(Signature): Recei ed by(Sig tvrej: `'i!7 > Date: Time:
only if collected): � H(Hand)=Hand Composite Sample "�_"� f) ' ( 7�: `� j"Q_L " )
Zero Headspace&Teflon septa for YES NO NIA 0 G(Grab)=Grab Sample Relinquished by(Signature): Received by(Signature): Date: Time:
VOAs: Container Type Codes:
Samples in Proper Containers: YES NO NIA m A=Amber Glass P=Plastic Relinquished by(Signature): Received by(Signature): Date: Time:
z GL=Clear Glass B=Bag
Chlorinated Samples De- YES NO NIA < TL=Teflon Lined Cap Relinquished by(Signature): Received by(Signature): Date: Time:
Chlorinated: VOA=40 ml Glass vial P ge 112 of 133

9800 Kincey Ave#100
ace Huntersville,NC 28078(704)875-9092 EVENT TYPE: UC12-SEMI-AN& -81712024 Proj. Mgr.: Stephanie Knott COC#: PAGE t f of l
North Carolina Wastewater Certification#:12 SEND REPORT TO: Keith Purgason ACttNumlClient ID: Sampled by(Sign Name): f `�
CLIENT: Union County Water 8299 Kensington Dr Table#: -
FACILITY: Twelve Mile Creek WRF,NCO085359 Waxhaw,NC 28173 Profile/Template: 16076 rint e:
ADDRESS: 8299 Kensington Drive,Waxhaw,NC 28173 [e-mail] Prelog/Bottle Ord.ID
Sample Collection Data Sample Containerl Preservative Analyses Requested
U)
LU
o . W U
3 0 U') � CC) o
O M w o C'j
SAMPLE ID °' °; L } m m N Coo 0- 0- CD �' o a v LAB USE ONLY
mo Co ? N �`� � �' o ~ o LAB SAMPLE ID
F- E o a� 0 0 m a' X N w r., ^ o V Cn Cn
c 0 1- U i. Q. v, ,ii N N o o V N d u' o o co o Q r r r- 'o
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d C Q Q -O Q C u' u' u' N H (n W M Q .U Q N _ O
C Cll m C W O }. '@ N !n N N _ Q �n O O. W r. N N O
m LU
O o N (O CD ~ CU C N co N N (/) U T .@ z d = N W N W C:� I— N a (n
a Cl- n a o a� n m U a� W , -O = N o .c o C a N U a) g 2 cA o U
E E E E E °' E E _ z O U) O CCv O o 0 co co can m E Z v m �° _ o C7 C7 c� w m ��/ 2//A
CD [p tC (6 f0 co L M O O p O Z N M U M m O O U) Cn > L Y E = Y O U O J CV E KS -6 O > N �. p v __((-(
U U U m Z S S Z = Z M d d J S K S
O
UC125 �_ N I T P 1 o X X X
UC12.5_6 AER 8/6l2024 �y� 8/712024 C)`tV 8/7/2024 ���� N T P 1 N X X b111
UC12-5_6 AER t 8r7/2024 Lf 05 N G P 1 !;� X X U ZS
UC12.5_6AER 8/612024 CS 8f7l2024 0y0(4 817/2024 (7y G?1 N T P 1 N X X -L
Comments: SHIPPED ON WET ICE Custody Seal Present: Custody Seal Number:
Sample Temp at Collection: INF °C EFF: °C 200.8= Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,A9,TI,Zn,Mo YES !NO
Sample Type Codes: Relinquished by(Signature):UCW Rec ived fly(Signatures: Date: Time:
Sample Temp at Receiving in Lab: INF: °C EFF: °C _ I-)
Q(Flow)=Automatic Flow Proportioned Sample ( � ��l%�.�� , =; //z/
Sample Temp of EFF Fecal Sample at Receiving in Lab(record oC o T(Time)=Automatic Time Proportioned Sample rRelinquilhed
fi wished by(Signat e ! Recei�ed by(Signature): p/" Date: Time:
only if collected): � H(Hand)=Hand Composite Sample 1'11 ✓ /t ?� I
Zero Headspace&Teflon septa for YES NO N/A 0 G(Grab)=Grab Sample by(Signature): Received by(Signature): Date: Time:
VOAs: < Container Type Codes:
Samples in Proper Containers: YES NO N/A m A=Amber Glass P=Plastic Relinquished by(Signature): Received by(Signature): Date: Time:
z GL=Clear Glass B=Bag
Chlorinated Samples De- YES NO NIA < TL=Teflon Lined Cap Relinquished by(Signature): Received by(Signature): Date: Time:
Chlorinated: VOA=40 ml Glass vial P e 113 of 133

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DG9U-40 mt.Amber Unpreserved vials(N/A; Page 117 of 133

aceAnalytical
Report of Analysis
Pace Analytical LLC
1377 South Park Drive
Kernersville, NC 27284
Attention: Stephanie Knott
Project Name: UC12-SEMI-AN & PPA-8/7-2024
Project Number: 92746299
Lot Number:ZH15017
Date Completed:08/19/2024
08/20/2024 12:47 PM
Approved and released by:
Project Coordinator 1: Brooke Speers
4r�Q pC�
ANSI WoolA"MdMion 8Wd
A C C R E D I T E D
qeO —
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety,without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 118 of 133
Page 1 of 16

PACE ANALYTICAL SERVICES, LLC
SC DHEC No:32010001 NELAC No: E87653 NC DENR No:329 NC Field Parameters No:5639
Case Narrative
Pace Analytical LLC
Lot Number: ZH15017
This Report of Analysis contains the analytical result(s)for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPS), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPS or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non-Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM
2320 B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011,
Fecal Coliform Colilert-18. If you have any questions regarding this report, please contact the Pace
Project Manager listed on the cover page.
Manual integration summaries are provided at the end of this report when applicable.
Low Level Mercury Analysis
The following sample was diluted 10x due to the nature of the sample matrix: ZH15017-001. The LOQ
has been elevated to reflect the dilution. The sample did not stay brominated.
Pace Analytical Services,LLC(formerly Shealy Environmetal Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172(803)791-9700 Fax[phone] www.pacelabs.com
Page 119 of 133
Page 2 of 16

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Pace Analytical LLC
Lot Number: ZH15017
Project Name: UC12-SEMI-AN & PPA-8/7-2024
Project Number: 92746299
Sample Number Sample ID Matrix Date Sampled Date Received
001 UC12-INF Aqueous 08/07/2024 0819 08/14/2024
002 UC12-INF FIELD BLANK Aqueous 08/07/2024 0819 08/14/2024
003 UC12-EFF Aqueous 08/07/2024 0803 08/14/2024
004 UC12-EFF FIELD BLANK Aqueous 08/07/2024 0803 08/14/2024
(4 samples)
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 120 of 133
Page 3 of 16

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Pace Analytical LLC
Lot Number: ZH15017
Project Name: UC12-SEMI-AN & PPA-8/7-2024
Project Number: 92746299
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 UC12-INF Aqueous Mercury(CVAFS) 1631E 9.29 ng/L 5
003 UC12-EFF Aqueous Mercury(CVAFS) 1631E 0.734 ng/L 7
(2 detections)
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 121 of 133
Page 4 of 16

Mercury (CVAFS)
Client:Pace Analytical LLC Laboratory ID:ZH15017-001
Description:UC12-INF Matrix:Aqueous
Date Sampled:08/07/2024 0819 Project Name:UC12-SEMI-AN&PPA-8/7-2024
Date Received:08/14/2024 Project Number:92746299
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 10 08/17/2024 0443 KAJ 08/16/2024 1423 16441
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Mercury(CVAFS) 7439-97-6 1631 E 9.29 5.00 ng/L 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range Q=Surrogate failure
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 122 of 133
Page 5 of 16

Mercury (CVAFS)
Client:Pace Analytical LLC Laboratory ID:ZH15017-002
Description:UC12-INF FIELD BLANK Matrix:Aqueous
Date Sampled:08/07/2024 0819 Project Name:UC12-SEMI-AN&PPA-8/7-2024
Date Received:08/14/2024 Project Number:92746299
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 08/17/2024 0449 KAJ 08/16/2024 1423 16441
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Mercury(CVAFS) 7439-97-6 1631E ND 0.500 ng/L 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range Q=Surrogate failure
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 123 of 133
Page 6 of 16

Mercury (CVAFS)
Client:Pace Analytical LLC Laboratory ID:ZH15017-003
Description:UC12-EFF Matrix:Aqueous
Date Sampled:08/07/2024 0803 Project Name:UC12-SEMI-AN&PPA-8/7-2024
Date Received:08/14/2024 Project Number:92746299
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 08/17/2024 0454 KAJ 08/16/2024 1423 16441
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Mercury(CVAFS) 7439-97-6 1631 E 0.734 0.500 ng/L 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range Q=Surrogate failure
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 124 of 133
Page 7 of 16

Mercury (CVAFS)
Client:Pace Analytical LLC Laboratory ID:ZH15017-004
Description:UC12-EFF FIELD BLANK Matrix:Aqueous
Date Sampled:08/07/2024 0803 Project Name:UC12-SEMI-AN&PPA-8/7-2024
Date Received:08/14/2024 Project Number:92746299
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 08/17/2024 0511 KAJ 08/16/2024 1423 16441
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Mercury(CVAFS) 7439-97-6 1631E ND 0.500 ng/L 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range Q=Surrogate failure
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 125 of 133
Page 8 of 16

QC Summary
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.) QC Data for Lot Number:ZH15017
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 126 of 133
Page 9 of 16

Mercury (CVAFS) - MB
Sample ID: ZQ16441-001 Matrix: Aqueous
Batch:16441 Prep Method:
Analytical Method: 1631 E Prep Date: 08/16/2024 1423
Parameter Result Q Dil LOQ Units Analysis Date
Mercury(CVAFS) ND 1 0.500 ng/L 08/17/2024 0405
LOQ=Limit of Quantitation ND=Not detected at or above the LOQ N=Recovery is out of criteria
P=The RPD between two GC columns exceeds 40
=RSD is out of criteria +=RPD is out of criteria
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.) QC Data for Lot Number:ZH15017
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 127 of 133
Page 10 of 16

Mercury (CVAFS) - LCS
Sample ID: ZQ16441-002 Matrix: Aqueous
Batch:16441 Prep Method:
Analytical Method: 1631 E Prep Date: 08/16/2024 1423
Spike
Amount Result %Rec
Parameter (ng/L) (ng/L) Q Dil % Rec Limit Analysis Date
Mercury(CVAFS) 5.00 4.93 1 99 75-125 08/17/2024 0416
LOQ=Limit of Quantitation ND=Not detected at or above the LOQ N=Recovery is out of criteria
P=The RPD between two GC columns exceeds 40%
=RSD is out of criteria +=RPD is out of criteria
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.) QC Data for Lot Number:ZH15017
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 128 of 133
Page 11 of 16

Mercury (CVAFS) - MS
Sample ID: ZH15017-003MS Matrix: Aqueous
Batch:16441 Prep Method:
Analytical Method: 1631 E Prep Date: 08/16/2024 1423
Sample Spike
Amount Amount Result %Rec
Parameter (ng/L) (ng/L) (ng/L) Q Dil % Rec Limit Analysis Date
Mercury(CVAFS) 0.734 5.00 5.50 1 95 71-125 08/17/2024 0500
LOQ=Limit of Quantitation ND=Not detected at or above the LOQ N=Recovery is out of criteria
P=The RPD between two GC columns exceeds 40%
=RSD is out of criteria +=RPD is out of criteria
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.) QC Data for Lot Number:ZH15017
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 129 of 133
Page 12 of 16

Mercury (CVAFS) - MSD
Sample ID: ZH15017-003MD Matrix: Aqueous
Batch:16441 Prep Method:
Analytical Method: 1631 E Prep Date: 08/16/2024 1423
Sample Spike
Amount Amount Result %Rec %RPD
Parameter (ng/L) (ng/L) (ng/L) Q Dil %Rec %RPD Limit Limit Analysis Date
Mercury(CVAFS) 0.734 5.00 5.30 1 91 3.7 71-125 24 08/17/2024 0505
LOQ=Limit of Quantitation ND=Not detected at or above the LOQ N=Recovery is out of criteria
P=The RPD between two GC columns exceeds 40%
=RSD is out of criteria +=RPD is out of criteria
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.) QC Data for Lot Number:ZH15017
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 130 of 133
Page 13 of 16

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 131 of 133
Page 14 of 16

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 132 of 133
Page 15 of 16

PACE ANALYTICAL SERVICES, LLC
DCP—Titfe: ENV-FRM-%VCOL-0286 02 Samples Reoeipt Checklist(SRC)
Effective Date.8/2/2022
Sample Receipt Checklist (SR(:)
C)icllt. PACE Cooler h edxed b AInie: CDR ie (A." 14 l.ot#: ZH:5011
!`Means ot'recei t; , Pace Client LJP.% U FedEX Other.
Wyesl 14Nol1, Wine cu tdxly teals present on die coolcr'
jYesj INa �/ NA Z.Ifd:r�tod seals xere resetui,v►ere th intact and w�brvJdxu".
H Strip lD: Na Chlorin:Strip ID: tiw -- Tested by."A
Oriolled temperature upon receipt!Derived(Connected)tempe'ntue upon receipt %Solid Strap-Cap ID:
34 j.3.4 cc NA itvA oC 1 A iMA oC NA yNA of
lethod'QI'emperat,are Blank[])A-ainsr Bottles IR(J m1D: 8 1R Cnln C'otrcctiou Factor: c °C
Method of coolant- 271 wet Ice Ice Packs Ice Mone
EYcs []No []NA
3. Were all coolers rcccivcd at or bclow 6.06'C7 If no,was Project Manager ndxifi dl?
PM wtts Notificd lay'pltonr,crnaii i facc4.048Cc(cud:le one).
Yes No J 4- is tic comninvia1 cuuiier's packing shp at acbcd to 111is ka ?
J Yes FINO 5. Were:proper CUSiody Imoc'd- mc'S(1'C111nlhllShrdb'LeCCIteJ)follower)''
Yes No 6- Were sample iDs listed on the COC and all si lc containers?
J Yes No 7. Was colle6on dMtc&butt listed on the C(x'and all sanrole containers?
Yes No 8.Did all cenumer label irforn ttion(Ill,date,time)atscc with the CO:?
J YesI jNu 9.Were tests to be performed listed on the COC?
QJ Yes []No 10.Did all samples tlnive in the proper containers for cash tca and/or in good c iitioil
(hmlw4wi,lids on.etc.)?
J Yd,Ro
o 11.Ni�as adequate sample volume available?
J Yes 12. Wac all sainplcs rmcivcd witlun'':ilhc holdiug blue or 48 hours.whichever aomes first•?
[Z]Yes []No 13.were all sm4les containers accounted)M'(No n:3ssin&"cess)
QY� [�No QNa 14.Wcrc VOA-8015C andRSK-ir.5 samples free of bubbles>"pca-sizc"('/a•'or fjunaiu
dliamleter)in any of the VOA vials!
Yes No J A 1.5.Wcre all DROAmeral.gAiii ent cant leg neceivcd a1 a Hof<2?
Yes No [7NAI 16,Were all cyanide samples received nt a H>12 and shufide sae les received. a 1t'>1•?
17.Vvcrc a app ca c N1 �, c)"un euo G.;.,�G08.3 (�=0.Smig! ).'amp s lire of
Yes [:]No [Z]NAresidinal chlorine?
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18.Was the quote number listed on the container lalbvl?If y c&Qiatc
:
Sample Preservation (Must be cuaVicted fof ajiy,-a Wle(s)incorrectly preserved or with hcadspacc.)
Saiuplc(s) xa were rcccivcd iiiLvrrectly preserved aud were adjustcd accordingly
in sample receiving with NA mL of circle one:H2SO4.HN05.HCL MOH using SR#
Time of preservatidan NA If snore than one presen�stive is ne &L please note in the comurents bet w.
Satmple($) NA were received Kith bubbles>G nun id (limiter.
Samrples(s j NA were received ritb TRC>0.5 mp'L Uf#19 is eta)and wcrc
adjusted accordingly in sample receiving with sodium tllimiinte(Na_S,,O,)with Urhiquc ID. '4A
C'oarnmcnts:
Qualtrax 10:56360 Pace's Analytical Servioes,LLC Page 1 of i
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 133 of 133
Page 16 of 16