WQ0011381_Modification_20240919

Initial Review
Reviewer nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
Permit Number (IR) * WQ0011381
Applicant/Permittee City of Hendersonville
Applicant/Permittee Address 145 5th Avenue East
Is the owner in BIMS? Yes No
Owner Type
Facility Name
County
Fee Category Minor
Is this a complete application?*
Yes No
Signature Authority
Signature Authority Title
Signature Authority Email
Document Type (if non -application)
Email Notifications
Is the facility in BIMS? Yes No
Municipal
City of Hendersonville Class A Residuals Program
Henderson
Does this need review by the hydrogeologist? * Yes No
Regional Office
CO Reviewer
Admin Reviewer
Fee Amount
Complete App Date
09119/2024
$348
Below list any additional email address that need notification about a new project.
Email Address
Comments to be added to email notfication
..........................................................................................................................................................................................................................................................................................................................
Comments for Admin
Comments for RO

Comments for Reviewer
Comments for Applicant

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
......................................................................................................................................................................................................................................................................................... ... ... ... ... ... .. ... ... ... ... ..
Name* Zachary Trammel
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
336-301-2626
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0011381
Has Current Existing permit number
Applicant/Permittee *
City of Hendersonville
Applicant/Permittee Address*
145 5th Avenue East
Facility Name *
City of Hendersonville Class A Residuals Program
Please provide comments/notes on your current submittal below.
Major modification to the City of Hendersonville Wastewater Treatment Facility's current Distribution of Class A Residuals permit to permit new
WWTF Biosolids Thermal Dryer project and increase the amounts of the final product to be treated and distributed per year. Note, the construction of
the WWTF Biosolids Thermal Dryer project that is the subject of this major modification application has been permitted under NPDES Authorization
to Construct permit number 025534A03. NCDEQ DWI project no. SRP-W-134-0060.
This resubmittal is being made at the request of the Division to reduce the number of pages in the application.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
DCARApplication_SRP-W-134-0060_2024.09.19.pdf 31.21MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617

Signature
/yjata4 � - OW/
Submission Date 9/19/2024

v
v MCKIM&CREED
September 19, 2024
North Carolina Department of Environmental Quality
Division of Water Resources
Non -Discharge Branch
Attn: Nathaniel Thornburg - 9t'' Floor, Office #942X
512 N. Salisbury Street, 9f Floor
Raleigh, NC 27604
ENGINEERS
SURVEYORS
PLANNERS
06496-0015
SUBJECT: Major Modification to Distribution of Class A Residuals
Permit WQ0011381 for the City of Hendersonville WWTF
Biosolids Thermal Dryer
Dear Mr. Nathaniel Thornburg:
We respectfully request approval for the Major Modification to the
Distribution of Class A Residuals Permit No. WQ0011381 for the
Hendersonville WWTF Biosolids Thermal Dryer project for the City of
Hendersonville's Wastewater Treatment Facility. This project involves a
facility modification to the Hendersonville WWTF consisting of the
construction of a new biosolids processing facility onsite and installation of a
new biosolids thermal dryer in the new facility.
The project consists of the construction of a new biosolids thermal drying
facility, the work for which includes, but is not limited to: demolition of
existing alkaline stabilization equipment including the lime day tank,
volumetric feeder, lime feed screw, solids processor, decking, stairs, and rail
system, and associated power and controls equipment; installation of new
dewatered cake conveyance equipment; installation of a new biosolids
thermal dryer system comprised of a dryer feed hopper, medium -
temperature direct fired belt dryer, dried biosolids discharge auger, dried
biosolids inclined screw conveyor, process blower, air heater, condenser,
8020 Tower Point Drive ductwork, cooling tower, cooling tower pump, wash stand, associated
piping, instrumentation, electrical and controls panels.
Charlotte. NC 28227
The project also includes modifications to the existing covered storage shelter
7 0 4 . 8 4 1 . 2 5 8 8 to enclose the southeast quadrant of the structure to house the new biosolids
thermal dryer and associated equipment, as well as enhancements to the
Fax [phone]
www.mckimcreed.com

covered storage shelter with new concrete push walls and curtain walls for
dried biosolids storage. Other tasks involve replacing the existing covered
storage shelter roofing, site grading, disposal of excess excavated materials
on -site, disposal of unsuitable excavated materials off -site at an approved
site, new concrete pavement, curb and gutter installation, new potable water
service piping to the new facilities, modifications to the existing potable
water service, installation of new natural gas service, new sanitary drainage
installation and connection to the existing in -plant sanitary sewer system,
modifications to existing utilities and utility structures, installation of new
electrical systems for the new equipment, integration of new instrumentation
and controls into the existing facility SCADA system, installation of a
photovoltaic (PV) solar energy system, and establishment of a site security
network with security cameras and door access control devices.
The estimated construction times are 540 consecutive calendar days from
Notice to Proceed (NTP) to Substantial Completion, and 600 consecutive
calendar days from NTP to Final Completion. Attached is the submittal
package necessary for the Major Modification to the Distribution of Class A
Residuals permit. We are submitting the following information:
• A check in the amount of $348.00 made payable to NCDEQ
• Distribution of Class A Residuals (DCAR 06-16) Application
o Attachment I: IV.5 - Onsite Storage Management Plan
• Current Distribution of Class A Residuals Permit No. WQ0011381
• Supporting Documentation
o Program Information
o Operation and Maintenance Plan
• Appendices
o Appendix A - Flow Diagrams
o Appendix B - City of Hendersonville WWTF Biosolids
Thermal Dryer Basis of Design Report: Section 4 - Biosolids
Management Market Analysis
o Appendix C - Product Information Sheet
o Appendix D - Preventative Maintenance Schedule
Residuals Source Certification (RSC 06-16) Form
o Attachment I: RSC Supporting Information
o Attachment II: 2023 Residuals Metals and Nutrients Analytical
Results
o Attachment III: 2024 Residuals Sampling Analytical Results
o Attachment IV: PFAS Sampling Analytical Results
o Attachment V: City of Lenoir's Lower Creek WWTP Residuals
Facility 2023 Annual Residuals Report
v� MgQM&CREED
ENGINEERS SURVEYORS PLANNERS

Note that City of Lenoir's Lower Creek WWTP Residuals Facility 2023
Annual Residuals Report includes analytical results and operational records
from 2023 demonstrating the Gryphon Environmental Model 1040 biosolids
thermal dryer's ability to meet the Class A biosolids requirements. This
equipment is nearly identical to the Gryphon Environmental Model 1050 that
is proposed to be installed at the Hendersonville WWTF. The primary
distinction being that the Model 1050 has a larger capacity than the Model
1040.
Please do not hesitate to contact me with any questions or comments by
phone at [phone] or by email at [e-mail].
Thank you,
McKim & Creed, Inc.
i
Zachary Trammel, PE
Regional Manager
Cc: Adam Steurer, PE, Utilities Director, City of Hendersonville
Garrett DeMoss, WWTF Manager, City of Hendersonville
Devin Owen, PE, Utilities Engineer, City of Hendersonville
Brent Detwiler, PE, City Engineer, City of Hendersonville
MCIQM&CREED
ENGINEERS SURVEYORS PLANNERS

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS
INSTRUCTIONS FOR FORM: DCAR 06-16 & SUPPORTING DOCUMENTATION
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted. the Applicant shall submit one original and two conies of the application and
suDDortine documentation
For more information, visit the Water Quality Permitting Section's Non-Di.scharve Permittinz Unit website
General — This application is for treatment, storage, transport, distribution, land application, and/or marketing of Class A (or Equivalent)
residuals under 15A NCAC 02T .1100.
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Distribution of Class A Residuals (FORM: DCAR 06-16):
® Submit the completed and appropriately executed Distribution of Class A Residuals (FORM: DCAR 06-16) form. Please do
not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to
the application may be made, as long as the attachments are numbered to correspond to the section and item to which they
refer.
® The project name should be consistent on the plans, specifications, etc.
® The Applicant's Certification on Page 3 of this form shall be signed in accordance with 15A NCAC 02T .0106(b). An alternate
person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 15A
NCAC 02T .0106(b).
® If this project is for a modification of an existing permit, submit one copy of the existing permit.
® Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to
operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units.
B. Application Fee (New and Major Modification Application Packages)
Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental
Quality (NCDEQ).
Facility Classification
Major (residuals permitted for distribution > 3,000 dry tons/year)
Minor (residuals permitted for distribution < 3,000 dry tons/year)
New Permit Major Modification r
$1,310 1 $395
$810
' - A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage;
adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted.
There is no fee for minor permit modifications.
C. Cover Letter (All Application Packages)
® List all items included in the application package, as well as a brief description of the requested permitting action.
INSTRUCTIONS FOR FORM: DCAR 06-16 Page] of 3

D. Program Information (All Application Packages)
® Provide a narrative explaining the following:
® How the materials will be handled and transported from where the residuals were produced to where it will be treated.
® How the residuals will be processed/treated (attach process flow diagram).
® How leachate collection will be handled.
® Where the residuals will be stored until processed.
® How the final product will be distributed (packaging, bulk, etc.)
® What nutrients or other constituents (i.e. nitrogen, phosphorous, aluminum, calcium, etc.) are used or recommended as the
limiting parameter for determination of residuals loading rate to ensure that it does not overload the soil and cause
contravention of surface water or groundwater standards, limit crop growth, or adversely impact soil quality.
® Attach a marketability statement detailing destinations and approximate amounts of the final product to be distributed.
® Provide either a label that shall be affixed to the bagged processed residual or an information sheet that shall be provided to the
person who receives the processed residual. The label or information sheet shall contain, at a minimum, the following
information:
® Name and address of the person who prepared the residual that is sold or given away.
® A statement that application of the residuals to the land shall be in accordance with the instructions on the label or
information sheet.
® A statement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered.
® A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored
residuals into any surface waters.
® Information on all applicable setbacks in accordance with 15A NCAC 02T .1108(b).
® A statement that the residuals shall be applied at agronomic or recommended rates for intended uses.
E. Detailed Plans and Specifications (Application Involving New or Changes to Treatment or Storage Units)
❑ Submit detailed plans and specifications that have been signed, sealed, and dated by a NC Professional Engineer per 15A
NCAC 02T .1104(a). Specifications for standard equipment may only be omitted for municipalities with approved standard
specifications, but use of the standard specifications must be noted on each sheet of the plans.
❑ Plans must include the following minimum items: a general location map, a topographic map, plan and profile view of the
residuals treatment and storage units as well as the proximity of the residuals treatment and storage units to other utilities and
natural features within 500 feet of all treatment and storage facilities, and detail drawings of all items pertinent to the residuals
treatment and storage units. Depict minimum separations required in 15A NCAC 02T .1108(a) on the plans.
❑ Specifications must include, at a minimum, the following for all items pertinent to residuals treatment and storage units:
description of materials to be used, methods of construction, quality of construction testing procedures to ensure the integrity
of the final product in accordance with 15A NCAC 02T .1104(a)(2)(B), including leakage and pressure testing as appropriate.
❑ Plans and specifications must not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR
CONSTRUCTION, etc.) that indicate that they are anything other than final plans and specifications. However, the plans and
specifications may be labeled with the phrase: FINAL DESIGN — NOT RELEASED FOR CONSTRUCTION.
F. Engineering Calculations (Application Involving New or Changes to Treatment or Storage Units)
❑ Submit all design calculations that have been signed, sealed, and dated by a NC Professional Engineer per 15A NCAC 02T
.1104(a).
G. Environmental Assessments (Maybe Required —See 15A NCAC 1C .0300)
❑ Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include
information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals
treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for
the construction of the subject facilities.
INSTRUCTIONS FOR FORM: DCAR 06-16 Page 2 of 3

H. Operation and Maintenance Plan (New and Renewal Application Packages)
® For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan.
® Submit the O&M Plan in accordance with 15A NCAC 02T .l 110 and include at a minimum:
® Operational functions; describe the operation of the program to show what operations are necessary for the program to function
and by whom the functions are to be conducted.
® Maintenance schedules; may include equipments calibration, maintenance of signs, etc.
® Safety measures; may include safety training program, manuals, signs, etc.
® Spill response plan; including control, containment, remediation, emergency contact information, etc.
® Inspection plan including the following information;
® Names and titles of personnel responsible for conducting the inspections.
® Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected
location(s) and inspection frequency are representative of the residuals management program.
® Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event
that noncompliance is observed.
® Sampling and monitoring plan including the following information;
® Names and titles of personnel responsible for conducting the sampling and monitoring.
® Detailed description of monitoring procedures including parameters to be monitored.
® Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow,
and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling
plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet
pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual
sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected
by cold temperatures.
ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL
SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS:
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY
DIVISION OF WATER RESOURCES
WATER QUALITY PERMITTING SECTION
NON -DISCHARGE PERMITTING UNIT
By U.S. Postal Service:
1617 MAIL SERVICE CENTER
RALEIGH, NORTH CAROLINA 27699-1617
TELEPHONE NUMBER: [phone]
By Courier/Suecial Deliverv:
512 N. SALISBURY STREET
RALEIGH, NORTH CAROLINA 27604
FAX NUMBER: [phone]
INSTRUCTIONS FOR FORM: DCAR 06-16 Page 3 of 3

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS
FORM: DCAR 06-16
I. APPLICANT INFORMATION:
1. Applicant's name: Citv of Hendersonville
Applicant type: ❑ Individual ❑ Corporation ❑ General Partnership E3 Privately -Owned Public Utility
❑ Federal ❑ State ® Municipal El County
Signature authority's name per 15A NCAC 02T .0106: John Comiet Title: AMA"
Applicant's mailing address: 145 5th Avenue East
City: Hendersonville State: NC Zip: 28792-
Telephone number: [phone] Email Address: iconnet(&,hvinc.gov
2. Consultant's name: Zachary Trammel. PE License Number (for P.E.): 046291
Affiliation: On Staff ® Retained (Firm: McKim & Creed. Inc.)
Consultant's mailing address: 8020 Tower Point Drive
City: Charlotte State: NC Zip: 28227-
Telephone number: [phone] Email Address: ztrammel(&.mckimcreed.com
3. Fee submitted: $348.00 (See Instruction B)
II. PERMIT INFORMATION:
1. Application is for (check all that apply): Q new, ® modified, ❑ renewed permit
2. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number: W00011381
Date of most -recently issued pen -nit: 02/01 /2020
Date of most -recently certified Attachment A (if different than the permit): 11/05/2019
III. FACILITY INFORMATION:
1. Name of residuals processing facility: Citv of Hendersonville Wastewater Treatment Facility
City: Hendersonville State: NC Zip: 28792-
Coordinates: Latitude: 35' 21' 1 3" Longitude: 82' 27' 54"
Datum: NAD-83 Level of accuracy: 6"
Method of measurement: GPS
County where facility is located: Henderson
2. Facility contact (person familiar with residuals preparation):
Name: Garrett DeMoss Title: WWTF Sunerintendent
Mailing address: 99 Balfour Road
City: Hendersonville State: North Carolina Zip: 28791-
Telephone number: [phone] E-mail address: udemossahvinc.cov
FORM: DCAR 06-16 Page 1 of 3

3. Is the residual process facility also the generator? 10 Yes; [a No
If No, please specify delivery frequency and quantity of residual to be processed:
4. Length of residuals storage at facility: 73.5 (minimum. at 2045 max. month conditions) days (Note: the Division requires
minimum 30 days storage in units that are separate from treatment system, i.e. not in clarifiers, aeration basins, etc.)
IV. RESIDUALS QUALITY INFORMATION:
1. Specify how these residuals will be distributed:
IN sold or given away in bags or other containers; IN lawn (bulk); H home garden (bulk);
Ca other (explain); , �
Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a
load capacity of one metric ton or less.
2. Complete the following if residuals are to be mixed with other materials:
Type of Materials
None
Amounts to be added
per 1.0 dry ton of residuals (dry ton)
3. Approximate amounts of the residuals received and processed at the facility: 1,770.25 dry tons per year.
4. Approximate amounts of the final product (processed residuals) to be distributed: 1,770.25 dry tons per year.
5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and
maximum storage times prior to distribution): See Attachment I
6. Does the facility have a stormwater management plan? ® Yes; El No
Explain whether the treatment and storage areas are under roof or how stormwater runoff will be handled: The treatment and
storage areas are under a roof and the floors are stoned to drains. All drains collecting stormwater runoff, leachate, or water,
from equipment/floor washdown that may be in contact with unstablized residuals or dried biosolids will be connected to the,
in -plant drain system to be returned to the Influent Pumnine Station for treatment prior to discharge.
V. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source)
Complete and submit the attached Residuals Source Certification and all associated documentation.
0
RSC 06-16.doc
FORM: DCAR 06-16 Page 2 of 3

Professional Engineer's Certification: (Application Involving New or Changes to Treatment or Storage Units)
I, Zachary Trammel. PE I attest that this application for
Citv of Hendersonville Wastewater Treatment Facilitv
has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge
the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal package
may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have reviewed
this material and have judged it to be consistent with the proposed design.
North Carolina Professional Engineer's Seal, Signature, and Date:
Applicant's Certification:
2y
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper
closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active
compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105.
Yes 0 No, Explain :�_
I, John Connet
(Signature Authority's Name — PLEASE PRINT)
attest that this application for Citv of Hendersonville Wastewater Treatment Facilitv
(Facility Name)
Citv Manacer
(Title)
has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources
may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically
granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action,
which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water
Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed
and that if all required supporting information and attachments are not included, this application package will be returned to me as
incomplete.
Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.613, any person who knowingly makes any false
statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to
exceed $10,000 as well as civil penalties up to $25,000 per violation.
Signature: John Connet(Jun 23, 2024 la t3 Eon
Date: 23/06/2024
FORM: DCAR 06-16 Page 3 of 3

Distribution of Residual Solids - Permit
Application WWTP Thermal Dryer
Final Audit Report 2024-06-23
Created: 2024-06-21
By: Adam Steurer ([e-mail])
Status: Signed
Transaction ID: CBJCHBCAABAA6_UvlFxofArzuUxrOMyVF7vEbm_w4j2p
"Distribution of Residual Solids - Permit Application WWTP Ther
mal Dryer" History
Document created by Adam Steurer ([e-mail])
2024-06-21 - 7:16:42 PM GMT
-- Document emailed to John Connet [e-mail]) for signature
2024-06-21 - 7:17:03 PM GMT
Email viewed by John Connet [e-mail])
2024-06-23 - 6:12:10 PM GMT
Document e-signed by John Connet [e-mail])
Signature Date: 2024-06-23 - 6:13:05 PM GMT - Time Source: server
�i Agreement completed.
2024-06-23 - 6:13:05 PM GMT
a Adobe Acrobat Sign

Attachment I: IV.5 - Onsite Storage Manasement Plan
Following the completion of the modifications to the existing Covered Storage Shelter, the
partially enclosed storage area will have approximately 10,500 ft2 of space available for storage
of dried biosolids. The biosolids thermal dryer is designed to produce up to 9.2 dry tons per day
(DT/d) of dried biosolids, operating 24 hours per day 5 days per week at future 2045 maximum
month conditions. This equates to a dried biosolids product rate of 10 wet tons per day (WT/d),
or 800 ft3/d, and 50 WT/week or 4,000 ft3/week, assuming a total solids content of 92% per the
dryer equipment basis of design, a dried biosolids bulk density of 251bs/ft3, and a 24 hour per
day 5 day per week operating schedule. Based on this information, the Covered Storage Shelter
will provide up to 73.5 days of dried biosolids storage at 2045 maximum month design
conditions assuming an average stockpile height of 4-ft, which is a conservative assumption for
dried biosolids. The estimated annual average dried biosolids production rate under base year
(2025) conditions is expected to be 2.82 WT/d or 225.8 ft3/d (normalized to an average daily
rate). Under base year annual average conditions, the Covered Storage Shelter will provide up
to 26.6 weeks or 186 days of storage assuming an average stockpile height of 4-ft.

ROY COOPER,
Governor
MICHAEL S. REGAN
Secretary
LINDA CULPEPPER
Direcrflr
NORTH CAROLINA
Environmental Quality
November 5, 20I9
LEA, SMITH — UTILITIES DIRECTOR
CITY OF HENDERSONVILLE
305 WiLLIAMs STREET'
HENDERSONVILLE, NORTH CAROLINA 28792
Dear Mr. Smith:
RECEIVED
NOV 13 2019
Hendersonville
Water and Sewer
Subject: Permit No. WQ0011381
City of Hendersonville DCAR
Distribution of Class A
Residuals
Henderson County
In accordance with your permit renewal request received August 7, 2019, and subsequent additional
information received November 5, 2019, we are forwarding herewith Permit No. WQ0011381 dated
November 5, 2019, to the City of Hendersonville for the operation of the subject residuals management
progl•am. Please note that this renewed permit shall become effective on February 1, 2020 (i.e., the day
after the expiration date of the existing permit).
Modifications to the subject permit are as follows: The permitted tonnage of Class A residuals that
is allowed in this permit has been dropped to zero dry tons per year. In order to for this permit to be able to
distribute Class A residuals, the Permittee shall submit a major modification request in accordance with
15A NCAC 02T .1104.
This permit shall be effective from February 1, 2020 through September 30, 2025, shall void Permit
No. WQ0011381 issued October 1, 2014, and shall be subject to the conditions and limitations as specified
therein. The Permittee shall submit a renewal application no later than April 3, 2025.
Please pay particular attention to the monitoring requirements listed in Attachment A for they may
differ from the previous permit issuance. Failure to establish an adequate system for collecting and
maintaining the required operational information shall result in future compliance problems.
The Division has removed the following permit conditions since the last permit issuance dated
October 1, 2014:
Old Condition 11.7- — This condition has been removed because this is not a surface disposal
unit permit.
Old Condition U.S. and 11.9. — These setback conditions have been consolidated into the new
Condition H.7.
OId Condition l[II.7. — This condition has been removed because it is covered under condition
III.S.
➢ Old Condition III.8.h. — Soil pH requirements for land application have been removed.
Yrnr� � �� North Caralirra Department of Emirptimerxal Quality 1 Division of Water Resources
��Jjl� 512 North Salisbur Street ! 1617 Mai Service Center I Race h North Carolina 27699-T617
L �.—'!+ 919.701900o

Mr. Lee Smith
November S, 2019
Page 2 of 2
Old Condition. 1I1.9. and 111.10. — These conditions have been removed because Utilization
Agreements are no longer required.
➢ Old Condition IV.b.f. — This condition has been removed.
➢ Old Condition V 1.2. —This condition has been removed because the permit is not voidable.
The following permit conditions are new since the last permit issuance dated October 1, 2014,
Condition 11.7. — All setbacks applicable to the I SA NCAC 02H .02190) rules at the time of
permitting have been added to the treatment and storage site setbacks. Setbacks to land applied
bulk residuals have been updated to meet the current 15A NCAC 02T .I 108 titles.
➢ Condition 111.6. — Class A residuals may be staged at the Iand application site for up to 30 days
for biological residuals and 60 days for non -biological residuals.
➢ Condition IIl_S.l. — Residual land application may not occur if the land application sites are
located within a WS- I watershed pursuant to I 5A NCAC 02.B .0212 or within the Critical area
of a WS-II, `IdS-111, or WS-IV watershed.
➢ Condition VI.8. — This permit shall not be renewed if the Permittee or any affiliation has not
paid the required annual fee.
Attachment A —The permitted tonnage of Class A residuals that is allowed in this permit has
been dropped to zero dry tons per year.
If any parts, requirements or limitations contained in this permit are unacceptable, the Permittee
has the right to request an adjudicatory hearing upon written request within 30 days following receipt of
this permit. This request shall be in the forin of a written petition, conforming to Chapter I SOB of the North
Carolina General Statutes, and filed with the Office of Administrative Hearings at 6714 Mail Service
Center. Raleigh, NC 27699-6714. Otherwise, this pemnit shall be final and binding.
If you need additional information concerning this permit, please contact Erick Saunders at (919)
707-3659 or erickson.saunders(t'ynedenr.Rov.
Sincerely,
inda Culpepper, Director
Division of Water Resources
cc; Henderson County Health Department (Electronic Copy)
Asheville Regional Office, Water Quality Regional Operations Section (Electronic Copy)
Laserfiche File (Electronic Copy)
Digital Perinit Archive (Electronic Copy)
Central Files

NORTH CAROLINA
ENVIRONMENTAL, MANAGEMENT COMMISSION
DEPARTMENT OF ENVIRONMENTAL QUALrff
RALEIGH
DISTRIBUTION OF CLASS A RESIDUALS PERMIT
In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as
amended, and other applicable Laws, Rules, and Regulations
PERMISSION IS HEREBY GRANTED TO
City of Hendersonville
Henderson County
FOR THE
operation of a residuals management program for the City of Hendersonville and consisting of the
distribution of Class A residuals generated by the approved facility listed in Attachment A, with no
discharge of wastes to surface waters, pursuant to the application received August 7, 2019, subsequent
additional information received November 5, 2019, and in conformity with other supporting data
subsequently filed and approved by the Department of Environmental Quality and considered a part of this
permit. The disposal of residuals is regulated under Title 40 Code of Federal Regulations Part 503. This
permit does not exempt the Permittee from complying with. Federal Regulation 40 CFR Part 503.
This permit shall be effective from February 1, 2020 through September 30, 2025, shall void Permit No.
WQ0011381 issued October 1, 2014, and shall be subject to the following conditions and limitations:
I. SCHEDULES
1. The Permittee shall request renewal of this permit on Division -approved forms no later theui April 3,
2025. [15A NCAC 02T .0105(b), 02T .0109]
II. PERFORMANCE STANDARDS
The Permittee shall maintain and operate the subject residuals management program so there is no
dischar ,c to surface waters, nor any contravention of groundwater or, surface water standards. In the
event the residuals management program fails to perform satisfactorily, including the creation of
nuisance conditions due to improper operation and maintenance, the Permittee shall immediately cease
distributing residuals, take immediate corrective actions, and contact the Asheville Regional Office
supervisor. [15A NCAC 02T .0108(b)(1)(A)]
2. This permit shall not relieve the Pernnittee of their responsibility for damages to groundwater or surface
water resulting from the operation of this residuals management program. [15A NCAC 02T
.0108(b)(1)(A)I
3. Only residuals generated by the facility listed in Attachment A are approved for distribution in
accordance with this permit. [15A NCAC 02T .1101]
WQ0011381 Version 4.0 Shell Version 190710 Page 1 of 10

4. Pollutant concentrations in distributed residuals shall not exceed the following Ceiling Concentrations
or Monthly Average Concentrations, on a dry weight basis:
Parameter (+
1
Arsenic
Cadmium 1�
- Copper
Lead
Mercury
Ceiling Concentration Monthly Average
Concentration
Molybdenum
Nickel
I Selenium
Zinc
[ 15A NCAC 02T . 1105(a), 02T .1105(c)]
(mglkg)
- 75 - -
85
4,300
940
57
75
420
100
7,500
(mg1k9)
41 - -
39
1,500
300
17
N/A
420
100
2,800
5. Class A biological residuals shall meet the pathogen reduction requirements in 15A NCAC 02T
.1106(a). Exemptions to this requirement shall be specified in Attachment A. [I5A NCAC 02T
.1106(a), 02T .1106(d)]
6. Class A biological residuals shall meet one of the vector attraction reduction alternatives in 15A NCAC
02T .1107(a). Exemptions to this requirement shall be specified in Attachment A. [15A NCAC 02T
.1107(a), 02T .1107(c)]
7. The facilities and sites herein were permitted per the following setbacks:
a. Setbacks for Class A land application sites are as follows (all distances in feet):
Liquid
Cake
Residuals Residuals 1
i.
Each private or public water supply source:
100
100
ii.
Surface waters such as intermittent and perennial streams, perennial
waterbodies, and wetlands:
I0D
25
HE
Surface water diversions such as ephemeral streams, waterways, and
ditches:
25
0
iv.
Groundwater lowering ditches where the bottom of the ditch
intersects the SHWT:
25
0
v.
Each well with exception of monitoring wells:
100
100
vi.
Bedrock outcrops:
25
0
' Unless otherwise noted in Attachment A, `cake" residuals are those that have greater than 15%
solids by weight and can be stacked without flowing, as well as can be handled, transported
and spread as a solid (e.g., using a backhoe, front end loader, slinger spreader, broadcast
spreader or other equipment designed for handling solid materials) without leaving any
significant liquid fraction behind.
[ 15A NCAC 02T .1 I08(b)]
WQOO 11381 Version 4.0 Shell Version 190710 Page 2 of 10

8. Residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in exceedance of
agronomic rates. Appropriate agronomic rates shall be calculated using expected nitrogen requirements
based on the determined Realistic Yield Expectations (RYE) using any of the following methods:
a. Division's pre -approved site specific historical data for specific crop or soil types by calculating
the mean of the best three yields of the last five consecutive crop harvests for each field.
b. North Carolina Historical Data for specific crop and soil types as provided by North Carolina State
University Department of Soil Science (http:/inutrients.soil.ncsu.eduivields/index.vilu). A copy
shall be kept on file and reprinted every five years in accordance wi#h Condition IV.6.
c. If the RYE cannot be determined using methods (a) or (b) above, the Permittee may use the RYE
and appropriate nutrient application rates reported in any of the following documents:
i. Crap management plan as outlined by the local Cooperative Extension Office, the North
Carolina Department of Agriculture and Consumer Services, the Natural Resource
Conservation Service, or other agronomist_
ii. Waste Utilization Plan as outlined by the Senate Bill 12I7 Interagency Group - Guidance
Document: Chapter I
(httn://www.ncay.r.,aov/SWC/techtdocuments/9th—Guidance—Doc--1 001 09.odf).
iii. Certified Nutrient Management Plan as outlined by the Natural Resources Conservation
Services (NRCS). These plans must meet the USDA-NRCS 590 Nutrient Management
Standards(ftc://ftD-fc.sc,.ejzov.usda.pov/NHQ/practice-standards/statidards/590.odf).
d. If the RYE and appropriate nutrient application rates cannot be determined, the Permittee shall
contact the Division to determine necessary action.
[ I 5A NCAC 02T .1 I 09(a)(1)(K)]
9. Prior to distributing CIass A residuals that have a sodium adsorption ratio (SAR) of 10 or higher. the
Permittee shall obtain and implement recommendations from at least one of the following. the local
Cooperative Extension Office; the Department of Agriculture and Consumer Services; the Natural
Resource Conservation Service; a North Carolina Licensed Soil Scientist; or an agronomist. The
recommendations shall address the sodium application rate, soil amendments (e.g., gypstun, etc.), or a
mechanism for maintaining site integrity and conditions conducive to crop growth. The Permittee shall
maintain written records of these recommendations and details of their implementation. The Pernsittee
shall notify third -party entities of the effects of a high SAR content residuals on their receiving sites.
[I5ANCAC 02T .0108(b)(I)(A)]
WQOO11391 Version 4.0 Shell Version 190710 Page 3 of 10

III_ OPERATION AND MAIlIUNANCE REOTIIREWNTS
1. The Permittee shall operate and maintain the residuals management program as a non -discharge system,
[I5A NCAC 027 .1100]
2. The Pennittee shall maintain a Division -approved Operation and Maintenance Plan that shall include:
a. Description of the program, and associated facilities and equipment, in sufficient detail to show
what operations are necessary for the program to function and by wham the functions are to be
conducted;
b. Description of anticipated maintenance of facilities and equipment associated with the program;
c. Include provisions for safety measures, including restriction of access to sites and equipment;
d. Spill control provisions:
i. Response to upsets and bypasses including control, containment, and rernediation; and
ii. Contact information for plant personnel, emergency responders, and regulatory agencies;
c. Detailed inspection procedures:
L Names or titles of personnel responsible for conducting inspections;
ii. Frequency and location of inspections, and procedures to assure that the selected locations and
inspection frequency are representative of the residuals management program; and
iii. Description of record keeping and actions to be taken by the inspector in the event that
noncompliance is observed;
f. Detailed sampling and monitoring procedures:
i. Names or titles of personnel responsible for conducting sampling and monitoring;
ii. Description of monitoring procedures including parameters to be monitored; and
iii. Sampling frequency and procedures to assure that representative samples are collected.
Fluctuation in temperature, flow, and other operating conditions can affect the quality of the
residuals gathered during a particular sampling event. The sampling plan shall account for any
foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to
meet pathogen and vector attraction reduction requirements.
[I5A NCAC 02T .I 110(a)]
I Upon the Water Pollution Control System Operators Certification Commission's (WPCSOCC)
classification of the residuals management program, the Permittee shall designate and employ a
certified operator in responsible charge (ORC), and one or more certified operators as back-up ORCs.
The ORC or their back-up shall visit the facilities in accordance with 15A NCAC 48G 0204 and shall
comply with all other requirement in 15A NCAC 08G 0204. 115A NCAC 02T .4117, 08G .0204]
4. The Permittee shall ensure that a copy of this permit and the Division -approved Operation and
Maintenance Plan is available when land applying bulk Class A residuals. [15A NCAC 42T .1110(b)]
5. The Permittee shall ensure that spill control provisions are available when transporting or land applying
bulk Class A residuals. [15A NCAC 02.T .1110(a)(4)]
6. Class A residuals may be staged at the land application site for up to 30 days for biological residuals
and 60 days for non -biological residuals. CIass A residuals shall be stared or staged in a manner to
prevent runoff of leachate and other wastewaters generated. [ 15A NCAC 02T . I 110(e), 02T .1110(d)]
7. Adequate measures shall be taken to prevent wind erosion and runoff from the bulk Class A residual
land application sites. [I5A NCAC 02T .0108(b)(1)(A)]
WQGO11391 Version 4.0 SheIl Version 190714 Page 4 of 10

8. Bulk Class A residuals shall not be land applied under the following conditions;
a. If the residuals are likely to adversely affect a threatened or endangered species listed under section
4 of the Endangered Species Act or its designated critical habitat;
b. If the application causes nuisance conditions;
c. If the land fails to assimilate the balk residuals or the application causes the contravention ofsurface
water or groundwater standards;
d. If the land is flooded, frozen, or snow-covered, or is otherwise in a condition such that runoff of
the residuals would occur;
e. Within the IWyear flood elevation, unless the residuals are injected or incorporated within a 24-
hour period following a residuals land application event;
f. During precipitation events, or within 24 hours following a rainfall event of 0.5 inches or greater
in a 24-hour period;
g. If the slope of the land is greater than 1011/o when liquid residuals are surface applied, or if the slope
of the land is greater than 18% when liquid residuals are injected or incorporated;
h. Ifthe land does not have an established vegetative cover crop unless the land is a Division -approved
no -till site, or the residuals are injected, or incorporated within a 24-hour period following the
application of residuals;
i. If the vertical separation of the seasonal high water table and the depth of residuals application is
less than one foot;
j. If the vertical separation of the depth to bedrock and the depth of residuals application is Iess than
one foot;
k. If the application exceeds agronomic rates; or
1. If the land application sites are located within a WS-I watershed pursuant to 15A NCAC 02B ,0212
or within the Critical Area of a WS-11 pursuant to Sub -Item (4)(g) of Rule 15A NCAC 02B .0212,
or within the Critical Area of a WS-III or WS-IV watershed pursuant to Sub -Item (4)(h) of Rules
15A NCAC 02B .02.15, and .0216.
[I5A NCAC 02T ,I 109(a)(I), 02T .1I09(b)]
9. The Permittee shall notify all third -party entities receiving bulk Class A residuals that land application
activities occurring on the third-party's property shall meet the requirements in 15A NCAC 02T
.1108(b) and 02T .1109(a)(1) (i.e., Conditions 1I.7.a. and III.B., respectively). [15A NCAC 02T
.1 103(a)(4), 02T _1103(a)(5)]
10. Bagged or other container Class A residuals shall have an affixed label or an information sheet provided
to the person receiving the Class A residuals. The label or information sheet shall contain the following:
a. The name and address of the person who prepared the residuals;
h. A statement that residual land application is prohibited except in accordance with the instructions
on the label or information sheet; _
c. A statement that the residuals shall be applied at agronomic rates and recommended rates for its
intended use.
[I 5A NCAC 02T. I 109(c)]
11. The Permittee shall not distribute hulk Class A residuals to any person or entity known to be applying
residuals contrary to the conditions of this permit. The Perm ittee shall report to the Asheville Regional
Office any person or entity known to be applying residuals contrary to the conditions of this permit.
[15A NCAC 02T .0108(b)(i)(A)]
WQ00113 81 Version 4.0 Shell Version 190710 Page 5 of 10

IV. MOWORING AND REPORTING REOUIREMENTS
1. The Permittee shall conduct and report any Division required monitoring necessary to evaluate this
program's impact on groundwater and surface water. [ 15A NCAC 02T .0108(c))
2. The residuals from each source generating facility shall be analyzed to demonstrate they are non-
hazardous under the Resoumc Conservation and Recovery Act (RCRA). Residuals that test or are
classified as a hazardous or toxic waste under 40 CFR Part 261 shall not be land applied. The analyses
(i.e., eorrosivity, ignitability, reactivity, and toxicity characteristic leaching procedure (TCLP)) shall be
performed at the frequency specified in Attachment A, and the Permittee shall maintain these results
for five years. Any exemptions from the requirements in this condition shall he specified in Attachment
A. The TCLP analysis shall include the following parameters, and the Federal regulatory level (mg/L)
is in parentheses:
iArsenic (5.0) 1,4-Dichlorobenzene (7.5) Nitrobenzene (2.0)
Barium (100.0) 1,2-Dichloroethane (0.5) Pentachlorophenol (100.0)
Benzene (0.5) 1, 1 -Dichloroethylene (0.7) Pyridine (5.0)
Cadmium (1.0) 2,4-Dinitrotoluene (0.13) Selenium (I.0)
Carbon tetrachloride (0.5) Endrin (0.02) Silver (5.0)
Chlordane (0.03)
Chlorobenzene(100.0)
Chloroform (6.0)
Chromium (5.0)
m-Cresol (200.0)
o-Cresol (200.0)
p-CresoI (200.0)
Cresol (200.0)
2,4-D (10.0)
Heptachlor (and its epoxide)
(0.008)
Hexachlorobenzene (0.I 3)
Hexachlorobutadiene (0.5)
- Hexachloroethane (3.0)
Lead (5.0)
Lindane (0.4)
Mercury (0-2)
Methoxychlor (10.0)
Meihyl ethyl ketone (204.0)
Tetrachloroethylene (0.7)
Toxaphene (0.5)
Trichloroethylene (0.5)
2,4,5-Trichlorophenol (400.0)
2,4,6-Trichlorophenol (2.0)
2,4,5-TP (Silvex) (1.0)
Vinyl chloride (0.2)
Once the residuals have been monitored for two years at the frequency specified in Attachment A, the
PermEittee may submit a permit modification request to reduce the frequency of this monitoring
requirement. In no case shall the monitoring frequency be less than once per permit cycle.
[15A NCAC 13A .0102(b), 02T .1101, 02T .11051
WQ0411381 Version 4.0 Shell Version 190710 Page 6 of 10

3. The residuals from each source generating facility shall be analyzed at the frequency specified in
Attachment A, and the Permittee shall maintain the results for a minimum
of five years. Each analysis
shall include the following parameters:
Aluminum- - -
Mercury
Potassium
Ammonia -Nitrogen —
-
- - Molybdenum
-
Selenium
Arsenic
-
Nickel
- - - - -
Sodium
Cadmium
Nitrate -Nitrite Nitrogen
Sodium Adsorption Ratio
- -
- (SAR) - -
Calcium
Percent Total Solids
` KN
Copper
pH
—
Zinc
- Lead
Phosphorus
Magnesium
Plant Available Nitrogen
-�
(by calculation)
[I5A NCAC 02T .I 1011
4. Residuals shall be monitored for compliance with pathogen and vector attraction reduction
requirements at the frequency specified in Attachment A. The monitoring results shall specify the
stabilization process utilized, and demonstrate compliance with the Class A pathogen reduction
requirements in 15A NCAC 02T .1I06(a), and one vector attraction reduction requirement in I5A
NCAC 02T .1107(a) shall be met. Any exemptions from the requirements in this condition shall be
specified in Attachment A. [15A NCAC 02T .1105(a), 02T .1107(a), 02T .1111(c)]
5. Representative samples of residuals that are prepared for distribution shall be collected and analyzed.
[15A NCAC 02T .I I I i(a)]
6. The Permittee shall maintain records for all bulk Class A residual distribution events. These records
shall include the following:
a. Residuals source (as listed in Attachment A);
b. Date of distribution;
c. Name and address of residuals recipient;
d. Volume of residuals distributed to each recipient; and
e. Intended use of residuals.
[15A NCAC 02T .0109(c)]
7. one hard copy and one electronic copy of an annual report shall be submitted on or before March is'.
The annual report shall meet the requirements described in the Instructions for Residuals AnoIication
Annual Revortin2 Forms. Instructions for reporting and annual report forms are available at
httn:l/deci.ne.iEov/about/divisions/water-i-esources/water-resources-nermits/wWewater-branch/non-
discharee_-i3ermittine-unitlrenorting-forms, or can be obtained by contacting theNon-Discharge Branch
directly. The annual report shall be submitted to the following address:
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina27699-1617
[I 5A NCAC 02T .1111(d)]
WQEl011381 Version 4.0 ShelI Version 190710 Pane 7 of 10

8. Noncompliance Notification
The Pertnittee shall report to the Asheville Regional Office, telephone number [phone], within
24 hours of first knowledge of the:
a. Any process unit failure (e.g., mechanical, electrical, etc.) rendering the facility incapable of
adequate residual treatment.
b. Any failure resulting in a discharge to surface waters.
c. Any time self -monitoring indicates the program has gone out of compliance with its permit
Iimitations.
d. Distribution of residuals abnormal in quantity or characteristic.
e. Any discharge from a vehicle or piping system transporting residuals.
Emergencies requiring reporting outside normal business hours shall call the Division's Emergency
Response personnel at telephone number [phone], [phone], or [phone], All
noncompliance notifications shall file a written report to the Asheville Regional Office within five days
of first knowledge of the occurrence, and this report shall outline the actions proposed or taken to ensure
the problem does not recur. [l5A NCAC 02T .0108(b)(1)(A)]
V. INSPECTIONS
1. The Permittee shall perform inspections and maintenance to ensure proper operation of the Pennittee's
storage and distribution facilities. [15A NCAC 02T .1110(f)]
2. The Permittee shall inspect the Pertnittee's residuals processing, storage, and transport facilities to
prevent malfunctions, facility deterioration, and operator errors that may result in discharges of wastes
to the environment, threats to human health, or public nuisances. The Permittee shall maintain an
inspection log that includes the date and time of inspection, observations made, and maintenance,
repairs, or corrective actions taken. The Permittee shall maintain this inspection log for a period of five
years from the date of inspection, and this log shall be trade available to the Division upon request.
[l5A NCAC 02T 0108(b)(1)(A), 02T .1110(f)]
Division authorized representatives may, upon presentation of credentials, enter and inspect any
property, premises, or place related to the distribution sites or facilities permitted herein at any
reasonable time for determining compliance with this permit. Division authorized representatives may
inspect or copy records maintained under the terms and conditions of this permit, and may collect
groundwater. surface water, or leachate samples. [G.S. 143-215.3(a)(2))
WQOO11381 Version 4.0 Shell Version 190710 Page 8 of 1€7

VZ. GENERAL CONDITIONS
1. Failure to comply with the conditions and limitations contained herein may subject the Permittee to a
Division enforcement action. [G.S. 143-215.6A, 143-2I5.613, 143-215.6C]
2. This permit is effective only with respect to the nature and volume of wastes described in the permit
application, and Division -approved plans and specifications. [G.S. 143-2IS. 1(d)]
3. Unless specifically requested and approved in this permit, there are no variances to administrative codes
or general statutes governing the construction or operation of the facilities permitted herein. [15A
NCAC 02T ,01 05(n)]
4_ The issuance of this permit does not exempt the Permittee from complying with all statutes, rules,
regulations, or ordinances that other jurisdictional government agencies (e.g., local, state, and federal)
may require. [15A NCAC 02T .Ol05(c)(6)]
5. If the permitted residuals program change ownership, or the Permittee changes their name. the
Perinittee shall submit a permit modification request on Division -approved forms. The Permittee shall
comply with all terms and conditions of this permit until the permit is transferred to the successor -
owner. [G.S. 143-215.1(d3)]
6. This permit is subject to revocation or modification upon 60-day notice from the Division Director. in
whole or part for:
a. violation of any terms or conditions of this permit or Administrative Code Title 15A Subehapter
D2T;
b. obtaining a permit by misrepresentation or failure to disclose all relevant facts;
c. the Pcrmittee's refusal to allow authorized Department employees upon presentation of credentials:
i. to enter the Permittee's premises where a system is located or where any records are required
to be kept;
ii. to have access to any permit required documents and records;
iii. to inspect any monitoring equipment or method as required in this permit; or
iv. to sample any pollutants;
d. the Permittee's failure to pay the annual fee for administering and compliance monitoring; or
e. a Division determination that the conditions of this permit are in conflict with North Carolina
Administrative Code or General Statutes.
[I5A NCAC 42T .D110]
WQ001138l Version 4.0 Shell Version 190710 Page 9 of 10

7. Unless the Division Director grants a variance, expansion of the facilities permitted herein shall not
occur if any of the following apply:
a. The Permittee or any parent, subsidiary, or other affiliate of the Permittee has been convicted of
environmental crimes under G.S, 143-215.613, or under Federal law that would othenvise be
prosecuted under G.S. 143-215.6B, and all appeals of this conviction have been abandoned or
exhausted.
b. The Perrnittee or any parent, subsidiary, or other affiliate of the Perrrlittee has previously abandoned
a wastewater treatment facility without properly closing the facility.
c. The Permittee or any parent, subsidiary, or other affiliate of the Pennittee has not paid a civil
penalty, and all appeals of this penalty have been abandoned or exhausted.
d. The Pennittee or any parent, subsidiary, or other affiliate of the Permittee is currently not compliant
with any compliance schedule in a permit, settlement agreement, or order.
e. The Permittee or any parent, subsidiary, or other affiliate of the Permittee has not paid an annual
fee.
[15A NCAC 02T .0120(b), 02T .0120(d)]
8. This pernlit shall not be renewed if the Permittee or any affiliation has not paid the required annual fee.
[ I SA NCAC 02T .0120(c)]
Permit issued this the 51' day of November 2019
NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION
,,,;;Linda Culpepper, Director
Division of Water Resources
By Authority of the Environmental Management Commission
Permit Number WQ001I381
WQ0011381 Version 4.0 Shell Version 190710 Pave 10 of 10

ATTACHMENT A — APPROVED RESIDUAL SOURCES
Certification Date: November 5, 2019
City of Hendersonville
Permit Number: WQ0011381 Version: 4.0
Monitoring
I Monitoring
Monitoring
Maximum
Owner Facility Name County permit
Dry Tons Frequency for
Frequency for
Frequency for Approved
Pathogen & Mineralization
RBiologicalResiduals
Number Residuals per Year haracNon-brardou i
Characteristics
f Metals and 5
a
Nutrients
Vector Attraction Rate
I+
Reduetionsas
City of I-iendersonville City of Hendersonville WWTP Henderson WQ0011381 Yes 0 Annually
See Table Below
See Table Below -
- - - = -
Total 0
--_ �
-- -
� -
I
1. Maximum Dry Tons per Year is the amount of residuals approved for land application from each permitted facility.
2. Analyses to demonstrate that residuals are non -hazardous (i.e., TCLP, ignitability, reactivity, and corrosivity) as stipulated under permit
Condition IV.2.
3. Testing of metals and nutrients as stipulated under permit Condition 1V.3.
4. Analyses of pathogen and vector attraction reductions as stipulated under permit Condition IVA.
5. Monitoring frequencies are based on the actual dry tons applied per year using the table below, unless specified above.
Dry Tons Applied Monitoring Frequency
Dry Tons Applied (metric tons)
(short tons per year) (40 CPR 503 and 15A NCAC 02T
< 290
< 319
Once per year (Annually)
> 290 to < 1,500
319 to < 1,650
f Once per quarter (4 x Year)
> 1,500 to < 15,000
? 1,650 to < 16,500
Once per 60 days (6 x Year)
15,000
a 16,500
Once per month (12 x Year)
If no land application events occur during a required sampling period (e.g., no land application occur during an entire year when annual monitoring is required), then no sampling data is
required during the period of inactivity. The annual report shall include an explanation for missing sampling data. Those required to submit the annual reportto United States Environmental
Protection Agency (US EPA) may be required to make up the missed sampling. Contact the US EPA for additional information.
WQ0011381 Version 4.0 Attachment A Page 1 of l

Hendersonville WWTF Biosolids Thermal Dryer
NCDEQ DWR Non -Discharge Unit
Distribution of Class A Residuals (DCAR) Application
SUPPORTING DOCUMENTATION
1. PROGRAM INFORMATION
a. Project Narrative
b. Marketability Statement
c. Product Information Sheet
2. OPERATION AND MAINTENANCE PLAN
APPENDICES:
APPENDIX A — Flow Diagrams
a. Existing WWTF Flow Diagram
b. Proposed WWTF Flow Diagram
APPENDIX B — City of Hendersonville WWTF Biosolids Thermal Dryer
Basis of Design Report: Section 4 - Biosolids Management Market Analysis
APPENDIX C — Product Information Sheet
APPENDIX D — Preventative Maintenance Schedule
Initially Submitted:
07/01/2024
Resubmitted:
09/ 19/2024
FINAL DESIGN
Issued for Review
Not for Construction
Hendersonville WWTF Biosolids Thermal Dryer September 2024
NCDEQ DWR Non -Discharge Unit - Distribution of Class A Residuals (DCAR) Application
06496-0015 1

1. Program Information:
1. Proiect Narrative
At the City of Hendersonville WWTF, raw wastewater undergoes preliminary and secondary
treatment, the residue (sludge) that accumulates throughout the treatment is processed by gravity
thickening and belt filter press (BFP) dewatering to produce a dewatered sludge cake with
approximately 17.5% Total Solids (TS) content by mass. The dewatered cake is currently hauled
from the WWTF and disposed of at the White Oak Landfill in Haywood County, NC at a rate of
$109.50/wet ton. Alternatively, the City may haul the dewatered cake to the Enoree landfill in
Greer, SC at a rate of $145/wet ton if the White Oak Landfill is unable to accept the solids. The
existing solids handling process flow diagram is included in Appendix A.
Following the completion of this project, waste activated sludge will continue to be pumped to
the existing gravity thickeners for thickening prior to dewatering. The thickened WAS will
continue to be pumped to the existing dewatering belt filter presses to be blended with polymer
and dewatered prior to thermal drying. The dewatered cake will then be transferred to the new
Thermal Dryer Building by a new dewatered cake conveyor beginning in the existing Processing
Room at the discharge end of the existing dewatered cake conveyor and discharging through the
roof of the Thermal Dryer Building into a 100 cubic foot (CF) dryer feed hopper located within
the Thermal Dryer Building. The southeast quadrant of the existing Covered Storage Shelter will
be converted into the new Thermal Dryer Building to house the new thermal dryer equipment.
After being processed in the dryer, the dried biosolids product will then be conveyed by new
dried biosolids shafted screw conveyors to the Covered Storage Shelter for storage or truck
loading. The remaining portion of the existing Covered Storage Shelter that is not converted into
the Thermal Dryer Building will be partially enclosed with walls on the north and east sides to
protect the dried biosolids from the elements. The proposed solids handling process flow diagram
is also included in Appendix A.
Access to the new Thermal Dryer Building will be provided by extending the existing concrete
pavement to the eastern side of the Covered Storage Shelter and new Thermal Dryer Building.
The new concrete apron will include a hammerhead turnaround area to provide easier access for
trucks and equipment. The existing curb and gutter at the transition from existing to new concrete
pavement will be removed, and new curb and gutter will be provided for the new pavement areas,
which will be tied into the existing curb and gutter. A new trench drain is proposed within the new
pavement areas to drain stormwater potentially contaminated by unstabilized biosolids back to the
Influent Pumping Station via the in -plant drain system. The new trench drain is proposed to be
tied into existing MH 15. Existing manhole MH 15 will be located within the new pavement area,
therefore its frame and cover must be adjusted to match the required pavement elevation to ensure
it is flush with the required pavement elevation.
2. Marketability Statement
Per the biosolids management market analysis completed for the project as described in the City
of Hendersonville WWTF Biosolids Thermal Dryer Basis of Design Report Section 4 - Biosolids
Management Market Analysis, included in Appendix B, it is anticipated that there are ample
potential horticulture and agriculture uses to easily absorb the expected biosolids fertilizer
production. If the City is unable to remove the dried biosolids due to seasonal usage trends or a
temporary lack of interest, the City will be able to store dried biosolids for an extended period of
time until interest or usage increase. The City will also be able to dispose of the dried biosolids in
Hendersonville WWTF Biosolids Thermal Dryer September 2024
NCDEQ DWR Non -Discharge Unit - Distribution of Class A Residuals (DCAR) Application
06496-0015 2

area landfills that are currently accepting the unstablized dewatered cake as a backup in extreme
situations.
3. Product Information Sheet
See Appendix C.
2. Operation and Maintenance Plan
In accordance with the requirements set forth by the North Carolina Department of Environmental
Quality using NCGS 143-215.1 and 143-215.3(a) based on 15A NCAC 02T .110, The City of
Hendersonville is implementing this Operation and Maintenance Plan.
1. Sludge Thickening
1.1 Purpose:
A. The purpose of the sludge thickeners is to thicken the waste activated sludge from the
final clarifiers prior to dewatering in the belt filter presses.
1.2 Equipment:
A. The sludge thickening system consists of two 50-foot diameter concrete tanks with 13-
foot sidewater depth, each outfitted with a rotating thickener mechanism that enhances
the gravity thickening of the waste activated sludge material and enables the decant of the
supernatant over the effluent weirs.
1.3 Relationship to Adjacent Units:
A. Waste activated sludge to the sludge thickeners comes from the waste sludge pumping
station through two 8-inch force mains. Thickened sludge is withdrawn from the
thickeners for chemical conditioning and application to the belt filter presses.
1.4 Operation:
A. Start-up Procedure — Before starting up the thickeners, verification should be made of the
following:
I. Check the bases to be sure that all debris such as rocks, concrete, and the like have all
been removed.
ii. Assure that equipment is properly aligned and leveled and that all scraper blades are
properly installed.
iii. Check the position of the weirs to assure that they are level and will allow for equal
flow distribution.
iv. Check out all components of the thickener drive mechanisms including confirmation
of lubricants, direction of rotation, and activation of torque overload sensing devices.
The operator should follow the manufacturer's instructions closely in placing the
thickener and appurtenant equipment into operation. Prior to admitting sludge flow,
the skimmer and collector mechanisms should be run for two or three hours with the
thickener empty to assure proper operating clearances and performance. After a
complete inspection, the thickener tank should be filled with clear water and the
wasting of sludge can commence.
Hendersonville WWTF Biosolids Thermal Dryer September 2024
NCDEQ DWR Non -Discharge Unit - Distribution of Class A Residuals (DCAR) Application
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B. Normal Operation - Under normal operating conditions waste activated sludge will be
discharged to the thickeners at substantially the same rate as the thickened sludge is
withdrawn. This procedure can be modified to gain the optimum results of alternate use
of the thickeners and control of the output to the belt filter presses. Sludge output from
the thickeners will go through one of the three belt filter press feed pumps located in the
thickener building. The thickened sludge is pumped to the Dewatering Building for
dewatering by the belt filter presses.
C. Alternate Operation - In the event one unit needs to be taken offline, the piping in the
Thickener Building is configured to allow the belt filter press feed pumps to be utilized in
pumping from one thickener unit to another.
D. Emergency Operation - In the event both thickeners are inoperable, the piping in the
Thickener Building is configured to allow waste sludge to be pumped directly to the belt
filter presses. This should only take place under emergency situations and only after
thickeners are full and recycling of waste sludge is exhausted.
1.5 Control:
A. Control of the thickener units relates to assuring proper speed of the rotating mechanisms,
no excessive torque on the drive assembly, and prevention of excess solids in the tank
overflows. All other control elements related to the sludge process are discussed in the
sludge dewatering section.
1.6 Maintenance:
A. Thickeners should be inspected daily for overheating, excessive noise, and general
appearance. The decant launder should be inspected for excess buildup of solids and
cleaned as necessary. A detailed preventative maintenance schedule is located in
Appendix D.
1.7 Operational Problems:
A. With appropriate daily inspection and preventative maintenance activities, the thickener
units should be relatively free of operational problems.
2. Sludge Dewatering
2.1 Purpose:
A. The sludge dewatering system is intended to remove excess water from the thickened
sludge.
2.2 Equipment:
A. The major components of the dewatering system are the two 2.0 meter continuous belt
filter presses located in the Press Room of the dewatering building. Each unit has a
nominal capacity of 90 gallons per minute and extracts water from the sludge after
conditioning it with polymer and conveying it on a belt through a series of rollers and
presses.
B. Support equipment for the belt filter press includes sludge feed pumps, polymer/sludge
mixing chamber, and washwater pumps.
C. The polymer feed system is closely related to the sludge dewatering system. The
application and feeding of the appropriate quantity of polymer is a necessary support
function for proper belt filter press performance.
2.3 Relationship to Adjacent Units:
Hendersonville WWTF Biosolids Thermal Dryer September 2024
NCDEQ DWR Non -Discharge Unit - Distribution of Class A Residuals (DCAR) Application
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A. Thickened sludge is conveyed from the thickeners to the belt filter presses through a belt
filter press feed pump unit for each of the two presses. A third feed pump is provided in
standby position and is valved into the sludge piping to be used in lieu of either of the
two primary belt pumps. The thickened sludge from the belt filter presses is discharged
onto a conveyor and is carried to the solids processor unit in the sludge building. Filtrate
from the belt filter presses is discharged to the in -plant sanitary sewer system and
returned to the wetwell of the WWTF influent pumping station.
2.4 Operation:
A. Start-up Procedure — Prior to placing the belt filter presses and their appurtenances into
operation, the following checks should be performed:
I. Confirm that all debris and materials have been removed.
ii. Check all equipment for proper installation including alignment, rigidity, foundation
mountings, belt tension, belt tracking and alignment devices functioning, and the like.
iii. Check all process piping for proper alignment and tight connections and all valves for
correct open / close status.
iv. Inspect electrical connections and power control devices.
v. Confirm the functioning of the control system.
When all of the above checks have been completed in accordance with the manufacturer's
recommendations, the individual belt filter presses can be started and run in a prewash
cycle. After initial running with no apparent problems, sludge may be introduced to the
belt filter press for dewatering.
B. Normal Operation — Under normal operating procedure, the belt filter press feed pumps
will draw sludge from the thickener(s), discharging it to the belt filter press mixing zone
for introduction of polymer. The sludge/polymer mixture proceeds through the belt filter
press and the dewatered sludge is deposited on the conveyor belt that conveys the sludge
to the Processing Room. All controls for the belt filter press and related equipment are
located in the Control Room of the Dewatering Building, and are intended to perform
automatically once proper start-up settings have been activated.
C. Alternate Operation — One or both belt filter presses can be operated at a time. Rates of
feeds can be varied, as can dosages of polymer. The controls for the system can be
operated manually or in the automatic mode.
D. Emergency Operation — No emergency procedures are defined. In the event that both belt
filter presses are inoperable, corrective measures should be undertaken immediately. If
both thickeners are full, wasting of sludge should be discontinued, and the valve between
the two wetwells in the recycle / waste sludge pump station can be opened to enable
recycling of the heavier sludge combined with the returned sludge to the mixed liquor.
2.5 Control:
A. Flow of the thickened sludge is controlled by the valves on the piping from the two
thickeners. Sludge may be withdrawn from either thickener. The feed rate is controlled by
the variable speed pumping equipment on each of the three pumping units. There is also
variable speed control for the polymer feed pumps. The signals for the running status and
alarms for the whole sludge dewatering system are indicated in the Control Room of the
Dewatering Building and interconnected to the Plant master control system. Flow
measurement of the thickened sludge flow to each belt filter press is provided by an
Hendersonville WWTF Biosolids Thermal Dryer September 2024
NCDEQ DWR Non -Discharge Unit - Distribution of Class A Residuals (DCAR) Application
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electromagnetic flow meter on each thickened sludge feed pipe in the Polymer Room of
the Dewatering Building.
2.6 Maintenance:
A. The lubrication and maintenance recommendations of the various equipment
manufacturers should be followed by the operating staff. These recommendations are
contained in the manuals provided by the manufacturers. Good "housekeeping" and
complete cleanup at the end of dewatering cycles is mandatory. A detailed preventative
maintenance schedule is located in Appendix D.
2.7 Operational Problems:
A. There are several potential problems that may be encountered in the operation of the
sludge dewatering system summarized as follows:
The characteristics of the thickened sludge may vary widely from time to time based
on the variables of the biological process taking place in the aeration basins.
ii. Changes in sludge characteristics may prescribe changes in polymer conditioning,
both in the type polymer and the dosage rate. Periodic evaluation of polymers should
be undertaken to assure that optimum performance is being pursued.
iii. The correct sludge feed rate may vary both with the nature of the sludge and the
polymer. Periodic varying of the feed rate will confirm that optimum performance is
being accomplished.
iv. Mechanical problems with the equipment may occur from time to time. There are
many mechanical components, and each requires proper maintenance and care.
Attention to the details suggested by the manufacturers' manuals should minimize
mechanical problems and avoid downtime.
3. Polvmer Feed Svstem
3.1 Purpose:
A. To provide polymer solution for the conditioning of the thickened sludge for dewatering
by the belt filter presses.
3.2 Equipment:
A. The polymer feed system is located in the Polymer Room of the Dewatering Building.
The system consists of pump, mixer, and control panel all as one unit. The system draws
water and polymer through inlet ports, mixes to appropriate levels, and discharges
emulsion polymer to the belt filter press. There are two polymer feed systems, each
dedicated to a corresponding belt filter press.
3.3 Relationship to Adjacent Units:
A. The polymer system is provided to add polymer solution to the belt filter presses as a
conditioner. The polymer is added directly from bulk storage totes. The dilution water is
supplied from the WWTF potable water supply.
3.4 Operation:
A. Start-up Procedure — Before placing the polymer feed system into operation after repairs,
the operating personnel should perform the following checks to ensure proper operation:
I. Check the pumping units and area around the polymer system for foreign materials
that must be removed prior to operation.
Hendersonville WWTF Biosolids Thermal Dryer September 2024
NCDEQ DWR Non -Discharge Unit - Distribution of Class A Residuals (DCAR) Application
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ii. Inspect all piping connections for proper tightness.
iii. Check all valves for proper operation.
iv. Inspect electrical connections to assure proper connections.
B. Normal Operation — Under normal operation, polymer will be fed as a conditioner for
thickened sludge at the belt filter press units. The polymer system feeds polymer to a
mixing chamber at each belt filter press. This mixing chamber combines the polymer
with the thickened sludge.
Investigation should be undertaken by the operating staff to confirm that the polymer
being fed is the best for application. From time to time due to changes in the influent
flow, it will be desirable to vary the dosage or to change the types of polymer used.
C. Alternate Operation — Alternate operation would include the use of different polymers
and different application rates.
D. Emergency Operation — No emergency procedures are defined. In the event both polymer
feed units are inoperable, corrective measures should be undertaken immediately.
Dewatering operations should be stopped until the polymer feed system is operational
again.
3.5 Controls:
A. Flow Controls — The two polymer feed system units are manifolded together so that each
system can provide polymer to either of the belt filter presses. Potable water is piped
directly to each unit with valves installed for isolation of each unit.
B. The units are operated from a control panel located at the unit and also allow for remote
start — stop operation from the belt filter presses.
3.6 Operational Problems:
A. There are several potential operational problems of feeding polymer in any wastewater
system. These relate to the change in influent wastewater and periodic reviews of the
polymer dosage and performance should be conducted. Changes should be made to
improve results.
B. Mechanical problems with the polymer feed units should be corrected reviewing
troubleshooting guides provided in the Operation and Maintenance Manual provided by
the manufacturers.
3.7 Maintenance:
A. Maintenance of equipment should be completed in accordance with the manufacturer's
Maintenance and Operation Schedule. A detailed preventative maintenance schedule is
located in Appendix D.
4. Sludge Treatment and Storage
4.1 Purpose:
A. The sludge treatment process is intended to improve the quality of the dewatered sludge
by stabilizing it to comply with 40CFR Part 503 Class A requirements.
4.2 Equipment:
A. The major equipment involved in sludge treatment is a biosolids thermal dryer,
conveyors, transfer devices, and their overall control.
Hendersonville WWTF Biosolids Thermal Dryer September 2024
NCDEQ DWR Non -Discharge Unit - Distribution of Class A Residuals (DCAR) Application
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4.3 Relationship to Adjacent Units:
A. The belt filter press is used for dewatering sludge before it enters the thermal drying
process. The belt filter press removes excess water from the sludge, making the sludge
more suitable for thermal drying. The conveyors then transport the dewatered cake to the
thermal dryer where it is dried and discharged to a covered storage shelter via inclined
screw conveyors.
4.4 Operation:
A. Operation of equipment should be completed in accordance with the manufacturer's
Operation and Maintenance manual.
4.5 Controls:
A. The biosolids thermal dryer is equipped with a comprehensive control system to monitor
and regulate the drying process effectively. The control system includes a motor control
center (MCC), programmable logic controllers (PLCs) and human -machine interfaces
(HMIs) to manage key parameters such as temperature, airflow, and residence time
within the dryer.
B. The control system incorporates safety interlocks and alarms to ensure safe operation and
prevent any potential hazards. Regular maintenance and calibration of the control system
components are essential to maintain optimal performance and compliance with
regulatory requirements.
C. Operators are trained to monitor the control system, respond to alarms promptly, and
make necessary adjustments to maintain efficient drying operations. The operation and
maintenance plan outlines detailed procedures for routine checks, troubleshooting, and
emergency response to ensure the reliable and safe operation of the biosolids thermal
dryer.
4.6 Operational Problems:
A. Mechanical problems with the thermal dryer should be corrected by reviewing
troubleshooting guides provided in the Operation and Maintenance Manual provided by
the manufacturers.
4.7 Maintenance:
A. Maintenance of equipment should be completed in accordance with the manufacturer's
Maintenance and Operation Schedule. A detailed preventative maintenance schedule is
located in Appendix D.
Overall Operation Plan
1. The City of Hendersonville's WWTF is permitted to discharge 4.8 MGD. The current
average flow is 2.46 MGD. The incoming waste stream is protected from excessive fats,
oils, and grease through a system of monitoring and permitting local dischargers.
2. The incoming waste stream is further protected from heavy metals and other toxins
through a system of permitting and monitoring.
3. The facility's activated sludge process is managed by the WWTF Manager and the
Laboratory Supervisor. The waste activated sludge generated from the activated sludge
process is pumped to the gravity thickeners for thickening prior to dewatering.
Hendersonville WWTF Biosolids Thermal Dryer September 2024
NCDEQ DWR Non -Discharge Unit - Distribution of Class A Residuals (DCAR) Application
06496-0015 8

4. Thickened waste activated sludge is transferred from the gravity thickeners to the belt
filter presses for dewatering by three belt filter press feed pumps located in the
Thickening Building. Belt filter press feed pump No. 2 operates as a common spare to
pump thickened sludge from either gravity thickener to either belt filter press.
5. The thickened sludge is pumped to each belt filter press's mixing chamber, where it is
combined with polymer solution fed from the two polymer feed systems. Each polymer
feed system may operate with either belt filter press.
6. The thickened sludge is dewatered by two 2.0 meter belt filter presses. Dewatered sludge
cake is discharged from each belt filter press onto a common dewatered cake conveyor
which transfers the dewatered cake to the Processing Room in the Dewatering Building.
7. The dewatered cake will be discharged from the existing dewatered cake conveyor into a
new pant -leg diverter in the Processing Room of the Dewatering Building. The pant -leg
diverter will either direct dewatered cake to the new dewatered cake conveyor to feed the
new biosolids thermal dryer, or direct dewatered cake to discharge into the Product
Storage Bay below the Processing Room where it may be removed and disposed of if the
biosolids thermal dryer is offline for maintenance or repairs.
Dewatered cake will be fed to the biosolids thermal dryer by a new dewatered cake
conveyor which will discharge dewatered cake into the biosolids thermal dryer feed
hopper. The dryer feed hopper will provide a small buffer volume immediately ahead of
the dryer to ensure a consistent feed rate of dewatered cake to the dryer. The dryer feed
hopper live bottom screws will transfer the dewatered cake to the dryer feed table where
the dewatered cake will be spread onto the dryer belt in an even layer to ensure consistent
dryness.
9. The biosolids thermal dryer will dry dewatered cake to a minimum total solids content of
90% TS. The biosolids thermal dryer controls will monitor and control the dried biosolids
material temperature as it exits the dryer, material time in dryer, air heater temperatures,
chamber temperatures, condenser in and out temperatures, condenser in and out humidity,
blower inlet temperature, blower flow rate, blower speed, combustion blower flow rate,
combustion blower speed, natural gas flow rate, leveler speed, belt speed, cooling tower
pump speed, and other pertinent operational and control values.
10. Dried biosolids will be discharged from the biosolids thermal dryer into a dryer discharge
auger screw conveyor which will convey the dried biosolids out of the Thermal Dryer
Room to an inclined screw conveyor under the Covered Storage Shelter. The dried
biosolids will be discharged from the inclined screw conveyor in the Covered Storage
Shelter to the concrete floor slab, or discharged into a dump truck for bulk distribution.
11. Dried biosolids discharged onto the concrete floor slab in the Covered Storage Shelter
will be transferred to product storage stockpiles in the Covered Storage Shelter by
WWTF operations staff using front-end loaders. The dried biosolids stockpiles will be
neatly organized by date produced and will be distributed to end users in order of "first -
in, first -out". The dried biosolids stockpiles will be regularly monitored for temperature
by WWTF operation staff and stockpiles will be regularly turned when stored for
extended periods to reduce self -heating of the dried biosolids.
Hendersonville WWTF Biosolids Thermal Dryer September 2024
NCDEQ DWR Non -Discharge Unit - Distribution of Class A Residuals (DCAR) Application
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12. All maintenance and calibration schedules are based on manufacturer's
recommendations.
13. Safety protocols are based on OSHA requirements.
14. All safety issues will be corrected in house as soon as noted.
15. All wet processes are either contained or directed to an internal drainage system that
leads back to the head of the plant.
Inspection Plan
1. Daily inspections are performed by the operation staff of all equipment, safety, and
records. Any problems are reported to the WWTF Manager or Operator in Responsible
Charge (ORC).
2. Weekly inspections are performed by the ORC of all equipment, safety, and records. Any
problems are reported to the WWTF Manager.
3. Monthly inspections are performed by the WWTF Manager of all equipment, safety, and
records. Any problems are reported to the Utilities Director.
4. Annual review performed by the Utilities Director.
5. Annual safety inspection performed by the City's Risk & Safety Officer.
6. During operational inspections if any noncompliant solids are observed they will be
reintroduced to the system or disposed of in an approved landfill.
7. All safety issues will be corrected in house by operations and maintenance staff as soon
as noted.
8. All records will be verified monthly by at least three people.
Sampling Plan
Once the new biosolids thermal drying facility is constructed, the fertilizer product will be
rigorously tested to verify its nutrient content and to ensure compliance with all USEPA,
NCDEQ, and USDA standards.
Fecal Coliform will be tested to meet the requirements of 15A NCAC 02T .1106(a)(2)(A). This
requirement will demonstrate that the fecal coliform density of the sample is less than one
thousand (1,000) MPN per gram of total solids on a dry weight basis. The pathogen reduction
requirements will also be met using Process to Further Reduce Pathogens — Heat Drying [ 15A
NCAC 02T .1106(a)(3)(F)]. The dried biosolids will be sampled to demonstrate that the biosolids
have a moisture content less than or equal to 10%. The temperature of the dried biosolids and the
wet bulb temperature of the gas in contact with the biosolids as it leaves the dryer will be
monitored to ensure one or both exceeds 80' C. The vector attraction reduction requirement will
be met using Alternative 7 — Drying of Stabilized Residuals per 15A NCAC 02T.1107(a)(7).
The following sampling plan and procedure will be implemented.
Hendersonville WWTF Biosolids Thermal Dryer September 2024
NCDEQ DWR Non -Discharge Unit - Distribution of Class A Residuals (DCAR) Application
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1. Sampling Locations: Specific points within the thermal dryer system where samples will be
collected, such as the inlet, outlet, and any other critical points for analysis.
a. Inlet: Sampling at the inlet of the thermal dryer allows for the analysis of the initial
characteristics of the biosolids entering the drying process. This can help in
monitoring the quality and composition of the feed material.
b. Outlet: Sampling at the outlet of the thermal dryer provides insights into the final
product characteristics, such as moisture content, temperature of the dried biosolids,
and overall quality of the dried biosolids. Samples shall be taken from the outlet of
the dryer as the dried biosolids are discharged into the dryer discharge auger.
c. Critical Points: Critical sampling points include temperature sensors, pressure
gauges, and/or specific internal components of the thermal dryer that are crucial for
monitoring and controlling the drying process effectively.
2. Sampling Frequency: Periodic sampling during operation and sampling at specific intervals
as follows:
a. Moisture Content: Collect samples from the outlet of the thermal dryer at the
beginning of each operational shift, and during normal operation at a minimum of
once daily to verify moisture content of the dried biosolids is less than or equal to
10%.
b. Dried Biosolids Temperature: The temperature of the dried biosolids at the outlet of
the thermal dryer shall be monitored continuously by the thermal dryer monitoring
and controls system to ensure the material at the outlet of the dryer exceeds 80' C.
Independently confirm the accuracy of the outlet temperature monitoring at least
once weekly.
c. Thermal Dryer Chamber Temperature: The temperature of the air in contact with the
biosolids in each chamber of the dryer will be monitored continuously by the thermal
dryer monitoring and controls system.
Sample Collection: Use appropriate sampling equipment and techniques to collect
representative samples of the biosolids at the designated sampling locations. Ensure that
samples are collected in a consistent manner to maintain accuracy and reliability. Samples
will be collected by the Laboratory Supervisor or the Laboratory Technician.
4. Sample Preparation: Prepare the collected samples for analysis by following standard
procedures, which may include homogenization, preservation, and labeling to ensure sample
integrity.
5. Analysis and Testing: Perform the necessary analyses on the samples to assess key
parameters such as moisture content, temperature, particle size distribution, and chemical
composition. Use approved methods and equipment for accurate and reliable results.
6. Record Keeping: Maintain detailed records of the sampling plan, procedures, sample
collection, analysis results, and any corrective actions taken based on the findings.
Documentation is essential for compliance, quality control, and process optimization.
The City of Hendersonville sampling plan will also include:
A full TCLP test on the dried biosolids, including corrosivity, ignitability, and reactivity will
be taken annually.
Hendersonville WWTF Biosolids Thermal Dryer September 2024
NCDEQ DWR Non -Discharge Unit - Distribution of Class A Residuals (DCAR) Application
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2. At a minimum of annually and a maximum of once per 60 days; sampling of the dried
biosolids will be conducted and samples will be analyzed for metals, nutrients, pathogens,
and vector attraction reductions including the following:
a. Aluminum
b. Ammonia -Nitrogen
c. Arsenic
d. Cadmium
e. Calcium
f. Copper
g. Fecal Coliform Density
h. Lead
i. Magnesium
j. Mercury
k. Molybdenum
1. Nickel
in. Nitrate -Nitrite Nitrogen
n. Percent Total Solids
o. pH
p. Phosphorus
q. Plant Available Nitrogen (by calculation)
r. Potassium
s. Selenium
t. Sodium
u. Sodium Absorption Ratio (by calculation)
v. Total Kjeldahl Nitrogen
W. Zinc
3. All sampling will be performed by WWTF laboratory staff.
4. Monitoring will be performed by WWTF operations staff.
5. Analyses will be performed by plant laboratory staff and Pace Analytical Services, LLC in
Ashville, NC.
Spill Response Plan
In the event of a spill, the following should be taken IMMEDITALY:
1. Make sure all personal and bystanders are safe, if not contact emergency services.
2. Halt the source of the spill (overturned truck, leaking valve, ruptured tank, etc.).
3. Contain the spill. Use straw bales or earthen barrier to form a dike to contain the spill.
Hendersonville WWTF Biosolids Thermal Dryer September 2024
NCDEQ DWR Non -Discharge Unit - Distribution of Class A Residuals (DCAR) Application
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4. Cleanup. Employ vacuum trucks. dump trucks, and loaders to remove as much of the spilled
material as possible. Use straw to soak -up the remaining material. Dispose of the same in an
approved landfill.
Flush the roadways with water if needed. If the Spill occurred on a tillable area, till the some
into the soil and spread lime if necessary. If a spill occurs on private property, final clean-up
should be to the satisfaction of the owner.
6. Notification. (This should be done as soon as safely possible.)
a. City of Hendersonville, WWTF — Garret DeMoss [phone]
b. NCDEQ —Asheville Regional Office [phone]
c. County Emergency Services (Sheriff, Fire Dept.) 911
7. Reporting:
The Permittee shall report by telephone to the NCDEQ — Asheville Regional Office,
telephone number [phone], as soon as possible, but in no case more than 24 hours or
on the next working day following the occurrence or first knowledge of the occurrence of any
of the following:
a. Surface disposal of residuals abnormal in quantity or characteristic.
b. Any failure of the surface disposal program resulting in a release of material to
surface waters.
c. Any time self -monitoring indicates the facility has gone out of compliance with its
permit limitations.
d. Any process unit failure. due to known or unknown reasons, rendering the facility
incapable of adequate residual treatment.
Any spill or discharge from a vehicle or piping system during residuals transportation. Any
emergency requiring immediate reporting (e.g., discharges to surface waters. imminent failure
of a storage structure, etc.) outside of normal business hours shall be reported to the
Division's Emergency Response personnel at telephone number [phone] or (919) 733-
3300. Persons reporting such occurrences by telephone shall also file a written report in letter
form within five days following first knowledge of the occurrence. This report shall outline
the actions taken or proposed to be taken to ensure that the problem does not reoccur.
8. Spill Prevention. The easiest way to clean a spill is to prevent one.
a. Ensure loading personal watch the vehicle being loaded.
b. Ensure all valves and lids are closed.
c. Inspect all seals and replace if necessary.
Hendersonville WWTF Biosolids Thermal Dryer September 2024
NCDEQ DWR Non -Discharge Unit - Distribution of Class A Residuals (DCAR) Application
06496-0015 13

APPENDIX A — Flow Diagrams
1. Existing WWTF Flow Diagram
2. Proposed WWTF Flow Diagram
Hendersonville WWTF Biosolids Thermal Dryer September 2024
NCDEQ DWR Non -Discharge Unit - Distribution of Class A Residuals (DCAR) Application
06496-0015

W
co
W
4" TWAS ,�i_6" TWAS
EX. BELT FILTER
PRESS PUMP NO. 1 C/)
4" TWAS 6" TWAS
4" TWAS7 C �—
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PRESS PUMP NO. 2
4" TWAS 6" TWAS
4" TWAS Ci �
EX. BELT FILTER
PRESS PUMP NO. 3
EX. THICKENER BUILDING
10 REV. NO.
DESCRIPTION
DATE k 10
♦ ♦ /
4
_ 0 6291 = -
D
FINAL DESIGN - ISSUED FOR REVIEW - NOT FOR CONSTRUCTION
21 JUN. 2024
C
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30 MAY 2024
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14 FEB. 2024
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10 NOV. 2023
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REVISIONS
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6" TWAS
EX. MANHOLE 19
EX BULKING
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EX BULKING
AGENTHOPPER
EX.
POLYMER EX. POLYMER ROOM
DRUM
3/4" FLEX TUBE
s :
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EX \ J
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FEED
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EX. POLYMER EX. POLYMER
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TANK NO. TANK NO.
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NTS
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v MCKIM&CREED ,o
a �
8020 Tower Point Drive emu r
Charlotte, North Carolina 28227 ---
Phone: [phone], Fax: [phone] l]
NC License# F-1222 1847
www.mckimcreed.com
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CITY OF HENDERSONVILLE, NC
/
The City of Four Seasons"
City of Hendersonville Engineering Department
305 Williams Street
Hendersonville, NC 28792
[phone] (office)
[phone] (fax)
www.cityofhendersonville.org
U
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a s
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HENDERSONVILLE WWTF BIOSOLIDS
THERMAL DRYER
GENERAL
EXISTING PROCESS FLOW DIAGRAM
ISSUE DATE: JUNE 2024 SCALE
MCE PROJ. # 06496-0015 G 0 1■ 0 1
DRAWN AST
DESIGNED ZMT NIA DRAWING NUMBER
CHECKED DES D
PROJ. MGR ZMT
r r ` REVISION
(STATUS: FINAL DESIGN - ISSUED FOR REVIEW
NOT FOR CONSTRUCTION
Autodesk Docs H06496-0015 - WWTF Biosolids Thermal Dryer/G01 01_G01 02_PFD rvt 6/21/2024 10 15 46 AM•

10 REV. NO.
DESCRIPTION
4" TWAS 6" TWAS
4" TWAS
wA
7 QEX. BELT FILTER
PRESS PUMP NO. 1
4" TWAS 6" TWAS
Q
4" TWAS
7 EX. BELT FILTER
PRESS PUMP NO. 2
4" TWAS 6" TWAS
30 r
4" TWAS
7 EX. BELT FILTEQR
PRESS PUMP NO. 3
EX. THICKENER BUILDING
D FINAL DESIGN - ISSUED FOR REVIEW - NOT FOR CONSTRUCTION
C 90% DESIGN SUBMITTAL - NOT FOR CONSTRUCTION
B 60% DESIGN SUBMITTAL - NOT FOR CONSTRUCTION
A 30% DESIGN SUBMITTAL - NOT FOR CONSTRUCTION
REVISIONS
TO EX.
INFLUENT
PUMP
STATION
DATE k 10
21 JUN. 2024
30 MAY 2024
14 FEB. 2024
10 NOV. 2023
EX.
POLYMER
DRUM
EX. POLYMER ROOM
314" FLEX TUBE
s :
2" PW
EX `J
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6" TWAS EX. POLYMER EX. POLYMER
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low
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r
EX. PRODUCT STORAGE
IF -1
IL J�
IL JI --- DEWATERED CAKE BYPASS —11111-
DIVERTER CHUTE
EX. DEWATERING BUILDING
PROPOSED PROCESS FLOW DIAGRAM
NTS
A
COOLING TOWER
OVERFLOW/DRAIN TO DRAIN
A
s
8" CWR
8" CWS
N 8" CWS
3" PW
COOLING TOWER PUMP
�
IF
WASH STAND
IF
IL
l
r
BELT WASH
DEWATERED
CAKE FEED RINSE WATER /
HOPPER FIRE SUPPRESSION
MEDIUM TEMPERATURE BELT DRYER
10 CITY OF HENDERSONVILLE, NC a
vMCKIM&CREED ` o "The City of Four Seasons"
8020 Tower Point Drive
Charlotte, North Carolina 28227 --- r
Phone: [phone], Fax: [phone] l]
NC License# F-1222 1847
www.mckimcreed.com
r �
City of Hendersonville Engineering Department
305 Williams Street
Hendersonville, NC 28792
[phone] (office)
[phone] (fax)
www.cityofhendersonville.org
r
CONDENSATE
TO DRAIN
A A
CONDENSATE PUMP
CONDENSER
r
L�
TO DRAIN � WASH WATER
Qw
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THERMAL DRYER ROOM
DRIED BIOSOLIDS STORAGE AREA
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DRIED BIOSOLIDS
STORAGE AREA
EX. COVERED STORAGE AREA
HENDERSONVILLE WWTF BIOSOLIDS
THERMAL DRYER
GENERAL
PROPOSED PROCESS FLOW DIAGRAM
PROCESS
BLOWER
F
DRYER EXHAUST
a- (VENT TO
ATMOSPHERE)
COMBUSTION AIR
A
AIR HEATER -COMBUSTION
BLOWER
NATURAL GAS SUPPLY
t
BLOWER/HEATER ROOM
ISSUE DATE: JUNE 2024 SCALE
MCE PROJ. # 06496-0015 O1.02
DRAWN AST
DESIGNED ZMT N/A DRAWING NUMBER
CHECKED DES D
PROJ. MGR ZMT
r r ` REVISION
(STATUS: FINAL DESIGN - ISSUED FOR REVIEW
NOT FOR CONSTRUCTION
Autodesk Docs H06496-0015 - WWTF Biosolids Thermal Dryer/G01 01_G01 02_PFD rvt 6/21/2024 10 16 16 AM•

APPENDIX B — City of Hendersonville WWTF Biosolids
Thermal Dryer Basis of Design Report: Section
4 — Biosolids Management Market Analysis
Hendersonville WWTF Biosolids Thermal Dryer September 2024
NCDEQ DWR Non -Discharge Unit - Distribution of Class A Residuals (DCAR) Application
06496-0015

HENDERSONVILLE WWTF BIOSOLIDS THERMAL DRYERI BASIS OF DESIGN REPORT
SECTION 4 BIOSOLIDS MANAGEMENT MARKET ANALYSIS
The City has proactively requested a market analysis, not only to understand the potential for the
biosolids disposal options, but also to assist in the selection of the thermal drying equipment. The
results from the Solids Sampling and Analysis, presented above, confirmed that the solids produced
at the WWTF have the characteristics to be a Class A "Exceptional Quality" biosolids fertilizer with
beneficial use. The distribution of the dried biosolids for beneficial use will replace the current
practice of landfilling un-stabilized wet cake solids (approximately 4,500 wet tons per year at 17.5%
total solids) generated by the WWTF at a significant and rapidly escalating cost of $109.50/wet ton.
Once dried, the amount of biosolids fertilizer that will be produced is expected to be about 800 tons
per year initially and expanding to approximately 2,000 tons per year by 2045. The biosolids fertilizer
is a valuable all -natural product that is an excellent soil amendment for lawns, trees, shrubs, and
flowers. It provides both a valuable source of nutrients that are essential to plant growth and organic
matter that enhances soil structure and quality. Based on similar biosolids products produced in the
United States, the Hendersonville organic based fertilizer was anticipated to have a nutrient content
(N-P-K) of about 5-3-0. The actual test results showed that the nutrient value most likely will result in
about 5-1-0 (see Appendix E for laboratory testing results). Once new biosolids thermal drying facilities
are constructed, the fertilizer product will be rigorously tested to verify its nutrient content and to
ensure compliance with all USEPA, NCDEQ, and USDA standards.
4.1 IDENTIFICATION OF POTENTIAL STAKEHOLDERS
Initially, potential stakeholders identified in the 2021 Solids Management Plan Evaluation were
confirmed with the City. Subsequently, further research was completed to add additional potential
stakeholders for the market evaluation. One of the resources to identify key stakeholders is the
Agribusiness Henderson County which coordinates the economic development partnership for
agricultural business in Henderson County. Another resource is the NC State Extension. A list of 28
potential businesses were identified as potential users of Class A biosolids product with proximity to
Henderson County. Potential stakeholders can be classified as follows:
Parks departments
Sod farms
Orchards
CIGM&CREED
v.Jacobs
FINAL I DUNE 2024 143
ENGINEERS SURVEYORS rNN,.-

HENDERSONVILLE WWTF BIOSOLIDS THERMAL DRYERI BASIS OF DESIGN REPORT
• Pasture farms
• North Carolina Department of Transportation
• Landscapers
• Horticultural production greenhouses
Following the identification of potential stakeholders, the level of interest, value of the product, and
large bulk users were evaluated.
4.2 PRODUCT SAMPLES AND POTENTIAL STAKEHOLDERS MEETINGS
From initial discussions, invitations for in -person meetings were sent to about 20 local businesses. In
preparation for the meetings, and with the purpose of obtaining a tangible sample of whatthe product
may look like, a visit to the City of Lenoir's biosolids drying facility took place on August 2911, 2023.
During this visit samples of their product (Figure 4.1) were packaged to offer to prospective users
during the meetings. A trip report is included in Appendix G. A one -page product fact sheet and
questionnaire (Appendix H) was also prepared to share with potential stakeholders and obtain further
information on value and level of interest. A list of potential users and interested stakeholders is
included in Appendix I.
Figure 4.1 - Lenoir Biosolids Fertilizer Product
The result of the in -person meetings and outreach effort is summarized as follows:
Mq<WREED Jacobs
FINAL I JUNE 2024 144
ENGINEM Svpvftm PflkPNfrd

HENDERSONVILLE WWTF BIOSOLIDS THERMAL DRYERI BASIS OF DESIGN REPORT
• Potential stakeholders and users believe they can move 1,000-1,200 tons per year of dried
biosolids if the price is right.
The product should not be promoted for use on food crops.
• Parks and Recreation Departments are potentially the most interested stakeholders,
beginning with the Henderson County Parks and Recreation Department (>500 acres) and
the City's Parks and Recreation Department (>100 acres).
• Other sod, tree, and forage crops can be great potential users with many hundreds of acres
available for agriculture in the County.
There is interest by several parties (Parks and Recreation Departments and sod farms) to
conduct field trials of the product produced by facility in Lenoir. The City will coordinate with
potential users to obtain product from the facility for field trials.
4.3 POTENTIAL LARGE SCALE BULK USERS/MARKETING PARTNERS IN
HENDERSON COUNTY
Hendersonville is located in agriculturally rich Henderson County. According to the USDA, Henderson
County has over 41,000 acres of active farmland based on the latest statistics published in 2017. In
NC, Henderson County is the second largest producer of fruits, trees, nuts, and berries and the third
largest revenue producer of nurseries, greenhouses, floriculture, and sod production. The USDA also
indicates that Henderson County has over 4,400 acres of forage land, over 4,300 acres of apple
orchards, and over 4,100 acres of corn for grain. The NC State extension office indicates there are over
1,500 acres of sod farms and over 1,500 acres of ornamental tree farms in the county. Although no
specific marketing partner was identified at this stage in project development, there are several
potential large-scale users (sod farms, parks, and forage and crop lands) that could absorb vast
amounts of the biosolids fertilizer product.
4.4 SUMMARY FINDINGS AND RECOMMENDATIONS
4.4.1 MARKET RESEARCH FINDINGS
The provided product fact sheet (Appendix H) and sample of a similar product was instrumental in
the ability to receive significant interest for use in the agriculture industry. Avoiding direct use on food
crops was recommended by stakeholders to avoid potential concerns with product use certifiers and
MCKsif�ia I �� EED 7 FINAL I JUNE 2024 145
Jacobs

HENDERSONVILLE WWTF BIOSOLIDS THERMAL DRYERI BASIS OF DESIGN REPORT
end users. Several stakeholders indicated there are ample potential horticulture and agriculture uses
to easily absorb the 1,000-1,200 tons of the expected biosolids fertilizer production. Strong interest
exists from Parks and Recreation Departments and at least one large sod producer to conduct field
trials of a similar dried biosolids fertilizer product being generated in Lenoir, NC. The City will help
stimulate this interest by procuring small quantities of the Lenoir biosolid fertilizer product so
potential users in Hendersonville can test its use to compare against their current fertilization
practices.
4.4.2 PREFERRED PRODUCT CHARACTERISTICS AND VALUE
The value of dried biosolids fertilizers varies based on geography and the amount of product
produced, as well as the price of competing products. A fairly uniform, granular, low dust product that
can be spread with broadcast spreaders is generally of higher value than irregular low -density
products produced by some driers. Generally speaking, a N-P-K nutrient content of at least 5-3-0 is
preferred. In the eastern US, the value of dried biosolids fertilizer product generally falls in the $10-
$20/ton range in bulk. Dried products with a higher N content will have higher value. Because of the
relatively small quantity of dried biosolids that will be produced in Hendersonville, the focus is to
ensure the material is used beneficially at a nominal price and not landfilled. Although no specific
value was able to be enumerated from this effort, several interviewees indicated the cost of fertilizer
has increased substantially in the past few years and are therefore interested in alternative products.
For example, Henderson County Parks and Recreation Department is paying $27 for a 50 lb. bag of
lawn/grass fertilizer which amounted to over $30,000 of fertilizer costs in 2022.
4.4.3 PRODUCT DISTRIBUTION AND MARKETING
Usage of fertilizers such as the dried biosolids fertilizer produced by the City is seasonal. For example,
sod farms in NC may produce 3 cuttings per year and will require fertilizer for use after harvesting of
one cutting and then preparation for growing a second cutting. Landscape activities on parks are
usually practiced in late winter or early spring prior to heavy use by visitors. Other agricultural uses of
the product are generally dictated by the crop type and the time of year that access is available, and
crops need fertilization. Therefore, covered storage of a dried fertilizer product for 3 to 4 months is
generally needed to keep the fertilizer product out of the weather when not in use. This can be done
at the point of production or atthe point of use. Uniformity of the product is also important. A granular
product that is fairly uniform in particle size with minimal dust is desired by most users. The nutrient
*,MCMM&CREE1D 7 FINAL I JUNE 2024 146
ENGINEERS SURVEYORS PEAT NUN Jacobs

HENDERSONVILLE WWTF BIOSOLIDS THERMAL DRYERI BASIS OF DESIGN REPORT
content is also important and must be regularly monitored to establish a guaranteed N-P-K value.
Bulk marketing by the truckload is recommended initially with a group of users to ensure the material
is beneficially reused in horticulture and agriculture instead of the existing practice of landfilling un-
stabilized wet cake solids.
4.4.4 LIST OF POTENTIAL NEW CUSTOMERS AND MARKETING PARTNERS
Appendix I provides a detailed list of potential market stakeholders and marketing partners that the
City should follow up with as the biosolids thermal drying project continues to develop. The
Henderson County Parks and Recreation Department, the City of Hendersonville Parks and Recreation
Department, and Turf Mountain Sod are interested in trialing a similar product from Lenoir and show
promise for potential long-term partnerships to utilize thermal dried biosolids in the future. The NC
Extension Service in Henderson, Buncombe, and Polk County, and Agribusiness Henderson County
will be great assets to communicate the value of the product to potential customers and to identify
new customers and marketing partners through their extensive networks.
SOURCES:
1) United States Department of Agriculture. 2017. 2017 Census of Agriculture County Profile:
Henderson County North Carolina. (cp37089.pdf (usda.gov))
Ott E�Gi�aEEC �Su�R ,CR E 7 FINAL I JUNE 2024 147
Jacobs

APPENDIX C — Product Information Sheet
Hendersonville WWTF Biosolids Thermal Dryer September 2024
NCDEQ DWR Non -Discharge Unit - Distribution of Class A Residuals (DCAR) Application
06496-0015

CITY OF HENDERSONVILLE CLASS A BIOSOLIDS
PRODUCT INFORMATION SHEET
1. BIOSOLIDS PRODUCT PREPARER CONTACT INFORMATION
Facility Name:
NPDES Permit #
Distribution of Class A Residuals Permit #
WWTF Manager Name:
Facility Address:
Phone Number:
Email:
Hendersonville WWTF
NCO025534
WQ0011381
Garrett DeMoss
99 Balfour Road
Hendersonville, NC 28792
[phone]
Qdemossnhvinc.Qov
2. DESCRIPTION
The product you are receiving is a dried biosolids material produced from the heat treatment of
residuals from municipal wastewater treatment. This product meets the standards for a Class A
biosolids product according to the EPA's 40 CFR Part 503 regulations and 15A NCAC 02T. 1100.
The material has been treated meeting Pathogen Reduction Requirements, Alternative 5: Process
to Further Reduce Pathogens — Heat Drying in accordance with 15A NCAC 02T .1106(a)(3)(F).
The material has been treated meeting Vector Attraction Reduction Requirements, Alternative 7:
Drying of Stabilized Residuals, in accordance with 15A NCAC 02T .1107(a)(7).
3. MOST RECENT NUTRIENT/METALS ANALYSIS OF BIOSOLIDS
Parameter
Result (mg/kg) N-P-K Ratios
Total Kjeldahl Nitrogen (TKN)
50,867 5.08%
Ammonia -Nitrogen (NH3-N)
2,483
Total Phosphorus (P)
9,707 0.97%
Total Potassium (K)
ND' 0%
Arsenic (As)
ND'
Cadmium (Cd)
1.3
Copper (Cu)
503.7
Lead (Pb)
26.9
Mercury (Hg)
1.2
Molybdenum (Mb)
ND'
Nickel (NO
52.0
Selenium (Se)
5.1
Zinc (Zn)
818.3
Footnotes:
1. ND = Not detected at or above the
reporting limit.
4. RESTRICTIONS
Land application of this Class A Biosolids Product is prohibited except in accordance with the
following instructions:

This Class A Biosolids Product shall not be applied under the following conditions:
a. To any site that is flooded, frozen, or snow-covered, or is otherwise in a condition
such that runoff of the Class A Biosolids Product into any surface waters would
occur.
b. If the application causes prolonged nuisance conditions.
C.
2. The Class A Biosolids Product shall be stored or staged in a manner to prevent runoff of the
Class A Biosolids Product into any surface waters.
3. The Class A Biosolids Product shall not be staged or stockpiled at the application site for
more than 30 days prior to application.
4. A copy of this Product Information Sheet shall be maintained at the site when bulk residuals
are being applied.
5. The residuals shall be prevented from entering any public or private water supply source
(including wells) and any surface waters (e.g. streams, lake, river, wetland)
6. Residuals should be land applied at agronomic rates and recommended rates for intended
uses.
7. The Permit Designee shall not distribute bulk residuals to any person or entity known to be
applying residuals contrary to the conditions of this Product Information Sheet, 40 CFR Part
503, and/or 15A NCAC 02T .1100.
5. SETBACKS
Applicable setbacks in accordance with 15A NCAC 02T.1108(b):
Description of Setback
Each private or public water supply source
Surface Waters (streams — intermittent and perennial, perennial
waterbodies, and wetlands)
Surface water diversions (ephemeral streams, waterways,
ditches)
Groundwater lowering ditches (where the bottom of the ditch
intersects the seasonal high water table, i.e. SHWT)
Each well with exception of monitoring wells
Bedrock outcrops
6. APPLICATION RATES
Setback Distance (feet)
100
25
0
0
100
0
The Class A Biosolids Product shall be applied at agronomic rates and recommended rates for
intended uses.

APPENDIX D — Preventative Maintenance Schedule
Hendersonville WWTF Biosolids Thermal Dryer September 2024
NCDEQ DWR Non -Discharge Unit - Distribution of Class A Residuals (DCAR) Application
06496-0015

Sludge Conveyor System
Inspect:
Check belt for tears, cracks, abrasions.
Check belt scraper for proper operation.
Check drive chain for build up of foreign matter on chain and
sprockets.
Check drives, belts, chain and overall operation for unusual noise.
Check drive chain tension. Tension station should move back and
forth approximately 1/8" to 1/4".
Check slide tube and for foreign buildup and lubricate guide
blocks as needed.
Check V-belt drive tension. Refer to manufacturer O&M for
procedure.
Check oil level in speed reducer.
Check sprocket wear and alignment.
Check roller chain tension and alignment. Refer to manufacturer
O&M for procedure.
Check rollers for free rotation.
Check drip pan bolt and nuts for proper tightness.
Check drive chain for wear. Refer to manufacturer O&M for
procedure.
Check sprocket bearings for wear, lubricate as needed.
Check all hardware at rollers and supports and carriages for
correct tightness.
Check motor for wear.
Check track for wear.
Frequency
D = Daily W = Weekly
M = Monthly S = Semi -Annually
A = Annually
D W M
X
X
X
X
X
X
X
X
X
X
S A OTHER
X
X
3 months
3 months
3 months
3 months
3 months
Hendersonville WWTF Biosolids Thermal Dryer September 2024
NCDEQ DWR Non -Discharge Unit - Distribution of Class A Residuals (DCAR) Application
06496-0015

Thickeners
Frequency
D =
Daily
W = Weekly
M
= Monthly
S = Semi -Annually
A =
Annually
D
W M
S A OTHER
Inspect:
Check surface skimmer for smooth operation at scum beach.
X
Check oil level in worn gear main drive.
X
Check worm gear air vent.
X
Grease worm gear bearings.
X
Check drive chain sprockets for loose bolts, setscrews or keys.
X
Check drive chain for excessive slack.
X
Check shear pin for wear and loose screws.
X
Grease lifting shaft.
X
Check action of lifting device.
X
Hose off skimmer assembly and inspect all components.
X
Seasonal change of oil in work gear drive. Refer to manufacturers
X
O&M.
Check torque overload switches for corrosion, manually trip
X
overload switch.
Remove shear pin and clean and grease.
X
Check scum trough and baffles for binding of scrum arin.
X
Check plow blades squeegees for bent or worn arts and check all
X
bolted connections for loose or missing bolts. Replace if
necessary.
Hendersonville WWTF Biosolids Thermal Dryer September 2024
NCDEQ DWR Non -Discharge Unit - Distribution of Class A Residuals (DCAR) Application
06496-0015

Belt Filter Press Wash Pumps
Inspect:
Check pumps for overheating, excessive noise, vibration or other
indication of trouble.
Drive units for excessive dirt, dust, etc.. Clean as necessary.
Impeller clearance, adjust as necessary.
Pumps for corrosion and wear.
Impellers and impeller casing and remove and deposits of scaling
Remove impeller and inspect it and casing for pitting or excessive
wear, repair or replace as necessary.
Clean and inspect motor and remove plug to drain condensate.
Check motors for excess dirt making sure the ventilating air inlet
is not blocked. Clean as necessary.
Check oil level in seal and bearing cavities. Add if necessary.
Frequency
D = Daily W = Weekly
M = Monthly S = Semi -Annually
A = Annually
D W M S A OTHER
X
X
X
X
X
X
3 months
3 months
3 months
Hendersonville WWTF Biosolids Thermal Dryer September 2024
NCDEQ DWR Non -Discharge Unit - Distribution of Class A Residuals (DCAR) Application
06496-0015

Belt Filter Press Feed Pumps
Inspect:
Check pumps for overheating, excessive noise, vibration or other
indication of trouble.
Drive units for excessive dirt, dust, etc.. Clean as necessary.
Impeller clearance, adjust as necessary.
Pumps for corrosion and wear.
Impellers and impeller casing and remove and deposits of scaling
Remove impeller and inspect it and casing for pitting or excessive
wear, repair or replace as necessary.
Clean and inspect motor and remove plug to drain condensate.
Check motors for excess dirt making sure the ventilating air inlet
is not blocked. Clean as necessary.
Check oil level in seal and bearing cavities. Add if necessary.
Frequency
D = Daily W = Weekly
M = Monthly S = Semi -Annually
A = Annually
D W M S A OTHER
X
X
X
X
X
X
3 months
3 months
3 months
Hendersonville WWTF Biosolids Thermal Dryer September 2024
NCDEQ DWR Non -Discharge Unit - Distribution of Class A Residuals (DCAR) Application
06496-0015

Belt Filter Presses
Inspect:
Check level of oil lubricator.
Check drip of oil lubricator.
Check air filter condensate discharge.
Was press and remove deposits.
Check oil in gear box, replace after 10,000 hours service.
Check doctor blades for wear.
Replace doctor blades.
Check spray pipe for proper operation.
Remove solids from spray pipes (turn hand wheel).
Clean inside belt washing box.
Replace spray pipe brush.
Replace spray nozzles.
Grease bearings.
Check bearings for excessive noise.
Grease rack and pinion.
Check sensor paddle on tracking device.
Check roller coverings.
Check belt wear, and replace as needed.
Frequency
D = Daily W = Weekly
M = Monthly S = Semi -Annually
A = Annually
D W M S A OTHER
X
X
X
X
X
X
X
I1/
X
X
X
3 months
10,000
hrs
20,000
hrs
3 months
Hendersonville WWTF Biosolids Thermal Dryer September 2024
NCDEQ DWR Non -Discharge Unit - Distribution of Class A Residuals (DCAR) Application
06496-0015

Biosolids Thermal Dryer
Inspect:
Chamber inspection: Minimal material buildup in chambers, spray
bars working properly
Dryer belt -centered, no rips or tears
Check HMI to determine if any alarms are repeating or must be
addressed
Exit material temperature within normal operating range: 175°F -
275°F
Air heater temperatures are within normal operating range: Below
450°F
Chamber temperatures are within normal operating range: 100°F -
350°F
Condenser filter inspection: No buildup of residue, no blinding
Frequency
D = Daily W = Weekly
M = Monthly S = Semi -Annually
A = Annually
D W M
X
X
X
X
X
X
X
Condenser in and out temperatures are within normal operating
range: Between 80' and 140°F X
temperature difference
Condenser differential pressure is within normal operating range:
Max 7.0 inWC; Normal pressure should be 4.0 inWC or less
Condenser humidity is within normal operating range: humidity in
—45%; humidity out —80%
Blower inlet temperature less than 190°F
Blower flow is within normal operating range:—8,OOOcftn -
20,000cfm depending on dryer size and condenser filter/coil
cleanliness
Tension rolls and chamber drain valve air lines are free of leaks
Motors: No excessive vibration
Sifter brush assembly is working as expected
Sifter basket is clean
Sifter basket is not experiencing excessive wear, no material
thinning or worn holes (Replaced if necessary)
Leveling auger and/or leveling brush are clean, no buildup of
material on flights or bristles
Control cabinet filters are clean (Replace filters if necessary)
Control cabinet air conditioner is operating normally, cabinet
temperature is below 85°F
Control cabinet air conditioner condensate line drain is clean, no
blockages
Cooling tower basin is clean: No biological growth or signs of
hard water (Treat cooling tower water as necessary)
Cooling tower fan is operational
Cooling tower spray bar is rotating and operating properly
Combustion blower filter is clean and free of debris
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
S A OTHER
Hendersonville WWTF Biosolids Thermal Dryer September 2024
NCDEQ DWR Non -Discharge Unit - Distribution of Class A Residuals (DCAR) Application
06496-0015

Air heater instrument air line valves have been bled to allow
condensate to drain
Air heater thermocouples are within normal operating range: This
should be comparative to the air heater set point 100°F - 400°F
Belt rinse pan and spray bar wands are void of material buildup
Exit material temperature sensor at exit hood are clean
Topside ductwork inspection: During start-up, start the process
blower but do not initiate the air heater. Walk topside and listen
for hissing or other indicators of air leaks or compromised o-rings.
Lid bolt inspection: While dryer is shutdown and once lids have
reached a safe temperature, inspect bolts for loosening and
tightened where necessary.
Injection plate inspection: While dryer is shutdown, follow the Lid
Lift Procedure starting on page 22 of the Gryphon O&M manual
to lift the lids. Inspect the perforated injection plates for
plugging/clogging. Clean as necessary using a Teflon safe
cleaning solution.
Skirt seal inspection: While dryer is shutdown, follow the Lid Lift
Procedure starting on page 23 of the Gryphon O&M manual to lift
the lids. Inspect the silicone skirt seals for wear or damage.
Replace if necessary.
Gearbox oil inspection: While dryer is shutdown, check the
gearbox oil levels and fill as required.
Blower flow meter inspection: Probe is cleaned, no buildup
Condenser inspection: While the dryer is shutdown, use the
condenser access panels to inspect the coil, filters, and basin for
cleanliness. Follow the Condenser Maintenance protocol on page
33 of the Gryphon O&M manual to properly clean the coil.
Following the filter and coil cleaning, inspect the condenser
basins for blockages and flush as required.
Sifter brush replacement: Verify sifter mechanical is de -
energized. Remove access plates on each side of sifter housing
and lockout sifter. Replace brushes that can be accessed by
hammering in new brushes against old ones - old brushes will be
pushed out the other end of the track by the new brushes. Re -
energize sifter to rotate sifter drum until more old brushes are
accessible. Repeat the process of replacing old with new. NOTE:
It may be beneficial to mark brushes that have been replaced to
keep track.
Skirt seal replacement: While dryer is shutdown, follow the Lid
Lift Procedure starting on page 23 of the Gryphon O&M manual
to lift the lids. Remove the existing skirt seals and dispose.
Replace with new set running a 1" bead of high temperature
silicone every 24-36". Lower the lids.
Preventive maintenance of electrical cabinet: To be performed
by a qualified electrician. With cabinet de -energized and locked
out, verify electrical connection torque on al VFDs, motor
starters, and terminal blocks.
/M
X
X
X
1N
/M
X
3 months
3 months
3 months
3 months
3 months
3 months
3 months
Hendersonville WWTF Biosolids Thermal Dryer September 2024
NCDEQ DWR Non -Discharge Unit - Distribution of Class A Residuals (DCAR) Application
06496-0015

Inspect and tighten bolts on iniection plates: While dryer is
shutdown, follow the Lid Lift Procedure starting on page 29 of
the Gryphon O&M manual to lift the lids. Once lids and X
chambers have reached a safe temperature, inspect the injection
plate torx bolts for loosening and tightened where necessary.
Gearbox oil chance: Per the manufacturer's instructions for each X
gearbox, perform an oil change.
Schedule NFPA Air Heater Inspection with Gryphon
/M
Hendersonville WWTF Biosolids Thermal Dryer September 2024
NCDEQ DWR Non -Discharge Unit - Distribution of Class A Residuals (DCAR) Application
06496-0015

Parameter
NH4-N
NO3-N + NO2-N
TKN
Organic-N (TKN - NH4-N)
Year
1
2
3
4
5
Result (mg/kg)
2,483.33
50,866.67
48,383.34
Starting Org-N (mg/kg)
48,383.34
33,868.34
28,788.09
26,485.04
25,425.64
Mineralization Rate
30%
15%
8%
4%
3%
Mineralized Org-N
(mg/kg)
14,515.00
5,080.25
2,303.05
1,059.40
762.77
Org-N Remaining
(mg/kg)
33,868.34
28,788.09
26,485.04
25,425.64
24,662.87
Note: Initial year Org-N mineralization rate per Table 3, Waste Type Municipal - Other; McGinnis, M., M. Buchanan, C.
Stokes, and B. Cleveland. 2011. Waste and compost analysis guide. NC Dep. Agric. Consumer Serv., Raleigh, NC
First Year PAN 5-Year Max. Adj. PAN
(mg/kg) (mg/kg)
16,998.33 26,203.80

DWR
Division of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
RESIDUALS SOURCE CERTIFICATION
INSTRUCTIONS FOR FORM: RSC 06-16
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking
the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the
required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one
original and two copies of the application and suuuorting documentation
For more information, visit the Water Quality Permitting Section's Non-Discharze Permitting Unit
General — This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or
disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without a corresponding application form (FORM:
RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below.
A. Residuals Source Certification (FORM: RSC 11-15):
® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not make any unauthorized
content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the
attachments are numbered to correspond to the section and item to which they refer.
❑ For new or renewed permits, submit a separate certification for each source facility.
® For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification.
® Complete the residuals source facility summary page. List all new, renewed, or modified facilities.
B. Residuals Source -Generating Facility Information:
® For each source facility, attach the following:
® Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Mau Guidance for Residuals Land
AnDlication Permits".
® Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals are to be generated,
treated, processed, and stored at the facility.
® Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8. Ensure that the amount
of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this
amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other
additives that are added to the residuals during processing.
® Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling
frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or
the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and
monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed.
C. Residuals Quality Information:
® For each source facility, attach the following:
® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification.
® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction
requirements.
® For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of
residuals generated from a similar facility along with the description of similarities of the two facilities.
INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1

RESIDUALS SOURCE FACILITY SUMMARY
Applicant's name: jity of Hendersonville
Status Facility Permit Holder Facility Name
Code
M City of Hendersonville City of Hendersonville W WTF
County Permit Number
Henderson WQ0011381
a Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted)
b The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility).
Maximum Dry Tons Per Year
Current " Proposed
0 1,770.25
SUMMARY FOR FORM: RSC 06-16 Page 1

DWR
Division of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: City of Hendersonville WWTF
2. Facility permit holder is: ❑ Federal, State, Local Government, or Private.
Facility permit issued by: ® Div. of Water Resources, Div. of Environmental Health,
or E] Other (explain: W.
3. Facility contact person and title: Garrett DeMoss, WWTF aN
Complete mailing address: 19 Balfour Road
City: Hendersonville State: Zip: 28791M
Telephone number: 8( 28) 697-3077 E-mail address: tdemoss(a,hvinc.sov
4. Facility physical address: 99 Balfour Road
City: Hendersonville State: F Zip: 28792-_
Coordinates: Latitude: 35' 21' 13" Longitude: 82' 27' 54"
Datum: NAD-83 Level of accuracy: 6"
Method of measurement: GPS
5. Purpose of the facility:
�] treatment of municipal wastewater, [ji treatment of 100% domestic wastewater,
treatment of potable water, j treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: N % industrial and N % domestic)
q other (explain: = ).
6. Does the facility have an approved pretreatment program: Yes No
7. Facility permitted/design flow: E MGD and facility average daily flow: M MGD
8. Average amount of residuals being generated at this facility - dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: The biosolids thermal dryer is desiened to process up to 9.2 dry tons per day (DT/d) of dried biosolids,
operative 24 hours per day 5 days per week at future 2045 maximum month conditions. This equates to a dried biosolids production rate of 10
wet tons per day (WT/d), equal to 800 ft3/d, and 50 WT/week equal to 4.000 ft3/week, assumim a total dry solids content of 92% per the dryer
eauioment basis of desien, a dried biosolids bulk density of 251bs/ft3, and a 24 hour per day 5 day per week operative schedule.
Type and volume of residuals storage (i.e., outside of residuals treatment units): Followim the completion of the modifications to the existine
Covered Storaee Shelter, the partiallv enclosed storage area will have approximately 10.500 ftz of space available for storage of dried biosolids.
This equates to a storage duration of 73.5 days at the full rated capacity of the biosolids thermal dryer system under 2045 maximum month
conditions assumim an average stockpile heieht of 4-ft. Under current annual average conditions, the Covered Storaee Shelter will provide up to
251 days of storage capacity assumine an average stockpile heieht of 4-ft.
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
40 CFR Part 503 or 40 CFR Part 257.
FORM: RSC 06-16 Pagel of5

Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503,
otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
Biological 0 Non -Biological
Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or
the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated
sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA:
(Note - this item
does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal,
domestic
wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: yes no.
If yes, list the number(s): =
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: 0 yes 0 no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for
corrosivity, ignitability, and reactivity:
Laboratory: Pace Analytical Services, LLC and Date of analysis: 7/9/2024 (*), 7/11/2024 (**), 7/10/2024 (***)
Passed corrosivity test: ® yes rj no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: ® yes [] no. Flashpoint: = °F (> 140°F)
Passed reactivity test: kj yes lWo. HCN: = mg/kg (<250) & H2S: = mg/kg (<500)
TCLP Parameter Limit Result TCLP Parameter
Limit
Result
(mg/1) (mg/1)
(mg/1)
(mg/1)
Arsenic 5.0 ND* Hexachlorobenzene
0.13
ND***
Barium 100.0 ND* Hexachloro-1,3-Butadiene
0.5
ND***
Benzene 0.5 ND** Hexachloroethane
3.0
ND***
Cadmium 1.0 ND* Lead
5.0
ND*
Carbon Tetrachloride 0.5 ND** Lindane
0.4
ND*
Chlordane 0.03 ND* Mercury
0.2
ND*
Chlorobenzene 100.0 ND** Methoxychlor
10.0
ND*
Chloroform 6.0 ND** Methyl Ethyl Ketone
200.0
ND**
Chromium 5.0 ND* Nitrobenzene
2.0
ND***
m-Cresol 200.0 0.0818*** Pentachlorophenol
100.0
ND***
o-Cresol 200.0 ND*** Pyridine
5.0
ND***
p-Cresol 200.0 0.0818*** Selenium
1.0
ND*
Cresol 200.0 0.0818*** Silver
5.0
ND*
2,4-D 10.0 ND*** Tetrachloroethylene
0.7
ND**
1,4-Dichlorobenzene 7.5 ND*** Toxaphene
0.5
ND*
1,2-Dichloroethane 0.5 ND** Trichloroethylene
0.5
ND**
1,1-Dichloroethylene 0.7 ND** 2,4,5-Trichlorophenol
400.0
ND***
2,4-Dinitrotoluene 0.13 ND*** 2,4,6-Trichlorophenol
2.0
ND***
FORM: RSC 06-16 Page 2 of 5

Endrin 0.02 ND*
Heptachlor and its Hydroxide 0.008 ND*
2,4,5-TP (Silvex) 1.0 ND***
Vinyl Chloride 0.2 ND**
4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling
concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following
metal parameters:
Laboratory: Pace Analvtical Services. LLC and Date of analysis: 09/11/2023
Parameter
Arsenic
Cadmium
Copper
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Ceiling
Concentration Limits
(ClassA & ClassB)
(mg1kg)
75
85
4,300
840
57
75
420
100
7,500
Monthly Average
Concentration Limits
(Class A Only)
(mg1kg)
41
39
1,500
300
17
n/a
420
100
2,800
Result
(mg1kg)
ND
1.3
503.7
26.9
1.2
ND
52.0
5.1
818.3
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the
following metal parameters:
Laboratory: = and Date of analysis:
Distance from Disposal Unit to
Boundary to Closest Property
Line
(meters, check one)
>Obut <25
❑
> 25 but < 50
❑
> 50 but < 75
❑
> 75 but < 100
❑
> 100 but < 125
❑
> 125
Result (mg/kg)
Arsenic
Chromium
Nickel
(mg1kg)
(mg1kg)
(mg1kg)
30
200
210
34
220
240
39
260
270
46
300
320
53
360
390
62
450
420
FORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: M %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient
parameters:
Laboratory: Pace Analytical Services, LLC and Date of analysis: 09/11/2023
Parameter
Result
(mg1kg)
Aluminum
11,266.67
Ammonia -Nitrogen
2,483.33
Calcium
8,476.7
Magnesium
1,930.0
Nitrate -Nitrite Nitrogen
ND
pH (Standard Unit)
6.8
Phosphorus
9,706.67
Potassium
ND
Sodium ND
Total Kjeldahl Nitrogen 50,866.67
c. Using the results listed in Item IL 5b. above, calculate the sodium adsorption ration (SAR): 0_0
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the
Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an
agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g.,
gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN of the residuals: 30 %. This rate is a (check one):
default value, or actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the
selected default value is appropriate to be applied to these residuals: N_M_ is the fraction of oreanic N that is converted into inoreanic N in the soil.
Mineralization rates for conversion of Oreanic N to inoreanic N decrease with time and will be hiehest in year 1 and decrease each year throueh
ey ar 5.
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
Surface 16,998.33
Injection/Incorporation NA
First (1st) Year PAN
(mg1kg)
Five -Year
Maximum Adjusted PAN
(mglkg)
26,203.80
NA
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the
latest analyses: The residuals were also analyzed for PFAS content per the attached Analytical Report from Enthalpv Analytical, LLC — Ultratrace.
The results from this analysis indicated that the residuals contain very low levels of PFAS and are not currently industrially impacted. Refer to Section
3.1 of the Basis of Desien Report included in Appendix B of the DCAR Application submittal for detailed analysis and discussion of the PFAS
sampline and results.
FORM: RSC 06-16 Page 4 of 5

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
Alternative 1 [15ANCAC 02T. I 106(b)(3)(A)] - Time/Temperature Compliance.
q Alternative 2 [15A NCAC 02T. I 106(b)(3)(B)] - Alkaline Treatment.
q Alternative 3 [15A NCAC 02T.I106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
EJ Alternative 4 [15A NCAC 02T. I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.I106(b)(3)(E(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: composting, E heat drying, ❑ heat treatment,
thermophilic aerobic digestion, beta ray irradiation,
gamma ray irradiation, or i pasteurization.
b. For Land Application of Class B:
Alternative 1 [15A NCAC 02T. I 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02T. I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: aerobic digestion, air drying, ;] anaerobic digestion,
composting, or I lime stabilization.
c. For Surface Disposal.
Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
q Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
Exempt -If Daily Cover Alternative is chosen in Item I1.8. below [15A NCAC 02T.1106(a)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107. specify how residuals will meet the VAR requirements:
r
❑ Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
Alternative 2 [15A NCAC 02T. I 107(a)(2)] -
40-Day Bench Scale Test (Anaerobic Digestion).
E]
Alternative 3 [15A NCAC 02T. I 107(a)(3)] -
30-Day Bench Scale Test (Aerobic Digestion).
E]
Alternative 4 [15A NCAC 02T.I 107(a)(4)] -
Specific Oxygen Uptake Rate Test (Aerobic Digestion).
E]
Alternative 5 [15A NCAC 02T. I 107(a)(5)] -14-Day
Aerobic Processes.
E]
Alternative 6 [15A NCAC 02T.I 107(a)(6)] -
Alkaline Stabilization.
Alternative 7 [15A NCAC 02T.I 107(a)(7)] -
Drying of Stabilized Residuals.
E]
Alternative 8 [15A NCAC 02T. I 107(a)(8)] -
Drying of Unstabilized Residuals.
Alternative 9 [15A NCAC 02T. I 107(a)(9)] -
Injection.
❑
Alternative 10 [I5ANCAC 02T.I107(a)(10)] - Incorporation.
q
Alternative for Surface Disposal Units Only
- Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)].
J
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these
residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

ATTACHMENT I: RSC SUPPORTING INFORMATION
B. Residuals Source -Generating Facility Information:
A. Vicinity Map — Reference the vicinity map displayed on the cover sheet of the detailed plans
included in Appendix D of the NCDEQ DWR Non -Discharge Unit - Distribution of Class A
Residuals (DCAR) Application submittal.
B. Process Flow Diagram — Reference the Proposed WWTF Flow Diagram included in Appendix A
of the NCDEQ DWR Non -Discharge Unit - Distribution of Class A Residuals (DCAR)
Application submittal.
C. Quantitative justification for residuals production rate — The 2045 WWTF Solids Handling Mass
Balance summarized in the table below projects 4.85 dry tons per day of dewatered sludge
produced from the belt filter presses. This is calculated by summing 95% of the mass of the
thickened sludge from the gravity thickeners and 100% of the mass of the polymer to belt filter
press feed sludge. At this rate, 1770.25 dry tons per year of residuals are projected to be generated
at the facility under 2045 annual average daily conditions. Refer to Section 2 of the Basis of
Design Report included in Appendix B of the DCAR Application Submittal for detailed
descriptions of the projected residuals production rates.
2045 WWTF Solids Handling Mass Balance - AADF
Solids Flow Mass (dry Mass
Flow Stream Concentration (gpd) Ib/d) (DT/d)
Sludge from Clarifiers (WAS) 0.80% 168,389 11,235 5.62
Thickened Sludge from Gravity Thickeners 3.36% 35,376 10,111 5.06
Supernatant from Gravity Thickeners 0.10% 134,711 1,123 0.56
Polymer to Belt Filter Press Feed Sludge 0.50% 2,425 101 0.05
Dewatered Sludge from Belt Filter Press 17.50% 9,707 4.85
Filtrate from Belt Filter Press 0.19% 31,905 506 0.25
D. Sampling Plan — Reference the sampling plan included in the Supporting Documentation —
Operation and Maintenance Plan submitted with the NCDEQ DWR Non -Discharge Unit -
Distribution of Class A Residuals (DCAR) Application.
C. Residuals Quality Information:
A. Refer to Attachment V to the RSC Form containing the City of Lenoir's Lower Creek WWTP
Residuals Facility Annual Residuals Report for the 2023 calendar year. The report includes
analytical results and operational records from 2023 demonstrating the Gryphon Environmental
Model 1040 biosolids thermal dryer's ability to meet the Class A biosolids requirements. It is
important to note that the Gryphon Environmental Model 1040, which has been successfully
Hendersonville WWTF Biosolids Thermal Dryer September 2024
NCDEQ DWR Residuals Source Certification (RSC) Supporting Information
06496-0015 1

utilized at the Lower Creek WWTP, is nearly identical in design and functionality to the proposed
Model 1050 that is intended for installation at the Hendersonville WWTF. The primary distinction
lies in the capacity, with the Model 1050 designed to handle a larger volume of biosolids. This
similarity ensures that the operational success and compliance demonstrated by the Model 1040
can be expected from the Model 1050, thereby supporting its anticipated performance in the
Hendersonville facility.
II.5.c. SAR Value:
A. Refer to Attachment III to the RSC Form containing the 2024 Residuals Sampling Analytical
Results, including the SAR value for the biosolids on page 4 of 27 of the Pace Analytical Report
of Laboratory Analysis.
II.5.d. and II.5.e. PAN Calculations:
A. The equations to calculate PAN is as follows: PAN = NH4-N + (NO3-N + NO2-N) + NM. NM is the
fraction of organic N that is converted into inorganic N in the soil. Mineralization rates for
conversion of Organic N to inorganic N decrease with time and will be highest in year 1, and
decrease each year through year 5 for the purposes of these calculations.
Parameter Result (mg/kg)
NH4-N 2,483.33
NO3-N + NO2-N -
TKN 50,866.67
Organic-N (TKN -
NH4-N) 48, 383.34
Mineralization
Starting Org-N Rate
Year (mg/kg) (%)
1 48,383.34 30%
2 33,868.34 15%
3 28,788.09 8%
4 26,485.04 4%
5 25,425.64 3%
Org-N
Mineralized Remaining
Org-N (mg/kg) (mg/kg)
14,515.00 33,868.34
5,080.25 28,788.09
2,303.05 26,485.04
1,059.40 25,425.64
762.77 24,662.87
Note: Initial year Org-N mineralization rate per Table 3, Waste Type Municipal - Other; McGinnis, M.,
M. Buchanan, C. Stokes, and B. Cleveland. 2011. Waste and compost analysis guide. NC Dep.
Agric. Consumer Serv., Raleigh, NC
First Year PAN
(mg/kg)
5-Year Max. Adj.
PAN
(mg/kg)
Hendersonville WWTF Biosolids Thermal Dryer
NCDEQ DWR Residuals Source Certification (RSC) Supporting Information
06496-0015
September 2024
P"

16,998.33 1 26,203.80
Hendersonville WWTF Biosolids Thermal Dryer September 2024
NCDEQ DWR Residuals Source Certification (RSC) Supporting Information
06496-0015 3

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
September 15, 2023
Mr. Alexander Lillie
City of Hendersonville WWTP
99 Balfour Road
Hendersonville, NC 28792
RE: Project: DEWATERED SLUDGE 9/5/23
Pace Project No.: 92686384
Dear Mr. Lillie:
Enclosed are the analytical results for sample(s) received by the laboratory on September 06, 2023. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Katharine E Burnham
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 23

Project: DEWATERED SLUDGE 9/5/23
Pace Project No.: 92686384
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water#: LA029
Virginia/VELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 2 of 23

Project: DEWATERED SLUDGE 9/5/23
Pace Project No.: 92686384
Lab ID Sample ID
92686384001 DEWATERED SLUDGE 0950
92686384002 DEWATERED SLUDGE 1130
92686384003 DEWATERED SLUDGE 13:40
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
SAMPLE ANALYTE COUNT
Method
EPA 601 OD
EPA 7471 B
SM 254OG-2011
S W-846
EPA 160.4 / SM2540B-2011
EPA 9045D
EPA 350.1 Rev 2.0 1993 Mod
EPA 351.2 Rev 2.0 1993
EPA 353.2 Rev 2.0 1993
EPA 365.1 Rev 2.0 1993
EPA 601 OD
EPA 7471 B
SM 254OG-2011
S W-846
EPA 160.4 / SM254OB-2011
EPA 9045D
EPA 350.1 Rev 2.0 1993 Mod
EPA 351.2 Rev 2.0 1993
EPA 353.2 Rev 2.0 1993
EPA 365.1 Rev 2.0 1993
EPA 601 OD
EPA 7471B
SM 254OG-2011
S W-846
EPA 160.4 / SM254OB-2011
EPA 9045D
EPA 350.1 Rev 2.0 1993 Mod
EPA 351.2 Rev 2.0 1993
EPA 353.2 Rev 2.0 1993
EPA 365.1 Rev 2.0 1993
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Analytes
Analysts Reported Laboratory
DBB1
13
PASI-A
BM
1
PASI-A
KDF
1
PASI-C
KDF
1
PASI-C
RVS
1
PASI-A
YEG
1
PASI-A
ARJ
1
PASI-A
MFO
1
PASI-A
NCF
3
PASI-A
Zip
1
PASI-A
DBB1
13
PASI-A
BM
1
PASI-A
KDF
1
PASI-C
KDF
1
PASI-C
RVS
1
PASI-A
YEG
1
PASI-A
ARJ
1
PASI-A
MFO
1
PASI-A
NCF
3
PASI-A
Zip
1
PASI-A
DBB1
13
PASI-A
BM
1
PASI-A
KDF
1
PASI-C
KDF
1
PASI-C
RVS
1
PASI-A
YEG
1
PASI-A
ARJ
1
PASI-A
MFO
1
PASI-A
NCF
3
PASI-A
Zip
1
PASI-A
Page 3 of 23

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: DEWATERED SLUDGE 9/5/23
Pace Project No.: 92686384
Sample: DEWATERED SLUDGE Lab ID: 92686384001 Collected: 09/05/23 09:50 Received: 09/06/23 15:20 Matrix: Solid
0950
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
Aluminum
10600 mg/kg
48.9
1 09/11/23 09:18
09/11/23 17:42
7429-90-5
Arsenic
ND mg/kg
12.2
1 09/11/23 09:18
09/11/23 17:42
7440-38-2
Cadmium
1.2 mg/kg
0.49
1 09/11/23 09:18
09/11/23 17:42
7440-43-9
Calcium
8040 mg/kg
122
1 09/11/23 09:18
09/11/23 17:42
7440-70-2
Copper
481 mg/kg
24.4
1 09/11/23 09:18
09/11/23 17:42
7440-50-8
Lead
25.6 mg/kg
4.9
1 09/11/23 09:18
09/11/23 17:42
7439-92-1
Magnesium
1830 mg/kg
48.9
1 09/11/23 09:18
09/11/23 17:42
7439-95-4
Molybdenum
ND mg/kg
24.4
1 09/11/23 09:18
09/11/23 17:42
7439-98-7
Nickel
49.4 mg/kg
2.4
1 09/11/23 09:18
09/11/23 17:42
7440-02-0
Potassium
ND mg/kg
2440
1 09/11/23 09:18
09/11/23 17:42
7440-09-7
Selenium
ND mg/kg
4.9
1 09/11/23 09:18
09/11/23 17:42
7782-49-2
Sodium
ND mg/kg
2440
1 09/11/23 09:18
09/11/23 17:42
7440-23-5
Zinc
786 mg/kg
4.9
1 09/11/23 09:18
09/11/23 17:42
7440-66-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation Method:
EPA 7471 B
Pace Analytical Services - Asheville
Mercury
1.2 mg/kg
0.15
5 09/08/2314:40
09/12/2313:06
7439-97-6
2540G Total Percent Solids
Analytical Method: SM 2540G-2011
Pace Analytical Services - Charlotte
Total Solids
17.1 %
0.10
1
09/07/23 15:36
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
82.9 %
0.10
1
09/07/23 15:26
N2
160.4 Total Volatile Solids
Analytical Method: EPA 160.4 / SM2540B-2011
Pace Analytical Services - Asheville
Total Volatile Solids
696000 mg/kg
10000
1
09/07/23 18:24
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C
6.8 Std. Units
0.10
1
09/14/23 15:07
H3
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod.
Preparation Method:
EPA 350.1 Rev 2.0
1993 Mod.
Pace Analytical Services - Asheville
Nitrogen, Ammonia
2640 mg/kg
53.3
1 09/12/23 15:36
09/13/23 12:34
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Kjeldahl, Total
50700 mg/kg
2170
10 09/08/23 18:37
09/09/23 07:13
7727-37-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,
except in full,
Date: 09/15/2023 08:29 AM
without the written consent of Pace
Analytical
Services, LLC.
Page 4 of 23

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: DEWATERED SLUDGE 9/5/23
Pace Project No.: 92686384
Sample: DEWATERED SLUDGE Lab ID: 92686384001 Collected: 09/05/23 09:50 Received: 09/06/23 15:20 Matrix: Solid
0950
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, NO2 plus NO3
ND mg/kg 23.5 1 09/06/23 22:32 09/07/23 00:36 M1
Nitrogen, Nitrate
ND mg/kg 23.5 1 09/06/23 22:32 09/07/23 00:36 14797-55-8
Nitrogen, Nitrite
ND mg/kg 23.5 1 09/06/23 22:32 09/07/23 00:36 14797-65-0
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Phosphorus
9680 mg/kg 163 30 09/13/2314:18 09/14/2310:56 7723-14-0
Date: 09/15/2023 08:29 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 23

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: DEWATERED SLUDGE 9/5/23
Pace Project No.: 92686384
Sample: DEWATERED SLUDGE Lab ID: 92686384002 Collected: 09/05/23 11:30 Received: 09/06/23 15:20 Matrix: Solid
1130
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
Aluminum
11300 mg/kg
48.7
1 09/11/23 09:18
09/11/23 17:44
7429-90-5
Arsenic
ND mg/kg
12.2
1 09/11/23 09:18
09/11/23 17:44
7440-38-2
Cadmium
1.3 mg/kg
0.49
1 09/11/23 09:18
09/11/23 17:44
7440-43-9
Calcium
8370 mg/kg
122
1 09/11/23 09:18
09/11/23 17:44
7440-70-2
Copper
503 mg/kg
24.3
1 09/11/23 09:18
09/11/23 17:44
7440-50-8
Lead
26.4 mg/kg
4.9
1 09/11/23 09:18
09/11/23 17:44
7439-92-1
Magnesium
1920 mg/kg
48.7
1 09/11/23 09:18
09/11/23 17:44
7439-95-4
Molybdenum
ND mg/kg
24.3
1 09/11/23 09:18
09/11/23 17:44
7439-98-7
Nickel
52.5 mg/kg
2.4
1 09/11/23 09:18
09/11/23 17:44
7440-02-0
Potassium
ND mg/kg
2430
1 09/11/23 09:18
09/11/23 17:44
7440-09-7
Selenium
4.9 mg/kg
4.9
1 09/11/23 09:18
09/11/23 17:44
7782-49-2
Sodium
ND mg/kg
2430
1 09/11/23 09:18
09/11/23 17:44
7440-23-5
Zinc
824 mg/kg
4.9
1 09/11/23 09:18
09/11/23 17:44
7440-66-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation Method:
EPA 7471 B
Pace Analytical Services - Asheville
Mercury
1.6 mg/kg
0.11
5 09/08/2314:40
09/12/2313:14
7439-97-6
2540G Total Percent Solids
Analytical Method: SM 2540G-2011
Pace Analytical Services - Charlotte
Total Solids
17.4 %
0.10
1
09/07/23 15:36
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
82.6 %
0.10
1
09/07/23 15:26
N2
160.4 Total Volatile Solids
Analytical Method: EPA 160.4 / SM2540B-2011
Pace Analytical Services - Asheville
Total Volatile Solids
693000 mg/kg
10000
1
09/07/23 18:24
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C
6.8 Std. Units
0.10
1
09/14/23 15:11
H3
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod.
Preparation Method:
EPA 350.1 Rev 2.0
1993 Mod.
Pace Analytical Services - Asheville
Nitrogen, Ammonia
2400 mg/kg
52.2
1 09/12/23 15:36
09/13/23 12:35
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Kjeldahl, Total
50500 mg/kg
2870
10 09/08/23 18:37
09/09/23 07:14
7727-37-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,
except in full,
Date: 09/15/2023 08:29 AM
without the written consent of Pace
Analytical
Services, LLC.
Page 6 of 23

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: DEWATERED SLUDGE 9/5/23
Pace Project No.: 92686384
Sample: DEWATERED SLUDGE Lab ID: 92686384002 Collected: 09/05/23 11:30 Received: 09/06/23 15:20 Matrix: Solid
1130
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, NO2 plus NO3
ND mg/kg 22.9 1 09/06/23 22:32 09/07/23 00:40
Nitrogen, Nitrate
ND mg/kg 22.9 1 09/06/23 22:32 09/07/23 00:40 14797-55-8
Nitrogen, Nitrite
ND mg/kg 22.9 1 09/06/23 22:32 09/07/23 00:40 14797-65-0
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Phosphorus
9780 mg/kg 160 30 09/13/2314:18 09/14/2310:56 7723-14-0
Date: 09/15/2023 08:29 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 23

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: DEWATERED SLUDGE 9/5/23
Pace Project No.: 92686384
Sample: DEWATERED SLUDGE Lab ID: 92686384003 Collected: 09/05/23 13:40 Received: 09/06/23 15:20 Matrix: Solid
13:40
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
Aluminum
11900 mg/kg
50.2
1 09/11/23 09:18
09/11/23 17:47
7429-90-5
Arsenic
ND mg/kg
12.6
1 09/11/23 09:18
09/11/23 17:47
7440-38-2
Cadmium
1.4 mg/kg
0.50
1 09/11/23 09:18
09/11/23 17:47
7440-43-9
Calcium
9020 mg/kg
126
1 09/11/23 09:18
09/11/23 17:47
7440-70-2
Copper
527 mg/kg
25.1
1 09/11/23 09:18
09/11/23 17:47
7440-50-8
Lead
28.8 mg/kg
5.0
1 09/11/23 09:18
09/11/23 17:47
7439-92-1
Magnesium
2040 mg/kg
50.2
1 09/11/23 09:18
09/11/23 17:47
7439-95-4
Molybdenum
ND mg/kg
25.1
1 09/11/23 09:18
09/11/23 17:47
7439-98-7
Nickel
54.1 mg/kg
2.5
1 09/11/23 09:18
09/11/23 17:47
7440-02-0
Potassium
ND mg/kg
2510
1 09/11/23 09:18
09/11/23 17:47
7440-09-7
Selenium
5.3 mg/kg
5.0
1 09/11/23 09:18
09/11/23 17:47
7782-49-2
Sodium
ND mg/kg
2510
1 09/11/23 09:18
09/11/23 17:47
7440-23-5
Zinc
845 mg/kg
5.0
1 09/11/23 09:18
09/11/23 17:47
7440-66-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation Method:
EPA 7471 B
Pace Analytical Services - Asheville
Mercury
0.80 mg/kg
0.045
2 09/08/2314:40
09/12/2313:24
7439-97-6
2540G Total Percent Solids
Analytical Method: SM 2540G-2011
Pace Analytical Services - Charlotte
Total Solids
17.8 %
0.10
1
09/07/23 15:36
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
82.2 %
0.10
1
09/07/23 15:26
N2
160.4 Total Volatile Solids
Analytical Method: EPA 160.4 / SM2540B-2011
Pace Analytical Services - Asheville
Total Volatile Solids
691000 mg/kg
10000
1
09/07/23 18:25
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C
6.8 Std. Units
0.10
1
09/14/23 15:13
H3
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod.
Preparation Method:
EPA 350.1 Rev 2.0
1993 Mod.
Pace Analytical Services - Asheville
Nitrogen, Ammonia
2410 mg/kg
47.7
1 09/12/23 15:36
09/13/23 12:36
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Kjeldahl, Total
51400 mg/kg
2680
10 09/08/23 18:37
09/09/23 07:16
7727-37-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,
except in full,
Date: 09/15/2023 08:29 AM
without the written consent of Pace
Analytical
Services, LLC.
Page 8 of 23

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: DEWATERED SLUDGE 9/5/23
Pace Project No.: 92686384
Sample: DEWATERED SLUDGE Lab ID: 92686384003 Collected: 09/05/23 13:40 Received: 09/06/23 15:20 Matrix: Solid
13:40
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
353.2 Nitrogen, NO2/NO3 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, NO2 plus NO3 ND mg/kg 22.3 1 09/06/23 22:32 09/07/23 00:41
Nitrogen, Nitrate ND mg/kg 22.3 1 09/06/23 22:32 09/07/23 00:41 14797-55-8
Nitrogen, Nitrite ND mg/kg 22.3 1 09/06/23 22:32 09/07/23 00:41 14797-65-0
365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Phosphorus 9660 mg/kg 162 30 09/13/2314:18 09/14/2310:57 7723-14-0
Date: 09/15/2023 08:29 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 23

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: DEWATERED SLUDGE 9/5/23
Pace Project No.: 92686384
QC Batch: 798216 Analysis Method: EPA 7471 B
QC Batch Method: EPA 7471 B Analysis Description: 7471 Mercury
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92686384001, 92686384002, 92686384003
METHOD BLANK: 4134314 Matrix: Solid
Associated Lab Samples: 92686384001, 92686384002, 92686384003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Mercury
mg/kg
ND 0.0060
09/12/2312:26
LABORATORY CONTROL SAMPLE:
4134315
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Mercury
mg/kg
0.083
0.098
117 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4134316
4134317
MS
MSD
92685484018
Spike
Spike MS
MSD MS MSD % Rec
Parameter
Units Result
Conc.
Conc. Result
Result % Rec % Rec Limits RPD Qual
Mercury
mg/kg 0.019
0.087
0.09 0.12
0.11 113 107 75-125 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/15/2023 08:29 AM without the written consent of Pace Analytical Services, LLC.
Page 10 of 23

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: DEWATERED SLUDGE 9/5/23
Pace Project No.: 92686384
QC Batch: 798815
Analysis Method:
EPA6010D
QC Batch Method: EPA 3050B
Analysis Description:
6010 MET
Laboratory:
Pace Analytical Services - Asheville
Associated Lab Samples: 92686384001, 92686384002,
92686384003
METHOD BLANK: 4137316
Matrix: Solid
Associated Lab Samples: 92686384001, 92686384002,
92686384003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Aluminum
mg/kg
ND
10.0
09/11/2317:21
Arsenic
mg/kg
ND
2.5
09/11/2317:21
Cadmium
mg/kg
ND
0.10
09/11/2317:21
Calcium
mg/kg
ND
25.0
09/11/2317:21
Copper
mg/kg
ND
5.0
09/11/2317:21
Lead
mg/kg
ND
1.0
09/11/2317:21
Magnesium
mg/kg
ND
10.0
09/11/2317:21
Molybdenum
mg/kg
ND
5.0
09/11/2317:21
Nickel
mg/kg
ND
0.50
09/11/2317:21
Potassium
mg/kg
ND
500
09/11/2317:21
Selenium
mg/kg
ND
1.0
09/11/2317:21
Sodium
mg/kg
ND
500
09/11/2317:21
Zinc
mg/kg
ND
1.0
09/11/2317:21
LABORATORY CONTROL SAMPLE:
4137317
Spike
LCS
LCS %
Rec
Parameter
Units
Cone.
Result
% Rec Limits
Qualifiers
Aluminum
mg/kg
500
528
106
80-120
Arsenic
mg/kg
50
51.5
103
80-120
Cadmium
mg/kg
50
52.7
105
80-120
Calcium
mg/kg
500
533
107
80-120
Copper
mg/kg
50
53.3
107
80-120
Lead
mg/kg
50
53.1
106
80-120
Magnesium
mg/kg
500
506
101
80-120
Molybdenum
mg/kg
50
52.8
106
80-120
Nickel
mg/kg
50
52.8
106
80-120
Potassium
mg/kg
500
512
102
80-120
Selenium
mg/kg
50
49.4
99
80-120
Sodium
mg/kg
500
526
105
80-120
Zinc
mg/kg
50
52.6
105
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4137318
4137319
MS
MSD
92685964001
Spike
Spike
MS
MSD MS
MSD
% Rec
Parameter
Units Result
Cone.
Cone.
Result
Result % Rec % Rec
Limits RPD Qual
Aluminum
mg/kg 977
1550
1610
2620
2860
106 117
75-125 9
Arsenic
mg/kg ND
155
161
152
164
98 102
75-125 8
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/15/2023 08:29 AM without the written consent of Pace Analytical Services, LLC.
Page 11 of 23

QUALITY CONTROL DATA
Project: DEWATERED SLUDGE 9/5/23
Pace Project No.: 92686384
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
4137318
MS
92685964001
Spike
Parameter
Units
Result
Conc.
Cadmium
mg/kg
ND
155
Calcium
mg/kg
820
1550
Copper
mg/kg
ND
155
Lead
mg/kg
ND
155
Magnesium
mg/kg
242
1550
Molybdenum
mg/kg
ND
155
Nickel
mg/kg
2.4
155
Potassium
mg/kg
ND
1550
Selenium
mg/kg
ND
155
Sodium
mg/kg
ND
1550
Zinc
mg/kg
33.1
155
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
4137319
MSD
Spike MS MSD MS MSD % Rec
Conc. Result Result % Rec % Rec Limits RPD Qual
161 158 170 102 106 75-125 7
1610 2280 2710 94 118 75-125 17
161 167 180 107 111 75-125 7
161 160 172 103 106 75-125 7
1610 1710 1920 95 105 75-125 12
161 158 170 101 105 75-125 7
161 160 174 102 106 75-125 8
1610 1620 1760 100 106 75-125 9
161 147 158 95 98 75-125 7
1610 2260 2480 98 108 75-125 9
161 177 199 93 103 75-125 12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/15/2023 08:29 AM without the written consent of Pace Analytical Services, LLC.
Page 12 of 23

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: DEWATERED SLUDGE 9/5/23
Pace Project No.: 92686384
QC Batch: 798342 Analysis Method: SW-846
QC Batch Method: SW-846 Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92686384001, 92686384002, 92686384003
SAMPLE DUPLICATE: 4135071
92685748001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 9.4 9.2 3 N2
SAMPLE DUPLICATE: 4135072
92686258002 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 96.3 96.3 0 N2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/15/2023 08:29 AM without the written consent of Pace Analytical Services, LLC.
Page 13 of 23

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: DEWATERED SLUDGE 9/5/23
Pace Project No.: 92686384
QC Batch: 798406 Analysis Method: EPA 160.4 / SM2540B-2011
QC Batch Method: EPA 160.4 / SM2540B-2011 Analysis Description: 160.4 Total Volatile Solids
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92686384001, 92686384002, 92686384003
SAMPLE DUPLICATE: 4135445
92686384002 Dup
Parameter Units Result Result RPD Qualifiers
Total Volatile Solids mg/kg 693000 694000 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/15/2023 08:29 AM without the written consent of Pace Analytical Services, LLC.
Page 14 of 23

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: DEWATERED SLUDGE 9/5/23
Pace Project No.: 92686384
QC Batch: 799638 Analysis Method: EPA 9045D
QC Batch Method: EPA 9045D Analysis Description: 9045 pH
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92686384001, 92686384002, 92686384003
SAMPLE DUPLICATE: 4141747
92687211001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 5.6 5.4 2 H3
SAMPLE DUPLICATE: 4141748
92687211008 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 5.4 5.5 1 H3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/15/2023 08:29 AM without the written consent of Pace Analytical Services, LLC.
Page 15 of 23

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: DEWATERED SLUDGE 9/5/23
Pace Project No.: 92686384
QC Batch: 799078 Analysis Method: EPA 350.1 Rev 2.0 1993 Mod.
QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod. Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92686384001, 92686384002, 92686384003
METHOD BLANK: 4138738 Matrix: Solid
Associated Lab Samples: 92686384001, 92686384002, 92686384003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Nitrogen, Ammonia
mg/kg
ND 9.3
09/13/23 12:26
LABORATORY CONTROL SAMPLE:
4138739
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Nitrogen, Ammonia
mg/kg
439
455
104 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4138740
4138741
MS
MSD
92686409001
Spike
Spike MS
MSD MS MSD % Rec
Parameter
Units Result
Conc.
Conc. Result
Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia
mg/kg 1350
2510
2510 3950
3950 104 104 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/15/2023 08:29 AM without the written consent of Pace Analytical Services, LLC.
Page 16 of 23

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: DEWATERED SLUDGE 9/5/23
Pace Project No.: 92686384
QC Batch: 798539 Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92686384001, 92686384002, 92686384003
METHOD BLANK: 4135868 Matrix: Solid
Associated Lab Samples: 92686384001, 92686384002, 92686384003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Nitrogen, Kjeldahl, Total
mg/kg
ND 50.0
09/09/23 06:45
LABORATORY CONTROL SAMPLE:
4135869
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total
mg/kg
1000
1030
103 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4135870
4135871
MS
MSD
92686249001
Spike
Spike MS
MSD MS MSD % Rec
Parameter
Units Result
Conc.
Conc. Result
Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total
mg/kg 36300
4480
4290 43100
43600 153 171 90-110 1 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/15/2023 08:29 AM without the written consent of Pace Analytical Services, LLC.
Page 17 of 23

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: DEWATERED SLUDGE 9/5/23
Pace Project No.: 92686384
QC Batch: 798161
Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993
Analysis Description: 353.2 Nitrate + Nitrite
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92686384001, 92686384002,
92686384003
METHOD BLANK: 4134149
Matrix: Solid
Associated Lab Samples: 92686384001, 92686384002,
92686384003
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Nitrogen, Nitrate
mg/kg
ND 4.0
09/07/23 00:34
Nitrogen, Nitrite
mg/kg
ND 4.0
09/07/23 00:34
Nitrogen, NO2 plus NO3
mg/kg
ND 4.0
09/07/23 00:34
LABORATORY CONTROL SAMPLE:
4134150
Spike LCS
LCS % Rec
Parameter
Units
Cone. Result
% Rec Limits Qualifiers
Nitrogen, Nitrate
mg/kg
15 15.0
100 90-110
Nitrogen, Nitrite
mg/kg
10 10.2
102 90-110
Nitrogen, NO2 plus NO3
mg/kg
25 25.2
101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4134151 4134152
MS MSD
92686384001
Spike Spike MS
MSD MS MSD
% Rec
Parameter
Units Result
Cone. Cone. Result
Result % Rec % Rec
Limits RPD Qual
Nitrogen, Nitrate
mg/kg ND
87.4 87.4 98.9
102 113 117
90-110 3
Nitrogen, Nitrite
mg/kg ND
58 58 65.4
69.7 103 110
90-110 6
Nitrogen, NO2 plus NO3
mg/kg ND
145 145 164
172 111 116
90-110 4 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/15/2023 08:29 AM without the written consent of Pace Analytical Services, LLC.
Page 18 of 23

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: DEWATERED SLUDGE 9/5/23
Pace Project No.: 92686384
QC Batch: 799200 Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92686384001, 92686384002, 92686384003
METHOD BLANK: 4139452 Matrix: Solid
Associated Lab Samples: 92686384001, 92686384002, 92686384003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Phosphorus
mg/kg
ND 1.0
09/14/2310:50
LABORATORY CONTROL SAMPLE:
4139453
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Phosphorus
mg/kg
50
52.2
104 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4139454
4139455
MS
MSD
92685996001
Spike
Spike MS
MSD MS MSD % Rec
Parameter
Units Result
Conc.
Conc. Result
Result % Rec % Rec Limits RPD Qual
Phosphorus
mg/kg 108
74.5
74.5 224
261 156 205 90-110 15 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/15/2023 08:29 AM without the written consent of Pace Analytical Services, LLC.
Page 19 of 23

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALIFIERS
Project: DEWATERED SLUDGE 9/5/23
Pace Project No.: 92686384
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/15/2023 08:29 AM without the written consent of Pace Analytical Services, LLC. Page 20 of 23

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
DEWATERED SLUDGE 9/5/23
Pace Project No.:
92686384
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92686384001
DEWATERED
SLUDGE
0950
EPA 3050B
798815
EPA 6010D
798840
92686384002
DEWATERED
SLUDGE
1130
EPA 3050B
798815
EPA 6010D
798840
92686384003
DEWATERED
SLUDGE
13:40
EPA 3050B
798815
EPA 6010D
798840
92686384001
DEWATERED
SLUDGE
0950
EPA 7471 B
798216
EPA 7471 B
798604
92686384002
DEWATERED
SLUDGE
1130
EPA 7471 B
798216
EPA 7471 B
798604
92686384003
DEWATERED
SLUDGE
13:40
EPA 7471 B
798216
EPA 7471 B
798604
92686384001
DEWATERED
SLUDGE
0950
SM 2540G-2011
798597
92686384002
DEWATERED
SLUDGE
1130
SM 2540G-2011
798597
92686384003
DEWATERED
SLUDGE
13:40
SM 2540G-2011
798597
92686384001
DEWATERED
SLUDGE
0950
SW-846
798342
92686384002
DEWATERED
SLUDGE
1130
SW-846
798342
92686384003
DEWATERED
SLUDGE
13:40
SW-846
798342
92686384001
DEWATERED
SLUDGE
0950
EPA 160.4 / SM2540B-
798406
2011
92686384002
DEWATERED
SLUDGE
1130
EPA 160.4 / SM2540B-
798406
2011
92686384003
DEWATERED
SLUDGE
13:40
EPA 160.4 / SM2540B-
798406
2011
92686384001
DEWATERED
SLUDGE
0950
EPA 9045D
799638
92686384002
DEWATERED
SLUDGE
1130
EPA 9045D
799638
92686384003
DEWATERED
SLUDGE
13:40
EPA 9045D
799638
92686384001
DEWATERED
SLUDGE
0950
EPA 350.1 Rev 2.0
1993
799078
EPA 350.1 Rev 2.0
1993
799229
Mod.
Mod.
92686384002
DEWATERED
SLUDGE
1130
EPA 350.1 Rev 2.0
1993
799078
EPA 350.1 Rev 2.0
1993
799229
Mod.
Mod.
92686384003
DEWATERED
SLUDGE
13:40
EPA 350.1 Rev 2.0
1993
799078
EPA 350.1 Rev 2.0
1993
799229
Mod.
Mod.
92686384001
DEWATERED
SLUDGE
0950
EPA 351.2 Rev 2.0
1993
798539
EPA 351.2 Rev 2.0
1993
798675
92686384002
DEWATERED
SLUDGE
1130
EPA 351.2 Rev 2.0
1993
798539
EPA 351.2 Rev 2.0
1993
798675
92686384003
DEWATERED
SLUDGE
13:40
EPA 351.2 Rev 2.0
1993
798539
EPA 351.2 Rev 2.0
1993
798675
92686384001
DEWATERED
SLUDGE
0950
EPA 353.2 Rev 2.0
1993
798161
EPA 353.2 Rev 2.0
1993
798165
92686384002
DEWATERED
SLUDGE
1130
EPA 353.2 Rev 2.0
1993
798161
EPA 353.2 Rev 2.0
1993
798165
92686384003
DEWATERED
SLUDGE
13:40
EPA 353.2 Rev 2.0
1993
798161
EPA 353.2 Rev 2.0
1993
798165
92686384001
DEWATERED
SLUDGE
0950
EPA 365.1 Rev 2.0
1993
799200
EPA 365.1 Rev 2.0
1993
799473
92686384002
DEWATERED
SLUDGE
1130
EPA 365.1 Rev 2.0
1993
799200
EPA 365.1 Rev 2.0
1993
799473
92686384003
DEWATERED
SLUDGE
13:40
EPA 365.1 Rev 2.0
1993
799200
EPA 365.1 Rev 2.0
1993
799473
Date: 09/15/2023 08:29 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 21 of 23

"Alii
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CHAIR[ -OF -CUSTODY Analytical Request Document
Company:
Address: j 9 g J.7� f 11A r al p!
Report To: 1
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Copy To: J(_n `I
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Customer Project Name/Number:
Chain -of -Custody is a LEGAL DOCUMENT - Complete all relevent fields
Billing Information:
Email To:
Site Collection Info/Address:
State: County)/!City: Time Zone Collected:
NCI 1j ,tie— [ ]PT[ ]MT[ ]CT WET
Phone: oaf 3o i
Email: J `~ ry
site/ acility ID #:
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Compliance Monitoring?
kj Yes [ )No
Collected By (print):
Co e e By (signature):
Sample Disposal:
[7[Dispose as appropriate [ ] Return
Purchase#:
Quote #: N'PnO-
Turnaround Date Required:
Ala
Rush: sw - (yL I
[ ] Same Day [ ] Next Day
DW PWS ID #:
DW Location Code:
Imme late y Pace on Ice:
(Y] Yes [ ] No
Held Filtered (if applicable):
[ i Yes [ ]NO
I ] Archive:
] ] 2 Day [ ] 3 Day [ ] 4 Day [ ] S Day
Analysis,
( ] Hold'
(Expedite Charges Apply)
* Matrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water Oft Wastewater(WW),
Product (P), Soil/Solid (SLJ, Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT)
Comp / Collected (or Res lit of
End
i Customer Sample ID
Matrix Grab Compo:ICe Start)Composite
Cl Ctns
Date Time Date Time
�itZW�t�mr�� Slu,l�-�T
,�
9"�-23 �9�� A//ri rr�
.. ►I
�� �� 9f_?T)J30
\• .t
►, 9,5-t.3 (349 :1�
Customer Remarks / Special Conditions / Possible Hazards: Type of Ice Used:
LAB USE ONLY -Affix Woi WO# ; 92686384
ALL SHAI
92686384
" Preservative Types. (1) nitric acid, (2) sulfuric acid, (3) hydrochloric acid, (4) sodium hydroxide, (5) zinc acetate,
(6) methanol, (7) sodium bisulfate, (S) sodium thiosulfate, (9) hexane, {A) ascorbic acid, (B) ammonium sulfate,
(C) ammonium hydroxide, (D) TSP, (U) Unpreserved, (0) other
Analyses Lab Profile/Line:
Lab Sample Receipt Checklist:
Custody Seals Present/Intact )�
Custody Signatures Present NA
Collector Signature Present Y NA
Bottles Intact NA
Correct Bottles ' NA
t�
Sufficient Volume NA
Samples Received on Ice NA
VOA - Headspace Acceptable Y N
.rJ
USDA Regulatod Boils Y N&
Samples in Holding Time Q✓N
Residual Chlorine Present N A7
•
!)
Cl Strips:
Sample pH A ejtable N(�t�A }
J1
PH Strips:
Sulfide Present Y N (AD
�
Lead Acetate Strips:
�3
`
LAB USE ONLY:
rt
Lab Sample # / Comments:
o
X
XXXXxx
-/70�
Blue Dry None (SHORT HOLDS PRESENT (<72 hours): W N N/A
Packing Material Used: n / Lab Tracking #: �� 2 8 13
,.,
I t I I w1� , 7 Radchem samples) screened (<Soo cpm): Y N A Samples received via:
'V '[ L ) FEDEX UPS Client
+Relinquished by/Company: (Signature) Date/Time: leceived by/Company: (Signature) Date/Time:
Y� 1z
Relinquished by/Company: (Signature) Date/Time: I teceived by/Comp y: (Si Date/Time:
--Q z . a I um a,,t v/&/z3 /52z
Relinquished by/Company: (Sfgnature)----_� Date/Time: 1 Received by/Company: (5ignature) Date/Time:
CourierC-Pace CourieCourie
MT1L LAB USE ONLY
Table #:
Acctnum:
(Template:
PM:
PB:
Lab Sample Temperature Info:
Temp Blank Received: Y N
Therm ID#: -`( .� [ oyzNA.
Cooler 1 Temp Upon Receipt: S_�LoC
Cooler 1 Therm Corr. Factor: 0 oC
Cooler 1 Corrected Temp: �oC
Comments:
Trip Blank Received: Y N (
HCL McOH TSP Other
Non Conformance(s): PAge 22 of 23
YES / NO I of:

O o
o ?
4 �
a m
zi
o SO
rD
� a
R 1
ru w
w
aro
m
a
ro
o �
c v
tA
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a
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a
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w
m
d
3
m
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ro
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a
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a CD
CD
C
A n at
s R tA
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a �
I
BP4U 125-m.L P1astfc Unpreserv" (N/A) (CI-)
BR3U=350.mLPlastic Unpreserved{N/A)
Bp2U-504'mL Plastic Unpreserved (N/A)
i BPSU-1:1iter PlasticUnpreaerved (N/A)
�i BP4S425:mLPlasticH2S.Gl4.(p+t2j(CI}
BP3N-250 mL plgstic HNO3.- (PH :<22) ..
13P4Z125MLFlastic:ZNAce44e=&NaOR(4)
BP4U-125 rnLPlastic NaOH (pH.>12) (C1-}
! WGrU-Wlde-mouthed Gless]ar UnPraserye{
AG1U-1JlterArriber Unpreserved N/A1.(09.
I
ACR1M-7.Iite.rArnberHC1(pH<2)
A133U-2.50 mL Amber Unpreserved (N/A) (CI-)
AG25=1IRer:.knberH2SO4(pH i2),
AG35-250 rr L.Amber K2S94 (pH <Z)
::DG94-40 mLAmber NH4.CI (N/A)(CI-)
DG9 H-40 m L VpA HCI'(N/A)
VG9T-40!n L VOA Na2S209 (N/A)
VG9U4.0 mL.VUA-Unpreserved (14 -
OG9Y-40 rnL VOA H3Po4 (N/A)
0
KM-50 mL Plastic Vn.preservgd (N/A)
V/GK (3 vialsPer kit): VPH/Gas ktt(N/A)
SP5T-125.mL;5terilt;Plastic (NIA —lab.)
SM259 mLS dle Plastic (NIA —lab)
SM-250 mL Plastic (NH2)25D4 (93.-9:7)
AG4U-300 mL ArnbgrUnpreservsd
Y56U-2D m4.scintillatjan vials {N/A}
©69U-40 mL Amber Unpressfved vlals,(N/A)
s 4 n
I� S C-m
0
�2'
m tr a m :r
x ~�.= d
rL Cf c
CL
Cr AD IN
CL
W A
. c
a=a ro
C-
tz
't7
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1n" 3
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(D . .
W , ^
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N
N
F v
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f C
ID CO
o
[o
OD
N
W
A
Page 23 of 23

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
July 26, 2024
Mr. Alexander Lillie
City of Hendersonville WWTP
99 Balfour Road
Hendersonville, NC 28792
RE: Project: CLASS B SLUDGE
Pace Project No.: 92740056
Dear Mr. Lillie:
Enclosed are the analytical results for sample(s) received by the laboratory on July 03, 2024. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni for
Katharine E Burnham
[e-mail]
828-417-6061
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 27

Project: CLASS B SLUDGE
Pace Project No.: 92740056
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water#: LA029
Virginia/VELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 2 of 27

Project: CLASS B SLUDGE
Pace Project No.: 92740056
Lab ID Sample ID
92740056001 DEWATERING SLUDGE
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Analytes
Method
Analysts
Reported
Laboratory
EPA 8081 B
SEM
9
PASI-C
EPA 8082A
BAJ
8
PASI-C
EPA 601OD
DBB1
1
PASI-A
EPA 601OD
DBB1
9
PASI-A
EPA 601 OD
EWS
1
PASI-A
EPA 7470A
KML
1
PASI-A
EPA 8270E
ICO
18
PASI-C
EPA 8260D
SAS
14
PASI-C
SW-846
CHC
1
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 27

ANALYTICAL RESULTS
Project: CLASS B SLUDGE
Pace Project No.: 92740056
Sample: DEWATERING SLUDGE Lab ID: 92740056001 Collected: 07/02/24 14:33 Received: 07/03/24 11:47
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Matrix: Solid
CAS No. Qual
8081 TCLP Pesticides RVE
Analytical Method: EPA 8081 B Preparation Method: EPA 3510C
Leachate Method/Date: EPA 1311; 07/05/24 16:40
Initial
pH: 5.73; Final
pH: 5
Pace Analytical Services - Charlotte
gamma-BHC (Lindane)
ND ug/L
0.50
1
07/08/24 22:23
07/09/24 13:55
58-89-9
Chlordane (Technical)
ND ug/L
3.0
1
07/08/24 22:23
07/09/24 13:55
57-74-9
Endrin
ND ug/L
0.50
1
07/08/24 22:23
07/09/24 13:55
72-20-8
Heptachlor
ND ug/L
0.50
1
07/08/24 22:23
07/09/24 13:55
76-44-8
Heptachlor epoxide
ND ug/L
0.50
1
07/08/24 22:23
07/09/24 13:55
1024-57-3
Methoxychlor
ND ug/L
1000
1
07/08/24 22:23
07/09/24 13:55
72-43-5
Toxaphene
ND ug/L
3.0
1
07/08/24 22:23
07/09/24 13:55
8001-35-2
Surrogates
Decachlorobiphenyl (S)
129 %
19-200
1
07/08/24 22:23
07/09/24 13:55
2051-24-3
Tetrachloro-m-xylene (S)
113 %
10-137
1
07/08/24 22:23
07/09/24 13:55
877-09-8
8082 GCS PCB
Analytical Method: EPA 8082A Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
PCB-1016 (Aroclor 1016)
ND ug/kg
187
1
07/09/24 10:36
07/10/24 18:24
12674-11-2
PCB-1221 (Aroclor 1221)
ND ug/kg
187
1
07/09/24 10:36
07/10/24 18:24
11104-28-2
PCB-1232 (Aroclor 1232)
ND ug/kg
187
1
07/09/24 10:36
07/10/24 18:24
11141-16-5
PCB-1242 (Aroclor 1242)
ND ug/kg
187
1
07/09/24 10:36
07/10/24 18:24
53469-21-9
PCB-1248 (Aroclor 1248)
ND ug/kg
187
1
07/09/24 10:36
07/10/24 18:24
12672-29-6
PCB-1254 (Aroclor 1254)
ND ug/kg
187
1
07/09/24 10:36
07/10/24 18:24
11097-69-1
PCB-1260 (Aroclor 1260)
ND ug/kg
187
1
07/09/24 10:36
07/10/24 18:24
11096-82-5
Surrogates
Decachlorobiphenyl (S)
70 %
10-174
1
07/09/24 10:36
07/10/24 18:24
2051-24-3
6010 MET ICP
Analytical Method: EPA6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
Sodium
ND mg/kg
1890
1
07/17/2414:18
07/18/2410:12
7440-23-5
6010 MET ICP, TCLP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 07/05/24 16:40
Initial
pH: 5.73; Final
pH: 5
Pace Analytical Services - Asheville
Arsenic
ND mg/L
0.050
1
07/09/24 00:57
07/09/24 14:17
7440-38-2
Barium
ND mg/L
0.25
1
07/09/24 00:57
07/09/24 14:17
7440-39-3
Cadmium
ND mg/L
0.0050
1
07/09/24 00:57
07/09/24 14:17
7440-43-9
Calcium
43.1 mg/L
1.0
1
07/09/24 00:57
07/09/24 14:17
7440-70-2
Chromium
ND mg/L
0.050
1
07/09/24 00:57
07/09/24 14:17
7440-47-3
Lead
ND mg/L
0.025
1
07/09/24 00:57
07/09/24 14:17
7439-92-1
Magnesium
14.3 mg/L
0.50
1
07/09/24 00:57
07/09/24 14:17
7439-95-4
Selenium
ND mg/L
0.10
1
07/09/24 00:57
07/09/24 14:17
7782-49-2
Silver
ND mg/L
0.025
1
07/09/24 00:57
07/09/24 14:17
7440-22-4
Sodium Adsorption Ratio, SAR
Analytical Method: EPA 6010D
Pace Analytical Services - Asheville
Sodium Adsorption Ratio
0.0 meq/L
1
07/26/24 10:16
REPORT OF LABORATORY ANALYSIS
N2
This report shall not be reproduced, except in full,
Date: 07/26/2024 06:37 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 27

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: CLASS B SLUDGE
Pace Project No.: 92740056
Sample: DEWATERING SLUDGE
Lab ID: 92740056001 Collected:
07/02/24
14:33
Received: 07/03/24 11:47 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture,
sample size and any dilutions.
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
7470 Mercury, TCLP
Analytical Method:
EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311; 07/05/24 16:40
Initial pH: 5.73; Final
pH: 5
Pace Analytical
Services - Asheville
Mercury
ND
mg/L
0.00020
1
07/09/24 04:35
07/09/24 17:40
7439-97-6
8270E TCLP RVE
Analytical Method:
EPA 8270E Preparation Method:
EPA 3510C
Leachate Method/Date: EPA 1311; 07/05/24 16:40
Initial pH: 5.73; Final
pH: 5
Pace Analytical
Services - Charlotte
1,4-Dichlorobenzene
ND
ug/L
50.0
1
07/08/24 22:24
07/10/24 12:47
106-46-7
2,4-Dinitrotoluene
ND
ug/L
50.0
1
07/08/24 22:24
07/10/24 12:47
121-14-2
Hexachloro-1,3-butadiene
ND
ug/L
50.0
1
07/08/24 22:24
07/10/24 12:47
87-68-3
Hexachlorobenzene
ND
ug/L
50.0
1
07/08/24 22:24
07/10/24 12:47
118-74-1
Hexachloroethane
ND
ug/L
50.0
1
07/08/24 22:24
07/10/24 12:47
67-72-1
2-Methyl phenol(o-Cresol)
ND
ug/L
50.0
1
07/08/24 22:24
07/10/24 12:47
95-48-7
3&4-Methylphenol (m&p Cresol)
81.8
ug/L
50.0
1
07/08/24 22:24
07/10/24 12:47
15831-10-4
Nitrobenzene
ND
ug/L
50.0
1
07/08/24 22:24
07/10/24 12:47
98-95-3
Pentachlorophenol
ND
ug/L
100
1
07/08/24 22:24
07/10/24 12:47
87-86-5
Pyridine
ND
ug/L
50.0
1
07/08/24 22:24
07/10/24 12:47
110-86-1
2,4,5-Trichlorophenol
ND
ug/L
50.0
1
07/08/24 22:24
07/10/24 12:47
95-95-4
2,4,6-Trichlorophenol
ND
ug/L
50.0
1
07/08/24 22:24
07/10/24 12:47
88-06-2
Surrogates
Nitrobenzene-d5 (S)
61
%
10-133
1
07/08/24 22:24
07/10/24 12:47
4165-60-0
2-Fluorobiphenyl (S)
63
%
10-130
1
07/08/24 22:24
07/10/24 12:47
321-60-8
Terphenyl-d14 (S)
69
%
10-193
1
07/08/24 22:24
07/10/24 12:47
1718-51-0
Phenol-d6 (S)
39
%
10-130
1
07/08/24 22:24
07/10/24 12:47
13127-88-3
2-Fluorophenol (S)
52
%
10-130
1
07/08/24 22:24
07/10/24 12:47
367-12-4
2,4,6-Tribromophenol (S)
89
%
10-166
1
07/08/24 22:24
07/10/24 12:47
118-79-6
8260D MSV TCLP
Analytical Method:
EPA 8260D Leachate Method/Date:
EPA 1311; 07/10/24 13:58
Pace Analytical
Services - Charlotte
Benzene
ND
ug/L
100
20
07/11/24 20:36
71-43-2
2-Butanone (MEK)
ND
ug/L
200
20
07/11/24 20:36
78-93-3
Carbon tetrachloride
ND
ug/L
100
20
07/11/24 20:36
56-23-5
Chlorobenzene
ND
ug/L
100
20
07/11/24 20:36
108-90-7
Chloroform
ND
ug/L
100
20
07/11/24 20:36
67-66-3
1,4-Dichlorobenzene
ND
ug/L
100
20
07/11/24 20:36
106-46-7
1,2-Dichloroethane
ND
ug/L
100
20
07/11/24 20:36
107-06-2
1,1-Dichloroethene
ND
ug/L
100
20
07/11/24 20:36
75-35-4
Tetrachloroethene
ND
ug/L
100
20
07/11/24 20:36
127-18-4 J(M1)
Trichloroethene
ND
ug/L
100
20
07/11/24 20:36
79-01-6
Vinyl chloride
ND
ug/L
100
20
07/11/24 20:36
75-01-4
Surrogates
1,2-Dichloroethane-d4 (S)
114
%
70-130
20
07/11/24 20:36
17060-07-0
Toluene-d8 (S)
103
%
70-130
20
07/11/24 20:36
2037-26-5
4-Bromofluorobenzene (S)
98
%
70-130
20
07/11/24 20:36
460-00-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/26/2024 06:37 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 27

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: CLASS B SLUDGE
Pace Project No.: 92740056
Sample: DEWATERING SLUDGE Lab ID: 92740056001 Collected: 07/02/24 14:33 Received: 07/03/24 11:47 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture 82.6 % 0.10 1 07/05/24 11:45 N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/26/2024 06:37 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 27

Project: CLASS B SLUDGE
Pace Project No.: 92740056
QC Batch: 866707
QC Batch Method: EPA 7470A
Associated Lab Samples: 92740056001
METHOD BLANK: 4465626
Associated Lab Samples: 92740056001
Parameter Units
Mercury mg/L
LABORATORY CONTROL SAMPLE: 4467439
Parameter Units
Mercury mg/L
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 7470A
Analysis Description: 7470 Mercury TCLP
Laboratory: Pace Analytical Services - Asheville
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.00020 07/09/2417:21
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
0.0025 0.0025 99 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4467440 4467441
MS MSD
92739996001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/L ND 0.0025 0.0025 0.0024 0.0025 96 99 75-125 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/26/2024 06:37 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 27

Project: CLASS B SLUDGE
Pace Project No.: 92740056
QC Batch: 868926
QC Batch Method: EPA 3050B
Associated Lab Samples: 92740056001
METHOD BLANK: 4478325
Associated Lab Samples: 92740056001
Parameter Units
Sodium mg/kg
LABORATORY CONTROL SAMPLE: 4478326
Parameter Units
Sodium mg/kg
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA6010D
Analysis Description: 6010 MET
Laboratory: Pace Analytical Services - Asheville
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 500 07/18/2410:06
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
500 561 112 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4478327 4478328
MS MSD
92740056001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sodium mg/kg ND 1920 1870 2510 2440 101 100 75-125 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/26/2024 06:37 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 27

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: CLASS B SLUDGE
Pace Project No.: 92740056
QC Batch: 866706
Analysis Method:
EPA 601 OD
QC Batch Method: EPA 3010A
Analysis Description:
6010 MET TCLP
Laboratory:
Pace Analytical Services - Asheville
Associated Lab Samples: 92740056001
METHOD BLANK: 4465626
Matrix: Water
Associated Lab Samples: 92740056001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Arsenic
mg/L
ND
0.050
07/09/2413:48
Barium
mg/L
ND
0.25
07/09/2413:48
Cadmium
mg/L
ND
0.0050
07/09/2413:48
Calcium
mg/L
ND
1.0
07/09/2413:48
Chromium
mg/L
ND
0.050
07/09/2413:48
Lead
mg/L
ND
0.025
07/09/2413:48
Magnesium
mg/L
ND
0.50
07/09/2413:48
Selenium
mg/L
ND
0.10
07/09/2413:48
Silver
mg/L
ND
0.025
07/09/2413:48
LABORATORY CONTROL SAMPLE:
4467436
Spike
LCS
LCS % Rec
Parameter
Units
Cone.
Result
% Rec Limits
Qualifiers
Arsenic
mg/L
2.5
2.4
98
80-120
Barium
mg/L
2.5
2.4
95
80-120
Cadmium
mg/L
2.5
2.4
95
80-120
Calcium
mg/L
25
23.1
93
80-120
Chromium
mg/L
2.5
2.4
95
80-120
Lead
mg/L
2.5
2.4
95
80-120
Magnesium
mg/L
25
25.7
103
80-120
Selenium
mg/L
2.5
2.5
99
80-120
Silver
mg/L
1.2
1.2
96
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4467437
4467438
MS
MSD
92739996001
Spike
Spike
MS
MSD MS MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result % Rec
% Rec
Limits
RPD
Arsenic
mg/L
ND
2.5
2.5
2.7
2.8
110
113
75-125
2
Barium
mg/L
ND
2.5
2.5
2.7
2.8
107
110
75-125
3
Cadmium
mg/L
ND
2.5
2.5
2.7
2.8
107
110
75-125
3
Calcium
mg/L
ND
25
25
27.3
27.9
107
110
75-125
2
Chromium
mg/L
ND
2.5
2.5
2.7
2.7
107
109
75-125
3
Lead
mg/L
ND
2.5
2.5
2.7
2.8
107
110
75-125
3
Magnesium
mg/L
ND
25
25
28.8
29.4
115
117
75-125
2
Selenium
mg/L
ND
2.5
2.5
2.8
2.8
111
114
75-125
2
Silver
mg/L
ND
1.2
1.2
1.3
1.4
107
110
75-125
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/26/2024 06:37 PM without the written consent of Pace Analytical Services, LLC.
Qual
Page 9 of 27

Project:
CLASS B SLUDGE
Pace Project No.:
92740056
QC Batch:
867507
QC Batch Method:
EPA 8260D
Associated Lab Samples: 92740056001
METHOD BLANK: 4471436
Associated Lab Samples: 92740056001
Parameter
1,1-Dichloroethene
1,2-Dichloroethane
1,4-Dichlorobenzene
2-Butanone (MEK)
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
Tetrachloroethene
Trichloroethene
Vinyl chloride
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
QUALITY CONTROL DATA
Analysis Method:
Analysis Description
Laboratory:
Matrix: Water
EPA 8260D
8260D MSV TCLP
Pace Analytical Services - Charlotte
Blank
Reporting
Units
Result
Limit
Analyzed
ug/L
ND
5.0
07/11/2412:31
ug/L
ND
5.0
07/11/2412:31
ug/L
ND
5.0
07/11/2412:31
ug/L
ND
10.0
07/11/2412:31
ug/L
ND
5.0
07/11/2412:31
ug/L
ND
5.0
07/11/2412:31
ug/L
ND
5.0
07/11/2412:31
ug/L
ND
5.0
07/11/2412:31
ug/L
ND
5.0
07/11/2412:31
ug/L
ND
5.0
07/11/2412:31
ug/L
ND
5.0
07/11/2412:31
%
117
70-130
07/11/2412:31
%
96
70-130
07/11/2412:31
%
103
70-130
07/11/2412:31
Qualifiers
LABORATORY CONTROL SAMPLE:
4471435
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
1,1-Dichloroethene
ug/L
20
23.0
115
69-131
1,2-Dichloroethane
ug/L
20
21.9
110
70-130
1,4-Dichlorobenzene
ug/L
20
19.8
99
70-130
2-Butanone (MEK)
ug/L
40
38.8
97
67-133
Benzene
ug/L
20
20.8
104
70-130
Carbon tetrachloride
ug/L
20
19.7
99
70-130
Chlorobenzene
ug/L
20
19.8
99
70-130
Chloroform
ug/L
20
21.4
107
70-130
Tetrachloroethene
ug/L
20
18.0
90
70-130
Trichloroethene
ug/L
20
19.8
99
70-130
Vinyl chloride
ug/L
20
23.1
115
66-140
1,2-Dichloroethane-d4 (S)
%
111
70-130
4-Bromofluorobenzene (S)
%
105
70-130
Toluene-d8 (S)
%
101
70-130
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/26/2024 06:37 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 27

QUALITY CONTROL DATA
Project: CLASS B SLUDGE
Pace Project No.: 92740056
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
4471437
MS
92740056001
Spike
Parameter
Units
Result
Cone.
1,1-Dichloroethene
ug/L
ND
20
1,2-Dichloroethane
ug/L
ND
20
1,4-Dichlorobenzene
ug/L
ND
20
2-Butanone (MEK)
ug/L
ND
40
Benzene
ug/L
ND
20
Carbon tetrachloride
ug/L
ND
20
Chlorobenzene
ug/L
ND
20
Chloroform
ug/L
ND
20
Tetrachloroethene
ug/L
ND
20
Trichloroethene
ug/L
ND
20
Vinyl chloride
ug/L
ND
20
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
4471438
MSD
Spike
MS
MSD
MS
MSD
% Rec
Cone.
Result
Result
% Rec
% Rec
Limits RPD
20
ND
ND
110
111
64-162
20
ND
ND
109
102
68-145
20
ND
ND
103
94
70-140
40
1871
1921
70
82
57-156
20
ND
ND
104
98
68-144
20
ND
ND
78
89
70-147
20
ND
ND
104
100
70-143
20
ND
ND
110
109
67-148
20
ND
ND
48
51
70-145
20
ND
ND
80
81
70-152
20
ND
ND
89
92
51-178
113
115
70-130
98
97
70-130
103
103
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/26/2024 06:37 PM without the written consent of Pace Analytical Services, LLC.
Qual
J(M1)
Page 11 of 27

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: CLASS B SLUDGE
Pace Project No.: 92740056
QC Batch: 866613
Analysis Method:
EPA 8081 B
QC Batch Method: EPA 3510C
Analysis Description:
8081 TCLP Pesticides
RV
Laboratory:
Pace Analytical Services - Charlotte
Associated Lab Samples: 92740056001
METHOD BLANK: 4465433
Matrix: Water
Associated Lab Samples: 92740056001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Chlordane (Technical)
ug/L
ND
3.0
07/09/24 15:02
Endrin
ug/L
ND
0.50
07/09/24 15:02
gamma-BHC (Lindane)
ug/L
ND
0.50
07/09/24 15:02
Heptachlor
ug/L
ND
0.50
07/09/24 15:02
Heptachlor epoxide
ug/L
ND
0.50
07/09/24 15:02
Methoxychlor
ug/L
ND
1000
07/09/24 15:02
Toxaphene
ug/L
ND
3.0
07/09/24 15:02
Decachlorobiphenyl (S)
%
140
19-200
07/09/24 15:02
Tetrachloro-m-xylene (S)
%
125
10-137
07/09/24 15:02
LABORATORY CONTROL SAMPLE:
4466953
Spike
LCS
LCS %
Rec
Parameter
Units
Cone.
Result
% Rec Limits
Qualifiers
Endrin
ug/L
1.2
1.8
142
33-190
gamma-BHC (Lindane)
ug/L
1.2
1.7
134
32-148
Heptachlor
ug/L
1.2
1.8
142
32-149
Heptachlor epoxide
ug/L
1.2
1.6
124
37-149
Methoxychlor
ug/L
3.8
4.71
125
35-171
Decachlorobiphenyl (S)
%
150
19-200
Tetrachloro-m-xylene (S)
%
144
10-137 J(SO)
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4466954
4466955
MS
MSD
92740056001
Spike
Spike
MS
MSD MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result % Rec % Rec
Limits RPD Qual
Endrin
ug/L
ND
1.2
1.2
1.5
1.7
116 132
10-200 13
gamma-BHC (Lindane)
ug/L
ND
1.2
1.2
1.5
1.7
119 136
13-163 13
Heptachlor
ug/L
ND
1.2
1.2
1.4
1.7
111 139
10-172 22
Heptachlor epoxide
ug/L
ND
1.2
1.2
1.2
1.4
96 111
10-168 15
Methoxychlor
ug/L
ND
3.8
3.8
3.71
4.21
99 113
13-183
Decachlorobiphenyl (S)
%
132 140
19-200
Tetrachloro-m-xylene (S)
%
115 128
10-137
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/26/2024 06:37 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 27

Project:
CLASS B SLUDGE
Pace Project No.:
92740056
QC Batch:
866673
QC Batch Method:
EPA 3546
Associated Lab Samples: 92740056001
QUALITY CONTROL DATA
Analysis Method: EPA 8082A
Analysis Description: 8082 GCS PCB
Laboratory: Pace Analytical Services - Charlotte
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
METHOD BLANK: 4467238
Matrix:
Solid
Associated Lab Samples: 92740056001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
PCB-1016 (Aroclor 1016)
ug/kg
ND
32.5
07/10/24 12:31
PCB-1221 (Aroclor 1221)
ug/kg
ND
32.5
07/10/24 12:31
PCB-1232 (Aroclor 1232)
ug/kg
ND
32.5
07/10/24 12:31
PCB-1242 (Aroclor 1242)
ug/kg
ND
32.5
07/10/24 12:31
PCB-1248 (Aroclor 1248)
ug/kg
ND
32.5
07/10/24 12:31
PCB-1254 (Aroclor 1254)
ug/kg
ND
32.5
07/10/24 12:31
PCB-1260 (Aroclor 1260)
ug/kg
ND
32.5
07/10/24 12:31
Decachlorobiphenyl (S)
%
86
10-174
07/10/24 12:31
LABORATORY CONTROL SAMPLE & LCSD:
4467239
4467240
Spike
LCS LCSD
LCS LCSD
% Rec Max
Parameter
Units
Conc.
Result Result
% Rec % Rec
Limits RPD RPD Qualifiers
PCB-1016 (Aroclor 1016)
ug/kg
169
124 86.9
73 52
36-130 35 30 J(R1)
PCB-1260 (Aroclor 1260)
ug/kg
169
139 104
82 62
38-133 30 30
Decachlorobiphenyl (S)
%
94 72
10-174
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/26/2024 06:37 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 27

Project: CLASS B SLUDGE
Pace Project No.: 92740056
QC Batch: 866612
QC Batch Method: EPA 3510C
Associated Lab Samples: 92740056001
QUALITY CONTROL DATA
Analysis Method: EPA 8270E
Analysis Description: 8270E TCLP MSSV
Laboratory: Pace Analytical Services - Charlotte
METHOD BLANK: 4465433
Matrix:
Water
Associated Lab Samples: 92740056001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
1,4-Dichlorobenzene
ug/L
ND
50.0
07/09/24 11:29
2,4,5-Trichlorophenol
ug/L
ND
50.0
07/09/24 11:29
2,4,6-Trichlorophenol
ug/L
ND
50.0
07/09/24 11:29
2,4-Dinitrotoluene
ug/L
ND
50.0
07/09/24 11:29
2-Methyl phenol(o-Cresol)
ug/L
ND
50.0
07/09/24 11:29
3&4-Methylphenol (m&p Cresol)
ug/L
ND
50.0
07/09/24 11:29
Hexachloro-1,3-butadiene
ug/L
ND
50.0
07/09/24 11:29
Hexachlorobenzene
ug/L
ND
50.0
07/09/24 11:29
Hexachloroethane
ug/L
ND
50.0
07/09/24 11:29
Nitrobenzene
ug/L
ND
50.0
07/09/24 11:29
Pentachlorophenol
ug/L
ND
100
07/09/24 11:29
Pyridine
ug/L
ND
50.0
07/09/24 11:29
2,4,6-Tribromophenol (S)
%
98
10-166
07/09/24 11:29
2-Fluorobiphenyl (S)
%
66
10-130
07/09/24 11:29
2-Fluorophenol (S)
%
57
10-130
07/09/24 11:29
Nitrobenzene-d5 (S)
%
70
10-133
07/09/24 11:29
Phenol-d6 (S)
%
42
10-130
07/09/24 11:29
Terphenyl-d14 (S)
%
71
10-193
07/09/24 11:29
Qualifiers
LABORATORY CONTROL SAMPLE:
4466948
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
1,4-Dichlorobenzene
ug/L
500
142
28
10-130
2,4,5-Trichlorophenol
ug/L
500
404
81
36-150
2,4,6-Trichlorophenol
ug/L
500
397
79
30-151
2,4-Dinitrotoluene
ug/L
500
374
75
46-160
2-Methyl phenol(o-Cresol)
ug/L
500
351
70
32-130
3&4-Methylphenol (m&p Cresol)
ug/L
500
324
65
29-130
Hexachloro-1,3-butadiene
ug/L
500
112
22
10-130
Hexachlorobenzene
ug/L
500
452
90
40-139
Hexachloroethane
ug/L
500
116
23
10-130
Nitrobenzene
ug/L
500
338
68
33-136
Pentachlorophenol
ug/L
1000
758
76
19-156
Pyridine
ug/L
500
270
54
10-130
2,4,6-Tribromophenol (S)
%
102
10-166
2-Fluorobiphenyl (S)
%
66
10-130
2-Fluorophenol(S)
%
54
10-130
Nitrobenzene-d5 (S)
%
67
10-133
Phenol-d6 (S)
%
40
10-130
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/26/2024 06:37 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 27

Project: CLASS B SLUDGE
Pace Project No.: 92740056
LABORATORY CONTROL SAMPLE: 4466948
Parameter Units
Terphenyl-d14 (S) %
QUALITY CONTROL DATA
Spike LCS LCS
Cone. Result % Rec
61
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
% Rec
Limits Qualifiers
10-193
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
4466949
4466950
MS
MSD
92739445001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,4-Dichlorobenzene
ug/L
ND
500
500
81.4
87.5
16
18
10-130
7
2,4,5-Trichlorophenol
ug/L
ND
500
500
184
203
37
41
10-174
10
2,4,6-Trichlorophenol
ug/L
ND
500
500
174
199
35
40
10-173
14
2,4-Dinitrotoluene
ug/L
ND
500
500
165
180
33
36
29-168
9
2-Methyl phenol(o-Cresol)
ug/L
ND
500
500
163
178
33
36
10-130
9
3&4-Methylphenol (m&p
ug/L
ND
500
500
152
163
30
33
10-132
7
Cresol)
Hexachloro-1,3-butadiene
ug/L
ND
500
500
66.3
67.9
13
14
10-130
2
Hexachlorobenzene
ug/L
ND
500
500
172
196
34
39
27-145
13
Hexachloroethane
ug/L
ND
500
500
70.2
68.1
14
14
10-130
3
Nitrobenzene
ug/L
ND
500
500
154
174
31
35
10-145
12
Pentachlorophenol
ug/L
ND
1000
1000
299
325
30
32
10-178
8
Pyridine
ug/L
ND
500
500
6.51
85.5
1
17
10-130
J(M1)
2,4,6-Tribromophenol (S)
%
41
44
10-166
2-Fluorobiphenyl (S)
%
33
36
10-130
2-Fluorophenol(S)
%
28
31
10-130
Nitrobenzene-d5 (S)
%
33
36
10-133
Phenol-d6 (S)
%
20
23
10-130
Terphenyl-d14 (S)
%
26
29
10-193
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/26/2024 06:37 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 27

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
CLASS B SLUDGE
Pace Project No.:
92740056
QC Batch:
866260
QC Batch Method:
SW-846
Associated Lab Samples: 92740056001
QUALITY CONTROL DATA
Analysis Method: SW-846
Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
SAMPLE DUPLICATE: 4465633
92739855001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 12.0 11.5 4 N2
SAMPLE DUPLICATE: 4465634
92740158015 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 13.4 13.4 0 N2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/26/2024 06:37 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 27

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALIFIERS
Project: CLASS B SLUDGE
Pace Project No.: 92740056
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
MDL-Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.
J(M1) Estimated Value. Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS)
recovery.
J(R1) Estimated Value. RPD value was outside control limits.
J(SO) Estimated Value. Surrogate recovery outside laboratory control limits.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/26/2024 06:37 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 27

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
CLASS B SLUDGE
Pace Project No.:
92740056
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92740056001
DEWATERING SLUDGE
EPA 3510C
866613
EPA 8081 B
866858
92740056001
DEWATERING SLUDGE
EPA 3546
866673
EPA 8082A
866844
92740056001
DEWATERING SLUDGE
EPA 3050B
868926
EPA 6010D
869002
92740056001
DEWATERING SLUDGE
EPA 3010A
866706
EPA 6010D
866722
92740056001
DEWATERING SLUDGE
EPA6010D
871265
92740056001
DEWATERING SLUDGE
EPA 7470A
866707
EPA 7470A
866718
92740056001
DEWATERING SLUDGE
EPA 3510C
866612
EPA 8270E
866769
92740056001
DEWATERING SLUDGE
EPA 8260D
867507
92740056001
DEWATERING SLUDGE
SW-846
866260
Date: 07/26/2024 06:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 18 of 27

Pace® Location Requested (City/State(:
/��1jj]]� Pace Analytical Asheville CHAIN -OF -CUSTODY Analytical Request Document
W v 927 4OO56
(,(�/ ej 2225 Riverside Or., Asheville, NC 28804 Chain-nf-Custody is a LEGAL DOCUMENT - Complete all relevant fields
O
Company Name: City of Hendersonville WVVTP Contact/ReportTo: Alexander Lillie
rn
Street Address: 99 Balfour Road, Hendersonville, NC 28792 Phone a: [phone]
111111111111111111111111
CU
d
E-Mail: [e-mail]
92740056
Cc E-Mall:
Customer Project N:
Specify Container Size "
"Container Size: 11)1L, (2) 500m1, 131250ml., (Q
125mL, (1} Wemt, I6140mLvial, (7) Encore, (8)
Project Name: TCLP Class B Sludge Invoice To: Accounts Payable
` (
I I ) I [ I l ! I
TerraCore,(9190ml.. 11DI Other
Invoice E-Mail I [e-mail]
Identify Container Preservative Type—
••• Preservative Types; (1) None, (2) HNO3, (1)
Site Collection Info/Fadl Ity 1D (as applicable): Purchase order p 11i
I J
I t I t I ( I y I ` I
]
H2SOa.141 MCI, (s) NaDH, (e) Z. Aretate,17)
applicable:
NaHSO4, (81 Sod. Thiusulfale, 191 Ascorbic Acid, 1101
Analysis Requested
McOH, (il) Omer
Quote p:
Prof. Mgr: o
Time Zone Collected: I ) AK I I PT [ ] MT [ I CT [ ] ET County / State Drlgin of sample(s): North Carolina
Katharine Burnham
Data Deliverables: Regulatory Program (OW, RCRA, etc,) as applicable: Reportable [ J Yes [ ] No
ACctNum / Client ID: -
I I Level II I ) Level III I ) Level IV Rush (Pre -approval required): DW PWSID N or W W Permit N as applicable:
>
Table N: m
I j Same Day I] 1 Day [] 2 Day [] 3 Day I ] Other
d
7
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E 4U15 Date Results [ ]Yes [ ]No
V
p a w
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�Proffle/Template: A
�FieldFiltered(ifapplicable);
I 1 Other Requested: Analysis:
a
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2692
` atrix Codes (Insert In Matrix box below): Drinking Water (DW), Ground Water (GW), Waste Water (WWI, Product 0 ], Soil/Solid (SS), Oil (OL), Wipe (WP), Tissue ITS), Bioassay
U
d 0- ) d U
Prelog / Bottle Ord. ID: c
(8), Vapor M. Surface Water (SW),Sediment (SED), Sludge MI. Caulk (CM, LAachate (1.11. Biosolid (RS), Other JOTI
�
�
U � � � F
EZ 3132128 .2
Comp / Composite Start Collected or Composite End p Res. Chlorine
o
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c�I o a m
Customer Sample ID Matrix
-
toLd
10 m
Sample Comment
Grab Date Time Date Time Cont. Results Units
n
1
m m to
a
Additional Instructions from Pace`:
eellnquiyhed byf[ moony. (j5/1/0+arurel
Relinquished by Conn(any, lilgnaturej
7r
id 5�
Relinquished by Company: (Signature
Relinqulshud by/Comp,my: 0IS-rave1
Collected By:
[Printed Name)
Signature:
Dalc%Tlme:
R.- by/L ny:(Signature)
` f
Ari
Outefnme:
Received bylCompany (Signature)
Date/nme:
Receive y/Company: (Signature)
Date/Tlme:
Recelved by/Company: iMS-turel
Customer Remarks / Special Conditions / Possible Hazards:
A Coeiars: Thermometer 10. Correction actor J'q: Obs. Temp. (-Cl Corrected'remp. Pc) On Ire:
9zT�'?5 3.4pc 3.-L°C Y
pure/ilme: Trad[Ine Number:
7l3l��-� lf4l �
Darn/time:
7/_3/Z4 / XS/ Delivered by: [ j In- - C Person [Durier
Wn,l ime. (O
Dau./7. .
Submitting a sample via this chain of custody constitutes acknowledgment and acceptance of the Pace' Terms and Conditions found at https:/Iwww.pacelabs.com/resource-Ilbrary/resource/pace-terms-and-conditions/
[ I FeclEX [ I UPS I ) Other
Page: 1 of 1
ENV-FRM-00RQ-0019 v02 110123

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/// BP3U-250 mL Plastic Unpreserved (N/A)
BP2U-500 mL Plastic Unpreserved (N/A)
BP1U-1 liter Plastic Unpreserved (N/A)
BP4S-125 mL Plastic H2SO4 (pH <2) (Cl-)
/ / BP3N-250 mL plastic HNO3 (pH <2)
/ BP4Z-125 mL Plastic ZNAcetate & NaOH (>9)
SP45-125 mL Plastic NaOH (pH > 12) (Cl-)
WGFU-Wide-mouthed Glassjar Unpreserved
\S/ AG1U-1 liter Amber Unpreserved (N/A) (Cl-)
AG2H-1liter Amber HCl(pH <2)
AG31.1-250 mL Amber Unpreserved (N/A) (CI-)
AGIS-1 liter Amber H2SO4 (pH <2)
AG35-250 mL Amber H2SO4 [pH <2)
DG94-40 mL Amber NH4Cl (N/A)(CI-)
DG9H-40 mL VOA HCI (N/A)
V G9T-40 m L VOA N a2S2 03 (N/A)
VG9U-40 mL VOA Unpreserved (N/A)
DGSIV-40 ml VOA H3PO4 (N/A)
KP7U-50 mL Plastic Unpreserved (N/A)
V/GK (3 vials per kit)-VPH/Gas kit (N/A)
SPST-125 mL Sterile Plastic (N/A —lab)
SPZT-250 ml. Sterile Plastic (N/A —lab)
MR-250 mL Plastic (NH2 )2504 (9.3-9.7)
AGOU-100 mL Amber Unpreserved (N/A) (Cl-)
VSGU-20 mL Scintillation vials (N/A)
DG9U-40 mL Amber Unpreserved vials (N/A)
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Pace Analytical Services, LLC
acea
July 10, 2024
Katharine Burnham
Pace Analytical -Asheville, NC
2225 Riverside Drive
Asheville, NC 28804
RE: Pace Asheville 92740056
Dear Katharine Burnham:
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
Please find enclosed the analytical results for the 1 sample(s) the laboratory received on 7/8/24 10:04 am and logged in
under work order HG00994. All testing is performed according to our current TNI accreditations unless otherwise noted.
This report cannot be reproduced, except in full, without the written permission of Pace Analytical Services, LLC.
If you have any questions regarding your report, please contact your project manager. Quality and timely data is of the
utmost importance to us.
Pace Analytical Services appreciates the opportunity to provide you with analytical expertise. We are always trying to
improve our customer service and we welcome you to contact the General Manager, Lisa Grant, with any feedback you
have about your experience with our laboratory at 309-683-1764 or [e-mail].
Amy Holmes
Project Manager
[phone]
[e-mail]
Customer #: 72-105473
www.pacelabs.com
Page 1 of 7

ace
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
SAMPLE RECEIPT CHECK LIST
Items not applicable will be marked as in compliance
Work Order HG00994
YES Samples received within temperature compliance when applicable
YES COC present upon sample receipt
YES COC completed & legible
NO Sampler name & signature present
YES Unique sample IDs assigned
YES Sample collection location recorded
YES Date & time collected recorded on COC
YES Relinquished by client signature on COC
NO COC & labels match
YES Sample labels are legible
YES Appropriate bottle(s) received
YES Sufficient sample volume received
YES Sample containers received undamaged
YES Zero headspace, <6 mm present in VOAvials
NO Trip blank(s) received
YES All non -field analyses received within holding times
NO Short hold time analysis
YES Current PDC COC submitted
YES Case narrative provided
Customer #: 72-105473
www.pacelabs.com
Page 2 of 7

ace
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
Sample: HGO0994-01 Sampled: 07/02/24 14:33
Name: DEWATERING SLUDGE Received: 07/08/24 10:04
Alias: 92740056001 Matrix: Sludge
Parameter Result Unit Qualifier Prepared Dilution MRL Analyzed Analyst Method
Herbicides - TCLP - STL
2,4-D < 0.0500 mg/L V2 07/09/24 10:40 1 0.0500 07/10/24 08:32 SCI SW 8321 B
Silvex < 0.0500 mg/L V2 07/09/24 10:40 1 0.0500 07/10/24 08:32 SCI SW 8321 B
Customer #: 72-105473
www.pacelabs.com
Page 3 of 7

ace
QC SAMPLE RESULTS
Pace Analytical Services, LLC
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
Spike Source %REC
Parameter Result Unit Qual Level Result %REC Limits
Batch B437468 - 06-SW 3510C CPA Herbicides - SW 8321E
Blank (B437468-BLK1)
2,4-D
< 0.0500
mg/L
Silvex
< 0.0500
mg/L
Surrogate: DCAA
0.00707
mgA-
LCS (B437468-BS1)
2,4-D
0.00812
mg/L
Silvex
0.00844
mg/L
Surrogate: DCAA
0.00719
mg1L
Matrix Spike (B437468-MS1)
Sample: HGO0705-01
2,4-D
< 0.0500
mg/L
Silvex
0.00559
mg/L
Surrogate: DCAA
0.00127
mgA-
Matrix Spike Dup (B437468-MSD1)
Sample: HGO0705-01
2,4-D
< 0.0500
mg/L
Silvex
0.00587
mg/L
Surrogate: DCAA
0.00
mgA-
Prepared:07/08/24 Analyzed:07/10/24
0.01000 71
10-153
Prepared:07/08/24 Analyzed:07/10/24
0.01000 81
10-129
0.01000 84
10-132
0.01000 72
10-153
Prepared:07/08/24 Analyzed:07/10/24
0.01000 ND
40-120
0.01000 ND 56
40-120
0.01000 13
10-153
Prepared:07/08/24 Analyzed:07/10/24
0.01000 ND
40-120
0.01000 ND 59
40-120
X 0.01000
10-153
RPD
5
RPD
Limit
20
20
Customer #: 72-105473
www.pacelabs.com
PTV- 7
Page 4 of 7

Pace Analytical Services, LLC
ace
NOTES
2231 W. Altorfer Drive
Peoria, IL 61615
[phone]
Specifications regarding method revisions, method modifications, and calculations used for analysis are available upon request. Please
contact your project manager.
Not a TNI accredited analyte
Certifications
CHI - McHenry, IL - 4314-A W. Crystal Lake Road, McHenry, IL 60050
TNI Accreditation for Drinking Water and Wastewater Fields of Testing through IL EPA Accreditation No. 100279
Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17556
PIA- Peoria, IL - 2231 W. Altorfer Drive, Peoria, IL 61615
TNI Accreditation for Drinking Water, Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation
No.100230
Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory Registry No. 17553
Drinking Water Certifications/Accreditations: Iowa (240); Kansas (E-10338); Missouri (870)
Wastewater Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338)
Solid and Hazardous Material Certifications/Accreditations: Arkansas (88-0677); Iowa (240); Kansas (E-10338)
SPMO - Springfield, MO - 1805 W Sunset Street, Springfield, MO 65807
USEPA DMR-QA Program
STL - Hazelwood, MO - 944 Anglum Rd, Hazelwood, MO 63042
TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through KS KDHE Certification No. E-10389
TNI Accreditation for Wastewater, Solid and Hazardous Material Fields of Testing through IL EPA Accreditation No. - 200080
Illinois Department of Public Health Bacterial Analysis in Drinking Water Approved Laboratory, Registry No. 171050
Qualifiers
V2 Acceptance criteria for the Continuing Calibration Verification (CCV) were exceeded high with associated non -detect samples.
The associated non -detect results are qualified and reported.
X Surrogate failure due to matrix interfernce present within the chromatography
Certified by: Amy Holmes, Project Manager
Q pCCRF�.
TNI
eORA'��
Customer #: 72-105473
www.pacelabs.com
Page 5 of 7

internal Transfer Chain of Custody
I
IIIII�I1II�lI�IIINIIII�Nllllllllllllllll
III
❑ Rush Multiplier X
❑ Samples Pre -Logged into eCOC
Workorder: 92740056
Workorder Name: CLASS B SLUDGE
Report To
Subcontract To
Katharine E Burnham
Pace Analytical Hazelwood
Pace Analytical Asheville
944 Anglum Rd.
2225 Riverside Dr.
Hazelwood, MO 63042
Asheville, NC 28804
Phone [phone]
Phone [phone]
State Of Origin: NC
Cert. Needed: ❑ Yes
Owner Received Date:
Preserved Containers
0(�60qqLj - ace
❑ No
7/3/2024 Results Requested By: 7/18/2024
Requested Analysis
Sample Collect
Item Sample ID Type Datelrime Lab ID Matrix [�L,A�yB USE ONLY
1 DEWATERING SLUDGE PS 7/2/2024 14:33 92740056001 Solid 1 X % V
2
�4
I5
Comments
Transfers (Released By Daterrime 3eceived By DatelTime .!
1 1�11 {}r�t� �! . ' �(v i' i1 / /2 ivy l
Y ��
13 ,-
Cooler Temperature on Receipt �°C f Custody Sea! r Y ,for N Received on Ice Y or N Samples Intact ( � or N
***In order to maintain client confidentiality, location/name of the sampling site, sampler's name and signature may not b provided on this COG document.
This chain of custody is considered complete as is since this information is available in the owner laboratory.
IR Gun # g S Coor�rrection Factor (Deg C)�i' tt
Observed Temp (Deg CJ8 2 Corrected Temp (Deg
Delivery Meth : FedEx PS Watk"in USPS Other
�D
CD-Z
D
a) J
o n Friday, July 05. 2024 3:43:50 PM
V J
J
FMT-ALL-C-002rev.00 241VIarch2009 Page 1 of 1

INTER —LABORATORY WORK ORDER # 92740056
(To be completed by sending tab)
Face Ship To
Pace Analytical Hazelwood Sending Project No 92740056
944 Anglum Rd. Receiving Project No
j Hazelwood, MO 63042 Check Box for Consolidated Invoice ^
Phone [phone]�
Date Prepared 07/05/24
REQUESTED COMPLETION DATE..7/1812024
Sending Region IR92-Charlotte Sending Project Mgr. Katharine E Burnham
Receiving Region S874 External Client City of Hendersonville WWTP
(State of Sample Origin NC QC Deliverable STD REPORT
All questions should be addressed to sending project manager.
Requested Reportable Units Report Wet or Dry Weight'? Dry Weight F1 IRWO Lab Need to run? Cert. Needed
WORK REQUESTED
Container Type Quantity of Preservative Quantity of ACOde
Method Description containers Samples
6321 TCLP AG1U Lipreserveo 1 1 1 SI-21WET
Special Requirements: Report B, Standard Report. (B).FR Only no EDD (0)
FOR ANALYTICAL WORK COMPLETED THIS SECTION ALSO
Return Samples to Sending Region ❑ Yes No
DISPOSITION of FORM
Original sent to the receiving lab - Copy kept at the sending lab.
When work completed: Original sent to the ASM at the receiving laboratory, Copies are made to corporate as needed.
Acode Desc
SUB PAST WET
Friday, July 05, 2024 3:43:50 PM FMT-ALL-C-001 rev.00 24March2009
Page 7of7

City of Hendersonville
99 Balfour Rd.
Hendersonville, NC 28792
WWTP
Client Project# Drying Shed
Samples Received: 6/5/2023
Analytical Report
0623-731
PFAS by Isotope Dilution (soils/solids)
PFAS - M1633
Report Issue Date: 7/05/2023
I certify that to the best of my knowledge all analytical data presented in this report have been checked for completeness,
accuracy, errors and legibility in addition to having been conducted in accordance with approved protocol, and that all
deviations and analytical problems are summarized in the appropriate narrative(s). This analytical report was prepared in
Portable Document Format (.PDF) and contains 20 pages. This report shall not be reproduced except in full without
approval of the laboratory. This will provide assurance that parts of the report are not taken out of context.
Signature:
Laura Boivin, QAAssociate II
Addendum:
Enthalpy Analytical, LLC — Ultratrace
�� Mark Hager, Project Manager
0: 910-876-6894/ F: 910-212-6886
ENTHALPY [e-mail] / www.enthalpy.com
A N A L Y T I C A L 2714 Exchange Drive, Wilmington, NC 28405

1
ENTHALPY
A N A L Y T I C A L
Summary of Results
EU 0623-731 Page 2 of 20

Enthalpy Analytical
Job No.: 0623-731-1 PFAS by Isotope Dilution (soils/solids)
City of Hendersonville Client Project: Drying Shed Site: WWTP
Summary
Compound
CAS
Solids
ng/g
Acids
PFBA
375-22-4
<LOD (0.952) U
PFPeA
2706-90-3
<LOD (0.140) U
PFHxA
307-24-4
0.657 J
PFHpA
375-85-9
<LOD (0.164) U
PFOA
335-67-1
<LOD (0.103) U
PFNA
375-95-1
<LOD (0.0516) U
PFDA
335-76-2
<LOD (0.109) U
PFUnDA
2058-94-8
<LOD (0.0979) U
PFDoDA
307-55-1
<LOD (0.115) U
PFTrDA
72629-94-8
<LOD (0.347) U
PFTeDA
376-06-7
<LOD (0.165) U
Sulfonates
PFBS
375-73-5
<LOD (0.181) U
PFPeS
2706-91-4
<LOD (0.123) U
PFHxS
355-46-4
<LOD (0.199) U
PFHpS
375-92-8
<LOD (0.193) U
PFOS
1763-23-1
0.507 J
PFNS
68259-12-1
<LOD (0.159) U
PFDS
335-77-3
<LOD (0.135) U
PFDoS
79780-39-5
<LOD (2.78) U
4:2 FTS
757124-72-4
<LOD (0.115) U
6:2 FTS
27619-97-2
<LOD (0.0701) U
8:2 FTS
39108-34-4
<LOD (0.134) U
Sulfonamidos
N-EtFOSA
4151-50-2
<LOD (0.298) U
N-EtFOSAA
2991-50-6
0.720 J
N-EtFOSE
1691-99-2
<LOD (8.93) U
N-McFOSA
31506-32-8
<LOD (0.298) U
N-McFOSAA
2355-31-9
0.734 J
N-McFOSE
24448-09-7
<LOD (8.93) U
PFOSA
754-91-6
<LOD (0.206) U
PFECAs
ADONA
919005-14-4
<LOD (0.595) U
HFPO-DA
13252-13-6
<LOD (0.177) U
NFDHA
151772-58-6
<LOD (0.298) U
PFMOBA
863090-89-5
<LOD (1.79) U
PFMOPrA
377-73-1
<LOD (0.298) U
PFESAs
11C1-PF3OUdS
763051-92-9
<LOD (0.595) U
9CI-PF3ONS
756426-58-1
<LOD (0.595) U
PFEESA
113507-82-7
<LOD (0.298) U
FTCAs
3:3 FTCA
356-02-5
<LOD (21.8) U
5:3 FTCA
914637-49-3
<LOD (2.58) U
7:3 FTCA
812-70-4
<LOD (2.78) U
EU 0623-731 Page 3 of 20

1
ENTHALPY
A N A L Y T I C A L
Detailed Results
EU 0623-731 Page 4 of 20

Enthalpy Analytical
Job No.: 0623-731-1 WAS by Isotope Dilution (soils/solids)
City of Hendersonville Client Protect: Drying Shed Site: WWTP
Enthalpy ID
0623-731-001-2
Prep Batch
EU15460
Sample Name
Solids
Prep Date
2023-06-14 11:24
Matrix
Solid
Analysis Date
2023-06-15 08:09
Sampling Date
2023-06-02 09:32
Analyst
brneff
Received Date
2023-06-06
Instrument
Aragom
Acids
Sulfonates
Sulfonamidos
PFECAs
PFEEAs
FTCAs
ES
Compound
PFBA
PFPeA
PFHxA
PFHpA
PFOA
PFNA
PFDA
PFUnDA
PFDoDA
PFTrDA
PFTeDA
PFBS
PFPeS
PFHxS
PFHpS
PFOS
PFNS
PFDS
PFDoS
4:2 FTS
6:2 FTS
8:2 FTS
N-EtFOSA
N-EtFOSAA
N-EtFOSE
N-McFOSA
N-McFOSAA
N-McFOSE
PFOSA
ADONA
HFPO-DA
NFDHA
PFMOBA
PFMOPrA
11 CI-PF3OUdS
9CI-PF30NS
PFEESA
3:3 FTCA
5:3 FTCA
7:3 FTCA
MPFBA
M5PFPeA
M3PFBS
M2-4:2 FTS
M5PFHxA
M3HFPO-DA
M4PFHpA
M3PFHxS
M2-6 2 FTS
M8PFOA
M9PFNA
M8PFOS
M2-8:2 FTS
M8FOSA-I
M6PFDA
d3-N-McFOSAA
d5-N-EtFOSAA
M7PFUdA
MPFDoA
M2PFTeDA
d3-N-McFOSA
d5-N-EtFOSA
d7-N-McFOSE
d9-N-EtFOSE
CAS
375-22-4
2706-90-3
307-24-4
375-85-9
335-67-1
375-95-1
335-76-2
2058-94-8
307-55-1
72629-94-8
376-06-7
375-73-5
2706-91 A
355-46-4
375-92-8
1763-23-1
68259-12-1
335-77-3
79780-39-5
757124-72-4
27619-97-2
39108-34A
4151-50-2
2991-50-6
1691-99-2
31506-32-8
2355-31-9
24448-09-7
754-91-6
919005-14-4
13252-13-6
151772-58-6
863090-89-5
377-73-1
763051-92-9
756426-58-1
113507-82-7
356-02-5
914637-49-3
812-70-4
Formatted LOD
Resull ng/g
ng/g
<LOD 0.952
<LOD 0.140
0.657 0.0810
<LOD 0.164
<LOD 0.103
<LOD 0.0516
<LOD 0.109
<LOD 0.0979
<LOD 0.115
<LOD 0.347
<LOD 0.165
<LOD 0.181
<LOD 0.123
<LOD 0.199
<LOD 0.193
0.507 0.0992
<LOD 0.159
<LOD 0.135
<LOD 2.78
<LOD 0.115
<LOD 0.0701
<LOD 0.134
<LOD 0.298
0.720 0.199
<LOD 8.93
<LOD 0.298
0.734 0.0982
<LOD 8.93
<LOD 0.206
<LOD 0.595
<LOD 0.177
<LOD 0.298
<LOD 1.79
<LOD 0.298
<LOD 0.595
<LOD 0.595
<LOD 0.298
<LOD 21.8
<LOD 2.58
<LOD 2.78
Extracted Mass (g) 1.01
Extract Vol (mQ 0.6
Split Factor N/A
% Solids 29.9 %
Dry Weight Equiv. (g) 0.30
LOQ Recovery Recovery Flags
ng/g Limits
1.79 U
1.79 U
1.79 J
1.79 U
1.79 U
1.79 U
1.79 U
1.79 U
1.79 U
1.79 U
1.79 U
1.58 U
1.68 U
1.63 U
1.70 U
1.66 J
1.72 U
1.72 U
2.78 U
1.67 U
1.70 U
1.71 U
1.79 U
1.79 J
8.93 U
1.79 U
1.79 J
8.93 U
1.79 U
1.69 U
1.79 U
1.79 U
1.79 U
1.79 U
1.68 U
1.67 U
1.79 U
21.8 U
2.58 U
2.78 U
20-150% 55.7%
20-150% 52.6%
20-150% 68.1%
20-150% 47.5%
20-150% 55.3%
20-150% 39.5%
20-150% 65.0%
20-150% 50.8%
20-150% 70.8%
20-150% 58.9%
20-150% 59.7%
20-150% 57.6%
20-150% 60.1%
20-150% 56.3%
20-150% 58.4%
20-150% 8.5% Q
20-150% 8.5% Q
20-150% 54.2%
20-150% 44.6%
20-150% 11.3% Q
10-200% 4.6% Q
10-200% 4.1 % Q
10-200% 23.3%
10-200% 13.5%
EU 0623-731 Page 5 of 20

F, 0 �7�0-
ENTHALPY
A N A L Y T I C A L
QC Data
EU 0623-731 Page 6 of 20

Enthalpy Analytical
Job No.: 0623-731-1 WAS by Isotope Dilution (soils/solids)
City of Hendersonville
Client Protect: Drying Shed Site: WWTP
Enthalpy ID
MB_15460_WAS Prep Batch
EU15460
Sample Name
MB_15460_WAS Prep Date
2023-06-14 11:24
Matrix
solids Analysis Date
2023-06-15 07:01
Sampling Date
Analyst
brneff
Received Date
Instrument
Aragom
Acids
Sulfonates
Sulfonamidos
PFECAs
PFEEAs
FTCAs
ES
Compound
PFBA
PFPeA
PFHxA
PFHpA
PFOA
PFNA
PFDA
PFUnDA
PFDoDA
PFTrDA
PFTeDA
PFBS
PFPeS
PFHxS
PFHpS
PFOS
PFNS
PFDS
PFDoS
4:2 FTS
6:2 FTS
8:2 FTS
N-EtFOSA
N-EtFOSAA
N-EtFOSE
N-McFOSA
N-McFOSAA
N-McFOSE
PFOSA
ADONA
HFPO-DA
NFDHA
PFMOBA
PFMOPrA
11 CI-PF3OUdS
9CI-PF30NS
PFEESA
3:3 FTCA
5:3 FTCA
7:3 FTCA
MPFBA
M5PFPeA
M3PFBS
M2-4:2 FTS
M5PFHxA
M3HFPO-DA
M4PFHpA
M3PFHxS
M2-6 2 FTS
M8PFOA
M9PFNA
M8PFOS
M2-8:2 FTS
M8FOSA-I
M6PFDA
d3-N-McFOSAA
d5-N-EtFOSAA
M7PFUdA
MPFDoA
M2PFTeDA
d3-N-McFOSA
d5-N-EtFOSA
d7-N-McFOSE
d9-N-EtFOSE
CAS
375-22-4
2706-90-3
307-24-4
375-85-9
335-67-1
375-95-1
335-76-2
2058-94-8
307-55-1
72629-94-8
376-06-7
375-73-5
2706-91 A
355-46-4
375-92-8
1763-23-1
68259-12-1
335-77-3
79780-39-5
757124-72-4
27619-97-2
39108-34A
4151-50-2
2991-50-6
1691-99-2
31506-32-8
2355-31-9
24448-09-7
754-91-6
919005-14-4
13252-13-6
151772-58-6
863090-89-5
377-73-1
763051-92-9
756426-58-1
113507-82-7
356-02-5
914637-49-3
812-70-4
Formatted LOD
Resull ng/g
ng/g
<LOD 0.288
<LOD 0.0424
<LOD 0.0245
<LOD 0.0497
<LOD 0.0312
<LOD 0.0156
<LOD 0.0330
<LOD 0.0296
<LOD 0.0349
<LOD 0.105
<LOD 0.0500
<LOD 0.0547
<LOD 0.0371
<LOD 0.0603
<LOD 0.0585
<LOD 0.0300
<LOD 0.0481
<LOD 0.0409
<LOD 0.840
<LOD 0.0349
<LOD 0.0212
<LOD 0.0405
<LOD 0.0900
0.0736 0.0603
<LOD 2.70
<LOD 0.0900
0.0774 0.0297
<LOD 2.70
<LOD 0.0622
<LOD 0.180
<LOD 0.0534
<LOD 0.0900
<LOD 0.540
<LOD 0.0900
<LOD 0.180
<LOD 0.180
<LOD 0.0900
<LOD 6.60
<LOD 0.780
<LOD 0.840
Extracted Mass (g) 1
Extract Vol (mQ 0.6
Split Factor N/A
% Solids 100.0 %
Dry Weight Equiv. (g) 1.00
LOQ Recovery Recovery Flags
ng/g Limits
0.540 U
0.540 U
0.540 U
0.540 U
0.540 U
0.540 U
0.540 U
0.540 U
0.540 U
0.540 U
0.540 U
0.479 U
0.508 U
0.494 U
0.515 U
0.501 U
0.520 U
0.521 U
0.840 U
0.506 U
0.514 U
0.518 U
0.540 U
0.540 J
2.70 U
0.540 U
0.540 J
2.70 U
0.540 U
0.511 U
0.540 U
0.540 U
0.540 U
0.540 U
0.509 U
0.504 U
0.540 U
6.60 U
0.780 U
0.840 U
20-150% 73.6%
20-150% 70.6%
20-150% 83.4%
20-150% 62.6%
20-150% 69.6%
20-150% 48.9%
20-150% 78.5%
20-150% 62.9%
20-150% 93.0%
20-150% 71.0%
20-150% 73.4%
20-150% 67.1%
20-150% 77.0%
20-150% 51.2%
20-150% 68.8%
20-150% 49.2%
20-150% 45.6%
20-150% 64.6%
20-150% 54.8%
20-150% 18.1%Q
10-200% 4.7% Q
10-200% 5.0% Q
10-200% 23.8%
10-200% 14.9%
EU 0623-731 Page 7 of 20

Enthalpy Analytical
Job No.: 0623-731-1 PFAS by Isotope Dilution (soils/solids)
City of Hendersonville
Client Project: Drying Shed Site: WWTP
Enthalpy ID
OPR_15460_PFAS
Prep Batch
EU15460
Extracted Mass (g)
1
Sample Name
OPR_15460_PFAS
Prep Date
2023-06-14 11:24
Extract Vol (ml-)
0.6
Matrix
solids
Analysis Date
2023-06-15 07:23
Split Factor
N/A
Sampling Date
Analyst
brneff
% Solids
100.0%
Received Date
Instrument
Aragorn
Dry Weight Equiv. (g)
1.00
Compound
CAS
Formatted
LOD
LOQ
Recovery
Recovery Flags
Result
ng/g
ng/g
Limits
ng/g
Acids
PFBA
375-224
5.88
0288
0.540
66.6-120%
78.4%
PFPeA
2706-90-3
5.98
0.0424
0.540
69.3-115%
79.8%
PFHxA
307-244
6.38
0.0245
0.540
66.9-116%
85.0%
PFHpA
375-85-9
6.37
0.0497
0.540
59.3-123%
84.9%
PFOA
335-67-1
620
0.0312
0.540
64.3-126%
82.6%
PFNA
375-95-1
5.99
0.0156
0.540
69.3-116%
79.9%
PFDA
335-76-2
5.93
0.0330
0.540
55.4-129%
79.1%
PFUnDA
2058-94-8
6.00
0.0296
0.540
55.3-130%
80.0%
PFDoDA
307-55-1
626
0.0349
0.540
53.5-140%
83.5%
PFTrDA
72629-94-8
25.6
0.105
0.540
12-237%
341.7% Q
PFTeDA
376-06-7
5.85
0.0500
0.540
47.7-148%
78.0%
Sulfonates
PFBS
375-73-5
5.41
0.0547
0.479
55.5-123%
81.3%
PFPeS
2706-914
5.49
0.0371
0.508
642-122%
77.8%
PFHxS
355464
5.89
0.0603
0.494
47-135%
85.9%
PFHpS
375-92-8
622
0.0585
0.515
562-140%
87.0%
PFOS
1763-23-1
5.89
0.0300
0.501
65.8-120%
84.6%
PFNS
68259-12-1
5.63
0.0481
0.520
59.3-122%
78.1%
PFDS
335-77-3
4.57
0.0409
0.521
44.5-129%
632%
42 FTS
757124-724
5.50
0.0349
0.506
56.5-126%
782%
62 FTS
27619-97-2
5.82
0.0212
0.514
60.3-130%
81.6%
82 FTS
39108-344
5.47
0.0405
0.518
40.4-150%
75.9%
Sulfonamidos
N-EtFOSAA
2991-50-6
622
0.0603
0.540
662-124%
82.9%
N-McFOSAA
2355-31-9
6.61
0.0297
0.540
60.9-128%
88.1%
PFOSA
754-91-6
5.62
0.0622
0.540
38.8-150%
74.9%
PFECAs
HFPO-DA
13252-13-6
626
0.0534
0.540
49-130%
83.5%
ES
MPFBA
20-150%
78.6%
M5PFPeA
20-150%
72.1%
M3PFBS
20-150%
81.1%
M242 FTS
20-150%
61.4%
M5PFHxA
20-150%
68.5%
M3HFPO-DA
20-150%
47.3%
M4PFHpA
20-150%
77.8%
M3PFHxS
20-150%
58.0%
M2-62 FTS
20-150%
94.3%
M8PFOA
20-150%
76.0%
M9PFNA
20-150%
73.7%
M8PFOS
20-150%
63.6%
M2-82 FTS
20-150%
73.7%
M8FOSA-I
20-150%
50.4%
M6PFDA
20-150%
70.3%
d3-N-McFOSAA
20-150%
422%
d5-N-EtFOSAA
20-150%
34.7%
M7PFUdA
20-150%
62.6%
MPFDoA
20-150%
51.7%
M2PFTeDA
20-150%
8.7% Q
EU 0623-731 Page 8 of 20

1
ENTHALPY
A N A L Y T I C A L
Narrative Summary
EU 0623-731 Page 9 of 20

Enthalpy Analytical Narrative Summary
Company City of Hendersonville
Job No. 0623-731-1 PFAS by Isotope Dilution (soils/solids)
Client ID. Drying Shed Site: WWTP
1. Custody
Christina Kurnath received the sample on June 05, 2023 at 25.6 °C after being relinquished by
City of Hendersonville. The sample was received in good condition.
Prior to, during, and after analysis, the samples were kept under lock with access only to
authorized personnel by Enthalpy Analytical, LLC
Table 1 - Sample Inventory
EU Lab Sample ID Client Sample ID Matrix
0623-731-001-2 Solids Solid
Table 2 - Sample Inventory — not reported
EU Lab Sample ID Client Sample ID
0623-731-001-1 Solids
2. Methods and Analytes
A list of analytes of interest and corresponding methods of analysis is shown in Table 3.
Abbreviations are defined in the listed Appendices.
Table 3 - Methods and Analytes
EU Method Analytes Cleanup Method
EU-047 PFAS - M1633 List ENVI-Carb
3. Analysis
The samples were analyzed using Waters Acquity UPLC equipped with Xevo TQ MS (LC/MS/
MS "Aragorn").
Sample was initially screened by direct inject analysis to determine extraction mass for analysis.
One to two grams of sample was vortexed in methanol. An aliquot of the methanol solution was
fortified with Extraction Standard (ES) and Injection Standard (IS) then conditioned with a
methanol:water solution prior to injection.
For solid chemical material (SCM) samples, the sample was homogenized, spiked with ES, and
vortexed. Methanol was added to the sample and vortexed to mix contents. The sample was
then sonicated and centrifuged. The supernatant was extracted via SPE.
Cleanup procedures were performed on the extract. Each final sample extract was transferred
to an autosampler vial and spiked with IS prior to analysis
EU 0623-731 Page 10 of 20

Enthalpy Analytical Narrative Summary
Company City of Hendersonville
Job No. 0623-731-1 PFAS by Isotope Dilution (soils/solids)
Client ID. Drying Shed Site: WWTP
4. Calibration
In the initial calibration, the reported analytes exhibited R A 2 of>_ 0.99. The reported analytes in
the calibration standards, continuing calibration (concal) and Initial Calibration Verification (ICV)
met the accuracy criterion for native analytes, except as noted below.
3:3 FTCA fell above method control limits in the opening concal of the analytical sequence. This
analyte was not detected above LOQ in the sample; therefore, the data is reportable without
adverse impact.
The Technical Director extended the method criteria for certain non -legacy analytes that do not
have their own internal standard and exhibit observed variability during calibration.
5. QC Notes
Except where noted below, the QC sample analyses passed all method criteria.
QC samples that did not meet method acceptance criteria were:
PFTrDA fell above method recovery criteria in OPR-15460-PFAS. This analyte was not detected
above LOQ in the sample. The data is accepted with no adverse impact.
Target analytes are quantified based on their ratio to their labeled standard analogs. As a result,
low or high labeled standard recovery in the method blank (MB) and OPR does not cause any
change to ratios or contribute any additional error in the measurement of the target analyte(s).
The data has been accepted and reported with no further action.
Analytes were detected in the method blank (MB) above LOD but less than 1/2 LOQ, meeting
method criteria.
The samples were extracted within the 28-day from collection holding time and analyzed within
the 28-day from extraction to analysis holding time required by the method.
Samples received above 6 °C, client notified in order acknowledgment documentation.
EU 0623-731 Page 11 of 20

Enthalpy Analytical Narrative Summary
Company City of Hendersonville
Job No. 0623-731-1 PFAS by Isotope Dilution (soils/solids)
Client ID. Drying Shed Site: WWTP
6. Reporting Notes
The results presented in this report are representative of the samples as provided to the
laboratory.
Solid results are reported on a dry weight basis. "As Is" results are available upon request.
Some labeled extraction standards in the sample analyses fell outside the control limits for ES
recovery, as denoted by the "Q" qualifier. The target analytes are quantified based on their ratio
to their labeled standard analogs. As a result, low or high labeled standard recovery do not
cause any change to ratios or contribute any additional error in the measurement of the target
analytes. The data have been accepted and reported with no further actions.
Manual integrations were performed on analytes in the ICAL, controls, and samples to correct
baseline -to -baseline integration as well as integrate all isomers for compounds that have both
linear and branched isomers.
These analyses met the requirements of the TNI Standard. Any deviations from the
requirements of the reference method or TNI Standard have been stated above.
Enthalpy Analytical, LLC in Wilmington NC is accredited to perform EPA Draft Method 1633 by
ANAB for DoD QSM 5.4 and to perform SOP EU047 by the Louisiana Department of
Environmental Quality to the 2009 TNI Standard under certificate number 05075.
Differences between SOP EU047 (the method used) and US EPA Draft 1633 are not expected
to impact the quality of the data nor comparability.
EU 0623-731 Page 12 of 20

� General Reporting Notes — Data Qualifiers
ENTHALPY
A N A L Y T I C A L
The following are general reporting notes that are applicable to all Enthalpy Analytical, LLC -
Wilmington, NC data reports, unless specifically noted otherwise.
General Data Oualifiers
• B —The analyte was found in the method blank, at a concentration that was at least 10% of the
amount in the sample.
• Cxx — Two or more congeners co -elute. In EDDs, C denotes the lowest IUPAC congener in a co -
elution group and additional co-eluters for the group (`xx') are shown with the number of the
lowest IUPAC co-eluter.
• E — The reported concentration exceeds the calibration range (upper point of the calibration
curve). For HRMS data, this condition does not imply additional measurement uncertainty. For
LC-MS/MS data, these values should be considered as having measurement uncertainty higher
than values within the calibration range.
• EDL — Estimated Detection Level: The EDL is unique to isotope dilution methods and reflects
the conditions of analysis at the time of analysis, including the equipment used. Where the MDL
is a static value, the EDL is a dynamic value.
• EMPC — Estimated Maximum Possible Concentration: EMPC is specific to Dioxin/Furan tests to
indicate the determined ion -abundance ratio was outside the allowed theoretical range (usually
due to being near the detection limit, although it can very rarely be caused by a co -eluting
interference). The EMPC concentration is adjusted to reflect the value at the theoretical ion -
abundance ratio.
• IR — The ion ratio between the primary and secondary ions was observed to be outside the
method criteria. The analyte concentration may be inaccurate due to interference.
• J — The analyte has a concentration below the minimum calibration level (LOQ value) but greater
than the LOD. These values should be considered as having measurement uncertainty higher than
values within the calibration range
• L - Indicates that an analyte has a concentration below the Minimum Detection Limit (MDL).
The reported concentration is not recommended for regulatory use as the analyte signal may have
a signal-to-noise ratio less than the criteria deemed necessary to be considered a detected analyte.
• LOD — Limit of Detection: For reports conforming to the DOD ELAP QSM, this is the QSM-
defined LOD. For reports conforming to TNI requirements (but not DOD ELAP QSM
requirements), this value is the minimum detection limit (MDL). The LOD is adjusted for sample
weight or volume.
• LOQ — Limit of Quantitation: For reports conforming to the DOD ELAP QSM, this is the QSM-
defined LOQ. For reports conforming to TNI requirements (but not DOD ELAP QSM
requirements), this value is the reporting limit (RL). The LOQ is adjusted for sample weight or
volume.
EU116 v6 (General Reporting Notes -Data Qualifiers) Enthalpy Analytical, LLC — Wilmington, NC
EU 0623-731 Page 13 of 20

� General Reporting Notes — Data Qualifiers
ENTHALPY
ANALYTICAL
• <LODQ — Analyte was not found at a concentration high enough to be reported as detected. It is
reported as less than the LOD, and the LOD is given in the parentheses.
• <LOQQ — Analyte was not found at a concentration high enough to be reported as above the
QSM-defined LOQ or TNI defined Reporting Limit. It is reported as less than the LOQ, and the
LOQ is given in the parentheses.
• ND — Indicates a non -detect.
• NR — Indicates a value that is not reportable due to issues observed in sample preparation or
analysis.
• PR— The associated congener(s) Ware) poorly resolved.
• QI — Indicates the presence of a quantitative interference.
• RL — Reporting Limit. Lowest reportable value. The level is higher than the MDL.
• SI — Denotes "Single Ion Mode" and is utilized for PCBs where the secondary ion trace has a
significantly elevated noise level due to background PFK. Responses for such peaks are
calculated using an EMPC approach based solely on the primary ion area(s) and may be
considered estimates.
• U — The analyte was not detected.
• V / Q — The labeled standard recovery is not within method control limits.
• X — Indicates the result is from re-injection/repeat/second-column analysis.
Lab Identifiers/ Data Attributes
• AR — Indicates use of the archived portion of the sample extract.
• CU —Indicates a sample that required additional clean-up prior to HRMS injection/processing.
• D —Dilution Data. Result was obtained from the analysis of a dilution. The number that follows
the "D" indicates the dilution factor.
• DE — Indicates a dilution performed with the addition of ES (Extraction Standard) solution.
• DUP — Designation for a duplicate sample.
• MS — Designation for a matrix spike.
• MSD — Designation for a matrix spike duplicate.
• R — Indicates a re -extraction of the sample.
• RJ — Indicates a reinjection of the sample extract.
EU116 v6 (General Reporting Notes -Data Qualifiers)
EU 0623-731 Page 14 of 20
Enthalpy Analytical, LLC — Wilmington, NC

� General Reporting Notes — Data Qualifiers
ENTHALPY
ANALYTICAL
• S — Indicates a sample split. The number that follows the "S" indicates the split factor.
• SAT — Indicates an analyte saturated the detector.
EU116 v6 (General Reporting Notes -Data Qualifiers)
EU 0623-731 Page 15 of 20
Enthalpy Analytical, LLC — Wilmington, NC

PFAS Compound Acronym List
Acronym I CAS # I Compound Name
* Analyte is not accredited for SOP EU047
A PFBA
375-22-4
A PFPeA
2706-90-3
#, A PFHxA
307-24-4
#, A PFHpA
375-85-9
#, A PFOA
335-67-1
#, A PFNA
375-95-1
#, A PFDA
335-76-2
#, A PFUnA (PFUnDA)
2058-94-8
#, A PFDoA (PFDoDA)
307-55-1
# PFTrDA (PFTriA)
72629-94-8
# PFTeDA (PFTA)
376-06-7
#, A PFBS
375-73-5
A PFPeS
2706-91-4
#, A PFHxS
355-46-4
A PFHpS
375-92-8
#, A PFOS
1763-23-1
PFNS
68259-12-1
PFDS
335-77-3
A 4:2 FTS
757124-72-4
A 6:2 FTS
27619-97-2
A 8:2 FTS
39108-34-4
PFOSA (FOSA)
754-91-6
# N-McFOSAA
2355-31-9
# N-EtFOSAA
2991-50-6
#, A HFPO-DA
13252-13-6
*, #, A 110-PHOWS
763051-92-9
*, #, A 9CI-PF30NS
756426-58-1
*, #, A ADONA
919005-14-4
*,A PFEESA
113507-82-7
*, A PFMOBA (PFMBA)
863090-89-5
*, A NFDHA
151772-58-6
*, A PFMOPrA (PFMPA)
377-73-1
* PFMOAA
674-13-5
* PF02HxA
39492-88-1
*
PF030A
39492-89-2
*
PF04DA
39492-90-5
*
PF05DA
39492-91-6
*
Nafion Byproduct 1
29311-67-9
*
Nafion Byproduct 2
749836-20-2
*
PEPA
267239-61-2
*
PMPA
13140-29-9
*
10:2 FTS
120226-60-0
*
N-EtFOSA
4151-50-2
*
N-EtFOSE
1691-99-2
*
N-McFOSA
31506-32-8
*
N-McFOSE
24448-09-7
*
801212-59-9
*
67905-19-5
PFECA G
PFHxDA
R-PSDA (Nafion Byproduct
* 4)
A710
ENTHALPY
IIM-4l 4 i 1 L 4 L
# Method 537.1 Accredited A Method 533 Accredited
Perfluorobutanoic Acid
Perfluoropentanoic Acid
Perfluorohexanoic Acid
Perfluoroheptanoic Acid
Perfluorooctanoic Acid
Perfluorononanoic Acid
Perfluorodecanoic acid
Perfluoroundecanoic acid
Perfluorododecanoic acid
Perfluorotridecanoic acid
Perfluorotetradecanoic acid
Perfluorobutane sulfonic acid
Perfluoropentane sulfonic acid
Perfluorohexane sulfonic acid
Perfluoroheptane sulfonic acid
Perfluorooctane sulfonic acid
Perfluorononane sulfonic acid
Perfluorodecane sulfonic acid
4:2 fluorotelomer sulfonic acid
6:2 fluorotelomer sulfonic acid
8:2 fluorotelomer sulfonic acid
Perfluorooctane sulfonamide
N-methyl perfluorooctane sulfonamido acetic acid
N-ethyl perfluorooctane sulfonamido acetic acid
2,3,3,3-Tetrafluoro-2-(1,1,2,2,3,3,3-heptafluoropropoxy)-propanoic acid (Gen-X)
11-chloroeicosafluoro-3-oxaundecane-l-sulfonic acid
9-chlorohexadecafluoro-3-oxanonane-l-sulfonic acid
4,8-dioxa-3H-perfluorononanoic acid
Perfluoro(2-ethoxyethane)sulphonic acid
Perfluoro-4-methoxybutanic acid
Nonafluoro-3,6-dioxaheptanoic acid
Perfluoro-3-methoxypropanoic acid
Perfluoro-2-methoxyacetic acid
Perfluoro (3,5-dioxahexanoic) acid
Perfluoro (3,5,7-trioxaoctanoic) acid
Perfluoro (3,5,7,9-tetraoxadecanoic) acid
Perfluoro(3,5,7,9,11-pentaoxadodecanoic) acid
Nafion Byproduct 1
Nafion Byproduct 2
Perfluoro-2-ethoxypropanoic acid
Perfluoro-2-methoxypropanoic acid
Fluorotelomer sulfonate 10:2
N-ethylperfluoro-l-octanesulfonamide
2-(N-methylperfluoro-l-octanesulfonamido)-ethanol
N-methylperfluoro-l-octanesulfonamide
2-(N-methylperfluoro-l-octanesulfonamido)-ethanol
4-(HeptafIuoroisopro poxy)hexafluorobutanoic acid
Perfluorohexadecanoic acid
2416366-18-0 Perfluoro-4-(2-sulfoethoxy)pentanoic acid
EU 0623-731 Page 16 of 20

PFAS Compound Acronym List
Acronym CAS # I Compound Name
* Analyte is not accredited for SOP EU047
Hydrolyzed PSDA (Nafion
* Byproduct5) 2416366-19-1
R-PSDCA (Nafion Byproduct
* 6) 2416366-21-5
* EVE Acid
* FBSA
* Hydro -EVE Acid
* R-EVE Acid
* NVHOS
* PFDoS
* PFODA
* 3:3 FTCA
* 5:3 FTCA
* 7:3 FTCA
* N-AP-FHxSA
* N-CMAmP-6:2 FOSA
i
A710
ENTHALPY
IIM-4l 4 i 1 L 4 L
69087-46-3
30334-69-1
773804-62-9
2416366-22-6
1132933-86-8
79780-39-5
16517-11-6
356-02-5
914637-49-3
812-70-4
50598-28-2
34455-29-3
# Method 537.1 Accredited A Method 533 Accredited
2-fIuoro-2-[1,1,2,3,3,3-hexafluoro-2-(1,1,2,2-tetrafluoro-2-suIfoethoxy) pro poxy]-acetic acid
1,1,2,2-tetrafluoro-2-[1,2,2,3,3-pentafIuoro-1-(trifIuorom ethyl)propoxy] ethanesulfonic
acid
2,2,3,3-tetrafluoro-3-({1,1,1,2,3,3-hexafluoro-3-[(1,2,2-trifluoroethenyl)oxy]propan-2-
yl}oxy)propionic acid
Perfluorobutylsulfonamide
2,2,3,3-TetrafIuoro-3-{[1,1,1,2,3,3-hexafluoro-3-(1,2,2,2-tetrafl uoroethoxy)pro pan-2-
yl]oxy}propanoic acid
4-(2-carboxy-1,1,2,2-tetrafluoroethoxy)-2,2,3,3,4,5,5,5-octafluoro-pentanoic acid
Perfluoroethoxysulfonic acid
Perfluorododecane sulfonic acid
Perfluorooctadecanoic acid
2H,2H,3H,3H-Perfluorohexanoic acid
2H,2H,3H,3H-Perfluorooctanoic acid
2H,2H,3H,3H-Perfluorodecanoic acid
N-(3-(Dimethylamino)propyl)tridecafluoro-l-hexanesulfonamide
N-(Ca rboxymethyl)-N,N-dimethyl-3-(((3,3,4,4,5,5,6,6,7,7,8,8,8-
tridecafluorooctyl)sulfonyl)amino)1-propanaminium
EU 0623-731 Page 17 of 20

�-
ENTHALPY
A N A L Y T I C A L
Sample Custody
EU 0623-731 Page 18 of 20

��
Special Handling:
l$ Standard Turn Around Time
Chain
of Custody Record
Rush Turn Around Time - Date Needed
• All Fast
TATs Subject to Approval by Enthalpy Analytical,
LLC
e
HALPY
• All Samples Disposed of After 6 months Unless Otherwise Instructed.
Enthalpy Ultratrace Job#: CDC Page
i � lS
of
Enthalpy Analytical -Wilmington, NC has added enhancements to
standard methods to improve accuracy, precision
and permit an assessment of laboratory performance in
the conte.t of your specific data needs.
II I'
Client Name: .•(Y 7P rt tAJrlS-1 vi 1 i2 w UJT P
Project Number:
PO#:
This Chain of Custody is applicable to
Project Manager: Q12x..n)t I—i ��t�•�7i,0. �.WM
Site Name: brr'A� Sl,.
Telephone#:
y}A-G9"T-30^1-7
Non -Air samples. Standard TAT differ
per analysis and are provided by
Report To: Alt n� J L: I Tc_
Location: 'W VV T p
Email:
, h
11 " L- G_� W 4 L _ ot,0 ✓
request.
Client Special Instructions:
a
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Matrix: GW-Groundwater, WW-Wastewater, NW -Non -Potable Water, DW-Drinking Water, S-
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PF = PFOA/PFOS
Soil, SL-Sludge, BT-Biological Tissue, O-Other
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---- -- -- ------
G=Grab C=Composite Q=Quality Control
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Ship samples to: 2712A Exchange Drive • Wilmington, NC 28405
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❑ Iced ❑ Ambient °C
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Office: 2714 Exchange Drive • Wilmington, NC 28405 • [phone] • www.enthalpy.com
EU 0623-731 Page 19 of 20

This Is The Last Page
�-
ENTHALPY
A N A L Y T I C A L
Of This Report.
EU 0623-731 Page 20 of 20

Initial Review
Reviewer
nathaniel.thornburg
Is this submittal an application? (Excluding additional information.)
Yes No
If not an application what is the submittal type? *
Annual Report Year*
Permit Number (IR)*
Applicant/Permittee
Annual Report
Residual Annual Report
Additional Information
Other
2023
W00010059
City of Lenoir
Email Notifications
_ ._ 11 . _..._. _..._......... . _..._.._...__..._........ ........_............. ...... _..._....... _..._. _...... _..._._..._.._..._._..._......._.......
Does this need review by the hydrogeologist? * Yes No
Regional Office Asheville
CO Reviewer
Admin Reviewer Wanda Gerald

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Elisa Triplett
Email Address* Phone Number*
[e-mail] 8287574462
Project Information
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* Wastewater Irrigation High -Rate Infiltration
Other Wastewater Reclaimed Water
Closed -Loop Recycle Residuals
Single -Family Residence Wastewater Other
Irrigation
Permit Number:* WO0010059
Has Current Existing permit number
Applicant/Permittee Address* 1905 Broadland Road
Facility Name* City of Lenoir Class A Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2023 Combined Sheets for State Report.pdf 2.2MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
G
Submission Date 2/15/2024

February 15, 2024
City of Lenoir
P.O. Box 958 Lenoir, NC 28645-0958
Subject: Annual Residuals Report CY 2023
Enclosed is a copy of the 2023 calendar year Annual Residuals Report for the City of Lenoir's
Lower Creek WWTP Residuals Facility; permit number WQ0010059.
Blowing Rock has not brought any of their sludge to our facility the entire year of 2022,
however they are listed as a source.
The regular quarterly samples as per the permit were not collected or analyzed for the 1st
quarter 2023. There has been significant turnover in lab personnel and the sample collection
was inadvertently missed.
If there are any questions or if any further information is needed please call me at (828) 757-
4462 or email me at IrtriplettPci.lenoir.nc.us
Sincerely,
Elisa R. Triplett
Superintendent WWTP

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WO PERMIT #: W00010059 FACILITY NAME: Lower Creek WWTP
PHONE: [phone] COUNTY: Caldwell OPERATOR: Jake soots
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
❑r Distribution and Marketing (complete Parts A, B, and C)
Was the facility
in operation during the past calendar year? Yes
❑,. No
❑ 0
If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Volume
(dry tons)
Recipient Information
Month
Sources(s) (include NPDES # if
Amendment/
applicable)
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
WWTP sludge from the
0
71.37
71.37
David Powell
60
Hay
February
following sources:
0
94.82
94.82
Clay Wilson, Tony Ramsey
54
Hay
March
0
61.96
61.96
Jeff Branch, David Spears
20
Hay
April
Lower Creek WWTP
0
54.38
54.38
Ronnie Cardwell, Lynn Bean(
49
Hay
May
Gunpowder Creek WWTP
0
96.54
96.54
Ronnie Cardwell
12
Hay
June
Lenoir Water Treatment Plant
0
66.41
66.41
City of Lenoir
24
Ball field
July
0
101.88
101.88
David Powell
25
Hay
August
0
220.25
220.25
ell,lackey, Chuck Calloway,.
191
Hay
September
0
150.89
150.89
David Powell,Hendersonvillc
98
Hay
October
0
196.07
196.07
ell,lackey, Chuck Calloway,.
165
Hay
November
0
158.37
158.37
David Powell, John Moore
111
Hay
December
0
92.05
92.05
David Powell
12
Hay
Total from FORM DMSDF (sup)
Totals:
Annual (dry tons):
0
1364.99
1364.99
821
Amendment(s) used:
Bulking Agent(s) used:
* If more space is
required, attach additional information
sheets (FORM DMSDF (supp)):
Total Number of Form DMSDF (Supp)l
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit ❑ Yes
(including but not limited to items 1-3 below) issued by the Division of Water Resources: 0 No 0, If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(�fE
2-15-2024
Signature of Permittee Date Signature of Preparer** Date
(if different from Permittee)
**Preparer is defined in 40 CFR Part 5039(r) and 15A NCAC 2T .1102 (26)
DENR FORM DMSDF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0010059
Facility Name: City of Lenoir - Lower Creek WWTP
Residual Source WQ # or
NPDES #:
WWTP Name:
Residual Analysis Data
NCO023981
Lower Creek WWTP
Laboratory: 1)
2)
3)
4)
5)
Ceiling Sample or Composite Date
Parameter Conc.
(mpg) Limit MISSED 6/6/2023 8/22/23 12/19/23
Meritech
Statesville Analytical
Percent Solids (%)
NA
89.6
81.8
77.6
Arsenic
75
4.79
1.81
1.91
Cadmium
85
1.13
0.924
0.398
Copper
4,300
438
312
405
Chromium
NA
19.6
16.3
14.8
Lead
840
20.9
18.1
18.2
Mercury
57
0.29
0.232
0.316
Molybdenum
75
5.45
2.65
3.16
Nickel
420
22.8
21.1
25.8
Selenium
100
3.86
1.6
<0.644
Zinc
7,500
633
522
711
Total Phosphorus
NA
15,100
11,400
16,900
TKN
NA
2,450
39,400
6,850
Ammonia -Nitrogen
NA
1,920
4,840
123
Nitrate and Nitrite
NA
<11.2
<12.2
<12.9
a For surface disposal facilities
the ceiling concentration
limits listed
in this
form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
2-15-2024
Signature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0010059 Laboratory: 1) Meritech
Facility Name: City of Lenoir - Lower Creek WWTP 2) Statesville Analytical
Residual Source NCO023981 3)
NPDES # or WQ#: 4)
WWTP Name: Lower Creek WWTP 5)
Residual Analysis Data
Sample or Composite Date
Parameter
(mg/kg)
missed 6/6/23
8/22/23
12/9/23
Aluminum
10,600
8,000
14,900
Calcium
9,600
7,180
9,380
Magnesium
2,900
2,600
2,840
Potassium
Silver
5.12
2.35
1.57
Sodium
484
522
514
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
C%a. % 2-15-2024
Signature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF - B (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Lenoir -Lower Creek WWTP WQ Permit Number: WQ0010059
WWTP Name: Lower Creek WWTP
NPDES Number: NCO023981
Monitoring Period: From l/l/2023
To 12/31/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A: Alt. A (time/temp) ❑ 1 Alt B (Alk Treatment)❑ 1 Alt. C (Prior Testing)❑
AItD (No Prior Test) ❑ 1 Process to Further Reduce Pathogengs 0
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑ Heat Drying 0 Heat Treatment ❑ Thermophilic ❑
Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑
Class B: JAlt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ 1 Air Drying ❑ 1 Composting ❑ JAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
f
Allowable Level Pathogen Density Number oFrequency Sample Analytical
Parameter in Sludge Minimum Geo. Mean Maximums Units Excee- of Analysis 'Type Tech-
dences niaue
2 x 10 to the MPN
6th power
per gram of
Fecal Coliform total solids CFU
1000 mpn per gram
of total solid (dry <1000 <1000 <1000 MPN/G 0 7 G Mult.tube
weight)
Salmonella bacteria 3 MPN per 4 grams
(in lieu of fecal total solid (dry
coliform) weight)
Vector Attraction Reduction (15A NCAC 62T .1107) - Please indicate alternative performed:
Alt.I (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ IAlt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑�
Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Elisa Triplett, WWTP Superintendent
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
2-15-2024
Signature of Preparcr* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

CITY OF LENOI R
LENOIR BLEND
INFORMATION AND INSTRUCTIONS
PERSON(S) PREPARING THE RESIDUALS: Jake Soots, Biosolids Operator
ADDRESS OF BIOSOLIDS TREATMENT
CONTACT TELEPHONE NUMBER:
ALTERNATE CONTACT:
City of Lenoir, Lower Creek WWTP Biosolids Treatment
P.O. Box 958, 1905 Broadland Road
Lenoir, NC 28645
828-757-2198
Elisa Triplett, WWT Supt. (same phone #)
No- The land application of the residuals is prohibited except in accordance with the instructions
on this information sheet.
No- The residuals shall not be applied to any site that is flooded, frozen or snow-covered.
►Adequate procedures shall be provided to prevent surface runnoff from carrying any
disposed or stored residuals into any surface waters.
No- There shall be a 50 foot buffer between application site and any public or private water
supply source (including wells) and any stream, lake, river or natural drainage way.
► Person(s) accepting the residuals shall be responsible for soil testing their own sites to
ensure that the receiving soil can accept the residuals and to ensure that the crop or plants
will not be harmed.

Lower Creek WWTP Biosolids Test Results
Residuals Facility Permit # WQ0010059
NPDES # NCO023981
MISSED
.,
o
Plant
SAMPLE a,
o 0,:tf
m
0,
�, 0, N
Available
o
E o
cU z o
o
Nitrogen
COLLECTION I° Y z
Q( z
z z
z z m
(P.A.N.)
Quarter (mq/kq)
(mq/kq)
(mq/kq)
(mq/kq)
(mq/kq)
1st QTR 2023
0.35
-
0.00%
NOTES: 10,000 mg/L = 1 %
P.A.N. = (Min. Rate) x (TKN - Ammonia) + 0.5 x Ammonia + Nitrate + Nitrite
Other Parameters:
Total Phosphorous
mg/kg
0.0000%
Calcium (as Ca)
mg/kg
0.00% CCE
Percent Solids
%
Fecal Coliform Maximum
counts/kg
Fecal Coliform Geometric Mean
counts/kg
(Limit is 1,000,000 counts/kg)
pH
S.U.
OTHER LIMITED PARAMETERS
O J
O)
CB C
C�L6
Q (Q
- C
U U �
C U)
2E U-
(6 07
Q
COMMENTS
Arsenic (As) * 75
41
Cadmium (Cd) 85
39
Chromium (Cr) 3,000
Copper (Cu) 4,300
1,500
All Parameters are
Lead (Pb) * 840
300
below allowable
Mercury (Hg) 57
17
Molybdenum (Mo) 75
----
permit limits.
Nickel (Ni) 420
420
Selenium (Se) * 100
100
Zinc (Zn) 7,500
2,800
All samples were collected by City of Lenoir laboratory personnel and analyzed by Statesville Analytical,
and Meritech Labs
The samples collected were representative of what is distributed to end users.
The samples collected were representative of what is distributed to end users.

Lower Creek WWTP Biosolids Test Results
Residuals Facility Permit # WQ0010059
NPDES # NCO023981
c�
o
Plant
Y a),
o �,
a)
a) ��,
N m
Available
c� o
E o
(Uz o
L o
Nitrogen
O
I.-z
E
Q z
z� z
z z
C:
(P.A.N.)
Julv, August, Sept. (mq/kq)
(mq/kq)
(mq/kq)
(mq/kq)
2E �
(mq/kq)
3rd quarter 2023 39,400
4,840
12.2
---
0.35
14,528.20
(collected 8/22/2023)
1.45%
NOTES: 10,000 mg/L = 1 %
P.A.N. = (Min. Rate) x (TKN - Ammonia) + 0.5 x Ammonia + Nitrate + Nitrite
Other Parameters:
Total Phosphorous
11,400
mg/kg
1.1400%
Calcium (as Ca)
7,180
mg/kg
1.80%
CCE
Percent Solids
81.8
%
Fecal Coliform Maximum
<1000
counts/kg
Fecal Coliform Geometric Mean
<1000
counts/kg
(Limit is 1,000,000 counts/kg)
OTHER LIMITED PARAMETERS
0
0�
L
L
E
:ECB
+'
E
U Y
0)
U
O> O E
>+ Y_
Z O
U U t
2 Q U
C N E
Qa�
O
U
Arsenic (As)*
75
41
1.81
Cadmium (Cd)
85
39
0.924
Chromium (Cr)
3,000
16.3
All
Copper (Cu)
4,300
1,500
312
Parameters
Lead (Pb)*
840
300
18.1
are below
Mercury (Hg)
57
17
0.232
allowable
Molybdenum (Mo)
75
----
2.65
permit
Nickel (Ni)
420
420
21.1
limits.
Selenium (Se)*
100
100
1.6
Zinc (Zn)
7,500
2,800
522
SAR (Sodium Adsorption Ratio) __> 10 3.14
Limit Result
All samples were collected by City of Lenoir laboratory personnel and analyzed by Statesville Analytical,
and Meritech Labs
The samples collected were representative of what is distributed to end users.

Lower Creek WWTP Biosolids Test Results
Residuals Facility Permit # WQ0010059
NPDES # NCO023981
c�
o
Plant
o
0)
m�
N
m
Available
ohoo
zoo
��
Nitrogen
� Y z
Q z
z� z
z z
(P.A.N.)
Oct, Nov Dec (mq/kq)
(mq/kq)
(mq/kq)
(mq/kq)
(mq/kq)
4t" quarter 2023 6,850 123 12.9 0.35 2,428.85
(collected 12/19/2023) 0.24%
NOTES: 10,000 mg/L = 1 %
P.A.N. = (Min. Rate) x (TKN - Ammonia) + 0.5 x Ammonia + Nitrate + Nitrite
Other Parameters:
Total Phosphorous
16,900
mg/kg
Calcium (as Ca)
0
mg/kg
Percent Solids
77.6
%
Fecal Coliform Maximum
<1000
counts/kg
Fecal Coliform Geometric Mean
<1000
counts/kg
OTHER LIMITED PARAMETERS
0
0
cu
0)
0) a) E
Z O
O> O i=
C N E
U U
2< U J
<a�
Arsenic (As)
75
41
1.91
Cadmium (Cd)
85
39
0.398
Chromium (Cr)
3,000
14.8
Copper (Cu)
4,300
1,500
405
Lead (Pb)
840
300
18.2
Mercury (Hg)
57
17
0.316
Molybdenum (Mo)
75
----
3.16
Nickel (Ni)
420
420
25.8
Selenium (Se)
100
100 <
0.644
Zinc (Zn)
7,500
2,800
711
1.6900%
0.00% CCE
(Limit is 1,000,000 counts/kg)
All samples were collected by City of Lenoir laboratory personnel and analyzed by Statesville Analytical,
and Meritech Labs
The samples collected were representative of what is distributed to end users.

Lower Creek WWTP Biosolids Test Results
Residuals Facility Permit # WQ0010059
NPDES # NCO023981
c�
g
Plant
Co 0)
o 0,
��,
��,
N
m
Available
o ho
o
L-zoo
��
Nitrogen
�Yz
Qz
z�z
zz
Cam'
(P.A.N.)
Quarter (mq/kq)
(mq/kq)
(mq/kq)
(mq/kq)
(mq/kq)
2nd quarter 2023 2,450 1,920 11.2 0.35 1,156.70
(Collected: 6/6/2023) 0.12%
10,000 mg/L = 1 %
P.A.N. = (Min. Rate) x (TKN - Ammonia) + 0.5 x Ammonia + Nitrate + Nitrite
Other Parameters:
Total Phosphorous
15,100
mg/kg 1.5100%
Calcium (as Ca)
9,600
mg/kg 2.40% CCE
Percent Solids
89.6
%
Fecal Coliform Maximum
<1000
counts/kg
Fecal Coliform Geometric Mean
<1000
counts/kg (Limit is 1,000,000 counts/kg)
OTHER LIMITED PARAMETERS
O J
C
O
O)
CB C
N O
N
Q C6
'P
O) 0)
_ U
0
U
U7
CB
U U t
20 UE
Q
Arsenic (As)
75
41
4.79
Cadmium (Cd)
85
39
1.13
Chromium (Cr)
3,000
19.60
Copper (Cu)
4,300
1,500
438
Lead (Pb) *
840
300
20.9
Mercury (Hg)
57
17
0.29
Molybdenum (Mo)
75
----
5.45
Nickel (Ni)
420
420
22.8
Selenium (Se)
100
100
3.86
Zinc (Zn)
7,500
2,800
633
SAR (Sodium Adsorption
Ratio) __> 10
Limit Result
All samples were collected by City of Lenoir laboratory personnel and analyzed by Statesville Analytical,
and Meritech Labs
The samples collected were representative of what is distributed to end users.

2023 Temperature and %Solids of Dry Product
Date
%Dry
Temp
Date
% Dry
Temp
Date
%Dry
Temp
1/2
91
201
2/1
94
205
3/6
92
211
1/3
91
202
2/6
93
208
3/7
91
213
1/4
94
201
2/7
92
210
3/8
92
209
1/9
92
205
2/13
94
214
3/12
91
207
1/10
99
212
2/14
93
209
MWER
3/14
92
207
1/11
95
210�
2/15
92
208
3/15
91
206
1/16
96
214
2/20
92
207
3/20
92
203
1/17
93
216
2/21
92
210
3/21
92
203
1/18
93
217
2/22
94
213
3/22
92
205
1/23
90
206
2/27
92
211
3/27
92
209
1/24
92
204
2/28
93
214
3/29
91
208
1/25
91
212
1/30
93
202
1/31
91
206
Date
% Dry
Temp'
Date
% Dry
Temp
Date
%Dry
Temp
4/3
91
208�
5/1
91
209
6/1
93
217
4/4
92
209
5/2
91
207
6/5
91
220
4/5
91
210�
5/3
91
210
6/6
91
219
4/10
92
207
5/8
92
213
6/7
91
215
4/11
92
209
5/9
91
214
6/12
91
217
4/12
91
210
5/10
92
213
6/13
91
218
4/17
92
212
5/15
91
216
6/14
92
218
4/18
91
214
5/16
92
214
6/20
91
212
4/24
91
210
5/17
91
217
6/22
97
214
4/25
92
208�
5/22
92
215
6/26
92
220
5/23
92
212
6/27
91
213
5/24
91
218
6/28
91
216
5/29
92
215
5/30
91
217
unsii\
Date
%Dry
Temp
Date
% Dry
Temp
Date
% Dry
Temp
7/10
99
220�
8/1
92
215
9/2
92
217
7/11
10
218
8/2
91
217
9/4
93
221
7/12
92
218
8/7
92
213
9/5
96
220
7/17
93
217
8/8
91
213
9/11
91
214
7/18
92
214
8/9
91
217
9/12
91
219
7/19
92
218
8/14
91
215
9/13
92
221
7/24
91
216
8/15
92
218
9/18
91
217
7/25
91
220
8/16
92
246
9/19
93
215
7/26
93
216
8/21
92
220
9/20
93
217
7/31
91
219
�
8/22
92
217
,
9/25
92
220
8/23
91
218
9/26
92
215
8/28
92
216
9/27
91
219
8/29
90
219
8/30
92
221

2023 Temperature and %Solids of Dry Product
Date
% Dry
Temp
Date
% Dry
Temp
10/2
91
217
11/1
91
213
10/3
92
221�
11/6
93
219
10/9
91
215
11/7
95
221
10/10
91
211
11/13
91
218
10/11
92
213
11/14
90
221
10/16
93
210
11/15
92
212
10/17
93
214
11/20
91
217
10/18
91
217
11/21
92
222
10/23
91
210�
11/27
92
216
10/24
93
214
11/28
91
218
10/25
91
217
11/29
91
212
10/30
91
212
11/30
90
218
IM
O\\\\\�
\\\\\\\
\\\\\\\'
\\\\\\\
\o
boo ��o
Date
% Dry
Temp
12/4
92
219
12/5
91
214
12/6
92
216
12/11
93
214
12/12
94
210
12/18
92
217
12/19
91
213
12/20
95
215

Contact: Lisa Triplett
Client: City of Lenoir
1905 Broadland Road
Lenoir NC 28645
Meritech Work Order # 060623146
Mer itech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Sample: 060623-Biosolids Grab
Report Date: 6/15/2023
NPDES #: NCO023981
Date Sample Rcvd: 6/6/2023
6/6/2023
Parameters
Results
Analvsis Date
Renorting Lim
Method
% Total Solids
89.6 %
6/6/23
0-100 %
SM 2540B
Ammonia, Nitrogen
1,920 mg/kg
6/8/23
10 mg/kg
EPA 350.1
TKN
2,450 mg/kg
6/9/23
20 mg/kg
EPA 351.1
Nitrate/Nitrite, Nitrogen
<11.2 mg/kg
6/13/23
11.2 mg/kg
EPA 353.2
Nitrogen, total
2,450 mg/kg
6/13/23
20.0 mg/kg
EPA 353.2
Aluminum, total
10,600 mg/kg
6/13/23
2.50 mg/kg
EPA 200.7
Arsenic, total
4.79 mg/kg
6/13/23
0.060 mg/kg
EPA 200.7
Cadmium, total
1.13 mg/kg
6/13/23
0.100 mg/kg
EPA 200.7
Calcium, total
9,600 mg/kg
6/13/23
10.0 mg/kg
EPA 200.7
Chromium, total
19.6 mg/kg
6/13/23
0.250 mg/kg
EPA 200.7
Copper, total
438 mg/kg
6/13/23
1.00 mg/kg
EPA 200.7
Lead, total
20.9 mg/kg
6/13/23
0.500 mg/kg
EPA 200.7
Magnesium, total
2,900 mg/kg
6/13/23
10.0 mg/kg
EPA 200.7
Mercury, total
0.290 mg/kg
6/13/23
0.02 mg/kg
EPA 245.1
Molybdenum, total
5.45 mg/kg
6/13/23
0.500 mg/kg
EPA 200.7
Nickel, total
22.8 mg/kg
6/13/23
2.0 mg/kg
EPA 200.7
Phosphorus, total
15,100 mg/kg
6/13/23
2..00 mg/kg
EPA 200.7
Selenium, total
3.86 mg/kg
6/13/23
0.500 mg/kg
EPA 200.7
Silver, total
5.12 mg/kg
6/13/23
0.250 mg/kg
EPA 200.7
Sodium, total
484 mg/kg
6/13/23
20.0 mg/kg
EPA 200.7
Zinc, total
633 mg/kg
6/13/23
0.500 mg/kg
EPA 200.7
Cyanide, total
<OS58 mg/L
6/8/23
0.558 mg/L
EPA 335.4
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Analytical Results
City of Lenoir
1905 Broadland Road
Lenoir, NC 28633
Receive Date: 05/30/2023
Reported: 06/05/2023
For:
Comments: GEOMETRIC MEAN: 9.0 MPN/g
J Q�r
3 G3
STATESVILLE
ANALYTICAL
1
Sample Number
Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
230530-13-01
Fecal Coliforms
1
9.3
MPN/g
SM92210E-2006
05/30/2023
MD
230530-13-01
Percent Solids
1
86.1
%
SM254OB-2011
05/30/2023
MD
230530-13-02
Fecal Coliforms
2
9.4
MPNIg
SM92210E-2006
05/30/2023
MD
230530-13-02
Percent Solids
2
85.5
%
SM25409-2011
05/30/2023
MD
230530-13-03
Fecal Coliforms
3
3.5
MPNfg
SM92210E-2006
05/30/2023
MD
230530-13-03
Percent Solids
3
86.1
%
SM254OB-2011
05/30/2023
MD
230530-13-04
Fecal Coliforms
4
5.8
MPNIg
SrvM92210E-2006
05/30/2023
MD
230530-13-04
Percent Solids
4
86.2
%
SM254OB-2011
05/30/2023
MD
230530-13-05
Fecal Coliforms
5
87.9
MPNIg
SM92210E-2006
05/30/2023
MD
230530-13-05
Percent Solids
5
86.0
%
SM254OB-2011
05/30/2023
MD
230530-13-06
Fecal Coliforms
6
9.3
MPN/g
SM92210E-2006
05130/2023
MD
230530-13-06
Percent Solids
6
86.0
%
SM254OB-2011
05/30/2023
MD
230530-13-07
Fecal Coliforms
7
12.8
MPNIg
SM92210E-2006
05/30/2023
MD
230530-13-07
Percent Solids
7
86.0
%
SM254OB-2011
05/3012023
MD
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Pagel of 4

Contact: Lisa Triplett
Client: City of Lenoir
1905 Broadland Road
Lenoir NC 28645
Meritech Work Order # 082223138
Mer itech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Sample: 082223-Biosolids Grab
Report Date: 9/7/2023
NPDES #: NCO023981
Date Sample Rcvd: 8/22/2023
8/22/2023
Parameters
Results
Analvsis Date
Reuortin Lg imit
Method
% Total Solids
81.8 %
8/23/23
0-100 %
SM 2540B
Ammonia, Nitrogen
4,840 mg/kg
8/28/23
10 mg/kg
EPA 350.1
TKN
39,400 mg/kg
8/29/23
20 mg/kg
EPA 351.1
Nitrate/Nitrite, Nitrogen
<1.2.2 mg/kg
9/6/23
12.2 mg/kg
EPA 353.2
Nitrogen, total
39,400 mg/kg
9/6/23
20.0 mg/kg
EPA 353.2
Aluminum, total
8,000 mg/kg
8/24/23
2.50 mg/kg
EPA 200.7
Arsenic, total
1.81 mg/kg
8/24/23
0.060 mg/kg
EPA 200.7
Cadmium, total
0.924 mg/kg
8/24/23
0.100 mg/kg
EPA 200.7
Calcium, total
7,180 mg/kg
8/24/23
10.0 mg/kg
EPA 200.7
Chromium, total
16.3 mg/kg
8/24/23
0.250 mg/kg
EPA 200.7
Copper, total
312 mg/kg
8/24/23
1.00 mg/kg
EPA 200.7
Lead, total
18.1 mg/kg
8/24/23
0.500 mg/kg
EPA 200.7
Magnesium, total
2,600 mg/kg
8/24/23
10.0 mg/kg
EPA 200.7
Mercury, total
0.232 mg/kg
8/29/23
0.02 mg/kg
EPA 245.1
Molybdenum, total
2.65 mg/kg
8/24/23
0.500 mg/kg
EPA 200.7
Nickel, total
21.1 mg/kg
8/24/23
2.0 mg/kg
EPA 200.7
Phosphorus, total
11,400 mg/kg
8/24/23
2.00 mg/kg
EPA 200.7
Selenium, total
1.60 mg/kg
8/24/23
0.500 mg/kg
EPA 200.7
Silver, total
2.35 mg/kg
8/24/23
0.250 mg/kg
EPA 200.7
Sodium, total
1,280 mg/kg
8/24/23
20.0 mg/kg
EPA 200.7
Zinc, total
522 mg/kg
8/24/23
0.500 mg/kg
EPA 200.7
Cyanide, total
1.43 mg/L
8/24/23
0558 mg/L
EPA 335.4
1 hereby certify that I have reviewed and approve these data. Q �
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Analytical results
STATESVILLE
ANALYTICAL
City of Lenoir'
-
1905 Broadland Road
�r j
Ul
r
Lenoir, NC 28633
Receive Date: 08/23/2023
Reported: 08/25/2023
For: 082323 Biosolids
Comments: Geometric
Mean: 320
MPN/g
Sample Number Parameter
Sample ID Result
Unit
Method
Analyzed
Analyst
230823-15-01 Fecal Coliforms
F-1
(Li-9i 6zi
MPN/g
SM9221 CE-2014
08/23/2023
CL
230823-15-01 Percent Solids
F-1
83.5
%
SM264OB-2011
08/23/2023
CL
230823-15-02 Fecal Coliforms
F-2
C1065
MPN/g
SM9221 CE-2014
08/23/2023
CL
230823-15-02 Percent Solids
F-2
84.5
%
sM25406 za11
08/23/2023
CL
230823-15-03 Fecal Coliforms
F-3
108 f
MPN/g
SM9221 CE-2014
08/23/2023
CL
230823-15-03 Percent Solids
F-3
83.2
%
SM254OB-2011
08/23/2023
CL
230823-15-04 Fecal Coliforms
F-4
1
�5.9
MPNIg
sM9zz1 cs-2o,4
08/23/2023
CL
230823-15-04 Percent Solids
F-4
%
SM254OB-2011
08/23/2023
CL
230823-15-05 Fecal Coliforms
F-5
98
MPN/g
sM9221 cE-2014
08/23/2023
CL
230823-15-05 Percent Solids
F-5
85.9
%
SM254OB-2011
08/23/2023
CL
230823-15-06 Fecal Coliforms
F-6
200
MPN/g
SM9221 CE-2014
08/23/2023
CL
230823-15-06 Percent Solids
F-6
84.9
%
SM254OB-2011
08/23/2023
CL
230823-15-07 Fecal Coliforms
F-7
200 )
MPNIg
SM9221 CE-2014
08/23/2023
CL
230823-15-07 Percent Solids
F-7
qD
sM254OB-2011
08/23/2023
CL
Respectfully submitted,
/GCc. 1�12
oo1
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 a Statesville, NC 28687 e 704/872/4697
Page 1 of 4

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Lisa Triplett Report Date: 1 2 2024
Client: City of Lenoir / /
NPDES #: NC0023981
1905 Broadland Road
Lenoir NC 28645 Date Sample Rcvd: 12/19/2023
Meritech Work Order # 121923195 Sample: 121923-Biosolids Grab 12/19/2023
Parameters
Results
Analvsis Date
Renortin Limit
Method
% Total Solids
77.6 %
12/19/23
0-100 %
SM 2540B
Ammonia, Nitrogen
123 mg/kg
12/27/23
10 mg/kg
EPA 350.1
TKN
6,850 mg/kg
1.2/27/23
20 mg/kg
EPA 351.1
Nitrate/Nitrite, Nitrogen
<12.9 mg/kg
12/22/23
12.9 mg/kg
EPA 353.2
Nitrogen, total
6,850 mg/kg
12/27/23
20.0 mg/kg
EPA 353.2
Aluminum, total
14,900 mg/kg
12/20/23
2.50 mg/kg
EPA 200.7
Arsenic, total
1.91 mg/kg
12/20/23
0.060 mg/kg
EPA 200.7
Cadmium, total
0.398 mg/kg
12/20/23
0.100 mg/kg
EPA 200.7
Calcium, total
9,380 mg/kg
12/20/23
10.0 mg/kg
EPA 200.7
Chromium, total
14.8 mg/kg
12/20/23
0.250 mg/kg
EPA 200.7
Copper, total
405 mg/kg
12/20/23
1.00 mg/kg
EPA 200.7
Lead, total
18.2 mg/kg
12/20/23
0.500 mg/kg
EPA 200.7
Magnesium, total
2,840 mg/kg
12/20/23
10.0 mg/kg
EPA 200.7
Mercury, total
0.316 mg/kg
12/26/23
0.02 mg/kg
EPA 245.1
Molybdenum, total
3.16 mg kg
12/20/23
0.500 mg/kg
EPA 200.7
Nickel, total
25.8 mg/kg
12/20/23
2.0 mg/kg
EPA 200.7
Phosphorus, total
16,900 mg/kg
12/20/23
2.00 mg/kg
EPA 200.7
Selenium, total
<0.644 mg/kg
12/20/23
0.644 mg/kg
EPA 200.7
Silver, total
1.57 mg/kg
12/20/23
0.250 mg/kg
EPA 200.7
Sodium, total
514 mg/kg
12/20/23
20.0 mg/kg
EPA 200.7
Zinc, total
711 mg/kg
12/20/23
0.500 mg/kg
EPA 200.7
SAR
1.05 -
12/20/23
-
-
Cyanide, total
<0.500 mg/L
12/28/23
0.500 mg/L
EPA 335.4
PH
•6.9 S.U.
12/22/23
1.0 - 14.0 S.U.
SM 4500-HB
I hereby certify that 1 have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] i`ax.[phone]

City of Lenoir
1905 Broadland Road
Lenoir, NC 28633
Receive Date:
Reported:
For:
Comments:
Analytical Results
12/19/2023
12/20/2023
GEOMETRIC MEAN: 398 MPN/g
ba:3
STATESVILLE
ANALYTICAL
Sample Number
Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
231219-14-01
Fecal Coliforms
F1
1990
MPN/g
SMM21 CE-2014
12/19/2023
CL
231219-14-01
Percent Solids
F1
80.4
%
SM254❑B-2011
12/19/2023
MD
231219-14-02
Fecal Coliforms
F2
108
MPN/g
SM9221 CE-2014
12/19/2023
CL
231219-14-02
Percent Solids
F2
83.4
%
SM25403-2011
12/19/2023
MD
231219-14-03
Fecal Coliforms
F3
1944
MPN/g
SM9221 CE-2014
12/19/2023
CL
231219-14-03
Percent Solids
F3
82.3
%
SM2540B-2011
12/19/2023
MD
231219-14-04
Fecal Coliforms
F4
87
MPN/g
SM9221 CE-2014
12/19/2023
CL
231219-14-04
Percent Solids
F4
80.8
%
SM254OB-2011
12/19/2023
MD
231219-14-05
Fecal Coliforms
F5
1993
MPN/g
SM9221 CE-2014
12/19/2023
CL
231219-14-05
Percent Solids
F5
80.3
%
SM254OB-2011
12/19/2023
MD
231219-14-06
Fecal Coliforms
F6
298
MPN/g
SM9221 CE-2014
12J19/2023
CL
231219-14-06
Percent Solids
F6
80.8
%
SM2540B-2011
12/19/2023
MD
231219-14-07
Fecal Coliforms
F7
74
MPN/g
SM9221 CE-2014
12/19/2023
CL
231219-14-07
Percent Solids
F7
80.8
%
SM254❑B-2011
12J19/2023
MD
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
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