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HomeMy WebLinkAboutWQ0002857_Monitoring - 07-2024_20240913Monitoring Report Submittal Permit Number#* Name of Facility:* Month:* July WQ0002857 Piedmont Custom Meats WWTP Report Information Type * NDMR, NDAR-1, NDAR-2, NDMLR Confirmation Email Address: Name of Submitter: * Signature: Date of submittal: Initial Review Year:* 2024 Upload Document* Piedmont Custom_July 2024.pdf 1.97MB PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Jessica.Mize@pacelabs.com Jessica Mize Reviewer: Wanda.Gerald 9/13/2024 This will be filled in automatically Is the project number correct?* W00002857 Is the monitoring report accepted?* Yes NO Regional Office* Winston-Salem Reviewer: _anonymous Review Date: 9/16/2024 FORM: NDMR 03-12 NON -DISCHARGE MONITORING REPORT (NDMR) Page of Permit No.: W00002857 Facility Name: Piedmont Custom Meats WWTF County: Caswell Month: July Year: 2024 PPI: 001 ❑ Influent ED Effluent ❑ No Flow generated Parameter Monitoring Point: [:1 Influent R] Effluent ❑ Groundwater Lowering ❑ Surface Water Parameter Code -Pp� 50050 50060 31616 00610 00626 00620 00600 00400 00665 00530 00310 00940 70300 o�. A IxO P U) WcE: O 9 ' o U o o U c oQ E E � i9 zti m o- „ zF m S3 Z S a p }9 qc a c a vU) vvcm c =im W pto v t U w ro oU GE p 24-hr hrs GPD mg/L X1100 mL mg1L amWL, mg/L rng1L su mg1L mg/L m91L mg/L mgfL 1 1,209 2 1,209 3 08:55 0.75 1,209 ' <0.01 6.4 4 902 5 902 61 902 7 902 8 902; 9 902 10 902 11 09:20 3.5 769 <0.01 33,000 94.3 149 <0.040 1 149 6.3 15.4',. 185 339 : 116 870. 12 769 13 769 14 769_ _ 15 769 : 16 769 17 807 18 807 19 08:00 0.25 807 <0.01 6.4 20 807 21 807 22 15:40 0.25 1 807 <0.01 6.4 231 807 24 807 25 813 26 813 27 813 28 291 15:00 0.25 813 <0.01 6.3 30 813 311 813 Average: 861 ' 0.00 33000.00 94.30 149.00 0.00 =149:00 15.40Y 185.00 339.00 116.00 870.00 Daily Maximum: 1,209 0.01 33,000.00 94.30 149.00 0.04 L.149.00L 6.40 15.40 185.00 339.00 116.00 870.00 Daily Minimum: 769 0.01 33000.00 94.30 149.00 0.04 'C49i0>): 6.30 15A0 185.00 339.00 116.00 870.00 Sampling Type: Estimate Grab Grab Grab t3iAb.: Grab drab ._;:. Grab Grab Grab Grab Monthly Avg. Limit: 5,000 Daily Limit: Sample Frequency:1 Monthly I Weekly 3xyr 3xyr 3xyr 3xyr 3xyr Weekly 3xyr.. 3xyr 3xyr -, FORM: NDMR 03-12 NON -DISCHARGE MONITORING REPORT (NDMR) Page of Sampling Person(s) Certified Laboratories Name: Glenn Price Name: Pace Analytical Laboratories Name: Name: n�n�+ �11 mnni4nrinn j+afn and ammnlinn frariiianr_iPC inP_P_t thp_ rp_rliiirp_rnpnft in Aftael7mLant A Of vour ne-rmit? Compliant El Non -Compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective Gl.11 Ul RZ; lance. MttOU I GUUMU4101 05;GG D 11 Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: Glenn Price Permittee: Baron Neal MCDuffe (Authorized Agent) Certification No.: 987931120771 Signing Official: Baron Neal McDuffie Grade: II Phone Number: 336-408-7924 Signing Official's Title: Field Services Director (Pace Analytical Services) Has the ORC changed since the previous NDMR? ❑ Yes O No Phone Number: 336-402-9924 Permit Expiration: 3/31 /2021 Signature Date Date SignatuZand By this signature, I certify that this report is acacrate and complete to the best of my knowledge. I certify, under penalty of law, that this doctachments were prepared under my direction or supervision in accordance with a system designed to assfied personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, aocurate, and complete. I am aware that there are significant penalties for submitting false Information, including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 FORM NDAR-1 10-13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page Permit No.: WQ0002857 Facility Name: Piedmont Custom Meats WWTF County: Caswell • irrigation occur Area (acres): Area (acres): Area (acres): Area (acres): at thiS lacility? I Cover Crop: • '. 1 • '. 1 • '. 1 • '. 1 Annual Rate (in): Annual Rate (in�., Annual Rate (in):: Annual Rate (in):, Field Irrigated?' ©���©_ 1.1 •1 � 11: 1.1 �� 11: 1.1 •1 � 11: 1.1 �� 1 1• m ___ __ -_-- ---- -_-- ---- M-onthly Loading:1.1 ��_ /•1 -�_ / 1 _�_ 1.1 _�� FORM: NDAR-1 10-13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page of Did the application rates exceed the limits in Attachment B of your permit? Were adequate measures taken to prevent effluent ponding in or runoff from the sites? Was a suitable vegetative cover maintained on all sites as specified in your permit? Were all setbacks listed in your permit maintained for every application to each permitted site? Were all freeboards maintained in accordance with the specified freeboard heights in your permit? 1-6mpliant ❑ Non -Compliant ttK.pliant ❑ Non -Compliant tQ &mpliant ❑ Non -Compliant W'Compliant ❑ Non -Compliant VC/.mpliant ❑ Non -Compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: Glenn Price Permittee: Baron Neal McDuffie (Authorized Agent) Certification No.: 987931/20771 Signing Official: Baron Neal McDuffie Grade: I I Phone Number: 336-408-7924 Signing Official's Title: Field Service Director (Pace Analytical Services Has the ORC changed since the previous NDAR-1? ❑ Yes p No Phone Number: 336-402-9924 Permit Exp.: b Signature Date Signatu Date By this signature, I certify that this report is accurrate and complete to the best of my knowledge. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my Inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the Information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and Imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Pace Analytical Services, LLC 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 July 31, 2024 Larry Moore Piedmont Custom Meats 430 NC Highway 49 South Asheboro, NC 27205 RE: Project: Piedmont Custom Meats- July Pace Project No.: 92741251 Dear Larry Moore: Enclosed are the analytical results for sample(s) received by the laboratory on July 11, 2024. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Eden If you have any questions concerning this report, please feel free to contact me. Sincerely, Stephanie Knott stephanie.knoft@pacelabs.com 704-977-0981 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC- Pagel of 25 (-�Face' Project: Piedmont Custom Meats- July Pace Project No.: 92741251 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 Pace Analytical Services Eden 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 CERTIFICATIONS South Carolina Laboratory ID: 99030 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 North Carolina Wastewater Certification #: 633 Virginia/VELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Page 2 of 25 (-�Face' SAMPLE ANALYTE COUNT Project: Piedmont Custom Meats- July Pace Project No.: 92741251 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92741251001 MW-1 SM 254OC-2015 DAW 1 PASI-E EPA 350.1 Rev 2.0 1993 LRB 1 PASI-E EPA 353.2 Rev 2.0 1993 LRB 1 PASI-E SM 9222D-2015 DAW 1 PASI-E EPA 120.1-1982 SMS 1 PASI-A EPA 300.0 Rev 2.1 1993 JCM 2 PASI-A SM 531OB-2014 MJP 1 PASI-A 92741251002 MW-4 SM 254OC-2015 DAW 1 PASI-E EPA 350.1 Rev 2.0 1993 LRB 1 PASI-E EPA 353.2 Rev 2.0 1993 LRB 1 PASI-E SM 9222D-2015 DAW 1 PASI-E EPA 120.1-1982 SMS 1 PASI-A EPA 300.0 Rev 2.1 1993 JCM 2 PASI-A SM 53108-2014 MJP 1 PASI-A 92741251003 MW-5 SM 254OC-2015 DAW 1 PASI-E EPA 350.1 Rev 2.0 1993 LRB 1 PASI-E EPA 353.2 Rev 2.0 1993 LRB 1 PASI-E SM 9222D-2015 DAW 1 PASI-E EPA 120.1-1982 SMS 1 PASI-A EPA 300.0 Rev 2.1 1993 JCM 2 PASI-A SM 531 OB-2014 MJP 1 PASI-A 92741251004 Effluent SM 254OC-2015 DAW 1 PASI-E SM 254OD-2015 JMM2 1 PASI-E EPA 353.2 Rev 2.0 1993 LRB 1 PASI-E SM 521OB-2016 VLG 1 PASI-E SM 9222D-2015 DAW 1 PASI-E TKN+NO3+NO2 Calculation MDW 1 PASI-A EPA 300.0 Rev 2.1 1993 JCM 1 PASI-A EPA 350.1 Rev 2.0 1993 NCF 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 CEM 1 PASI-A EPA 365.1 Rev 2.0 1993 Zip 1 PASI-A PASI-A = Pace Analytical Services -Asheville PAS I-E = Pace Analytical Services - Eden REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, L.L.C. Page 3 of 25 (_�Face' ANALYTICAL RESULTS Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Project: Piedmont Custom Meats- July Pace Project No.: 92741251 Sample: MW-1 Lab ID: 92741251001 Collected: 07/11124 10:18 Received: 07/11/24 13:13 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services - Eden Total Dissolved Solids 332 mg/L 50.0 1 07/12/24 14:21 350.1 Ammonia EDN Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Ammonia ND mg/L 0.10 1 07/15/24 14:40 7664-41-7 353.2 NO2/NO3 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Nitrate 22.4 mg/L 0.20 5 07/12/24 09:33 14797-55-8 MBIO 9222D Fecal Collform EDN Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Eden Fecal Coliforms ND CFU/100 mL 1.0 1 07/11124 15:25 07/12/24 14:51 120.1 Specific Conductance Analytical Method: EPA 120.1-1982 Pace Analytical Services -Asheville Specific Conductance 490 umhos/cm 10.0 1 07/19/24 17:51 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 53.6 mg/L 1.0 1 07/14/24 05:16 16887-00-6 Sulfate 3.4 mg/L 1.0 1 07/14/24 05:16 14808-79-8 5310E TOC Analytical Method: SM 531 OB-2014 Pace Analytical Services -Asheville Total Organic Carbon ND mg/L 1.0 1 07/22/24 06:54 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/31/2024 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 25 �ce' ANALYTICAL RESULTS Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Project: Piedmont Custom Meats- July Pace Project No.: 92741251 Sample: MW-4 Lab ID: 92741251002 Collected: 07/11/24 10:44 Received: 07/11/24 13:13 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services - Eden Total Dissolved Solids 685 mg/L 125 1 07/12/24 14:21 350.1 Ammonia EDN Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Ammonia ND mg/L 0.10 1 07/15/24 14:39 7664-41-7 353.2 N021NO3 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Nitrate 2.3 mg/L 0.040 1 07/12/24 09:30 14797-55-8 MBIO 9222D Fecal Coliform EDN Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Eden Fecal Coliforms ND CFU/100 mL 1.0 1 07/11/24 15:25 07/12/24 14:51 120.1 Specific Conductance Analytical Method: EPA 120.1-1982 Pace Analytical Services - Asheville Specific Conductance 1060 umhos/cm 10.0 1 07/19/24 17:53 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 249 mg1L 5.0 5 07/14/2410:13 16887-00-6 Sulfate 5.7 mg/L 1.0 1 07/14/24 05:31 14808-79-8 531 OB TOC Analytical Method: SM 531 OB-2014 Pace Analytical Services -Asheville Total Organic Carbon ND mg/L 1.0 1 07/22/24 07:11 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/31/2024 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 25 (_�Face� ANALYTICAL RESULTS Project: Piedmont Custom Meats- July Pace Project No.: 92741251 Pace Analytical Services, LLC 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 Sample: MW-5 Parameters Lab ID: 92741251003 Collected: 07/11/24 11:00 Results Units Report Limit DF Received: 07/11/24 13:13 Matrix: Water Prepared Analyzed CAS No. Qua] 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services - Eden Total Dissolved Solids 228 mg/L 25.0 1 07/12/24 14:21 350.1 Ammonia EDN Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Ammonia ND mg/L 0.10 1 07/15/24 14:46 7664-41-7 353.2 NO2/NO3 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Nitrate 0.29 mg/L 0.040 1 07/12/24 09:32 14797-55-8 MBIO 9222D Fecal Coliform EDN Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Eden Fecal Coliforms ND CFUI100 mL 1.0 1 07/11/24 15:25 07/12/24 14:51 120.1 Specific Conductance Analytical Method: EPA 120.1-1982 Pace Analytical Services - Asheville Specific Conductance 414 umhos/cm 10.0 1 07/19/24 17:55 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 97.0 mg/L 1.0 1 07/14/24 05:46 16887-00-6 Sulfate ND mg/L 1.0 1 07/14/24 05:46 14808-79-8 5310B TOC Analytical Method: SM 531 OB-2014 Pace Analytical Services -Asheville Total Organic Carbon ND mg/L 1.0 1 07/22/24 07:31 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/31/2024 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 25 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 ANALYTICAL RESULTS Project: Piedmont Custom Meats- July Pace Project No.: 92741251 Sample: Effluent Lab ID: 92741251004 Collected: 07/11/24 11:17 Received: 07/11/24 13:13 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services - Eden Total Dissolved Solids 870 mg/L 250 1 07/12/24 14:21 2540D Total Suspended Solids Analytical Method: SM 254OD-2015 Pace Analytical Services - Eden Total Suspended Solids 185 mg/L 45.5 1 07/11/24 15:07 353.2 NO2IN03 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Nitrate ND mg1L 0.040 1 07/12/24 09:37 14797-55-8 5210E BOD, 5 day EDN Analytical Method: SM 521OB-2016 Preparation Method: SM 521OB-2016 Pace Analytical Services - Eden BOD, 5 day 339 mg/L 2.0 1 07/12/24 11:38 07/17/24 14:25 MBIO 9222D Fecal Coliform EDN Analytical Method: SM 922213-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Eden Fecal Coliforms 33000 CFU/100 mL 1.0 1 07/11/24 15:25 07/12/24 14:51 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services -Asheville Total Nitrogen 149 mg/L 0.040 1 07/31/24 13:01 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 116 mg/L 3.0 3 07/14/2410:28 16887-00-6 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia 94.3 mg1L 1.0 10 07/23/24 18:17 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, Kjeldahl, Total 149 mg/L 10.0 10 07/30/24 15:55 07/31/24 09:38 7727-37-9 353.2 Nitrogen, N021NO3 pres. Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, NC2 plus NO3 0.15 mg/L 0.040 1 07/27/24 04:20 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.01993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 15.4 mg1L 0.25 5 07/22/2418:29 07/23/2412:13 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/31/2024 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 25 (- �gace, QUALITY CONTROL DATA Project: Piedmont Custom Meats- July Pace Project No.: 92741251 QC Batch: 867894 Analysis Method: SM 254OC-2015 QC Batch Method: SM 254OC-2015 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92741251001, 92741251002, 92741251003, 92741251004 METHOD BLANK: 4473558 Matrix: Water Associated Lab Samples: 92741251001, 92741251002, 92741251003, 92741251004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Dissolved Solids mg/L ND 25.0 07/12/24 14:20 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 4473559 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Dissolved Solids mg/L 250 264 106 90-110 SAMPLE DUPLICATE: 4473560 92740401001 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L 5320 5060 5 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/31 /2024 01:03 PM without the written consent of Pace Analytical Services, LLC, Page 8 of 25 (-)Pace, QUALITY CONTROL DATA Project: Piedmont Custom Meats- July Pace Project No.: 92741251 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 867598 Analysis Method: SM 254OD-2015 QC Batch Method: SM 254OD-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92741251004 METHOD BLANK: 4472062 Matrix: Water Associated Lab Samples: 92741251004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 07111/24 15:06 LABORATORY CONTROL SAMPLE: 4472063 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 248 99 90-110 SAMPLE DUPLICATE: 4472064 92741251004 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 185 178 4 SAMPLE DUPLICATE: 4472065 92740923001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 247 240 3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/31 /2024 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 25 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QUALITY CONTROL DATA Project: Piedmont Custom Meats- July Pace Project No.: 92741251 QC Batch: 868209 Analysis Method: EPA 350.1 Rev 2.0 1993 QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia, EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92741251001, 92741251002, 92741251003 METHOD BLANK: 4474835 Matrix: Water Associated Lab Samples: 92741251001, 92741251002, 92741251003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Ammonia mg/L ND 0.10 07/15/24 14:29 LABORATORY CONTROL SAMPLE: 4474836 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Ammonia mg/L 5 5.3 105 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4474837 MS 92741322001 Spike Parameter Units Result Conc. Nitrogen, Ammonia mg/L ND 5 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4475421 MS 92741306001 Spike Parameter Units Result Conc. Nitrogen, Ammonia mg/L ND 5 4474838 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits RPD 5 5.2 5.2 104 105 90-110 0 4475422 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits RPD 5 5.4 5.4 107 107 90-110 0 Results presented on this page are in the units indicated by the "Units" column except whore an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/31/2024 01:03 PM without the written consent of Pace Analytical Services, LLC. Qual Qual Page 10 of 25 (-�Face, QUALITY CONTROL DATA Project: Piedmont Custom Meats- July Pace Project No.: 92741251 QC Batch: 867745 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92741251001, 92741251002, 92741251003, 92741251004 METHOD BLANK: 4472981 Matrix: Water Associated Lab Samples: 92741251001, 92741251002, 92741251003, 92741251004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mg/L ND 0.040 07/12/24 09:23 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 4472982 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/L 1.5 1.5 97 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4472983 4472984 MS MSD 92741251001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Nitrate mg/L 22.4 1.5 1.5 23.8 23.8 91 95 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an aftemats unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/31 /2024 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 25 (-`gacell QUALITY CONTROL DATA Project: Piedmont Custom Meats- July Pace Project No.: 92741251 QC Batch: 867770 Analysis Method: SM 521 OB-2016 QC Batch Method: SM 521OB-2016 Analysis Description: 5210E BOD, 5 day Final EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92741251004 METHOD BLANK: 4473034 Associated Lab Samples: 92741251004 Parameter Units BOD, 5 day mg1L LABORATORY CONTROL SAMPLE: 4473035 Parameter Units BOD, 5 day mg/L Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.0 07117/2412:32 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 198 174 88 84.6-115 SAMPLE DUPLICATE: 4473037 92741246001 Dup Parameter Units Result Result BOD, 5 day mg/L 104 84.8 RPD Qualifiers 20 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/31/2024 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 25 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QUALITY CONTROL DATA Project: Piedmont Custom Meats- July Pace Project No.: 92741251 QC Batch: 867801 Analysis Method: SM 9222D-2015 QC Batch Method: SM 9222D-2015 Analysis Description: 9222D Fecal Coliform(MF)-EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92741251001, 92741251002, 92741251003, 92741251004 METHOD BLANK: 4473131 Matrix: Water Associated Lab Samples: 92741251001, 92741251002, 92741251003, 92741251004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL ND 1.0 07/12/24 14:51 METHOD BLANK: 4473133 Matrix: Water Associated Lab Samples: 92741251001, 92741251002, 92741251003, 92741251004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL ND 1.0 07/12/24 14:51 SAMPLE DUPLICATE: 4473132 92741251001 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms CFU/100 mL ND ND Results presented on this page are in the units Indicated by the "Units" column except where an altemate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/31 /2024 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 25 (-' 'ace, QUALITY CONTROL DATA Project: Piedmont Custom Meats- July Pace Project No.: 92741251 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 869534 Analysis Method: EPA 120.1-1982 QC Batch Method: EPA 120.1-1982 Analysis Description: 120.1 Specific Conductance Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92741251001, 92741251002, 92741251003 METHOD BLANK: 4481539 Matrix: Water Associated Lab Samples: 92741251001, 92741251002, 92741251003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Specific Conductance umhos/cm ND 10.0 07/19124 17:26 LABORATORY CONTROL SAMPLE: 4481540 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Specific Conductance umhos/cm 1410 1400 99 90-110 SAMPLE DUPLICATE: 4481541 92740403002 Dup Parameter Units Result Result RPD Qualifiers Specific Conductance umhos/cm 65.1 65.0 0 SAMPLE DUPLICATE: 4481542 92740458003 Dup Parameter Units Result Result RPD Qualifiers Specific Conductance umhos/cm 607 607 0 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/31 /2024 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 25 (-�Face' QUALITY CONTROL DATA Project: Piedmont Custom Meats- July Pace Project No.: 92741251 QC Batch: 868042 Analysis Method: EPA 300.0 Rev 2.1 1993 QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92741251001, 92741251002, 92741251003, 92741251004 METHOD BLANK: 4474476 Matrix: Water Associated Lab Samples: 92741251001, 92741251002, 92741251003, 92741251004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride mg/L ND 1.0 07/13/24 23:50 Sulfate mg/L ND 1.0 07/13/24 23:50 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 4474477 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride mg/L 50 51.9 104 90-110 Sulfate mg/L 50 52.1 104 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4474478 4474479 MS MSD 92741663002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride mg/L 50.8 50 50 99.9 93.0 98 84 90-110 7 M1 Sulfate mg/L 32.4 50 50 83.2 83.6 101 102 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4474480 4474481 MS MSD 92741217001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride mg/L 36.0 50 50 81.3 82.1 91 92 90-110 1 Sulfate mg/L 972 50 50 1010 1020 74 87 90-110 1 M1 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 07/31/2024 01:03 PM without the written consent of Pace Analytical Services, I.I.C. Page 15 of 25 (-�Face' QUALITY CONTROL DATA Project: Piedmont Custom Meats- July Pace Project No.: 92741251 QC Batch: 870336 Analysis Method: EPA 350.1 Rev 2.0 1993 QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92741251004 METHOD BLANK: 4485116 Associated Lab Samples: 92741251004 Parameter Units Nitrogen, Ammonia mg/L LABORATORY CONTROL SAMPLE: 4485117 Parameter Units Nitrogen, Ammonia mg/L Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.10 07/23/2417:35 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 5 5.2 104 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4485118 4485119 MS MSD 92741084001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[ Nitrogen, Ammonia mg/L 1.4 5 5 6.5 6.5 101 100 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4485120 4485121 MS MSD 92741088001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L 142 5 5 150 148 157 101 90-110 2 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/31/2024 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 25 (-�Face' QUALITY CONTROL DATA Project: Piedmont Custom Meats- July Pace Project No.: 92741251 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 871680 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92741251004 METHOD BLANK: 4491255 Matrix: Water Associated Lab Samples: 92741251004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg/L ND 0.50 07/31/24 07:34 LABORATORY CONTROL SAMPLE: 4491256 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg/L 10 10 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4491257 4491258 MS MSD 92743259001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 39.8 10 10 55.6 52.0 158 122 90-110 7 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4491259 4491260 MS MSD 92743259002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 35.4 10 10 50.6 50.0 153 146 90-110 1 M1 Results presented an this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/31/2024 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 25 (-�Face' Project: Piedmont Custom Meats- July Pace Project No.: 92741251 QC Batch: 871458 QC Batch Method: EPA 353.2 Rev 2.0 1993 Associated Lab Samples: 92741251004 METHOD BLANK: 4490673 Associated Lab Samples: 92741251004 Parameter Units Nitrogen, NO2 plus NO3 mg/L QUALITY CONTROL DATA Analysis Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, preserved Laboratory: Pace Analytical Services -Asheville Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0,040 07/27/24 04:01 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 4490674 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mg/L 2.5 2.5 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4490675 MS 92742356001 Spike Parameter Units Result Conc. Nitrogen, NO2 plus NO3 mg/L 7.7 2.5 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4490677 MS 92741435002 Spike Parameter Units Result Conc. Nitrogen, NO2 plus NO3 mg/L 0.45 2.5 4490676 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits RPD 2.5 10.3 10.3 102 103 90-110 0 4490678 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits RPD 2.5 3.0 3.0 101 101 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/31/2024 01:03 PM without the written consent of Pace Analytical Services, LLC. Qual Qual Page 18 of 25 (-�Face' QUALITY CONTROL DATA Project: Piedmont Custom Meats- July Pace Project No.: 92741251 QC Batch: 869954 Analysis Method: EPA 365.1 Rev 2.01993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92741251004 METHOD BLANK: 4483601 Matrix: Water Associated Lab Samples: 92741251004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/L ND 0.050 07/2312411:08 LABORATORY CONTROL SAMPLE: 4483602 Spike Parameter Units Conc. Phosphorus mg/L 2.5 Pace Analytical Services, LLC 1377 South Park Drive Kemersville. NC 27284 (704)977-0981 LCS LCS % Rec Result % Rec Limits Qualifiers 2.5 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4483603 4483604 MS MSD 92741187001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 5.6 2.5 2.5 7.8 7.8 89 88 90-110 0 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4483605 4483606 MS MSD 92741187002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L ND 2.5 2.5 2.4 2.4 95 97 90-110 2 Results presented on this page are in the units indicated by the "units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/3112024 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 25 ace'� QUALITY CONTROL DATA Project: Piedmont Custom Meats- July Pace Project No.: 92741251 QC Batch: 869884 Analysis Method: SM 531 OB-2014 QC Batch Method: SM 531 OB-2014 Analysis Description: 5310E TOC Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92741251001, 92741251002, 92741251003 METHOD BLANK: 4483437 Matrix: Water Associated Lab Samples: 92741251001, 92741251002, 92741251003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Organic Carbon mg/L NO 1.0 07122/24 02:21 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977.0981 LABORATORY CONTROL SAMPLE: 4483438 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg1L 25 24.8 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4483439 MS 92741110002 Spike Parameter Units Result Conc. Total Organic Carbon mg1L NO 25 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4483441 MS 92741110003 Spike Parameter Units Result Conc. Total Organic Carbon mg/L NO 25 4483440 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits RPD 25 23.6 23.8 94 95 90-110 1 4483442 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits RPD 25 23.9 24.3 95 97 90-110 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/31/2024 01:03 PM without the written consent of Pace Analytical Services, LLC. Qual Qua] Page 20 of 25 �ce' QUALIFIERS Project: Piedmont Custom Meats- July Pace Project No.: 92741251 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference INC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as 'Total' may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. ANALYTE QUALIFIERS M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/31/2024 01:03 PM without the written consent of Pace Analytical Services, L-C. Page 21 of 25 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Piedmont Custom Meats- July Pace Project No.: 92741251 Lab ID 92741251001 92741251002 92741251003 92741251004 92741251004 92741251001 92741261002 92741251003 92741251001 92741251002 92741251003 92741251004 92741251004 92741251001 92741251002 92741251003 92741251004 92741251001 92741251002 92741251003 92741251004 92741251001 92741251002 92741251003 92741251004 92741251004 92741251004 92741251004 92741251004 92741251001 92741251002 92741251003 Sample ID M W-1 MW-4 MW-5 Effluent Effluent M W-1 MW-4 MW-5 MW-1 MW-4 MW-5 Effluent Effluent MW-1 MW-4 MW-5 Effluent M W-1 MW-4 MW-5 Effluent MW-1 MW-4 MW-5 Effluent Effluent Effluent Effluent Effluent MW-1 MW-4 MW-5 Date: 07/31/2024 01:03 PM QC Batch Method SM 254OC-2015 SM 254OC-2015 SM 2540C-2015 SM 2540C-2015 SM 2540D-2015 EPA 350.1 Rev 2.01993 EPA 350.1 Rev 2.01993 EPA 350.1 Rev 2.01993 EPA 353.2 Rev 2.0 1993 EPA 353.2 Rev 2.0 1993 EPA 353.2 Rev 2.0 1993 EPA 353.2 Rev 2.0 1993 SM 521 OB-2016 SM 9222D-2015 SM 9222D-2015 SM 9222D-2015 SM 9222D-2015 EPA 120.1-1982 EPA 120.1-1982 EPA 120.1-1982 TKN+NO3+NO2 Calculation EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 EPA 350.1 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 EPA 353.2 Rev 2.0 1993 EPA 365.1 Rev 2.0 1993 SM 531OB-2014 SM 531OB-2014 SM 531OB-2014 QC Batch 867894 867894 867894 867894 867598 868209 868209 868209 867745 867745 867745 867745 867770 867801 867801 867801 867801 869534 869534 869534 B72365 868042 868042 868042 868042 870336 871680 871458 869954 869884 869884 869884 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Analytical Method SM 521OB-2016 SM 9222D-2015 SM 922213-2015 SM 922213-2015 SM 9222D-2015 Analytical Batch 868173 867802 867802 867802 867802 EPA 351.2 Rev 2.0 1993 872211 EPA 365.1 Rev 2.0 1993 870242 Page 22 of 25 ,v+rns.nn.uu�•nu�/tuQnpYplDYe•sw,a1•aXOlal�MtaJLAle1pN•�YgwfWOYtalaflPMMM//SGuu le Wnolt.&VDCrjmlu ta/Wu-Q"f T 10 i and x.y.,ra: 1•••,a.e•D �+•^�LM.+••+••. ++ ynm l••+Ir.atl a..e.ro v..t^M+. 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