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NCG200349_DMR_20240903
Omni Omnon Bo l LLC 7575 West Jefferson Boulevard Fort Wayne, India#$L4(fta rtm ent .^f Environmental Qu.;;,/ Received SEP n 3 2024 August 29,2024 Winston-S,.lem Regional Office Division of Water Resources Attn: DWR Central Files 1617 Mail Service Center Raleigh,North Carolina 27699-1617 Division of Energy,Mineral, and Land Resources Winston-Salem Regional Office 450 Hanes Mill Road, Suite 300 Winston-Salem,North Carolina 27105 RE: 2024 July and August Discharge Monitoring Reports OmniSource,LLC—Winston-Salem COC No.NCG200349 To whom it may concern: Please find enclosed with this submittal the July and August 2024 Discharge Monitoring Reports (DMRs) for our OmniSource, LLC facility in Winston-Salem (Forsyth County). Stormwater samples were collected and analyzed from three (3) outfalls during both the July and August sampling events. The following DMRs are included in this submittal: July 2024-DMR with Qualitative Monitoring Reports(QMRs)and analytical data August 2024—DMR with Qualitative Monitoring Reports(QMRs)and analytical data If you have any questions regarding this submittal,please contact me via phone(260-450-4030)or by e-mail at mark.anderson@omnisource.com. IA 1�"� � 'Si�ncerellyy, I� Y v Mark Anderson OSE Environmental Manager Attachments: a w .. =a E 0 J \ Ewe N `� OCR L% _C •o c a C o o as v W zc E Do L ~ O J O Y L V C L N �-+ 41 W ❑ Y m Z D « \� OQ N y c m O UI Vi m N `X. NO W p'❑❑ to O J f O N 0 0 0 0 N O N Z N H N y L Y .0 � 2 3 3' ❑ cc U Erm m O d > N a X O o O nmi Oi a o (p N N �>. O a o E N v o c� y l Y❑❑❑ W u u ~ 0 0 0 'o o m 3 o E 3 L G W C O W O O y 0 Ul v J O C. >-' z a) p ❑❑■ g z v m E m XXE o Vf O L a O •L O p u a m _ C w r ,� v v 'a v o, E v a .v, io+ •. `w }pj O J J ¢ O G u1 'y O Y polp =� C fj W CD O O L Z o C \ .y O O E u (0 E rn 10 E r�i n �° N v 00 > c v j E � '� O N 3 ] J 41 ` d m v y 'm Ul y �+ E �n a +w-• N y O 3 v c Ve m {- 6 V \ \ M rn m ch 0 0 m �E J U m d 'o N O N « m o N w m y O cJ E 'Q 4Z G �` OA O N = O pp -O LL L C Ul VI �y UI m C O C) m c 0] J 'in t M M m (7 N ry 3 p U N '� c m = o 21 o m o C7 c m = m m E cu -C U V1 Z m ¢ o N v N v m 'W C m j j rn Z O En c E a o v a v v = o O w t/1 ac u u W \ N N N N OG N O m Q C u O Gl IA Ol N N iN N N 42 6 m ar y j c c w o u E o o o o in _ o O O L Z m E cla OW N d VI E ^ O. d a F O K O w ¢ Q >Z LL O O OF of a: } O O E O O Oz 01 Q o '� O " fO l7 E ' Z 0 t-• c in Cc: •- m u O m m E m °' O o .mc a°1i °1 E w ¢ O W g u C m m a z c 2 a u LL u a K.C. Environmental Quolity Stol-IIINI': ter Discharge Outhill (SDO) Qualitative Monitoring Report For guidance onfilling out thisform,pleas.visit litlps://deq.ne.gov/about/divisions/energy-mineral-land-resources/ npdes-stomnvater-gps Permit No.: NI /C.' / / / / 11 / 1 or Certificate of Coverage No.: N/C_/C1' Facility Name: OrninSource SE Winston-Salem Facility _ Count}: Forsyth phone No. (336) 461-1440 Jared Spillman Inspector: Hv�nw vrnA[�� �ifr��r Date of Inspection: 7(_yy-/2,y Time of Inspection: a3�.51 Total event precipitation(inches): 0- bb All permits require qualitative monitoring to be performed during a"measurable storm event." - A"measurable storm event' is a storm event that results in an actual discharge from the permitted site outfall. The pmvious measurable storm event must have been at Ica t 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period,and the permittee obtains approval from the local DF.\1[,R Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: :;&,;_1�0^ (Signature of permittee or Designee) 1. Outfall Description; Outfall NO. I Structure(pipe,ditch,etc.): Receiving Stream: Tri'outary t_� 3�.uh; `c,rb; Desuibe the industrial activities that occur within the outfall drainage area: Lae 1�i Si (J� Page I of 2 KIC. . Eaviranmentat Quality Storniwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out thisjorm,please visit littps://deq.tic.gov/abottUdivisioiis/energy-mineral-land-resources/ opdes-stornnvater-gps Permit No.: N_IU ! / / / / ! or Certificate of Coverage No.: N/C Y Facility Name: OniinSOUrce SE tNinston-Salenl Facility County: Forsyth Phone No. (336) 461-1440 Jared Spillman Inspector: _���p,vvnarK �iC�in S r Date of Inspection: 71 LT-12N Time of Inspection: I V 15 Total Event Precipitation(inches): 030 All permits require qualitative monitoring to be performed during a"measurable storm event." I A"measurable storm event" is a storm event that results in an netaud discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permitlee is able to document that a shorter interval is representative for local stoma events during the sampling period,and the permittee obtains approval from the local DEMI R (_Regional Office. III•thi signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature ermittee or Dosignce) i 1. Outfall Description: Outfall No. 2 Structure(pipe,ditch,eta): P1 pAL Receiving Stream: Tributary to Bush] Fcik Describe the industrial activities that occur within the outfall drainage area: Sad—Ssffip� _ VYv1aA� �}V�o�Af� �04 �r�ll�Q and Si\AA Page I oft KC. . EnNronmenfal Qualify Stornlwater Discharge Outfab (SDO) Qualitative Monitoring Report For guidance onffllingoat thisform,please visit litips://deq.iie.gov/alwul/divisions/energy-mineral-land-resotirecs/ npdes-stornuvaler-gps PermitNo.: N/C! 1 ! ,' / 1 or Certificate of Coverage No.: NIC/G' PacilityName: OminSource SE Winston-Salem Facility County: Forsyth Phone No. (336) 461- 1440 Jared Spillman Inspector: g„-ny r T�L0.KSwr Date of Inspection: -7 12T� _ Time of Inspection: 14'.t > No ��Aw 'total Event Precipitation(inches): m •1_,0 All pennits require qualitative monitoring to be performed during a"measurable storm event." A"measurable storm event" is a storm event that results in as actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. 'rho 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period,and the permitter obtains approval from the local DE\ILR Regional Office. ---------- ---- - --- ------ ------ -- - ------------- -- By this signature,I certify that this report is accurate and complete to the beat of my knowledge: (Signature of Permittee or Designee) I 1. Oulfall Description Outfall No. 4 Structure(pipe,ditch,etc.): 9 Receiving Stream: TributafY tO Bush/ Describe the industrial activities that occur within the outfall drainage area: omktfi k,_Trig&_ i i i I Pao. 1 Cd2 KC.. . Environmental Quality StorniNvater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out thisform,please visit httpsd/deq.ne.gov/aboulldivisions/energy-mineral-land-resources/ npdes-stornnvater-g ps Permit No.: N_/C! / ! I I ! or Certificate of Coverage No.: NIC!G.! 1•'acility Name: OminSource SE IP/inston-Salem Facility County: Forsyth phone No. (336) 461-1440 Jared Spillman Inspector: .y .,i Rla"6.. Date of Inspection: .]1 vs- /Zy Time of Inspection: )a1 it S Total Event Precipitation(inches): o-3J All permits require qualitative monitoring to be performed during a"measurable storm event." A'hncasurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the pernittee is able to document that a shorter interval is representative for local storm events during the sampling period,and the permittce obtains approval from the local DENIER Regional Office. fay this signature,I certify that this report is accurate and complete to the best of my knowledge: (Signature of permittee or Designee) 1. Outrall Description: Outfall\o. _ S Structure(pipe,ditch,etc.): �;_P0 Receiving Stream: ributary to B-;s%ry 'r 0fr; Describe the industrial aelivities that occur within the outfall drainage area: 6% p�►�-lm+_ Page I of 2 Pace Analytical services,LLC 9800 Kinoey Ave. Suite 100 aceHuntersville,NC 28078 (704)875-9092 August 09, 2024 Chris Hay EnviroTrac 7343 W. Friendly Avenue Suite J Greensboro, NC 27410 RE: Project: OminSource Winston-Salem Pace Project No.: 92744250 Dear Chris Hay: Enclosed are the analytical results for sample(s)received by the laboratory on July 26,2024. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual,where applicable,unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: •Pace National-Mt.Juliet •Pace Analytical Services-Asheville If you have any questions concerning this report,please feel free to contact me. Sincerely, Zachary J Tierney zachary.tierney@parelabs.com (386)672-5668 Project Manager Enclosures cc: Annamarie Blauser,EnviroTrac Ltd Gail Hay,EnviroTrac,Ltd. Elizabeth Taccone,Envirotrac-NC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical services,LLC. Page 1 of 17 B Pace Analytical Services,LLC 9800 Kincey Ave. Suite 100 ��� Hunlersville,NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: OminSource Winston-Salem Pace Project No.: 92744250 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 927442500011 OUTFALL-1 EPA 200.7 Rev 4.41994 DBB1 3 PASI-A EPA1664B DAL 2 PAN SM 254OD-2015 AGM 1 PASI-A SM 522OD-2011 JP1 1 PASI-A 92744250002 OUTFALL-2 EPA 200.7 Rev 4.41994 DBB1 3 PASI-A EPA 1664E DAL 2 PAN SM 254OD-2015 AGM 1 PASI-A SM 5220D-2011 JP1 1 PASI-A 92744250003 OUTFALL-5 EPA 200.7 Rev 4.41994 DBB1 3 PASI-A EPA 1664E DAL 2 PAN SM 2540D-2015 AGM 1 PASI-A SM 5220D-2011 JP1 1 PASI-A PAN=Pace National-Mt.Juliet PASI-A=Pace Analytical Services-Asheville REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 3 of 17 Pace Analytical Services,LLC 9800 Kincey Ave. Suite 100 ���- Huntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OminSource Winston-Salem Pace Project No.: 92744250 Sample: OUTFALL-2 Lab ID: 92744260002 Collected: 07/25/24 13:58 Received: 07/26/24 12:30 Matrix:Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method:EPA 200.7 Rev 4.41994 Preparation Method:EPA 200.7 Rev 4.41994 Pace AnalytcaI Services-Asheville Copper 1030 ug/L 5.0 1 07/27/24 16:32 07/30/24 17:32 7440-50-8 Lead 444 ug/L 5.0 1 07/27/24 16:32 07/30/24 17:32 7439-92-1 Zinc 1040 ug/L 10.0 1 07/27/24 16:32 07/30/24 17:32 7440£6-6 Wet Chemistry 1664D Analytical Method:EPA 1664B Preparation Method:1664E Pace National-Mt.Juliet Oil and Grease NO ug/L 5000 1 08/08/24 17:04 08/08/24 22:55 Total Petroleum Hydrocarbons ND ug/L 5000 1 08/08/24 17:04 08/09/24 00:11 2640D Total Suspended Solids Analytical Method:SM 254OD-2015 Pace Analytical Services-Asheville Total Suspended Solids 109 mg/L 35.7 1 07/31/24 19:40 6220D COD Analytical Method:SM 5220D-2011 Preparation Method:SM 5220D-2011 Pace Analytical Services-Asheville Chemical Oxygen Demand 176 mg/L 25.0 1 08/02/24 02:23 08/02/24 05:31 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Dale:08/09/2024 11:20 AM without the written consent of Pace Analytical Services,LLC. Page 5 of 17 Pace Analytical Services,LLC _ 9800 KinceyAve. Suite 100 ��� Huntersvllle,NC 28076 (704)875-9092 QUALITY CONTROL DATA Project: OminSource Winston-Salem Pace Project No.: 92744250 QC Balch: 871515 Analysis Method: EPA 200.7 Rev 4.41994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92744250001,92744260002 METHOD BLANK: 4490827 Matrix: Water Associated Lab Samples: 92744250001,92744250002 - Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper ug/L ND 5.0 07/30/2415:58 Lead ug/L NO 5.0 07/30/2415:58 Zinc ug/L NO 10.0 07/30/2415:58 LABORATORY CONTROL SAMPLE: 4490828 Spike LCS LCS %Rec Parameter Units Cone. Result %Rec Limits Qualifiers Copper ug/L 500 494 99 85-115 Lead ug/L 500 507 101 85-115 Zinc ug/L 500 603 101 85-115 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4490831 4490832 MS MSD 92743383002 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Cone. Cone. Result Result %Rec %Rec Limits RPD Qual Copper ug/L ND 500 500 516 511 103 102 70-130 1 Lead ug1L NO 500 500 499 500 100 100 70-130 0 Zinc ug/L 33.6 500 500 540 540 101 101 70-130 0 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4490833 4490834 MS MSD 92743887003 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Cone. Cone. Result Result %Rec %Rec Limits RPD Qual Copper ug/L ND 500 500 495 508 99 102 70-130 3 Lead ug/L ND 500 500 484 499 97 100 70-130 3 Zinc ug/L ND 500 500 487 499 97 99 70-130 2 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Dale:08/09/2024 11:20 AM without the written consent of Pace Analytical Servkes,LLC. Page 7 of 17 Pace Analytical Services,LLC 9800 Kincey Ave. Suite 100 ��� Huntersville,NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OminSource Winston-Salem Pace Project No.: 92744250 QC Balch: 2339244 Analysis Method: EPA 1664E QC Batch Method: 1664A Analysis Description: Wet Chemistry 1664E Laboratory: Pace National-Mt.Juliet Associated Lab Samples: 92744250001,92744250002,92744250003 METHOD BLANK: R4104618-1 Matrix: Water Associated Lab Samples: 92744250001,92744250002,92744250003 - Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease ug/L ND 5000 08108124 22:55 LABORATORY CONTROL SAMPLE&LCSD: R4104618-2 R4104618-3 Spike LCS LCSD LCS LCSD %Rec Max Parameter Units Cone. Result Result %Rec %Rec Limits RPD RPD Qualifiers Oil and Grease ug/L 40000 36400 40200 91.0 101 78.0-114 9.92 20 MATRIX SPIKE SAMPLE: R4104618-4 L1762821-01 Spike MS MS %Rec Parameter Units Result Cone. Result %Rec Limits Qualifiers Oil and Grease ug/L 8890 40000 25300 41.0 78.0-114 MIL Results presented on this page are in the units indicated by the'Units"column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except In full, Date:08/09/2024 11:20 AM without the when consent of Pace Analytical Services,LLC. Page 9 of 17 Pace Analytical services,LLC 9800 Kincey Ave. Suite 100 ��� Hunlersville,NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OmmSource Winston-Salem Pace Project No.: 92744250 QC Batch: 872445 Analysis Method: SM 254OD-2015 QC Batch Method: SM 254OD-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92744250001,92744250002,92744259003 METHOD BLANK: 4494812 Matrix: Water Associated Lab Samples: 92744250001,92744250002,92744250003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L NO 2.5 07/31/24 19:36 LABORATORY CONTROL SAMPLE: 4494813 Spike LCS LCS %Rae Parameter Units Cone. Result %Rec Limits Qualifiers Total Suspended Solids mg/L 250 248 99 90-110 SAMPLE DUPLICATE: 4495118 92744243001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 17600 20700 16 SAMPLE DUPLICATE: 4495119 92744250002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 109 104 4 Results presented on this page are in the units initiated by the"Units•column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/09/2024 11:20 AM without the written consent of Pace Analytical Services,LLC. Page 11 of 17 Pace Analytical services,LLC 9800 Kinsey Ave. Suite 100 ��� Hunlersville,NC 28078 (704)075-9092 QUALIFIERS Project: OminSource Winston-Salem Pace Project No.: 92744250 DEFINITIONS DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot. NO-Not Detected at or above adjusted reporting limit. TNTC-Too Numerous To Count ' J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL-Practical Quantitation Limit. RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S-Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is a combined concentration. Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values. LCS(D)-Laboratory Control Sample(Duplicate) MS(D)-Matrix Spike(Duplicate) DUP-Sample Duplicate RPD-Relative Percent Difference NC-Not Calculable. SG-Silica Gel-Clean-Up U-Indicates the compound was analyzed for,but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded unfit the final step prior to reporting.Therefore,calculated parameters that are typically reported as "Total"may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes. TNI-The NELAC Institute. SAMPLE QUALIFIERS Sample:92744250001 Ill Wet Chemistry by Method 1664B-Total Oil&Grease Is non-detect.Extract was not processed through silica gel. Sample:92744250002 Ill Wet Chemistry by Method 1664E-Total Oil&Grease is non-detect.Extract was not processed through silica gel. Sample:92744250003 Ill Wet Chemistry by Method 1664E-Total OII&Grease is non-detect.Extract was not processed through silica gel. ANALYTE QUALIFIERS Mt Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample(LCS)recovery. ML Matrix spike recovery and/or matrix spike duplicate recovery was below laboratory control limits.Result may be biased low. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08109/202411:20 AM without the written consent of Pace Analytical Services,LLC. Page 13 of 17 ace DC#_Title: ENV-FRM-HUN1-0083 v05 Sample Condition Upon Receipt Effective Date:05/24/2024 Laboratory receiving samples: Asheville❑ Eden❑ Greenwood❑ Huntersville Raleigh[] Mechanicssviille❑ AtlannAtlanta[] Kernersvillen Win 1011144� Client Name: Project#: WO# a 92744250 Courier. ❑Fe�Ex ❑UPS ❑LISPS []Client ❑Commercial ©PSce ❑Other: 92744250 Custody Seal Present? ❑Yes ZNo Seals Intact? ❑Yes ❑No AN/A — Dale/initials Person Examining Contents: — a c Ing a er a: Mere—Wrap LIBubble Bags LJNone LJ Other 8iologiwl Tissur.�Frozen?cn- � Thermometer: ❑Yes ❑No y iN/A ❑IR Gun ID: %LQP Type of ice: ❑Wet ❑Blue ❑None Correction Factor: Cooler Temp: _�_ Add/Subtract('C) © Temp should be above freezing to 6'C Cooler Temp Corrected('C): Ol a9 has begun Osamples out of temp a teria.Samples on Ice,cooling process USDA Regulated Soll(❑N/A,water sample) Did samples originate In a quarantine zone within the United States:CA,NY,or SC Didsamples Originate from a foreign source(internationally, check maps)?❑Yes ❑No including Hawaii and Puerto Rica)?❑Yes ONO _ Comments/Discrepancy: Chain of Custody Present? ❑No ❑N/A 1. Samples Arrived within Hold Time? s ❑No ❑N/A 2. Short Hold Time Analysis(c72 hr.)? []Yes E!�No ❑N/A 3. Rush Turn Around Time Requested? ❑Yes ❑NA 4. Sufficient Volume? l,.n,w� r-�❑No ❑N/A S. Correct Containers Used? U!*as ONO ❑N/A 6. -Pace Containers Used? (yr€s ONO ❑N/A Containers Intact? es ONO ❑N/A 7. Dissolved analysis:Samples Field Filtered? es ❑No ❑N/A 8. Sample Labels Match COC? QY�No ❑N/A 9. -Includes Date/Time/ID/Analysis Matrix: 1 Headspace in VOA Vials(>5.6mm)? ❑Yes ONO UfWA 10. Trip Blank Present? Oyes ONO Trip Blank Custody Seals Present? Oyes ONO Ylrl/n COMMENTS/SAMPLE DISCREPANCY Field Data Required? Oyes ONO _ Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Date/Time: Project Manager SCURF Review: Date: Project Manager SRF Review: Date: Qualtrax ID:69614 Page 1 of 2 Page 15 of 17 a S \a \' Cb _ n P o �ryffyy N '^ E y ^ i Z ➢ � O f F o a s o i 6'i _ a z ^ n n 3 3 O ay �9 99 g � U1 a n N < ^O Z OE 30 71 i g a ^ s 55gg`` 1669 SGT-HEM.TPH ' 200.7 MET ICP '_— t O^ 25400 Total Suspended Solids •.a� c z \ 5220DCOD o^ a !. 6 < P ^ C N In p z � ~It 0 3 C a o 0 is o ly7 'n. 2 a m 0Go m p _ 8 tab Use On o 6 _ i p^p 3 ��a co a'., � i'.i 4gP� �8`;-• � IN �• C 3s 0 lDd 3 ; ] lFg �3Fy _ ✓ 3 Peetervlibnwn<onlwmtMe Nen4(wd lof a U„�R, Page 17 of 17 T w Y Q� r v O ��w-lJ N Q Q \ 0➢ a- N � 7 U C U O YC C] R1 !.7 (� Z VI C E M N N N l0 `1 — W w C fp O_1:1 N f t0 0 0 'v o . - O N a E w C p�❑ > ti C p O' vi w Q1 Q) a. w T W O w w U d C C w E w V) 2 I- -o j a W E way > U.- i ...: O ,U tJ ❑ N L 0 m m m a m w m N O a w E O z a y o E N o C p .� J f In O O a O Y t Vl N m cr❑❑ O N O O Y w Z j u El = m m o`er o. � > v vX o Y QI J O (") N N fp VI ❑Q w m w a �0 £ a co 'r E L 3 o w Q N VI t O H o 0 0 0 0 o in a 0 Z 3 M L G W C O y�j N a p p Y Q _y; tv J ~ } m o o n Z � g z v � hOE � w O_ O C7 C I •L p Z O u � W t( O N O YV Cm «f0 v aN ,c YE E14 O m F p y v O N O J J Q O ,= O cac C sC U m Q v N 'O O -6 Y w 4- W t L w N C w yLi oj O V N tQ/1 CI Z C V w w w 3 C o w G m> > c u Y m o L Z N X 9 \ O 3 Y w O (0 O c �n '� co U E +� Y O .. (,) N y W O y CA 'a p N o O pad cM p h 7 c > C O O N O E w w t p w QJ a w w is " 3 Y w n « O N 3 w J aL+ — t4 0 H Qxj E m C D E E M �' a r f0 N - Q' G rn " M •'' c O w w LL to C •c Li! 12` o C F v w to w Y u N a.. f0 7I m it w O C M CI m `9 � � ` c z � n � � � � � , @ `-' 3 o aki o v T v 5 v d v c w w n 3 w o 'Y c U N c `m c @ r op -a F m E : •w N O Z ¢ o fY`a N aEi u m v c Q ti z O z w c E w w v w v y W L Z 'o J U U a d \ N N N O c N m O E m `0 l7 m QCl vl v o o a o Q`0i 'L-' E a% d c m ti w m vai - u m m uo E oro o 0 0 �' 3 0 .wJ m N w c o �n c N L I l7 c w p �. a •.- s_ " a r O E Z < E m 0° O :° EL � 3 a o LLU L G m QI 3 A C 3 tYa w O w 7 W d E U NO >> G O •NU 2 ' E YE cE u Q o o o z o Z � OO No N w E '• E +° Qci 3 w u p - `° LL F- Z = w Q u O O o 0 " m l7 E a .Y p J_ Z Q E Y O C N w U w E N N O O L w O +w+ E i•+ E W Q O w 0 (L 47 n m a O O w O N U LL CUD O. Z C KC. Envtronmentol Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidmtce onfrlfing out thisform,please visit Mips://deq.tic.gov/abouUdivisioiis/energy-mineral-land-resources/ npdes-storniwater-gps Permit No.: N_/C/ / ! l l 1 / / or Certificate of Coverage No.: NICIGI facility Name: OminSource SE Winston-Salem Facility County: Forsyth Phone No. (336) 461-144o Jared Spillman Inspector: sn.wvnc."t_ 6-��r Date of Inspection: l ram{ f 12—ti Time of Inspection: Total Event Precipitation(inches): 4.1 q All permits require qualitative monitoring to be performed during a"measurable storm event." A"measurable storm even(' is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period,and the permittee obtains approval from the local DEMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: It,�n " (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. I Structure(pipe,ditch,etc.): pa— Receiving Stream: Tributary to Sushy Fork Describe the industrial activities that occur within the outfall drainage area: p3¢11i n ��rwnT2 AA Paget oft Swlr-242,Last modified 00)112018 Kra Enrlronmentat Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report %orguidance oufilling out lhisform,please nish littps://deq.iie.gov/abouttdivisioiis/eiiergy-mineral-Iattd-resources/ npdes-stonuwnter-gps Pennit No.: N_/C! / / / / / / / or Certificate of Coverage No.: N/C!G! Facility Name: OminSource SE VVinston-Salem Facility County: Forsyth Phone No. (336) 461-1440 Jared Spiliman Inspector: A,—,,o,wy4t-z &_ &o w Date of Inspection: Time of Inspection: Total Event Precipitation(inches): All permits require qualitative monitoring to be performed during a"measurable storm event." A"measurable storm event" is a storm event that results in an actual discharge front the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period,and the permittee obtains approval from the local DEMLR Regional Office. By this signature, er , I ceti�rfy that this report is accurate and complete to the best of my knowledge: 2s�! � (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. 2 Structure(pipe,ditch,etc.): Pi pe- Receiving Stream: Tributary to Bushy Fork � Describe the industrial activities that occur within the outfall drainage area: lbAk%^A bt� Page I of 2 swu-ztz,r:"t���uuncur.ntrzats KC Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report rorguirinnce onftlling out thisfonn,please visit https://deq.itc.gov/abotit/divisions/energy-mineral-land-resources/ npdes-stornwater-gps Permit No.: N_/C/ ! / / ! / ! ! or Certificate of Coverage No.: N/C/G/ Facility Name: OminSource SE Winston-Salem Facility County: Forsyth Phone No. (336) 461-1440 Jared Spillman Inspector: A-,mVxa or+4L SjALtb8X Date of Inspection: $ ( $ / V/ Time of Inspection: 1H'D*7 , Total Event Precipitation(inches): Ll•-1 y N a �C oW All permits require qualitative monitoring to be performed during a"measurable storm event." A"measurable storm event" is a storm event that results in an actnal discharge front the permitted site outfall. The previous measurable storm event nest have been at least 72 hours prior. The 72-hour storm interval does not apply if the pennittee is able to doctmtent that a shorter interval is representative for local stonn events during the sampling period,and the permittee obtains approval from the local DEMLR Regional Office. _--- By this signature, 1 certify that this report is accurate and complete to the best of my knowledge: (Signature of Pennittee or Designee) I. Outfall Description: Outfall No. q _ Structure(pipe,ditch,etc.): Receiving Stream: Tributary to Bushy Fork Describe the industrial activities that occur within the outfall drainage area: nta:E4i&e �-QAEQJ Page I of 2 suvu•2a2,r,,,tmaam ltK.or2nts KC. Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form,please WWI hops://deq.tic.gov/abonUdivisioiis/energy-mineral-laud-resources/ npdes-slonnwater-gps Pennit No.: N_IC/ 1 / ! / / / / or Certificate of Coverage No.: N/C/G/ Facility Name: OnlillSOUrce SE Winston-Salem Facility Counly: Forsyth Phone No. (336) 461-1440 Jared Spillman Inspector: �, vnw w.n ti TSLe, �•� Date of Inspection: $ ( St l 2f1 Time of Inspection: ll-i 1 Total Event Precipitation(inches): 4 14 All permits require qualitative monitoring to be performed during a"measurable storm event." A"measurable storm event' is a storni event that results in all actual discharge from the permitted site oulfnll. The previous measurable storm event most have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period,and the permittee obtains approval from the local DEMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permid-ce or Designee) 1. Outfall Description: Outfall No. r'J Structure (pipe,ditch,etc.): Q'I pe Receiving Stream: Tributary to Busny Fork Describe the industrial activities that occur within the outfall drainage area: 6 pc�_y i Page I of 2 Skcu.242.Lmt miwfnd 06'aldat8 Pace Analytical Services,LLC 9800 KlnceyAve. SuRe 100 ��� Huntersville,NC 28078 (704)875-9092 August 23, 2024 Chris Hay EnviroTrac 7343 W. Friendly Avenue Suite J Greensboro, NC 27410 RE: Project: OminSource Winston-Salem Pace Project No.: 92746856 Dear Chris Hay: Enclosed are the analytical results for sample(s)received by the laboratory on August 09,2024. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual,where applicable,unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: •Pace National-Mt.Juliet •Pace Analytical Services-Asheville If you have any questions concerning this report,please feel free to contact me. Sincerely, Zachary J Tierney zachary.lierney@pacelabs.com (386)672-5668 Project Manager Enclosures cc: Annamarie Blauser,EnviroTrac Ltd Gail Hay,EnviroTrac,Ltd. Elizabeth Taccone,Envirotrac-NC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, 6 wKinwt the written consent of Pace Analytical Services,LLC. Page 1 of 16 Pace Analytical Services,LLC 9800 KinceyAve. Suite 100 ��� Hunlersviile,NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: OminSource Winston-Salem Pace Project No.: 92746856 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92746856001 OUTFALL-1 EPA 200.7 Rev 4.41994 CRW 3 PASI-A EPA 1664E DAL 2 PAN SM 254OD-2016 AGM 1 PASI-A SM 5220D-2011 JPt 1 PASI-A 92746B56002 OUTFALL-2 EPA 200.7 Rev 4.41994 CRW 3 PASI-A EPA1664B DAL 2 PAN SM 254OD-2015 AGM 1 PASI-A SM 5220D-2011 JP1 1 PASI-A 92746856003 OUTFALL-3 EPA 200.7 Rev 4.41994 CRW 3 PASI-A EPA 1664B DAL 2 PAN SM 254OD-2015 AGM 1 PASI-A - SM 5220D-2011 JP1 1 PASI-A PAN=Pace National-Mt.Juliet PASI-A=Pace Analytical Services-Asheville REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 3 of 16 Pace Analytical Services,LLC ��� 9800 uncey Ave. Suite IDO Hunlersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Om]nSource Winston-Salem Pace Project No.: 92746856 Sample: OUTFALL-2 Lab ID: 92746866002 Collected: 08/08/24 16:00 Received: 08/09/24 12:35 Matrix:Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua] 200.7 MET ICP Analytical Method:EPA 200.7 Rev 4.4 1994 Preparation Method:EPA 200.7 Rev 4.4 1994 Pace Analytical Services-Asheville Copper 163 uglL 5.0 1 08/14/2415:44 0811512415:10 7440-50-8 Lead 39.7 ug/L 5.0 1 08/1412415:44 08/1W416:10 7439-92-1 Zinc 212 ug/L 10.0 1 08/14/2415:44 08/lM415:10 7440-66-6 Wet Chemistry'1664B Analytical Method:EPA 1664B Preparation Method:1664E Pace National-Mt.Juliet Oil and Grease NO mg/L 5.00 1 08/21/24 16:16 08/21/24 22:14 Total Petroleum Hydrocarbons NO mg/L 5.00 1 08/21/24 16:16 08122/2412:00 2540D Total Suspended Solids Analytical Method:SM 254OD-2015 Pace Analytical Services-Asheville Total Suspended Solids 18.0 mg/L 3.3 1 08/13/24 13:16 5220D COD Analytical Method:SM 5220D-2011 Preparation Method:SM 5220D-2011 Pace Analytical Services-Ashev]lle Chemical Oxygen Demand 33.5 mg/L 25.0 1 08/14/24 01:24 08/14/24 04:19 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except In full, Date:081231202410:42 AM without the written consent of Pace Analytical Services,LLC. Page 5of 16 Pace Analytical Services,LLC 9800KlnyAve. Suite 100 Huntersville,NC 28078ace (704)875-9092 QUALITY CONTROL DATA Project: OminSource Winston-Salem _ Pace Project No.: 92746856 QC Batch: 875611 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.41994 Analysis Description: 200.7 MET Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92746856001,92746856002,92746856003 METHOD BLANK: 4510269 Matrix: Water Associated Lab Samples: 92746856001,92746856002,92746856003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper ug/L NO 5.0 08/15124 14:30 Lead ug/L NO 5.0 08/15/24 14:30 Zinc ug/L NO 10.0 08/15/2414:30 LABORATORY CONTROL SAMPLE: 4510270 Spike LCS LCS %Rec - Parameter Units Cone. Result %Rec Limits Qualifiers Copper ug/L 500 510 102 85-115 Lead ug/L 500 508 102 85-115 Zinc ug/L 500 520 104 85-115 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4510271 4510272 MS MSD 92746850004 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Cone. Cone. Result Result %Rec %Rec Limits RPD Qual Copper ug/L 427 500 500 973 976 109 110 70-130 0 Lead ug/L 417 500 500 939 945 104 106 70-130 1 Zinc ug/L 3060 500 500 3620 3630 111 114 70-130 0 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4510273 4510274 MS MSD 92746850005 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Cone. Cone. Result Result %Rec %Rec Limits RPD Qual Copper ug/L 102 500 500 627 621 105 104 70-130 1 . Lead ug/L 772 500 500 600 593 105 103 70-130 1 Zinc ug/L 384 500 500 903 902 104 104 70-130 0 Results presentee on this page are in the units Indicated by the"Units-column except where an alternate unit is presented to the fight of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Dale:08/23/2024 10:42 AM without the written consent of Pace Analytical Services,LLC. Page 7 of 16 Pace Analytical services,LLC ace 9800 uncey Ave. C28078 uite 100 Huntersville,NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OminSource Winston-Salem _ Pace Project No.: 92746856 QC Batch: 2348042 Analysis Method: EPA 1664E QC Batch Method: 1664A Analysts Description: Wet Chemistry 1664B Laboratory: Pace National-Mt.Juliet Associated Lab Samples: 92746856001,92746856002,92746856003 METHOD BLANK: R411 0 5 7 9-1 Matrix: Water Associated Lab Samples: 92746856001,92746856002,92746856003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L NO 5.00 08/22/24 12:00 LABORATORY CONTROL SAMPLE&LCSD: R4110579-2 R4110579-3 Spike LCS LCSD LCS LCSD %Rec Max Parameter Units Conc. Result Result %Rec %Rec Limits RPD RPD Qualifiers Total Petroleum Hydrocarbons mg/L 20.0 14.2 14.3 71.0 71.5 64.0-132 0.702 34 MATRIX SPIKE SAMPLE: R4110579-4 L1767918-02 Spike MS MS %Rec Parameter Units Result Conc. Result %Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 40.0 24.5 61.2 64.0-132 ML Results presented on this page are in the units indicated by the"Units"colurm except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/23/2024 10:42 AM vrithout the wrglen consent of Pace Analytical Services,LLC. Page 9 of 16 Pace Analytical Services,LLC ^/� 9800Kincey Ave. Suile100 / P Hunlersville,NC 28078 1.1 V�,/ (704)875-9092 QUALITY CONTROL DATA Project: OminSource Winston-Salem Pace Project No.: 92746856 QC Batch: 875416 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92746856001,92746856002,92746856003 METHOD BLANK: 4509501 Matrix: Water Associated Lab Samples: 92746856001,92746856002,92746856003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 08/14/24 04:13 LABORATORY CONTROL SAMPLE: 4509502 Spike LCS LCS %Rec Parameter Units Conic. Result %Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 779 104 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4509503 4509504 MS MSD 92746691001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Chemical Oxygen Demand mg/L ND 100 100 127 114 124 110 90-110 11 M1,R1 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4509505 4509506 MS MSD 92746850004 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Chemical Oxygen Demand mg/L 118 100 100 226 226 108 108 90-110 0 Results presented on this page are In the units Indicated by the"Units"column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/23/2024 10:42 AM without the when consent of Pace Analytical Services,LLC. Page 11 of 16 Pace Analytical Services,LLC ���,. 9800 unceyAve. Su28078 Huntersville,NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: OminSource Winston-Salem - Pace Project No.: 92746856 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92746866001 OUTFALL-1 EPA 200.7 Rev 4.41994 875611 EPA 200.7 Rev 4.41994 875733 92746856002 OUTFALL-2 EPA 200.7 Rev 4.41994 875611 EPA 200.7 Rev 4.41994 875733 92746866003 OUTFALL-3 EPA 200.7 Rev 4.41994 875611 EPA 200.7 Rev 4.41994 875733 92746856001 OUTFALL-1 1664B 2347715 EPA1664B 2347715 92746866001 OUTFALL-1 1664B 2348042 EPA1664B 2348042 92746856002 OUTFALL-2 1664E 2347715 EPA 1664B 2347715 92746856002 OUTFALL-2 1664B 2348042 EPA1664B 2348042 92746866003 OUTFALL-3 1664B 2347715 EPA1664B 2347715 92746866003 OUTFALL-3 1664B 2348042 EPA1664B 2348042 92746866001 OUTFALL-1 SM 2540D-2015 874968 92746856002 OUTFALL-2 SM 254OD-2015 874968 - 92746866003 OUTFALL-3 SM 254OD-2015 874968 92746856001 OUTFALL-1 SM 522OD-2011 875416 SM 5220D-2011 875448 92746866002 OUTFALL-2 SM 5220D-2011 875416 SM 5220D-2011 875448 92746856003 OUTFALL-3 SM 5220D-2011 875416 SM 5220D-2011 875448 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except In full, Date:08/231202410:42 AM without the written consent of Pace Analytical Services,LLC. Page 13 of 16 lFace DC#_Title: ENV-FRM-HUN1-0083 v05_Sample Condition Upon Receipt _ L Effective Date:05/24/2024 'Checkmarktop belief box ifpH and/or dechlorination is verified andwithin the projeetN �0aa 92746856 acceptance range for preservation samples. Excepdonz:VOA,GoEform,TOC,Oil and Grease,ORO/8035(water)OOC,lII{g pM: 2JT Oue Date: 08/20/24 "Bottom half of box Is to list number of bottles CLIENT:ENT: 92-Env i rcTra "'Check all unpreserved Nitrates for chlorine J Laboratory Recelvingtocation:Asheville E] Eden❑ Greenwood[] Huntersville E] Raleigh[] MechannavwcL, ..vd,udV AWJ x,dv„<u i Client �r`U cf fJ`ficw" M,; Profile ?(Eircicone) r!t-i_1.U"1Notes it z z Y i z o n 3 R n B b z c ct a _ O _ u > > > a o o i c 6 !J i U O n & E E E E E E _ E — E E E E E G cc I 3 4 5 6 7 8 9 10 11 12 pH Adjustment log for Preserved Samples adjusted added Note: Whenever there is a discrepancy affecting North Carolina compliance samples,a copy of this form will be sent to the North Carolina OENR Certification Office(i.e. Out of hold,incorrect preservative,out of temp,incorrect containers. Qualtrax ID: 69614 Page 2 of 2 Page 15 of 16