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Home My WebLink AboutNC0025305_Historical information_20080201Chapel Hill, NC 27510 Report Summary Thursday February 07, 2008 Description: Cogen Steamline Drain >pliei 1. sentativeWTBeasley, ESC Rep,r. ND Larry Daw University of North Carolina-Chapel Hill 212 Finley Golf Course Road Environmental Science Corp. A2LA GA - NJ - AZ - by you, the client, < questions regarding this data package, please do E87487 - R-140 Entire Report Reviewed By: Laboratory Certification Numbers AL - 90010, 2006, NY IN - SC MN 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 This report may not be reproduced, except in full, without written approval from Environmental Science Corp. 2 Samples Reported: 02/07/08 13:28 Printed: 02/07/08 16:09 Page 1 of 13 Report Number: L330131 Samples Received: 02/02/08 Client Project: Tax I.D. 62-0814289 CT - PH-0197, FL ENV375,DW21704, 1 Est. 1970 Jinformattion S’ 3/5 AhDU rave a. ni6$ita/e to / - 1461-01, AIHA - 09227, 923, IN - C-TN-01, KY - TN002, SC - 84004, TN - 0612, MN - 047-999-395, . - 1-2327, 0016, NC - 00109, WV - 233 WI - 998093910 40660, CA KYUST - < VA - 11742, The analytical results in this report are based upo: , and are for your exclusive use/ ' > no- REPORT OF ANALYSIS February 07,2008 ESC Sample # :L330131-01 Site ID Sample ID DRAIN 1 Project # : Parameter Result Det. Limit Units Method Dil.Date BDL Page 2 of 13 1 1 1 Environmental Science Corp. 625 Base/Neutrals w/ TIC Acenaphthene Acenaphthylene Anthracene % Rec. % Rec. % Rec. mg/1 mg/1 mg/1 Volatile Organics Benzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane 2-Chloroethyl vinyl ether Chloroform Chloromethane 1.2- Dichlorobenzene 1.3- Dichlorobenzene 1.4- Dichlorobenzene Dichlorodifluoromethane 1.1- Dichloroethane 1,2 -Dichloroethane 1.1- Dichloroethene trans-1,2-Dichloroethene 1.2- Dichloropropane cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Methylene Chloride Methyl tert-butyl ether Naphthalene 1.1.2.2- Tetrachloroethane Tetrachloroethene Toluene 1.1.1- Trichloroethane 1.1.2- Trichloroethane Trichloroethene Trichlorofluoromethane Vinyl chloride Surrogate Recovery Toluene-d8 Dibromofluoromethane 4-Bromofluorobenzene Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Date Received Description BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 99.9 101. 96.2 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0050 0.0010 0.0010 0.0010 0.0050 0.050 0.0050 0.0025 0.0010 0.0010 0.0010 0.0050 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0050 0.0050 0.0050 0.0010 0.0010 0.0050 0.0010 0.0010 0.0010 0.0050 0.0010 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 625 625 625 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/06/08 02/06/08 02/06/08 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 J L Daw 02/01/08 09:50 Larry Daw University of North Carolina-Chapel 212 Finley Golf Course Road Chapel Hill, NC 27510 Collected By : Collection Date : 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 February 02, 2008 Cogen Steamline Drain Tax I.D. 62-0814289 ESt. 1970 REPORT OF ANALYSIS ESC Sample # :L330131-01 Site ID Sample ID DRAIN 1 Project # : Parameter Result Units Method Dil.Date BDL Page 3 of 13 Environmental Science Corp. i i i i Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) mg/1 mg/1 mg/1 mg/1 Date Received Description Benzidine Benzo(a)anthracene Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(g,h,i)perylene Benzo(a)pyrene Bis(2-chlorethoxy)methane Bis(2-chloroethyl)ether Bis(2-chloroisopropyl)ether 4-Bromophenyl-phenylether 2-Chloronaphthalene 4-Chlorophenyl-phenylether Chrysene Dibenz(a,h)anthracene 3.3- Dichlorobenzidine 2.4- Dinitrotoluene 2,6-Dinitrotoluene Fluoranthene Fluorene Hexachlorobenzene Hexachloro-1,3-butadiene Hexachlorocyclopentadiene Hexachloroethane Indenofl,2,3-cd)pyrene Isophorone Naphthalene Nitrobenzene n-Nitrosodimethylamine n-Nitrosodiphenylamine n-Nitrosodi-n-propylamine Phenanthrene Benzylbutyl phthalate Bis(2-ethylhexyl)phthalate Di-n-butyl phthalate Diethyl phthalate Dimethyl phthalate Di-n-octyl phthalate Pyrene 1.2.4- Trichlorobenzene Acid Extractables 4-Chloro-3-methylphenol 2-Ch1oropheno1 2.4- Dichlorophenol 2.4- Dimethylphenol BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.050 0.0010 0.0010 0.0010 0.0010 0.0010 0.010 0.010 0.010 0.010 0.010 0.010 0.0010 0.0010 0.010 0.010 0.010 0.0010 0.0010 0.010 0.010 0.010 0.010 0.0010 0.010 0.0010 0.010 0.050 0.010 0.010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.010 0.010 0.010 0.010 0.010 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 J L Daw 02/01/08 09:50 Larry Daw University of North Carolina-Chapel 212 Finley Golf Course Road Chapel Hill, NC 27510 Collected By : Collection Date : 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 February 02, 2008 Cogen Steamline Drain Tax I.D. 62-0814289 Est. 1970 Det. Limit February 07, 2008 REPORT OF ANALYSIS February 07, 2008 ESC Sample # :L330131-01 Site ID Sample ID DRAIN 1 Project # : Parameter Result Det. Limit Units Method Dil.Date Reported: 02/07/08 13:28 Printed: 02/07/08 16:09 Page 4 of 13 Environmental Science Corp. Date Received Description 4.6- Dinitro-2-methylphenol 2,4-Dinitrophenol 2-Nitrophenol 4-Nitrophenol Pentachlorophenol Phenol 2.4.6- Trichlorophenol Surrogate Recovery Nitrobenzene-d5 2 -Fluorobiphenyl p-Terphenyl-dl4 Phenol-d5 2 -Fluorophenol 2.4.6- Tribromophenol BDL BDL BDL BDL BDL BDL BDL 77.3 74.7 102 . 12.3 25.5 62.3 0.010 0.010 0.010 0.010 0.010 0.010 0.010 % Rec. % Rec. % Rec. % Rec. % Rec. % Rec. mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 625 625 625 625 625 625 625 625 625 625 625 625 625 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 1 1 1 1 1 1 1 1 1 1 1 1 1 J L Daw 02/01/08 09:50 Larry Daw University of North Carolina-Chapel 212 Finley Golf Course Road Chapel Hill, NC 27510 Collected By : Collection Date : 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 February 02, 2008 Cogen Steamline Drain Tax I.D. 62-0814289 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. ESt. 1970 REPORT OF ANALYSIS February 07, 2008 ESC Sample # :L330131-02 Site ID Sample ID TRIP BLANK Project # : Result Det. Limit Units Method Dil.Parameter Date BDL Reported: 02/07/08 13:28 Printed:02/07/08 16:09 Page 5 of 13 1 1 1 Environmental Science Corp. % Rec. % Rec. % Rec. Date Received Description Volatile Organics Benzene Bromod i chiorome thane Bromoform Bromome thane Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane 2-Chloroethyl vinyl ether Chloroform Chloromethane 1.2- Dichlorobenzene 1.3- Dichlorobenzene 1.4- Dichlorobenzene Dichlorodifluoromethane 1.1- Dichloroethane 1.2- Dichloroethane 1.1- Dichloroethene trans-1,2-Dichloroethene 1.2- Dichloropropane cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Methylene Chloride Methyl tert-butyl ether Naphthalene 1.1.2.2- Tetrachloroethane Tetrachloroethene Toluene 1.1.1- Trichloroethane 1.1.2- Trichloroethane Trichloroethene Trichlorofluoromethane Vinyl chloride Surrogate Recovery Toluene-d8 Dibromofluoromethane 4-Bromofluorobenzene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 103 . 107 . 95.2 0.0010 0.0010 0.0010 0.0050 0.0010 0.0010 0.0010 0.0050 0.050 0.0050 0.0025 0.0010 0.0010 0.0010 0.0050 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0050 0.0050 0.0050 0.0010 0.0010 0.0050 0.0010 0.0010 0.0010 0.0050 0.0010 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 624 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 02/04/08 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 J L Daw 02/01/08 00:00 Larry Daw University of North Carolina-Chapel 212 Finley Golf Course Road Chapel Hill, NC 27510 Collected By : Collection Date : Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 February 02, 2008 Cogen Steamline Drain Tax I.D. 62-0814289 ESt. 1970 Sample #Analyte Qualifier L330131-01 Bis(2-ethylhexyl)phthalate J4 Page 6 of 13 Attachment A List of Analytes with QC Qualifiers Qualifier Meaning J4 Qualifier Report Information In addition to the ERA qualifiers adopted TIC Page 7 of 13 Precision - The agreement between a set of samples or between duplicate samples. Relates to how close together the results are and is represented by Relative Percent Differrence. - Tentatively Identified Compound: Compounds detected in samples that are not target compounds, internal standards, system monitoring compounds, or surrogates. The associated batch QC was outside the established quality control range for accuracy. Attachment B Explanation of QC Qualifier Codes Definitions Accuracy - The relationship of the observed value of a known sample to the true value of a known sample. Represented by percent recovery and relevant to samples such as: control samples, matrix spike recoveries, surrogate recoveries, etc. Surrogate - Organic compounds that are similar in chemical composition, extraction, and chromotography to analytes of interest. The surrogates are used to determine the probable response of the group of analytes that are chem ically related to the surrogate compound. Surrogates are added to the sample and carried through all stages of preparation and analyses. ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and as required by most certifying bodies including NELAC. ' by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical results. Each qualifier is designated in the qualifier explanation as either EPA or ESC. Data qualifiers are intended to provide the ESC client with more detailed information concerning the potential bias of reported data. Because of the wide range of constituents and variety of matrices incorporated by most EPA methods,it is common for some compounds to fall outside of established ranges. These exceptions are evaluated and all reported data is valid and useable unless qualified as 1R1 (Rejected). Sample: L330131-01 Account: Sample: L330131-02 Account: Summary of Remarks For Samples Printed 02/07/08 at 16:09:54 TSR Signing Reports: 134 R5 - Desired TAT UNVNCCH Received: 02/02/08 09:00 Due Date: 02/08/08 00:00 RPT Date: 02/07/08 13:28 UNVNCCH Received: 02/02/08 09:00 Due Date: 02/08/08 00:00 RPT Date: 02/07/08 13:28 Chapel Hill, NC 27510 February 07, 2008 L330131 Analyte Result Date Analyzed Batch Page 8 of 13 Environmental Science Corp. Quality Assurance Report Level II 1.2.4- Trichlorobenzene 2.4.6- Trichlorophenol 2.4- Dichlorophenol 2.4- Dimethylphenol 2.4- Dinitrophenol 2.4- Dinitrotoluene 2.6- Dinitrotoluene 2 -Chloronaphthalene 2 -Chlorophenol 2-Nitrophenol 3,3-Dichlorobenzidine 4.6- Dinitro-2-methylphenol 4 -Bromophenyl-phenylether 4-Chloro-3-methylphenol 4-Chlorophenyl-phenylether 4-Nitrophenol Acenaphthene Acenaphthylene Anthracene Benzidine Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo (k)fluoranthene University of North Carolina-Chapel Hill Larry Daw 212 Finley Golf Course Road mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/04/08 01:48 02/06/08 10:27 02/06/08 10:27 02/06/08 10:27 02/06/08 10:27 02/06/08 10:27 02/06/08 10:27 02/06/08 10:27 02/06/08 10:27 02/06/08 10:27 02/06/08 10:27 02/06/08 10:27 02/06/08 10:27 02/06/08 10:27 02/06/08 10:27 02/06/08 10:27 02/06/08 10:27 02/06/08 10:27 02/06/08 10:27 02/06/08 10:27 02/06/08 10:27 02/06/08 10:27 02/06/08 10:27 02/06/08 10:27 02/06/08 10:27 02/06/08 10:27 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 . 01 .01 .01 .01 .01 . 01 . 01 .01 .01 .01 .01 . 01 .01 .01 . 01 . 01 .01 . 01 . 01 . 01 . 01 . 01 . 01 . 01 . 01 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 753-5858 1-800-767-5859 Fax (615) 758-5859 1,1,1-Trichloroethane 1.1.2.2- Tetrachloroethane 1.1.2- Trichloroethane 1.1- Dichloroethane 1.1- Dichloroethene 1.2- Dichlorobenzene 1.2- Dichloroethane 1.2- Dichloropropane 1.3- Dichlorobenzene 1.4- Dichlorobenzene 2-Chloroethyl vinyl ether Benzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,3-Dichloropropene Dichlorodifluoromethane Ethylbenzene Methyl tert-butyl ether Methylene Chloride Naphthalene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride Laboratory Blank Units 1 Est. 1970 Tax I.D. 62-0814289 < . 001 < . 001 < .001 < . 001 < . 001 < . 001 < .001 < . 001 < . 001 < .001 < . 001 < . 001 < .001 < . 001 < . 005 < . 001 < . 001 < . 001 < . 001 . 005 . 001 . 001 . 005 . 001 . 001 . 005 . 005 . 001 . 005 . 001 . 001 . 001 . 005 . 001 62-0814289Tax I.D. Est.1970 Chapel Hill, NC 27510 February 07,2008 L330131 Benzylbutyl phthalate 02/06/08 10:27. 01 WG343273ppm Analyte Result Date Analyzed Batch Analyte Limit% Rec Batch Page 9 of 13 Environmental Science Corp. 10 : 27 10:27 10 : 27 10:27 10 : 27 10 : 27 10:27 10 : 27 10 : 27 10:27 10 : 27 10 : 27 10 : 27 10 : 27 10 : 27 10:27 10 : 27 10 : 27 10 : 27 10 : 27 10 : 27 10:27 10 : 27 10 : 27 10 : 27 10 : 27 10 : 27 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 Quality Assurance Report Level II 0.0523 0.0570 0.0532 0.0510 0.0457 0.0496 0.0509 0.0526 0.0523 0.0471 0.197 0.0505 0.0552 0.0458 0.0552 0.0551 0.0518 0.0512 0.0507 0.0528 0.0471 0.0437 0.0458 0.0494 0.0517 0.0475 0.0485 0.0487 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 02/06/08 105 . 114 . 106 . 102. 91.5 99.1 102. 105 . 105. 94.1 78.9 101. 110 . 91.5 110 . 110 . 104 . 102 . 101. 106 . 94.2 87.4 91.6 98.8 103 . 95.0 97.1 97.3 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm ppm 67-137 72- 128 79-123 67-133 60-130 75- 122 63- 137 74-122 73- 131 70-121 0-171 67- 126 68- 133 60-139 45-175 64- 141 77-125 73-138 49-155 66- 126 45-152 73-131 39-189 76- 129 51-142 64-125 56-145 67- 135 .01 . 01 . 01 .01 . 01 . 01 < .01 < . 01 < .01 < .01 < . 01 < . 01 < .01 < .01 < .01 < .01 < .01 < .01 < . 01 < . 05 < .01 < .01 < .01 < .01 < .01 .01 .01 . 05 . 05 . 05 . 05 . 05 . 05 .05 . 05 . 05 . 05 .25 . 05 . 05 . 05 . 05 . 05 . 05 . 05 . 05 . 05 . 05 . 05 . 05 . 05 . 05 . 05 . 05 .05 Bis(2-chlorethoxy)methane Bis(2-chloroethyl)ether Bis(2-chloroisopropyl)ether Bis(2-ethylhexyl)phthalate Chrysene Di-n-butyl phthalate Di-n-octyl phthalate Dibenz(a,h)anthracene Diethyl phthalate Dimethyl phthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone n-Nitrosodi-n-propylamine n-Nitrosodimethylamine n-Nitrosodiphenylamine Naphthalene Nitrobenzene Pentachlorophenol Phenanthrene Phenol Pyrene University of North Carolina-Chapel Hill Larry Daw 212 Finley Golf Course Road 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Laboratory Blank Units ) 1,1,1-Trichloroethane 1.1.2.2- Tetrachloroethane 1.1.2- Trichloroethane 1.1- Dichloroethane 1.1- Dichloroethene 1.2- Dichlorobenzene 1.2- Dichloroethane 1.2- Dichloropropane 1.3- Dichlorobenzene 1.4- Dichlorobenzene 2-Chloroethyl vinyl ether Benzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,3-Dichloropropene Dichlorodifluoromethane Ethylbenzene Methyl tert-butyl ether Methylene Chloride Naphthalene Tetrachloroethene Laboratory Control Sample Units Known Vai Result Tax I.D.62-0814289 ESt.1970 Chapel Hill, NC 27510 February 07,2008 L330131 Toluene mg/1 .05 0.0498 99.7 72-122 WG343200 Analyte Limit% Rec Batch Page 10 of 13 Environmental Science Corp. Quality Assurance Report Level II trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride Laboratory Control Sample Units Known Vai Result mg/1 mg/1 mg/1 mg/1 mg/1 PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm 0.00688 0.00815 0.00759 0.00992 0.00342 0.0102 0.0109 0.00852 0.00734 0.00729 0.0113 0.00611 0.00922 0.00796 0.00971 0.00389 0.00880 0.00874 0.0109 0.00151 0.0110 0.0114 0.0103 0.0114 0.0108 0.00816 0.00865 0.00715 0.00793 0.0151 0.0107 0.0103 0.0123 0.0111 0.00805 0.00442 0.0107 0.00975 0.00657 0.0108 0.00668 0.00572 0.0109 0.00912 0.00948 0.00426 0.0114 0.00729 0.00713 0.00576 0.0108 0.00338 0.0117 0.0459 0.0463 0.0498 0.0545 0.0481 91.8 92.6 99.6 109. 96.3 67-129 66-137 74-126 54- 156 55- 153 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343200 WG343200 WG343200 WG343200 WG343200 68.8 81.5 75.9 99.2 34.2 102 . 109. 85.2 73.4 72.9 113 . 61.1 92.2 79.6 97.1 38.9 88.0 87.4 109 . 15.1 110. 114 . 103 . 114 . 108 . 81.6 86.5 71.5 79.3 151. 107 . 103 . 123 . 111. 80.5 44.2 107 . 97.5 65.7 108 . 66.8 57.2 109. 91.2 94.8 42.6 114 . 72.9 71.3 57.6 108 . 33.8 117 . 26-103 49-118 46-115 40-124 10-125 56-128 56- 121 44- 110 38- 114 35- 118 46- 145 24-119 45- 105 47- 116 49- 116 10-66 48- 110 48- 113 55-127 0-46 57- 115 63-125 50- 123 39- 143 45- 126 22-154 42-116 26-115 32-115 47- 143 58- 113 51- 131 51-138 39- 144 36- 128 10- 135 53- 119 49- 116 21-116 51-121 4-126 15-109 40- 143 48- 126 47-122 11- 69 59- 143 29-103 31-105 20-122 54- 112 17-52 46- 130 . 05 .05 .05 .05 .05 .01 .01 .01 .01 .01 . 01 .01 . 01 .01 .01 .01 .01 .01 .01 .01 .01 . 01 . 01 .01 .01 .01 .01 .01 .01 .01 .01 . 01 . 01 . 01 .01 . 01 .01 .01 . 01 . 01 . 01 .01 . 01 .01 .01 .01 .01 .01 .01 . 01 .01 . 01 . 01 .01 . 01 .01 .01 . 01 University of North Carolina-Chapel Hill Larry Daw 212 Finley Golf Course Road 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 1.2.4- Trichlorobenzene 2.4.6- Trichlorophenol 2.4- Dichlorophenol 2.4- Dimethylphenol 2.4- Dinitrophenol 2.4- Dinitrotoluene 2.6- Dinitrotoluene 2 -Chloronaphthalene 2 -Chlorophenol 2-Nitrophenol 3,3-Dichlorobenzidine 4.6- Dinitro-2-methylphenol 4 -Bromophenyl-phenylether 4-Chloro-3-methylphenol 4-Chlorophenyl-phenylether 4-Nitrophenol Acenaphthene Acenaphthylene Anthracene Benzidine Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzylbutyl phthalate Bis(2-chlorethoxy)methane Bis(2-chloroethyl)ether Bis(2-chloroisopropyl)ether Bis(2-ethylhexyl)phthalate Chrysene Di-n-butyl phthalate Di-n-octyl phthalate Dibenz(a,h)anthracene Diethyl phthalate Dimethyl phthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indenod, 2,3-cd)pyrene Isophorone n-Nitrosodi-n-propylamine n-Nitrosodimethylamine n-Nitrosodiphenylamine Naphthalene Nitrobenzene Pentachlorophenol Phenanthrene Phenol Pyrene 1 Tax l.D.62-0814289 ESt.1970 Chapel Hill, NC 27510 February 07, 2008 L330131 Analyte Batch of 13Page 11 Environmental Science Corp. 1.2.4- Trichlorobenzene 2.4.6- Trichlorophenol 2.4- Dichlorophenol 2.4- Dimethylphenol 2.4- Dinitrophenol 2.4- Dinitrotoluene 2.6- Dinitrotoluene 2 -Chloronaphthalene 2 -Chlorophenol 2-Nitrophenol 3,3-Dichlorobenzidine 4.6- Dinitro-2-methylphenol 4-Bromophenyl-phenylether 4-Chloro-3-methylphenol 4-Chlorophenyl-phenylether 4-Nitrophenol Acenaphthene Acenaphthylene Anthracene Benzidine Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene University of North Carolina-Chapel Hill Larry Daw 212 Finley Golf Course Road mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 mg/1 Quality Assurance Report Level II PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm Ppm PPm PPm PPm PPm Ppm 0.0512 0.0567 0.0528 0.0498 0.0479 0.0489 0.0505 0.0506 0.0523 0.0466 0.172 0.0497 0.0548 0.0470 0.0558 0.0558 0.0521 0.0507 0.0507 0.0518 0.0472 0.0434 0.0485 0.0492 0.0527 0.0476 0.0492 0.0503 0.0488 0.0471 0.0446 0.0503 0.0537 0.0487 0.0082 0.0089 0.0085 0.0116 0.0040 0.0094 0.0098 0.0095 0.0078 0.0087 0.0097 0.0059 0.0087 0.0082 0.0098 0.0038 0.0096 0.0094 0.0096 0.0014 0.0095 0.0098 0.0106 0.0105 0.0087 0.0523 0.0570 0.0532 0.0510 0.0457 0.0496 0.0509 0.0526 0.0523 0.0471 0.197 0.0505 0.0552 0.0458 0.0552 0.0551 0.0518 0.0512 0.0507 0.0528 0.0471 0.0437 0.0458 0.0494 0.0517 0.0475 0.0485 0.0487 0.0498 0.0459 0.0463 0.0498 0.0545 0.0481 0.0068 0.0081 0.0075 0.0099 0.0034 0.0102 0.0109 0.0085 0.0073 0.0072 0.0113 0.0061 0.0092 0.0079 0.0097 0.0038 0.0088 0.0087 0.0109 0.0015 0.0110 0.0114 0.0103 0.0114 0.0108 1.85 0.165 0.690 5.64 0.532 2.01 0.322 1.24 3.29 2.07 2.51 3.81 1.00 1.53 1.25 82 90 85 116 41 94 99 95 79 87 98 60 87 83 99 39 96 94 96 15 96 98 106 105 88 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343200 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 17.7 9.58 11.8 15.4 17.1 7.76 10.0 11.1 6.97 17.8 14.3 2.49 5.46 3.70 1.84 0.515 9.11 7.59 12.4 3.37 13.8 14.6 3.36 8.11 20.2 38 28 28 36 50 24 23 30 36 35 31 50 26 22 26 37 26 28 24 50 20 22 32 31 37 102 113 106 100 96 98 101 101 105 93 69 99 110 94 112 112 104 101 101 104 94 87 97 98 105 95 98 101 98 94 89 101 107 97 20 20 20 20 20 20 20 20 20 20 27 20 20 20 20 20 20 20 1.95 0.529 0.749 2.38 4.67 1.25 0.849 3.75 0.151 0.966 13.4 1.56 0.737 2.77 1.06 1.35 0.609 1.02 0.0091 20 20 20 20 24 20 20 20 20 20 20 20 20 20 20 20 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 1,1,1-Trichloroethane 1.1.2.2- Tetrachloroethane 1.1.2- Trichloroethane 1.1- Dichloroethane 1.1- Dichloroethene 1.2- Dichlorobenzene 1.2- Dichloroethane 1.2- Dichloropropane 1.3- Dichlorobenzene 1.4- Dichlorobenzene 2-Chloroethyl vinyl ether Benzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,3-Dichloropropene Dichlorodifluoromethane Ethylbenzene Methyl tert-butyl ether Methylene Chloride Naphthalene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride Laboratory Control Sample Duplicate Units LCSD Res Ref Res RPD Limit %Rec Tax I.D.62-0814289 Est.1970 Chapel Hill, NC 27510 February 07, 2008 L330131 Benzylbutyl phthalate 0.0078 0.0081 4.51 29 78 WG343273ppm Analyte Batch Batch number /Run number / Sample number cross reference * * Calculations are performed prior to rounding of reported values of 13Page 12 Environmental Science Corp. Quality Assurance Report Level II WG343200: WG343273: R351416: R351792: L330131-01 02 L330131-01 PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm Ppm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm 0.0097 0.0086 0.0095 0.0128 0.0094 0.0090 0.0111 0.0096 0.0075 0.0043 0.0095 0.0100 0.0079 0.0098 0.0073 0.0068 0.0101 0.0101 0.0096 0.0046 0.0105 0.0087 0.0084 0.0058 0.0097 0.0039 0.0106 0.0086 0.0071 0.0079 0.0151 0.0107 0.0103 0.0123 0.0111 0.0080 0.0044 0.0107 0.0097 0.0065 0.0108 0.0066 0.0057 0.0109 0.0091 0.0094 0.0042 0.0114 0.0072 0.0071 0.0057 0.0108 0.0033 0.0117 38 50 47 24 21 22 22 30 27 33 28 25 50 23 50 50 30 31 33 50 23 45 43 50 22 33 28 97 87 96 128 95 91 111 97 75 44 95 100 79 98 74 68 101 101 97 47 105 88 85 59 98 40 106 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 WG343273 11.6 19.1 18.8 16.8 12.4 12.0 10.3 13.7 7.07 0.909 11.2 2.53 18.6 9.25 9.69 17.4 7.22 10.6 1.88 8.97 8.12 18.3 16.9 2.23 10.0 16.1 9.82 Laboratory Control Sample Duplicate Units LCSD Res Ref Res RPD Limit %Rec University of North Carolina-Chapel Hill Larry Daw 212 Finley Golf Course Road 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Bis(2-chlorethoxy)methane Bis(2-chloroethyl)ether Bis(2-chloroisopropyl)ether Bis(2-ethylhexyl)phthalate Chrysene Di-n-butyl phthalate Di-n-octyl phthalate Dibenz(a,h)anthracene Diethyl phthalate Dimethyl phthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone n-Nitrosodi-n-propylamine n-Nitrosodimethylamine n-Nitrosodiphenylamine Naphthalene Nitrobenzene Pentachlorophenol Phenanthrene Phenol Pyrene Chapel Hill, NC 27510 February 07, 2008 L330131 of 13Page 13 Environmental Science Corp. University of North Carolina-Chapel Hill Larry Daw 212 Finley Golf Course Road Quality Assurance Report Level II 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Matrix Spike and Matrix Spike Duplicate - is two aliquots of an environmental sample that is spiked with known concentrations of target analytes. The percent recovery of the target analytes also has statistical control limits. If any recoveries that are outside the method control limits, the sample that was selected for matrix spike/matrix spike duplicate analysis is flagged with either a "J5" or a "J6". The relative percent difference (%RPD) between the matrix spike and the matrix spike duplicate recoveries is all calculated. If the RPD is above the method limit, the effected samples are flagged with a "J3" qualifier. Laboratory Control Sample - is a sample of known concentration that is carried through the digestion/extraction and analysis process. The percent recovery, expressed as a percentage of the theoretical concentration, has statistical control limits indicating that the analytic process is "in control". If a target analyte is outside the control limits for the laboratory control sample or any other control sample, the parameter is flagged with a "J4" qualifier for all effected samples. Tax I.D. 62-0814289 Est. 1970 The data package includes a summary of the analytic results of the quality control samples required by the SW-846 or CWA methods. The quality control samples include a method blank, a laboratory control sample, and the matrix spike/matrix spike duplicate analysis. If a target parameter is outside the method limits, every sample that is effected is flagged with the appropriate qualifier in Appendix B of the analytic report. Method Blank - an aliquot of reagent water carried through the entire analytic process. The method blank results indicate if any possible contamination exposure during the sample handling, digestion or extraction process, and analysis. Concentrations of target analytes above the reporting limit in the method blank are qualified with the "B" qualifier. Bill, «L330131.pdf» 2 From: Daw, Larry (Environment Health & Safety) Sent: Monday, February 25, 2008 11:50 AM To: Lowery, William (Energy Services) Subject: FW: Lab report L330131 Attached are the lab results for the latest sample collected from the drain. Nothing was identified above the detection limits, so you are free to do what you want with the water. Apparently, the lab sent me these results almost two weeks ago. For some reason I did not receive the results. Thanks for asking. Please let me know if you have any questions or concerns. From: Mark Beasley [mailto:mbeasley@envsci.com] Sent: Monday, February 25, 2008 11:24 AM To: Daw, Larry (Environment Health &. Safety) Subject: Lab report L330131 This E-mail and any attached files are confidential, and may be copyright protected. If you are not the addressee, any dissemination of this communication is strictly prohibited. If you have received this message in error, please contact the sender immediately and delete/destroy all information received. Thanks Mark Beasley Environmental Science Corp Phone: 800-767-5859 ext 176 Email: mbeasley(5)envsci.com Larry Daw, L.G. Geophysicist/Licensed Geologist The University of North Carolina at Chapel Hill Department of Environment, Health & Safety 1120 Estes Drive Extension Campus Box 1650 Chapel Hill, NC 27599-1650 (919) 962-6666 (919) 883-7019 Mobile (919) 962-0227 Fax JLDAW@ehs.unc.edu http://ehs.unc.edu/ Client Date Sample Rcvd:9/24/08 Long Creek Court Merittch Work Order #09240870 Sample: Effluent Grab 9/24/08 Paraxiieters Result Analysis Date Reporting Limit Method iSampled, but analysis lost or not performed due to lab error. 1 certify that 1 have reviewed and approve these data. 600Zm/TB103E)Vd E8Z8-E69-BT6 85^0 I I I Report Date: Revision Date: SM 5210B SM 2540 D EPA 350.1 EPA 351.1 EPA 353.2 EPA 353.2 SM 9222D 9/30/08 10/29/08 X3 X3 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 dlMM CldQdXO 9/25/08 9/25/08 9/29/08 8/13/08 8/15/08 8/15/08 9/24/08 2.0 mg/L 1 mg/L 0.1 mg/L 0.20 mg/L 0.10 mg/L 0.20 mg/L 1 col/lOOml t I 5.6 mg/L 4 mg/L 0.6 mg/L 1.98 mg/L N/A mg/L N/A mg/L < 1 col/100ml Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Dennis Wilson Wilson's Wastewater Services PO Box 112 Oxford, NC 27565 Laboratory Representative BOD, & day Total Suspended Solids Ammonia, Nitrogen TKN Nitratj^/Nitrite, Nitrogen Nitrogen, total Fecal Coliform Qualifier NC004S631NPDES#G) Tel:Wilson's Wastewater Services 1-81S-&S3-S7S3Cient Fax 1-819-4t3-87S3 Address: P.O.# Project #Long Creek CourtAttertion: tf Composite? juired - Monthly BOD/TSS1GEffluent NHs.Ntot-HsSO,1G 1G 10Fecal Coliform1GEffluent 3 Comments:Method of Shipment: Time: Time:Received by: □Other 5^!^ Date 1 10 MZTMncoRd RMsvflte,NC 27320 Trne 1 Date 2 • of Conta. PO Box 112 Oxford, NC 27565 cs ro ld lO I cn LD CO I co co co Coop? Grab? "O I> Qm 4^ ro CS) C3 CO CS 4X cn co PH: 33S-342474S FAX: 336-342-1522 EMAIL- wtdabQbeUscuth.net Trne 2 OX o Q s:s: -iT3 MEMTECH, INC. EWVIROMMENTAL LABORATOBffiS A Dfmwi of V^tor Yw*w>fo<f)f »nti Corttmtx, Kk. Dennis M. Wilson Person Taking Sample(Signatur^-^y^ Tests pH OK? C12OK? Chain of Custody Record (COC) : SfflTpfe L LocaticnflO# Mo □, eMdby:/ Lab Use Only On Ice? vm these resuta be used for regulatory purposes? Yes P.uiroiinjdby- /3,z7 Date Tme Z " Date: Time: /J Date: Trne QFedEx □ UPS Date Dale: FieinquKhed by.