WQ0001492_Monitoring - 07-2024_20240823

Monitoring Report Submittal
Permit Number#* WQ0001492
Name of Facility:* Elementis Chromium Castle Hayne Manufacturing Facility
Month: * July Year: * 2024
Report Information
Type* Upload Document*
GW-59 7-24 Occidental GW-59 Submittal.pdf
PDF Only
Confirmation Email Address:
Name of Submitter: *
Signature:
Date of submittal:
Initial Review
8.39MB
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59).
[e-mail]
Scott Drury
.Scoll Drary
Reviewer: Wanda.Gerald
8/23/2024
This will be filled in automatically

Is the project number correct?* W00001492
Is the monitoring report accepted?* Yes NO
Regional Office* Wilmington
Reviewer: _anonymous
Review Date: 8/26/2024

hart hickman
SMARTER ENVIRONMENTAL SOLUTIONS
Via Electronic Upload
August 27, 2024
NC Department of Environmental Quality
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: July 2024 Groundwater Monitoring Compliance Report Forms
Elementis Chromium Castle Hayne Manufacturing Facility
Occidental Chemical Corporation SDR Permit No. WQ0001492
Castle Hayne, North Carolina
H&H Job No. OXY-004
Dear Sir or Madam:
On behalf of Glenn Springs Holdings, Inc. (for Occidental Chemical Corporation), Hart &
Hickman, PC (H&H) is submitting the attached Groundwater Quality Monitoring: Compliance
Report Forms (GW-59A and GW-59) and laboratory analytical report for groundwater samples
collected during July 2024 in accordance with the Occidental Chemical Corporation Surface
Disposal of Residuals (SDR) Permit No. WQ0001492 for the Elementis Chromium Castle Hayne
Manufacturing Facility. Under the terms of the SDR permit, groundwater within an established
Compliance Boundary (generally surrounding the Quarry as depicted in Figure 1) is monitored on
a semi-annual basis (during July and November) for chloride, total chromium, total iron, total
nickel, pH, and total dissolved solids (TDS).
Note that the chromium business of Elementis plc (including Elementis Chromium, LP) was
purchased by Yildirim Holding A.S. (a Dutch -Turkish industrial group headquartered in Istanbul
and Amsterdam) during January 2023, and the Facility is now being operated under the name
American Chrome and Chemicals, LLC (ACC). Legal obligations and contracts between
Occidental and Elementis remain in effect between Occidental and ACC.
Background Information
The facility is currently operating under a 1999 Corrective Action Plan (I -CAP) for remediation of
compounds of concern (COCs) in groundwater above standards by processes of natural attenuation
pursuant to 15A NCAC 2L .0106(1). The COCs addressed by the 1-CAP are chlorides, iron, pH,
and TDS. The objective of the 1-CAP is to reduce COC concentrations which exceed target
cleanup concentrations at or outside of the compliance boundary established in the SDR permit by
natural attenuation. The target cleanup concentrations for the COCs except total iron are the
2923 South Tryon Street, Suite 100 3921 Sunset Ridge Rd, 5uite 301
Charlottc, NC 28203 Rafcigh, NC 27607 www.hdrthickman.com
704.586.0007 main 919.847A241 main

Division of Water Quality
August 27, 2024
Page 2
2L Standards. For total iron, the target cleanup concentrations are background levels established
under a now -expired Special Order by Consent (SOC) agreement. Annual natural attenuation
groundwater monitoring reports are submitted to the NC Department of Environmental Quality
(DEQ) Division of Water Resources (DWR) to satisfy the 1-CAP monitoring reporting
requirements.
The results of the July 2024 monitoring indicate the presence of COCs covered by the 1-CAP above
2L Standards or background. Immediate notification of elevated iron, chloride, and TDS
concentrations and pH levels outside the 2L Standard range was not made to DWR after receipt of
the analytical results because these conditions are already known to DWR and are addressed under
the 1-CAP. Immediate notification of elevated chromium in well MW-24/CPW-4D was not made
after receipt of the analytical results because this condition is attributable to the Plant Process Area
(PPA) of the site and is already known to DEQ. Chromium impacts associated with the PPA are
being managed under an Administrative Agreement (AA) for Voluntary Assessment and Remedial
Action under the Inactive Hazardous Sites Branch (IHSB) Registered Environmental Consultant
(REC) Program, DEQ ID NCD057454670. Because chromium and nickel are not COCs in the 1-
CAP, if chromium and/or nickel concentrations are detected above the 2L Standards in the
compliance wells (other than chromium in well MW-24/CPW-4D), notification is made to DEQ
in accordance with the SDR permit. There were no detection of chromium or nickel above 2L
Standards in the July 2024 compliance well samples (other than chromium in well MW-24/CPW-
4D)
If you have any questions or need additional information, please do not hesitate to contact us at
[phone].
Sincerely,
Hart & Hickman, PC
S �a-
Scott Drury, PE
Project Manager
Attachments
Steve Hart, PG
Principal
cc: Dr. Morella Sanchez -King, PhD, PE - DWR (via email)
Ms. Teresa Jordan, PE — Glenn Springs Holdings (via email)
Mr. Sean Coury, PE — Coury Science & Engineering (via email)
https://hartWck.slta epoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Oxychem/Quarry/Quarry L-Cap
Sampling/2024/July/Cover Letter.docx
hart hickman
SMARTER ENVIRONMENTAL SOLUTIONS

GW-59A COMPLIANCE REPORT FORM Permit #W0[1(101492
(Subinit one each monitoring period with Gll� 59 forms.)
I
Enter date monitoring results were due. ( 0130124 ) Will this monitoring report (GW-59 and GW-59A)
YES
NO
be submitted after the established due date?
X
2
Was any required information missing on the GW-59 report forms?
YES
NO
X
IF the answer to question 1 or 2 is "YES" list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap,
YES
NO
missing identification plate, area overgrown, etc.)? If the answer is "Yes" contact the Regional Office for
guidance.
X
4
Are any monitored constituents equal to or above the established standards?
YES
NO
X
If the answer to question 4 is "NO", skip to section 8.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the space provided below:
See enclosed Summary of Affected Wells
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
YES
NO
same constituent(s) in the same well(s) in the last two years?
X
If the answer to question 5 is "NO", skip to section 8.
If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years).
See enclosed Summary of Affected Wells
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
X
If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly
located; contact the Regional Office.
Immediate notification of elevated iron, chloride, and TDS concentrations and pH levels outside the 2L Standard range was
not made since these conditions were already known to DWR. Immediate notification of elevated chromium in MW-24
(CPW-4D) was not made since this condition is attributable to the Plant Process Area (PPA) of the site and was already
known to DEQ. Chromium impacts associated with the PPA are being managed under an Administrative Agreement (AA)
for Voluntary Assessment and Remedial Action under the Inactive Hazardous Sites Branch (IHSB) Registered
Environmental Consultant (REC) Program, DEQ ID NCD057454670.
7
Is the permittee implementing previously approved actions required by the Division involving this
YES
NO
groundwater quality problem?
X
If the answer to question 7 is "YES" describe those actions in the space provided below.
If the answer to question 7 is "NO",
houndadgs surrounding this facility, Failure to dn so may subiect the to a Notigg of Wolation.
fines. andlar penalties_
The facility is currently operating under a Corrective Action Plan for ground water remediation by natural attenuation
under the provisions outlined in 15A NCAC 2L.0106(1).
8
The person completing this portion (G W-59A) of the monitoring report should sign below and submit this
form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby acknowledge that the above information was evaluated and the information submitted in this
report (Compliance Rep rt GW-59A) is true and complete to the best of my knowledge.
� z
Signature of Authorized Agent for i tee (Steve Hart, PG, Principal, Hart& Hickman, PC) ate
(Glenn Springs Holdings, Inc./Occidental Chemical Corp)
GW-59A 12/8/2003

SUBMIT FORM ON YELLOW PAPER ONLY
EPARTM ENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
Waffil),6117
IVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAILSERVICECENTER,RALEIGH,NC27699-1617 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 4/30/2028
Facility Name: Elementis Chromium Castle Hayne Manufacturing Facility
Non -Discharge UIC
Permit Name (if different): Occidental Chemical Corporation
NPDES Other WODD01492
Facility. Address: 5408 Holly Shelter Rd
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Castle Ha ne INC 28249 County New Hanover
❑ Spray Field ❑ Remediation:
Contact Person: Teresa Jordan
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: 34°21'46.2200",-077°52'12.3200"
No, of wells to be sampled: 24
❑ Water Source Heat Pump x❑ Other: Surface Disposal of Residuals
from Perm!
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-1 / CPW-13S
Date sample collected: 7/15/2024
FIELD ANALYSES:
WAS
Well Depth: 38 ft.
Well Diameter: 4 in.
pH 00400: 6.81 units Temp. 000lo: °C
DRY at
Depth to Water Level 82546: 7.66 ft. below measuring point
Screened Interval: 28 ft. to
38 ft. Spec. Cond. 00094: µMhos
time ofsampling,
Measuring Point is 2.65 ft. above land surface
Relative M.P. Elevation: 14.95 ft.
Odor 000m:
check
Volume of water pumped/bailed before sampling: 0.75
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: EYES
❑ NO and field acidified: ® YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 7/15/24-7/29124
Laboratory Name: SGS North America Inc. / Hart & Hickman (pH) Certification No. 487 / 5356
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 842 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC 00680 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 6.40 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034 10 U
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 20,400
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0)
Specific Conductance 00095 µMhos
K - Potassium 00937
mg/L method #
Total Ammonia 00610 mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625 mg/L
Ni - Nickel 01067 10 U
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOG Removal /o
Steve Hart, PG, Principal, Hart & Hickman, PC Authorized Agent)
Permittee (or Authorized Aqent) Name and Title - Please print or type
GW-59 Rev.8/2013
re of Permittee (or
fs/21 !7'
(Date)

SUBMIT FORM ON YELLOW PAPER ONLY
• •
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
�11'IstON OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
• • •
ifi17MAIL SERVICE CENTER, RALEIGH,NC27699-1617 Phone:[phone]
FACILITY INFORMATION Please PdntCdeartyorType
PERMIT Number: Expiration Date: 4/30/2028
Facility Name: Elementis Chromium Castle Ha ne Manufacturin2 Facility
Nan -Discharge UIC
Permit Name (if different): Occidental Chemical Corporation
NPDES Other W00001492
Facility Address: 5408 Holly Shelter Rd
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Castle Ha ne NC 28249 County New Hanover
❑ Spray Field ❑ Remediation:
Contact Person: Teresa Jordan
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: 34°21'51.6400",-077°52'30.2400"
No. of wells to be sampled: 24
❑ Water Source Heat Pump 0 Other: Surface Disposal of Residuals
iFrom Pemrt
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-2 / CPW-14S
Date sample collected: 7/17/2024
FIELD ANALYSES:
WAS
Well Depth: 28 ft.
Well Diameter: 4 in,
pH 00400: 6.80 units Temp. 000lo: °C
DRY at
Depth to Water Level szsas: 7.63 ft. below measuring point
Screened Interval: 18 ft. to
28 ft. Spec. Cond. 00094: µMhos
time ofsampling,
Measuring Point is 2.73 ft. above land surface
Relative M.P. Elevation: 12.53 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling: 0.75
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: fit❑ YES ❑ NO and field acidified: ® YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed- 7117/24-7/29/24
Laboratory Name: SGS North America
Inc. / Hart & Hickman H Certification No. 487 / 5356
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead o1o5i ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 878 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC o068o mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 148 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034 10 U
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 3,100
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0)
Specific Conductance 00095 µMhos
K - Potassium 00937
mg/L method #
Total Ammonia 00610 mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625 mg/L
Ni - Nickel 01067 10 U
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs:
Steve Hart, PG, Principal, Hart & Hickman, PC Authorized Agent)
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.8/2013
iplete, and that the laboratory analytical date
possibNily of fines ane imprisonment for kn
1
mg/L VOC Removal%
'*/-Zr /2¢
(Date)

SUBMIT FORM ON YELLOW PAPER ONLY
pEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
,
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-Io7-6so6
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 4/30/2028
Facility Name: Elementis Chromium Castle Hayne Manufacturing Facility
Non -Discharge UIC
Permit Name (if different): Occidental Chemical Corporation
NPDES Other WQ0001492
Facility Address: 5408 Holly Shelter Rd
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Castle Hayne NC 28249 County New Hanover
❑ Spray Field ❑ Remediation:
Contact Person: Teresa Jordan
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: 34°22'04.7700",-077°52'21.5000"
No. of wells to be sampled: 24
❑ Water Source Heat Pump ❑x Other: Surface Disposal of Residuals
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-3 / CPW-15S
Date sample collected: 7/16/2024
FIELD ANALYSES:
WAS
Well Depth: 40 ft.
Well Diameter: 4 in.
pH 00400: 7.20 units Temp. 000lo: °C
DRY at
Depth to Water Level 82546: 9.77 ft. below measuring point
Screened Interval: 25 ft. to
40 ft, Spec. Cond. 00094: µMhos
time of sampling,
Measuring Point is 3.56 ft. above land surface
Relative M.P. Elevation: 13.76 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling: 0.75
gallons
Appearance
nc;re; ❑
Samples for metals were collected unfiltered: EYES ❑ NO and field acidified: EYES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 7/16/24-7/29/24
Laboratory Name: SGS _North America
Inc. / Ha_rt& Hickman (pH) _ Certification No. 487 / 5356
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead o1o51 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issoived Solids:Total 70300 1,240 mg/L
Al - Aluminum olim
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC 00680 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 162 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total o1o34 10 U
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 100 U
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0)
pedfic Conductance 00095 µMhos
K - Potassium 00937
mg/L method #
Total Ammonia 00610 mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3as N: Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625 mg/L
Ni - Nickel 01067 10 U
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Steve Hart, PG, Principal, Hart & Hickman, PC Authorized Agent)
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.8/2013
nature Of Permittde (or Authorized A,,it!)0
8 z,1
(Date)

SUBMIT FORM ON YELLOW PAPER ONLY
•
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
�
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 4/30/2028
Facility Name: Elementis Chromium Castle Hayne Manufacturing Facility
Non -Discharge UIC
Permit Name (if different): Occidental Chemical Corporation
NPDES Other W00001492
Facility Address: 5408 Holly Shelter Rd
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Castle Ha ne INC 28249 County New Hanover
❑ Spray Field ❑ Remediation:
Contact Person: Teresa Jordan
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: 34'22'25.7100",-077°51'58.5900"
No. of wells to be sampled: 24
❑ Water Source Heat Pump ❑x Other: Surface Disposal of Residuals
from Pawn!
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-8 / CPW-8DR
Date sample collected: 7/17/2024
FIELD ANALYSES:
WAS
Well Depth: 87 ft.
Well Diameter: 4 in.
pH o040o: 7-02 units Temp. 000lo: °C
DRY at
Depth to Water Level 82546: 5.61 ft. below measuring point
Screened Interval: 67 ft. to
87 ft. Spec. Cond. 00094: µMhos
time ofsampling,
Measuring Point is 3.15 ft. above land surface
Relative M.P. Elevation: 8.35 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling: 0.75
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: ❑fit YES ❑
NO and field acidified: ® YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 7/17/24-7/29/24
Laboratory Name: SGS North America Inc. / Hart & Hickman H Certification No. 487 / 5356
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead o1o51 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 800 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC 00680 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 233 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total o1o34 to U
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 1,520
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0)
Specific Conductance 00095 µMhos
K - Potassium 00937
mg/L method #
Total Ammonia 00610 mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625 mg/L
Ni - Nickel 01067 l o U
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Steve Hart, PG, Principal, Hart & Hickman, PC Authorized Agent)
Permittee (or Authorized Aqent) Name and Title - Please print or type
GW-59 Rev.8/2013
Siqnature of Permittee iarAtrtn
�1
(Date)

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print 0early or Type
PERMIT Number: Expiration Date: 4/30/2028
Facility Name: Elementis Chromium Castle Ha ne Manufacturing Facility
Non -Discharge UIC
Permit Name (if different): Occidental Chemical Corporation
NPDES Other WQ0001492
Facility Address: 5408 Holly Shelter Rd
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Castle Ha ne NC 28249 County New Hanover
❑ Spray Field ❑ Remediation:
Contact Person: Teresa Jordan
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: 34°22'21.7300",-077'52'11,7100"
No. of wells to be sampled: 24
❑ Water Source Heat Pump ❑7t Other: Surface Disposal of Residuals
57, P.rmtt
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-9 / CPW-9D
Date sample collected: 7/17/2024
FIELD ANALYSES:
WAS
Well Depth: 108 ft.
Well Diameter: 4 in.
pH oo40o: 7.13 units Temp. 000ia °C
DRY at
Depth to Water Level 82546: 5.44 ft. below measuring point
Screened Interval: 88 ft. to
108 ft. Spec. Cond. 00094: µMhos
+
time of sampling,
Measuring Point is 2.57 ft. above land surface
Relative M.P. Elevation: 8.37 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling: 0.75
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: EYES
❑ NO and field acidified: ® YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 7/17/24-7/29/24
Laboratory Name: SGS North America Inc. / Hart & Hickman (PH) Certification No. 487 / 5356
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 1,650 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC 00680 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 211 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total o1o34 10 U
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 100 U
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0)
Specific Conductance 00095 µMhos
K - Potassium 00937
mg/L method #
Total Ammonia 00610 mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625 mg/L
Ni - Nickel 01067 10 U
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%.
Steve Hart. PG, Principal, Hart & Hickman, PC Authorized Agent)
Permittee (or Authorized Aqent) Name and Title - Please print or type
VVV-V:7
MCV. O/GV I

SUBMIT FORM ON YELLOW PAPER ONLY
•
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Pnnr Clearly or Type
PERMIT Number: Expiration Date: 4/30/2028
Facility Name: Elementis Chromium Castle Hayne Manufacturing Facility
Non -Discharge UIC
Permit Name (if different): Occidental Chemical Corporation
NPDES Other W00001492
Facility Address: 5408 Holly Shelter Rd
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Castle Ha ne NC 28249 County New Hanover
❑ Spray Field ❑ Remediation:
Conlact Person: Teresa Jordan
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:34°22'13.9300",-077°52'19,0700"
No. of wells to be sampled. 24
❑ Water Source Heat Pump ® Other: Surface Ois oral of Residuals
ham Perm:;
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-10 / CPW-10D Date sample collected: 7/16/2024
FIELD ANALYSES:
WAS
Well Depth: 100 ft.
Well Diameter: 4 in,
pH 00400: 9.28 units Temp. 000lo: °C
DRY at
Depth to Water Level 82546: 7.65 ft. below measuring point
Screened Interval: 60 ft. to
100 ft. Spec. Cord, 000sa: µMhos
time ofsampling,
Measuring Point is 3.38 ft. above land surface
Relative M.P. Elevation: 10.38 ft.
Odor 000s5:
check
Volume of water pumped/bailed before sampling: 0.75
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: ❑!t YES
❑ NO and field acidified: © YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 7/16/24-7/29/24
Laboratory Name: SGS North America
—
Inc / Hart & Hickman (pH) Certification No. 487 / 5356
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead o1o51 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly tumid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 1,310 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC oosso mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 160 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034 10 U
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 100 U
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0)
Specific Conductance 00095 µMhos
K - Potassium 00937
mg/L method #
Total Ammonia 00610 mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625 mg/L
Ni - Nickel 01067 10 U
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Steve Hart, PG, Principal, Hart & Hickman, PC Authorized Agent)
Permittee (or Authorized Apent) Name and Title - Please print or type
GW-59 Rev.8/2013
�G
nature of Permittee {or Authorized Aue

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT 8, NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING;
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 4/30/2028
Facility Name: Elementis Chromium Castle Ha ne Manufacturing Facility
Non -Discharge UIC
Permit Name (if different): Occidental Chemical Corporation
NPDES Other W00001492
Facility Address: 5408 Holly Shelter Rd
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Castle Hayne NC 28249 County New Hanover
❑ Spray Field ❑ Remediation:
Contact Person: Teresa Jordan
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Weil Location/Site Name: 34°22'09.7700".-077°51'39.4400"
No. of wells to be sampled: 24
❑ Water Source Heat Pump © Other: Surface Disposal of Residuals
Mwn Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-11 / CPW-1S
Date sample collected: 7/15/2024
FIELD ANALYSES:
WAS
Well Depth: 32 ft.
Well Diameter: 2 in.
pH 00400: 6.74 units Temp. 000lo: °C
DRY at
time, of
time, of
Depth to Water Level 82546: 5.51 ft. below measuring point
Screened Interval: 17 ft. to
32 ft. Spec. Cond. 00094: µMhos
Measuring Point is 2.0 ft. above land surface
Relative M.P. Elevation: 26.40 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling: 0.75
gallons
Appearance
here.❑
Samples for metals were collected unfiltered: !t❑ YES
❑ NO and field acidified: ® YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 7/15/24-7/29/24
Laboratory Name: SGS North America Inc, / Hart & Hickman (pH) Certification No 487 / 5356
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead o1o51 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids -Total 70300 484 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC 00680 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 5.10 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034 10 U
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 11,700
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0)
Specific Conductance 00095 µMhos
K - Potassium 00937
mg/L method #
Total Ammonia 00610 mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625 mg/L
Ni - Nickel 01067 10 U
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs:
Steve Hart, PG, Principal, Hart & Hickman, PC Authorized Agent)
Permittee for Authorized A4ent) Name and Title - Please ynnt or type
GW-59 Rev.8/2013
and that the laboratory analytical date
ility of fines and imprisonment for kn
EN
IN
VOC Removal%
o.e)

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone:[phone]
FACILITY INFORMATION Please PON Clearly or Type
PERMIT Number: Expiration Date: 4/30/2028
Facility Name: Elementis Chromium Castle Ha ne Manufacturing Facility
Non -Discharge UIC
Permit Name (if different): Occidental Chemical Corporation
NPDES Other WQ0001492
Faciltty Address: 5408 Holly Shelter Rd
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Castle Hayne NC 28249 County New Hanover
❑ Spray Field ❑ Remediation:
Contact Person: Teresa Jordan
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: 34°22'03.3000".-077°51'56.8900"
No. of wells to be sampled: 24
❑ Water Source Heat Pump Other: Surface Disposal of Residuals
0, Pe57
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-12 / CPW-12D
Date sample collected: 7/15/2024
FIELD ANALYSES:
WAS
Well Depth: 98 ft.
Well Diameter: 4 in.
pH 00400: 6.93 units Temp. 000lo: °C
DRY at
Depth to Water Level 82546: 8.46 ft. below measuring point
Screened Interval: 58 ft. to
98 ft. Spec. Cond. 00094: µMhos
time of
sampling,
g,
Measuring Point is 0.80 ft. above land surface
Relative M.P. Elevation: 14.10 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling: 0.75
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: ❑fit YES ❑
NO and field acidified: EYES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 7115124-7/29124
Laboratory Name: SGS North America Inc. I Hart & Hickman (H) Certification No 487 / 5356
PARAMETERS MOTE. Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 896 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC 00680 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 4.70 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034 10 U
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 8,580
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0)
pecif3c Conductance 00095 µMhos
K - Potassium 00937
mg/L method #
Total Ammonia 00610 mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; ArrRrgnla Wttogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625 mg/L
Ni - Nickel 01067 10 U
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs:
Steve Hart, PG, Principal, Hart & Hickman, PC Authorized Agent)
Permittee (or Authorized Anent) Name and Title - Please print or type
GW-59 Rev.8/2013
mg/L Effluent Total •
tplete and that the laboratory analytical data was p
possibility of fines and impriso iment for kno ing
mg/L VOC Removal%
'As l2
Matel

SUBMIT FORM ON YELLO'vv PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print CleaffyorType
PERMIT Number: Expiration Date: 4/30/2028
Facility Name- Elementis Chromium Castle Ha ne Manufacturing Facility
Non -Discharge UIC
Permit Name (if different). Occidental Chemical Corporation
NPDES Other VV00001492
Facility Address: 5408 Holly Shelter Rd
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Castle Ha ne NC 28249 County New Hanover
❑ Spray Field ❑ Remediation:
Contact Person: Teresa Jordan
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Weil Location/Site Name: 34°21'46.2200",-077°52'12.3200"
No. of wells to be sampled: 24
❑ Water Source Heat Pump ® Other: Surface Disposal of Residuals
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-13 / CPW-13D Date sample collected: 7/15/2024
FIELD ANALYSES:
WAS
Well Depth: 80 ft.
Well Diameter: 4 in.
pH 00400: 6.80 units Temp. 00010: °C
DRY at
Depth to Water Level 82546: 9.90�ft. below measuring point
Screened Interval: 70 ft. to
80 ft. Spec. Cond. 00094: µMhos
time ofsampling,
Measuring Point is 2.53 ft. above land surface
Relative M.P. Elevation: 15.13 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling: 0.75
gallons
Appearance
here ❑
Samples for metals were collected unfiltered: ❑fit YES
❑ NO and field acidified: © YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 7/15/24-7/29/24
Laboratory Name: SGS North America Inc. / Hart & Hickman H Certification No. 487 / 5356
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 1,390 mg/L
Al - Aluminum oil o5
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC 00680 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 155 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034 10 U
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 298
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0)
pecrfic Conductance 00095 µMhos
K - Potassium 00937
mg/L method #
Total Ammonia 00610 mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3as N; Ammonia Nit"n, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625 mg/L
Ni - Nickel 01067 10 U
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
• •
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
•
DIV+SION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 4/30/2028
Facility Name: Elementis Chromium Castle Hayne Manufacturing Facility
Non -Discharge UIC
Permit Name (if different): Occidental Chemical Corporation
...
NPDES Other W00001492
Facility Address: 5408 Holly Shelter Rd
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Castle Ma rie NC 28249 County New Hanover
❑ Spray Field ❑ Remediation:
Contact Person: Teresa Jordan
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: 34°21'51.6400",-077°52'30.2400"
No. of wells to be sampled: 24
❑ Water Source Heat Pump 0 Other: Surface Disposal of Residuals
am Pwnro
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-14 / CPW-14D
Date sample collected: 7/17/2024
FIELD ANALYSES:
WAS
Well Depth: 80 ft.
Well Diameter: 4 in.
pH 00400: 6.80 units Temp. 000lo: °C
DRY at
time of
Depth to Water Level 82546: 8.12 ft. below measuring point
Screened Interval: 75 ft. to
85 ft. Spec. Cond. 00094: µMhos
sampling,
Measuring Point is 3.44 ft. above land surface
Relative M.P. Elevation: 12.94 ft.
Odor 000m:
check
Volume of water pumped/bailed before sampling: 0.75
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: ® YES ❑
NO and field acidified: ® YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 7/17/24-7/29/24
Laboratory Name: SGS North America Inc. / Hart & Hickman H Certification No. 487 / 5356
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 1,510 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC 00680 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 164 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total o1o34 10 U
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 2,340
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0)
pecific Conductance 00095 µMhos
K - Potassium 00937
mg/L method #
Total Ammonia 00610 mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Totap
Mn - Manganese 01055
ug/L , method #
TKN as N 00625 mg/L
Ni - Nickel 01067 10 U
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Steve Hart, PG, Principal. Hart & Hickman, PC Authorized Agent)
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.8/2013
Siqnature of Permittee (or
8/2[ l'L.
(Date)

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 4/30/2028
Facility Name: Elementis Chromium Castle Ha ne Manufacturing Facility
Non -Discharge UIC
Permit Name (if different): Occidental Chemical Corporation
NPDES Other WQ0001492
Facility Address: 5408 Holly Shelter Rd
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Castle Ha ne NC 28249 County New Hanover
❑ Spray Field ❑ Remediation:
Contact Person: Teresa Jordan
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: 34°22'04.7700",-077°52'21.5000"
No, of wells to be sampled: 24
❑ Water Source Heat Pump ❑x Other: Surface Disposal of Residuals
hom Periril
SAMPIJNG INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-15 / CPW-15D
Date sample collected: 7/16/2024
FIELD ANALYSES:
WAS
Well Depth: 74 ft.
Well Diameter: 4 in.
pH 00400: 7.28 units Temp. 000lo: °C
DRY at
time o f
Depth to Water Level 82546: 9.25 ft. below measuring point
Screened Interval: 64 ft. to
74 ft. Spec. Cond. 00094: µMho
—
sampling,
P g•
Measuring Point is 3.64 ft. above land surface
Relative M.P. Elevation: 13.64 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling: 0.75
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: fit❑ YES ❑
NO and field acidified: ® YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 7116/24-7/29/24
Laboratory Name: SGS North America Inc. / Hart & Hickman H Certification No. 487 / 5356
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead o1o51 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 796 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC om8o mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 129 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034 10 U
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 100 U
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0)
pecific Conductance 00095 µMhos
K - Potassium 00937
mg/L method #
Total Ammonia 00610 mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625 mg/L
Ni - Nickel 01067 10 U
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs mg/L VUU rtemovat io
Steve Hart, PG, Principal, Hart & Hickman, PC Authorized Agent)
Permittee (or Authorized Aqent) Name and Title - Please print or type

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 4/30/2028
Facility Name: Elementis Chromium Castle Ha ne Manufacturing Facility
Non -Discharge UIC
Permit Name (if different): Occidental Chemical Corporation
NPDES Other WQ0001492
Facility Address: 5408 Holly Shelter Rd
_
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Castle Ha ne NC 28249 County New Hanover
❑ Spray Field ❑ Remediation:
Contact Person: Teresa Jordan
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: 34'22'34.0100",-077°51'43.9000"
No. of wells to be sampled: 24
❑ Water Source Heat Pump ❑>It Other: Surface Disposal of Residuals
Ilium Pornir
SAMPLING INFORMATION
If WELT_
WELL ID NUMBER (from Permit): MW-16 / CPW-6S
Date sample collected: 7/17/2024
FIELD ANALYSES:
WAS
Well Depth: 42 ft.
Well Diameter: 4 in.
pH 00400: 6.72 units Temp. 000lo: °C
DRY at
time ofsampling,
Depth to Water Level 82546: 13.18 ft. below measuring point
Screened Interval: 27 ft. to
42 ft. Spec. Cond. 00094: µMhos
Measuring Point is 3.59 ft. above land surface
Relative M.P. Elevation: 15.79 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling: 0.75
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: EYES
❑ NO and field acidified: ®YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 7/17/24-7/29/24
Laboratory Name: SGS North America Inc. / Hart & Hickman H Certification No. 487 / 5356
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use WIN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 1,440 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC 00680 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 174 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034 10 U
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 100 U
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0)
pecific Conductance 00095 µMhos
K - Potassium 00937
mg/L method #
Total Ammonia oo6lo mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen: NH3as N: Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625 mg/L
Ni - Nickel 01067 to U
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs. mg/L VOG Removal%
Steve Hart, PG, Principal, Hart & Hickman, PC Authorized Agent)
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.8/2013
ure
Aqent)
W //
Z Z.i G
(Date)

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT 8, NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVtSIQN OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please PfnrClearly orType
PERMIT Number: Expiration Date: 4/30/2028
Facility Name: Elementis Chromium Castle Ha ne Manufacturing Facility
Non -Discharge UIC
Permit Name (if different): Occidental Chemical Corporation
NPDES Other WQ0001492
Facility Address: 5408 Holly Shelter Rd
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Castle Hayne NC 28249 County New Hanover
❑ Spray Field ❑ Remediation:
Contact Person: Teresa Jordan
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:34°22'18.4900",-077°51'46.3100"
No. of wells to be sampled: 24
❑ Water Source Heat Pump ❑x Other: Surface Disposal of Residuals
hon, Panrit]
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-17 / CPW-7S
Date sample collected: 7/16/2024
FIELD ANALYSES:
WAS
Well Depth: 28 ft.
Well Diameter: 4 in.
pH o040o: 7.00 units Temp. 000lo: °C
DRY at
Depth to Water Level 82546: 8.74 ft. below measuring point
Screened Interval: 12 ft. to
28 ft- Spec. Cond. 00094: µMhos
time ofsampling,
Measuring Point is 0.94 ft. above land surface
Relative M.P. Elevation: 15.14 ft.
Odor oo085:
check
Volume of water pumped/bailed before sampling: 0.75
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: ® YES
❑ NO and field acidified: ® YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 7/16/24-7/29/24
Laboratory Name: SGS North America Inc. / Hart & Hickman (pH) Certification No. 487 / 5356
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead o1o51 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 2,900 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC 00680 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 6.00 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total o1o34 10 U
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 10,200
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0)
Specific Conductance 00095 µMhos
K - Potassium 00937
mg/L method #
Total Ammonia 00610 mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625 mg/L
Ni - Nickel 01067 141
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs:
Steve Hart, PG, Principal, Hart & Hickman, PC Authorized Agent)
Permittee (or Authorized Aqent) Name and Title - Please print or type
GW-59 Rev.8/2013
•
iplete, and that the laboratory analytical data was produced using approved methods of analysis by a
possffiifityof fines and Imprisonrrant for knowing violations.
MINIM

SUBMIT FORM ON YELLOW PAPER ONLY
pEPARTM ENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-161T Phone: [phone]
FACILITY INFORMATION: Please Print Clearly or Type
PERMIT Number: Expiration Date: 4/30/2028
Facility Name: Elementis Chromium Castle Ha ne Manufacturin Facilit
Non -Discharge UIC
Permit Name (if different): Occidental Chemical Corporation
NPDES Other W00001492
Facility Address: 5408 Holly Shelter Rd
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Castle Hayne NC 28249 County New Hanover
❑ Spray Field ❑ Remediation:
Contact Person: Teresa Jordan
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: 34'22'25.7100",-077°51'58.5900"
No, of wells to be sampled: 24
❑ Water Source Heat Pump ❑7t Other: Surface Disposal of Residuals
Gun Palrtll
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-18 / CPW-8S
Date sample collected: 7/17/2024
FIELD ANALYSES:
WAS
Well Depth: 36 ft.
Well Diameter: 4 in.
pH 00400: 7.30 units Temp. 000lo: °C
DRY at
time of
Depth to Water Level 82546: 5.16 ft. below measuring point
Screened Interval: 21 ft. to
36 ft. Spec. Cond. 00094: µ Mhos
sampling, p g,
Measuring Point is 2.85 ft. above land surface
Relative M.P. Elevation: 7.95 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling: 0.75
gallons
Appearance
here:❑
Saales fzr metals were collected unfiltered: ❑>It YES
❑ NO and field acidified: IN YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 7/17/24-7/29/24
Laboratory Name: SGS North America Inc. / Hart & Hickman (H) Certification No 487 / 5356
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 666 mg/L
Al - Aluminum o11o5
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC 00680 mg/L
Ca - Calcium oo916
mg/L
Chloride 00940 63.4 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total o1o34 10 U
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 100 U
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0)
pecific Conductance 00095 µMhos
K - Potassium 00937
mg/L method #
Total Ammonia 00610 mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese o1055
ug/L , method #
TKN as N 00625 mg/L
Ni - Nickel 01067 10 U
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Steve Hart, PG, Principal, Hart & Hickman, PC Authorized Agent) ('. o
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Perm;for Autlicrized Agent)
GW-59 Rev.8/2013
IA
iDatci

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
� �
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please PnnrClearlyorType
PERMIT Number: Expiration Date: 4/30/2028
Facility Name: Elementis Chromium Castle Hayne Manufacturing Facility
Non -Discharge UIC
Permit Name (if different): Occidental Chemical Corporation
NPDES Other WQ0001492
Facility. Address: 5408 Holly Shelter Rd
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Castle Hayne NC 28249 County New Hanover
❑ Spray Field ❑ Remediation:
Contact Person: Teresa Jordan
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: 34°22'21.7300".-077'52'11.7100"
No. of wells to be sampled: 24
❑ Water Source Heat Pump 0 Other: Surface Dis al of Residuals
frrom PErrtt[1
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-19 / CPW-9S
Date sample collected: 7/17/2024
FIELD ANALYSES:
WAS
Well Depth: 38 ft.
Well Diameter: 4 in.
pH 00400: 7.04 units Temp. 000lo: °C
DRY at
Depth to Water Level 82546: 6.20 ft. below measuring point
Screened Interval: 23 ft. to
38 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 2.58 ft. above land surface
Relative M.P. Elevation: 8.28 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling: 0.75
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: fit❑ YES ❑ NO and field acidified: ® YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 7/17/24-7/29/24
Laboratory Name: SGS North America Inc. / Hart & Hickman (pH) Certification No. 487 / 5356
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead o1o5i ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 502 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC 00680 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 50.8 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total o1o34 10 U
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 1.020
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0)
Specific Conductance 00095 µMhos
K - Potassium 00937
mg/L method #
Total Ammonia 00610 mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625 mg/L
Ni - Nickel 01067 10 U
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
C, d
Steve Hart, PG, Principal, Hart & Hickman, PC Authorized Agent) L d f ZL
Permittee (or Authorized Aqent) Name and Title - Please print or type Signawre of Permittee (or Authorized Agent) ❑at• l
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTM ENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIV#SION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION PieasePHniClaarfyorType
PERMIT Number: Expiration Date: 41'30,2028
Facility Name: Elementis Chromium Castle Havne Manufacturing Facility
Nan -Discharge UIC
Permit Name (if different): Occidental Chemical Corporation
NPDES Other W00001492
Facility Address: 5408 Holly Shelter Rd
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Castle Ha ne NC 28249 County New Hanover
❑ Spray Field ❑ Remediation:
Contact Person: Teresa Jordan
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: 34'22'13.9300",-077*52'19.0700"
No. of wells to be sampled: 24
❑ Water Source Heat Pump >It❑ Other: Surface Dfsposal of Residuals
Srorn PenrYt
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-20 / CPW-10S
Date sample collected: 7/16/2024
FIELD ANALYSES:
WAS
Well Depth: 35 ft.
Well Diameter: 4 in.
pH 00400: 7.01 units Temp. 000lo: °C
DRY at
Depth to Water Level 82546: 8.22 ft. below measuring point
Screened Interval: 20 ft. to
35 ft. Spec. Cond. 000sa: µMhos
time ofsampling,
Measuring Point is 3.43 ft. above land surface
Relative M.P. Elevation: 10.33 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling: 0.75
gallons
Appearance
here.❑
Samples for metals were collected unfiltered: fit❑ YES
❑ NO and field acidified; ® YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 7/16/24-7/29/24
Laboratory Name: SGS North America
Inc. / Hart & Hickman (pH) Certification No. 487 / 5356
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 570 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC 00680 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 64.9 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total o1o34 10 U
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 100 U
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0)
Specific Conductance 00095 µMhos
K - Potassium 00937
mg/L method #
Total Ammonia 00610 mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625 mg/L
Ni - Nickel 01067 10 U
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%.
Steve Hart, PG, Principal, Hart & Hickman, PC Authorized Agent)
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.8/2013
re of Permittee * Authorized Aqent)

SUBMIT FORM ON YELLOW PAPER ONLY
IARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:ONISION
MMI
OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Cleady or Type
PERMIT Number: Expiration Date: 4/30/2028
Facility Name: Elementis Chromium Castle Hayne Manufacturing Facility
Non -Discharge UIC
Permit Name (if different): Occidental Chemical Corporation
NPDES Other WQ0001492
Facility Address: 5408 Holly Shelter Rd
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Castle Ha ne NC 28249 County New Hanover
❑ Spray Field ❑ Remediation:
Contact Person: Teresa Jordan
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: 34'22'31.7100",-077'51'38.6900"
No. of wells to be sampled: 24
❑ Water Source Heat Pump ❑7t Other: Surface Disposal of Residuals
Irom PprrrrS
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-21 / CPW-5S
Date sample collected: 7/17/2024
FIELD ANALYSES:
WAS
Well Depth: 34 ft.
Well Diameter: 4 in.
pH 00400: 7.30 units Temp. 000lo: °C
DRY at
time of
Depth to Water Level 82546: 7,40 ft. below measuring point
Screened Interval: 19 ft. to
34 ft. Spec. Cond. 00094: µMhos
sampling,
Measuring Point is 2.48 ft. above land surface
Relative M.P. Elevation: 9.88 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling: 0.75
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: IN YES
❑ NO and field acidified: ® YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 7/17/24-7/29/24
Laboratory Name: SGS North America Inc. / Hart & Hickman H Certification No 487 / 5356
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead o1051 ug/L
Coliform: MF Fecal 31616 /1 OOmL
Nitrate (NO3) as N 00620
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100ml-
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 966 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC 00680 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 123 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total o1034 10 U
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 1,580
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0)
Specific Conductance 00095 µMhos
K - Potassium 00937
mg/L method #
Total Ammonia 00610 mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese o1o55
ug/L , method #
TKN as N 00625 mg/L
Ni - Nickel 01067 10 U
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VUG Kemoval /o
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DfV351ON OF WATER RESOURCES- INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1517 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Ctearfy or Type
PERMIT Number: Expiration Date: 413OM28
Facility Name: Elementis Chromium Castle Hayne Manufacturing Facility
Non -Discharge UIC
Permit Name (if different): Occidental Chemical Corporation
NPDES Other WQ0001492
Facility. Address: 5408 Holly Shelter Rd
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Castle Ha ne NC 28249 County New Hanover
❑ Spray Field ❑ Remediation:
Contact Person: Teresa Jordan
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: 34°22'14.4900",-077°51'31.0900"
No. of wells to be sampled: 24
❑ Water Source Heat Pump © Other: Surface tits sal of Residuals
[from Perml!
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-22 / CPW-2D
Date sample collected: 7/15/2024
FIELD ANALYSES:
WAS
Well Depth: 75 ft.
Well Diameter: 4 in.
pH 00400: 6.90 units Temp. 000lo: °C
DRY at
Depth to Water Level 82546: 23.70 ft. below measuring point
Screened Interval: 45 ft. to
60 ft. Spec. Cond. 00094: µ Mhos
time of
sampling,
Measuring Point is 3.0 ft. above land surface
Relative M.P. Elevation: 25.36 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling: 0.75
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: 9 YES
❑ NO and field acidified: 9 YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 7/15/24-7/29/24
Laboratory Name: SGS North America Inc. / Hart & Hickman (pH) Certification No. 487 / 5356
PARAMETERS NOTE: Values should reflect dissolved and
colloidal concentrations.
COD 00335 rng/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 554 mg/L
Al -Aluminum o11o5
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC 00680 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 11.6 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total o1o34 10 U
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 4,550
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0)
pecific Conductance 00095 µMhos
K - Potassium 00937
mg/L method #
Total Ammonia 00610 mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Anvmnia Nilrogan, Total)
Mn - Manganese o1o55
ug/L , method #
TKN as N 00625 mg/L
Ni - Nickel 01067 10 U
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Steve Hart, PG, Principal, Hart & Hickman, PC Authorized Agent)
Permittee (or Authorized Aqent) Name and Title - Please print or type
GW-59 Rev.8/2013
Siqnature of
(2-
29 AI
(Datef

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT a, NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Pr+nrClearlyorType
PERMIT Number: Expiration Date: 4/30/2028
Facility Name: Elementis Chromium Castle Ha ne Manufacturing Facility
Non -Discharge UIC
Permit Name (if different): Occidental Chemical Corporation
NPDES Other WOD001492
Facility Address: 5408 Holly Shelter Rd
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Castle Ha ne NC 28249 County New Hanover
❑ Spray Field ❑ Remediation:
Contact Person: Teresa Jordan
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:34*22'19.9800",-077'51'25 3900"
No. of wells to be sampled: 24
❑ Water Source Heat Pump © Other: Surface Disposal of Residuals
ffrom Permill
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-23 / CPW-3D
Date sample collected: 7/16/2024
FIELD ANALYSES:
WAS
Well Depth: 105 ft.
Well Diameter: 4 in.
pH 00400: 6.93 units Temp. 000lo: °C
DRY at
Depth to Water Level 82546: 28.84 ft. below measuring point
Screened Interval: 57 ft. to
97 ft. Spec. Cond. 00094: µ Mhos
time of
sampling,
Measuring Point is 3,0 ft. above land surface
Relative M.P. Elevation: 27.42 ft
Odor 00085:
check
Volume of water pumped/bailed before sampling: 0.75
gallons
Appearance
here: El
Samples for metals were collected unfiltered: ® YES
❑ NO and field acidified: ® YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 7/16/24-7/29/24
Laboratory Name: SGS North America Inc. / Hart & Hickman (PH) Certification No. 487 / 5356
PARAMETERS NOTE: Values should reflect dissolved and
colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 572 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC 00680 mg/L
Ca - Calcium oo916
mg/L
Chloride 00940 32.9 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034 to U
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 1,320
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0)
pecific Conductance 00095 µMhos
K - Potassium 00937
mg/L method #
Total Ammonia 00610 mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen: NH3asN, Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625 mg/L
Ni - Nickel 01067 10 U
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs mg/L Effluent Total VOCs: mg/L VOC Removal%
Steve Hart, PG, Principal, Hart & Hickman, PC Authorized Agent)
Permittee (or Authorized Aqent) Name and Title - Please print or type
GW-59 Rev.8/2013
Mee far Autherized Agent)
11
2 A-1

SUBMIT FORM ON YELLOW PAPER ONLY
DEPAR71Y1ENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
bIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please FWnf Clearly or Type
PERMIT Number: Expiration Date: 41301202E
Facility Name: Elementis Chromium Castle Hare Manufacturing Facility
Non -Discharge UIC
Permit Name (if different): Occidental Chemical Corporation
NPDES Other W00001492
Facility Address: 5408 Holly Shelter Rd
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Castle Ha ne INC 28249 County New Hanover
❑ Spray Field ❑ Remediation:
Contact Person: Teresa Jordan
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: 34°22'24.6800",-077°51'25.8700"
No. of wells to be sampled: 24
❑ Water Source Heat Pump © Other: Surface Disposal of Residuals
from Perm.'
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-24 / CPW-4D
Date sample collected: 7/17/2024
FIELD ANALYSES:
WAS
Well Depth: 75 ft.
Well Diameter: 4 in.
pH 00400: 6.75 units Temp. 000lo: °C
DRY at
Depth to Water Level 82546: 27.83 ft. below measuring point
Screened Interval: 60 ft. to
75 ft. Spec. Cond. 00094: µMhos
time of sampling,
Measuring Point is 3.0 ft. above land surface
Relative M.P. Elevation: 26.99 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling: 0.75
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: 0 YES
❑ NO and field acidified: © YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed- 7/17/24-7/29/24
Laboratory Name: SGS North America Inc. / Hart & Hickman (pH) Certification No. 487 / 5356
PARAMETERS NOTE: Values should reflect dissolved and
colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 630 mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC 00680 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 53.7 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total o1034 3,780
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 100 U
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0)
pecific Conductance 00095 µMhos
K - Potassium 00937
mg/L method #
Total Ammonia 00610 mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; N113as N; Ammma Nilropn. Total)
Mn - Manganese o1o55
ug/L , method #
TKN as N 00625 mg/L
Ni - Nickel 01067 10 U
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Steve Hart, PG, Principal, Hart & Hickman, PC (Authorized Agent)
Permittee (or Authorized Aqent) Name and Title - Please print or type
GW-59 Rev.8/2013
Siqnature of Permittee far Auth
W,
S/2-r
fn] l'e

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DWISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or7y#s
PERMIT Number: Expiration Date: 4/30/2028
Facility Name: Elementis Chromium Castle Ha ne Manufacturing Facility
Non -Discharge UIC
Permit Name (if different): Occidental Chemical Corporation
NPDES Other WQ0001492
Facility. Address: 5408 Holly Shelter Rd
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Castle Ha ne NC 28249 County New Hanover
❑ Spray Field ❑ Remediation:
Contact Person: Teresa Jordan
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: 34'22'31.7100",-077°51'38.6900"
No. of wells to be sampled; 24
❑ Water Source Heat Pump ❑x Other: Surface Disposal of Residuals
kom pam )
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-25 / CPW-5D
Date sample collected: 7/17/2024
FIELD ANALYSES:
WAS
Well Depth: 99 ft.
Well Diameter: 4 in.
pH 00400: 7.70 units Temp. 000lo: °C
DRY at
time of
Depth to Water Level 82546: 8.60 ft. below measuring point
Screened Interval; 59 ft. to
99 ft, Spec. Cond. 00094: µMhos
sampling,
Measuring Point is 2.61 ft. above land surface
Relative M.P. Elevation: 10.01 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling: 0.75
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: EYES
❑ NO and field acidified: ® YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 7/17124-7/29/24
Laboratory Name: SGS North America Inc. / Hart & Hickman (pH) Certification No. 487 / 5356
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids -Total 70300 1.710 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC 00680 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 567 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034 10 U
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 100 U
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0)
Specific Conductance 00095 µMhos
K - Potassium 00937
mg/L method #
Total Ammonia 00610 mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625 mg/L
Ni - Nickel 01067 10 U
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs mg/L Effluent Total VUC:s: mg/L vvt. Kemovat-ro
Steve Hart, PG, Princi pal, Hart & Hickman, PC Authorized Agent)
Permittee (or Authorized Aqent) Name and Title - Please print or type
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
RMATiON Please Print Clearly or Type
ity Name: Elementis Chromium Castle Ha ne Manufacturing Facility
fit Name (if different): Occidental Chemical Corporation
ity Address: 5408 Holly Shelter Rd
Castle Havne INC 28249 County New Hanover
act Person: Teresa Jordan
Location/Site Name: 34'22'34.0100",-077°51'43.9000"
Telephone#: [phone]
No, of wells to be sampled:
24
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER RALEIGH, NC 27699-1617 Phone: [phone]
PERMIT Number:
Expiration Date: 4/30/2028
Non -Discharge
UIC
NPDES
Other W00001492
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
❑ Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
© Other: Surface Disposal of Residuals
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): MW-26 / CPW-6D
Date sample collected: 7/17/2024
FIELD ANALYSES:
WAS
Well Depth. 101 ft.
Well Diameter: 4 in.
pH 00400: 9.23 units Temp. 00010: °C
DRY at
time ofsampling,
Depth to Water Level 82546: 13.87 - ft. below measuring point
Screened Interval: 61 ft. to 101 ft.
Spec. Cond. 00094: µMhos
Measuring Point is 3.27 ft. above land surface
Relative M.P. Elevation: 15.77 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling: 0.75
gallons
Appearance
here:
El
Samoles for metals were collected unfiltered: ® YES
❑ NO and field acidified: ® YES ❑ NO
Date sample analyzed: 7/17/24-7/29/24
Laboratory Name:
SGS North America Inc. / Hart & Hickman (pH) Certification No. 487 / 5356
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg/L
Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616
/100mL
Nitrate (NO3) as N 00620
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 656
mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
TOC 00680
mg/L
Ca - Calcium 00916
. mg/L
Chloride 00940 146
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
10 U ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
100 U ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑ Yes (0) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
method #
Total Ammonia 00610
mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese o1o55
ug/L
, method #
TKN as N 00625
mg/L
Ni - Nickel 01067
10 U ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs mg/L Effluent Total VUGs: mg/L vUL, Kemoval ro

SUBMIT FORM ON YELLOW PAPER ONLY
OEPARTIt1ENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING.
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION PAmw Print Clearly or Type
PERMIT Number: Expiration Date: 4/30/2028
Facility Name: Elementis Chromium Castle Hayne Manufacturing Facility
Non -Discharge UIC
Permit Name (if different): Occidental Chemical Corporation
NPDES Other WQ0001492
Facility Address: 5408 Holly Shelter Rd
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Castle Ha ne INC 28249 County New Hanover
❑ Spray Field ❑ Remediation:
Contact Person: Teresa Jordan
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: 34'22'18.4900",-077*51'46.3100"
No. of wells to be sampled: 24
❑ Water Source Heat Pump Other: Surface Disposal of Residuals
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-27 / CPW-7D
Date sample collected: 7/16/2024
FIELD ANALYSES:
WAS
Well Depth: 98 ft.
Well Diameter: 4 in.
pH 00400: 6.73 units Temp. 000lo: °C
DRY at
Depth to Water Level 82546: 11.95 ft. below measuring point
Screened Interval: 58 ft. to
98 ft. Spec. Cond. 00094: µMhos
time ofsampling,
Measuring Point is 0.09 ft. above land surface
Relative M.P. Elevation: 14.59 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling: 0.75
gallons
Appearance
here:❑
Sampies for metals were collected unfiltered: ® YES
❑ NO and field acidified: ® YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 7/16/24-7/29/24
Laboratory Name: SGS North America Inc. / Hart & Hickman H Certification No. 487 / 5356
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 1100mL
Nitrate (NO3) as N 00620
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 906 mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC oo66o mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 19.5 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034 10 U
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 6.130
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0)
pecific Conductance 00095 µMhos
K - Potassium 00937
mg/L method #
Total Ammonia 00610 mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625 mg/L
Ni - Nickel 01067 10 U
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Steve Hart, PG, Principal. Hart & Hickman, PC Authorized Agent)
Permittee (or Authorized Aqent) Name and Title - Please print or type
GW-59 Rev.8/2013
re of Pemnittee for Authorizednt)I
1(2,
017P}

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 4/30/2028
Facility Name: Elementis Chromium Castle Ha ne Manufacturing Facility
Non -Discharge UIC
Permit Name (if different): Occidental Chemical Corporation
NPDES Other W00001492
Facility Address: 5408 Holly Shelter Rd
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Castle Ha ne NC 28249 County New Hanover
❑ Spray Field ❑ Remediation:
Contact Person: Teresa Jordan
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: 34°22'03.3000".-077°51'56.8900"
No. of wells to be sampled: 24
❑ Water Source Heat Pump ❑>It Other: Surface Disposal of Residuals
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-28 / CPW-12S
Date sample collected: 7/16/2024
FIELD ANALYSES:
WAS
Well Depth: 34 ft.
Well Diameter: 4 in.
pH 00400: 6.69 units Temp. 000lo: °C
DRY at
Depth to Water Level 82546: 7.92 ft. below measuring point
Screened Interval: 19 ft to
34 ft. Spec. Cond. 000sa: µMhos
time of sampling,
Measuring Point is 0.81 ft. above land surface
Relative M.P. Elevation: 14.11 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling: 0.75
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: fit❑ YES
❑ NO and Feld acidified: ® YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 7/16/24-7/29/24
Laboratory Name: SGS North America Inc. / Hart & Hickman H Certification No. 487 / 5356
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 980 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
TOC 00680 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 4.00 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034 10 U
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 7.940
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0)
Specific Conductance 00095 µMhos
K - Potassium 00937
mg/L method #
Total Ammonia 00610 mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625 mg/L
Ni - Nickel 01067 IOU
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs. mg/L Effluent Total VOCs: mg/L VOC Removal%
GW-59 Rev.8/2013

APPROXIMATE
- 0 600 1,200
- - SCALE IN FEET
NORTHEAST CAPE FEAR RIVER
�.\ STURGEON
CREEK
R/VERSw / \ \ MW-20/CPW-10S - _MW`/CPW-9S' \.
AMP r MW-9/CPW-9D
1 /
�:�.. MW-10/CPW-10D \tea /vORcl
/I I
MW-3/CPW-15S' ` ...
�RTIN-MARIETTA MW-15/CPW-15D
I / /- / - �� \
AGGREGATES
PROPERTY / �`M
r I I�MW-14/CPW-14D
MW-2/CPW-14S
d
QUARRY SECTION #2
APPROXIMATELY 70 ACRESRE-ROUTED
/
STURGEON CREEK \ \% �/ MW-28/CPS
-' MW-13/CPW-13D ya
�CANAL-___j *MW-1/CPW-13S
MARTI N-MARI ETTA
AGGREGATES PROPERTY
PROPERTY LINE
SURFACE WATER FEATURE
- - - - - - - QUARRY LIMITS (RESIDUALS SURFACE DISPOSAL UNITS)
— — — — COMPLIANCE BOUNDARY
— — — REVIEW BOUNDARY
MTMTMTMTMTMTMTMTM'TM�TMTM'* RAILROAD TRACKS
UPPER AQUIFER (SHALLOW) MONITOR WELL
o LOWER AQUIFER (DEEP) MONITOR WELL
LCW-1 D \
�.:.... ... Ri�ER
WELL IDENTIFICATION LIST
SDR PERMIT ID
FACILITY ID
MW-1
CPW-13S
MW-2
CPW-14S
MW-3
CPW-15S
MW-8
CPW-8DR
MW-9
CPW-9D
MW-10
CPW-10D
MW-11
CPW-1S
MW-12
CPW-12D
MW-13
CPW-13D
MW-14
CPW-14D
MW-15
CPW-15D
MW-16
CPW-6S
MW-17
CPW-7S
MW-18
CPW-8S
MW-19
CPW-9S
MW-20
CPW-10S
MW-21
CPW-5S
MW-22
CPW-2D
MW-23
CPW-3D
MW-24
CPW4D
MW-25
CPW-5D
MW-26
CPW-6D
MW-27
CPW-7D
MW-28
CPW-12S
ER SWAMP
6

Summary of Affected Wells (Pagel of 2)
Elementis Chromium Castle Hayne Manufacturing Facility
Castle Hayne, NC
H&H Job No. OXY-004
Well ID
Sample Date
pH
(a. u.)
TDS
(mg/L)
Chloride
(mg/L)
Chromium
(pg/L)
Iron
(pg/L)
Nickel
(pg/L)
NC 2L Standard'
6.5-8.5
500
250
10
300
100
Site -Specific Standard
NE
NE
NE
NE
3,300 / 7,300 / 10,500
NE
11/01/21
6.09
772
6.47
4 U
22,600
2 U
07/05/22
6.58
844
6.77
4 U
23,900
2 U
MW-1 / CPW-13S
11/09/22
5.95
796
6.22
4 U
24 500
2 U
07/25/23
6.36
752
6.44
0.615 J
21,200
0.624 J
11/13/23
6.37
780
7.17
0.251 U
25 000
0.486 J
07/15/24
6.81
842
6.4
10 U
20,400
10 U
11/04/21
6.95
782
167
4 U
4,580
2 U
07/05/22
7.17
830
166
4 U
3 500
2 U
MW-2/CPW-14S
11/08/22
6.93
770
161
4U
4,350
2U
07/24/23
6.93
696
160
0.489 J
3 920
0.326 J
11/15/23
7.17
696
166
0.251 U
3,550
0.605 J
07/17/24
6.80
878
148
10 U
3,100
10 U
11/04/21
7.75
518
148
4 U
1,590
2 U
07/05/22
7.33
760
169
4 U
200 U
4.53
MW-3 / CPW-15S
11/08/22
6.88
720
166
4 U
200 0
6.07
07/24/23
7.22
920
177
0.481 J
50 U
6.06
11/15/23
7.28
996
182
0.702 J
352
4.95
07/16/24
7.20
1,240
162
10 U
100 U
10 U
11/03/21
6.92
808
207
4 U
446
2 U
07/06/22
7.39
796
223
6.14
453
2 U
MW-8 / CPW-8DR
11/09/22
6.89
752
193
4 U
453
2 U
07/25/23
7.13
772
208
1.09 J
337
0.304 J
11/14/23
7.48
722
197
0.406 J
355
0.386 J
07/17/24
7.02
800
233
10 U
1,520
10 U
11/03/21
6.77
1,630
220
4.11
200 U
2 U
07/06/22*
7.33
1,580
219
4.47
200 U
2 U
MW-9 / CPW-9D
11/08/22
6.91
1,550
214
4.06
200 U
3.05
07/25/23
6.96
1,410
208
3.57 J
50 U
1.35 J
11/14/23
6.82
1,430
210
3.93 J
50 U
1.71 J
07/17/24
7.13
1,650
211
10 U
100 U
10 U
11/03/21
9.83
1,100
112
5.08
200 U
2 U
07/06/22
9.33
1,250
182
4 U
200 U
2 U
MW-10 / CPW-10D
11/08/22
9.25
1,230
141
4 U
200 U
10.2
07/24/23
8.98
1,040
189
11.1
83.3 J
1.58 J
11/14/23
8.93
984
149
3.55 J
50 U
1.26 J
07/16/24
9.28
1,310
160
10 U
100 U
10 U
11/01/21
6.36
420
4.78
4 U
9,510
2 U
07/04/22
6.68
408
5.25
4 U
10,000
2 U
MW-11 / CPW-1S
11/10/22
6.51
374
4.79
4 U
12,600
2 U
07/26/23
6.54
398
4.56
1.95 J
13,800
0.422 J
11/15/23
6.72
280
4.88
1.38 J
10,200
0.248 J
07/15/24
6.74
484
5.1
10 U
11,700
10 U
11/03/21
6.64
796
4.94
4 U
2 U
07/05/22
7.33
770
4.85
4 U
2 U
MW-12 / CPW-12D
11/09/22
6.88
754
4.57
4 U
2 U
07/26/23
6.64
786
4.79
0.828 J
1.20 J
11/13/23
6.49
668
4.93
0.251 U
E858
1.06 J
07/15/24
6.93
896
4.7
10 U
10U
11/01/21
6.55
1100
158
4 U
2 U
07/05/22
6.96
1 180
150
4 U
2 U
MW-13 / CPW-13D
11/09/22
6.40
1200
151
4 U
2 U
07/25/23
6.63
1,280
157
1.15 J
539
0.667 J
11/13/23
6.47
992
167
1.15 J
544
0.305 J
07/15/24
6.80
1,390
155
10 U
298
10 U
11/04/21
6.73
1,430
173
4 U
3,020
2 U
07/05/22
7.00
1,530
173
69.6
2 960
2 U
08/01/22
7.21
4 U
MW-14 / CPW-14D
11/08/22
6.84
1,580
168
4 U
2 900
2 U
07/24/23
6.78
1,400
170
0.781 J
2,430
0.559 J
11/15/23
6.54
1,340
177
6.34 J
2,720
0.603 J
07/17/24
6.80
1,510
164
10 U
2,340
10 U
11/04/21
6.97
602
118
4 U
200 U
2 U
07/05/22
7.26
612
121
5.39
200 U
2 U
MW-15 / CPW-15D
11/08/22
7.03
592
122
4 U
200 U
2 U
07/24/23
7.02
584
146
0.880 J
50 U
0.403 J
11/15/23
6.65
520
145
0.251 U
50 U
0.192 J
07/16/24
7.28
796
129
10 U
100 U
10 U
11/04/21
6.12
862
63.7
4 U
200 U
2 U
07/07/22
6.60
1,050
88.2
4.67
200 U
2 U
MW-16 / CPW-6S
11/09/22
6.02
1,170
51.4
4 U
200 U
2 U
07/26/23
6.19
932
80.0
3.54 J
50 U
0.912 J
11/15/23
6.43
738
60.7
3.06 J
50 U
0.572 J
07/17/24
6.72
1,440
174
10 U
100 U
10 U
09/20/21
6.99
7,280 / 7,050
134 / 136
11/04/21
6.80
724
6.86
4 U
6,210
125
07/04/22
7.24
1,290
7.85
10.8
13,300
59.4
MW-17 / CPW-7S
08/01/22
7.34
-
-
4 U
-
--
11/10/22
7.18
1,050
7.03
4 U
19,900
20.8
07/25/23
6.96
2,450
5.05
0.401 J
6,500
38.0
11/14/23
7.54
2,690
5.24
4.02
26,800
22.1
07/16/24
7.00
2,900
6.0
10 U
10,200
14.1
08/12/21
7.62
5U/10U
50U/100U
11/03/21
6.96
326
79.2
4 U
200 U
2 U
07/06/22
7.55
380
92.8
30.1
200 U
2 U
MW-18 / CPW-8S
08/01/22
7.51
-
-
4 U
-
--
11/09/22
6.93
392
99.5
4 U
200 U
2 U
07/25/23
7.09
780
96.5
1.06 J
50 U
0.456 J
11/14/23
7.59
686
95.0
11.0
134 J
0.393 J
07/17/24
7.30
666
63.4
1 10 U
100 U
10 U
Attachment A (Page 1 of 2)
Hart & Hickman, PC

Summary of Affected Wells (Page 2 of 2)
Elementis Chromium Castle Hayne Manufacturing Facility
Castle Hayne, NC
H&H Job No. OXY-004
Well ID
Sample Date
pH
(a. U.)
TDS
(mg/L)
Chloride
(mg/L)
Chromium
(pg/L)
Iron
(pg/L)
Nickel
(pg/L)
NC 2L Standard'
6.5-8.5
500
250
10
300
100
Site -Specific Standard
NE
NE
NE
NE
3,300 / 7,300 / 10,500
NE
11/03/21
7.65
332
69.5
4 U
200 U
2 U
07/06/22*
7.20
376
49.1
4 U
442
2 U
MW-19 / CPW-9S
11/08/22
7.55
418
78.4
31.7
557
2 U
07/25/23
6.66
310
0.966
1.67 J
563
2.15
11/14/23
7.86
400
86.1
1.10 J
356
0.318 J
07/17/24
7.04
502
50.8
10 U
1,020
10 U
11/03/21
6.26
450
65.5
4 U
200 U
2 U
07/06/22
7.12
470
78.0
4 U
200 U
2 U
MW-20 / CPW-10S
11/08/22
6.38
428
74.2
4 U
200 U
2 U
07/24/23
6.56
418
76.8
1.81 J
50 U
0.344 J
11/14/23
6.97
426
80.1
2.94 J
328
0.412 J
07/16/24
7.01
570
64.9
1 o U
100 U
1 o U
11/02/21
6.94
976
132
5.89
90
2 U
07/06/22
7.40
896
128
6.21
60
2.06
MW-21 / CPW-5S
11/09/22
6.97
950
124
5.39
4
22 U
07/26/23
7.03
868
130
4.95
40
1.80 J
11/15/23
6.91
756
135
6.45
50
04750
2.13
07/17/24
7.30
966
123
10 U80
10 U
11/01/21
6.69
426
11.7
4 U
2 U
07/04/22
7.02
514
12.4
6.74
10
2 U
MW-22 / CPW-2D
11/10/22
6.66
516
12.2
4 U
480
2 U
07/26/23
6.55
534
12.3
1.13 J
4,170
0.405 J
11/15/23
6.97
434
12.7
0.849 J
4,670
0.285 J
07/15/24
6.90
554
11.6
1 o U
4 550
1 o U
11/01/21
6.39
582
33.2
4 U
3,030
2 U
07/04/22
7.21
612
31.3
11.0
3 290
2 U
08/01/22
6.92
4 U
MW-23 / CPW-3D
11/10/22
6.90
576
31.0
4 U
3 250
2 U
07/26/23
6.69
582
32.2
0.768 J
2,850
0.520 J
11/15/23
6.68
498
34.1
0.644 J
3,260
0.342 J
07/16/24
6.93
572
32.9
10 U
1,320
10 U
11/01/21
6.45
488
53.9
1,840
200 U
2.12
07/04/22
6.98
516
69.8
1,270
200 U
2 U
MW-24 / CPW-4D
11/10/22
6.72
496
64.8
1,510
200 U
2.13
07/26/23
6.81
512
66.9
1,340
50 U
1.85 J
11/15/23
6.51
432
61.5
2,880
50 U
2.60 J
07/17/24
6.75
630
53.7
3,780
100 U
10 U
11/02/21
7.35
1,670
605
4 U
200 U
3.05
07/06/22
7.86
1 640
602
4 U
200 U
2.64
MW-25 / CPW-5D
11/09/22
7.52
1 480
589
4 U
200 U
3.33
07/26/23
7.81
2020
619
1.16 J
50 U
3.37
11/15/23
8.06
1 230
628
2.51 J
50 U
3.50
07/17/24
7.70
1 710
567
10 U
100 U
10 U
11/02/21
10.61
374
113
4 U
200 U
2 U
07/07/22
10.23
344
125
4 U
200 U
2 U
11/09/22
9.51
388
136
4 U
200 U
2 U
MW-26 / CPW-6D
07/26/23
9.14
498
147
0.444 J
50 U
0.457 J
11/15/23
8.59
568
163
6.97
143 J
0.557 J
07/17/24
9.23
656
146
10 U
100 U
10 U
11/04/21
6.68
960
14.7
4 U
3,370
2 U
07/04/22
6.97
964
15.4
7.14
8,000
2 U
11/10/22
6.66
904
19.0
4 U
8,250
2 U
MW-27 / CPW-7D
07/26/23
6.72
858
15.0
1.13 J
8,160
0.886 J
11/14/23
6.72
792
15.7
0.753 J
6,720
0.395 J
07/16/24
6.73
906
19.5
10 U
6130
10 U
11/03/21
6.73
1 1,720
5.19
4 U
13,800
2 U
07/05/22
7.06
1,120
3.46
4 U
7,630
2 U
MW-28 / CPW-12S
11/09/22
6.64
1,330
3.58
4 U
12,000
2 U
07/25/23
6.92
804
3.74
0.543 J
7,030
0.679 J
11/14/23
6.50
826
4.29
6.03
7 890
0.512 J
07/16/24
6.69
980
4.0
10 U
7, 940
1 o U
Notes
15A NCAC 02L.0202 Ground Water Quality Standard
2 Site -specific target cleanup concentrations for iron are included in the DW R-approved May 28, 1999 I -CAP for remediation of compounds of concern above standards by processes of natural
attenuation pursuant to 15A NCAC 2L .0106(I). The target cleanup concentrations for iron are background levels established under a now -expired Special Order by Consent (SOC) agreement.
The site -specific target iron levels in the I -CAP are: 3.3 mg/L for Lower Aquifer Wells, 7.3 mg/L for Upper Aquifer non -Fluvial Deposits Wells, and 10.4 mg/L for Upper Aquifer Fluvial Deposits
Wells. CPW-1 S, CPW-7S, and CPW-12S wells are classified as Upper Aquifer non -Fluvial Deposits Wells. The remaining Upper Aquifer wells are classified as Upper Aquifer Fluvial Deposits
Wells.
mg/L = milligrams per liter; pg/L = micrograms per liter; U = not detected at the associated reporting limit; '-" indicates not analyzed; NE = not established
J-flag indicates estimated concentration detected above the laboratory minimum detection limit and belowthe reporting limit
Bold concentration exceeds the groundwater standard (site -specific standard for iron)
Data for permit compliance samples collected during the last three years included in table
* July 2022 MW-9/CPW-9D data presented in table are the laboratory reported MW-19/CPW-9S results, and vice versa. Based on previous data, it appears the reported data for each well was
reversed.
Attachment A (Page 2 of 2)
Hart & Hickman, PC

i0m
Scott, LA
The results set forth herein are provided by SGS North America Inc.
Technical Report for
GHD Services Inc.
GSHI:SDR Compliance Monitoring
SGS Job Number: LB4543
Sampling Dates: 07/15/24 - 07/17/24
Report to:
GHD Services Inc.
2055 Niagara Falls Blvd, Suite #3
Niagara Falls, NY 14304
[e-mail]; sheri.finn@
sdrury @ harthickman. com
ATTN: Sheri Finn
Total number of pages in report: 87
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable unless noted
in the narrative, comments or footnotes.
e Hardcopy 2.0
Automated Report
com;
4valu
BagawandossDirector North America
Client Service contact: Rebecca Hebert 337-237-4775
Certifications: LDEQ(2048), LDHH(LA150012), AR(14-045-04), AZ(AZ0805), FL(E87657), IL(200082), KY(#31),
NC(487), SC(73004001), NJ(LA007), TX(T104704186-18-16), WV(257)
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 500 Ambassador Caffery • Scott, LA 70583 • tel: [phone]
SGS is the sole authority for authorizing edits or modifications to this document. Please share your ideas about
Unauthorized modification of this report is strictly prohibited. how we can serve you better at:
Review standard terms at: http://www.sgs.com/en/terms-and-conditions [e-mail]
1 of 87
LB4543

August 7, 2024
GHD Services Inc.
2055 Niagara Falls Blvd
Niagara Falls, NY 14304
RE: SGS Job LB4543
The final report for SGS Job LB4543 has been amended from the original. This report replaces in its
entirety any previously submitted copy. Client Ids have been amended as per client request. The
attached report includes these revisions.
Please contact me at 337-237-4775 if I may be of further assistance in this matter, or if you have any
further questions regarding this data report.
Sincerely,
Rebecca Hebert
SGS North America Inc. -Scott
SGS North America Inc. Scott, LA 1 500 Ambassador Caffery Parkway Scott, LA 70583, USA t [phone] www.sgs.com
Member of the SGS Group (SGS SA)
� 2 of 87
LB4543

Sections:
Table of Contents
-I-
Section1: Sample Summary...................................................................................................
4
Section2: Summary of Hits....................................................................................................
6
Section3: Sample Results........................................................................................................
10
3.1: LB4543-1: MW-11/CPW-1S........................................................................................
11
3.2: LB4543-2: MW-22/CPW-2D........................................................................................
13
3.3: LB4543-3: MW-23/CPW-3D........................................................................................
15
3.4: LB4543-4: MW-24/CPW-4D........................................................................................
17
3.5: LB4543-5: MW-21/CPW-5S........................................................................................
19
3.6: LB4543-6: MW-25/CPW-5D........................................................................................
21
3.7: LB4543-7: MW-16/CPW-6S........................................................................................
23
3.8: LB4543-8: MW-26/CPW-6D........................................................................................
25
3.9: LB4543-9: MW-17/CPW-7S........................................................................................
27
3.10: LB4543-10: MW-27/CPW-7D....................................................................................
29
3.11: LB4543-11: MW-18/CPW-8S.....................................................................................
31
3.12: LB4543-12: MW-8/CPW-8DR...................................................................................
33
3.13: LB4543-13: MW-19/CPW-9S....................................................................................
35
3.14: LB4543-14: MW-9/CPW-9D......................................................................................
37
3.15: LB4543-15: MW-20/CPW-lOS..................................................................................
39
3.16: LB4543-16: MW-10/CPW-lOD..................................................................................
41
3.17: LB4543-17: MW-28/CPW-12S..................................................................................
43
3.18: LB4543-18: MW-12/CPW-12D..................................................................................
45
3.19: LB4543-19: MW-1/CPW-13S....................................................................................
47
3.20: LB4543-20: MW-13/CPW-13D..................................................................................
49
3.21: LB4543-21: MW-2/CPW-14S....................................................................................
51
3.22: LB4543-22: MW-14/CPW-14D..................................................................................
53
3.23: LB4543-23: MW-3/CPW-15S....................................................................................
55
3.24: LB4543-24: MW-15/CPW-15D..................................................................................
57
3.25: LB4543-25: DUP-1....................................................................................................
59
3.26: LB4543-26: DUP-2....................................................................................................
61
Section4: Misc. Forms............................................................................................................
63
4.1: Chain of Custody...........................................................................................................
64
Section 5: Metals Analysis - QC Data Summaries................................................................
70
5.1: Prep QC MP28647: Cr,Fe,Ni.........................................................................................
71
5.2: Prep QC MP28648: Cr,Fe,Ni.........................................................................................
78
Section 6: General Chemistry - QC Data Summaries..........................................................
83
6.1: Method Blank and Spike Results Summary..................................................................
84
6.2: Duplicate Results Summary..........................................................................................
85
6.3: Matrix Spike Results Summary.....................................................................................
86
6.4: Matrix Spike Duplicate Results Summary....................................................................
87
m

SGS North America Inc.
Sample Summary
GHD Services Inc.
GSHI: SDR Compliance Monitoring
Job No: LB4543
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
LB4543-1
07/15/24
15:20HW/AW7/18/24
AQ
Ground Water
MW-II/CPW-1S
LB4543-2
07/15/24
16:31 HW/AW7/18/24
AQ
Ground Water
MW-22/CPW-2D
LB4543-3
07/16/24
10:05 HW/AW7/ 18/24
AQ
Ground Water
MW-23/CPW-3D
LB4543-4
07/17/24
15:39 HW/AW7/ 18/24
AQ
Ground Water
MW-24/CPW-4D
LB4543-5
07/17/24
13:00HW/AW7/18/24
AQ
Ground Water
MW-21/CPW-5S
LB4543-6
07/17/24
13:06 HW/AW7/ 18/24
AQ
Ground Water
MW-25/CPW-5D
LB4543-7
07/17/24
13:51 HW/AW7/18/24
AQ
Ground Water
MW-16/CPW-6S
LB4543-8
07/17/24
13:50 HW/AW7/ 18/24
AQ
Ground Water
MW-26/CPW-6D
LB4543-9
07/16/24
12:29 HW/AW7/18/24
AQ
Ground Water
MW-17/CPW-7S
LB4543-10
07/16/24
13:20HW/AW7/18/24
AQ
Ground Water
MW-27/CPW-7D
LB4543-11
07/17/24
11:32 HW/AW7/18/24
AQ
Ground Water
MW-18/CPW-8S
LB4543-12
07/17/24
11:31 HW/AW7/18/24
AQ
Ground Water
MW-8/CPW-8DR
LB4543-13
07/17/24
10:41 HW/AW7/18/24
AQ
Ground Water
MW-19/CPW-9S
�
4 of 87
LB4543

SGS North America Inc.
Sample Summary
(continued)
GHD Services Inc.
GSHI: SDR Compliance Monitoring
Job No: LB4543
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
LB4543-14
07/17/24
10:42 HW/AW7/ 18/24
AQ
Ground Water
MW-9/CPW-9D
LB4543-15
07/16/24
16:32 HW/AW7/18/24
AQ
Ground Water
MW-20/CPW-IOS
LB4543-16
07/16/24
16:04HW/AW7/18/24
AQ
Ground Water
MW-10/CPW-IOD
LB4543-17
07/16/24
13:48 HW/AW7/18/24
AQ
Ground Water
MW-28/CPW-12S
LB4543-18
07/15/24
13:16 HW/AW7/18/24
AQ
Ground Water
MW-12/CPW-12D
LB4543-19
07/15/24
12:44 HW/AW7/18/24
AQ
Ground Water
MW-1/CPW-13S
LB4543-20
07/15/24
12:11 HW/AW7/18/24
AQ
Ground Water
MW-13/CPW-13D
LB4543-21
07/17/24
09:35 HW/AW7/18/24
AQ
Ground Water
MW-2/CPW-14S
LB4543-22
07/17/24
09:30HW/AW7/18/24
AQ
Ground Water
MW-14/CPW-14D
LB4543-23
07/16/24
14:54HW/AW7/18/24
AQ
Ground Water
MW-3/CPW-15S
LB4543-24
07/16/24
15:01 HW/AW7/18/24
AQ
Ground Water
MW-15/CPW-15D
LB4543-25
07/16/24
00:00 HW/AW7/18/24
AQ
Ground Water
DUP-1
LB4543-26
07/17/24
00:00 HW/AW7/ 18/24
AQ
Ground Water
DUP-2
�
5 of 87
LB4543

Summary of Hits
Job Number:
LB4543
Account:
GHD Services Inc.
Project:
GSHLSDR Compliance Monitoring
Collected:
07/ 15/24 thru 07/ 17/24
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
LB4543-1 MW-11/CPW-1S
Iron
11700
100
ug/1
EPA 200.7
Chloride
5.1
0.25
mg/1
EPA 300
Solids, Total Dissolved
484
2.5
mg/1
SM2540 C-I I
LB4543-2 MW-22/CPW-2D
Iron
4550
100
ug/1
EPA 200.7
Chloride
11.6
0.50
mg/1
EPA 300
Solids, Total Dissolved
554
2.5
mg/1
SM2540 C-I I
LB4543-3 MW-23/CPW-3D
Iron
1320
100
ug/1
EPA 200.7
Chloride
32.9
2.5
mg/1
EPA 300
Solids, Total Dissolved
572
2.5
mg/1
SM2540 C-I I
LB4543-4 MW-24/CPW-4D
Chromium
3780
10
ug/1
EPA 200.7
Chloride
53.7
2.5
mg/1
EPA 300
Solids, Total Dissolved
630
2.5
mg/1
SM2540 C-I I
LB4543-5 MW-21/CPW-5S
Iron
1580
100
ug/1
EPA 200.7
Chloride
123
2.5
mg/1
EPA 300
Solids, Total Dissolved
966
2.5
mg/1
SM2540 C-I I
LB4543-6 MW-25/CPW-5D
Chloride
567
13
mg/1
EPA 300
Solids, Total Dissolved
1710
2.5
mg/1
SM2540 C-I I
LB4543-7 MW-16/CPW-6S
Chloride
174
2.5
mg/1
EPA 300
Solids, Total Dissolved
1440
2.5
mg/1
SM2540 C-I I
LB4543-8 MW-26/CPW-6D
Chloride
146
2.5
mg/l
EPA 300
Solids, Total Dissolved
656
2.5
mg/1
SM2540 C-I I
Page 1 of 4
�
6 of 87
LB4543

Summary of Hits
Job Number:
LB4543
Account:
GHD Services Inc.
Project:
GSHLSDR Compliance Monitoring
Collected:
07/ 15/24 thru 07/ 17/24
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
LB4543-9 MW-17/CPW-7S
Iron
10200
100
ug/1
EPA 200.7
Nickel
14.1
10
ug/1
EPA 200.7
Chloride
6.0
1.3
mg/1
EPA 300
Solids, Total Dissolved
2900
2.5
mg/1
SM2540 C-I I
LB4543-10 MW-27/CPW-7D
Iron
6130
100
ug/1
EPA 200.7
Chloride
19.5
0.50
mg/1
EPA 300
Solids, Total Dissolved
906
2.5
mg/1
SM2540 C-I I
LB4543-11 MW-18/CPW-8S
Chloride
63.4
1.3
mg/1
EPA 300
Solids, Total Dissolved
666
2.5
mg/1
SM2540 C-I I
LB4543-12 MW-8/CPW-8DR
Iron
1520
100
ug/1
EPA 200.7
Chloride
233
6.3
mg/1
EPA 300
Solids, Total Dissolved
800
2.5
mg/1
SM2540 C-I I
LB4543-13 MW-19/CPW-9S
Iron
1020
100
ug/1
EPA 200.7
Chloride
50.8
1.3
mg/1
EPA 300
Solids, Total Dissolved
502
2.5
mg/1
SM2540 C-I I
LB4543-14 MW-9/CPW-9D
Chloride
211
6.3
mg/1
EPA 300
Solids, Total Dissolved
1650
2.5
mg/1
SM2540 C-I I
LB4543-15 MW-20/CPW-IOS
Chloride
64.9
2.5
mg/1
EPA 300
Solids, Total Dissolved
570
2.5
mg/1
SM2540 C-I I
LB4543-16 MW-10/CPW-IOD
Chloride
160
2.5
mg/l
EPA 300
Solids, Total Dissolved
1310
2.5
mg/1
SM2540 C-I I
Page 2 of 4
�
7 of 87
LB4543

Summary of Hits
Job Number:
LB4543
Account:
GHD Services Inc.
Project:
GSHLSDR Compliance Monitoring
Collected:
07/ 15/24 thru 07/ 17/24
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
LB4543-17 MW-28/CPW-12S
Iron
7940
100
ug/1
EPA 200.7
Chloride
4.0
0.25
mg/1
EPA 300
Solids, Total Dissolved
980
2.5
mg/1
SM2540 C-I I
LB4543-18 MW-12/CPW-12D
Iron
8580
100
ug/1
EPA 200.7
Chloride
4.7
0.25
mg/1
EPA 300
Solids, Total Dissolved
896
2.5
mg/1
SM2540 C-I I
LB4543-19 MW-1/CPW-13S
Iron
20400
100
ug/1
EPA 200.7
Chloride
6.4
0.25
mg/1
EPA 300
Solids, Total Dissolved
842
2.5
mg/1
SM2540 C-I I
LB4543-20 MW-13/CPW-13D
Iron
298
100
ug/1
EPA 200.7
Chloride
155
2.5
mg/1
EPA 300
Solids, Total Dissolved
1390
2.5
mg/1
SM2540 C-I I
LB4543-21 MW-2/CPW-14S
Iron
3100
100
ug/1
EPA 200.7
Chloride
148
2.5
mg/1
EPA 300
Solids, Total Dissolved
878
2.5
mg/1
SM2540 C-I I
LB4543-22 MW-14/CPW-14D
Iron
2340
100
ug/1
EPA 200.7
Chloride
164
2.5
mg/1
EPA 300
Solids, Total Dissolved
1510
2.5
mg/1
SM2540 C-I I
LB4543-23 MW-3/CPW-15S
Chloride
162
2.5
mg/1
EPA 300
Solids, Total Dissolved
1240
2.5
mg/1
SM2540 C-I I
LB4543-24 MW-15/CPW-15D
Chloride
129
2.5
mg/1
EPA 300
Solids, Total Dissolved
796
2.5
mg/1
SM2540 C-I I
Page 3 of 4
�
8 of 87
LB4543

Summary of Hits
Job Number:
LB4543
Account:
GHD Services Inc.
Project:
GSHLSDR Compliance Monitoring
Collected:
07/ 15/24 thru 07/ 17/24
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
LB4543-25 DUP-1
Chloride
162
2.5
mg/1
Solids, Total Dissolved
718
2.5
mg/1
LB4543-26 DUP-2
Chloride
65.5
1.3
mg/l
Solids, Total Dissolved
620
2.5
mg/1
EPA 300
SM2540 C-I I
EPA 300
SM2540 C-I I
Page 4 of 4
� 9 of 87
LB4543

sw�
Scott, LA
Section 3
Sample Results
Report of Analysis
� 10 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-11/CPW-IS
Lab Sample ID: LB4543-1 Date Sampled: 07/15/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1 j
Total Metals Analysis
Analyte Result RL
Units DF
Prep
Analyzed By
Method
Prep Method
Chromium < 10 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
Iron 11700 100
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
Nickel < 10 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
(1) Instrument QC Batch: MA28090
(2) Prep QC Batch: MP28647
RL = Reporting Limit
� 11 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-11/CPW-IS
Lab Sample ID: LB4543-1 Date Sampled: 07/15/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1 j
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chloride 5.1 0.25 mg/1 1 07/29/24 00:32 BD EPA 300
Solids, Total Dissolved 484 2.5 mg/1 1 07/ 18/24 13:49 xF SM2540 C-11
RL = Reporting Limit
� 12 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-22/CPW-2D
Lab Sample ID: LB4543-2 Date Sampled: 07/15/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1 N
Total Metals Analysis
Analyte Result RL
Units DF
Prep
Analyzed By
Method
Prep Method
Chromium < 10 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
Iron 4550 100
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
Nickel < 10 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
(1) Instrument QC Batch: MA28090
(2) Prep QC Batch: MP28647
RL = Reporting Limit
� 13 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-22/CPW-2D
Lab Sample ID: LB4543-2 Date Sampled: 07/15/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1 N
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chloride 11.6 0.50 mg/1 2 07/29/24 00:45 BD EPA 300
Solids, Total Dissolved 554 2.5 mg/1 1 07/ 18/24 13:49 xF SM2540 C-11
RL = Reporting Limit
� 14 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-23/CPW-3D
Lab Sample ID: LB4543-3 Date Sampled: 07/16/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1 w
Total Metals Analysis
Analyte Result RL
Units DF
Prep
Analyzed By
Method
Prep Method
Chromium < 10 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
Iron 1320 100
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
Nickel < 10 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
(1) Instrument QC Batch: MA28090
(2) Prep QC Batch: MP28647
RL = Reporting Limit
� 15 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-23/CPW-3D
Lab Sample ID: LB4543-3 Date Sampled: 07/16/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1 w
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chloride 32.9 2.5 mg/1 10 07/29/24 00:58 BD EPA 300
Solids, Total Dissolved 572 2.5 mg/1 1 07/ 18/24 13:49 xF SM2540 C-1 i
RL = Reporting Limit
� 16 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-24/CPW-4D
Lab Sample ID: LB4543-4 Date Sampled: 07/17/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1 P
Total Metals Analysis
Analyte Result RL
Units DF
Prep
Analyzed By
Method
Prep Method
Chromium 3780 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
Iron < 100 100
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
Nickel < 10 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
(1) Instrument QC Batch: MA28090
(2) Prep QC Batch: MP28647
RL = Reporting Limit
� 17 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-24/CPW-4D
Lab Sample ID: LB4543-4 Date Sampled: 07/17/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1 P
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chloride 53.7 2.5 mg/1 10 07/29/24 01:37 BD EPA 300
Solids, Total Dissolved 630 2.5 mg/1 1 07/ 18/24 13:49 xF SM2540 C-11
RL = Reporting Limit
� 18 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-21/CPW-5S
Lab Sample ID: LB4543-5 Date Sampled: 07/17/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1 P
Total Metals Analysis
Analyte Result RL
Units DF
Prep
Analyzed By
Method
Prep Method
Chromium < 10 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
Iron 1580 100
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
Nickel < 10 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
(1) Instrument QC Batch: MA28090
(2) Prep QC Batch: MP28647
RL = Reporting Limit
� 19 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-21/CPW-5S
Lab Sample ID: LB4543-5 Date Sampled: 07/17/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1 P
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chloride 123 2.5 mg/1 10 07/29/24 02:16 BD EPA 300
Solids, Total Dissolved 966 2.5 mg/1 1 07/ 18/24 13:49 xF SM2540 C-11
RL = Reporting Limit
� 20 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-25/CPW-5D
Lab Sample ID: LB4543-6 Date Sampled: 07/17/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
Total Metals Analysis
Analyte Result RL
Units DF
Prep
Analyzed By
Method
Prep Method
Chromium < 10 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
Iron < 100 100
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
Nickel < 10 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
(1) Instrument QC Batch: MA28090
(2) Prep QC Batch: MP28647
RL = Reporting Limit
� 21 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-25/CPW-5D
Lab Sample ID: LB4543-6 Date Sampled: 07/17/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chloride 567 13 mg/1 50 07/29/24 02:29 BD EPA 300
Solids, Total Dissolved 1710 2.5 mg/1 1 07/ 18/24 13:49 xF SM2540 C-1 i
RL = Reporting Limit
� 22 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-16/CPW-6S
Lab Sample ID: LB4543-7 Date Sampled: 07/17/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1 P
Total Metals Analysis
Analyte Result RL
Units DF
Prep
Analyzed By
Method
Prep Method
Chromium < 10 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
Iron < 100 100
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
Nickel < 10 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
(1) Instrument QC Batch: MA28090
(2) Prep QC Batch: MP28647
RL = Reporting Limit
� 23 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-16/CPW-6S
Lab Sample ID: LB4543-7 Date Sampled: 07/17/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1 P
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chloride 174 2.5 mg/1 10 07/29/24 02:41 BD EPA 300
Solids, Total Dissolved 1440 2.5 mg/1 1 07/ 18/24 13:49 xF SM2540 C-1 i
RL = Reporting Limit
� 24 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-26/CPW-6D
Lab Sample ID: LB4543-8 Date Sampled: 07/17/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1 P
Total Metals Analysis
Analyte Result RL
Units DF
Prep
Analyzed By
Method
Prep Method
Chromium < 10 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
Iron < 100 100
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
Nickel < 10 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
(1) Instrument QC Batch: MA28090
(2) Prep QC Batch: MP28647
RL = Reporting Limit
� 25 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-26/CPW-6D
Lab Sample ID: LB4543-8 Date Sampled: 07/17/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1 P
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chloride 146 2.5 mg/1 10 07/29/24 02:54 BD EPA 300
Solids, Total Dissolved 656 2.5 mg/1 1 07/ 18/24 13:49 xF SM2540 C-11
RL = Reporting Limit
� 26 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-17/CPW-7S
Lab Sample ID: LB4543-9 Date Sampled: 07/16/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
Total Metals Analysis
Analyte Result RL
Units DF
Prep
Analyzed By
Method
Prep Method
Chromium < 10 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
Iron 10200 100
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
Nickel 14.1 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
(1) Instrument QC Batch: MA28090
(2) Prep QC Batch: MP28647
RL = Reporting Limit
� 27 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-17/CPW-7S
Lab Sample ID: LB4543-9 Date Sampled: 07/16/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chloride 6.0 1.3 mg/1 5 07/29/24 03:07 BD EPA 300
Solids, Total Dissolved 2900 2.5 mg/1 1 07/ 18/24 13:49 xF SM2540 C-1 i
RL = Reporting Limit
� 28 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-27/CPW-7D
Lab Sample ID: LB4543-10 Date Sampled: 07/16/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
Total Metals Analysis
Analyte Result RL
Units DF
Prep
Analyzed By
Method
Prep Method
Chromium < 10 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
Iron 6130 100
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
Nickel < 10 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
(1) Instrument QC Batch: MA28090
(2) Prep QC Batch: MP28647
RL = Reporting Limit
� 29 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-27/CPW-7D
Lab Sample ID: LB4543-10 Date Sampled: 07/16/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chloride 19.5 0.50 mg/1 2 07/29/24 03:20 BD EPA 300
Solids, Total Dissolved 906 2.5 mg/1 1 07/ 18/24 13:49 xF SM2540 C-11
RL = Reporting Limit
� 30 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-18/CPW-8S
Lab Sample ID: LB4543-11 Date Sampled: 07/17/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
Total Metals Analysis
Analyte Result RL
Units DF
Prep
Analyzed By
Method
Prep Method
Chromium < 10 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
Iron < 100 100
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
Nickel < 10 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
(1) Instrument QC Batch: MA28090
(2) Prep QC Batch: MP28647
RL = Reporting Limit
� 31 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-18/CPW-8S
Lab Sample ID: LB4543-11 Date Sampled: 07/17/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chloride 63.4 1.3 mg/1 5 07/29/24 03:33 BD EPA 300
Solids, Total Dissolved 666 2.5 mg/1 1 07/ 18/24 13:49 xF SM2540 C-11
RL = Reporting Limit
� 32 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-8/CPW-8DR
Lab Sample ID: LB4543-12 Date Sampled: 07/17/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
Total Metals Analysis
Analyte Result RL
Units DF
Prep
Analyzed By
Method
Prep Method
Chromium < 10 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
Iron 1520 100
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
Nickel < 10 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 2
(1) Instrument QC Batch: MA28090
(2) Prep QC Batch: MP28647
RL = Reporting Limit
� 33 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-8/CPW-8DR
Lab Sample ID: LB4543-12 Date Sampled: 07/17/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chloride 233 6.3 mg/1 25 07/29/24 03:46 BD EPA 300
Solids, Total Dissolved 800 2.5 mg/1 1 07/ 18/24 13:49 xF SM2540 C-1 i
RL = Reporting Limit
� 34 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-19/CPW-9S
Lab Sample ID: LB4543-13 Date Sampled: 07/17/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
Total Metals Analysis
Analyte Result RL
Units DF
Prep
Analyzed By
Method
Prep Method
Chromium < 10 10
ug/1 1
07/ 18/24
07/22/24 RD
EPA 200.7 2
EPA 200.7 3
Iron 1020 100
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 3
Nickel < 10 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 3
(1) Instrument QC Batch: MA28090
(2) Instrument QC Batch: MA28102
(3) Prep QC Batch: MP28647
RL = Reporting Limit
� 35 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-19/CPW-9S
Lab Sample ID: LB4543-13 Date Sampled: 07/17/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chloride 50.8 1.3 mg/1 5 07/29/24 04:25 BD EPA 300
Solids, Total Dissolved 502 2.5 mg/1 1 07/ 18/24 13:49 xF SM2540 C-1 i
RL = Reporting Limit
� 36 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-9/CPW-9D
Lab Sample ID: LB4543-14 Date Sampled: 07/17/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
Total Metals Analysis
Analyte Result RL
Units DF
Prep
Analyzed By
Method
Prep Method
Chromium < 10 10
ug/1 1
07/ 18/24
07/22/24 RD
EPA 200.7 2
EPA 200.7 3
Iron < 100 100
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 3
Nickel < 10 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 3
(1) Instrument QC Batch: MA28090
(2) Instrument QC Batch: MA28102
(3) Prep QC Batch: MP28647
RL = Reporting Limit
� 37 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-9/CPW-9D
Lab Sample ID: LB4543-14 Date Sampled: 07/17/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chloride 211 6.3 mg/1 25 07/29/24 04:38 BD EPA 300
Solids, Total Dissolved 1650 2.5 mg/1 1 07/ 18/24 13:49 xF SM2540 C-1 i
RL = Reporting Limit
� 38 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-20/CPW-IOS
Lab Sample ID: LB4543-15 Date Sampled: 07/16/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
Total Metals Analysis
Analyte Result RL
Units DF
Prep
Analyzed By
Method
Prep Method
Chromium < 10 10
ug/1 1
07/ 18/24
07/22/24 RD
EPA 200.7 2
EPA 200.7 3
Iron < 100 100
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 3
Nickel < 10 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 3
(1) Instrument QC Batch: MA28090
(2) Instrument QC Batch: MA28102
(3) Prep QC Batch: MP28647
RL = Reporting Limit
� 39 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-20/CPW-IOS
Lab Sample ID: LB4543-15 Date Sampled: 07/16/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chloride 64.9 2.5 mg/1 10 07/29/24 04:50 BD EPA 300
Solids, Total Dissolved 570 2.5 mg/1 1 07/ 18/24 13:49 xF SM2540 C-1 i
RL = Reporting Limit
� 40 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-10/CPW-IOD
Lab Sample ID: LB4543-16 Date Sampled: 07/16/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
Total Metals Analysis
Analyte Result RL
Units DF
Prep
Analyzed By
Method
Prep Method
Chromium < 10 10
ug/1 1
07/ 18/24
07/22/24 RD
EPA 200.7 2
EPA 200.7 3
Iron < 100 100
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 3
Nickel < 10 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 3
(1) Instrument QC Batch: MA28090
(2) Instrument QC Batch: MA28102
(3) Prep QC Batch: MP28647
RL = Reporting Limit
� 41 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-10/CPW-IOD
Lab Sample ID: LB4543-16 Date Sampled: 07/16/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chloride 160 2.5 mg/1 10 07/29/24 05:03 BD EPA 300
Solids, Total Dissolved 1310 2.5 mg/1 1 07/ 18/24 17:25 xF SM2540 C-1 i
RL = Reporting Limit
� 42 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-28/CPW-12S
Lab Sample ID: LB4543-17 Date Sampled: 07/16/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
Total Metals Analysis
Analyte Result RL
Units DF
Prep
Analyzed By
Method
Prep Method
Chromium < 10 10
ug/1 1
07/ 18/24
07/22/24 RD
EPA 200.7 2
EPA 200.7 3
Iron 7940 100
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 3
Nickel < 10 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 3
(1) Instrument QC Batch: MA28090
(2) Instrument QC Batch: MA28102
(3) Prep QC Batch: MP28647
RL = Reporting Limit
w
3
V
� 43 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-28/CPW-12S
Lab Sample ID: LB4543-17 Date Sampled: 07/16/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chloride 4.0 0.25 mg/1 1 07/29/24 05:16 BD EPA 300
Solids, Total Dissolved 980 2.5 mg/1 1 07/ 18/24 17:25 xF SM2540 C-1 i
RL = Reporting Limit
w
3
V
� 44 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-12/CPW-12D
Lab Sample ID: LB4543-18 Date Sampled: 07/15/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
Total Metals Analysis
Analyte Result RL
Units DF
Prep
Analyzed By
Method
Prep Method
Chromium < 10 10
ug/1 1
07/ 18/24
07/22/24 RD
EPA 200.7 2
EPA 200.7 3
Iron 8580 100
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 3
Nickel < 10 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 3
(1) Instrument QC Batch: MA28090
(2) Instrument QC Batch: MA28102
(3) Prep QC Batch: MP28647
RL = Reporting Limit
w
3
00
� 45 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-12/CPW-12D
Lab Sample ID: LB4543-18 Date Sampled: 07/15/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chloride 4.7 0.25 mg/1 1 07/29/24 05:29 BD EPA 300
Solids, Total Dissolved 896 2.5 mg/1 1 07/ 18/24 17:25 xF SM2540 C-1 i
RL = Reporting Limit
w
3
00
� 46 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-1/CPW-13S
Lab Sample ID: LB4543-19 Date Sampled: 07/15/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
Total Metals Analysis
Analyte Result RL
Units DF
Prep
Analyzed By
Method
Prep Method
Chromium < 10 10
ug/1 1
07/ 18/24
07/22/24 RD
EPA 200.7 2
EPA 200.7 3
Iron 20400 100
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 3
Nickel < 10 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 3
(1) Instrument QC Batch: MA28090
(2) Instrument QC Batch: MA28102
(3) Prep QC Batch: MP28647
RL = Reporting Limit
� 47 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-1/CPW-13S
Lab Sample ID: LB4543-19 Date Sampled: 07/15/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chloride 6.4 0.25 mg/1 1 07/29/24 05:42 BD EPA 300
Solids, Total Dissolved 842 2.5 mg/1 1 07/ 18/24 17:25 xF SM2540 C-1 i
RL = Reporting Limit
� 48 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-13/CPW-13D
Lab Sample ID: LB4543-20 Date Sampled: 07/15/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
Total Metals Analysis
Analyte Result RL
Units DF
Prep
Analyzed By
Method
Prep Method
Chromium < 10 10
ug/1 1
07/ 18/24
07/22/24 RD
EPA 200.7 2
EPA 200.7 3
Iron 298 100
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 3
Nickel < 10 10
ug/1 1
07/ 18/24
07/ 19/24 RD
EPA 200.7 1
EPA 200.7 3
(1) Instrument QC Batch: MA28090
(2) Instrument QC Batch: MA28102
(3) Prep QC Batch: MP28647
RL = Reporting Limit
� 49 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-13/CPW-13D
Lab Sample ID: LB4543-20 Date Sampled: 07/15/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chloride 155 2.5 mg/1 10 07/29/24 05:55 BD EPA 300
Solids, Total Dissolved 1390 2.5 mg/1 1 07/ 18/24 17:25 xF SM2540 C-1 i
RL = Reporting Limit
� 50 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-2/CPW-14S
Lab Sample ID: LB4543-21 Date Sampled: 07/17/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
Total Metals Analysis
Analyte Result RL
Units DF
Prep
Analyzed By
Method
Prep Method
Chromium < 10 10
ug/1 1
07/ 18/24
07/22/24 RD
EPA 200.7 1
EPA 200.7 2
Iron 3100 100
ug/1 1
07/ 18/24
07/22/24 RD
EPA 200.7 1
EPA 200.7 2
Nickel < 10 10
ug/1 1
07/ 18/24
07/22/24 RD
EPA 200.7 1
EPA 200.7 2
(1) Instrument QC Batch: MA28103
(2) Prep QC Batch: MP28648
RL = Reporting Limit
� 51 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-2/CPW-14S
Lab Sample ID: LB4543-21 Date Sampled: 07/17/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chloride 148 2.5 mg/1 10 07/29/24 06:59 BD EPA 300
Solids, Total Dissolved 878 2.5 mg/1 1 07/ 18/24 17:25 xF SM2540 C-1 i
RL = Reporting Limit
� 52 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-14/CPW-14D
Lab Sample ID: LB4543-22 Date Sampled: 07/17/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
Total Metals Analysis
Analyte Result RL
Units DF
Prep
Analyzed By
Method
Prep Method
Chromium < 10 10
ug/1 1
07/ 18/24
07/22/24 RD
EPA 200.7 1
EPA 200.7 2
Iron 2340 100
ug/1 1
07/ 18/24
07/22/24 RD
EPA 200.7 1
EPA 200.7 2
Nickel < 10 10
ug/1 1
07/ 18/24
07/22/24 RD
EPA 200.7 1
EPA 200.7 2
(1) Instrument QC Batch: MA28103
(2) Prep QC Batch: MP28648
RL = Reporting Limit
� 53 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-14/CPW-14D
Lab Sample ID: LB4543-22 Date Sampled: 07/17/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chloride 164 2.5 mg/1 10 07/29/24 07:38 BD EPA 300
Solids, Total Dissolved 1510 2.5 mg/1 1 07/ 18/24 17:25 xF SM2540 C-1 i
RL = Reporting Limit
� 54 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-3/CPW-15S
Lab Sample ID: LB4543-23 Date Sampled: 07/16/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
Total Metals Analysis
Analyte Result RL
Units DF
Prep
Analyzed By
Method
Prep Method
Chromium < 10 10
ug/1 1
07/ 18/24
07/22/24 RD
EPA 200.7 1
EPA 200.7 2
Iron < 100 100
ug/1 1
07/ 18/24
07/22/24 RD
EPA 200.7 1
EPA 200.7 2
Nickel < 10 10
ug/1 1
07/ 18/24
07/22/24 RD
EPA 200.7 1
EPA 200.7 2
(1) Instrument QC Batch: MA28103
(2) Prep QC Batch: MP28648
RL = Reporting Limit
� 55 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-3/CPW-15S
Lab Sample ID: LB4543-23 Date Sampled: 07/16/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chloride 162 2.5 mg/1 10 07/29/24 07:51 BD EPA 300
Solids, Total Dissolved 1240 2.5 mg/1 1 07/ 18/24 17:25 xF SM2540 C-1 i
RL = Reporting Limit
� 56 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-15/CPW-15D
Lab Sample ID: LB4543-24 Date Sampled: 07/16/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
Total Metals Analysis
Analyte Result RL
Units DF
Prep
Analyzed By
Method
Prep Method
Chromium < 10 10
ug/1 1
07/ 18/24
07/22/24 RD
EPA 200.7 1
EPA 200.7 2
Iron < 100 100
ug/1 1
07/ 18/24
07/22/24 RD
EPA 200.7 1
EPA 200.7 2
Nickel < 10 10
ug/1 1
07/ 18/24
07/22/24 RD
EPA 200.7 1
EPA 200.7 2
(1) Instrument QC Batch: MA28103
(2) Prep QC Batch: MP28648
RL = Reporting Limit
� 57 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: MW-15/CPW-15D
Lab Sample ID: LB4543-24 Date Sampled: 07/16/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chloride 129 2.5 mg/1 10 07/29/24 08:04 BD EPA 300
Solids, Total Dissolved 796 2.5 mg/1 1 07/ 18/24 17:25 xF SM2540 C-1 i
RL = Reporting Limit
� 58 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: DUP-1
Lab Sample ID: LB4543-25 Date Sampled: 07/16/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
Total Metals Analysis
Analyte Result RL
Units DF
Prep
Analyzed By
Method
Prep Method
Chromium < 10 10
ug/1 1
07/ 18/24
07/22/24 RD
EPA 200.7 1
EPA 200.7 2
Iron < 100 100
ug/1 1
07/ 18/24
07/22/24 RD
EPA 200.7 1
EPA 200.7 2
Nickel < 10 10
ug/1 1
07/ 18/24
07/22/24 RD
EPA 200.7 1
EPA 200.7 2
(1) Instrument QC Batch: MA28103
(2) Prep QC Batch: MP28648
RL = Reporting Limit
� 59 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: DUP-1
Lab Sample ID: LB4543-25 Date Sampled: 07/16/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chloride 162 2.5 mg/1 10 07/29/24 09:08 BD EPA 300
Solids, Total Dissolved 718 2.5 mg/1 1 07/ 18/24 17:25 xF SM2540 C-1 i
RL = Reporting Limit
� 60 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: DUP-2
Lab Sample ID: LB4543-26 Date Sampled: 07/17/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
Total Metals Analysis
Analyte Result RL
Units DF
Prep
Analyzed By
Method
Prep Method
Chromium < 10 10
ug/1 1
07/ 18/24
07/22/24 RD
EPA 200.7 1
EPA 200.7 2
Iron < 100 100
ug/1 1
07/ 18/24
07/22/24 RD
EPA 200.7 1
EPA 200.7 2
Nickel < 10 10
ug/1 1
07/ 18/24
07/22/24 RD
EPA 200.7 1
EPA 200.7 2
(1) Instrument QC Batch: MA28103
(2) Prep QC Batch: MP28648
RL = Reporting Limit
� 61 of 87
LB4543

SGS North America Inc.
Report of Analysis
Client Sample ID: DUP-2
Lab Sample ID: LB4543-26 Date Sampled: 07/17/24
Matrix: AQ - Ground Water Date Received: 07/ 18/24
Percent Solids: n/a
Project: GSHLSDR Compliance Monitoring
Page 1 of 1
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chloride 65.5 1.3 mg/1 5 07/29/24 09:21 BD EPA 300
Solids, Total Dissolved 620 2.5 mg/1 1 07/ 18/24 17:25 xF SM2540 C-1 i
RL = Reporting Limit
� 62 of 87
LB4543

SCE
Scott, LA
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Section 4
� 63 of 87
LB4543

CHAIN OF CUSTODY PAGE OF 3
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LB4543: Chain of Custody
Page 1 of 6
� 64 of 87
LB4543

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LB4543: Chain of Custody
Page 2 of 6
� 65 of 87
LB4543

CHAIN OF CUSTODY PAGE 3 OF 3
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LB4543: Chain of Custody
Page 3 of 6
� 66 of 87
LB4543

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LB4543: Chain of Custody
Page 4 of 6
� 67 of 87
LB4543

R9rt # 156297-435 RR 8� 12/24
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LB4543: Chain of Custody
Page 5 of 6
SGS68 of 87
LB4543

SGS Sample Receipt Summary
Job Number: Ib4543 Client: GLENN SPRINGS HOLDINGS,INC
Project: GSHI CASTLE
HAYNE SEMIANNUAL QU
Date / Time Received: 7/18/2024 930:00 AM Delivery Method:
FEDEX Airbill Vs: 704303404064,704335404089
Cooler Temps (Raw Measured) °C: Cooler 2: (3.1); Cooler 1: (2.5);
Cooler Temps (Corrected) °C: Cooler 2: (2.9); Cooler 1: (2.3);
Cooler Security Y or N Y or N
Sample Integrity - Documentation
Y
3
or N
1. CustodySeals Present: ❑� ❑ 3. COC Present: 0 ❑
1. Sample labels present on bottles:
❑�
❑
�
2. Custody Seals Intact: W ❑ 4. Smpl Dates/Time OK ❑.r ❑
2. Container labeling complete:
❑�
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Cooler Temperature Y or N
3. Sample container label / COC agree:
❑✓
❑
1. Temp criteria achieved: r❑ ❑
Sample Integrity - Condition
Y
or N
2. Cooler temp verification: IR GUN
Sample recvd within HT:
❑�
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3. Cooler media: Ice (direct contact)
2. All containers accounted for:
0
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4. No. Coolers: 1
3. Condition of sample:
Intact
Quality Control Preservation Y or N N/A
Sample Integrity - Instructions
Y
or N N/A
1. Trip Blank present / cooler: ❑ ❑ ❑�
1. Analysis requested is clear:
0
❑
2. Trip Blank listed on COC: ❑ ❑ 0
2. Bottles received for unspecified tests
❑
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3. Samples preserved properly: J❑ ❑
3. Sufficient volume recvd for analysis:
❑�
❑
4. VOCs headspace free: ❑ ❑ ❑�
4. Compositing instructions clear:
❑
El
5. Filtering instructions clear:
❑
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Test Strip Lot #s: pH 1-12: pH 12+: Other: (Specify)
Comments
SM089-03
Rev. Date 12/7/17
LB4543: Chain of Custody
Page 6 of 6
� 69 of 87
LB4543

sw
Scott, LA
Section 5
Metals Analysis
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Matrix Spike and Duplicate Summaries
• Blank Spike and Lab Control Sample Summaries
• Serial Dilution Summaries
� 70 of 87
LB4543

BLANK RESULTS SUMMARY
Part 2 - Method Blanks
Login Number: LB4543
Account: CRANYNF - CUD Services Inc.
Project: GSHI:SDR Compliance Monitoring
QC Batch ID: MP28647 Methods: EPA 200.7
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 07/18/24
MB
letal RL IDL MDL raw final
Aluminum 200 13 15
Antimony 6.0 2 3.5
Arsenic 10 2.4 7.3
Barium 10 .36 1.2
Beryllium 4.0 .06 .6
Boron 100 .72 14
Cadmium 5.0 .14 .5
Calcium 300 3.8 22
Chromium 10 .39 1.7 0.14 <10
Cobalt 10 .26 1.1
Copper 10 .77 4
Iron 100 2.9 20 -1.2 <100
Lead 10 1.4 9
Magnesium 100 22 36
Manganese 10 .11 1.2
Molybdenum 10 .16 1.2
Nickel 10 .29 1.7 -0.16 <10
Potassium 500 50 110
Selenium 10 1.5 5.2
Silver 10 .57 2
Sodium 500 20 120
Strontium 10 .1 .5
Thallium 10 1.5 4
Tin 10 .74 2.8
Titanium 10 .41 .7
Vanadium 10 .39 1.2
Zinc 20 .18 5.6
Lithium 10 2.4 3
Associated samples MP28647: LB4543-1, LB4543-2, LB4543-3, LB4543-4, LB4543-5, LB4543-6, LB4543-7, LB4543-
8, LB4543-9, LB4543-10, LB4543-11, LB4543-12, LB4543-13, LB4543-14, LB4543-15, LB4543-16, LB4543-17,
LB4543-18, LB4543-19, LB4543-20
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
Page 1
� 71 of 87
LB4543

MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: LB4543
Account: CRANYNF - GHD Services Inc.
Project: GSHI:SDR Compliance Monitoring
QC Batch ID: MP28647 Methods: EPA 200.7
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 07/18/24
LB4543-1 Spikelot QC
letal Original MS MPICPMS6s Rec Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium 2.7 102 100 99.3 70-130
Cobalt
Copper
Iron 11700 15900 5000 84.0 70-130
Lead
Magnesium
Manganese
Molybdenum
Nickel 0.0 94.2 100 94.2 70-130
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Lithium
Associated samples MP28647: LB4543-1, LB4543-2, LB4543-3, LB4543-4, LB4543-5, LB4543-6, LB4543-7, LB4543-
8, LB4543-9, LB4543-10, LB4543-11, LB4543-12, LB4543-13, LB4543-14, LB4543-15, LB4543-16, LB4543-17,
LB4543-18, LB4543-19, LB4543-20
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
Page 1
� 72 of 87
LB4543

MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: LB4543
Account: CRANYNF - GHD Services Inc.
Project: GSHI:SDR Compliance Monitoring
QC Batch ID: MP28647 Methods: EPA 200.7
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 07/18/24
LB4543-1 Spikelot MSD QC
letal Original MSD MPICPMS6s Res RPD Limit
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium 2.7 105 100 102.3 2.9 20
Cobalt
Copper
Iron 11700 15900 5000 84.0 0.0 20
Lead
Magnesium
Manganese
Molybdenum
Nickel 0.0 94.4 100 94.4 0.2 20
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Lithium
Associated samples MP28647: LB4543-1, LB4543-2, LB4543-3, LB4543-4, LB4543-5, LB4543-6, LB4543-7, LB4543-
8, LB4543-9, LB4543-10, LB4543-11, LB4543-12, LB4543-13, LB4543-14, LB4543-15, LB4543-16, LB4543-17,
LB4543-18, LB4543-19, LB4543-20
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
Page 2
� 73 of 87
LB4543

MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: LB4543
Account: CRANYNF - GHD Services Inc.
Project: GSHI:SDR Compliance Monitoring
QC Batch ID: MP28647 Methods: EPA 200.7
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 07/18/24
LB4543-10 Spikelot QC
letal Original MS MPICPMS6s Rec Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium 1.4 92.9 100 91.5 70-130
Cobalt
Copper
Iron 6130 10500 5000 87.4 70-130
Lead
Magnesium
Manganese
Molybdenum
Nickel 0.0 95.9 100 95.9 70-130
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Lithium
Associated samples MP28647: LB4543-1, LB4543-2, LB4543-3, LB4543-4, LB4543-5, LB4543-6, LB4543-7, LB4543-
8, LB4543-9, LB4543-10, LB4543-11, LB4543-12, LB4543-13, LB4543-14, LB4543-15, LB4543-16, LB4543-17,
LB4543-18, LB4543-19, LB4543-20
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
Page 3
� 74 of 87
LB4543

MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: LB4543
Account: CRANYNF - GHD Services Inc.
Project: GSHI:SDR Compliance Monitoring
QC Batch ID: MP28647 Methods: EPA 200.7
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 07/18/24
LB4543-10 Spikelot MSD QC
letal Original MSD MPICPMS6s Res RPD Limit
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium 1.4 92.2 100 90.8 0.8 20
Cobalt
Copper
Iron 6130 10400 5000 85.4 1.0 20
Lead
Magnesium
Manganese
Molybdenum
Nickel 0.0 94.9 100 94.9 1.0 20
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Lithium
Associated samples MP28647: LB4543-1, LB4543-2, LB4543-3, LB4543-4, LB4543-5, LB4543-6, LB4543-7, LB4543-
8, LB4543-9, LB4543-10, LB4543-11, LB4543-12, LB4543-13, LB4543-14, LB4543-15, LB4543-16, LB4543-17,
LB4543-18, LB4543-19, LB4543-20
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
Page 4
� 75 of 87
LB4543

SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: LB4543
Account: CRANYNF - GHD Services Inc.
Project: GSHI:SDR Compliance Monitoring
QC Batch ID: MP28647 Methods: EPA 200.7
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 07/18/24
BSP Spikelot QC
letal Result MPICPMS6s Rec Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium 102 100 102.0 85-115
Cobalt
Copper
Iron 4980 5000 99.6 85-115
Lead
Magnesium
Manganese
Molybdenum
Nickel 96.7 100 96.7 85-115
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Lithium
Associated samples MP28647: LB4543-1, LB4543-2, LB4543-3, LB4543-4, LB4543-5, LB4543-6, LB4543-7, LB4543-
8, LB4543-9, LB4543-10, LB4543-11, LB4543-12, LB4543-13, LB4543-14, LB4543-15, LB4543-16, LB4543-17,
LB4543-18, LB4543-19, LB4543-20
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
Page 1
76 of 87
LB4543

SERIAL DILUTION RESULTS SUMMARY
Login Number: LB4543
Account: CRANYNF - CUD Services Inc.
Project: GSHI:SDR Compliance Monitoring
QC Batch ID: MP28647 Methods: EPA 200.7
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 07/18/24
LB4543-1 QC
letal Original SDL 1:5 %DIF Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium 2.67 3.14 17.6 (a) 0-10
Cobalt
Copper
Iron 11700 11400 1.9 0-10
Lead
Magnesium
Manganese
Molybdenum
Nickel 0.00 0.00 NC 0-10
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Lithium
Associated samples MP28647: LB4543-1, LB4543-2, LB4543-3, LB4543-4, LB4543-5, LB4543-6, LB4543-7, LB4543-
8, LB4543-9, LB4543-10, LB4543-11, LB4543-12, LB4543-13, LB4543-14, LB4543-15, LB4543-16, LB4543-17,
LB4543-18, LB4543-19, LB4543-20
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
Page 1
� 77 of 87
LB4543

BLANK RESULTS SUMMARY
Part 2 - Method Blanks
Login Number: LB4543
Account: CRANYNF - CUD Services Inc.
Project: GSHI:SDR Compliance Monitoring
QC Batch ID: MP28648 Methods: EPA 200.7
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 07/18/24
MB
letal RL IDL MDL raw final
Aluminum 200 12 15
Antimony 6.0 1.6 3.5
Arsenic 10 2.8 7.3
Barium 10 .33 1.2
Beryllium 4.0 .03 .6
Boron 100 .48 14
Cadmium 5.0 .23 .5
Calcium 300 4.5 22
Chromium 10 .27 1.7 -0.040 <10
Cobalt 10 .23 1.1
Copper 10 .6 4
Iron 100 3.2 20 4.4 <100
Lead 10 1.2 9
Magnesium 100 24 36
Manganese 10 .07 1.2
Molybdenum 10 .24 1.2
Nickel 10 .61 1.7 -1.1 <10
Potassium 500 49 110
Selenium 10 4.4 5.2
Silver 10 .7 2
Sodium 500 33 120
Strontium 10 .12 .5
Thallium 10 2.6 4
Tin 10 .79 2.8
Titanium 10 .34 .7
Vanadium 10 .27 1.2
Zinc 20 .26 5.6
Lithium 10 3.5 3
Associated samples MP28648: LB4543-21, LB4543-22, LB4543-23, LB4543-24, LB4543-25, LB4543-26
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
Page 1
� 78 of 87
LB4543

MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: LB9593
Account: CRANYNF - GHD Services Inc.
Project: GSHI:SDR Compliance Monitoring
QC Batch ID: MP28698 Methods: EPA 200.7
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 07/18/24
LB9593-21 Spikelot QC
letal Original MS MPICPMS6s Rec Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium 0.88 94.6 100 93.7 70-130
Cobalt
Copper
Iron 3100 7310 5000 84.2 70-130
Lead
Magnesium
Manganese
Molybdenum
Nickel 0.0 98.7 100 98.7 70-130
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Lithium
Associated samples MP28698: LB9593-21, LB9593-22, LB9593-23, LB9593-29, LB9593-25, LB9593-26
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
Page 1
� 79 of 87
LB4543

MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: LB4543
Account: CRANYNF - GHD Services Inc.
Project: GSHI:SDR Compliance Monitoring
QC Batch ID: MP28648 Methods: EPA 200.7
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 07/18/24
LB4543-21 Spikelot MSD QC
letal Original MSD MPICPMS6s Res RPD Limit
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium 0.88 92.6 100 91.7 2.1 20
Cobalt
Copper
Iron 3100 7830 5000 94.6 6.9 20
Lead
Magnesium
Manganese
Molybdenum
Nickel 0.0 100 100 100.0 1.3 20
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Lithium
Associated samples MP28648: LB4543-21, LB4543-22, LB4543-23, LB4543-24, LB4543-25, LB4543-26
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
Page 2
m
80 of 87
LB4543

SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: LB4543
Account: CRANYNF - GHD Services Inc.
Project: GSHI:SDR Compliance Monitoring
QC Batch ID: MP28648 Methods: EPA 200.7
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 07/18/24
BSP Spikelot QC
letal Result MPICPMS6s Rec Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium 90.0 100 90.0 85-115
Cobalt
Copper
Iron 4540 5000 90.8 85-115
Lead
Magnesium
Manganese
Molybdenum
Nickel 97.8 100 97.8 85-115
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Lithium
Associated samples MP28648: LB4543-21, LB4543-22, LB4543-23, LB4543-24, LB4543-25, LB4543-26
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
Page 1
� 81 of 87
LB4543

SERIAL DILUTION RESULTS SUMMARY
Login Number: LB4543
Account: CRANYNF - CUD Services Inc.
Project: GSHI:SDR Compliance Monitoring
QC Batch ID: MP28648 Methods: EPA 200.7
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 07/18/24
LB4543-21 QC
letal Original SDL 1:5 %DIF Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium 0.880 2.49 183.0(a) 0-10
Cobalt
Copper
Iron 3100 3340 7.8 0-10
Lead
Magnesium
Manganese
Molybdenum
Nickel 0.00 0.00 NC 0-10
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Lithium
Associated samples MP28648: LB4543-21, LB4543-22, LB4543-23, LB4543-24, LB4543-25, LB4543-26
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
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sw
Scott, LA A I
Section 6
General Chemistry
QC Data Summaries
Includes the following where applicable:
• Method Blank and Blank Spike Summaries
• Duplicate Summaries
• Matrix Spike Summaries
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METHOD BLANK AND SPIKE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: LB4543
Account: CRANYNF - GHD Services Inc.
Project: GSHI:SDR Compliance Monitoring
MB Spike BSP BSP QC
malyte Batch ID RL Result Units Amount Result %Recov Limits
Chloride
GP13306/GN29274 0.25
0.0
mg/1
12.5
12.2
97.6
90-110%
Chloride
GP13307/GN29272 0.25
0.0
mg/1
12.5
12.3
98.4
90-110%
Solids, Total
Dissolved
GN29136 2.5
0.0
mg/1
1000
977
97.7
90-110%
Solids, Total
Dissolved
GN29136
mg/1
1000
980
97.7
90-110%
Solids, Total
Dissolved
GN29137
mg/1
1000
1010
101.3
90-110%
Solids, Total
Dissolved
GN29137 2.5
0.0
mg/1
1000
1010
101.3
90-110%
j
Sulfate
GP13307/GN29272 0.25
0.0
mg/1
12.5
11.9
95.2
90-110%
Associated Samples:
Batch GN29136:
LB4543-16,
LB4543-17, LB4543-18, LB4543-19,
LB4543-20,
LB4543-21,
LB4543-22,
LB4543-23,
LB4543-24, LB4543-
25, LB4543-26
Batch GN29137:
LB4543-1,
LB4543-2, LB4543-3, LB4543-4,
LB4543-5,
LB4543-6, LB4543-7,
LB4543-8,
LB4543-9,
LB4543-10,
LB4543-11, LB4543-12,
LB4543-13,
LB4543-14, LB4543-15
Batch GP13306:
LB4543-1,
LB4543-2, LB4543-3, LB4543-4,
LB4543-5,
LB4543-6, LB4543-7,
LB4543-8,
LB4543-9,
LB4543-10,
LB4543-11, LB4543-12,
LB4543-13,
LB4543-14, LB4543-15,
LB4543-16,
LB4543-17, LB4543-18, LB4543-19, LB4543-20
Batch GP13307:
LB4543-21,
LB4543-22, LB4543-23, LB4543-24,
LB4543-25,
LB4543-26
(*) Outside of
QC limits
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DUPLICATE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: LB4543
Account: CRANYNF - GHD Services Inc.
Project: GSHI:SDR Compliance Monitoring
QC Original DUP QC
malyte Batch ID Sample Units Result Result RPD Limits
Solids, Total Dissolved
GN29136
LB4543-16
mg/1
1310
1280
2.6
0-5s
Solids, Total Dissolved
GN29136
LB4543-26
mg/l
620
604
2.6
0-5%
Solids, Total Dissolved
GN29137
LB4543-6
mg/l
1710
1730
1.3
0-5%
Associated Samples:
Batch GN29136: LB4543-16,
LB4543-17, LB4543-18,
LB4543-19,
LB4543-20,
LB4543-21,
LB4543-22,
LB4543-23,
LB4543-24, LB4543-
IV
25, LB4543-26
Batch GN29137: LB4543-1,
LB4543-2, LB4543-3,
LB4543-4,
LB4543-5,
LB4543-6, LB4543-7,
LB4543-8,
LB4543-9,
LB4543-10,
LB4543-11, LB4543-12, LB4543-13,
LB4543-14,
LB4543-15
•
(*) Outside of QC limits
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MATRIX SPIKE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: LB4543
Account: CRANYNF - GHD Services Inc.
Project: GSHI:SDR Compliance Monitoring
QC Original Spike MS QC
malyte Batch ID Sample Units Result Amount Result %Rec Limits
Chloride
GP13306/GN29274
LB4543-3
mg/l
32.9
125
156
98.5
80-120%
Chloride
GP13306/GN29274
LB4543-20
mg/l
155
125
302
117.6
80-120%
Chloride
GP13307/GN29272
LB4543-21
mg/l
148
125
303
124.ON(a)
80-120%
Sulfate
GP13307/GN29272
LB4543-21
mg/l
283
125
448
132.ON(a)
80-120%
Q1
Associated Samples:
W
Batch GP13306: LB4543-1,
LB4543-2, LB4543-3, LB4543-4, LB4543-5,
LB4543-6,
LB4543-7,
LB4543-8,
LB4543-9,
LB4543-10,
LB4543-11, LB4543-12,
LB4543-13, LB4543-14, LB4543-15, LB4543-16,
LB4543-17,
LB4543-18,
LB4543-19,
LB4543-20
Batch GP13307: LB4543-21,
LB4543-22, LB4543-23,
LB4543-24, LB4543-25, LB4543-26
-19
(*) Outside of QC limits
(N) Matrix Spike Res. outside of QC limits
(a) Outside control limits due to matrix interference and/or sample nonhomogeneity.
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MATRIX SPIKE DUPLICATE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: LB9593
Account: CRANYNF - GHD Services Inc.
Project: GSHI:SDR Compliance Monitoring
QC Original Spike MSD QC
malyte Batch ID Sample Units Result Amount Result RPD Limit
Chloride
GP13306/GN29274
LB9593-3
mg/l
32.9
125
157
0.6
20%
Chloride
GP13306/GN29274
LB9593-20
mg/l
155
125
303
0.3
20%
Chloride
GP13307/GN29272
LB9593-21
mg/l
148
125
299
1.3
20%
Sulfate
GP13307/GN29272
LB9593-21
mg/l
283
125
993
1.1
20%
Q1
Associated Samples:
Batch GP13306: LB9593-1,
LB9593-2, LB9593-3, LB9593-9, LB9593-5,
LB9593-6,
LB9593-7,
LB9593-8,
LB9593-9,
LB9593-10,
LB9593-11, LB9593-12,
LB9593-13, LB9593-19, LB9593-15, LB9593-16,
LB9593-17,
LB9593-18,
LB9593-19,
LB9593-20
Batch GP13307: LB9593-21,
LB9593-22, LB9593-23,
LB9593-29, LB9593-25, LB9593-26
C
(*) Outside of QC limits
(N) Matrix Spike Res.
outside of QC limits
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