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WQ0034775_Monitoring - 07-2024_20240813
Monitoring Report Submittal Permit Number#* WQ0034775 Name of Facility:* Bakelite Synthetics Month: * July Year: * 2024 Report Information Type* Upload Document* GW-59 CLRS Permit WQ0034775 July 2024 Submittal.pdf 2.13MB PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Confirmation Email Address: * ben.moore@wsp.com Name of Submitter: * W. Ben Moore Signature: Wv- 43�r ��rA Date of submittal: 8/13/2024 This will be filled in automatically Initial Review Reviewer: Wanda.Gerald Is the project number correct?* W00034775 Is the monitoring report accepted?* Yes NO Regional Office* Wilmington Reviewer: _anonymous Review Date: 8/14/2024 GW-59A COMPLIANCE REPORT FORM Permit # WCL0034775 (,Vubn7lt one each neonlioring period with CIV--59 forms.) 1 Enter date monitoring results were due. (4 30 2024 ) Will this monitoring report (GW-59 and GW-59A) YES NO be submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? YI, S NO IF the answer to question 1 or 2 Is "YES", list /n the space provided below the well Identification number(s) and explain the problems encountered In obtaining the required Information, 3 Are nny of the monitor wells in need of repair or maintennitco (dannaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc,)? Ifthe answer is "Yes", contact tlleReglonalOfJtceforguidm7ce. 4 Are any monitored constituents equal to or above the established standards? tS NO If the answer to question 4 Is "NO", skip.to section 8. If the answer to question 4 Is "YES" list the affected wells Individually with constituents) and concentratlon(s) exceeding standards In the space provided below: WWMW-1: Ammonia Nitrogen (400 mg/L); Total Dissolved Solids (2490 mg/L); Sulfate (1570 mg/L); pH (6.33 su) WWMW-2: Total Ammonia Nitrogen (20.5 mg/L); Nitrate (20.8 mg/L); pH (5.52 su) 5 For the constituents identified In question 4 above, have standards been exceeded previously for the Y);S NO same constltuent(s) in the same well(s) In the last two years? If the answer to question 5 Is "NO", skip to section 8. If the answer to question 5 Is "YES'; list In the space provided below, each well with constltttent(s) exceeding standards, concentratlon(s) reported, and sample collection date for each occurrence (for the last two years). W WMW-l: Total Ammonla Nitrogen 580 mg/L (3/09/2022), 390 mgA (7/13/2022), 540 mg/L (11/02/2022), 490 mgA (3/08/2023), 390 mgA (7/12/2023); IDS 1260 mg/L (3/09/2022), 1130 mgA (7/13/2022) 744 mg/L (11/02/2022),1310 mgA (3/08/2023),1550 mg/L (7/12/2023),1970 mgA (11/15/2023); Sulfate 807 mgA (3/09/2022), 442 mgA (7/13/2022) 730 mgA (11/02/2022),1020 mgA (3/08/2023), 987 mg/L (7/12/2023), 2740 mgA (11/1512023); pH 6.47 su (11/15/2023) W WMW-2: Total Ammonia Nitrogen 26.1 mg/L (3/09/2022), 78.3 mgA 17/13/2022), 45.6 mg/L (11/02/2022), 8.8 mgA (3/08/2023), 7.5 mg/L (7/12/2023), 48.0 mgA (11115/2023); pH_5.92 sd (3/D9/2022), 6.21 su (7/13/2022), 5.89 su (11/02/2022), 6.39 su (3/08/20231, 5.08 su (7/12/2023). 5.40 su (11/15/23);; Nitrate 32.6 mg/L (3/09/2022),19.S mg/L (7/13/2022), 55.6 mgA (11/02/2022), 12.6 mg/L (3/08/1023), 10.2 mgA (7/12/2023),15.8 mg/L (11/15/2023) G Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer Is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. if the answer Is "NO'; monitoring wells may be Improperly located; contact the Regional Office. 7 Is the permittee Implementing previously approved actions required by the Division involving this Y1 S NO groundwater quality problem? If the answer to question 71s "YES", describe those actions In the space provided below. If the answer.to question 7Is "NO'; contact the Regional Office within 90 days: an evaluation may be required to determine the Impact the waste disposal system Is having at the review and comyllance boundaries surroundina this facility, Failure to do so may sublect the nermittee to a Notice of Violation fines, and/or penalties. The Lined Pond has been permanently removed from closed -loop recycle service. g The person completing this portion (GW--59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. F r e 9� t� _ _ �ya""r� ,rt ��ai� t ;�'� �. �S ,�i'�ti e � tt-'1 RE' �r poCE, t R' hilt tote tt�e�6 6 1 �Qq, 1,r., Sign lf ure of Permittee ( r Authorized Agent) bate GW-59A 12/8/2003 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W00034775 Expiration Date: January 31,2028 Facility Name: Bakelite LLC Non -Discharge UIC Permit Name (if different): Permit No. W00034775 Bakelite Synthetics —Riegelwood CLRS Closed -Loop Recycle System Columbus county NPDES Other Facility Address: 333 Neils Eddy Road TYPE OF PERMITTED OPERATION BEING MONITORED Riegelwood " NC 28456 County Columbus ❑ Lagoon ❑ Remediation: Infiltration Gallery �A'l s"' `"' ❑ Spray Field ❑ Remediation: Contact Person: Mr. Ronald Bazinet Telephone#: (910) 655-2263 ext 5257 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: WWMW-1 No. of wells to be sampled: 2 ❑ Water Source Heat Pump ® Other: CLRS (from Povn¢) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): WWMW-1 Date sample collected: July 17, 2024 FIELD ANALYSES: WAS Well Depth: 17.80 ft. Well Diameter: 2 in. H oo400: 6.10 p units Temp. °C DRY at Depth to Water Level 82546:10.47 ft. below measuring point Screened Interval: 7.8 ft. to 17.8 ft. Spec. Cond. oo094: 2980 µMhos time of sampling, Measuring Point is 2.45 g ft. above land surface Relative M.P. Elevation: 23.29 ft. Odor 000es: odor check Volume of water pumped/bailed before sampling: 4.0 gallons Appearance cloudy here:® Samples for metals were collected unfiltered: m YES ❑ NO and field acidified: ® YES ❑ NO LABORATORY INFORMATION Date sample analyzed: July 18- 26.2024 Laboratory Name: Environmental Chemists, Inc. Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead olos1 ug/L Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 0.08 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.67 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 703oo 2260 mg/L Al - Aluminum oilo5 mg/L Formaldehyde (8315A): 62 ug/L pH (Lab) 00403 units Ba - Barium 01007 ug/L 1,3-Dichlorobenzene: 0.55 ug/L TOC 0068o 26.6 mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 1030 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? M Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC(GWVOC) method # 8260low concentration Total Ammonia 00610 430 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Ronald Bazinet - Bakelite Site Leader Permittee (or Authorized Agent) Name and Tide - Please print or type GW-59 Rev.2/2010 1512� SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0034775 Expiration Date: January 31, 2028 Facility Name: Bakelite LLC Non -Discharge UIC Permit Name (if different): Permit No. W00034775 Bakelite Synthetics -Riegelwood CLRS Closed -Loop Recycle System Columbus County NPDES Other Facility Address: 333 Neils Eddy Road TYPE OF PERMITTED OPERATION BEING MONITORED Riegelwood ""°"' NC 28456 County Columbus ❑Lagoon El Remediation: Infiltration Gallery :. , s,;,. ❑ Spray Field ❑ Remediation: Contact Person: Mr. Ronald Bazinet Telephone#: (910) 655-2263 ext 5257 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: WWMW-2 No. of wells to be sampled: 2 ❑ Water Source Heat Pump 0 Other: CLRS (from Pormit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): WWMW-2 Date sample collected: July 17, 2024 FIELD ANALYSES: WAS Well Depth: 13.21 ft. Well Diameter: 2 in. pH 00400: 5.66 units Temp. 00010: 27.4 eC DRY at Depth to Water Level 82546: 8.24 ft. below measuring point Screened Interval: 3.21 ft. to 13.21 ft. Spec. Cond. 00094: 739 µMhos time of Measuring Point is 1.56 g ft. above land surface Relative M.P. Elevation: 15.89 ft. Odor 0008s: none sampling, check Volume of water pumped/bailed before sampling: 4.0 gallons Appearance clear here:® Samples for metals were collected unfiltered: 0 YES ❑ NO and field acidified: ® YES ❑ NO LABORATORY INFORMATION Date sample analyzed: July 18-26, 2024 Laboratory Name: Environmental Chemists, Inc. Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N o0615 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 25.6 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P D0665 0.52 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 256 mg/L AI - Aluminum 011o5 mg/L Formaldehyde (8315A): <50 ug/L pH (Lab) OD403 units Ba - Barium 01007 ug/L TOC oo680 8.3 mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total o1o34 ug/L Grease and Oils oo552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 130 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? 0 Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC (GWVOC) method # 8260 low concentration Total Ammonia oo610 54.8 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese oio5s ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Ronald Bazinet - Bakelite Site Leader ' Q / 5 L Permittee (or Authorized Agent) Name and Title - Please print or type Signature of nnittee (or Author ed A nt) (bate) GW-59 Rev.2/2010 h1ho.— to ANALYTICAL & CONSULTING CHEMISTS WSP USA E&I Inc 5710 Oleander Drive , Suite 110 Wilmington NC 28405 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 2&%0 • 910.347.5843 Lab/Fax info a environmentalchemists.com Date of Report: Aug 05, 2024 Customer PO #: Customer ID: 11070019 Report #: 2024-16350 Project ID: Bakelite Acme CLRS Lab ID Sample ID: 24-40395 Site: WWMW-01 Test Collect Date/Time 7/17/2024 9:10 AM Method Matrix Sampled by Water Client Results Date Analyzed Iron EPA200.7, Rev. 4.4. 1994 (Dissolved) 0.015 mg/L 07/24/2024 Manganese EPA 200.7, Rev. 4.4. 1994 (Dissolved) 1.20 mg/L 07/24/2024 Sulfate EPA300.0, Rev. 2.1. 1993 1030 mg/L 07/18/2024 Ammonia Nitrogen EPA 350.1, Rev. 2.0, 1993 430 mg/L 07/23/2024 Total Dissolved Solids (TDS) SM2540 C-2015 2260 mg/L 07/18/2024 Total Phosphorus SM 4500 P (F-H)-2011 0.67 mg/L 07/26/2024 Sulfide SM 4500 S D-2011 0.18 mg/L 07/24/2024 Total Organic Carbon (TOC) SM 5310 13-2014 26.6 mg/L 07/22/2024 1, 1, 1,2-Tetrachloroethane SW 846 Method 8260D/503013 <0.5 µg/L 07/23/2024 1, 1, 1 -Trichloroethane SW 846 Method 8260D/5030B <0.5 µg/L 07/23/2024 1,1,2,2-Tetrachloroethane SW 846 Method 826OD15030B <0.5 µg/L 07/23/2024 1,1,2-Trichloroethane SW 846 Method 8260015030E <0.5 µg/L 07/23/2024 1,1-Dichloroethane SW 846 Method 82BODIS030B <0.5 µg/L 07/23/2024 1,1-Dichloroethene SW 846 Method 8260DIS030B <0.5 µg/L 07/23/2024 1,1-Dichloropropene SW 846 Method 8260DIS030B <0.5 µg/L 07/23/2024 1,2,3-Trichlorobenzene SW 846 Method 8260D150308 <0.5 pg/L 07/23/2024 1,2,3-Trlchloropropane SW 846 Method 8260D15030B <0.5 µg/L 07/23/2024 1,2,4-Trichlorobenzene SW 846 Method 826OD15030B <0.5 µg/L 07/23/2024 1,2,4-Trimethyl benzene SW 846 Method 8260D/503013 <0.5 µg/L 07/23/2024 1,2-Dibromo-3-Chloropropane SW 848 Method 826OD15030B <0.5 µg/L 07/23/2024 1,2-Dibromoethane SW 846 Method 826013/503013 <0.5 µg/L 07/23/2024 1,2-Dichlorobenzene SW W Method 8260D16030B <0.5 µg/L 07/23/2024 1,2-Dichloroethane SW 846 Method 8260D/5030B <0.5 µg/L 07/23/2024 1,2-Dlchloropropane SW 846 Method 8260DIS030B <0.5 µg/L 07/23/2024 1,3,5-Trimethyl benzene SW 846 Method 8260D/5030B <0.5 pg/L 07/23/2024 1,3-Dichlorobenzene SW 846 Method 8260D150308 0.55 µg/L 07/23/2024 Report M. 2024-16350 Page 1 of 9 [en7viroehe]m ANALYTICAL & CONSULTING CHEMISTS WSP USA B&I Inc 5710 Oleander Drive , Suite 110 Wilmington NC 28405 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists_com Date of Report: Aug 05, 2024 Customer PO #: Customer ID: 11070019 Report M 2024-16350 Project ID: Bakelite Acme CLRS 1, 3-Dichloropropane SW 846 Method 8260015030E <0.5 pg/L 07/23/2024 1,4-Dichlorobenzene SW 646 Method 826OD15030B <0.5 pg/L 07/23/2024 2,2-Dichloropropane SW 846 Method 826OD15030B <0.5 pg/L 07/23/2024 2-Chlorotoluene SW 846 Method 8280D/5030B <0.5 pg/L 07/23/2024 4-Chlorotoluene SW 846 Method 826OD15030B <0.5 pg/L 07/23/2024 Benzene SW 846 Method 8260D15030B <0.5 pg/L 07/23/2024 Bromobenzene SW 846 Method 8260D/5030B <0.5 pg/L 07/23/2024 Bromochloromethane SW 846 Method 8260D15030B <0.5 pg/L 07/23/2024 Bromodichloromethane SW 846 Method 826OD15030B <0.5 pg/L 07/23/2024 Bromoform SW 846 Method 8260D/5030B <0.5 pg/L 07/23/2024 Bromomethane SW 846 Method 826OD15030B <0.5 pg/L 07/23/2024 Carbon tetrachloride SW 848 Method 82BOD15030B <0.5 pg/L 07/23/2024 Chlorobenzene SW 846 Method 8280D/5030B <0.5 pg/L 07/23/2024 Chloroethane SW 846 Method 826OD15030B <0.5 pg/L 07/23/2024 Chloroform SW 846 Method 8260D15030B <0.5 pg/L 07/23/2024 Chloromethane SW 846 Method 826OD15030B <0.5 pg/L 07/23/2024 cis- 1,2-Dichloroethene SW 846 Method 826OD150308 <0.5 pg/L 07/23/2024 cis- 1,3-Dichloropropene SW 846 Method 826OD15030B <0.5 pg/L 07/23/2024 Dibromochloromethane SW 846 Method 8260D150308 <0.5 pg/L 07/23/2024 Dibromomethane SW 846 Method 8260D15030B <0.5 pg/L 07/23/2024 Dichlorodifluoromethane SW 846 Method 8260D15030B <0.5 pg/L 07/23/2024 Ethylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 07/23/2024 Hexachlorobutadiene SW 646 Method 826OD15030B <0.5 pg/L 07/23/2024 Isopropylbenzene SW 846 Method MOD15030B <0.5 pg/L 07/23/2024 M+P Xylene SW 846 Method 8260D/5030B <1.0 pg/L 07/23/2024 Methylene chloride SW 846 Method 8260D15030B <0.5 pg/L 07/23/2024 Naphthalene SW 846 Method 8260D15030B <0.5 pg/L 07/23/2024 n-Butylbenzene SW 848 Method 8260D/5030B <0.5 pg/L 07/23/2024 n-Propylbenzene SW B48 Method 8280D/5030B <0.5 pg/L 07/23/2024 ortho-Xylene SW 846 Method 826OD15030B <0.5 pg/L 07/23/2024 Report #:. 2024-16350 Page 2 of 9 F -77 "Op". L h,— —'.Ill ANALYTICAL & CONSULTING CHEMISTS WSP USA E&I Inc 5710 Oleander Drive, Suite 110 Wilmington NC 28405 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax infoia environmentalchemists.com Date of Report: Aug 05, 2024 Customer PO #: Customer ID: 11070019 Report #: 2024-16350 Project ID: Bakelite Acme CLRS p-Isopropyltoluene SW 846 Method 826OD15030B <0.5 pg/L 07/23/2024 sec -Butyl benzene SW 846 Method 8260D/5030B <0.5 pg/L 07/23/2024 Styrene SW 846 Method 826013r50306 <0.5 pg/L 07/23/2024 tert-Butylbenzene SW 846 Method 8260D15030B <0.5 pg/L 07/23/2024 Tetrachloroethene SW 846 Method 826oDr5030B <0.5 pg/L 07/23/2024 Toluene SW 846 Method 8260Dl5030B <0.5 pg/L 07/23/2024 Trans-1 ,2-Dichloroethene SW 846 Method 826OD15030B <0.5 pg/L 07/23/2024 Trans-1,3-dichloropropene SW 846 Method 8260D/5030B <0.5 pg/L 07/23/2024 Trichloroethene SW 846 Method 8260D/5030B <0.5 pg/L 07/23/2024 Trichlorofluoromethane SW 846 Method 8260D/5030B <0.5 pg/L 07/23/2024 Vinyl chloride SW 846 Method 8260D/5030B <0.5 pg/L 07/23/2024 Formaldehyde SW846 8315A 62.0 pg/L 07/19/2024 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353 2 Rev. 2.0, 1993 < 0.02 mg/L 07/18/2024 Nitrate+Nitrite-Nitrogen EPA 353 2, Rev. 2.0, 1993 0.08 mg/L 07/22/2024 Nitrate Nitrogen Subtraction Method 0.08mg/L 07/22/2024 Total Nitrogen (Cale) Total Keldahl Nitrogen (TKN) EPA 351 2, Rev. 2.0, 1993 365 mg/L 07/26/2024 Total Nitrogen Total Nitrogen 365 mg/L 07/26/2024 Report #:: 2024-16350 Page 3 of 9 [env7irochem] ANALYTICAL & CONSULTING CHEMISTS WSP USA E&I Inc 5710 Oleander Drive , Suite 110 Wilmington NC 28405 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Aug 05, 2024 Customer PO #: Customer ID: 11070019 Report #: 2024-16350 Project ID: Bakelite Acme CLRS Lab ID Sample ID: 24-40397 Site: WWMW-02 Test Collect Date/Time 7/17/2024 9:30 AM Method Matrix Sampled by Water Client Results Date Analyzed Iron EPA 200.7 Rev. 4 4 1994 (Dissolved) 0.017 mg/L 07/24/2024 Manganese EPA 200 7 Rev 4 4 1994 (Dissolved) 0.153 mg/L 07/24/2024 Sulfate EPA 300 0 Rev. 2 1 1993 130 mg/L 07/18/2024 Ammonia Nitrogen EPA 350.1 Rev 2 0 1993 54.8 mg/L 07/23/2024 Total Dissolved Solids (TDS) SM 2540 c-2015 256 mg/L 07/18/2024 Total Phosphorus SM 4500 P (F-H)-2011 0.52 mg/L 07/26/2024 Sulfide SM 4500 S D-2011 <0.05 mg/L 07/24/2024 Total Organic Carbon (TOC) SM 5310 B-2014 8.3 mg/L 07/22/2024 1, 1, 1,2-Tetrachloroethane SW 846 Method 828OD15030B <0.5 µg/L 07/24/2024 1, 1, 1 -Trichloroethane SW B46 Method 8260D/5030B <0.5 pg/L 07/24/2024 1,1,2,2-Tetrachloroethane SW 846 Method 8260D/5030B <0.5 pg/L 07/24/2024 1,1,2-Trichloroethane SW 846 Method 826oD/5030B <0 5 pg/L 07/24/2024 1,1-Dtchloroethane SW 846 Method 8260D/5030B <0 5 pg/L 07/24/2024 1,1-Dichloroethene SW 846 Method 8260D/5030B <0.5 pg/L 07/24/2024 1,1-Dtchloropropene SW 846 Method 8260D/5030B <0.5 pg/L 07/24/2024 1,2,3-Trich lorobenzene SW 846 Method 826OD15030B <0.5 pg/L 07/24/2024 1,2,3-Trichloropropane SW 846 Method 826OD15030B <0.5 pg/L 07/24/2024 1,2,4-Trichlorobenzene SW 846 Method 826OD15030B <0.5 pg/L 07/24/2024 1,2,4-Trimethylbenzene SW 846 Method 8260015030E <0.5 pg/L 07/24/2024 1,2-Dibromo-3-Chloropropane SW 846 Method 8260015030B <0.5 pg/L 07/24/2024 1,2-Dibromoethane SW 846 Method 8260DI5030B <0.5 pg/L 07/24/2024 1,2-Dichlorobenzene SW 846 Method 8260DIS030B <0 5 pg/L 07/24/2024 1,2-Dichloroethane SW 846 Method 8260D/5030B <0 5 pg/L 07/24/2024 1,2-Dichloropropane SW 846 Method 8260D/5030B <0.5 pg/L 07/24/2024 1,3,5-Trimethylbenzene SW 8.46 Method 8260D15030B <0.5 pg/L 07/24/2024 1,3-Dichlorobenzene SW 846 Method 8260D/5030B <0 5 pg/L 07/24/2024 Report #' 2024-16350 Page 4 of 9 envirochem ANALYTICAL & CONSULTING CHEMISTS WSP USA E&I Inc 5710 Oleander Drive , Suite 110 Wilmington NC 28405 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 2" • 910.347.5843 Lab/Fax info�a!environmentalchemists-com Date of Report: Aug 05, 2024 Customer PO #: Customer ID: 11070019 Report #: 2024-16350 Project ID: Bakelite Acme CLRS 1, 3-Dichloropropane SW 846 Method 826OD15030B <0.5 pg/L 07/24/2024 1,4-Dichlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 07/24/2024 2,2-Dichloropropane SW 846 Method 8280D/5030B <0.5 pg/L 07/24/2024 2-Chlorotoluene SW 846 Method 826OD15030B <0.5 pg/L 07/24/2024 4-Chlorotoluene SW 846 Method 8260D/5030B <0.5 pg/L 07/24/2024 Benzene SW 846 Method 8260D/5030B <0.5 pg/L 07/24/2024 Bromobenzene SW 846 Method 8260D/5030B <0.5 pg/L 07/24/2024 Bromochloromethane SW 846 Method 8260D/5030B <0.5 pg/L 07/24/2024 Bromodichloromethane SW 846 Method 8260D/5030B <0.5 pg/L 07/24/2024 Bromoform SW 846 Method 8260D15030B <0.5 pg/L 07/24/2024 Bromomethane SW 846 Method 826OD15030B <0.5 pg/L 07/24/2024 Carbon tetrachloride SW 846 Method 8260D15030B <0.5 pg/L 07/24/2024 Chiorobenzene SW 846 Method 826OD15030B <0.5 pg/L 07/24/2024 Chloroethane SW 846 Method 8260015030E <0.5 pg/L 07/24/2024 Chloroform SW 846 Method 8260D150306 <0.5 pg/L 07/24/2024 Chloromethane SW 846 Method 8260D/5030B <0.5 pg/L 07/24/2024 cis- 1,2-Dichloroethene SW 846 Method 826OD150308 <0.5 pg/L 07/24/2024 cis-1,3-Dichloropropene SW 846 Method 8260DIS030B <0.5 pg/L 07/24/2024 Dibromochloromethane SW 646 Method 826OD15030B <0.5 pg/L 07/24/2024 Dibromomethane SW 846 Method 8260D/5030B <0.5 pg/L 07/24/2024 Dichlorodifluoromethane SW 846 Method 8260D/5030B <0.5 pg/L 07/24/2024 Ethylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 07/24/2024 Hexachlorobutadiene SW 846 Method 626OD15030B <0.5 pg/L 07/24/2024 Isopropylbenzene SW 846 Method 8260D/50308 <0.5 pg/L 07/24/2024 M+P Xylene SW 846 Method 8260D/50308 <1.0 pg/L 07/24/2024 Methylene chloride SW 846 Method 8260D/5030B <0.5 pg/L 07/24/2024 Naphthalene SW 846 Method 82600/5030B <0.5 pg/L 07/24/2024 n-Butylbenzene SW 846 Method 8260015030E <0.5 pg/L 07/24/2024 n-Propylbenzene SW 846 Method 826OD15030B <0.5 pg/L 07/24/2024 ortho-Xylene SW 646 Method 826OD15030B <0.5 pg/L 07/24/2024 Report #:: 2024-16350 Page 5 of 8 LL • ANALYTICAL & CONSULTING CHEMISTS WSP USA E&I Inc 5710 Oleander Drive , Suite 110 Wilmington NC 28405 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info a,environmentalchemists.com Date of Report: Aug 05, 2024 Customer PO #: Customer ID: 11070019 Report #: 2024-16350 Project ID: Bakelite Acme CLRS p-Isopropyltoluene SW B46 Method 8260D/5030B <0.5 pg/L 07/24/2024 sec-Butylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 07/24/2024 Styrene SW 846 Method 8260D/5030B <0.5 pg/L 07/24/2024 tert-Butylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 07/24/2024 Tetrachloroethene SW 846 Method 8260D/5030B <0.5 pg/L 07/24/2024 Toluene SW 846 Method 828OD15030B <0.5 pg/L 07/24/2024 Trans-1,2-Dichloroethene SW 846 Method 8260D15030B <0.5 pg/L 07/24/2024 Trans-1,3-dichloropropene SW 846 Method 826013/503013 <0.5 pg/L 07/24/2024 Trichloroethene SW 846 Method 8260D/5030B <0.5 pg/L 07/24/2024 Trichlorofluoromethane SW 846 Method 826013/503013 <0.5 pg/L 07/24/2024 Vinyl chloride SW 846 Method 826013/503013 <0.5 pg/L 07/24/2024 Formaldehyde SW846 8315A <50 pg/L 07/19/2024 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 0.22 mg/L 07/18/2024 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0, 1993 25.8 mg/L 07/22/2024 Nitrate Nitrogen Subtraction Method 25.6 mg/L 07/22/2024 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 2.0, 1993 41.8 mg/L 07/26/2024 Total Nitrogen Total Nitrogen 67.6 mg/L 07/26/2024 Report M. 2024-16350 Page 6 of 9 [en7virrochem] ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 * 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax info@environmentalchemists.com WWMW-03 NOT PART OF PERMIT MONITORING REQUIREMENTS WSP USA E&I Inc Date of Report: Aug 05, 2024 5710 Oleander Drive, Suite 110 Customer PO #: Wilmington NC 28405 Customer ID: 11070019 Attention: Report #: 2024-16350 Project ID: Bakelite Acme CLRS Lab ID Sample ID: 24-40398 Site: WWMW-03 Test Iron Manganese Sulfate Ammonia Nitrogen Total Dissolved Solids (TDS) Total Phosphorus Sulfide Total Organic Carbon (TOC) 1,1,1,2-Tetrachloroethane 1, 1, 1 -Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1, 3, 5-Trimethylbenzene 1, 3-Dichlorobenzene Collect Date/Time Matrix 7/17/2024 9:50 AM Water Method EPA 200.7, Rev. 4.4, 1994 (Dissolved) EPA 200.7, Rev. 4.4, 1994 (Dissolved) EPA 300.0, Rev. 2.1, 1993 EPA 350.1, Rev, 2.0, 1993 SM 2540 C-2015 SM 4500 P (F-H)-2011 SM 4500 S D-2011 SM 5310 B 2014 SW 846 Method 8260D15030B SW 846 Method 8260D15030B SW 846 Method 826OD/50308 SW 846 Method 8260D/503013 SW 846 Method 8260D15030B SW 846 Method 8260D/5030B SW 846 Method 8260D/5030B SW 846 Method 8260D/5030B SW 846 Method 8260D/5030B SW 846 Method 8260D150308 SW 846 Method 826OD15030B SW 846 Method 826OD15030B SW 846 Method 8260D/5030B SW 846 Method 8260D/5030B SW 846 Method 8260D/5030B SW 846 Method 8260D/5030B SW 846 Method 8260D/5030B SW 846 Method 8260D15030B Results Sampled by Client Date Analyzed 0.088 mg/L 07/24/2024 0.043 mg/L 07/24/2024 19 mg/L 07/18/2024 160 mg/L 07/23/2024 311 mg/L 07/18/2024 0.41 mg/L 07/26/2024 1.08 mg/L 07/24/2024 13.3 mg/L 07/22/2024 <0.5 pg/L 07/25/2024 <0.5 pg/L 07/25/2024 <0.5 pg/L 07/25/2024 <0.5 pg/L 07/25/2024 <0.5 pg/L 07/25/2024 <0.5 pg/L 07/25/2024 <0.5 pg/L 07/25/2024 <0.5 pg/L 07/25/2024 <0.5 pg/L 07/25/2024 <0.5 pg/L 07/25/2024 <0.5 pg/L 07/25/2024 <0.5 pg/L 07/25/2024 <0.5 pg/L 07/25/2024 <0.5 pg/L 07/25/2024 <0.5 pg/L 07/25/2024 <0.5 pg/L 07/25/2024 <0.5 pg/L 07/25/2024 <0.5 pg/L 07/25/2024 Report #: 2024-16350 Page 7 of 9 roww--. Environmental Chemists, Inc. envirochem W2 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info",t environmentalchcmists.com WWMW-03 NOT PART OF PERMIT MONITORING REQUIREMENTS WSP USA E&I Inc Date of Report: Aug 05, 2024 5710 Oleander Drive , Suite 110 Customer PO #: Wilmington NC 28405 Customer ID: 11070019 Attention: Report #: 2024-16350 Project ID: Bakelite Acme CLRS 1,3-Dichloropropane SW 846 Method 8260015030E <0.5 pg/L 07/25/2024 1,4-Dichlorobenzene SW 846 Method 826OD15030B <0.5 pg/L 07/25/2024 2,2-Dichloropropane SW 846 Method 8260D/5030B <0.5 pg/L 07/25/2024 2-Chlorotoluene SW 846 Method 8260D/5030B <0.5 pg/L 07/25/2024 4-Chlorotoluene SW 846 Method 8280D150308 <0.5 pg/L 07/25/2024 Benzene SW 846 Method 8260D/5030B <0.5 pg/L 07/25/2024 Bromobenzene SW 846 Method 8260D15030B <0.5 pg/L 07/25/2024 Bromochloromethane SW 846 Method 8260D/5030B <0.5 pg/L 07/25/2024 Bromodichloromethane SW 846 Method 8260D150308 <0.5 pg/L 07/25/2024 Bromoform SW 846 Method 826OD15030B <0.5 pg/L 07/25/2024 Bromomethane SW 846 Method 8260D 50308 <0.5 pg/L 07/25/2024 Carbon tetrachloride SW 846 Method 8260D 50308 <0.5 pg/L 07/25/2024 Chlorobenzene SW 846 Method 826OD15030B <0.5 pg/L 07/25/2024 Chloroethane SW 846 Method 8260DIS030B <0.5 pg/L 07/25/2024 Chloroform SW 846 Method 826oD/50308 <0.5 pg/L 07/25/2024 Chloromethane SW 846 Method MOD15030B <0.5 pg/L 07/25/2024 cis- 1,2-Dichloroethene SW 846 Method 826OD15030B <0.5 pg/L 07/25/2024 cis- 1,3-Dichloropropene SW 846 Method 8260D/5030B <0.5 pg/L 07/25/2024 Dibromochloromethane SW 846 Method 826OD15030B <0.5 pg/L 07/25/2024 Dibromomethane SW 846 Method 8260D15030B <0.5 pg/L 07/25/2024 Dichlorodifluoromethane SW 846 Method 8260D1503GB <0.5 pg/L 07/25/2024 Ethylbenzene SW 846 Method 8260D15030B <0.5 pg/L 07/25/2024 Hexachlorobutadiene SW 846 Method 826OD150308 <0.5 pg/L 07/25/2024 Isopropylbenzene SW 846 Method 826OD15030B <0.5 pg/L 07/25/2024 M+P Xylene SW 846 Method 826OD15030B <1.0 pg/L 07/25/2024 Methylene chloride SW 846 Method 8260D/5030B <0.5 pg/L 07/25/2024 Naphthalene SW 846 Method 8280D/5030B <0.5 pg/L 07/25/2024 n-Butylbenzene SW 846 Method 8260D/50308 <0.5 pg/L 07/25/2024 n-Propylbenzene SW 846 Method 826OD15030B <0.5 pg/L 07/25/2024 ortho-Xylene SW 846 Method 8260D/5030B <0.5 pg/L 07/25/2024 Report #-: 2024-1635o Page 8 of 9 F"00- 0 "1"7 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com WWMW-03 NOT PART OF PERMIT MONITORING REQUIREMENTS WSP USA E&I Inc Date of Report: Aug 05, 2024 5710 Oleander Drive, Suite 110 Customer PO #: Wilmington NC 26405 Customer ID: 11070019 Attention: Report #: 2024-16350 Project ID: Bakelite Acme CLRS p-Isopropyltoiuene SW 846 Method 826OD15030B <0.5 pg/L 07/25/2024 sec -Butyl benzene SW 846 Method 8260D/5030B <0.5 pg/L 07/25/2024 Styrene SW 846 Method 826OD15030B <0.5 pg/L 07/25/2024 tert-Butyl benzene SW 846 Method 826OD15030B <0,5 pg/L 07/25/2024 Tetrachloroethene SW 846 Method 826OD15030B <0.5 pg/L 07/25/2024 Toluene SW 846 Method 826OD15030B <0.5 pg/L 07/25/2024 Trans-1,2-Dichloroethene SW 846 Method 826OD15030B <0.5 pg/L 07/25/2024 Trans-1,3-dichloropropene SW 846 Method 8260015030E <0.5 pg/L 07/25/2024 Trichloroethene SW 846 Method 8260015030B <0.5 pg/L 07/25/2024 Trichlorofluoromethane SW 846 Method 826OD15030B <0.5 pg/L 07/25/2024 Vinyl chloride SW 846 Method 8260D15030B <0.5 pg/L 07/25/2024 Formaldehyde SW846 8315A <50 pg/L 07/19/2024 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 0.02 mg/L 07/18/2024 Nitrate+Nitrate-Nitrogen EPA 353.2, Rev. 2.0, 1993 0.19 mg/L 07/22/2024 Nitrate Nitrogen Subtraction Method 0.17 mg/L 07/22/2024 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 355.2, Rev. 2.0, 1993 121 mg/L 07/26/2024 Total Nitrogen Tutal Nitrogen 121 mg/L 07/26/2024 Comment Sample 40395 and40395 Dup had pH > 2 Reviewed by: Report #. 2024.16350 Page 9 of Cnviroehem) ANALYTICAL & CONSULTING CHEMISTS LCS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info;a:environmentalchemists.com WSP QC - 2024-16350 Parameter True Value m /L Result mg'L % Recovery Limits % Ammonia 5.0 5.4 108 90-110 Iron 2.00 2.02 101 90-110 Manganese 1.00 1.00 100 90-110 NO2 0.60 0.54 90 90-110 NO3 & NO2 1.00 1.01 101 90-110 Sulfate 50.0 47.0 94 90-110 TDS 600 600 100 90-110 Sulfide 0.50 0.47 94 90-110 TOC 10.0 10.5 105 90-110 TKN 4.0 3.9 98 1 90-110 TP 1.60 1.56 98 1 90-110 MS/MSD Parameter True Value mg;-'L Recovery mg/L Recovery % Difference Limits % Recovery Limits % Difference Ammonia 4.0 4.0/3.9 100/98 2 80-120 <20 Iron 1.00 1.02/0.95 102/95 7 80-120 <20 Manganese 0.100 0.101/0.098 101 `98 3 80-120 :5 20 NO2 0.50 0.51 /0.51 1021,102 102 0 80-120 < 20 NO3 & NO2 0.50 0.49/0.49 98.'98 0 80-120 :5 20 Sulfate 10.0 8.2/8.2 82/82 0 80-120 <20 TDS N. A N/A N/A N/A 80-120 < 20 Sulfide 0.50 0.43/0.44 86,188 2 70-130 < 30 TOC 5.0 5.2 104 N/A 80-120 <20 TKN 4.0 4.1/4.1 102/102 0 80-120 :520 TP 1.60 1.35/1.29 8411 3 80-120 <_ 20 Environmental Chemists, Inc. envirochem ANALYTICAL. & CONSULTING CHEMISTS DUPLICATE SAMPLES 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info(?environmentalchemists.com Parameter Results M9 L % Difference Limits Ammonia N/A N; A NiA < 10 Iron N/A NIA N/A N/A Manganese N/A NIA N/A N/A NO2 N/A N/A N/A <_ 10 NO3 & NO2 N/A N/A N/A < 20 Sulfate <5 <5 0 < 10 TDS 413 413 0 < 10 Sulfide <0.05 <0.05 0 < 10 TOC 2.9 2.9 0 < 10 TKN N/A N/A N/A <10 TP N/A N/A NIA <10 BLANK Parameter Results M91L Limit mg"E Ammonia <0.1 0.1 Iron �-0.005 0.005 Manganese <=0.005 0.005 NO2 <0.01 0.01 NO3 & NO2 <0.01 0.01 Sulfate <2.5 2.5 TDS <2.5 2.5 Sulfide <0.025 0.025 TOC <0.25 0.25 TKN <0.25 0.25 TP <0.02 0.02 Client Sample Results Client: Environmental Chemists Inc Project/Site: 40395,40397,40398 Client Sample ID: #40395 Date Collected: 07117124 09:10 Date Received: 07/18/24 10:09 Method: SW846 8315A - Carbonyl Compounds by HPLC Analyte Result Qualifier RL Formaldehyde 62 50 Unit ug/L Job ID: 705-2135-1 Lab Sample ID: 705-2135-1 Matrix: Water D Prepared Analyzed Dil Fac 07119/24 12-28 07/19/24 20-32 1 Eurofins Atlanta Page 8 of 15 r , _ 1 „ 3'�O T26'2024 Client Sample Results Client: Environmental Chemists Inc Job ID: 705-2135-1 Project/Site 40395,40397,40398 Client Sample ID: #40392 Lab Sample ID: 705-2135-2 Date Collected: 07/17/24 09:30 Matrix: Water Date Received: 07/18124 10:09 Method: SW846 8315A - Carbonyl Compounds by HPLC Analyte Result Qualifier RL Unit D Prepared Analyzed_ Dill Fac Formaldehyde ND 5o u91 07/19/24 12.8 07l19/24 20 43 1 Eurofins Atlanta Page 9 of 15 7/26/2024 Client Sample Results Client: Environmental Chemists Inc Project/Site: 40395, 4 0397.40398 Client Sample ID: #40398 Date Collected: 07/17/24 09:50 Date Received: 07118f24 10:09 ~Method: SW846 8315A - Carbonyl Compounds by HPLC Analyte Result Qualifier RL Formaldehyde ND 5Q Job ID:705-2135-1 Lab Sample ID: 705-2135-3 Matrix: Water Unit D Prepared Analyzed ail Fac uj/L 07/19/24 12:28 07/19/24 20-54 1 Eurofins Atlanta Page 10 of 15 7/26/2024 n 3 a 3 C. M N o _ 0. 131 t� n O 3 C fD o N S rD fD a 3 W a Sample Type C)H4P1(-)+(Dc) % n (-Aan Composite J1 or Grab G) 0 G) 6) ® G) GZ -0 G) T L71 Container 7 S r Q Chlorine ::11% mg1L a pH of bottle m Q LAB ID a ch NUMBER NONE HCL W — H2SO4 M HNO3 M NAOH D THIO I <' CD O Q FILTERED Z W OTHER Z 1 —{ c7o (57 1' W p } Cti m JD 3 s ca N lu 0 M a I I in rD a� 3 CA O 11 CA O CA r u N a ro A O M rn zZ n v c` m z p X v O O m z -i T Drn 0 O z z A Zr v 2 0 2 o r rn N v m 0 � o z y w -4 zN 0 N � � � co CL f9 O 7 v a c-' M a — m 3 0 fD o c � M m CL 3 W V Sample Type Composite or Grab (A 0 a 6) o a -0 Container (P or G) M Chlorine � .. a NM Q - mg1L ITI - � h 11 pH of bottle j 3 C l CD 7 LAB ID 'Y NUMBER m rn N NONE HCL m - H2SO4 HNO3 IT! NAOH CD < I < < M THIO � o„ FILTERED 12 z W 1,. -D OTHER d 3 I � U (", Pu C r N II N Q X C p as r m a fJ t0 `-� N C 0 0 r r m n O z D z v 0 z 0 n 0 c N 0 v 0 0 3 M y v e� rs M M 3 a 2) c v X c"o (n 3 z X .a 0 O czc C M z 0 a �o N � a a 61 y CL � e lw W o' —tt v lit (D 0 M tD o c � M a 3 3 W Sample Type o 0 � n 0 0 Composite or Grab c) Container (P or G) Chlorine mglL pH of bottle <D LAB ID NUMBER CP NONE HCL {� -- H2SO4 m N HNO3 M NAOH D < ' TH I O O a W FILTERED Z OTHER LtJ m ch ro m 0 O r r rn 0 O z D z v n 2 Z O 0 C 1) O v