WQ0018087_Monitoring - 07-2024_20240730

C\\alppoeklyea
July 29, 2024
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Subject: Permit No. WQ0018087
Cape Fear Manufacturing Facility
Surface Disposal of Class B Residuals (Dedicated)
Brunswick County
Dear Division of Water Resources:
The following information is being submitted electronically:
1) Compliance and Monitoring Form (GW-59) for the 6 wells associated with the Sludge Disposal Unit.
2) Laboratory analysis for these same wells.
3) Compliance Report Form GW-59A.
4) Summary of the Groundwater Monitoring Results.
As shown in the summary, some of the results are above permit limits. However, these results remain consistent
with previous results. The regional office has received this data.
No additional actions are planned at this time.
If additional information is needed, please feel free to contact me at 704-560-7570 or Larry Young at 910-264-
2564.
Best Regards,
Jeff Ross
Global Safety Health and Environmental Director
Alpek Polyester USA, LLC
Alpek Polyester USA, LLC
7621 Little Ave, Suite 5009 Charlotte, NC 28226
877-432-2766(toll-free) 9 704-940-7500(main) • www.alpekpolyester.com

GW-59A COMPLIANCE REPORT FORM Permit #WQ0018087
(Submit one each monitoring period with GW-59 forms.)
j
Enter date monitoring results were due. (U7I31/2024 ) Will this monitoring report (GW-59 and GW-59A)
YES
NO
be submitted after the established due date?
X
2
Was any required information missing on the GW-59 report forms?
YES
NO
X
iF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the requited information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
identification plate, area overgrown, etc.)? If the answer is "Yes ", contact the Regional Officefor guidance.
X
4
Are any monitored constituents equal to or above the established standards?
YES
NO
X
If the answer to question 4 is "NO", skip to section 8.
if the answer to question 4 is "YES" list the affected wells individually with constituents) and concentration(s)
exceeding standards in the space provided below:
See attached summary of groundwater results
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
YES
NO
same constituent(s) in the same well(s) in the last two years?
X
If the answer to question 5 is "NO", skip to section 8.
If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years).
See attached summary of groundwater results
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
X
If the answer is "YES", a groundwater quality problem maybe occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. if the answer is "NO", monitoring wells may be improperly
located, contact the Regional Office.
7
Is the permittee implementing previously approved actions required by the Division involving this
groundwater quality problem?
YES
X
NO
If the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation,
fines, and/or penalties.
The regional office has asked that we continue to monitor per the permit.
8
The person completing this portion (GW-59A) of the monitoring report should sign below and submit this
form with GW-59 forms for required wells to the address provided at the top of the current G W-59 form.
I hereby acknowledge that the above information was evaluated and the information submitted in this
report (Compliance Report GW-59A) is true and complete to the best of my knowledge.
Signature of Permittee (or Authorized Agent) Date
GW-59A 12/8/2003

Cape Fear Sludge Disposal Unit Monitoring Well Permit Standard Exceedances 2020 to Present
Parameter
Permit
Standard
Units
MW-2A
Dec-21 Dec-22 Dec-23 Jun-24
Cobalt
0.001
mg/l
0.002
0.002
1 0.003
0.003
Parameter
Permit
Standard
Units
MW-2B*
Dec-20 Jun-21 Jun-22 Jun-23 Dec-23 Jun-24
Ammonia Nitrogen
1.5
mg/L
32.9
18.0
40.5
32.5
36.8
23.8
Total Dissolved Solids
500
mg/L
692
845
750
758
723
Arsenic
0.01
mg/L
0.02
0.02
0.016
0.026
0.015
0.042
Cobalt
0.001
mg/L
0.022
0.013
0.010
0.009
0.013
Lead
0.015
mg/l
0.019
Methylene Chloride
0.05
ug/l
0.57
Parameter
Permit
Standard
Units
MW-2C*
Dec-20 Jun-21 Jun-22 Jun-23 Dec-23 Jun-24
Total Dissolved Solids
500
mg/L
504
744
621
621
624
572
Nitrate
10
mg/t
21.2
15.5
11.3
12.0
Arsenic
0.01
mg/l
0.014
0.015
Cobalt
0.001
mg/t
0.021
0.019
0.019
0.022
0.022
Lead
0.015
mg/t
0.021
pH
5.5
5.13
5.31
Parameter
Permit
Standard
Units
MW-2D* *
Jun-21 Jun-22 Dec-22 Jun-23 Dec-23 Jun-24
Ammonia Nitrogen
1.5
mg/L
57.3
38.8
43.7
33.6
41.3
40.1
Arsenic
0.01
mg/L
0.02
0.021
0.011
0.02
Cobalt
0.001
mg/L
0.003
0.003
0.002
0.006
Methylene Chloride
0.05
ug/t
I
1 0.53

Parameter
Permit
Standard
Units
MW-2E
Dec-20 Jun-21 Dec-21 Jun-22 Dec-22 Jun-23 Dec-23 Jun-24
Ammonia Nitrogen
1.5
mg/l
5.5
3.3
8.4
3.3
22.9
39.2
34.8
18.2
Arsenic
0.01
mg/l
0.013
Lead
0.015
mg/l
0.005
0.004
0.003
0.003
0.006
0.005
0.005
Methylene Chloride
0.05
ug/t
I
1
9
1
1 0.58
Parameter
Permit
Standard
Units
M W-3A* * *
Jun-22
Methylene Chloride
0.05
ug/l
0.64
pH
5.5
5.38
* Dry in December, 2021 and December, 2022
** Dry in December 2021
*** Background Welt

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
�^+;'?T S �•�$—'
(VISISKON OF WATER QUAL'IT`/ INFORMATION�PROCESSING UNIT
COMPLIANCE REPORT FORM
817N11►tG SERVICE_�EI�T£R RALEIGH NC276991617 :Phone:.(919)a733r3221
PERMIT Number: WQ0018087 Expiration Date: Jan. 31, 2027
FACILITY INFORMATION Please PrintCleadyorType
Facility Name: Alpek Polyester/DAK Americas LLC,
Cape Fear Site
Non -Discharge UIC
NPDES Other
Permit Name (if different):
Facility Address: 3216 Cedar Creek Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Fayetteville (Street) NC 28312 County Brunswick
(city) (State) (Zip)
❑ Spray Field ❑ Remediation:
Contact Person: Matthew Hendrickson
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Down Gradient/Monitoring Well # 2A No. of wells to be sampled: 6
❑ Water Source Heat Pump ® Other: Surface Disposal Res.Sol
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW # 2A
Date sample collected:
06/20/24
FIELD ANALYSES:
WAS
Well Depth: 13.0 ft.
Well Diameter:
2.0 in.
pH 6.4 units Temp. 20.3 °C
DRY at
Depth to Water Level: 7.7 ft. below measuring point
Screened Interval:
3.0 ft. to 13.0
ft. Spec. Cond. µMhos
time of
MeasuringPoint is 1.92 ft. above land surface
Relative M.P. Elevation:
20.39 ft.
Odor Sulfur (Mild)
sampling,
check
Volume of water pumped/bailed before sampling:
3 gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered: ®YES
❑ NO and field acidified: [EYES
❑ NO
LABORATORY INFORMATION
Date sample analyzed: 06/20/24 - 06/27/24
Laboratory Name: Envirochem
Certification No. 37729
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
<0.02 mg/I
Pb - Lead <0.01 mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
0.05 mg/I
Zn - Zinc <0.01 mg/I
Coliforw MF Total /100mI
Phosphorus. Total as P
0.06 mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 284 mg/I
Al - Aluminum
mg/I
Cobalt - 0.003 mg/I
pH (when analyzed) 6.6 units
Ba - Barium
mg/I
Selenium - <0.01 mg/I
TOC mg/I
Ca - Calcium
mg/I
Chloride <5 mg/I
Cd - Cadmium
<0.001 mg/I
Arsenic <0.01 mg/I
Chromium: Total
<0.01 mg/I
Grease and Oils mg/I
Cu - Copper
<0.01 mg/l
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/l
Hg - Mercury
<0.0002 mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method #
Total Ammonia 0.5 mg/I
Mg - Magnesium
2.66 mg/I
method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
method #
TKN as N mg/I
Ni - Nickel
<0.01 mg/1
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Jeff Ross - Global Safety, Health & Environmental Director 7/ 2g12oa
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of PernIffittee (or ruthanzed Agent) (Date)
GW-59 Rev.1/2007

oummi i rumm u1V I — I UVV r/iYCK UNL7
ROUNDWATER QUALITY MONITORING:
OMPLIANCE REPORT FORM
FACILITY INFORMATION crease runt weany or r ype
Facility Name: Alpek Polyester/DAK Americas LLC, Cape Fear Site
Permit Name (if different):
Facility Address: 3216 Cedar Creek Road
Fayetteville (S`r`et) NC 28312 County Brunswick
(C't) (State) (Zip)
Contact Person: Matthew Hendrickson _ Telephone#: [phone]
Well Location/Site Name: Down Gradient/Monitoring Well # 2B No. of wells to be sampled: 6
PERMIT Number: WQ0018087 Expiration Date: Jan. 31, 2027
Non -Discharge UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
❑ Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump © Other: Surface Disposal Res.Sol
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW # 2B
Date sample collected: 06/20/24
FIELD ANALYSES:
WAS
Well Depth: 13 ft.
Well Diameter: 2.0 in.
pH 6.7 units Temp. 21.8 °C
DRY at
Depth to Water Level: 10.7 ft, below measuring point
Screened Interval: 3 ft. to 13 ft.
Spec. Cond. µMhos
time of
Measuring Point is 2•9 ft. above land surface
Relative M.P. Elevation: 24 ft.
Odor Musty
sampling,check
Volume of water pumped/bailed before sampling:
5 gallons
Appearance Tan/Turbid
here: ❑
Samples for metals were collected unfiltered: ®YES
❑ NO and field acidified: ® YES El NO
sample analyzed: 06/20/24 - 06/27/24 Laboratory Name: Envirochem
IAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
mg/I
Nitrite (NO2) as N
0.03 mg/I
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
0.03 mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
0.67 mg/I
(No'.e: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Dissolved Solids: Total
723 mg/l
Al - Aluminum
mg/I
pH (when analyzed)
6.6 units
Ba - Barium
mg/I
TOC
mg/l
Ca - Calcium
mg/I
Chloride
12 mg/l
Cd - Cadmium
<0.001 mg/I
Arsenic
0.042 mg/l
Chromium: Total
0.033 mg/I
Grease and Oils
mg/l
Cu - Copper
0.012 mg/I
Phenol
mg/l
Fe - Iron
mg/I
Sulfate
mg/I
Hg - Mercury
<0.0002 mg/I
Specific Conductance
µMhos
K - Potassium
mg/I
Total Ammonia
23.8 mg/I
Mg - Magnesium
8.37 mg/1
(Ammonia Nitrogen; N1­13as N, Ammonia Nitrogen, Total)
Mn- Manganese
mg/I
TKN as N
mg/I
Ni - Nickel
<0.01 mg/I
Certification No. 37729
Pb - Lead 0.019 mg/I
Zn - Zinc 0.031 mg/I
Other (Specify Compounds and Concentration Units):
Cobalt - 0.013 mg/1
Selenium - <0.01
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Report Attached? ® Yes (1) ❑ No (0)
VOC . method #
method #
method #
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Jeff Ross - Global Safety, Health & Environmental Director
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.112007
Signature of Permittee (or Authorized Aqent)
/y17 /zca

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
IVISION 0P ATER.QUALI. 4NFOR'M M N"PROCESSING UNIT
• •
COMPLIANCE REPORT FORM
617 MAIL SERVICE CENTER RALEIGH, NC 27699-1617 .Phone; [phone] r•
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: WQ0018087
Expiration Date: Jan. 31, 2027
Facility Name: Alpek Polyester/DAK Americas LLC, Cape Fear Site
Non -Discharge
UIC
Permit Name (if different):
NPDES
Other
Facility Address: 3216 Cedar Creek Road
TYPE OF PERMITTED OPERATION
BEING MONITORED
Fayetteville (streat) NC 28312 County Brunswick
❑ Lagoon
❑ Remediation: Infiltration Gallery
(City) (State) (Zip)
❑ Spray Field
❑Remediation:
Contact Person: Matthew Hendrickson Telephone#: [phone]
❑ Rotary Distributor
❑ Land Application of Sludge
Well Location/Site Name: Down Gradient/Monitoring Well # 2C No. of wells to be sampled: 6
❑ Water Source Heat Pump
❑?C Other: Surface Disposal Res.Sol
WELL ID NUMBER (from Permit): MW # 2C _ Date sample collected: 06/20/24
Well Depth: 13 ft. Well Diameter: 2.0 in.
Depth to Water Level: 8.3 ft. below measuring point Screened Interval: 3 ft. to 13 ft.
Measuring Point is 3.05 ft. above land surface Relative M.P. Elevation: 25 ft.
Volume of water pumped/bailed before sampling: 5 gallons
Samples for metals were collected unfiltered: ®YES ❑ NO and field acidified: 5dYES ❑ NO
FIELD ANALYSES:
pH 5.9 units
Spec. Cond.
Odor None
Appearance Tat
If WELL
Temp. 20.5 °C DRY at
µMhos time of
sampling,
I sample analyzed: 06/20/24 - 06/27/24
Laboratory Name: Envirochem
Certification No. 37729
AMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
mg/I
Nitrite (NO2) as N
0.07 mg/l
Pb - Lead 0.021 mg/I
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
8.96 mg/I
Zn - Zinc 0.041 mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
1.44 mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/l
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
572 mg/I
Al -Aluminum
mg/I
Cobalt - 0.022 mg/1
pH (when analyzed)
6.1 units
Ba - Barium
mg/I
Selenium - <0.01 mg/I
TOC
mg/I
Ca - Calcium
mg/I
Chloride
12 mg/I
Cd - Cadmium
<0.001 mg/I
Arsenic
0.015 mg/I
Chromium. Total
0.034 mg/I
Grease and Oils
mg/I
Cu - Copper
0.016 mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
mg/I
Hg - Mercury
<0.0002 mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance
µMhos
K - Potassium
mg/I
VOC method #
Total Ammonia
< 0.2 mg/l
Mg - Magnesium
10.1 mg/I
method #
(Ammonia Nitrogen, NH, as N; Ammonia
Nitrogen, Total)
Mn - Manganese
mg/I
, method #
TKN as N
mg/I
Ni - Nickel
0.022 mg/I
method #
For Remedlation Systems Only .. • • •
I certify that to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a
DWQ-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
Jeff Ross - Global Safety, Health & Environmental Director
Permittee (or Authorized Aqent) Name and Title- Please pnnt - Signature . - D-
GW-59 Rev. 1 fi
here: ❑

SUBMIT FORM ON YELLOW PAPER ONLY
ROUNDWATER QUALITY MONITORING:
OMPLIANCE REPORT FORM
Please Print Clearly or Type
Facility Name: Alpek Polyester/DAK Americas LLC, Cape Fear Site
Permit Name (if different):
Facility Address: 3216 Cedar Creek Road
Fayetteville (Stfeet) NC 28312 County Brunswick
(city) (State) (zip)
Contact Person: Matthew Hendrickson Telephone#: [phone]
Well Location/Site Name: Down Gradient/Monitoring Well # 2D No. of wells to be sampled: 6
PERMIT Number: WQo018087
Non -Discharge
NPDES
Expiration Date
UIC
Other
Jan. 31,
PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
❑ Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump 0 Other: Surface Disposal Res. Sol
If WELL
WELL ID NUMBER (from Permit): MW # 2D
Well Depth: 13 ft.
Depth to Water Level: 8.7 ft. below measuring point
Measuring Point is 3.0 ft. above land surface
Volume of water pumped/bailed before sampling:
Samples for metals were collected unfiltered: ®YES
Date sample collected: 06/20/24
Well Diameter: 2.0 in.
Screened Interval: 3 ft. to 13 ft.
Relative M.P. Elevation: 22 ft.
3 gallons
❑ NO and field acidified: ® YES ❑ NO
FIELD ANALYSES:
pH 6.5 units Temp. 22.1 °C
Spec. Cond. µMhos
Odor Sulfur
Appearance Clear
WAS
DRY at
time of
sampling,
check
here: ❑
LABORATORY INFORMATION
Date sample analyzed: 06/20/24 - 06/27/24
Laboratory Name: Envirochem
Certification No. 37729
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
0.11 mg/l
Pb - Lead 0.013 mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
<0.02 mg/I
Zn - Zinc 0.033 mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
0.96 mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/1
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 235 mg/I
Al -Aluminum
mg/I
Cobalt - 0.006 mg/I
pH (when analyzed) 6.6 units
Ba - Barium
mg/I
Selenium - <0.01
TOC mg/l
Ca - Calcium
mg/I
Chloride 5 mg/I
Cd - Cadmium
<0.001 mg/I
Arsenic 0.020 mg/I
Chromium: Total
0.041 rri
Grease and Oils mg/I
Cu - Copper
<0.010 mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
<0.0002 mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance AlMhos
K - Potassium
mg/I
VOC method #
Total Ammonia 40.1 mg/I
Mg - Magnesium
4.41 mg/I
method #
(Ammonia Nitrogen; 11113as N; Ammonia Nitrogen, Total)
Mn - Manganese
mg/1
, method #
TKN as N mg/I
Ni - Nickel
<0.01 mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Jeff Ross - Global Safety, Health & Environmental Director _ �- 71,;—;q `2262—
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee uthorized Agent) (Date)
GW-59 Rev.112007

SUBMIT FORM ON YELLOW PAPER ONLY
ROUNDWATER QUALITY MONITORING:
OMPLIANCE REPORT FORM
FACILITY INFORMATION Please PnntCleadyorType
Facility Name: Alpek Polyester/DAK Americas LLC, Cape Fear Site
Permit Name (if different):
Facility Address 3216 Cedar Creek Road
Fayetteville (StfCe{) NC 28312 County Brunswick
(City) [State) (Zip)
Contact Person: Matthew Hendrickson Telephone#: [phone]
Well Location/Site Name: Down Gradient/Monitoring Well # 2E No. of wells to be sampled: 6
�1B1.733 3229 ,.
PERMIT Number: WQ0018087 Expiration Date: Jan. 61, ZUZ/
Non -Discharge UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
❑ Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump R3 Other: Surface Disposal Res.Sol
-LID NUMBER (from Permit): MW # 2E _ Date sample collected: 06/20/24
1 Depth: 13 ft. Well Diameter: 2.0 in.
th to Water Level: 8.3 ft. below measuring point Screened Interval: 3 ft. to 13 ft,
Isuring Point is 3•0 ft. above land surface Relative M.P. Elevation: 23 ft.
ime of water pumped/bailed before sampling: 3 gallons
soles for metals were collected unfiltered: ®YES ❑ NO and field acidified: ® YES ❑ NO
Date sample analyzed: 06/20/24 - 06/27/24 Laboratory Name: Envirochem
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
mg/I
Nitrite (NO2) as N
0.12 mg/I
Coliform: MF Fecal
/100m1
Nitrate (NO3) as N
0.34 mg/I
Coliform: MF Total
1100ml
Phosphorus: Total as P
1.31 mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Dissolved Solids: Total
161 mg/I
Al -Aluminum
mg/I
pH (when analyzed)
6.6 units
Ba - Barium
mg/I
TOC
mg/I
Ca - Calcium
mg/I
Chloride
9 mg/I
Cd - Cadmium
<0.001 mg/I
Arsenic
<0.01 mg/I
Chromium: Total
0.013 mg/1
Grease and Oils
mg/I
Cu - Copper
<0.01 mg/1
Phenol
mg/I
Fe - Iron
mg/I
Sulfate
mg/I
Hg - Mercury
<0.0002 mg/I
Specific Conductance
µMhos
K - Potassium
mg/I
Total Ammonia
18.2 mg/I
Mg - Magnesium
2.39 mg/I
(Ammonia Nitrogen: NH,ias N: Ammonia
Nitrogen, Total)
Mn -Manganese
mg/I
TKN as N
mg/I
Ni - Nickel
<0.01 mg/I
FIELD ANALYSES:
pH 6.6 units
Spec. Cond.
Odor Mild Sulfur
Appearance Tan/Tint
WELL
Temp. 20.6 eC DRY at
µMhos time of
sampling,
Certification No. 37729
Pb - Lead <0.01 mg/I
Zn - Zinc <0.01 mg/I
Other (Specify Compounds and Concentration Units):
Cobalt - 0.005 mg/1
Selenium - <0.01 mg/I
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Report Attached? ® Yes (1) ❑ No (0)
VOC method #
method #
method #
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
term Rtee (Or AUmorizea Agent) Name ana i me- rieu5 print of type
GW-59 Rev.1/2007
701

JUrSIVII I r-UKIVI UN YLLLUVV YAt''LK UNLY
ROUNDWATER QUALITY MONITORING:
OMPLIANCE REPORT FORM
FACILITY INFORMATION Please PdntCleadyorType
Facility Name: Alpek Polyester/DAK Americas LLC, Cape Fear Site
Permit Name (if different):
Facility Address: 3216 Cedar Creek Road
Fayetteville ($ffeet) NC 28312 County Brunswick
(city) (state) (Zip)
ontact Person: Matthew Hendrickson Telephone#: [phone]
fell Location/Site Name: Background/Monitoring Well # 3A No. of wells to be sampled: 6
utNAH I MEN I GF HNVIR©NMrN1�l1RpbSOUi13CES
DIVISION OF WATER QUALITY•INFORNIATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 `,Phone:.[phone] -
PERMIT Number: wQo01so87 Expiration Date: ,fan. 31, 2027
Non -Discharge UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
❑ Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump X Other: Surface Disposal Res.Sol
LL ID NUMBER (from Permit): MW # 3A Date sample collected: 06/20/24
II Depth: 13.25 ft. Well Diameter: 2.0 in.
)th to Water Level: 5.8 ft. below measuring point Screened Interval: 3.25 ft. to 13.3 ft.
3suring Point is 1.76 ft. above land surface Relative M.P. Elevation: 24.78 ft.
ume of water pumped/bailed before sampling: 3 gallons
nples for metals were collected unfiltered: ®YES ❑ NO and field acidified: ® YES ❑ NO
ate sample analyzed: 06/20/24 - 06/27/24 Laboratory Name: Envirochem
ARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
mg/I
Nitrite (NO2) as N
<0.02 mg/I
Coliform: MF Fecal
/I00ml
Nitrate (NO3) as N
0.05 mg/I
Coliform: MF Total
/loom]
Phosphorus: Total as P
0.24 mg/I
(Note: Use MPN method for highly turbid
samples)
Orthophosphate
mg/I
Dissolved Solids: Total
168 mg/I
Al -Aluminum
mg/I
pH (when analyzed)
6.4 units
Ba - Barium
mg/I
TOC
mg/I
Ca - Calcium
mg/I
Chloride
16 mg/I
Cd - Cadmium
<0.001 mg/I
Arsenic
<0.010 mg/I
Chromium: Total
<0.010 mg/I
Grease and Oils
mg/I
Cu- Copper
<0.010 mg/I
Phenol
mg/I
Fe - Iron
mg/I
Sulfate
mg/I
Hg - Mercury
<0.0002 mg/I
Specific Conductance
µMhos
K - Potassium
mg/I
Total Ammonia
<0.3 mg/I
Mg - Magnesium
1.98 mg/I
(Ammonia Nitrogen; NH,as N; Ammonia
Nitrogen, Total)
Mn -Manganese
mg/I
TKN as N
mg/I
Ni - Nickel
<0.01 mg/I
FIELD ANALYSES:
pH 5.8 units
Spec. Cond.
Odor Mild Sulfur
Appearance Clear
If WELL
Temp. 19.7 eC DRY at
µMhos time of
sampling,
Certification No. 37729
Pb - Lead <0.010 mg/I
Zn - Zinc <0.01 mg/I
Other (Specify Compounds and Concentration Units):
Cobalt - <0.001 mg/I
Selenium - <0.01 ma/1
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Report Attached? ® Yes (1) ❑ No (0)
VOC method #
method #
method #
method #
N
For Remediation Systems Only Reports): • • •
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a
DWQ-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
Jeff Ross - Global Safety, Health & Environmental Director
7 1;-20A
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee . •_
GVV-59 Rev. 11

FF'"w- 741 Environmental Chemists, Inc.
W2 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
® 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 f 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
OAK Americas
Date of Report: Jul 03, 2024
1205 Culbreth Drive Suite 200
Customer PO #:
Wilmington NC 28405
Customer ID: 08100044
Attention:
Report #: 2024-14195
Project ID: Monitoring Well
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
24-34710 Site: MW-2A
6/20/2024
11:30 AM Water jcb/em
Test
Method
Results
Date Analyzed
Color
car
Clear
06/20/2024
Depth to water, ft.
Depth to water, Ft.
7.7 feet
06/20/2024
Copper
EPA 200.7, Rev 4A, 1994
<0.01 mg/L
06/26/2024
Lead
EPA 200.7, Rev 4.4, 1994
<0.01 mg/L
06/26/2024
Magnesium
EPA 200.7, Rev4A, 1994
2.66 mg/L
06/26/2024
Nickel
EPA 200.7, Rev 4.4,1094
<0.01 mg/L
06/26/2024
Selenium
EPA 200.7. Rev 4.4,104
<0.01 mg/L
06/26/2024
Zinc
EPA 200.7, Rev 4.4,1994
<0.01 mg/L
06/26/2024
Arsenic
EPA 200.7, Rev. 4 4. 1994
<0.01 mg/L
06/26/2024
Chromium
EPA 200.7, Rev 4.4.1994
<0.01 mg/L
06/26/2024
Cadmium
EPA 200.8, Rev. 5.4,19M
<0.001 mg/L
06/26/2024
Cobalt
EPA 200.8. Rev. 5.4, 1994
0.003 mg/L
06/26/2024
Mercury
EPA 245.1, Rev. &0.1994
<0.0002 mg/L
06/25/2024
Ammonia Nitrogen
EPA 350.1, Rev. 10,1993
0.5 mg/L
06/24/2024
Gallons bailed before sampling
Gam^$ Baia before sampling
3(dry) gallons
06/20/2024
Odor
QuVitative
Sulfur(Mild)
06/20/2024
Total Dissolved Solids (TDS)
SM 2540 C-2015
284 mg/L
06/20/2024
Temperature
SM 2550 B-2010
20.3 C
06/20/2024
pH
SM 4500 H B-2011
6.6 units
06/21 /2024
pH analyzed out of hold time of 15 minutes.
SM 4500 H 8-2011
6.4 units
06/20/2024
Total Phosphorus
SM 45M P (F•H)-2011
0.06 mg/L
06/2812024
Chloride
SM4500 ci E-2011
< 5 mg/L
06/24/2024
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0.1993
< 0.02 mg/L
06/20/2024
Nitrate+Nitrite-Nitrogen
EPA 353.2. Rev. 2 0.1993
0.06 mg/L
06/24/2024
Report * 2024-14195 Page 1 of 12

Lenviroche]m
Arta rnWAL & CONSULTING CHEMISTS
OAK Americas
1206 Culbreth Drive Suite 200
Wilmington NC 28405
Attention:
Environmental Chemists, Inc.
66M Windmill Way, Wilmington, NC 28405 8 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.4735702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 m 910.347.5843 Lab/Fax
info(olenvironmentalchemists.com
Date of Report: Jul 03, 2024
Customer PO 0:
Customer ID: 08100044
Report 0: 2024-14195
Project ID: Monitoring Well
Nitrate Nitrogen Subtracdon prod 0.05 mg/L 06/27/2024
Report k 2024-14196 Pa0e 2 of 12

r` iEnvironmental Chemists, Inc.
-716W2 Windmill Way, Wilmington, NC 28405 - 910.392,0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28W + 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info(wenvironmentalchemists com
DAK Americas
Date of Report: Jul 03, 2024
1205 Culbreth Drive Suite 200
Customer PO #:
Wilmington NC 28405
Customer ID: 08100044
Attention:
Report #: 2024-14195
Project ID: Monitoring Well
Lab ID Sample ID:
Collect Date/Time matrix Sampled by
24-34711 Site: MW 28
6/20/2024
9:55 AM Water jcb/em
Test
Method
Results
Date Analyzed
Color
COW
Tan/Turbid
06/20/2024
Depth to water, ft.
Depth to water, Ft.
10.7 feet
06/20/2024
Copper
EPA 200.7, Rev 4.4,1%4
0.012 mg/L
06/26/2024
Lead
EPA 200.7, Rev 4.4. 1994
0.019 mg/L
06/26/2024
Magnesium
EPA 200.7, Rev 4 4,1994
8.37 mg/L
06/26/2424
Nickel
EPA 200.7, Rev 4.4,1994
<0.01 mg/L
06/26/2024
Selenium
EPA 200.7, Rev 4.4. IM
<0.01 mg/L
06/26/2024
Zinc
EPA 200.7, Rev 4.4. 1994
0.031 mg/L
06/26/2024
Arsenic
EPA 200.7, Rev. 4.4, 1994
0.042 mg/L
06/26/2024
Chromium
EPA 200.7, Rev. 4 4,19"
0.033 mg/L
06/26/2024
Cadmium
EPA 200.8. Rev 5.4.1904
<0.001 mg/L
06/26/2024
Cobalt
EPA 200.8. Rev. 5.4,1994
0.013 mg/L
06/27/2024
Mercury
EPA 245.1. Rev. 3.0,1994
<0.0002 mg/L
06/26/2024
Ammonia Nitrogen
EPA 350.1, Rev. 2.0.1993
23.8 mg/L
06/24/2024
Gallons bailed before sampling
130ons Bailed before sampling
5.0 gallons
06/20/2024
Odor
Quay
Musty
06/20/2024
Total Dissolved Solids (TDS)
SM 2540 C-2015
723 mg/L
06/20/2024
Temperature
SM 2550 e-2010
21.8 C
06/20/2024
pH
SM 4500 H 8-2011
6.6 units
06/21 /2024
pH analyzed out of hold time of 15 minutes.
SM 4500 H B-2011
6.7 units
06/20/2024
Total Phosphorus
SM 4500 P (F-H) 2011
0.87 mg/L
06/28/2024
Chloride
SWS00 Cl E-2011
12 mg/L
06/24/2024
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA353.2, Rev. 2.o.19s3
0.03 mg/L
06/20/2024
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev_ 2.0,1993
0.06 mg/L
06/24/2024
Report #:: 2024-14195 Page 3 of 12

F077
envirochem
ANALYncN. $ coNsut nw CHB► WS
OAK Americas
1205 Culbreth Drive Suite 200
Wilmington NC 28405
Attention:
Environmental Chemists, Inc.
66M Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC MAO • 910.347.5843 Lab/Fax
info` �environmentalchemist&com
Date of Report: Jul 03, 2024
Customer P© #:
Customer ID: 08100044
Report #: 2024-14195
Project ID: Monitoring Well
Nitrate Nitrogen Subtraction Mew 0.03 mg/L 06/27/2024
Report#.: 2024-14195 Page 4 of 12

F0000- -- Environmental Chemists, Inc.
iL ' ! tS M Windmill Way, Wilmington, NC 28405 z. 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347—W Lab/lax
ANALYn1CAL & CONSULTW3 CHEMIST$ [e-mail]
OAK Americas
Date of Report: Jul 03, 2024
1206 Culbreth Drive Suite 200
Customer PO #:
Wilmington NC 28405
Customer ID: 08100044
Attention:
Report #: 2024-14195
Project ID: Monitoring Well
Lab ID Sample 1D:
Collect DatelTime Matrix Sampled by
24-34712 Site: MW-2C
6/20/2024
10:30 AM Water jcb/em
Test
Method
Results Date Analyzed
Color
Color
Tan
06/20/2024
Depth to water, ft.
oath to water, Ft.
8.3 feet
06/20/2024
Copper
EPA 200.7, Rev 4A, 1994
0.016 mg/L
06/26/2024
Lead
EPA 200.7. Rev 4A, 1994
0.021 mg/L
06/26/2024
Magnesium
EPA 200.7, Rev 4A, 1994
10.1 mg/L
06/28/2024
Nickel
EPA 200.7. Rev 4.4.1994
0.022 mg/L
06/26/2024
Selenium
EPA 200.7. Rev 4.4.1994
<0.01 mg/L
06/26/2024
Zinc
EPA 200.7. Rev 4 4, 1994
0.041 mg/L
06/26/2024
Arsenic
EPA 200.7, Rev 4 4 19M
0.015 mg/L
06/26/2024
Chromium
EPA 200 7, Rev 4 4,104
0.034 mg/L
06/26/2024
Cadmium
EPA 20o S. Rev 5 4, 1994
<0.001 mg/L
06/26/2024
Cobalt
EPA 200 s. Rev 5 4, 1%4
0.022 mg/L
06/27/2024
Mercury
EPA 2451, Rev 3 0.1994
<0.0002 mg/L
06/25/2024
Ammonia Nitrogen
EPA 350.1. Rev 2 0,1993
< 0.2 mg/L
06/24/2024
Gallons bailed before sampling
Ga ions Bailed bak to samp3 n®
5.0 gallons
06/20/2024
Odor
Quatitauve
None
06/20/2024
Total Dissolved Solids (TDS)
SM 2540 C-2015
572 mg/L
06/20/2024
Temperature
SM 2660 B-2010
20.5 C
06/20/2024
pH
SM4500H5.2011
6.1 units
06/21/2024
pH analyzed out of hold time of 15 minutes.
SM 4500 H 8-2011
5.9 units
/20/2024
Total Phosphorus
SM 4600 P (F-H)-2011
1.44 mg/L
06/28/2024
Chloride
SM4500 0 E-2011
12 mg/L
06/24/2024
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 363.2, Rev 2.0,1993
0.07 mg/L
06120/2024
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev 2.0, 1993
9.03 mg/L
06/24/2024
Report #:: 2024-14105 Page 5 of 12

[enviroeche]m
ANALYTICAL a CON8UlMHQ CHEMMM
DAK Americas
1206 Culbreth Drive Suite 200
Wilmington NC 28405
Attention.
Environmental Chemists, Inc.
66M Windmill Way, Wilmington, NC 28405 ° 910.392,0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ® 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 , 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Jul 03, 2024
Customer PO #:
Customer ID: 08100044
Report #: 2024-14195
Project ID: Monitoring Well
Nitrate Nitrogen Subtraction Method 8.96 mg/L 06/27/2024
Report #:- 2024-14195 Page 8 of 12

Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 2W5 - 910.392.0223 Lab • 910.392.4424 Fax
® 710 Bowsertown Road, Manteo, NC 27954 * 252.4735702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
DAK Americas
1205 Culbreth Drive Suite 200
Wilmington NC 28406
Attention:
Date of Report: Jul 03, 2024
Customer PO #:
Customer ID: 08100044
Report Al., 2024-14195
Project ID: Monitoring Well
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
24-34713 Site: MW-213
6/20/2024
10:55 AM Water jcb/em
Test
Method
Results
Date Analyzed
Color
Color
Clear
06/20/2024
Depth to water, ft.
©epth to Water, Ft
8.7 feet
06/20/2024
Copper
EPA 200.7, Rev 4.4, 1994
0.010 mg/L
06/26/2024
Lead
EPA 200.7, Rev 4.4, 1994
0.013 mg/L
06/26/2024
Magnesium
EPA 200.7, Rev 4.4,1994
4.41 mg/L
06/26/2024
Nickel
EPA 200.7, Rev 4.4,1994
<0.01 mg/L
06/26/2024
Selenium
EPA 200.7, Rev 4.4. 1994
<0.01 mg/L
06/26/2024
Zinc
EPA 200.7, Rev 4.4,1994
0.033 mg/L
06/2612024
Arsenic
EPA 200.7, Rev. 4A 1994
0.020 mg/L
06/26/2024
Chromium
EPA 200.7. Rev. 4A.1994
0.041 mg/L
06126/2024
Cadmium
EPA 200.8. Rev. 5.4, 1994
<0.001 mg/L
06/26/2024
Cobalt
EPA 200.8. Rev. 5.4,1994
0.006 mg/L
06/27/2024
Mercury
EPA 245.1. Rev. 3.0.1994
<0.0002 mg/L
06/2 12024
Ammonia Nitrogen
EPA 360.1, Rev. 7-0.1993
40.1 mg/L
06/24/2024
Gallons bailed before sampling
Galion Bailed before sampling
3(dry) gallons
06/20/2024
Odor
Quaittaflve
Sulfur
06/20/2024
Total Dissolved Solids (TDS)
SM 2540 c-2015
235 mg/L
06/20/2024
Temperature
SM2550 B-2010
22.1 C
06/2012024
PH
SM 4600 a B-2011
6.6 units
06/21/2024
pH analyzed out of hold time of 15 minutes
SM 4500 H B-2011
6.5 Unit"5
06/20/2024
Total Phosphorus
SM 4500 P (F-I1)-2011
0.96 mg/L
96/2$12024
Chloride
SM4500 cl E-2011
5 mg/L
06/24/2024
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0.1993
0.11 mg1L
06/20/2024
Nitrate+Nitrite-Nitrogen
EPA 363.2, Rev. 2.0, 1993
< 0.02 mg/L
06/24/2024
Report #:: 2024-14195 Page 7 of 12

Environmental Chemists, Inc.
envirochle"M6W2 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab 910.392.4424 Fax
® 710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5M3 L.ab/Fax
ANALYTICAL S CONSULTING CHEMISTS info@environmentalchemists com
DAK Americas Date of Report: Jul 03, 2024
1205 Culbreth Drive Suite 200 Customer PO #:
Wilmington NC 28405 Customer ID: 08100044
Attention: Report #: 2024-14195
Project ID: Monitoring Well
Nitrate Nitrogen subfracUm MOW <0.02 mg/L 06/27/2024
Report # 2024i4195 Page 8 of 12

Environmental Chemists, Inc®
7enviiroe7heiln, 66M Windmill Way, Wilmington, NC 28405 3 910.392.0223 Lab 910.392.4424 Fax
710 Dowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28W a 910.347.5843 Lab/Fax
ANALYTICAL S CONwLnNQ CHEMISTS info(a environmentalchcmists corn
OAK Americas Date of Report: Jul 03, 2024
1205 Culbreth Drive Suite 200 Customer PO #:
Wilmington NC 28405 Customer ID: 08100044
Attention: Report #: 2024-14195
Project ID: Monitoring Well
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
24-34714 Site: MW-2E 6/20/2024 9:25 AM Water jcb/em
Test Method Results Date Analyzed
Color
color
Tan/Tint
06/20/2024
Depth to water, ft
Depth 10 Water, Ft
8.3 feet
06/20/2024
Copper
EPA 200.7, Rev 4A.1994
<0.01 mg/L
06/26/2024
Lead
EPA 200.7, Rev 4.4, 1994
<0.01 mg1L
06/26/2024
Magnesium
EPA 200.7, Rev 4A. 1994
2.39 mg/L
06/26/2024
Nickel
EPA 200.7, Rev 4.4,1994
<0.01 mg/L
06/26/2024
Selenium
EPA 200.7, Rev 4.4, 1994
<0.01 mg/L
06/26/2024
Zinc
EPA 200 7, Rev 4.4, 1994
<0.01 mg/L
06/26/2024
Arsenic
EPA 200 7, Rev. 4.4,1994
<0.01 mg/L
06/26/2024
Chromium
EPA 200.7, Rev. 4.4,1994
0.013 mg/L
06/26/2024
Cadmium
EPA 200.8. Rev. 5.4,1994
<0.001 mg/L
06/26/2024
Cobalt
EPA 200.8 Rev. 5.4, 1994
0.005 mg/L
06/27/2024
Mercury
EPA 245.1, Rev. 3.0. 1994
<0.0002 mg/L
06/25/2024
Ammonia Nitrogen
EPA 350.1, Rev. 2.0. 1993
18.2 mg/L
06/24/2024
Gallons bailed before sampling
Gallons Bailed before sampling
3(dry) gallons
06/20/2024
Odor
Qualitative
Mild Sulfur
06/20/2024
Total Dissolved Solids (TDS)
sM2540 C-2015
161 mg/L
06/20/2024
Temperature
Sew 2550 B-2010
20.6 C
06/20/2024
pH
sac 4500 H s.2011
6.6 units
06/2112024
pH analyzed out of told time of 15 minutes.
SM 4500 H &2011
6,6 units
06/20/2024
Total Phosphorus
SM 4500 P (F.H)-2011
1.31 mg/L
06/28/2024
Chloride
ShM500 Cl E-2011
9 mg/L
06/24/2024
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA 3532. Rev. 2.0.1993
0.12 mg/L
06/20/2024
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0,1993
0.46 mg/L
06/26/2024
Report #:. 2024-14195 Page 9 of 12

Environmental Chemists, Inc.
envirochem j 6W2 Windmill Way, Wilmington, NC 28405 ? 910.392.0223 Lab � 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5848 Lab/Fax
ANALYTICAL A CONSUUNG CHEMISTS infoQa environmentalchemists com
DAK Americas Date of Report: Jul 03, 2024
1205 Culbreth Drive Suite 200 Customer PO #:
Wilmington NC 28406 Customer ID: 08100044
Attention: Report #: 2024-14195
Project ID: Monitoring Well
Nitrate Nitrogen SW*acbm Meswd 0.34 mg/L 06/27/2024
KepoR A: WOZ4.141 w
page 10 of a I

�"7
Environmental Chemists, Inc.
envirochem I W2 Windmill Way, Wilud gton, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 , 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
DAK Americas
Date of Report: Jul 03, 2024
1205 Culbreth Drive Suite 200
Customer PO #:
Wilmington NC 28405
Customer ID: 08100044
Attention:
Report #: 2024-14195
Project ID: Monitoring Well
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
24-34715 Site: MW-3A
6/20/2024
8:50 AM Water jcb/em
Test
Method
Results
Date Analyzed
Color
cow
Clear
06/20/2024
Depth to water, ft.
DePM to Weller, Ft
5.8 feet
06/20/2024
Copper
EPA 200.7, Rev 4A,1994
<0.010 mg/L
06/26/2024
Lead
EPA 200.7. Rev 4.4,104
<0.010 mg/L
06/26/2024
Magnesium
EPA 200.7. Rev 4.4,1994
1.98 mg/L
06/26/2024
Nickel
EPA 200.7. Rev 4A.1994
<0.01 mg/L
06/26/2024
Selenium
EPA 200.7, Rev 4.4.1994
<0.01 mg/L
06/26/2024
Zinc
EPA 200.7, Rev 4.4,1994
<0.01 mg/L
06/26/2024
Arsenic
EPA 200.7, Rev. 4.4, 1994
<0.010 mg/L
06/26/2024
Chromium
EPA 200.7, Rev. 4.4,1994
<0.010 mg/L
06/26/2024
Cadmium
EPA 200.8, Rev. 5.4.1994
<0.001 mg/L
06/26/2024
Cobalt
EPA 200.8. Rev. 5.4,1994
<0.001 frig/L
06/26/2024
Mercury
EPA 245.1. Rev. 3.0.1994
<0.0002 mg/L
06/25/2024
Ammonia Nitrogen
EPA 350.1. Rev. 2A,1993
0.3 fig/L
06/24/2024
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
06/20/2024
Odor
Quartaave
Mild Sulfur
06/20/2024
Total Dissolved Solids (TDS)
SM 254a c-2015
168 mg/L
06/20/2024
Temperature
SM2550 B-2010
19.7 C
06/20/2024
pH
SM 4500 H B-2011
6.4 units
06/21/2024
pH analyzed out of hold time of 15 minutes
SM 4500 H B-2011
5.8 units
06/20/2024
Total Phosphorus
SM 4500 P (F-H)-2011
0.24 mg/L
06/28/2024
Chloride
SLU500 Cl E-2011
16 mg/L
06/24/2024
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2. Rev. 2.0, 1993
< 0.02 mg/L
06/20/2024
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.o,1993
0.05 mg/L
06/25/2024
Repod #:: 2024-14195 Page 11 of 12

envirochem
DAK Americas
1205 Culbreth Drive Suite 200
Wilmington NC 28405
Attention:
Environmental Chemists, Inc,
6602 Windmill Way, Wdadngton, NC 28405 u 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info(e,)environmentalchemists.com
Date of Report: Jul 03, 2024
Customer PO #:
Customer ID: 08100044
Report #: 2024-14195
Project ID: Monitoring Well
Nitrate Nitrogen Subtraction Method 0.05 mg/L 06/27/2024
Comment:
Reviewed by:
Reports:: 2024.14195 Page 12 of 12

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Monitoring Report Submittal
...................................................
Permit Number#* WQ0018087
Name of Facility:* Alpek Polyester USA, LLC - Cape Fear Manufacturing Facility (Formally DAK Americas LLC)
Month: * July Year: * 2024
Report Information
Type* Upload Document*
GW-59 Semiannual Monitoring Well Report_07302024.pdf 29.6MB
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59).
Confirmation Email Address: * [e-mail]
Name of Submitter: * Phyllis H Simmons
Signature:
(��l:l '�f t SvirrarswJ
Date of submittal: 7/30/2024
This will be filled in automatically
Initial Review
Reviewer: Wanda.Gerald

Is the project number correct?* WQ0018087
Is the monitoring report accepted?* Yes No
Regional Office* Wilmington
Reviewer: _anonymous
Review Date: 8/12/2024