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HomeMy WebLinkAboutNCG030669_2024 DMR_20240715 NCDEQ Division of Energy, Mineral and Land Resources Stormwater Discharge Monitoring Report (DMR) Form for NCG030000 Metal Fabrication Click here for instructions Complete,sign,scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report(DMR) Upload form within 30 days of receiving sampling results. Mail the original,signed hard copy of the DMR to the appropriate DEMLR Regional Office. Certificate of Coverage No. NCGO3 0669 Person Collecting Samples: Robert Hensley Facility Name: AFS MFG LLC Laboratory Name: Pace Analytical Facility County: ROWAN Laboratory Cert. No.: DW#37706,WW#12, DW#37712,WW#40 Discharge during this period: ✓)Yes 0 No (if no,skip to signature and date) Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances?rjYes Ei No If so,which Tier(I, II,or Ill)? A copy of this DMR has been uploaded electronically via https://edocs.deq.nc.gov/Forms/SW-DMR es El No Date Uploaded: 1 1 } 5 1 . y Analytical Monitoring Requirements for Outfalls with Industrial Activities—Benchmarks in(Red) Parameter Parameter Outfall 1B Outfall 2 Outfall Outfall Outfall Code N/A Receiving Stream Class C C N/A Date Sample Collected MM/DD/YYYY 6/27/2024 6/27/2024 46529 24-Hour Rainfall in inches 0.23" 0.23" C0530 TSS in mg/L(100 or 50*) <2.5 mg/L <2.5 mg/L pH in standard units(6.0-9.0 FW, 00400 7.39 7.21 6.8-8.5 SW) 01119 Copper,total recoverable in mg/L <0.0050 mg/L <0.0050 mg/L (0.010 FW,0.0058 SW) 01051 Lead,total recoverable in mg/L <0.0050 mg/L <0.0050 mg/L (0.075 FW,0.22 SW) Zinc,total recoverable in mg/L(0.126 01094 FW,0.095 SW) <0.0100 mg/L <0.0100 mg/L 00340 Chemical Oxygen Demand(COD)in <25.0 mglL <25.0 mg/L mg/L(120) 00552 Non-Polar Oil&Grease in mg/L(15) <4.9 mg/L <4.8 mg/L *Outfalls to Outstanding Resource Waters(ORW),High Quality Waters(HQW),Trout Waters(Tr)and Primary Nursery Areas(PNA) have a benchmark TSS limit of 50 mg/L.All other water classifications have a benchmark of 100 mg/L FW(Freshwater)SW(Saltwater) Notes(optional): "I certify by my signature below,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who manage the system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,accurate,and complete.I am aware that there are significant penalties for submitting false informati n,including the ossibility of fines and imprisonment for knowing violations." .S gnat re of Permittee or Delegated Authorized Individual Date K1emA . ►c\CV1btI hey.i,gd.11Csi\ Al . COrY-N - 1 0y 210 3 512. Email Address Phone Number �/J/ p�f Pace Analytical Services,LLC }°�n 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 6�[VVV 66JJ (704)875-9092 July 05, 2024 Robert Hensley Agility Fuel Systems 1010 Corporate Center Drive Salisbury, NC 28146 RE; Project: Stormwater Pace Project No.: 92739249 Dear Robert Hensley: Enclosed are the analytical results for sample(s)received by the laboratory on June 28, 2024. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNVNELAC Standards and the laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network; •Pace Analytical Services-Asheville •Pace Analytical Services-Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyriek Hooks tyriek.hooks@pacelabs.com 704-977-0947 Project Manager Enclosures cc: Kulema McKoy, Hexagon Agility REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 1 of i 4 Pace Analytical Services,LLC � 9800 Kincey Ave. Suite 100 aceHuntersville,NC 28078 (704)875-9092 CERTIFICATIONS Project: Stormwater Pace Project No,: 92739249 Pace Analytical Services Charlotte South Carolina Laboratory ID:99006 South Carolina Certification#:99006001 9800 Kincey Ave.Ste 100,Huntersville,NC 28078 South Carolina Drinking Water Cert.#:99006003 North Carolina Drinking Water Certification#:37706 Florida/NELAP Certification#:E87627 North Carolina Field Services Certification#:5342 Kentucky UST Certification#:84 North Carolina Wastewater Certification#:12 Louisiana DoH Drinking Water#:LA029 South Carolina Laboratory ID:99006 VirginiaNELAP Certification#:480221 Pace Analytical Services Asheville 2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030 Florida/NELAP Certification#:E87648 South Carolina Certification#:99030001 North Carolina Drinking Water Certification#:37712 VirginiaNELAP Certification#:460222 North Carolina Wastewater Certification#:40 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 2 of 14 Pace Analytical Services,LLC 9800 Kincey Ave. Suite 100 'ace'P°1� Huntersville,NC 28078 m�irf 1F./ (704)875-9092 SAMPLE ANALYTE COUNT Project: Stormwater Pace Project No.: 92739249 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92739249001 OUTFALL 1B GRAB EPA 1664E DVR 1 PASI-C EPA 200.7 Rev 4.4 1994 DBB1 3 PASI-A SM 2540D-2015 MOW 1 PASI-A SM 5220D-2011 JP1 1 PASI-A 92739249002 OUTFALL 2 GRAB EPA 1664B DVR 1 PASt-C EPA 200.7 Rev 4.4 1994 DBB1 3 PASt-A SM 2540D-2015 MDW 1 PAS1-A SM 5220D-2011 JP1 1 PASI-A PASI-A=Pace Analytical Services-Asheville PASI-C=Pace Analytical Services-Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 3 of 14 Pace Analytical Services,LLC �]/'� �°� 9800 Kincey Ave. Suite 100 •a 1 e Huntersville,NC 28078 "ace- {✓ (704)875-9092 ANALYTICAL RESULTS Project: Stormwater Pace Project No.: 92739249 Sample: OUTFALL 1B GRAB Lab ID: 92739249001 Collected: 06/27/24 08:30 Received: 06/28/24 13:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual 1664 SGT-HEM,TPH Analytical Method:EPA 1664E Pace Analytical Services-Charlotte Total Petroleum Hydrocarbons ND mg/L 4.9 1 07/01/24 20:26 200.7 MET ICP Analytical Method:EPA 200.7 Rev 4.4 1994 Preparation Method:EPA 200.7 Rev 4.4 1994 Pace Analytical Services-Asheville Copper ND ug1L 5.0 1 06/29/24 12:25 07/02/24 15:07 7440-50-8 Lead ND ug/L 5.0 1 06/29/24 12:25 07/02/24 15:07 7439-92-1 Zinc ND ug/L 10.0 1 06/29/24 12:25 07/02/24 15:07 7440-66-6 2540D Total Suspended Solids Analytical Method:SM 2540D-2015 Pace Analytical Services-Asheville Total Suspended Solids ND mg/L 2.5 1 07/04/24 12:05 5220D COD Analytical Method:SM 5220D-2011 Preparation Method:SM 5220D-2011 Pace Analytical Services-Asheville Chemical Oxygen Demand ND mg/L 25.0 1 07/03/24 01:55 07/03/24 05:16 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:07/05/2024 11:27 AM without the written consent of Pace Analytical Services,LLC. Page 4 of 14 Pace Analytical Services,LLC 9800 Kincey Ave. Suite 100 'ace /�°� Huntersvitle,NC 28078 l�6✓VV (704)875-9092 ANALYTICAL RESULTS Project: Stormwater Pace Project No.: 92739249 Sample: OUTFALL 2 GRAB Lab ID: 92739249002 Collected: 06/27/24 09:30 Received: 06/28/24 13:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM,TPH Analytical Method:EPA 16648 Pace Analytical Services-Charlotte Total Petroleum Hydrocarbons ND mg/L 4.8 1 07/01/24 20:26 200.7 MET 1CP Analytical Method:EPA 200.7 Rev 4.4 1994 Preparation Method:EPA 200.7 Rev 4.4 1994 Pace Analytical Services-Asheville Copper ND ug/L 5.0 1 06/29/24 12:25 07/02/24 15:16 7440-50-8 Lead ND ug/L 5.0 1 06/29/24 12:25 07/02/24 15:16 7439-92-1 Zinc ND ug/L 10.0 1 06/29/24 12:25 07/02/24 15:16 7440-66-6 2540D Total Suspended Solids Analytical Method:SM 2540D-2015 Pace Analytical Services-Asheville Total Suspended Solids ND mg/L 2.5 1 07/04/24 12:05 5220D COD Analytical Method:SM 5220D-2011 Preparation Method:SM 5220D-2011 Pace Analytical Services-Asheville Chemical Oxygen Demand ND mg/L 25.0 1 07/03/24 01:55 07/03/24 05:16 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:07/05/2024 11:27 AM without the written consent of Pace Analytical Services,LLC. Page 5 of 14 ,., Pace Analytical Services,LLC 9800 Kincey Ave. Suite 100 pace Huntersville,NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92739249 QC Batch: 865383 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 SGT-HEM,TPH Laboratory: Pace Analytical Services-Charlotte Associated Lab Samples: 92739249001,92739249002 METHOD BLANK: 4461318 Matrix: Water Associated Lab Samples: 92739249001,92739249002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 07/01/24 20:18 LABORATORY CONTROL SAMPLE: 4461319 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 17.0 85 64-132 MATRIX SPIKE SAMPLE: 4461320 35887265001 Spike MS MS %Rec Parameter Units Result Conc. Result %Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 4.9U 19.4 15.9 70 64-132 SAMPLE DUPLICATE: 4461321 92738981001 Dup Parameter Units Result Result RPD Qualifiers Total Petroleum Hydrocarbons mg/L ND ND Results presented on this page aro in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:07/05/2024 11:27 AM without the written consent of Pace Analytical Services,LLC. Page 6 of 14 Pace Analytical Services,LLC '/'� 9800 Kincey Ave. Suite 100 ace, Huntersville,NC 28078 4[666ddd (704)875-9092 QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92739249 QC Batch: 865137 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92739249001,92739249002 METHOD BLANK: 4460410 Matrix: Water Associated Lab Samples; 92739249001,92739249002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper ug/L ND 5.0 07/02/24 14:42 Lead ug/L ND 5.0 07/02/24 14:42 Zinc ug/L ND 10.0 07/02/24 14:42 LABORATORY CONTROL SAMPLE: 4460411 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Copper ug/L 500 509 102 85-115 Lead ug/L 500 509 102 85-115 Zinc ug/L 500 513 103 85-115 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4460412 4460413 MS MSD 92738675001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Copper ug/L 0.023 500 500 696 684 135 132 70-130 2 M1 mg/L Lead ug/L ND 500 500 486 474 97 95 70-130 2 Zinc ug/L 0.024 500 500 471 460 89 87 70-130 2 mg/L MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4460416 4460417 MS MSD 92738668002 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Copper ug/L 0.066 500 500 597 613 106 109 70-130 3 mg/L Lead ug/L 0.0097 500 500 524 536 103 105 70-130 2 mg/L Zinc ug/L 0.10 500 500 622 638 104 107 70-130 2 mg/L Results presented on this page are In the units indicated by the"Units"column except whore an alternate unit Is presented to the right of the result, REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:07/05/2024 11:27 AM without the written consent of Pace Analytical Services,LLC. Page 7 of 14 Pace Analytical Services,LLC /� 9800 Kincey Ave. Suite 100 / Hunlersvllie,NC 28078 6�L 6J (704)875-9092 QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92739249 QC Batch: 866170 Analysis Method: SM 2540D-2015 QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92739249001,92739249002 METHOD BLANK: 4465360 Matrix: Water Associated Lab Samples: 92739249001,92739249002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 07/04/24 12:02 LABORATORY CONTROL SAMPLE: 4465361 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Total Suspended Solids mg/L 250 242 97 90-110 SAMPLE DUPLICATE: 4465380 92739227001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 47.3 38.0 22 SAMPLE DUPLICATE: 4465381 92739310001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 328 303 8 Results presented on this page are in the units indicated by the"Units"column except whore an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:07/05/2024 11:27 AM without the written consent of Pace Analytical Services,LLC. Page 8 of 14 Pace Analytical Services,LLC /� 9800 Kincey Ave. Suite 100 p d _¢�G V Huntersville,NC 28078 �•! (704)875-9092 QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92739249 QC Batch: 865855 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92739249001,92739249002 METHOD BLANK: 4463630 Matrix: Water Associated Lab Samples: 92739249001,92739249002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 07/03/24 05:11 LABORATORY CONTROL SAMPLE: 4463631 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 775 103 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4463632 4463633 MS MSD 92738821001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Chemical Oxygen Demand mg/L 30.3 100 100 142 142 111 111 90-110 0 M1 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4463634 4463635 MS MSD 92739723004 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Chemical Oxygen Demand mg/L ND 100 100 125 118 109 102 90-110 6 R1 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:07/05/2024 11:27 AM without the written consent of Pace Analytical Services,LLC. Page 9 of 14 Pace Analytical Services,LLC 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 GGE���iii✓✓✓ (704)875-9092 QUALIFIERS Project: Stormwater Pace Project No.: 92739249 DEFINITIONS DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot. ND-Not Detected at or above adjusted reporting limit. TNTC-Too Numerous To Count J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL-Practical Quantitation Limit. RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S-Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is a combined concentration. Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values. LCS(D)-Laboratory Control Sample(Duplicate) MS(D)-Matrix Spike(Duplicate) DUP-Sample Duplicate RPD-Relative Percent Difference NC-Not Calculable. SG-Silica Gel-Clean-Up U-Indicates the compound was analyzed for,but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as "Total"may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes. TNI-The NELAC Institute. ANALYTE QUALIFIERS M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample(LCS)recovery. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not he reproduced,except in full, Date:07/05/2024 11:27 AM without the written consent of Pace Analytical Services,LLC. Page 10 of 14 Pace Analytical Services,LLC 9800 Kincey Ave. Suite 100 ,,' ce' Huntersvllle,NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Stormwater Pace Project No.: 92739249 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92739249001 OUTFALL 1B GRAB EPA 1664E 865383 92739249002 OUTFALL 2 GRAB EPA 1664E 865383 92739249001 OUTFALL 1B GRAB EPA 200.7 Rev 4.4 1994 865137 EPA 200.7 Rev 4.4 1994 865165 92739249002 OUTFALL 2 GRAB EPA 200.7 Rev 4.4 1994 865137 EPA 200.7 Rev 4.4 1994 865165 92739249001 OUTFALL 1B GRAB SM 2540D-2015 866170 92739249002 OUTFALL 2 GRAB SM 2540D-2015 866170 92739249001 OUTFALL 1B GRAB SM 5220D-2011 865855 SM 5220D-2011 865874 92739249002 OUTFALL 2 GRAB SM 5220D-2011 865855 SM 5220D-2011 865874 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in tut), Date:07/05/2024 11:27 AM without the written consent of Pace Analytical Services,LLC. Page 11 of 14 DC#_Title: ENV-FRM-HUN1-0083 v05_Sample Condition Upon Receipt 'iraace Effective Date: 05/24/2024 i Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville [r Raleigh Mechanicsvillefl AttantAi`1 ,r.....�--•.,r-r' Sample Condition Client Name: Pro ect#: WO# : 92739249 Up on Recet t �_ 'AO(I1 f y j G!P( f 4-rim. ' Courier: Commercial Opade Ex ❑LP5 Other: ['ClientEllClienEll111 ' 1 111111 92739249 Custody Seal Present? Des ❑No Seals Intact? Dyes ❑No ✓[IN/A �,//r Date/Initials Person Examining Content01 :/i�/ (-' Z3.2�Packing Material: ['Bubble Wrap [/Bubble Bags ['None E Other Biological Tissue roren? 7hermomete f� -�rr;I /�(/,1 Des ONo [ N/A IR Gun ID: f lt " f Type of Ice: 2Net ❑Blue ['None 1 3 Correction Factor: /�c, Cooler Temp: Add/Subtract(°C) V. Temp should be above freezing to 6°C �" ❑Samples out of temp criteria.Samples on ice,cooling process Cooler Temp Corrected(°C): v has begun USDA Regulated Soil(2/N/A,water sample) Did samples originate in a quarantine zone within the United States:CA,NY,or SC Did samples originate from a foreign source{internationally, (check maps)?Eves ❑No including Hawaii and Puerto Rico)?Des ❑No 1 Comments/Discrepancy: Chain of Custody Present? fes ❑Na ❑N/A 1 1. Samples Arrived within Hold Time? beg ❑No ON/A 12. Short Hold lime Analysis(<72 hr.)? Dyes QNo Rush Turn Around Time Requested? Eves bl'o EN/A 4. Sufficient Volume? [14es :No ❑N/A 5. Correct Containers Used? Oyes ❑No ❑N/A 6. -Pace Containers Used? 'mires ®No ❑N/A Containers Intact? tyres ❑No ❑N/A 7. ' t Dissolved analysis:Samples Field Filtered? Dyes ONO IfIrN/A 8. Sample Labels Match CDC? lis ❑No ❑N/A 9. -- -Includes Date/Time/ID/Analysis Matrix: Headspace in VOA Vials(s.5-6mm)? Dyes Otto [a/N/A 10, Trip Blank Present? ❑Yes ❑No [ ]jell/A ; 11. Trip Blank Custody Seals Present? Des ❑N 61 I COMMENTS/SAMPLE DISCREPANCY Field Data Required? Oyes ❑No Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Date/Time: Project Manager SCURF Review: Date: Project Manager SRF Review: Date: Qualtrax ID: 69614 Page 1 of 2 Page 12 of 14 DC# Title: ENV-FRM-HUN1-0083"Facev05_Sample Condition Upon Receipt ! Effective Date: 05/24/2024 'Check mark top half of box if pH and/or dechlorination is verified and within the M `: V 39249 acceptance range for preservation samples. Project � PM: TIH Due Date: 07/08/24 Exceptions:VOA,Coliform,TOC,Oil and Grease,DRO/8015(water)DOC,Wig ••Bottom half of box is to list number of bottles CLIENT: 82—Agility F "'Check all unpreserved Nitrates for chlorine Laboratory Receiving Location:Asheville❑ Eden❑ Greenwood❑ Huntersville Er RaleighO Mechanicsville❑ AtlantaD Kernersville❑ Client .r 4 Profile/e(Circle ono)3 f 2?.(5t Notes 2 :1 ! z I M1 a 2 A ri M E 2_ _'. ^ !. V 0 {y, i -7: L. .., Y ` i - 7 ^ . ; z V = `z z . n z 4 7 7 ' G x I C.' O V_ ; n 8 h j 1 nF. 1 2 7 O G Y. i - Y .. a T 7 u �. v _ E E 1 Y e c - o E e c E E c ' € ' E J c E g ' 'v. o _ c o 4 o N M 1 ^ I o 2 H o t '> 7 7 7 I 4 m o * M 7 N N — f g t, 7 X ' 1- N 1 1 c a 7 V 4 6 4 •M M1 Al 4l {{O771 Q, O� O,7t {] ` L� U' = G m G O t m o �S K 2 2 2 2 O C 2 > E Y > v+ I N i I m 2 7 i f .MI cc ! I S S � I €�i �'� 1 y —V'�so,� lin_ miiiii- 2 ! \ ,./L. 3NIMIIIIII 1 i N ; imi Li I t }{j D 111 1111111.0Et.IIIøUIu1 1 1111111111aliglill.6.11LIkkI I_ 8 \ .� k.k 1,la I' \ r------ la \' 4 ,�\\ N 11 \ I i N\\\\ 1 \ A 12 \\I \ \\\ \ N.L € E 616.E 1 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation ! Amount of Preservative Lot It adjusted added Note: Whenever there is discrepancy affecting North Carolina compliance samples,a copy of this form will be sent to the North Carolina DENR Certification Office(i.e. Out of hold,incorrect preservative,out of temp,incorrect containers. Qualtrax ID' 69614 Page 2 of 2 Page 13 of 14 4' x a 4, g �yj]R\ nt. v ^- -- °' o n a• c 3 n > i< a •�\� p : g .tea p °' w 7 .• € 1 `4 .2 a'' g = ^ n F 3 ' a z S ^ n c �. '_tys s aa' '� n o » - _ ° z % �+ 7. v r. F (� n c x = = _ ' r d E. o o co c+ v y - a 3 , 't x . E n ,<' 'p. A a - v " < o S " 3 ra Q < ai `^ ^ ^ - F. n o '^ f < ~ a'ri n N c. m m =1 `1 p - o _ " S2 � a W o g rn N A N 6+ _ 1 - = !L • C)Z n_ Cs,, ^ ywf N _. <O :=oa C zfa n` " a o Q a 3 � N 3 r o - : 'a 2 - F. - S o m a P aLQ P . In a s r -I u C n - N. :v ro F ''V m a� n^ -, o A 2 F 3 3 n m n n o c a -2 2 5 o o` `o m 3 0 o D_ p, ' 0 Et. •' o a 2 ^ • " " i o' " rs '� a v ~ a " 'If' - " m o a Z " b3 m , a s �i " O 3 n " G W -n � n ? n _ n S O - » Ob - TbD Q rJ O w/^ C n ' -ipa M a . 2a Ooboo r EliOC `1;„. M O xZ TI w n Q.o Pn lT a I1 VV Q 1\i o n $' n n w 0 ~ c °r Q '1 b v v a m _ o z v f.. \\ ? n n f a Yf 70 s �` 3 = v a - d y1 3 3 ......A fir+ tra " Sn a 1 - et) u r-� d O. n A n (mot 1 ''O`` ^ f - n H4,,, VI 3 " ? O o F. 0 �'1 A _ E. 3 M i� G c. 1 g =o o r'tl .. Y s• a o c R. g \ 1664 SGT-HEM,TP14 '.1 :\''. :: '-.7 3 200.7 MET!CP (Cs CO J Pb Z.�7 tic+o +t•� 'VEEP J y:i ^ ` ryC Fr S 7/04 •. \ 2540D Total Suspended Solidsr. — o 1. 8 0 F. P i n 1 ?, y l• f p- a �� 3 - ` '5220D COO `n 4a WV-. O 3 d ": o s4��`. o E t.� a ^ 2 — o 03 CowU c PI'P..' ^ n ^"` d N 5 2 n n a D -< y (A d K ___ A D 1 a O C� 1./'� .. -� 3' O m o 5' O " — — 2 a T u .0 3 s Lab Use Only v== m �• -cn g m co� A I � 2 _ " O iia^ 3 Ng' -. 3 S.^ 02 §� _ I _ _ a 3 0 F_ o�� 3 0 5 = la • - 0 2 z il n'. Frese vasion nomconrormmcr dendu�d ros -- Page 14 of 14 sample