WQ0016376_Monitoring - 06-2024_20240726

Monitoring Report Submittal
Permit Number#* WQ0016376
Name of Facility:* S&J VILLARI LIVESTOCK PROCESSING FACILITY - WARSAW
Month:* June Year: 2024
Report Information
Type* Upload Document*
NDMR, NDAR-1, NDAR-2, NDMLR WWT June 2024.pdf 5.31 MB
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59).
Confirmation Email Address: * [e-mail]
Name of Submitter: * Gerald Matthews
Signature:
Date of submittal: 7/26/2024
This will be filled in automatically
Initial Review
Reviewer: Wanda.Gerald

Is the project number correct?* W00016376
Is the monitoring report accepted?* Yes NO
Regional Office* Wilmington
Reviewer: _anonymous
Review Date: 7/29/2024

FOR10- N1UMR 03-12 NON -DISCHARGE MONITORING REPORT (NDMR) Page I of 4-
Permit No.: WQ0016376
Facility Name: S&J Villari Li�/estock Processing Facility-Warsa
County: Duplin
Month: June
Year: 2024
PPI: 001
Flow Measuring Point: ❑ tnfluent E] Effluent ❑ No flow generated
Parameter Monitoring Point: ❑ influent 0 Effluent E] Groundwater Lowering ❑Surface Water
Parameter Code -P
60050
00310
00940
50060
31616
00610
00625
00620
00600
00400
00666
70300
00530
0
'ap
Q E
ce
p
c
!13
P 6
0
-
'n
p
m
p
C
a
��
O Vi O
R€
d
c
E
t
3irn
Z
°i
O
Z
CL
C
0o ?:
N
o
cavO
in 0)
24-hr
hrs
GPD
mg/L I
mg/L
mg/L
#/100 ml-
mg/L
mg/L
mg/L
mg/L
su
mg/L
I mg/L
mg/L
1
07:00
6
75,895
2
07:00
6
16,139
3
07:00
10
70,291
4
07:00
10
71,738
5
07:00
10
76,209
6
07:00
10
75,690
<0.1
7.1
7
07:00
10
74,717
164
7.82
8
07:00
6
8,614
9
02:05
3
12,063
10
07:00
10
77,916
11
07:00
10
76,345
121
07:00
10
77,528
13
07:00
_
10
83,012
<0.1
7.1
14
07:00
10
72,012
15
07:00
8
10,915
16
07:00
6
8,976
17
07:00
10
87,583
18
07:00
10
75,626
19
07:00
10
1 77,623
124
7.81
20
07:00
10
77,923
<0.1
7.1
21
07:00
10
69,658
22
07:00
8
8,765
23
07:00
2
14,030
24
07:00
10
82,160
25
07:00
10
73,115
26
07:00
10
79,845
91
7.85
27
07:00
10
67,706
34
54
11200
83.3
89.7
<0.02
89.7
4.14
340
43
28
07:00
10
77,183
29
07:00
8
5,094
30
03:15
1
12,568
31
Average:
56,565
34.00
108.25
0.00
11.200.00
83.30
89.70
0.00
89.70
4.14
340.00
43.00
Daily Maximum:
87,583
34.00
164.00
0.10
11,200.00
83.30
1 89.70
0.02
89.70
7.85
4.14
340.00
43.00
Daily Minimum:
5,094
34.00
54.00
0.10
11,200.00
83.30
89.70
0.02
89.70
7.10
4.14
340.00
43.00
Sampling Type:
Recorder
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Avg. Limit:
100,260
_Monthly
Daily Limit:
Sample Frequency:
Recorder
Monthly
Monthly
Monthly
Monthly
Monthly
Monthly
Monthly
Monthly
Monthly
Monthly

FORM: NDMR03-12 NON -DISCHARGE MONITORING REPORT (NDMR) Page Z of—q-
Permit No.: WQ0016376
Facility Name: S&J Villari Livestock Processing Facility-Warsa
County: Duplin
Month: June
Year: 2024
PPI: 002
Flow Measuring Point: ❑ Influent 21 Effluent ❑ No Flow generated
Parameter Monitoring Point: ❑ Influent ❑ Effluent ❑ Groundwater Lowering Surface water
Parameter Code —►
60060
00625
00610
00620
00665
31616
00600
tw
() H
1%
O
C
0
EY
V N
O
li
.0
C
a) CD
Y at3
.�$Z
N
c
E
L
Z
(A
i4s
Fes— vl
t
E
Uo
u-
U
C
cn
O
~Z
24-hr
hrs
GPD
mg/L
mg/L
mg/L
mg/L
#/100 mL
mg/L
1
07:00
6
75,895
2
07:00
6
16,139
3
07:00
10
70,291
4
07:00
10
71,738
5
07:00
10
76,209
6
07:00
10
75,690
7
07:00
10
74,717
8
07:00
6
8,614
9
02:05
3
12.063
10
07:00
10
77,916
11
07:00
10
76.345
12
07:00
10
77,528
13
07:00
10
83,012
14
07:00
10
72,012
15
07:00
8
10,915
16
07:00
6
8,976
17
07:00
10
87,583
18
07:00
10
75,626
19
07:00
10
77,623
20
07:00
10
77,923
211
07:00
10
69.658
22
07:00
8
8,765
23
07:00
2
14,030
24
07:00
10
82,160
25
07:00
10
73,115
26
07:00
10
79.845
27
07:00
10
67,706
1.8
0.9
0.07
0.11
25
1.9
28
07:00
10
77,183
29
07:00
8
5,094
30
03:15
1
12,568
31
Average:
56.565
1.80
0.90
0.07
0.11
25.00
1.90
Daily Maximum:
87,583
1.80
0.90
0.07
0.11
25.00
1.90
Daily Minimum:
5,094
1.80
0.90
0.07
0.11
25.00
1.90
Sampling Type:
Recorder
Grab
Grab
Grab
Grab
Grab
Monthly Avg. Limit:
Daily Limit:
Sample Frequency:
Recorder
Monthly
Monthly
Monthly
Monthly
Monthly

f ORM: NDMR 03-12 NON -DISCHARGE MONITORING REPORT (NDMR) Page J of—*..
Permit No.: WQ0016376
Facility Name: S&J Villari Livestock Processing Facility-Warsa
County: Duplin
Month: June
Year: 2024
PPI: 003 TF___Iow
Measuring Point: ❑ Influent 0 effluent ❑ No flow generated
Parameter Monitoring Point: ❑ Influent ❑ effluent ❑ Groundwater Lowering [] surface water
Parameter Code -►
60060
00625
00610
00620
00666
31616
00600
` 0
a E
a~
O
O
N
Eir- 2
0O
LL
rtt
Y°
!9z
m
c
E
a
°
Z
o
o
a
u.
U
o
z
24-hr
hrs
GPD
mg/L
mg/L
mg/L
mg/L
#1100 mL
mg1L
1
07:00
6
75,895
2
07:00
6
16,139
3
07:00
10
70,291
4
07:00
10
71,738
6
07:00
10
76,209
6
07:00
10
75,690
7
07:00
10
74,717
8
07:00
6
8,614
9
02:05
3
12,063
10
07:00
10
77,916
11
07:00
10
76,345
12
07:00
10
77,528
13
07:00
10
83,012
14
07:00
10
72:012
15
07:00
8
10,915
161
07:00
6
8,976
17
07:00
10
87,583
18
07:00
10
75,626
19
07:00
10
77,623
20
07:00
10
77.923
21
07:00
10
6%658
221
07:00
8
8,765
23
07:00
2
14,030
24
07:00
10
82,160
25
07:00
10
73,115
26
07:00
10
79,845
27
07:00
10
67,706
25.7
18.6
0.52
2.47
>30000
26.3
281
07:00
10
77,183
29
07:00
8
5,094
30
03:15
1
12,568
31
Average:
56,565
25.70
18.60
0.52
2.47
1.00
26.30
Daily Maximum:
87.583
25.70
18.60
0.52
2.47
0.00
26.30
Daily Minimum:
5,094
25.70
1B.60
0.52
2.47
0.00
26.30
Sampling Type:
Recorder
Grab
Grab
Grab
Grab
Grab
Monthly Avg. Limit:
Daily Limit:
Sample Frequency:
Recorder
Monthly
Monthly
Monthly
Monthly
Monthly

FORM: NDMR 03-12.
NON -DISCHARGE MONITORING REPORT (NDMR)
Page _ * of *
Sampling Person(s) Certified Laboratories
Name: GERALD LAMAR MATTHEWS Name: Environmentat Chemists INC.
Name: Name: Water Agricultural Laboratories
Does all monitoring data and sampling frequencies meet the requirements in Attachment A of your permit? D Compliant ❑ Non -Compliant
If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective
action(s) taken. Attach additional sheets if necessary.
Operator in Responsible Charge (ORC) Certification
ORC: GERALD LAMAR MATTHEWS
Certification No.: 993131
Grade: S1 Phone Number: 910-289-7500
Has the ORC changed since the previous NDMR? [2] Yes ❑ No
Signature Date
By this signature, I certify that this report is accurrale and complete to the best of my knowledge.
Permittee Certification
Permittee: SAM VILLARI
Signing Official:
Signing Official's Title: OWNER
Phone Number: 910-293-2157
Permit Expiration: 11/30/2025
r_-
Signature Date
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information
submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for
gathering the information, the Information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am
aware that [here are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
Mail Original and Two Copies to:
Division of Water Quality
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617

FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Pa o� I- of
Permit No.: WQ0016376
Facility Name: S&J Villari Livestock Processing Facility -Warsaw
County: Duplin
Month: June
Year: 2024
Did irrigation
Field Name:
1
Field Name:
2
Field Name:
3
Field Name:
4
occur'
- Area (acres):
0.65
Area (acres):
1.16
Area (acres):
1.12
Area (acres):
1.07
at this facility?
Cover Crop:Coastal
Bermuda
Cover Crop:
P�
Coastal Bermuda
cover Crop:
P�
Coastal Bermuda
Cover Crop:
P'
Coastal Bermuda
Q YES ❑ NO
Hourly Rate (in):
0.6
Hourly Rate (in):
0.6
Hourly Rate (in):
0.6
Hourly Rate (In):
0.6
Annual Rate (in):
41.96
Annual Rate (in):
41.96
Annual Rate (in):
41.96
Annual Rate (in):
41.96
Weather
Freeboard
Field Irrigated?
i] YES ❑ NO
Field Irrigated?
11 YES ❑ No
Field Irrigated?
[i YES [) NO
Field Irrigated?
0 YES ❑ NO
°
U
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y
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r-
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> Q
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~'
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rn
"mom3'v
°
J
E rn
N x 0
°F
in
in
in
gal
min
in
in
min
in
in
gal
ruin
In
In
gal
min
In
in
1
C
60
54
2
C
3
CL
4
C
5
CL
61
CL
7
R
0.03
8
CL
9
R
0.02
10
R
0.03
11
C
121
C
13
C
14
C
15
C
16
C
17
C
6,370
21
0.36
0.36
11,368
38
0.36
0.36
10,976
36
0.36
0.36
10,486
35
0.36
0.36
181
C
19
C
5,298
21
0.30
0.30
9,455
38
0.30
0.30
9,129
36
1 0.30
0.30
8,722
1 35
0.30
1 0.30
20
C
21
C
22
C
6,392
21
036
0.36
11,408
38
0.36
0.36
11,015
36
0.36
0.36
10,523
35
0.36
0.36
23
CL
241
CL
25
C
4,091
13
0.23
0.23
7,301
23
0.23
0.23
7.049
22
0,23
0.23
6,734
21
0.23
0.23
26
CL
27
CL
28
CL
29
CL
0.03
30
R
1.25
60
66
31
r_
Monthly Loading:
22,151
1.26
17 94
39,532
1.26
17.94
-?y'
38,169
1.26
17.94
36,465
1.26
17.94
12 Month Floating Total (in):

FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page o2 of W
Permit No.: WQ0016376
Facility Name: S&J Villari Livestock Processing Facility -Warsaw
County: Duplin
Month: June
Year: 2024
Did irrigation occur
Field Name:
5
Field Name:
6
Field Name:
7
Field Name:
8
Area (acres):
1.19
Area (acres):
1.17
Area (acres):
1.05
Area (acres):
1.25
at this facility?
Cover Crop:Coastal
Bermuda
Cover Crop:
p'
Coastal Bermuda
Cover Crop:
p'
Coastal Bermuda
Cover Crop:
p'
Coastal Bermuda
E YES ❑ No
Hourly Rate (in):
0.6
Hourly Rate (in):
0.6
Hourly Rate (in):
0.6
Hourly Rate (in):
0.6
Annual Rate (in):
41.96
Annual Rate (in):
41.96
Annual Rate (in):
41.96
Annual Rate (in):
41.96
Weather
Freeboard
Field Irrigated?
Q YES ❑ NO
Field Irrigated?
YES [] No
Field Irrigated?
YES ❑ NO
Field Irrigated?
0 YES ❑ NO
T
p
°
t�
r
@
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E
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N2
°F
in
in
in
gal
min
in
in
gal
min
in
in
gal
min
In
in
gal
min
In
in
1
C
60
54
2
C
3
CL
4
C
5
CL
_
6
CL
7
R
0.03
_
8
CL
9
R
0.02
101
R
1
0.03
ill
C
_
12
C
13
C
14
C
15
C
16
C
171
C
1
11,662
39
0.36
0.36
11,466
38
0.36
0.36
10,290
34
0.36
0.36
12,250
40
0.36
0.36
181
C
19
C
9,700
39
0.30
0.30
9,537
38
0.30
0.30
8.559
34
0.30
0.30
10,189
1 40
0.30
0.30
20
C
21
C
22
C
11,703
39
0.36
0.36
11,506
38
0.36
0.36
10.326
34
0.36
0.36
12,293
40
0.36
0.36
23
CL
24
CL
26
C
7,489
24
0.23
0.23
7,363
23
0.23
0.23
6,608
21
0.23
0.23
7,867
1 25
0.23
0.23
26
CL
_
27
CL
28
CL
29
CL
0.03
30
R
1.25
60
66
_
31
_
^_
Monthly Loading:
4 5554
1.26
17.94
39,872
1.26
17.94
35,783
1.26
17.94
42,599
17.94
12 Month Floating Total (in):

FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page 3-of &
Permit No.: WQ0016376
Facility Name: S&J Villari Livestock Processing Facility -Warsaw
County: Duplin
Month: June
Year: 2024
Did irrigation
Field Name:
9
Field Name:
10
Field Name:
11
Field Name:
12
occur
Area (acres):
1
Area (acres):
1.46
Area (acres):
1.43
Area (acres):
1.23
at this facility?
Cover Crop:Coastal
Bermuda
Cover Crop:
p'
Coastal Bermuda
Cover Crop:
p�
Coastal Bermuda
Cover Crop:
p�
Coastal Bermuda
(] YES ❑ NO
Hourly Rate (in):
0.6
Hourly Rate (in):
0.6
Hourly Rate (in):
0.6
Hourly Rate (in):
0.6
Annual Rate (in):
41.96
Annual Rate (in):
41.96
Annual Rate (in):
41.96
Annual Rate (in):
41.96
Weather
Freeboard
Field Irrigated?
[) YES ❑ NO
Field Irrigated?
❑✓ YES ❑ NO
Field Irrigated?
l] YES ❑ NO
Field Irrigated?
YES ❑ NO
o
y
E
C
lY
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EL
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°F
in
In
in
gal
min
in
in
gal
min
In
in
gal
min
in
in
gal
min
in
in
1
C
60
54
2
C
3
CL
4
C
5
CL
6
CL
7
R
0.03
8
CL
9
R
0.02
10
R
0.03
11
C
12
C
13
C
_
14
C
15
C
16
C
17
C
9,800
40
0.36
0.36
14,308
47
0.36
0.36
14,014
46
0.36
0.36
12,054
40
0.36
0.36
18
C
19
C
8,151
32
0.30
0.30
11,901
47
0.30
0.30
11,656
46
0.30
0.30
10,026
40
0.30
0.30
20
C
21
C
22
C
9,835
32
0.36
1 0.36
14,358
47
0.36
0.36
14,063
46
0.36
0.36
12,097
40
0.36
0.36
23
CL
24
CL
25
C
6,294
20
0.23
0.23
9,189
29
0.23
0.23
9,000
28
0.23
0.23
7,741
24
0.23
0.23
26
CL
27
CL
28
CL
29L!jj
CL0.03
-- -
34,080
- --
301.25
60
66
31
Monthly
Loading:
1.26
17 94
49,756
1.26
1 '.94
n> >
`+:
48,733
1.26
17.94
41,918
,,: r"
;
1.26
17.94
12 Month Floating Total (in):

FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page ott_
Permit No.: WQ0016376
Facility Name: S&J Villari Livestock Processing Facility -Warsaw
County: Duplin
I Month: June
Year: 2024
Did irrigation
Field Name:
13
Field Name:
14E
Field Name:
14W
Field Name:
15
occur
at this facility?
Area (acres):
2.16
Area (acres):
13.73
Area (acres):
7.7
Area (acres):
0.73
Cover Crop:Coastal
Bermuda
Cover Crop:
p'
Coastal Bermuda
Cover Crop:
p'
Coastal Bermuda
Cover Crop:
P�
Coastal Bermuda
Q YES ❑ No
Hourly Rate (in):
0.6
Hourly Rate (in):
0.6
Hourly Rate (in):
0.6
Hourly Rate (in):
0.6
Annual Rate (in):
41.96
Annual Rate (in):
31.6
Annual Rate (in):
24.21
Annual Rate (in):
30.44
Weather
Freeboard
Field Irrigated?
❑ YES No
Field Irrigated?
Ul YES ❑ No
Field Irrigated?
0 YES iii No
Field Irrigated?
0 YES ❑ No
>.
m
o
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a
�'
a
E
a
f-
c
2
a
a
o
J q
a
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>
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a
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J
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J
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:
00
J
E zo
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_l
E
yc
-1
:
�_
LE'
v,
ta
>,
a0
J
E aC
►C
`EL
°0oa
J
OF
In
in
In
gal
min
in
in
gal
min
in
in
gal
min
in
in
gal
min
in
In
1
C
60
54
2
C
3
CL
4
C
5
CL
_
61
CL
7
R
0.03
8
CL
9
R
0.02
10
R
0.03
11
C
12
C
13
C
14
C
15
C
16
C
17
C
21,168
70
1 0.36
0.31
111,243
1 346
0.30
0.05
62,387
194
0.30
0.09
7,154
1 24
0.36
0.36
18
C
123,549
384
0.33
0.05
69,288
216
0.33
0.09'
19
C
17,607
70
0.30
0.26
96,239
346
0.26
0.04
53,972
194
0,26
0.08
5,950
24
0.30
0.30
20
C
112,576
308
0.30
0.06
63,135
172
0.30
0.11
21
C
93,846
308
0.25
0.05
52,631
172
0.25
0.09
22
C
21,243
70
0.36
0.31
44,768
211
0.12
0.03
25,106
119
0.12
0.06
7,179
24
0.36
0.36
23
CL
24
CL
100,569
346
0.27
0.05
56,401
194
0.27
0.08
25
C
13,594
43
0.23
0.23
4,594
14
0.23
0.23
26
CL
27
CL
_
28
CL
29
CL
0.03
30
R
1.25
60
66
31
Monthly Loading:
12 Month Floating Total (in)-
73,612
1.26
17.94
682,790
1.83
18A5
382,920
1.83
18.45
24,877
;'." y ,•
9.
1.262&tiL

FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page of b
Permit No.: WQ0016376
Facility Name: S&J Villari Livestock Processing Facility -Warsaw
County: Duplin
Month: June
Year: 2024
Did irrigation
Field Name:
16
Field Name:
17
Field Name:
Field Name:
occur
at this facility?
Area (acres):
1.25
Area (acres):
0.82
Area (acres):
Area (acres):
Cover Crop:
p'
Coastal Bermuda
Cover p'
Coastal Bermuda
Cover P�
CoverCro P'
Q YES ❑ No
Hourly Rate (in):
0.6
Hourly Rate (in):
0.5
Hourly Rate (in):
Hourly Rate (in):
Annual Rate (in):
13.83
Annual Rate (in):
16.95
Annual Rate (in):
Annual Rate (in):
Weather
Freeboard
Field Irrigated?
❑ YES (] No
Field Irrigated?
❑ YES ❑ NO
Field Irrigated?
'=1 YES ❑ NO
Field Irrigated?
❑ YES ❑ NO
>'
o
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m
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o
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a
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E M
~ E
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,�v
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(0 = J
°F
In
in
In
gal
min
in
in
gal
min
in
in
gal
min
in
in
gal
min
in
In
1
C
60
54
2
C
3
CL
4
C
5
CL
61
CL
7
R
0.03
8
CL
9
R
0.02
10
R
0.03
11
C
12
C
13
C
14
C
15
C
161
C
17
C
18
C
19
C
20
C
18,007
181
0.53
0.18
11,812
119
0.53
0.27
21
C
221
C
1
11,897
181
0.35
0.12
7.804
119
0.35
0.18
23
CL
24
CL
25
C
26
CL
27
CL
281
CL
29
CL
0.03
30
R
1.25
60
66
31
Monthly Loading:
29,904
0.88
19,616
0.88
0
0,00
0
0.00
12 Month Floating Total (in):
K
7.90
7.90

FORM NDAR-1 08-11 NON-DISCHAR(jE APPLICATION REPORT (NDAR-1) Page of -- --
Did the application rates exceed the limits in Attachment B of your permit?
❑J Compliant ❑ Non -Compliant
Were adequate measures taken to prevent effluent ponding in or runoff from the sites? [:1 Compliant Non -Compliant
Was a suitable vegetative cover maintained on all sites as specified in your permit? 0 Compliant ❑ Non -corn pliant
Were all setbacks listed in your permit maintained for every application to each permitted site? E,] Compliant Non -Compliant:
Were all freeboards maintained in accordance with the specified freeboard heights in your permit? I] compliant ❑ Non -Compliant
If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective
action(s) taken. Attach additional sheets if necessary.
Operator in Responsible Charge (ORC) Certification
ORC: Gerald Lamar Matthews
Certification No.: 993131
Grade: SI Phone Number: 910-289-7500
Has the ORC changed since the previous NDAR-1? _-1 Yes I] No
_22-1 Y
Signature Date
By this signature, I certify that this report is accurrate and complete to the best of my knowledge.
Permittee Certification
Permittee:
Sam Villari
Signing Official:
Signing Official's Title: Owner
Phone Number: 910-293-2157 Permit Exp.: 11/302025
Signature Date
I certify, under penally of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete I am aware that (here are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
Mail Original and Two Copies to:
Division of Water Quality
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617

FORM: NDMLR 10-13
NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page-A-ofs
Permit No.: WQ0016376
Facility Name: S&J Villari Livestock Processing Facility -Warsaw
County: Duplin
Month: June
Year: 2024
Field Name:
Zone 1
Field Name:
Zone 2
Field Name:
Zone 3
Field Name:
Zone 4
Field Name:
Zone 5
Area (acres):
0.65
Area (acres):
1.16
Area (acres):
1.12
Area (acres):
1.07
Area (acres):
1.19
Cover Crop:
Coastal Bermuda
Cover Crop:
Coastal Bermuda
Cover Crop:
Coastal Bermuda
Cover Crop:
Coastal Bermudg
Cover Crop:
Coastal Bermuda
Load Type:
PAN
Load Type:
PAN
Load Type:
PAN
Load Type:
PAN
Load Type:
PAN
Field Loaded?
YES ❑ No
Field Loaded?
Yes ❑ No
Field Loaded?
0 YES ❑ No
Field Loaded?
0 YES INo
Field Loaded?
F] YES ElNp
N
2
>
Z
¢
j
V
W
J
B
J
Z
o
>
Z
Q
CD
v
Q
_O
J
o
Z
a
v
o
>
Z
2N
u
tj
Z
N�
Mo
a
d
E
>
ZcZc
2
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lC
a
v
E Z
Q
j
>
N -
Zai c"
av
n Tj
ZZ
>, oC
-1EE
c
yO
J
ZE
�¢ao
jo
Month
gal
23,085
mg/L
Ibs/ac
Ibslac
gal
mg/L
Ibslac
Ibslac
_
gal
mg/L
lbs/ac
ibs/ac
gal
mg/L
lbs/ac
Ibs/ac
gal
mg/L
Ibslac
Ibs/ac
July
1 55.8
16.5
16.5
41,198
55.8
16.5
16.5
39,777
55.8
16.5
16.5
38,002
55.8
16.5
16.5
38,002
55.8
14.9
14.9
August
21,276
36.6
10.0
26.5
37,970
36.6
10.0
26.5
36,661
36.6
10.0
26.5
35,024
36.6
10.0
26.5
38,952
36.6
10.0
24.9
September
53,310
42.8
29.3
55.8
95,138
42.8
29.3
55.8
91,858
42.8
29.3
55.8
87,758
42.8
29.3
55.8
97,598
42.8
29.3
54.1
October
41,191
51.1
27.0
82.8
73,513
51.1
27.0
82.8
70,977
51.1
27.0
82.8
67,809
51.1
27.0
82.8
75,415
51.1
27.0
81.1
November
20,377
123
32.2
115.0
36,364
123
32.2
115.0
35,110
123
32.2
115.0
33,543
123
32.2
115.0
37,304
123
32.2
113.3
December
47,206
150
90.9
205.8
84,245
150
90.9
205.8
81,342
150
90.9
205.8
77,709
150
90.9
205.8
86,424
150
90.9
204.1
January
0
117
0.0
205.8
0
117
0.0
205.8
0
117
0.0
205.8
0
117
0.0
205.8
0
117
0.0
204.1
February
0
87.9
0.0
205.8
0
87.9
0.0
205.8
0
87.9
0.0
205.8
0
87.9
0.0
205.8
0
87.9
0.0
204.1
March
21,264
96.8
26.4
232.2
37,946
96.8
26A
232.2
36,638
96.8
26.4
232.2
35,002
96.8
26A
232.2
38,927
96.8
26.4
230.6
April
29,340
53.8
20.3
252.5
52,359
53.8
20.3
252.5
50,556
53.8
20.3
252.5
48,298
53.8
20.3
252.5
53,716
53.8
20.3
250.8
May
37,587
49.4
23.8
276.3
67,080
49.4
23.8
276.3
64,767
49.4
23.8
276.3
61,875
49.4
23.8
276.3
68,815
49.5
23.9
274.7
June
22,151
43.6
12.4
288.7
39,532
46.3
13.2
289.5
38,169
46.3
13.2
289.5
36,465
46.3
13.2
289.5
40,554
46.3
13.2
287.8
12 Month Floating PAN Load
(Ibslac/yr):
Annual PAN Load Limit
(Ibslaclyr):
288.7
350
289.5
350.00
-
2tt9.5
350.00
=_,
289.5
350.00
!
I
287.8
350.00

FORM: NDMLR 10-13 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page _ 1 of J7
Permit No.: WQ0016376
Facility Name: S&J Villari Livestock Processing Facility -Warsaw
County: Duplin
Month: June
Year: 2024
Field Name:
Zone 6
Field Name:
Zone 7
Field Name:
Zone 8
Field Name:
Zone 9
Field Name:
Zone 10
Area (acres):
1.17
Area (acres):
1.05
Area (acres):
1.25
Area (acres):
1
Area (acres):
1.46
Cover Crop:
Coastal Bermuda
Cover Crop:
Coastal Bermud
Cover Crop:
Coastal Bermuda
Cover Crop:
Coastal Bermuda
Cover Crop:
Coastal Bermuda
Load Type:
PAN
Load Type:
PAN
Load Type:
PAN
Load Type:
PAN
Load Type:
PAN
Field Loaded?
❑e YES ❑ No
Field Loaded?
[A YES ❑ NO
Field Loaded?
R1 YES ❑ NO
Field Loaded?
o YES ❑ NO
Field Loaded?
El YES ❑ NO
w
z
z�
�C
d
z o
a
z
a
a
z oz
aa
a
?
z
ao
z
a
zo o
a
z
a
a> a
tl
:�
a
o
2
a a
oaL
Q.
A
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d
a
a
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aa
mQ
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a
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7
J
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ai
B
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E�z
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>
04
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j
a
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2
o
'
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2
a
-6
-6
°a0
>
Month
gal
41,553
mg/L
Ibs/ac
Ibs/ac
gal
mg/L
lbs/ac
Ibs/ac
gal
mg/L
Ibs/ac
Ibs/ac
gal
mg/L
Ibslac
Ibs/ac
gal
mg/L
Ibs/ac
Ibslac
July
55.8
16.5
16.5
37,291
55.8
16.5
16.5
44,395
55.8
16.5
16.5
35,516
55.8
16.5
16.5
51,853
55.8
16.5
16.5
August
38,298
36.6
10.0
26.5
34,370
36.6
10.0
26.5
40,917
36.6
10.0
26.5
32,732
36.6
10.0
26.5
47,791
36.6
10.0
26.5
September
95,958
42.8
29.3
55.8
86,117
42.8
29.3
55.8
102,521
42.8
29.3
55.8
82,016
42.8
29.3
55.8
119,734
42.8
29.3
55.8
October
74,147
51.1
27.0
82.8
66,541
51.1
27.0
82.8
79,216
51.1
27.0
82.8
63,373
51.1
27.0
82.8
92,524
51.1
27.0
82.8
November
36,677
123
32.2
115.0
32,915
123
32.2
115.0
39,189
123
32.2
115.0
31,349
123
32.2
115.0
45,769
123
32.2
115.0
December
84,972
150
90.9
205.8
76,256
150
90.9
205.8
90,782
150
90.9
205.8
72,627
150
90.9
205.8
106,033
150
90.9
205.8
January
0
117
0.0
205.8
0
117
0.0
205.8
0
117
0.0
205.8
0
117
0.0
205.8
0
117
0.0
205.8
February
0
87.9
0.0
205.8
0
87.9
0.0
205.8
0
87.9
0.0
205.8
0
87.9
0.0
205.8
0
87.9
0.0
205.8
March
38,273
96.8
26.4
232.2
34,347
96.8
1 26.4
232.2
40,890
96.8
26.4
232.2
32,713
96.8
26.4
232.2
47,760
96.8
26.4
232.2
April
52,813
53.8
20.3
252.5
47,395
53.8
20.3
252.5
56,423
53.8
20.3
252.5
45,138
53.8
20.3
252.5 11
65,903
1 53.8
20.3
252.5
May
67,659
49.4
23.8
276.3
60,719
49.4
23.8
276.3
72,284
49.4
23.8
276.3
57,829
49.4
23.8
276.3
84,430
49.4
23.8
276.3
June 39,872 46.3
13.2
289.5
35,783
46.3
13.2
289.5
42,599
46.3
13.2
289.5 34,080
46.3
13.2
289.5
49,756
46.3
13.2
289.5
12 Month Floating PAN Load
289.5
289.5
289.5
>-a,
289.5
289.5
(Ibs/aclyr):
Annual PAN Load Limit
350
350 00
350.00
`
350.00
350.00
'
(Ibs/ac/yr):

FORM: NDMI.R 10-13 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page,_ of J
Permit No.: WQ0016376
Facility Name: S&J Villari Livestock Processing Facility -Warsaw
County: Duplin
Month: June
Year: 2024
Field Name:
Zone 11
Field Name:
Zone 12
Field Name:
Zone 13
Field Name:
Zone 14E
Field Name:
Zone 14W
Area (acres):
1.43
Area (acres):
1.23
Area (acres):
2.16
Area (acres):
13.73
Area (acres):
7.7
Cover Crop:
Coastal Bermuda
Cover Crop:
Coastal Bermuda
Cover Crop:
Coastal Bermuda
Cover Crop:
Coastal Bermuda
Cover Crop:
Coastal Bermuda
Load Type:
PAN
Load Type:
PAN
Load Type:
PAN
Load Type:
PAN
Load Type:
PAN
- -
Field Loaded?
R1 YES NO
Field Loaded?
L1 YES ❑ No
Field Loaded?
2 YES ❑ No
Field Loaded?
I ( YES ❑ No
Field Loaded?
0 YES ❑ No
d
z
z
d
z
°
z
z
°
z
aa=a
z
z
>�
DQ
za
z°
oa
0.
mo
a
..0ro
oa
a
IL
°
J
a
N
CD =
°
.
a
tM =?°
J
6t-
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7.N_
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'
z
,g
=
T 10
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�
Jao
zaJ
=
O
r
>
°
,<
E
> =O
a
j
7
>=a
7>
C
O
a
Month
gal
50,787
mg/L
Ibs/ac
Ibs/ac
gal
mg/L
Ibs/ac
Ibs/ac
gal
mg/L
Ibslac
Ibs/ac
gal
mg/L
Ibslac
Ibs/ac
gal
mg/L
Ibs/ac
Ibslac
July
55.8
16.5
16.5
43,684
55.8
16.5
16.5
76,713
55.8
16.5
16.6
413,380
55.8
14.0
14.0
231,830
55.8
14.0
14.0
August
46,808
36.6
10.0
26.5
40,262
36.6
10.0
26.5
70,703
36.6
10.0
26.5
387.717
36.6
8.6
22.6
217,438
36.6
8.6
22.6
September
117,284
42.8
29.3
55.8
100,881
42.8
29.3
55.8
177,154
42.5
29.1
55.6
282.056
42.8
7.3
30.0
168,183
42.8
7.3
30.0
October
90,623
51.1
27.0
82.8
77,948
51.1
27.0
82.8
136,884
51.1
27.0
82.6
1,122,333
51.1
34.8
64.8
588.398
51.1
32.6
62.5
November
44,828
123
32.2
115.0
38,559
123
32.2
115.0
67,712
123
32.2
114.8
875,365
123
65.4
130.2
490,920
123
65.4
127.9
December
103,855
150
90.9
205.8
89,330
150
90.9
205.8
156,871
150
90.9
205.6
127,319
150
11.6
141.8
71,402
150
11.6
139.5
January
0
117
0.0
205.8
0
117
0.0
205.8
0
117
0.0
205.6
765,274
117
54.4
196.2
429,178
117
54.4
193.9
February
0
87.9
0.0
205.8
0
87.9
0.0
205.8
0
87.9
0.0
205.6
711,660
87.9
38.0
234.2
399,110
87.9
38.0
231.9
March
46,778
86.8
23.7
229.5
40,236
96.8
26.4
232.2
70,658
96.8
26.4
232.0
506.716
96.8
29.8
264.0
284,173
96.8
29.8
261.7
April
64,548
53.8
20.3
249.7
55,520
53.8
20.3
252.5
97,500
53.8
20.3
252.3
956,377
53.8
31.3
295.2
536,350
53.8
31.3
293.0
May
1
82,693
49.4
23.8
273.6
71,128
49.4
23.8
276.3
124,908
49.4
23.8
276.1
118:810
49.4
3.6
298.8
66,630
49.4
3.6
296.5
June
48,733
46.3
13.2
286.7
41,918
13.2
289.5 73,612
46.3
13.2
289.3
682,790
46.3
19.2
318.0
382,920
46.3
19.2
315.7
12 Month Floating PAN Load
286.7
9.5
289.3
318.0(Ibs/ac/yr):
6]350.00
Annual PAN Load Limit
350
<
350.00
'
350.00
350.00
(Ibs/aclyr):

FORM: NDMLR 10-13 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page - of S
Permit No.: WQ0016376
Facility Name: S&J Villari Livestock Processing Facility -Warsaw
County: Duplin
Month: June
Year: 2024
Field Name:
Zone 15
Field Name:
Zone 16
Field Name:
Zone 17
Field Name:
Field Name:
Area (acres):
0.73
Area (acres):
1.25
Area (acres):
0.82
Area (acres):
Area (acres):
Cover Crop:
Norfolk
Cover Crop:
Coastal Bermuda
Cover Crop:
Coastal Bermuda
Cover Crop:
Cover Crop:
Load Type:
PAN
Load Type:
PAN
Load Type:
PAN
Load Type:
PAN
Load Type:
PAN
Field Loaded?
R1 YES ❑ No
Field Loaded?
C YES ❑ No
Field Loaded?
121 YES j] NO
Field Loaded?
❑ YES NO
Field Loaded?
❑ YES R] NO
_d
z
a
Z
d
z=
z
a
°m
zd
z
ma
°
dzzC
_a
aN=
z
aN
a
°o
aa
°��
V
�
a
°
a>
roa
O
s
>o
a
s
n
Y_>
J4
Q
Ra
N
>0
O
3 Z
d
J N
O Z
N
m N
J
O Z
d
co C
��
w J
m
z
N
N
q
O
3 Z
E
�"
.�
=J
Ea
7
£
w°
�J
Ea
7
E
��
N C
a�
=
Ea
7
E
N
c
Ea
O
E
��
N=
a'C.+
cJ
Ea
O
3
C
a 0
O
v a
O
C
O
g
V°
a
U°
C
�°
U a
>°
>
a �
>°
V
>°
a �
0
a v
Month
gal
25,927
mg/L
Ibs/ac
Ibslac
gal
mg/L
lbs/ac
Ibs/ac
gal
mg/L
Ibs/ac
Ibs/ac
gal
mg/L
lbs/ac
Ibslac
gal
mg/L
Ibs/ac
Ibslac
July
55.8
16.5
16.5
26,666
55.8
9.9
9.9
17,494
55.8
9.9
9.9
August
23,895
36.6
10.0
26.5
20.489
36.6
5.0
14.9
13,440
36.6
5.0
14.9
September
59,872
42.8
29.3
55.8
36,603
42.8
10.5
25A
24,011
42.8
10.5
25.4
October 1
46.262
51.1
1 27.0
82.8
27,706
51.1
1 9.4
34.8
18,175
51.1
9.4
34.8
November
22,884
123
32.2
115.0
24,526
123
20.1
55.0
16,089
123
20.1
55.0
December
53,018
150
90.9
205.8
27,168
150
27.2
82.1
17,822
150
27.2
82.1
January
0
117
0.0
205.8
0
117
0-0
82.1
0
117
0.0
82.1
February
0
87.9
0.0
205.8
0
87.9
0.0
82.1
0
87.9
0.0
82.1
March
_
23,879
96.8
26.4
232.2
25,515
96.8
16.5
98.6
16,737
96.8
16.5
98.6
April
32,952
53.8
20.3
252.5
25,348
53.8
9.1
107.7
16,628
53.8
9.1
107.7
May
42.214
49.4
23.8
276.3
24,259
49.4
8.0
115.7
15,914
49.4
8.0
115.7
June
24,877
46.3
13.2
289.5
29,904
46.3
9.2
125.0
19,616
46.3
9.2
125.0
12 Month Floating PAN Load
289.5
f
125.0
%:
125.0
(lbs/ac/yr):
350
t
:;,
350.00
'-:
350.00
0.00
0.00
_
Annual PAN Load Limit
(Ibslac/yr):

FORM: NDMLR 10-13 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page 5- If. IS —
Did the mass loading rates exceed the limits in Attachment B of your permit? [] Compliant ❑ Non -Compliant
If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the dates) of the non-compliance and describe the corrective
action(s) taken. Attach additional sheets if necessary.
Operator in Responsible Charge (ORC) Cortification
ORC: Gerald Lamar Matthews
Certification Number: 993131
Grade: SI Phone Number: 910-289-7500
Has the ORC changed since the previous NDMLR? ❑ Yes R] No
Permittee Certification
Permittee:
SAM VILLARI
Signing Official:
Signing Official's Title: OWNER
Phone No.: 910-293-2157 Permit Exp.: 11/30/25
rX
Signature Date
By this signature, I certify that this report is accurrate and complete to the best of my knowledge.
Signature Date
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the
information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly
responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations.
Mail Original and Two Copies to:
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617

�ar..i,.4{'�`�?•� u�' �� , } :". r �� 1,
-r
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ° 910.392.0223 Lab S 910.392.4424 Fax
710 Bowsertown Road, lvlanteo, NC 27954 ° 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 " 910.347.5843 Lab/Fax
info;d�enviaonmentalchemists.eom
Tha Ports Company
Date of Report: Jul 17, 2024
892 Penny Branch Road
Customer PO #:
Warsaw NC 28398
Customer ID: 08100099
Attention:
Report #: 2024-14776
Project ID: Effluent / Streams
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
24-36251 Site: Effluent
612712024
10:00 AM Water Gerald Matthews
Test
Method
Results
Date Analyzed
PAN
43.6 mg/L
07/08/2024
Used 39°1c Mineralization Rate
Ammonia Nitrogen
EPA 3501 Rev 20 1993
83.3mg/L
07/02/2024
Total Kjeldahl Nitrogen (TKN)
EPA 351 2. Rev 2 0. 1993
89.7 mg/L
07/03/2024
Nitrite Nitrogen
EPA 353.2, Rev 2 O. 1993
0.10 mg1L
06/27/2024
Fecal Coliform
IdmCoNeft-16
11200 MPN/100ml
06/2712024
Total Dissolved Solids (TDS)
SM 2540 C-2015
340 mg/L
06/27/2024
Residue Suspended (TSS)
SM 2540 0-2015
43.0 mg/L
07101/2024
Total Phosphorus
Sin 4500 P (P-M)-2011
4.14 mg/L
07/03/2024
BOD
SM 5210 8-2016
34 mg/L
06/28/2024
Chloride
SKU500 CI E-2011
54 mg/L
06/28/2024
Nitrate Nitrogen (Cale)
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev 2.0 1993
< 0.02 mg/L
06/28/2024
Nitrate Nitrogen
Subtraction Method
<0.02mg/L
06/2812024
Total Nitrogen (Cale)
Total Nitrogen To't' Nitrogen 89.7 mg/L 07/'03/2024
Report 0:: 2024-14775 Page 1 of 2

Environmental Chemists, Inc.
+.e irochem
ANALYTICAL & CONSULTING CHEMISTS
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
253-A �Vimington Highway, JacksonviLe, INC 28W 4 910.347.5843 Lab/Fax
info;a;cnvi ronmentalchemists.com
The Pork Company
Date of Report Jul 17, 2024
892 Penny Branch Road
Customer PO #:
Warsaw NC 28398
Customer ID: 08100099
Attention:
Report #: 2024-14776
Project ID: Effluent / Streams
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
24-36252 Site: Upstream #1
6/2712024
10:15 AM Water Gerald Matthews
Test
Method
Results
Date Analyzed
Ammonia Nitrogen
EPA 350.1. Rev. 2.0. 1993
0.9 mg/L
07/02/2024
Total Kjeldahl Nitrogen (TKN)
EPA 351.2. Ru. 2.0.1993
1.8 mg/L
07/03,12024
Nitrite Nitrogen
EPA 353.2, Rev. 2.0. 1993
0.t?2 mg/L
06/27/2024
Total Phosphorus
SM 4500 P (F-H)-2011
0.11 mg/L
07/03/2024
Fecal Coliform
SM 9222 0-2015 MF
25 Colonies/100ml- 06/27/2024
Nitrate Nitrogen (Cale)
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0, 1993
0.09 mg/L
06/2812024
Nitrate Nitrogen
&btavic-nMethod
0.07mg/L
06/2812024
Total Nitrogen (Cale)
Total Nitrogen
Total Nitrogen
1.9 mg/L
07/0312024
Lab ID Sample ID:
Collect DatefTime Matrix Sampled by
24-36253 Site: Downstream #1
6/27/2024
10:25 AM Water Gerald Matthews
Test
Method
Results
Date Analyzed
Ammonia Nitrogen
EPA 350.1, Rev 2.0. 1993
18.6 mg/L
07/0212024
Total Kjeldahl Nitrogen (TKN)
EPA 351.2, Rev 2.0. 1993
25.7 mg/L
07/03/2024
Nitrite Nitrogen
EPA 353.2, Rev. 2.0. 1993
0.02 mg/L
06/27/2024
Nitrate+Nitrite-Nitrogen
EPA 353.2. Rev_ 2A..1993
0.54 mg/L
07/10/2024
Total Phosphorus
SM4500 P (F-H)-2011
2.47 mg/L
07/03/2024
Fecal Coliform
SM 9222 D-2015 MF
>30000 Colonies/100ml- 06/27/2024
Nitrate Nitrogen (Cale)
Nitrate Nitrogen
subtraction Method
0.52mg/L
07/17/2024
Total Nitrogen (Cale)
Total Nitrogen
Total Nitrogen
26.3 mg/L
07/17/2024
Comment:
Reviewed by:
43
Repot; "P: 2024-14776
Page 2 of 2

Environmental Chemist, Inc., Wilmington, NC Lab #94
Sample Receipt Checklist
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Client. s 1'lC� � 0 Date: 2� � Report Number: 2024 - � �-7?b
1-1
Receipt of sample: E HEM Pickup . Client Delivery ❑
JUPS ❑ Fed Ex ❑ Other ❑
❑ YES
❑ NO IN N/A 1. Were custody seals present on the cooler?
❑ YES
10 NO JR N/A 2. If custody seals were present, were they intact/unbroken?
(Original temperature upon receipt .a °C Corrected temperature upon receipt °C
How temperature taken: ❑ Temperature Blank Against Bottles
IR Gun ID: Thomas Traceable S/N: 230222540 IR Gun Correction Factor °C: 0.0
YES
❑ NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
❑ NO
4. Were proper custody procedures (relinquished/received) followed?
YES
❑ NO
S. Were sample ID's listed on the COC?
YES
❑ NO
6. Were samples ID's listed on sample containers?
YES
❑ NO
7. Were collection date and time listed on the COC?
YES
❑ NO
8. Were tests to be performed listed on the COC?
YES
❑ NO
9. Did samples arrive in proper containers for each test?
YES
❑ NO
10. Did samples arrive in good condition for each test?
YES
❑ NO
11. Was adequate sample volume available?'
YES
❑ NO
112. Were samples received within proper holding time for requested tests?
YES
❑ NO
113. Were acid preserved samples received at a pH of <2?
❑ YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15. Were sulfide samples received at a pH >9?
YES
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES 113
NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
❑ NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SOQ HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

ENVIRONMENTAL CHEMISTS I14C OFFI E:910.3» 0223�IFAX910392-1.1245
Analytical 8 Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 into(�benvironmentalchemists.com
COLLECTION AND CHAIN of cusTnny
CLIENT: The Pork Company
PROJECT NAME: WWTF Effluent _
REPORT NO:
ADDRESS: 1012 US Hwy 117
CONTACT NAME:
PO NO:
Warsaw, NC 28398
REPORT TO: Gerald Matthews, ORC
PHONEIFAX:
Permit Number: WQ0016376
email:
%X0111lum UY.
Sample Identification
Collection
5AMPLE
w
h N a
a o 2
E o
TYPE: I = Influent,
elf Ccew
g
a "
E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Stodge, Other:
PRESERVATION -
m W J x
x O o °� ANALYSIS MQUESTED
S Z x * _ o
t
Time
Tempo
PPI-001 (Effluent-1/month)
�
Lt ysl
X
BOD,TSS,NO2 ~ �
1 IF+
G
PPI-001 Effluent-1/month
X
NO3# NH3, T'I N,"I'otal P, PAN, Dotal N
G
pH (field):
C
pi
X
Fecal Coliform
GG
P
G
March, July, November
PPI-001 Effl-Triannuals
C
P
X
TDS, Chloride
G
G
P
PPI.002 (Upstream)
o
C
p
�L
X
IN02
G
PPI-002 Upstream
P
�J
_
!`
X
Z
TKN, NH3, NO3, Total P, Total N
G
PPI-002 U stream)
C
X
Fecal Coliform
G
C
P
G
PPI-003 Downstream
a
X
NO2
G
PPI-003 (Downstream)
P
40.6
X
Z
TKN, NH3, NO3, Total P, Total N
G
P
PPI-003 Downstream G G X Fecal Coliform
Samples due 1/month
Transfer
1.
Relinquished By:
Date/Time
_ Received By:
Date/Time
2.
i emperature when rcecewea -u:
Delivered By: Received By: <Tste Date: Z�' c- Time �-
Comments• f TU NA OUND: