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WQ0018708_GW Monitoring_20071212
_Bay Tree Utility Company REG�IM r a _.- 33 West Bay Ridge Road AN Harrells.- NorthCarolina 28444 t (910) 588-4432 DENR—FALEREGONALD�7C�. December 12, 2007 Mr. Joel Shields NC Dept. of Natural Resources Division of Water Quality 225 Green St., Suite 714 Fayetteville, NC 28301 Dear Joel Shields: Please be advised that Mr. Brooks. Barwick.Will serve as,•signer for all pertinent business transactions for Bay Tree Utilities in the absence of ]Vlr: D.'.Stephen-Jones. IVIr. Jones is expected to be absent for an.extended period of time due to health reasons. Sincerely: D. Step . e nes . President, Lake Creek rporation d.b.a. Bay Tree Utility Company. • ACILArpWIN179171MATION Please Print Clearly or Type Bay Tree Lakes FacilityAddr6bs. -33-1W-.*Bay,Rid &e Road Harrelsl'sk2846 laden ounty Ste hen Jones (ZIP) --588-4432-, - ont erson:;_�� Telephone #9 10, 11 .- -,. - Z. - " � ` 4 aW ft/' Ite',Namei :Well #3 No. of Wells to be Sample& Ifff om7frm ilcall6n: Number (from. Permit):. For Groundwalbr Treatment Systems WellAdWl -Wel]L. #3 Wel(�De'70 Jt',_'Well Diameter: - 2 in. Check One: s(c"e6fi4d"Q`ritdrvaI::,, ft. ft. �" - ; , O'Influent. (98) — iM&fiir Depftfb� ,Ljq4eI:_Z, UP -ft. 'below measuring point. A El Effluent (99) Me I' as �6161 s —ft.; above land surface. ,2` Gall6iiiii'df�gWiitdr,,pumpecVb ed before sampling: Aja5 plecific'Coriclubtance uMhos % `Od TPr9p., or Appearance pW(� TOP Chlol Greas4 Phenol '`', sbifite SOCHI Tof a-. TKN` PERMIT 4: 'EXPIRATION DATE: _-2 L-01 Non:Dlscharge 1WQ00 18708 UIC NPDES TYPE OF PERMITTED, OPERATION BEING MONITORED".;,` - Lagoon —Rerhediallon: Infiltration Gallery 'I'.T.". w/ Spray Field Remediallon: Rotary Distributor, Land Application of Sludge". Other. NOTE: Values should reflect dissolved and colloidal concentrations. Date sample collected: 11"26-07 Date sample ana yze I Vann Laboratories. Oxford Llioxatory Ir Laboratory'Name: 4AS Certification -No.' 22, 75 .1 3, (SamplesE6 for metals ward'ccilected unfillered;..—Y NO and field acidified — YES NO). mg/I Nitrite (NO2) "as N moll NI - Nickel moll AFFebal &7ota <-1—Mooml. /I 00ml Nitrate (NO3):6s N moll Phosphorus: Total as P moll Pb - Lead Zn 'Zinc 11j,m6thbd for highly turbid camp 3). Orthophosphatd mg/l Ammonia Nitrogen mg/I, PIldsk. Total moll. Al - Aluminum moll Other (Specify Compounds and Ccincefitration units). analvzed), units Ba ma Barium /I moll Ca -Calcium I o moll' Cd - Cadmium V . ..... moll. Chromium: Total id;011s: moll Cu- Copper, t tolflg/l mg/l moll Fe - Iron gAntt ORGANICS: (GC,Gb/MS,HPLC),:"4.;:. mg/I -uMhos Hg .- Mercury. "n rMati g/l (Specify test and method'#. 41tach' Y': h d6 'dtgnce, b K - Potassium mg /I Report Attached? Yes_V(1)�:-, 0 a- moll Mg-'- Magnesium moll VOC method moll Mn- Manganese mg/l 7 methodkt,-, method ffwz", JC_.1 A-, 11101 #%gone name ana 1 ilia - I -lease print or type ----------- Pen FacHa : rr cor Screei Depth me azi"st Gall6t Fie ,5 ' PARR COD; Co 60,fi ' co"Ific, R Ea opecli T K INCie" Elm • )BIVIATION Please Print Cleady or Type ay. Tree Likes - 'different): ':33.,'W-l;l* Bay Ridixe, Road 2840county - W&) BlAden ...,Stephen Jones (zip) 910=588-4432 3on. Telephone # 6il 6'Name:— Well 15: No. of Wells to be,'Pampled: 4 ift16n Number (from Permit): -Well 15 For Groundwater treatment Systems 18- 11 ff %A/ If Ill Mare 2 In PERMIT 4: EXPIRATION DATE: UtO Non'-Discharge-WQ0018708 _UIC NPDES aPE OF PERMITTED OPERATION BEING MONITORED,` Lagoon —Rerhediallon: Infiltration GallerySpray Field Remedlationi: Rotary Distributor Land Application of Slul dge" Other: ft. to 0neCK one: D InflLtent (98) tAOTE: Values should reflect dissolved and tdr:Leveh' ft.,beloW measuring point. 0 EffIdent, (99) colloidal concentrations. lbIht:Is_,ft. ,above land surface. Mbr�,pumpedlballed before sampling: led: /L**'_67 Date sample a�nalyi�ld'&- Date sample collected: V Laboratory Name: Vana Labaratmcies, OKfimd laborabmT.,7r4��jp TempOCi'Odot- Specific, Qionduclance uMhos :,.'Appearance Cerilficallon-No. 22, 75 1. 7 N, ,MOaimpl�es for metalls-were,601lected unflItered,.—YiES.' NO and field acidified YES NO). — 6"g mg1I Nitrite (NO2)� as,N m 11 NI - Nickel AF:fecal: -e'] /100ml Nitrate (NO�) as, N' <0,16 mg/l Pb - Lead g/l AFF-Total— J1 00ml Phosphorus: Total'as'P_ ld- 0. 05 mg/I Zn - Zinc N ffib - I . hod for hIghly.lurbld samples)!, Orthophosph'ate'. mg/l Ammonia Nitrogen ��§611ds-,"Total mg1l Al - Aluminum mg/l Qther (Specify Compounds and, Cnn6eh6aII6'6`0nl6) analyzed) units. Ba - Barium.'— MCI mg/I Ca - Calcium , SIR tff 11,1 mg/I Cd - Cadmium L_ mg/l mg/I Chromium: Total a anmg/l mg/I Cu- Copper mg/l mg/I Te -Iron, PrOce *nbWlt ORGANICS: (GC,GC/MS,HPL mg/I Hg - Mercury to or pwQlgpc_g/I (Sp6cIfy test and method'#. Astach 1, ohdUctanice . kbos K - Potassium mg/l Report Attached?' Yes✓ (11) No" 0 @�m g/I Mg:& Magnesium mg/l bod VOC met # mg/I Mn -Manganese mg/l method-�.11 * 17;`-,� meth y 'W 7, 7; violations. I Z.) w print or type Perfnit Fibillt 77-,iWy Cohtaiy( t " -:- "S'. We V61fild ,Screen Nleasui �• Gallons -.17161dj'al v 9 (Nola :,U PH;Jcgi TOC Chloral ArsE01 Tots TKt )HMA1IQN Please Print Clearly, or 77 Type Bay Tree Lakes W:, Bay Ridize, Road 28466C;ounty_Bladen Stephen Jones, 04. 8) (4) Telephone #910-588-4432. No. of Wells to b6 Sa 4 (IromParm in Number (from Permit): Well # I For Groundvlater'Treatment Systems 2 Check One::, al ft. 0 Influ'ent.,'(98) below measuring point. f Is ft.-a*bove*:1drid surface.- Effluent .'(99)-- r,;pumped/bailed before sampling: 2.93 pH -S136-cific'Conductance 5 _, - --- . dM;, hos �mp 4C Odor Appearance ,. , , PERMIT M EXPIRATION DATE: f Non=Dlscharge WQ0018708 _UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED r Lagoon —Rernecriatlon: Infiltratio n . da' 118� ` y' Spray Field Remedlallon: ;Itg� Land Application Sludge' Rotary Distributor ,'4 of Other: NOTE: Values should r"e"flect dissolved and colloidal concentrations. Date sample collected- Date s -a Laboratory Name: Vam Mbomtorjes, QKEDrd Certification No.' 22, 75 jz6 7 ile:arial , v z e i FM,!(Sbm0Ies for;metals,wer6'collected unfiltered,.' YES�,.':_,: NO and field acidified YES NO). mg/I Nitrite, (NO2Ya mg/I Ni -Nickel K4 F Fd 6 a I 1100MI Nitrate (NO3) as N lb mg/I L Pb - ead MF Total'` J100ml Phosphorus: Tot8lbs P A 0,!r mg/I Zn - 'Zinc Wi'6'e.l.h.od for. highly turbid �Pbllft Total mg1I Orthophosphate Al - Aluminum mg/I Ammonia Nitro en 9 alfted) —Units Ba - Barium 10 mg/I MnIl Other (Specify Compounds and Conde a mg/I Ca - Calcium, mg/l mg/I Cd-- Cadmium n mg/1 mg/I Chromium: Total unite mg/I --77 id-,1011s mg/I Cu - Copper- ,j,xrn4%onvr1 mg/I mg/I Fe - Iron mg/I ORGANICS: (GC,GC/MS,HPI_C)'' mg/I uMhos Hg - Mercury K - Potassium Mg/I -mg/I (Specify test and method #. Attach lab report.) Report Attached?, ✓YeS�(1) '6hdu ctance or ' mg/l Mg'- Magnesium mg/I V00:method #= mg/I Mn - Manganese mg/I -, ., �,': , method#= method#. . 1111"llu 'Ale =a.nd5Tl'1' se (or I ze A 1) N a and Tille - Please print or type 77 CJ Signature of Pdrnli (Date): 9r or eii Ns.SON pH,-'(Wh Td&_ Chl6h—d Arserilcl GPhre"e'. 1 -6 1 n sulfat"d S'P6,601i Total �'- s I cerlifj tielnri - 7` G Please Print Clearly or Type 4`33.'W-.', Bay, Ridge -,Road jjjr) 7, 28466county Bladen �_Stephen Jones- (ZIP) Telephone #9 10-589-4432, 36;Na"me: W61142 No. of Wells to be Sampled.'"' 4 _dt16n`,Nu mber (frohn Permit): Well #2 For Grotmdwal�r, Treatment Systems Well Diameter: 2 In. Check One: ft. to ft. ❑ Influent ('98) te� e� , Level. 61240 M. below measuring point. 11 Effluent (99) 16AAHS , ft.-abo've land surface. af&i.,'ptjmpedlbailed before'sampling: i-;-pH' 1 4, 5_ .,"Specl"fic;'Conductance uMh os _-,,mj,,,Odot, ..'Appearance 'PERMIT M EXPIRATION DATE:- Non:Dlscharge WQ0018708 UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED;.&.[' Lagoon Rerbecliation: lnfiltrallbn Gallery spray Field RemedIallon: Rotary Distrlbulori, Land Application of Sludge',;; Other: NOTE* Values should reflect dissolved and colloidal concentrations. Date sample collected: Date Sam le'a'na"lyze Laboratory, Name: Van[iLibamtories, QQK&fiord rr,T r Certlflcallon.No: 22. 75,67 ff(Sdrriples for 'metals, wero'collected unfiltered ,,._-YES; ' NO and field acidified -YES NO). mg/I Nitrite (NO2) as, N mg/I Ni - Nickel jngk F 6 q a 1: <I 1I 00ml, Nitrate (NO3) as-N mg /I Pb - Lead /1 00ml Phosphorus: Total as. P < A, mg/I Zn 'Zinc .,Method for highly turbid sarnpljw. Orthophosphate mg/I Ammonia. Nitrogen ,bllds'Tbtal :��o m g/I Al - Aluminum ther (Specify Compounds and bo6c6nIraIlon":UnIt6. nalvzed) units 'Ba - Barium 11-no, mg/I Ca - Calcium :mg/ mg/I Cd - Cadmium., mg/I Chromium: Total mg/I mg/I Cu -Copper Gemou"11 mg/I Fe - Iron" tntorma E)walaorng/l ORGANICS: (GC,GC/MS,HPLC),, mg/I Hg - Mercury mg/I (Specify test and method'#. 6flach, iductance uMhos K - Potassium. mg/I Report Attached?, Yes V (1);,.,'Nd' mg1l Mg'- Magnesium mg/I 77.;-(0), VOO method mg/I Mn - Manganese mg/I methodJt7,w methiv 9.m ........... r alluf 15. FWP, .d J0 '40 , 10% F . Mrld MOSAi a7Zq,4_-.S and T111a - Plan, or type S 4 e- ,.,3 � vs. i � ...a— i x� ,.� `',.,� -> r s4,t.�� m vr%S -.� �• v .'tt�l� r rr-„•-a� 4 .'zif- t .s. - - 1_.- . -P.O. Box 668 Y �;, ... �-•T _� - .. _. -------------------- ... • •Wallace NC,• 28466 • - Phone: (919)28"966 - Fax: (910)285-3966 Well Samples Client. .�� pH Meter Model: 50 Date Sampled: - Serial # C000822Z Calibrated: Date: Time: S�dR . Sampled By: a � . Buffer 4.00 Al.�o Buffer 10.00 Buff, r•7.00%' 1,. D � - Analyst: Location Well 1. D. J, Depth of Well (ft) . : D 40 Depth to Water Level (ft) .• . Water Depth (ft) Well Vol. * 3• (Gals) Time Sampled.; 14/1 Temperature, °C �. �, s• • s•' Color Sampler's Signature: iE Q Daie:o t ^� 7 Phone: (910) 285-3966 Bay Tree -Lakes: Vann. Labor a o' ries P. O. Box:668. Wallace; NC 28466 , rt WaslewaterlD # ,t _ -- -- s Collected November 26,2007 PA44METER - UNITS DATE ANALYZED Well # 1 Well #2 Well f3 Well 15 PH - BOD5 mg%L COD mg1L Fecal Coliform co1.1100 ml 11-26 -07 < 1 < 1 < 1 < 1 Total Kjeldahl Nitrogen mg;X Total Residue (Dissolved] m91L 11-26-07 <40 <40 56 62 Total Suspended Residue mglL_ . Detergents MBAS mg1L Oil & Grease mglL Total Phosphorous mg1L • 12-6-07 <0..05 <0.05 0.26 <0. 05 Sulfides mgX Phenols uglL Total Chromium ug/L Total Copper ug/L Total Magnesium mglL Total Zinc ug/L Ammonia Nitrogen mg1L 11-26- 07 <0.20 <0.20 <0.20 . 2.38 Nitrate mg/L 1-28- 07. <0.10 <0:10 <040 <0.10 ` Chloride mg/L 1-29-07 8.2 4.7 6.5 11.1. TOC .. mg/L , 1-30-07 " —2.10 ;.:.;. 8:2 - 11.4 .; 9.15 *Analysis performed by Oxford Laboratory w. Signed: 77 •{ Tritest, Inc. 6624 F } w 3 u Page 1 of 3fi{ _ �' `•, ' ^`'- r ��,; k, �e a . i+ :-x. Su ite .` .. i ... Telephone 9164.63 9763 • WI�til7lriCjtOf1,::NC. - 28411 NC/WW ert. #. 075 Fax: 910-343-9688 - NC/DW Cert #t 37721 www.tntestmc.com Labo"ra-tory Pop 6rt, o — . Prepared for — Wayne Vann Vann Laboratories Report Date: 12/17/2007 PO Box 668 _ ,>_. _ Date Received: 11/27/2007 Wallace, NC 28466 Work Order#: 0711-56675 Project No.: Bay Tree Lakes Cust.'Code: VANN79.,. Project ID::, VL' 112607103-7 :TPHOS/NOX/6230D 'Gust.-P.O.# Vo. Sample ID Date -Sampled Time Sampled. Matrix Sample Type Condition 0.01 VL112607103 11/2,612007' 3:45 WW Grab 4 +/- 2 deg C Analyzed Test Performed Method Results Date Time Qualifier .. . Nitrate+Nitrite ' Attached *:6.48 mg/L 12/7/07. 16:21 No. Sample ID Date Sampled Tme Sampled Matrix Sample -Type Condition. 002 VL112607104 11/26/2007 - 3:10 GW Grab : 4 t/- 2 deg C Analyzed - Test Performed Method Results Dates Time Qualifier Phosphorus, Total EPA 365.4 *'<0'.05 mg/L -1216107 14:24 '. Nitrate EPA 353.2. *•<0.10.mg/L 11/28/07 11'-.00 �o. Sample ID Date Sampled .. Time.Sampled Matrix- Sample.Typ6 Condition . 003. VL112607105 1.1/26/2007 3:35 GW Grab .. 4 +l -2 deg C Analyzed Test Performed Method Results Date. •Time . Qualifier - Phosphorus, Total . EPA 365.4 * <0.05:mg/L 12/6/07 14:24 Nitrate EPA'.353.2 <0.10 mg/L 11/28/07 11:00 40. Sample ID Date Sampled ' Time Sampled Matrix Sample Type Condition' 004 VL1160 27106 11/26/2007 4:00 GW Grab 4 +/- 2 deg C' Analyzed Test Performed . Method Results Date .Time Qualifier Phosphorus, Total,._ :EPA _365.4 * 0.26 mg/L :.12/6/07: = 14:24 - .Nitrate :'_ -EPA.353.2 <0.1Qmg/L '11/28/07-.,11:00: -m z a � Telephone ,.910 768-9793f Fax 910-343 9688 `" WiIM www.tritestinc.com Wit- j NC/WW Bert..#: 075 l �C+ 28411 s NC/DW Cert.V; 37721 Laboratory Report Work Order #: 0711-56675 ;o. Sample ID Date Sampled Time Sampled Matrix Sample Type Condition )05 VL112607107 _ 11126/2001 4:20 GW Grab 4 +/- 2 deg C Analyzed Test Performed Method Results Date Time Qualifier Phosphorus, Total EPA 365.4 * <0.05 mg/L 1216/07 14:24 Nitrate EPA 353.2 <0.10 mg/L 11/28/07 11:00 lo. Sample ID Date Sampled Time Sampled Matrix Sample Type Condition )06 WELL #1 11/26/2007 4:20 GW Grab 4 +/- 2 deg C - Analyzed Test Performed Method Results " Date Time Qualifier M-6230D M-6230D ATTACHED 1215/07 6:32 lo. Sample ID Date Sampled Time Sampled • Matrix Sample Type. Condition )07 WELL #2 11/26/2007 4:20 GW Grab 4 +/- 2 deg C Analyzed Test Performed Method Results Date 4. Time Qualifier M-6230D ' M-6230D ATTACHED 1215/07 6:32 Io. Sample ID Date Sampled. Time Sampled Matrix Sample Type Condition )08 WELL #3 11126/2007 4:20 GW Grab 4 +1- 2'deg C Analyzed Test Performed Method Results Date Time Qualifier M-6230D' M-6230D ATTACHED 12/5/07 6:32 Tritest, Inc. z > yro- '�s 7 y.. _`"r'. j-ri•- r i {s 9 ?- ,`: Yelephone • 910 763-9793 � ` w ``t`, ' , $Ulte G '� � � NC a Fax: 910-343-9688 M. s 1WW 075, Wilmington; NC 28411 NCIDW cent#; 37721 .. . www.fritestinc.com .. Laboratory Report Work Order #: 0711-5667.5 Reviewed by:, est, Inc = r Dec.14 2007`1T.45AM "''Tr.i-te'st.`f�az " o Telephone:",Will) 834 Fax: (919) 834.641 vok N_o 8567 P, 28 7 <•��� i=RPagel of 7 f 1 y1CIVVW pert. #: 067 4 NC/DW Cert. #: 3.7131 La. bo.ratory' Report _. --Prepared for- MARY GODLEY Report -Date.: Report 211112007 TRITEST / WILMINGTON Date Received: 11/28/2007 6624 GORDON ROAD UNIT G Work Order#: 011.1-01514 WILMINGTON, NC 28411 Project No.: Cust: Co: OX9793 - Project ID: -0711-56675 .. Cust. P.O.M , No, Sample ID Date Sampled Time Sampled Matrix Sample Type, Condition 001 0711-56675=001 0:00 W1W Unknown 4 +1- 2 deg C Analyzed Test Performed Method Results Date '.-Time - Qualifier Nitrate -Nitrite EPA-363.2 .. 6.48 mg/L as N. 4 -. 12I7107 16:21 No.',' Sample ID, Date Sampled Time Sampled ' Matriz Sample Type - Condition 002 •. 0711-56675-002 0:00 WW' Unknown 4+1.2 deg C Analyzed TestPerformedMethod Results Date. ' Time Qualifier Total Phosphonis EPA 365.4 •' <0.05 rng1L 12/6107 14:24 No. Sample ID Date Sampled Time Sampled ' Matrix Sample. Type Condition 003 0711-56675-003 0.00 WW Unknown 4 +1. 2 deg C ,. Analyzed Test Performed .. Method. Results. Date Time Qualifier, , - Total Phosphorus EPA 365.4 • <0.05 mglL 12/6107 ,14:24 No. Sample ID Date Sampled' - . Time Sampled Matrix Sample Type Condition 004 . 0711-56675.004 .0:00 • WW. Unknown 4 +172 deg C Analyzed . . Test Performed Method Results Date Time Qualifier Total Phosphorus EPA 365A 0.26. mg1L 1216107 14:24 No. Sample ID " Date Sampled ";, ` Time Sampled Matrix ' : Sample -Type Condition. 005 ` 0711-56875-005 f> 0:00 _' .- WW • ,: Unknown .: 4 +/. 2 deg C _ Analyzed-. Test Performed Method. Results - Date Time Qualifier Total Phosphorus' ", - ;: - EPA 36SA : , _ <0.05 mg1L:-' 12/6107 14:24 -14. 200'7 10::45Am Tritest faz: o No 8567 P. 29." s r a e2of7 Y•.r, ` r 6701gConference Dr1've A Y'{ ,-+5�y .k' s i -.r r S.. r ..-.- ^^ r i ryiA* . E" c ' .a,s f r3 Raleigh, NO 2760T,4 =Telephone := (91r9) 834984 3 y �NCIWWCerL #' 067 V Fax: (919)V4-6497 _. _ . NCIDW Cert: #: 37731 La•b0' fa#ory R-ep�ort Bay Tree, Lakes Work Order* 0711.01.614 . No. Sample ID cell '� # 1, Date; Sampled Time, Sampled Matrix Sample Type Condition 006 . 0711-56675-DOB . -. "� 0:00 WW Unknown 4 +/- 2 deg-C Analyzed Test -Performed....'' Method Results' Date Time Qualifier VOCs in GW by 6230D ' 62300 1215107 6:32 Benzene 6230D <0;5 ug/L 1215107 6:32 Bromobenzene 6230D <0.5 ug/L „ 1215107_ 6:32 Bromochloromethane 6230D <0.5-ugfL 12/5107 6:32 Bromodichloromethane 6230D <0.5 ug/L 1215107 6:32 Bromoform '6230D <0.5 ugfL 1215101 6 32 Carbonite'trachloride �6230D <0.5 ug/L 1215107 6:32 Chlorobenzene 6230D <0.5 ugfL, 1215107 6:32 Chloroethane. - 62300 <0.5 ugfL . ► 1215107 6:32 'Chloroform 6230D `<0.5 ug/L 1215107' 6:32 Chloromethans . ; - 8230D .. <0.5 ugfL 1215107 6:32 . 2-Chlorotoluene 6230D <0.5 ugfL 1214107 6:3Z , 4-Chlorotoluene . - 6230D <0.5 ug/L 12007 6:32. Dibromochloromethane 6230D . <0:5 ug1L 1215107 6:32 7,2-Dibromo-3-chloropropane - 62300 <0.5.ug/i 12/5107 6:32 1,2-Dibromoethane . 6230D, <0:5 ug/L 1215107, 6:32 Dibromomethane . -62306 - <0.5 ug/L 1216/07' 6:32 ' Dichlorodifluoromethane ; •_ 6230D <0.5 ug/L 1215107 6:32 . 1,1-Dichloroethane 6230D c0.5 ug/L 12l5107 6:32 " . 1,2-Dichloroethane ; 6230D �<0.5. ug/L .1215107 6:32 1,1-131chloroethene 62300 <0,5 ugfL . 1215107- 6:32 cis-1,2-Dlchloroethene. 6230D <0.5 ugfL 1215/07 6:32 • trans-1,2-Di4hlor6ethene 6230D <ax ugfL , 1215107 6:32 1,2-Dichloropropans ; 6236D <0.5 ug/L _ 1215/07 6:32 -1,3-Dichloropropane 6230D . <0.5 ugfL 1215107 6:32- - 2,2-Dichloropropane 6236 <0.5 ugfL 1215107 6:32 1,1-Dichloropropene, . 6230D <0.5 ug/L 1215107 6,32 'cis-1,3-Dichloropr6pene .6230D <0.5 ug/L 1215/07 6.32 trans-1,34D16hloropropene' . 623013 - <0.5 ugfL, 1215/07. 6:32, Ethylbenzene : 6230D .<0.5 ug/L 1215/07 6:32 kexachlorobutadiene 6230D <0.5 u91L A215I07 :, 6:32 lsopropylbenzene 6230D <0.5 ug/L 12W07 ' 6:32 4-Isopr6pyltoluene- . 6230D c0.5 ug/L 1215107 6:32 Methylene chlorld.a 1230D <0,5 ug/L 1215107 6:32 jVaphthafene 6230D <0 5 ug/L 1215107. 6:32 n-Propylbenzene ' 6230D <0.5 ugfL 1215107 6.32 Styrene' 6230D- <0.5 ugfL 1215/07 6:32 1.1,1;2-Tetrachloroethene : 623CD Q.5:ug/L 12/5/07.:.6:32. 1;1,2,2 Tetrachloroetfiane 6230D" c0.5 ugfL. ',` 12/5/07 532- Tetrachloroethenet 6230D , <0. 5 ug1L '.171510T .6:32' Toluene _ 6Z30D <0 6 ugfL ,� -1215107. 6:32 1,2,3 Trichlorobenzene" 62300 <0.5ug1L 1215/07 -"6:32 . �,2,4-Trlchl6r666zene`" " ` 6230D <0.5 ug/L 1215107 . 6:32 T 10:45AM` °ritest' faz o w . o. E5:67`'' 'P 3' 670:1 Conference Drivew 5 Page 3 of 7 # s '_� .. ¢ '-n t. 7 •rr .r?':. z, a y'--sv t-i=E, n 'jx y,.. r¢ Y;'Raleigh� NC127607�� fiT: ti 'a r �' �. { ` . r.. t, � �. Telephone (919)_8344984 t ' NCIWIN Cart. #c o6T Fax: ; (919)834-6497 • - : _Y NC/DW pert # 37731 R Labo•ra:#ory.Repo:rf Bay"'Tree Lakes Work Order #: - 0711-01514 „ No. Sample, ID Pell # 1- � Date Sampled ' Time Sampled _ Matrix-,~' Sample Type Condition 006 ` 0711,56675.006 0:00 WW Unknown : 4 +1- 2 deg C y Analyzed - Test Performed' Method' Results „„ Date Time - Qualifier 1,1,1 TrlchlorokK4n' e, 6230D .' . ` <0.5ugrL , '' 1215107 ,6:32 1;1.,2.Trichloroethano 6230D " <0.5ugIL. 12/5l07 '6:32, - Trichloroethene ,6230D' <0:5ug/L 1215107 6:32 Trichlorofluoromethane 62301) <O.S uglL 1215107 ,6:32: 12,3 Trichloropropane . '6230D <0.5 uglL 1215107 .6:32 1,2,4-Trlmethylbenzene .6230D " �O:S,ugIL 1215107 6:32 1,3,54rimethylbenzene- 6236D 4.5 uglL : 1215i67 6:32 Vinyl chloride:, 6230D 0.5 ug/L 12/5107 6:32 o-Xylene 6230D ' <0.5 uglL. 12/5107 0:32 m,p-Xylene 6230D V0.5 u91L _1215107. 6.32 1,2-Dichlorobanrsno ' 6230D <1 uglL °, ` 1215107 6:3254- " 1,3-131chlorobenzene, 6230D <1' uglL 12J5/07 6:32 1,44Dichlorobenzene 623013 e1 uglL° 12/5/07 ", 6:32 No., Sample ID Well #2 ;Date Sampled Time Sampled ,Matrix Sample Type Condition 007 . , 071:1-56675-007 0:00 WW . . Unknown 4 +/-'2 deg C . Analyzed" Test Performed Method -. Results Date Time - Qualifier VOCs In.GW by 6230D 6230D 1215107 6:32 Benz®no 6230D <0:5 uglL 12I5107 6;32, . Bromobenzene ' .' ,_ 623013. <0.5 ug/L 1215107 6:32' '13romochloromethane = . 6230D <0.5 ug/L 1215107 6:32,- 13romodichloromethane ` _ 6230D ' '<0:5 uglL - = . 1215107 6:32 Bromoforni 6230D ` zp.5 ug/L 1215107 6:32 carbon tetrachloride 6230D:_ . <0.5 ug/L 1215107 6:32 Chlorobenzene 62306 <0.5 ug/L - 1215107 6:32 . '-Chloroethane' 62301) <0 5 ug/L 1215107 6:32 Chloroform ' " 6230D <0.5 uglL" 1215107: 6:32 Chloromethane 6230D . <0,5 uglL 1215107 6:32 2 Chlorotoluene 6230D <0.5 uglL 1215/07 6:32 " 4=Chlorotoluene' 6230D' e0,5 ug/L 1215/07 6:32 Dibroniochloromethane 62301) <0.5 ug/L 12I5/07 , 6:32 1,20bromo-3-chloropropane 62300, <0.5_u9lL 1215107 6:32" 1,2-Dlbromoethane:.. 6230D' <0.5 ug►L . 1215107• 6-31 Dibromomethane 8230D <0:5 u014 1214107 %6:32 Dichlorodifluoromethane 6230D <0:5.ug1L ' 121,5107`. 6:32 .'1,7-Dicfiloroethene 6230D <: <0.5 uglL 7215/07 6:32 1.2 D�chloroethane 6230D <0.5 ug1L 1215/07„ 6:32 7,1-Dlchl oethenA 6230D f <0 5 uglL 12/5!07 6,32 cis 1.2 D�chloroathene f' 6230D cO.S uglL 1216I07 _6.32 trans 1.2-Dlchloroethena 6230D <0 5 ug/L :1215/07 6:32 ' 856.7 I P. 31 . Dec,1.4,-20,07 10,` 45 AM Tritest" -fax . 0`U�TST ;a re.epj hoine: Fak,:._ (91 S Bay. Tree Lakes' No.� 7-Sample ID 007 07,11-56875-007. Well 12, N NCIDW Cert. 73 L'a b 6,ra to ry R. e p o. H Work drd'er#':' 071,11-011614 Date Sampled Time Sampled Matrix 0:00 WW Test Performed Method Results Sample Type Unknown deg Analyzed rIftle, -ri e ger 1,2-Oichloropropah.e. 6230D <0.5 ug/L 1216107 6:32 1,3 -Djchl&o'prop;;ne 62300 <0.5 ug/L., 6:32 42-DIchloropropane 6230D <0.5 uqIL .12/510T 1215107 6:32 1.1-Dichloropropenii 6230D <0.5 ug/L 1215107 6:32 cis-11,3-Dichloropropeno, 6230D <0Z ugfL 1215107 6:32 trans-1,3-Dichlor,opropene- 6130D <0.5 ug/L UAW 6:32 Et_ ._ ylbenzene 6230D ug/L .1215107, 6:32 Hiaxachlorobutadjen a, 6230D, <0.6 ug/L 1215107 6:32 I� opropylbenzene'. 6230P 0.5 ug/L. 1215/07 6:32 4.1sop, ropylloluehe : .6230D 4045 ug/L 1215joi.. 6:32 Methylene chloride' 6230D <0.5 ug/L 1215107 6:32 Naphthalene 6230D <0.5 ug/L 11215107 6:32 n -Propylbenzen�'. 6230D 40.5 u9IL 12/5107 6:32 Styrehe 6230D <0.5 ug/L 1215107 6:32 j,%I,2-Tetrachloro&thahq 6230D 40-5 ug/L 1215107 6:32 1i1,2,2-Tetraichlaroethane 6230D <0.6 ug/L 1215107 6:32 Tetrach! Aiethene 6230D =503 ug/L _1215107 6:32 Toluand 6230D' <0.5 ug/L 12/5107, 6:32 1,23-Trichlorobenzene = .6230D <0.5 ug/L 12/5107 6:32 1,2,4-TrIchloroben,z9he 6230D <04 ugIL 1215107 6,32 -1,1,1-Trichloroothane 6230D- 40.5 ug/L 1215107 6.32 11,11,24fichloroethane 6230D <0.5 ug/L 1215107' 6:32 Tkchloroethene:; 6230D <0.5 ugIL 1215107 6:32 .Trichlorofludroenethane 6230D .<0.5,ugfL 1215107 6.32 62301) <0.5 ug/L 1215107 6:32, 1 -T .,2,4 firnethy1benzene 6230D <0.5 ug/L 12ISM7 6:32 1,35-Trilmethylbenzefie .62306. <oz ugiL 12f5107 6:32 Vinyl chloride 6230D <0.5 ug/L 12/5/07 6:32 o-Xylone 6230D' <0.5 ug/L 1215/07 6:32 .m,p7XYIene: "62.30D <0.5 ug/L 1215W -6:32 1,2-Dichicrobenzene, 6230D �I ug/L 6:32 i.36DichWbbenzene' <1 ug/L 1215107, -6:32 1,4-01chlorobenzie'ne <1 601L 12/5107 6:32 Sample ID Well 13- Date Sampled Time Sampled Matrix Sample Type Condition 008 .07111-56675-068 0:00 WW Unknown 4 +1- 2 dog C .Analyzed -Ana Test P erformedMethod"Time ' Results :-Da Date; Qualifier VOCs in VW by 6230D - 'a 6230D 12f5/07 6:32 - 623013' ug L 112rSIOT., 6:32.- irotobe 6230D <0.5 ug/L 1215107 6.32 J'Dec. 14.--2007: 10 45AM7`I r i`t`e`st` fax". ' o = -_ No 85,67 K: 32: ` l aT 05 z 1 h 6701=Conference Drove, Page 5 of 7 Ra I® K. NCB 27607 Telephone r(919) 834=498a N rt # OW (919) 834-6497 v NC ert #: 37731 .: 3 L-a..b.orat-ory Reporf Bay Tree Lakes Work Order #: 0111-01514 No.. Sample ID Well #3 Date Sampled Time Sampled Matrix Sample Type Condition 008 0711.56675-008 - 0:60 WW Unknown' 4 +1- 2 deg C Analyzed Test Performed Method Results Date . Time Qualifier Bromochloromethane 6236D <0.5 ug/L 1215107 6:32 _ Bromodlchloromethane 62300 <0.5 ug/L 1215/07 6:32 aromoform .62300 <0.5 ug/L 1215107,, 6:32 Carbon tetrachloWe 6230D <O.d ug/L . 1215107. 6:32 Chlorobenzene 6230D' <0.5 ug/L 12/5107 6:32 'Chloroethane 6230D <0;5 uglL 1215107 6:32 Chloroform 6230D ' <0:5 ug/L-' 1215107, 6:32 Chloromethane- 6236D <0.5 uglL 1215107 6:32 2-Chlorototuene 6230D ` <6.5 ug/L 1216107 6:32 4-Chlorotoluene 6230D <01 ug/L + 12/5107 6:32 - Dibromochloromethane 62300 <0.5 uglL . • 1215107 6:82 1,2-Dibromo-3-chioropropane. 6230D - <0.5-uglL • 12I5107 6:32 1,2-Dlbromoethane 6230D <0.5 ug1L 1215107 6:32 Dibromomethane 6230D- <0.5 ug1L' 12/5/07 ' 6:32 Dichlorodifluoromethane .62300. <6.5.ugIL ' 1215107 6:32 1,1-Dichl6roethene d230D <0.5 ug/L - 1215107 6:32 1.2-Dichloroethane 6230D <0,5 ug/L 1215107 6:32 1,1-Dichloroethene 6230D <0.5 ug/L. 1215107 6:32 cis-1,2-Dichloroethene '62300 <0.5 ug/L 1215107 6:32 trans-1,2-Dichloroethene 6230D <0.5 ug/L 1215107 :6:32 1,2-Dichicropropane , 6230D ' <0.5 ug/L 1215107 6:32 1,3-Dichloropropane 6230D <0.5 ug/L, 1215107 6:32 2,2-Dichloropropane 62300 <0.5 ug/L _ 12/5/07 6:32 '1,1-Dichloropropene 6230D ; <0.5 ug/L 1215107 6:32 cls-4,3-Dichloropropene 623013 . <0.5uglL 1215/07 6:32 trans-1,3-Dichloropropene 6230D <0.5 uglL 1215107 6:32 Ethylbenzens " 6230D <0.5 ug/L 1215107, 6:32 -- 14exachlorobutadiene 62300 <0.6,ug/L .1215107 - 6:32 lsopropylbenzone 6230D <0:5 ug1L 1215107 6:32 '44sopropyltolu6ne 6230D <0.5 uglL 1215107 6:32 Methylene chlorlde , 6230D <0,5 ug/L 1215167 6:3.2 Naphthalene.. 6230D <0.5 ug/L 12/5/07 6:32 n-Propylbenzene 6230D -0.5 ug/L 1215107 6:32 Styrene ' 6230D . <0,5 uglL 12/5107 . 6:32 1,1,1,2 Tetrachloroethane 6230D <0.5'ug/L 1215107 6:32 - 1,1;2,24e"chloroethane 62301) <0,5 uglL . ,' 1215107 6:32 Tetrachloroethene ' } 62300 <0.5"uglL 12/5/07 6:32 _ Toluene . _ 62300' <0.5 ug/L 1215107, 1:32 -1,2,3-Trichlorobeimne 6230D " <0.5 ug/L ; 12/5107-_ ' 6:32 1,2,4 Trichlorobenzene . 6230D_ <0.5,ug/L 9215J07: 6:32 TrlcttloroetFiane 6230D " <0.5 ug/L 1215/07 -- 6:3Z. 1,1,2 Tnctiloroethane , 6230D. 1215107: 6:32 . - = Trlchloroethane,� 5 62300 c0.5 ug/L" 1215/07 6.32 _' _ Trlchlorofluoromethane 6230D <06 use/L 1215107 ' 6:32 +. `200T 10.:45AM=` 'TrJt i "fax o NO'.' P;' 33 - } aT�ST � .. 6701 Conference Page 6 1 iI Y 'r • L 4-, .yA {ttl Raleigh; NC r27607 Telephone (919) 834-4984NClvvvuCentc os7 . Fax:(919) 8 34-6497 . NC/Dw cart. : 37731:. Laborafor.y „Report Bay Tree Lakes Work.Order #: 0711-01614 No.'Sample-ID Well. #3 `. Date Sampled Time Sampled , Matrix = Sample Type. Condition 008 071146675-008' ' . 0:00 WWI Unknown 4 +/- 2 deg C Analyzed Test Performed Method .Results : Date Time Qualifier 1,2,3-Trichloropr6pane 6230D '<0.5 uglL IW5107 -6:32 1,2,4-Trimethylbenzene 62300 . <0.5 ug/L 1215107 6:32 1,3,5-Trimethylbenzene .'6230D <0.5, ug/L 12/5L07 _6:32 Vinyl chloride 6230D <0.5 ug/L 1215/07 6:32 o Xylene 62301) <0.5' ug/L 1215107 6:32 m.p Xylene 6230D '<0.5 ug1L 1215107 6:32 .1,2-Dichlorobenzene 6230D . <1 uglL 1215107 6,32 1,3-Dichlorobenzene 6230D. <7 ug/L. 12/5/07 6:32 1,4-Dichlorobenzene : 6230D <1 u'91L 1215107 6:32 . 0. Noy Sample ID Well 15 :Date Sampled Time Sampled Matrix _ Sample Type Condition . 009 0711-56676-009, 0:00 WW Unknown 4_t/. 2 deg C Analyzed Test Performed Method Results Date Time Qualifier VOCs in. GW by 6230D 6230D 121W07 6:32 Benzene 6230D <04 ug►L 1215107 6:32 Bromobanzeno ` 6230D <0:5 ug/L 1215107, -6:32 Bromuchloromethane 6230D <0.6 ug/L ' 12/5/07 - 6:32 Bromodlchloro`-methane 6230D <0.5 ug/L.12/5/07 6:32 Bromoform, 6230D <0.5 ug/L 1215107 6:32 Carbon tetrachloride - 6230D c0.5 uglL 1215/07 ", 6:32 Qhlorobenzene 6230D <0.5 ug/L 12/5/07 6:32 Chtoroethane 6230D <0.6 uglL 1215107 : 6:32 " Chloroform 6230D <0.5 ug►L 1215107 6:32' Chloro methane .6230D <0.5 ug/L 12/5107 6.32 , 2-Chlorotoluerie 6230D <0.5 ug/L 1215107 6:32 4-Chlorotaluene <0.5 uglL' 1216/07 6:32 Dibromochlorome#iane _6230D 6230D <0.5 ug/L 1215/07 6:32 �1,2-Dibromo-3-chloropropane 6230D <0.5 uglL 12/5107 6:32 1,2=Dlbromoethane 6230D <0.5 ug/L 12/5107 6:32 Dibromomethane 62300 <0.5 uglL: 1215/07 6:32 Dichlorodifluoromethane 6230D <0.5 ugIL 1215107 6:32 1,1-01chlcroethnne 6230D COX u41L 12/5/07.: 6:32 1,2-Dichloroethane 62300 <05 uglL 12/5107: 6:32 1,14Dlchloroethene 623OD <0.5 ug/L 12/5/07 6:32 cls-1,2-1011chloroethene'' - 6230D .40:5 ug/L 12/5107, 6:32 - imns-a 2-Dichl6roethene . ' _ 62300. : , ; <0.5, ug/L - 12/5107, 6,32 ` 1,2-Dichloropropane 6230D <OA uglL _ 1216/07 : 6:32 �1,3 D1ch16�ropropane 6230D <0.5 ug1L = " ' ' 1215107, 6c32 - - Q,24, ichloropropane 6230D_ ' - <0.5 ug►L ` 1215/07 _'6:32: '1,7-01chloropropene ' f 6230D = < <0.5 uglL 1215107 6:32 Dec. 14:- 2-001" 10` 46AM- Tr'i'tesr `fix o' .: - No 8561 K 34 F r 6701 Conference�Drive f f �� PageTc�f 7- 4 t z , L Raleigh NC 276Q7e Telephone (919) 834-4984 ; ° r t ' NCIWW�Cert 067 ' Fax: (919) 834-�6497 ek `NcIDW Cert_. #: 37731 Labo'rato'-ry Rep.ort Bay Tree Lakes Work Order#P 67111.01514 No_� . Sample ID Well 15 Date Sampled Time Sampled Matrix Sample Type 'Condition 008 0711-56675-009 0:00 ,VWII : Unknown. 4 +/- 2 deg C Analyzed Test Performed Method " Results Date 'Time Qualifier cis-1.3-Dichloropropene 6230D <0:5 ug/L `' S215/O7-• 6:32 trans-1,3�0Ichloropropona '6230D <0.5 uglL 1215107 6:32 Ethylbenzene 6230D <0.5 ug/L 121510T 6:32 Hexachlorobutadlene 6230D <0.5 ugIL - 12/5/07 6:32 lsopropyl6enzene 6230D <0:5 uglL 1215/07 6:32 4-Isopropyltoluene 6230D <0.5 ug/L .1215107 6:32 Methylene chloride 6230D _ <0;5 u9IL ''.' 12/5/07 6:32 ' Naphthalene 6230D <0.5 091E 1215107' 6:32 n-Propyibenzene 6230D - <0.5 ug/L _ 1215107 ' 6:32 Styrene . 6230D <0:5 ug1L r: 1215/07- 6:32 1,1,1,2 Tetrachloroethane ' 6230D_ .4 4.5 uglL 1215/07 6:32 1.1.2.2-Tetrachloroethans 6230D <0.5 uglL -1215107 6.32 Tetrachloroethone; 6230D <0.5 ug/L - 12/5- . 6:32 Toluene 6230D <05 uglL 12J5/07 6:32 1,2,3 Trichlorobenzene 6230D <0.5 ug1L 12/5/07 6:39 1,2,4-Trichlorobenzone 6230D <0.5 ug/L 1215107 6:32 1,1,1-Tricyloroethane 6230D :;.<O.S 091E 12/5/07� 6:32 1,1,2-Trichloroethane . 6230D " <0.5 uglL 1215107, 6:32 Trlchloroethene -623013 - <0.5 uglL 1215107 6:32 TrichlorcNoromethane 6230D '<0.5 ug/L 1215/07 -6:32 11,2,3-Trlchloropropane ' 8230D.- <O.S 091E 12/5/07 6:32 1,2,4=Trimethylbenzene 6230D <0.5 091E 1215107 6:32 `1,3,5-Trimethylbenzene 6230D <0.5 ug/L ' 1215107 6:32 Vinyl chloride 6230D . ' <0:5 uglL 1215107 6:32 o-Xyleno 6230D <0:5 ug/L 12/5107 6:32 •- .m.p Xylene 6230D . <0.5 ug/L 1215/07 6:32 1,2-Dichlorobenzene •6230D <1.091E 1vsw 6:32 1,3-Dichlorobenzene 6230D <1091E 1215/07, 6:32 IA-Dichlorobenzene 6230D . <1 ug/L 1215107 6:32 M� ' ;& Please Print Clearly or Type .Facility Game: ;r Ba4 Ti Permit Name (If`di f f erent): :... Ate.,_:--. 33 W.' l E;4lls 28466County $laden �y ( Ids) (ZIP) Stephen Jones Telephone #9 20-588-4432 Con act Person: P 4 Well Location/ Site Name: Well # 1 No. of Wells to be Sampled: rom um Well Identification Number (from Permit): Well I i For Groundwater Treatment Systems Weil Depth: ,Zg&D ft. Well Diameter: 2 in. Check One; Screened Interval: _____—ft. to It. . . ❑ Influent (98) Depth to Water Level: ___.Z2ft. below measuring point. O Effluent (99) Measuring Point is—ft. above land surface. Gallons of water pumped/balled before sampling: 04 Field analysis: pH.-._._ 4�'.�� , Specific Conductance uMhos Temp. .—..1703 OC, Odor Appearance PERMIT #: EXPIRATION DATE: - Non -Discharge, W00018708 UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Rernedlation: Infillral - a ✓ Spray Field Remediallon: 140=2 `" �..� Rotary Distributor Land Appilcallon �o©f Sludge Other: HAll It q1 2 n P NOTE: - Values should reflect dissolved and colloidal concentrations. Date sample collected: llzo.f Date rsample ,Nozed: 27 Laboratory Name: Ua°° Certificatlon.No: 22, 75 PARAMETEg (Samples for metals were collected unfiltered. YES NO and field acidified COD mg/I Nitrite (NO2) as N mgll Coliform: MF Fecal < / Coliform: MF Total /100ml /i 00ml Nitrate (NOs) as N Phosphorus: Total as P mg/l cw02 mg/l (Not®: Use MPN method for highly turbid samples) Orthophosphate mg/I mg/I Dissolved Solids: Total mgll Al - Aluminum pH (when analyzed) units- Ba - Barium mg/I �./� TOC iry0�0 mg/l Ca - Calcium mg/I Chloride hs, mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and.0iis mg/I Cu - Copper mg/I Phenol mg/1 Fe - Iron, mg/I Sulfate - mg/l Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia •<d'?D mg/l Mg - Magnesium mg/l TKN as td mg/I Mn - Manganese mg/l - YES ' NO) Ni - Nickel mg/ Pb - Leap mg/ Zn - Zinc mg/ Ammonia Nitrogen mg/ Other (Specify Compounds and Concentration Unit. ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach tab report.) Report Attached? Yes (1) No ._. VOC method # method,#/_____.__ method # Permlttee (or Aulhorked Agenl) Name and Tiller Please print or type GWI-59 Rev.:4198 na ura qI Perm Iloe (or Auihorirrc genli 4 & ouwrvn i rvmm vlV r c&6vry nmr-cm uNLY Please Print Clearly or Type .Facility Name: Bay Tree Lakes Permit NaMS (if d33 W.t)Ba Ridge Road Facility Address: Harrel.ls W1 28466County - Biaden Contact Person: Stephen Jones Telephone #910-588 4432 Well Location/ Site Name: Well #2 No. of Wells to be Sampled,4 rom arm Well Identification Number (froin Permit):' Well 12 For Groundwater Treatment Systems Well Depth:ft. Well Diameter: 2 in. Check One: Screened Interval: ft. to ft. ❑ Influent (98) Depth to Water Level:ft. below measuring point. ❑ Effluent (99) Measuring Point is ft. above land surface. Gallons of water pumpedlbailed before sampling: Azey Field analysis: pH— 3 , Specific Conductance - uMbos Temp. °C, Odor I Appearance PERMIT M EXPIRATION DATE: !j'-o Non:Discharge W00018708 UlC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Rerhedlatlon: Infiltration Gallery' _Spray Field Remediatton: Rotary Distributor Land Applica���O Other.�I1 I DOTE: Values should reflect dissolved and 04-AY 0 9 2007 colloidal concentrations. Date sample collected:' Date sample analyzed:. Laboratory' Name: Qacni�=ies, 0�d � ' Certification No. 22, 75 PARAMETER$ (Samples for metals were collected unfiltered YES NO and field acidified COD mgA Nitrite (NO2) as N mgA Coliform: MF Fecal < I /100ml Nitrate (NO3) as N <0-10 mgA Coliform: MF Total /100ml Phosphorus: Total as P <0 62 mg/I (Note: llse MPN method for highly turbid samples) Orthophosphate mg/l Dissolved Solids: Total J-9 mgA At - Aluminum _ mg/l pH (when analyzed) units Ba - Barium mg/i TOO Y-44 mg/i Ca - Calcium mg/I Chloride Z"o mg/l Cd - Cadmium mg/1 Arsenic mg/I Chromium: Total mg/I Grease and.0ils mgA Cu - Copper mg/I Phenol mg/I Fe - Iron mg/I Sulfate mg/l Hg - Mercury mg/1 Specific Conductance uMhos K - Potassium mg/I Total Ammonia <62(? mgA Mg'- Magnesium mg/I TKN as td - mg/I Mn - Manganese mg/l - YES ' NO) N1- Nickel mg/I Pb - Lead mg/i Zn - Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and. Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method '#. Attach lab report.) Report Attach.edT Yes (1) No (0) VOC method # method. methol # s Permlttee (or Authorized Agont) Name and 7111e -Please printor type J 8l0 ©Vh59 Rev. A/98 nature o • erm flee tar ut Nrrc gent) A, Facility Name: pay free LaKeu permit Name (if, dgferen))II„� u Boa R��a i Stephen .tones - - Telepnone -- - - Conttaot Person: We11 #3 No. of Wells to be Sampled: 4 erm Well Location/ site Name: r°m Well Identification rvumoer tirom 5„, ...„_.._.._._...__.. -- . Well Depth: ' Z0ft• Well Diameter:2 in. Check One: Screened Interval: ft. to _�. ft. . 0 Influent (98) Depth to Water Level: B4O ft. below measuring point. [I Effluent (99) Measuring Point is ft- above land surface. Gallons of water pumpedi al ad before sampling: /Z 0 S ecifio Conductance uMhos Field analysis: •pH MI ec. Ya Odor Appearance - Values should reflect dissolved and colloidal concentrations. • Date sample collected: T,d° Laboratory' Name: Vasa 'A"" __ ' Cerllticatton.No: 22, 75 EARAMMBA (Samples for metals were collected -unfiltered _._.YES _____NO and field acidified mg/l Nitrite (NO2) as N mg/I COD Coliform: MF Fecal �' I / 1OOml Nitrate (NO3) as N Phosphorus: Total as P - o�zk42!g/l m m Coliform: MF Total /100m1 Orthophosphate mgll ll (Note: Use MPN method for highly turbid Samples) Dissolved Solids: Total q mg/i Al - Aluminum mgll mg/I pH (when analyzed) 3 015`r-- units mg/ I Ba - Barium Ca - Calcium mg/I TOO Chloride 7, L mg/I mg/i Cd - Cadmium Chromium: Total mg/1 mg/l Arsenic Grease and.0ils mg/l Cu - Copper mg/1 mg/l Phenol mg/I mg/I Fe - Iron Hg - Mercury _ - melt Sulfate Specific Conductance hos �" K - Potassium Mg =Magnesium mg/l melt Total Ammonia ____—�` TKN as N mgn mg/I Mn - Manganese mg/i YES • . NU) , NI - Nickel mg/l Pb - Lead mg/1 Zn - Zinc mg/l .Ammonia Nitrogen mg/1 Other (specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.). Report AttachedT Yes (1) No. (0 V0�_ : melbod # method., meth+ # r permittee (or Authorized Agont) Name and Title -please t ar type GWI-59 Rev.: 4/98 a, ouorvu r r%jmivr vry r er-rwvv r^rcrs ut%. r �ec;iLITY i FORMATION Please Print Clearly or Type .Facility 14ame: Bay Tree Lakes Permit Name (if diferenl): Facility Address: 3 W. Ba Ridge Road flarrells t 28466County Bladen Contaco t Persn: Stephen Jones tZIP) Telephone #910-588-4432 - Well Location/ Site Name: Well #5 No. of Wells to be Sampled: 4 rom arm Well Identification Number (from Permit): Well iF- For Groundwater Treatment Systems Well Depth: , ft. Well Dlameter: 2 in, Check One: Screened Interval: ft. to It. . ❑ Influent (98) Depth to Water Level: Z ft. below measuring point, ❑ Effluent (99) Measurlrig Point Is ft. above land surface. Gallons of water pumped/bailed before sampling: X73 Field analysis: -pH A..o r Specific Conductance uMhos Temp, /bd °C, Odor Appearance PERMIT #: - EXPIRATION DATE: _ S•Zy94— Non=Discharge,_WQ0018708 UIC NPDES JyPE OF PERMITTED OPERATION BEING MONIOf it DR ECF— 9l-lx Lagoon Reihediatlon: tnliltratl a $�9��i Spray Field Remedfallon: Rotary Distributor Land Application of SludgePlAy 0 9, 20[ Other: NOTE: Values should reflect dissolved and colloidal concentrations. Date sample collected: -T.�'�0 67 Date sample analyzed:' Laboratory Name: Vaoa labarayries, Offmd Laboratory Certification.No; 22, 75 PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified COD mg/I Nitrite (NO2) as N mgll Coliform: MF Fecal < 1_/100ml Nitrate (NO3) as N Ate mg/l Coliform: MF Total /100ml Phosphorus: Total' as P b mg/l (Note: Use MPN method for highly turbld samples) Dissolved Solids: Total , 00 mg/l Orthophosphate Al - Aluminum mg/I mg/i pH (when analyzed) units Ba - Barium mg/1 TOG 7'45 mgli Ca - Calcium mgll Chloride ls.Z mg/I Cd - Cadmium mg/1 Arsenic mg/I Chromium: Total mg/l. Grease and•Oils mg/I Cu - Copper mg/1 Phenol mg/I Fe - Iron mg/l Sulfate mg/1 Hg - Mercury mg/1 Specific Conductance Potassium mg/i Z, lol�Mmos Total Ammonia g M- g = Magnesium mg/I TKN as N mg/I Mn - Manganese mg/i YES —NO). Ni - Nickel mg/I Pb - Lead .T mg/1 Zn - Zinc mg/l Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration knits) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method#. Attach lab report.) Report Attached?' Yes(1) No ____..(0) VOC : metbod # method m Permittee (or Authorized Agont) Name and 7RIe - Please print or type f3Vir-59 R®Y: d19tf • ' , nalur8 0 , erm i ae (or Aui r md• gnnq • ( ate) v. -1-6__1 - W QO-O/87O�i - GPS Field Sheet Project/ Location Date Time GPS File No. Field Latitude Field ' Longitude 'Corrected Latitude Corrected Longitude Comments TArZPeEe. T&V MW - (p dZ I0: Ali. $1 ZO y/5.4. � ,� 3y 83-*3� 78 8305(0 I 4 �Siiv j. PZe,c qn T H 7W I1� a I0.4 ,cM- SJ�O �/5t3 3 y/ •78z93y 03 78. $3/ 37� q o.. . L T`H 77AJ mw.- ;L �� ro:� $ IV. 178 .$191; '78 83yt 87 �� N� 74 � �� Qom, SJ.� 0 N� 314, 779 ash 78. 8 , 93J•'�PM- T P 7W �M �/�2O Y I �O 35h 78.�� G ! oA j 78. 61 s.7 Sd97 1. _ ,. - _ -- _ - — 2.3_ 3,qRr � � �- 3 - S/�o y/78 � , `' �„-�L,� ® � `' `• .z•S7 , S0�®`� �:� � ® - .;.1�91 501 78. yZ 31 �� `' r�►r.� 12, .. L• t:0/ S/�dL/lg4- 3y' 6900 8.ga/6q \\ \\ O F A �� '�% 5/�Q / �- ® 37� ,,0 / o 8 �1 / i22�'2 \ l ��- ,. � 2043F q ,: t: ro 5120y, 8 C_ — 4 341, G9o407 9108 !a. gZZJ43 Zloy 0� �• l•�� ,. '' - i �, r• 1:12- Stud 351. (OYo 5'0 / 78 W ��� GROUNDWATER SECTION Page 1 of I Report to: FRO CHAIN OF CUSTODY (COC) RECORD i (check one): [®j CENTRAL j❑ 1 ARO [❑ 1 WaRO NC DENR/DWQ LABORATORY For Investigation of: Lake Creek-- Bay Tree Lake Incident No.WQ 0018708 Sample collector (print name) i . and GW-54 forms completed by: Bill Todd Sample collector's signature: Field storage conditions and location (when applicable): NUMBER Lab Use Only I DATE ; SAMPLED TIME SAMPLED OF CONTAINERS LAB NO. SAMPLE ID QUAD. NO. LOCATION Bay Tree Lake Y 5 IvIW-1 Bay Tree Lake `ai6A� 5 MW-2 Bay Tree Lake MW-3 Bay Tree Lake 5 MW-5 I. Time I DateTTime yceived by (signature):, Date Relin uished by (s' nature): Dateeceived by (signature): Date Time Relinquished by (signature): by (signature):, ; I, Date Time Relinquished by (signature):DateReceived I I Method of Shipment (check one): State Courier® Hand -delivered[] Federal Express[] UPS[] Other: Sealed by: Broken by: Security Type and Conditions: INTRALABORATORY LAB NUMBERS FROM CHAIN THROUGH OF CUSTODY NUMBER BOTTLES - Lab use vni ANALYSES REQUESTED RELINQUISHED BY: RECEIVED gY DATE TIME I i� �I. I 1' port to: FRO GROUNDWATER SECTION CHAIN OF CUSTODY (COC) RECORD NC DENRIDWQ LABORATORY (check one): I® I CENTRAL I❑ I ARO I❑ I WaRO Page 1 of 1 For Investigation of: Lake Creek— Bay Tree Lake Incident No.W 0018708 JUL Sample collector (print name) �� and GW-54 forms completed by: Bill Todd Sample collector's signature: t R-- FAYR - LE REGIONAL OFFICE Field storage conditions and location (when applicable): - Lab Use Only LAB NO. SAMPLE ID QUAD. NO. LOCATION j DATE, SAMPLED TIME SAMPLED NUMBER OF CONTAINERS �C(2 ll MW-1 Bay Tree Lake —lG-o? , R D,�n 5 j(;j4 99 �� 11 MW-2 Bay Tree Lake ! ? 1(,11116 i9 5 MW-3 Bay Tree Lake l �C 5 . MW-5 Bay Tree Lake _ ` 5 I f ' I f 1 Relinquished by (s' nature): Date Time M We by (signatur to Time Relinquished by (signature): Date Time Rec ived by (signature): 1 Date Time, Relinquished by (signature): Date Time Received by (signature): Date Time Method of Shipment (check one): State Courier® Hand -delivered❑ Federal Express[] UPSO, Other: Security Type and Conditions: Sealed by: P � en by: INTRALABORATORY CHAIN OF CUSTODY - Lab Use Onlv LAB NUMBERS FROM THROUGH . ANALYSESA • • • ®®'I ® MEMBER Pagel of'1 Microbac Laboratories, Inc. FAYETTEVILLE DIVISION INVOICE 2592 HOPE MILLS ROAD FAYETTEVILLE. NC 28306 NO. 53410 (910) 864-1920 FAX (910) 864-8774 R. W. SANDERS, SR. - V.P. & MANAGING DIRECTOR http://www.microbac.corh E-Maii'l: rsanders@microbac.com NC DENW - DWQ (Aquifer Prot) Mr. Art Barnhardt . 225 Green Street, #714 . Fayetteville, NC 28301 Sampling done on 071161107, Sample received at lab or': 07176107 LAS REPORT NO.- CLIENT ACCOUNT NO ' TERMS : `DATE I CLIENT PURCHASE ORDER NO. 0707-00619 N022 NET 30 DAYS ' 07/31/07 Description ;._ '. ' Rate i Date. Quantity ` :Extended COLIFORM, FECAL $27.00 I 4 $ 108.00 i Y ki.: y Total Amount $ 108.00 F a� z �� 1$0.00 Prepaid Amount CHEMISTRY MICROBIOLOGY • FOOD SAFETY CONSUMER PRODUCTS : Amount . WATER . AIR WASTES • FOOD PHARMACEUTICALS NUTRACEUTICALS Due . $ 108.00 ``LAB REPORT`NO CLIENT ACCOUNT NO" TERMS DATE Invoice' Number 0707-00619 N022 NET 30 DAYS 07/31/07 53410 M/W Samples - Lake Creek - Bay Tree Lake Please include this Invoice Stub with all remittances • CHEMISTRY MICROBIOLOGY • FOOD SAFETY • CONSUMER PRODUCTS Amourit° 108.00 WATER - AIR WASTES • FOOD • PHARMACEUTICALS` NUTRACEUTICALS Due ®. Microbac: Laboratories, Inc. Page 1 of 1 FAYETTEVILLE DIVISION 2592 HOPE MILLS ROAD STATE CERT ID. FAYETTEVILLE, NC 28306 NC #11 (910) 864-1920 FAX (910) 86428774 NC437714 R. W. SANDERS, VICE PRESIDENT USDA #3787 http://www.tnicrobac.cotn E=Mail: rsanders@microbac.com CHEMISTRY MICROBIOLOGY • FOOD SAFETY • CONSUMER PRODUCTS WATER • AIR WASTES • FOOD • PHARMACEUTICALS • NUTRACEUTICALS. NC DENW - DWQ (Aquifer Prot) Mr. Todd 225 Green Street, #714 Fayetteville, NC 28301 Permit No. Sampler: Todd CERTIFICATE OF ANALYSIS Date Reported: Date Received: Subject: M/W Samples - Lake Creek _.Bay Tree Lake SMP Test Method COLIFORM, FECAL COLIFORM, FECAL SM18 9222D SM18 9222D Result <1 cfu%100 ml <1 cfu/100 ml Order Number. Invoice No.: Customer #: Sample Date: Sample Time: I , I 7/31 /2007 7/16/2007 0707-00619 53410 N022 7/16/2007 0:00 Date , . Time Tech 7/16/2007 15:07 f 7/16/2007 15:07 MAI MAI Tr'z �27 5 '' � ,- COLIFORM, FECAL SM18 9222D <2 cfu/100 ml 7/16/2007 15:07 MAI COLIFORM, FECAL SM18 9222D <2 cfu/100 mi." 7/16/2007 15:07 MAI i 1 RESPECTFULLY SUBMITTED: MICROBAC LABORATORIES, INC. Thank you for your business. We invite your feedback on our level of service to you. Please contact the Laboratory Director, Ron Sanders at 910-864-1920 , Robert Morgan, COO, at rmorgan@microbac.com or Trevor Boyce, CEO, at tboyce@microbac.com with any comments or suggestions. I I LAB CODES -NID = None Detected NIF = None Found < =.Less than > = Greater than Est. = Estimated The data and other information contained on this, and other accom an in documents, represent only the sam le s analyzed and is rendered u MEMBER P Y 9 P Y P �) Y upon the condition that it is not to be reproduced wholly or in part for advertising or other purposes without written approval from the laboratory. - USDA-EPA-NIOSH Testing Food Sanitation Consulting Chemical and Microbiological Analyses and Research W9 DWO LaboratorySection Wesufts Sample ID: AB19430 Loc. Descr.: LAKE CREEK - BAY TRACE LAKE • PO Number# 7G0582 Location ID: WQ0018708 VisitlD County: BLADEN - `adF W AT�QG Collect Date: 07/1612007 River Basin Report To FROAP q Collect Time:: 12:13 _ r Region: FRO � a e� _ ✓ ; 'I Date Received: 67/17/2007 ' Collector: B TODD E Nil r08:20 Time Received: Sample Matrix: GROUNDWATER AUGO 7 2W7 1 MONITORING WELL F1 /I Late es rte is MMA Loc. Type: `—[\'1J Sample Depth Date Reported: 08/02/2007 DENR—FAYETTEVILLEREGIONALCIFFICE Emergency Yes/No COC Yes/No YES Sample Qualifiers and Comments Routine Qualifiers For a,more detailed description of these qualifier codes refer to www.dwglab.org under Staff Access A-Value'reported is the average of two or more determinations N3-Estimated concentration is < PQL and >MDL B1-Countable membranes with <20 colonies; Estimated NE -No established - ---- -- � ---- --� -- - B2- Counts from all'filfers were zero. P-Elevated PQL due to matrix interference and/or sample dilution 133- Countable membranes with more than 60 or 80 colonies; Estimated - — - - Q1-Holding time exceeded prior to receipt at lab. B4-Filters have counts of both >60 or 80 and < 20; Estimated Q2- Holding time exceeded fallowing receipt by lab 135-Too many colonies were present; too numerous to count (TNTC) PQL- Practical Quantitation Limit -subject to change due to instrument sensitivity J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated U-Samples analyzed for this compound but not detected J3-The sample matrix interfered with the ability to make any accurate determination; Estimated X1-Sample not analyzed for this.compound J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated - N1-The component has been tentatively identified based on mass spectral library search and has an estimated value LAB Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 1 of 2 NC 1n2VQ La6oxatory Section 1�esuCts Sample ID AB19430 07/16/2007 Ls tyti0 ID: W00018708 Collect Date: �. °Loc. Descr.: LAKE CREEK - BAY TRACE LAKE C Collect Time::, 12:13 i�\, Visit ID CAS # Analyte Name PQL Result Qualttier units Anatysuuate Approvea toy ►uate Method Reference 7/17107 7/17/07 MIC TOC In liquid 2.0 7.0 mg/L ADEXTER CGREEN Method Reference APHA5310B-20th 7/26/07 8/1107 WET Total Dissolved Solids In liquid 12 62 mg/L AWILLIAMS CGREEN Method Reference APHA254OC-18TH 7/19/07 7/27/07 Chloride 1.0 8.7 mg/L MIBRAHIM MOVERMAN Method Reference EPA 300.0 .7/17/07 7/20/07 Fluoride 0.4 0.4 U mg/L MIBRAHIM MOVERMAN Method Reference EPA 300.0 7/17/07 7/20/07 Ion Chromatography TITLE mg/L MIBRAHIM MOVERMAN Method Reference EPA.300.0 7/17/07 7/20/07 . Sulfate 2.0 4.6 mg/L MIBRAHIM MOVERMAN Method Reference EPA300.0 7117107 7/20107 NUT NH3 as N In liquid 0.02 2.8 mg/L as N MAJAYI CGREEN Method Reference LaclO-107-06-1-J 7/191,07 7/23/07 NO2+NO3 as N In liquid 0.02 0.02 U mg/L as N MAJAYI CGREEN Method Reference LaC10-107-04-1-c 7/19/07 7/25/07 Nitrate as N In liquid 0.02 0.02 U mg/L as N MOVERMAN CGREEN Method Reference Lachatl07-04-1-c, 7/23/07 7/23/07 Nitrite as N In liquid 0.01 0.01 U mg/L as N GBELK CGREEN Method Reference Lachatl07-04-1-c 7/18/07 7/23/07 Laboratory Section>> 1623 Mail,Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 2 of 2 GROUNDWATER FIELD/LAB FORM Location code WQ 0018 County_Bladen, Quad No Serial No. Lat. Long. North Carolina Department of Environment and Natural Resources DIVISION OF WATER QUALITY -GROUNDWATER SECTION SAMPLE TYPE SAMPLE PRIORITY G Z � Water ZI Routine Lab Numbermtq r ❑ Soil ❑ Emergency Date Recei ed d ( Time314 ❑ Other Redd By: rom:Bus ours r, and Del., IL ® Chain of Custody Other: Report To: AR CFFed. MRO, RRO, WaRO, WiRO, Data Entry By: Ck: WSRO, Kinston Trust, Central Off., Other: Date Reported: Shipped by: Bus, oune , Hand Del., Other: Purpo Collector(s):_BillTodd Date �T lr' �T�me eZ ' 3 B seline, Complaint, ompliance (LUST, Pesticide Study; Federal Trust, Other: FIELD ANALYSES Owner �4.�Ce Cl�c'_c� iC r 04q ��� e -� Aid pH 400 44 i Spec. Cond.94 at 25°C Temp.lo PT. °C Odor /'llzO 'C'_ Annearance A4 a"-8 Field Analysis By: _BillTodd LABORATORY ANALYSES BOD 310 mg/L COD High 340 mg/L COD Low 335 mg/L Coliform: MF Fecal 31616 /loom[ Coliform: MF Total 31504 /100ml X TOC 680 mg/L Turbidity 76 NTU Residue, Suspended 530 mg/L pH 403 units Alkalinity to pH 4.5 410- --- mg/L Alkalinity to pH 8.3 415_ mg/L Carbonate 445 mg/L Bicarbonate 440 mg/L Carbon dioxide 405 mg/L X Chloride 940 mg/L Chromium: Hex 1032 ug/L Color: True 80 CU Cyanide 720 mg/L Lab Location or Site Description of samplin oint E ! I e_s d / Sampling Method Ai j a Sample Interval Remarks um°. bailer. etc.) (Pumping time, air.temp., etc.) X Diss. Solids 70300 mg/L Fluoride 951 mg/L Hardness: Total 900 mg/L Hardness (non-carb) 902 mg/L Phenols 32730 ug/1 Specific Cond. 95 uMhos/cm X Sulfate 945 mg/L Sulfide 745 mg/L Oil and Grease mg/L X NH3 as N 610 mg/L TKN as N 625 mg/L X NO2 + NO3 as N 630 mg/L P:.Total as P 665 mg/L X Nitrate (NO3 as N) 620 mg/L X Nitrite (NO2 as N) 615 mg/L GW-54 REV. 7/03 For Dissolved Analysis -submit filtered sample and write "DIS" in block. Ag-Silver 46566 u /L AI -Aluminum 46557 u /L As -Arsenic 46551 u /L Ba-Barium 46558 u /L Ca -Calcium 46552 m /L Cd-Cadmium 46559 u /L Cr-Chromium 46559 u /L Cu-Copper46562 u /L Fe -Iron 46563 u /L Hg-Mercury 71900 u /L K-Potassium 46555 m /L Mg-Magnesium.46554-- - --- m /L- Mn-Manganese 46565 u /L Na-Sodium 46556 m /L Ni-Nickel u /L Pb-Lead 46564 u /L Se -Selenium u /L Zn-Zinc 46567 u /L Or anochlorine Pesticides Or ano hos horns Pesticides Nitrogen Pesticides Acid Herbicides PCBs Semivolatile Organics TPH-Diesel Range Volatile Organics(VOA bottle TPH-Gasoline Range TPH-BTEX Gasoline Range LAB USE ONLY Temperature on arrival (°C): LOW r Sample ID: AB19429 Loc. Descr.: LAKE CREEK - BAY TRACE LAKE PO Number# 7G0581 Location ID: WQ0018708 VisitiD County: BLADEN Q W AT�Q Collect Date: 0711612007 River Basin `�j QG Report To FROAP RECEIVED y U \ Collect Time:: 11:40 t Region: FRO .. ;, *ti..,:,/;y � Date Received: 07/17/2007 Collector: B,TODD AUG ,o 2W7 g- Time Received: 08:20 Sample Matrix: 'GROUNDWATER \ Late Rep Logrted: D MMA Loc. Type: MONITORING WELL , Date Reported: 08/02/2007 Sample Depth DENR — FAYE i UiLE REGIONAL OFFICE Emergency Yes/No COC Yes/No YES Sample Qualifiers and Comments Routine Qualifiers For a more detailed description of these qualifier codes refer to www.dwqlab.org under Staff Access A -Value reported is the average of two or more determinations N3-Estimated concentration is < PQL and >MDL Bl-Countable membranes with <20 colonies; Estimated _ _ ___ _ - _ _ ______, __ NE=No established PQL _ B2-Counts from all filters were zero: - - - - P-Elevated PQL due to matrix interference and/or sample dilution 133- Countable membranes with -more than-60 or 80 colonies;' Estimated - -- - - -' - - - — - _ Q1-Holding time exceeded prior to receipt at lab. B4-Filters have counts of both >60 or 80 and < 20; Estimated Q2- Holding time exceeded following receipt by lab 135-Too many colonies were present; too numerous to count (TNTC) PQL- Practical Quantitation Limit -subject to change due to instrument sensitivity J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated U- Samples analyzed for this compound but not detected J3-The sample matrix interfered with the ability to make any accurate determination; Estimated X1-Sample not analyzed for this compound J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated N1-The component has been tentatively identified based on mass spectral library search and has an estimated value LAB' Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 1 of 2 s� �C DWQ .Laboratory Section 1�esufts Sample ID aB1s42s •location ID: WQ00187d8 Collect Date: 07/16/2007 Loc. Descr.; e, ` x Time:: 11:40 " LAKE CREEK -BAY TRACE LAKE Collect Visit ID ICAS # Analyte Name, PQL Result Qualifier Units Analyst/Date Approved By /Date Method Reference 7/17/07 7/17/07 m1c . TOC In liquid 2.0 9.6 mgfL ADEXTER CGREEN Method Reference APHA5310B-20th 7/26/07 8/1/07' WET Total Dissolved Solids In liquid 12 41 mgfL " AWILLIAMS - ` .CGREEN Method Reference APHA2540G18TH ' ` 7/19i07 7/27/07 Chloride 1.0 12' mgfL MIBRAHIM MOVERMAN Method Reference EPA 300.0 7117/07 7/20/07 Fluoride 0.4- 0.4 U mgfL MIBRAHIM MOVERMAN Method Reference EPA 300.0 7/17/07 7120107 Ion Chromatography TITLE_ mg/L MIBRAHIM' MOVERMAN Method Reference EPA 300.0 7117/07 7/20/07 Sulfate 2.0 11 mg1L MIBRAHIM MOVERMAN Method Reference EPA300.0 7/17/07 7/20/07 NUT NH3 as N In liquid 0.02 -- 0.04 mg/L as N ' MAJAYI CGREEN Method Reference LaclO-107-06-1-J 7/19/07 7/23/07 NO2+NO3 as N In liquid 0.02 0.56 mg/L as N MAJAYI CGREEN Method Reference 1.600-107-04-1-c 7/19/07 7/25/07 Nitrate as N In liquid . 0A2 -0.56 " mg1L as N MOVERMAN CGREEN Method Reference Lachat107-04-1-c 7/23/67 7/23/07, Nitrite as N In liquid_ 0.01 0.01 U mgfL as N GBELK CGREEN Method Reference Lachat107-04-1-c 7/18/07 7123107 Laboratory Section>> 1623 Mali Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 2 of 2 fl. North Carolina GROUNDWATER FIELD/LAB FORM Department of Environment and Natural Resources DIVISION OF WATER QUALITY -GROUNDWATER SECTION Location code_WQ 0018708 SAMPLE TYPE SAMPLE PRIORITY n County_Bladen )4 Water 0 Routine D qaboNrumber rVT_ Quad No Serial No. Soil El EmergencyDate Receive91 Time: 9• Lat. Lon ❑Other 3 Rec'd By: From:Bus oude 3 Hand Del., Chain of Custody Other: Report To: ARO FRO MRO, RRO, WaRO, WiRO,. I Data Entry By: Ck: WSRO, Kinston FO Fed. Trust, Central Off., Other: Date -Reported: Shipped by: Bus, ourier Hand Del., Other: Purpos Collector(s):_BillTodd ?���o-c5 Time )Baseline, Complaint, Complianc LUST, Pesticide Study, Federal Trust, Other: Date r% (circle one) / FIFI n ANA -1 YgPR Owner L AiZe. C reP ek 7-Ife-P_ pH 400 A-t . Y -Spec. Cond Temp.to • 9, fl 1 °C Odor A 4 Appearance qk[>'. f e cz U Field Analysis By:_BillTodd LABORATORY ANALYSES BOD 310 mg/L COD High,340 mg/L COD Low 335 mg/L , Coliform: MF Fecal 31616 /100ml . Coliform: MF Total 31504 /100ml X TOC 680 mg/L Turbidity 76 NTU Residue, Suspended 530 mg/L pH 403units _ Alkalinity to pH 4.5 410 mg/L Alkalinity to pH 8.3 415 mg/L Carbonate 445 mg/L ' Bicarbonate 440 mg/L Carbon dioxide 405 mg/L X Chloride 940 mg/L Chromium: Hex 1032 uglL Color: True 80 Cu Cyanide 720mg/L Lab 25°C Location or Site Description of sampling Sampling Method X Diss. Solids 70300 mg/L Fluoride 951 mg/L Hardness: Total 900 mg/L Hardness (non-carb) 902 mg/L Phenols 32730 ug/1 Specific Cond. 95 uMhos/cm X Sulfate 945 mg/L Sulfide 745 - mg/L Oil and Grease mg/L X NH3 as N 610 mg/L TKN as N 625 mg/L X NO2 + NO3 as N 630 mg/L. P: Total as P 665 mg/L X Nitrate (NO3 as N) 620 mg/L X Nitrite (NO2 as N) 615 mg/L GW-54 REV. 7/03 For Dissolved Analysis -submit filtered sample and write "DIS" in block. Sample Interval (Pumping time, air temp.; etc,) Ag-Silver 46566 u /L AI -Aluminum 46557 u /L As -Arsenic 46551 u /L Ba-Barium 46558 a /L Ca-Calcium'46552 m /L Cd-Cadmium 46559 u /L Cr-Chromium 46559 u /L Cu-Copper 46562 u /L Fe -Iron 46563 u /L Hg-Mercury 71900 u /L K-Potassium 46555 m /L - My-K4a4n_esium46554- -- --m /L- - Mn-Manganese 46565 u /L Na-Sodium 46556 m /L Ni-Nickel u /L Pb-Lead 46564 u /L Se -Selenium u /L Zn-Zinc 46567 u /L Acid Herbicides TPH-Diesel TPH-Gasoline ITemperature on arrival (°C): I DB Laboratoty Section Wesults Loc. Descr.: LAKE CREEK - BAY TRACE LAKE Location ID: W00018708 County: BLADEN " t� WArr4 River Basin ,Report To FROAP �� V\ Region: FRO .A1�a�. �I _ Collector: B TODD A 7 \� Sample Matrix: GROUNDWATER- -AUG 01 2Ml Loc. Type: MONITORING WELL Sample Depth DEhR-FA1'ErfE11iLLEREGIONALOMCE Sample ID: AB19428 PO Number# 7GO580 VisitlD Collect Date: 07/16/2007 Collect Time:: 11:10 Date Received: 07/17/2007 Time Received: 08:20 Labworks LoginlD MMA Date, Reported: 08/02/2001 Emergency Yes/No COC Yes/No YES Sample Qualifiers and -Comments Routine Qualifiers For a more detailed description of these qualifier codes refer to www.dwqlab.org under Staff Access A -Value reported is the average of two or more determinations N3-Estimated concentration is < PQL and >MDL �B1-Countable membranes�with20•colonies; Estimated 132- Counts from all filters were zero. P-Elevated PQL due _to,matr'ix interference and/or sample dilution.. _ 63- Countable membranes with more than 60 or 80 colonies; Estimated Q1-Holding time exceeded prior to receipt at lab. 134-Filters have counts of both >60, or 80 and < 20; Estimated Q2- Holding time exceeded following receipt by lab B5-Too many colonies were present; too numerous to count (TNTC) PQL-,Practical Quantitation Limit -subject to change due to instrument sensitivity J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated U- Samples analyzed for this compound but not detected J3-The sample matrix interfered with the ability to make any accurate determination; Estimated X1-Sample not analyzed for this compound , J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated NI -The component has been tentatively identified based on mass spectral library search and has an estimated value LAB Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Pagel of 2 jr: XC (D Q Laboratory Section ResuftS Sample ID AB19428 Location ID: W00018708 Collect Date: 07/1612007 Loc. Descr.: LAKE CREEK - BAY TRACE LAKE Collect Time:: 11:10 Visit ID r fop i? CAS # Analyte Name P61L Result tdualttler - units Anatysvuale • Approvea tsy /uate, Method Reference 7/17/07 7/17/07 MIC TOC In liquid 2.0 7.7 mgfL ADEXTER CGREEN Method Reference APHA5310B-20th 7126/07 8/1107 WET Total Dissolved Solids In liquid 12 29 M91L AWILLIAMS CGREEN Method Reference APHA2540C-18TH 7/19107 7/27/07 Chloride 1.0 4.0 mg/L MIBRAHIM MOVERMAN Method Reference EPA 300.0 7/17/07 7120/07 Fluoride 0.4 OA U mgfL MIBRAHIM MOVERMAN Method Reference EPA 300.0 7/17/07 7120/07 Ion Chromatography TITLE_ mgfL MIBRAHIM MOVERMAN Method Reference EPA 300.6 7/17/07 7/20/07 Sulfate 2.0 2.0 U mgfL MIBRAHIM MOVERMAN Method Reference EPA 300.0 7117/07 7/20/07 NUT NIi3 as N In liquid 0.02 0.10 mg/L as N MAJAYI CGREEN Method Reference Lac10-107-06-W 7/19/07 7123/07 NO2+NO3 as N In liquid 0.02 0.02 U mgfL as N MAJAYI CGREEN Method Reference LaclO-107-04-1-c 7/19/07 7/25/07 Nitrate as N In liquid 0.02 0.02 U mgfL as N MOVERMAN CGREEN Method Reference Lachat107-04-1-c 7/23/07 7/23./07 Nitrite as N In liquid 0.01 0.01 U mglL as N GBELK CGREEN —----------- - -- ---——MethodReference - _--__Lachal10Z04-1-c___—_ 7/18107 7/23/07 .Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 2 of 2 GROUNDWATER FIELD/LAB FORM r�-- D) C' p North Carolina Department of Environment and Natural Resources DIVISION OF WATER QUALITY -GROUNDWATER SECTION Location code_WQ 0018708 SAMPLE TYPE SAMPLE PRIORITY 0 �j�%1 County_Bladen C1 Water 0 Routine 0 Lab Number VA0M4 �, `� Quad No Serial No. El soil El Emergency' �Date Received Time ' Cam✓ Lat. Long. ❑ Other Rec'd By: frorn7Bus, uri Hand Del., ® Chain of Custody Othef: Report To: ARO, RO MRO, RRO, WaRO, WiRO, Data EntryBy: Ck: WSRO, Kinston FO Fed. Trust, Central Off., Other: Date Reported: Shipped by: Bus, ourler Hand Del., Other: Purpose: . Collector(s):_BilITO Date Time + /0 Baseline; Co mplaint,< ompliance LUST, Pesticide Study, Federal Trust, Other: (circle one) _ FIELD ANALYSES Owner />< A 6?1' Z 'eclkl t-Ake pH 400 Spec. Cond.94 at 250C Temp.lo LT,-, °C Odor e � .� uxl Appearance /1 Field Analysis By:_BiIITodd LABORATORY ANALYSES BOD 310 mg/L COD High 340 mg/L COD Low 335 mg/L Coliform: MF Fecal 31616 /100ml Coliform: MF Total 31504 /100ml X TOC 680 mg/L Turbidity 76 NTU Residue, Suspended 530 mg/L pH 403 units Alkalinity to pH 4.5 410 mg/L Alkalinity to pH 8.3 415 mg/L Carbonate 445 mg/L Bicarbonate 440 mg/L Carbon dioxide 405 mg/L X Chloride 940 mg/L Chromium: Hex 1032 ug/L Color: True 80 CU Cyanide 720 mg/L Lab Com Location or Site 1-n,4 A.4,o Description of samplin oint Uj e 'C Sampling Method r'tr e:2 Sample Interval Remarks umo. ai er. a c. X Diss. Solids 70300 mg/L Fluoride 951 mg/L Hardness: Total 900 mg/L Hardness (non-carb) 902 mg/L Phenols 32730 ug/I Specific Cond. 95 uMhos/cm X Sulfate 945 mg/L Sulfide 745 mg/L Oil and Grease mg/L , X NH3 as N 610 mg/L TKN as N 625 mg/L X NO2 + NO3 as N 630 mg/L P: Total as P 665 mg/L X Nitrate (NO3as N) 620 mg/L X Nitrite (NO2 as N) 615 mg/L GW-54 REV. 7/03 For Dissolved Analysis -submit filtered sample and write "DIS" in block. (Pumping time, air temp., etc.) Ag-Silver 46566 u /L AI -Aluminum 46557 u /L As -Arsenic 46551 u /L Ba-Barium 46558 u /L Ca -Calcium 46552 m /L Cd-Cadmium 46559 u /L Cr-Chromium 46559 u /L Cu-Copper 46562 u /L Fe -Iron 46563- u /L Hg-Mercury 71900 u /L K-Potassium 46555 m /L Mg -Magnesium 46554 ^m /L Mn-Manganese 46565 u /L- Na-Sodium 46556 m /L Ni-Nickel u /L Pb-Lead 46564 u /L Se -Selenium u /L Zn-Zinc 46567 u /L Or anochlorine Pesticides Or ano hos horus Pesticides Nitrogen Pesticides Acid Herbicides PCBs Semivolatile Organics TPH-Diesel Range Volatile Organics (VOAbottle) TPH-Gasoline Range TPH-BTEX Gasoline Range LAB USE ONLY Temperature on arrival (04 WC—DWO Laborato ection Wesults AB19427 LAKE CREEK - BAY TRACE LAKE Sample ID: Loc. Descr.: PO Number# 7G0579 Location ID: W60018708 VisitlD County: BLADEN �Q� WA Collect Date: 07/16/2007 River Basin Collect Time:: 10:40 Report To FROAP Region: FRO EEIVE1) r t , ; .ram:, � Date Received: 07/17/2007 Collector. TODD B tom* a "u �"�^� Time,Received: 08:20 Sample Matrix: GROUNDWATER .AUGy Q 7 2007 Loc. Type: MONITORING WELL / I\ Late Reporks rted: D MMA y� Date Reported: - "08/02/2007 Sample Depth DENR—FAYTfEViLLE REGIONAL OFFICE U Emergency Yes/No COC Yes/No YES Sample Qualifiers and Comments Routine Qualifiers For a more detailed description of these qualifier•codes refer to WWW-dwglab.brg under Staff Access A -Value reported is the average of two or more determinations N3-Estimated concentration is < PQL and >MDL —`- - B1--CCountablemembranes'with <20,colonies; Estimated- - - �-- ----------- ---- - - ----- NE -No established PQL -- — - — _ _B2- Counts from all filters were zero.__ - - - - - - - P-Elevated PQL due to matrix interference and/or sample dilution 133- Countable membranes with more than 60 or 80 colonies; Estimated Q1-Holding time exceeded prior to receipt at lab. 84-Filters have counts of both>60 or 80 and < 20; Estimated Q2- Holding time exceeded following receipt by lab B5-Too many colonies were present; too numerous to count (TNTC) PQL- Practical Quantitation Limit -subject to change due to instrument sensitivity . J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated U-Samples analyzed for this compound but not detected J3-The sample matrix interfered with the ability to make any accurate determination; Estimated X1-Sample not analyzed for this compound . J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated NI -The component has been tentatively identified based on mass spectral library search and has an estimated value LAB Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 1 of 2 �� �C 1�ZVQ La6oyatory Section 1�esuCts Sample ID AB19427 Location 0711612007 ID? WQ0018708 � Collect Date: Loc. Descr.: LAKE CREEK - BAY TRACE LAKE ( Collect Time:: 10:40 Visit ID CAS # Analyte Name PQL Result Qualifier Units Analyst/Date Approved By /Date - Sample temperature at receipt by lab 1.2 °C DSAUNDERS MMATHIS Method Reference 7/17/07 7/17/07 mic TOG In liquid 2.0 2.1 mg1L ADEXTER CGREEN Method Reference APHA53108-20th 7/26/07 8/1107 WET Total Dissolved Solids In liquid 12 22 J2 mg/L AWILLIAMS CGREEN Method Reference APHA2540C-18TH 7119107 7127107 Chloride 1.0 3.8 mg/L MIBRAHIM MOVERMAN Method Reference EPA 300.0 7/17/07 7/20/07 Fluoride 0.4 OA U mg1L MIBRAHIM MOVERMAN. Method Reference EPA300.0 7/17/07 7/20/07 Ion Chromatography TITLE_ mg/L MIBRAHIM MOVERMAN - Method Reference EPA 306.0 7/17/07 7/20107 Sulfate 2.0 7.3 mg1L MIBRAHIM MOVERMAN Method Reference EPA300.0 7/17/07 7/20/07 NUT NH3 as N In liquid 0.02 0.02 mg1L as N MAJAYI "CGREEN Method Reference LaclO-107-06-1-J 7/19/07 7/23/07 NO2+NO3 as N In liquid 0.02 0.02 U mg1L as N MAJAYI CGREEN Method Reference Lac10-107-04-1-c 7/19107 7/25107 Nitrate as N In liquid 0.02': 0.02 U mg/L as N MOVERMAN. CGREEN Method Reference Lachat107-04-1-c 7/23/07 7/23/07 Nitrite as N In liquid 0.01 0.01 U mg/L as N GBELK CGREEN - - — - -- - Method Reference - - Lachat107-04-1-c_- _ 7/18107 7/23/07 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 2 of 2 OUNDWATER FIELD/LAB FORM Location code_WQ 0018708, County_Bladen Quad No North Carolina Department of Environment and Natural Resources DIVISION OF WATER QUALITY -GROUNDWATER SECTION SAMPLE PRIORITY !n � V� ® Routine Q Lab Number El Emergency Date Received Tim : �- Rec'd By: From. -Bus, ouri , Hand Del., III aln o us o y Other'. Report To: ARO, FRO MRO, RRO, WaRO, WiRO, Data Entry By: Ck: WSRO, Kinston FO Fed. Trust, Central Off., Other: Date Reported: Shipped by: Bus, oune Hand Del., Other: Purpose: Collector(s):_BillTodd / y Time /r� : y ts_q.�Baseline, Complaint, Compliance LUST, Pesticide Study, Federal Trust, Other: Date — /(6-f�/ (circle one) FIELD ANALYSES Owner /_'4je_v- LA pH 400 Spec. Con .94 at 250C Location or Site 7T6 M jo w Temp.lo °C Odor -yiW, e. Description of sampling point GJ e-i t jve4 Appearance 818 A& _ Sampling Method .4, fi!=2 Sample Interval Field Analysis Remarks umD. naileF. a c. By:_BillTodd (Pumping time, air temp., etc.) LABORATORY ANALYSES Serial No. Long. _ BOD 310 mg/L COD High 340 mg/L COD Low 335 mg/L Coliform: MF Fecal 31616 /loom] Coliform: MFTotal 31504 /loom[ X TOC 680 mg/L Turbidity 76 NTU Residue, Suspended 530 mg/L pH 403 _ units Alkalinity to pH 4.5 410 mg/L Alkalinity to pH 8.3 415 mg/L Carbonate 445 mg/L Bicarbonate 440 mg/L Carbon dioxide 405 mg/L X Chloride 940 mg/L Chromium: Hex 1032 ug/L Color. True 80 Cu Cyanide 720 mg/L Lab SAMPLE TYPE M Water ❑ Soil ❑ Other VCh' fC td X Diss. Solids 70300 mg/L Fluoride 951 mg/L Hardness: Total 900 mg/L Hardness (non-carb) 902 mg/L Phenols 32730 ugh Specific Cond. 95 uMhos/cm X - Sulfate.945 mg/L Sulfide 745 mg/L Oil and Grease mg/L X NH3 as N 610 mg/L - TkN as N 625 mg/L X NO2 + NO3 as N 630 mg/L P: Total as P 665 mg/L X Nitrate (NO3as N) 620 mg/L X Nitrite (NO2 as N) 615 mg/L REV. 7/03 For Dissolved Analysis -submit filtered sample and write "DIS" in block. Ag-Silyer46566 u /L AI -Aluminum 46557 u /L As -Arsenic 46551 u /L Ba-Barium 46558 u /L Ca -Calcium 46552 m /L Cd-Cadmium 46559 u /L Cr-Chromium 46559 u /L Cu-Copper46562 u /L Fe -Iron 46563 u /L Hg-Mercury 71900 u /L K-Potassium 46555 m /L Mg -Magnesium 46554 m /L Mn-Manganese 46565- u /L Na-Sodium 46556 m /L Ni-Nickel u /L Pb-Lead 46564 u /L• Se -Selenium u /L Zn-Zinc46567 u /L Or anochlorine Pesticides Or ano hos phorus Pesticides Nitrogen Pesticides Acid Herbicides PCBs Semivolatile Organics TPH-Diesel Range Volatile Or- anics OA bottle TPH-Gasoline Range TPH-BTEX Gasoline Range LAB USE ONLY Temperature on arrival (°C): y. 4 NC DENR/DWQ Laboratory Report to: FRO - Sample Anomaly Report (SAR) `� Lab Number: AB19427 Sample ID: MW 1 U, Station Location: Lake Creek , County: Bladen Region: FRO Bay Tree Lake ample Type: Groundwater - ; Priority: Routine Collector: Bill Todd Water Date collected: 7/16/2007 Date received: 7/17/2007 Date analyzed: 7/19/2007 Affected Parameter(s): Total Dissolved Solids . Analytical Area (check one): NWCH ❑METALS ❑VOA ❑SVOA ❑NUT ❑MICRO ❑PEST ' I The following anomalies occurred (check all that apply): ❑Samples ❑Improper container used ❑VOA vials with headspace ❑Sulfide samples with headspace i ❑Samples not received, but listed on fieldsheet ❑Samples received, but not listed on fieldsheet ❑Mislabeled as to tests, preservatives, etc. ❑Holding time expired ❑Prior to receipt in lab ❑After receipt in lab ❑Insufficient quantity for analysis ❑Sample exhibits gross non -homogeneity ❑Sample not chemically preserved properly ❑pH out of range (record pH):<2 i ❑Improper chemical i ❑Residual chlorine present in sample ❑Color interference ❑Heavy emulsion formed during extraction ❑Sample bottle broken in lab - no reportable results ❑Other (specify): NQuality Control ❑Instrument failure -no reportable results ❑Analyst error - no reportable results ❑ Surrogates ❑None added ❑Recovery outside acceptance limits ❑Spike recovery ❑None added ❑Recovery outside acceptance limits NFailed to meet criteria for precision ❑Internal standards ❑Blank contamination ❑QC data reported outside of controls (e.g., QCS, LCS) ❑Incorrect procedure used ❑SOP intentionally modified with QA and Branch Head approval ❑Invalid instrument calibration ❑Elevated detection limits due to: ❑Insufficient sample volume _ Comments: Sample was run at 100 mis. 18ing/L (1.8 mg/100m1) of TDS were found within the second duplicate, below the 2:5mg of residue stated by the SOP for an accurate sample. Duplicates of the sample were also not within 56/o of the duplicate average. The first duplicate that was run produced a 25mg/L result. If this sample had not been duplicated, the sample would have passed precision criteria for a minimum of 2.5mg of residue. Corrective Action: 1 ❑Samples were rejected by DWQ Lab. Authorized by: Date: ❑Accepted and analyzed after notifying the collector or contact person and determining that another sample could not be secured. ❑Sample(s) on hold until: i ®Sample reported with qualification. Data! qualification code used:J2 ❑Other (explain): Notification Required? ❑ Yes ❑ No Person Contacted: Date: Form completed by: r i Lead Chemist evyi�� initial): ❑BIOCHEM�[Tf.'7 ❑PEST [-]METALS ❑VOA, Branch Head Review (in QA/QC Review ( itial) Date: 7/25/2007 ❑SVOA Logged into database by (initial): QA\Forms\Laboratory\SAR 10/23/Oldbs Microbac�, r T NAME & ADDRESS: �,n 74d 0) Fayetteville Division 2592 Hope Mills Road - Fayetteville, NG 1t33uti (ylu) 004- 1 WZU I oo-+-of I" IGA CHAIN OF CUSTODY RECORD PAGE 1 OF 1 PRaECTrLacATION: TYPE OF ANALYSIS PRESERVATION (CODE) La/!e N , ..,s, L � ?,uzej ee� o� Sample Type Sample SampleCHLORINE Start Date Start Time Date Tlme COMP GRAB � pH D.O.D O TEMP CHLORINE LAB ID # w - 3 she -- -=-- Date Time Received by:� nme Comments or Special Hazards: - Date y 1 7 G o? 1 1� 2-Relinquished `J Time Temp: Received b Date Time Y Dat Relinquished by:. 4 3 Date Time Recelved by: Date Time pH: Relinquished by: B Date Time Received by: Date Time Flow: Relinquished by: B 7 Additional Sample Comments: North Carolina GROUNDWATER FIELD/LAB FORM Department of Environment and Natural Resources DIVISION OF WATER QUALITY -GROUNDWATER SECTION Location code_WQ 0018708 SAMPLE TYPE SAMPLE PRIORITY Couhty_Bladen Water ® Routine LQ Lab Number Quad No Serial No. ❑ Soil ❑ Emergency Date Received Time: Lat. Long. ❑ Other ,- Rec'd By.- From:Bus, Courier, Hand Del., X Chain of Custody Other: Report To: ARO, FRO MRO, RRO, WaRO, WiRO, Data Entry By: Ck: WSRO, Kinston FO. Fed. Trust, Central Off—Cither: Date Reported: Shipped by: Bus, oune Hand Del., Other: Purpose: Collector(s):_BillTodd Date / Baseline, Complaint, Compliance LUST, Pesticide Study, Federal Trust,.Other: y (d �I (circle one) FIELD ANALYSES Owner 4,4,4a C :2e e__ , ft '%e ` Z_4 e pH 400- l Spec. Con 4 at 250C Location or Site e, M 1A (A} ' Temp.10 Sr'J °C Odor lr�,w a Description of sampling point bJ z 11 Ne.a . Appearance_ C' .9 A) Sampling Method a�� f�q2 Sample Interval Field -Analysis Remarks umo. bailer. etc.] By:_BIIITodd (Pumping time, air temp., etc.) LABORATORY ANAI YSFS BOD 310 mg/L COD High 340 mg/L COD Low 335 mg/L Coliform: MF Fecal 31616 /loom] Coliform: MF Total 31504 " /100ml X TOC 680 mg/L Turbidity 76 NTU Residue, Suspended 530 mg/L pH 403 units Alkalinity to pH 4.5 410 mg/L Alkalinity to pH-8.3 415 mg/L Carbonate 445 mg/L Bicarbonate 440 mg/L Carbon dioxide 405 mg/L X Chloride 940 mg/L Chromium: Hex 1032 ug/L Color: True 80 CU Cyanide 720 mg/L Lab X Diss. Solids 70300 mg/L Fluoride 951 . mg/L Hardness: Total 900 mg/L Hardness (non-carb) 902 mg/L Phenols 32730 ug/1 Specific Cond. 95 uMhos/cm X Sulfate 945 mg/L Sulfide 745 mg/L Oil and -Grease mg/L X NH3 as N 610 mg/L TKN as N 625 mg/L X NO2 + NO3 as N 630 mg/L P: Total as P 665 mg/L X Nitrate (NO3 as N) 620 mg/L X Nitrite (NO2 as N) 615 mg/L GW-54 REV. 7/03 For Dissolved Analysis -submit filtered sample and write "DIS" in block. Ag-Silver 46566 u /L AI -Aluminum 46557 u /L As -Arsenic 46551 u /L Ba-Barium 46558 u /L Ca -Calcium 46552 m /L Cd-Cadmium 46559 u /L Cr-Chromium 46559 u /L Cu-Copper46562 u /L Fe -Iron 46563 u /L Hg-Mercury71900 u /L K-Potassium 46555 m /L Mg -Magnesium 46554 Mn-Manganese 46565 -- - - u /L Na-Sodium 46556 m /L Ni-Nickel u /L Pb-Lead 46564 u /L Se -Selenium u /L Zn-Zinc 46567 u /L Or ano hos horus Pesticides Nitro en Pesticides Acid Herbicides PCBs Semivolatile Or anics TPH-Diesel Ran e Volatile Organics(VOA bottle TPH-Gasoline Range TPH-BTEX Gasoline Range LAB USE ONLY Temperature on arrival (°C): yr' vq 99a Compliance Inspection Report Permit: WQ0018708 Effective: 08/22/01 Expiration: 08/31/06 Owner: Lake Creek Corporation I SOC: Effective: Expiration: Facility: Lake Creek Corp-Baytree Lakes i County: Bladen ` r Region: Fayetteville Contact Person: Steve Jones Title: Phone: 910-588-4432 Directions to Facility: System Classifications: I Primary ORC: William E Stafford Certification: 989284 Phone: 910-862-4800 Secondary ORC(s): F On -Site Representative(s): Related Permits: Inspection Date: 07/16/2007 Entry Time:,10:00 AM Primary Inspector: Bill Todd Secondary Inspector(s): Reason for Inspection: Routine Permit Inspection Type: Surface Irrigation Facility Status: Q Compliant Q Not Compliant Question Areas: Miscellaneous Questions NWells (See attachment summary) Exit Time: 01:00 PM1 Phone:910-433-3300 Inspection Type: Compliance Sampling Page: 1 7 A Permit: WO0018708 Owner - Facility: Lake Creek Corporation Inspection Date: 07/16/2007 Inspection Type: Compliance Sampling Reason for Visit: Routine Inspection Summary: I, Bill Todd traveled to Bay Tree Lakes to meet with Wayne Vann of Vann Labs to conduct or to split -sample with Van Labs the wells at Bay Tree Lakes. We sampled MW-1, MW-2, Mw-3 and MW-5 for all the paramters that are required in the permit. All of My samples wer sent to the DWQ lab in Raleigh with the exception of the Coliform sample which were delivered to Micr-Bac in Fayetteville. The sample results showed that The wells at Bay Tree were completely in compliance. Page: 2 I North Carolina Department of Environment, Health, and Natural Resources j Division of Environmental Health, Public Water Supply Section SOURCE INFORMATION Date Form Completed GROUND WATER Owner Assigned Source Code Well Name purchase, name of seller i WOl WD � �1�, If purchase, seller ID# Source Begin Date Direct Influence Date MM - YY Location of well within the system (If purchase MM - DD - YY location of master meter) IACROSS ROAD FROM OFFICE, BEHIND FIRE DEPT L !: 05/30/08 b Code G=Ground ❑ W=Purchase/G G Y=G w/direct influence Z=W w/direct influence Availability P=Permanent E=Emergency I=Interim S=Seasonal i O=Other Latitude (N) Longitude (W) Deg. Min Sec Deg Min Sec 34 41 18.77 78 24 58.67 Ifpurchase, use sell is primary source lfat/longg�)II r 3 �. 3 g sy %� .— . / $ . ' � (p �� % Vulnerable VOC'sl Y N How Determined G=GPS ❑ M=Map GPS File Name S=Surveyed D=Differential GPS MM - DID - YY Assessment Date 01-01-90 ENTRY POINT INFORMATION Owner Assigned , Entry Point Code Entry Point Name L-- E01 TANK SITE Use Code Availability Entry Point Begin Date Entry Point End Date =Ground/Permanent 1E P=Year-round S=Seasonal D�1 =Ground/non-Permanent E=Emergency u I=Interim O=Other MM/YY MM/YY Location: AT WELL #1 Well Site: Owned or controlled? Y (Y,N) Control Area (100' radius?) Y (Y,N) If no, explain: —_ Sources of pollution/distance: STORAGE BUILDINGS NEAR WELL HEAD Y --- Surface water within 200'? FN In N If yes, actual distance If yes, bact. samples collected? tl (YIN) Adequate slope? Y (Y,N) Flooding? N (Y,N) Maintenance: OK Well House: Free of stored materials? N (Y,N) Properly drained? Y (Y,N) Locked? Y . (Y,N) Condition of house: OK Type of freeze protection: HOUSED ,�V` ell biameter �10'-'" Type: DRILLED Yield (gpm): _ UNK Properly sealed? Y (Y,IN) ; (If unknown, Properly vented? Y (Y,N) Casing Depth UNKK�ft put'UNK') Well depth: UNK Concrete slab adequate? Y (Y,N) If no, explain: Size of blow -off: 2" Sample tap?: Before treatment? Y (Y,N) Meter available? Y (Y,N) i Size: >3' After Treatment? Y (Y,N) Pumps: Capacity: GPM: SUB HP' 7 1/,'2 Pump intake depth: UNK Auxiliary Power? N (Y,N) Type pump: SUB _ C G_5_ O 6-Po C�/�ptClTt'J,- Height above floor;(pump/casing): SUB 6 / 20"+- Storage at well site: Elev: r Hydro: 6,000— Ground: f If hydro,"air volume control? N (Y,N) Safety valves: Y (Y,N) Coded?. UNK (Y,N) High service pumps: 1. _ gpm. hp 2. gpm hp 3. gpm ` hp 'Auxiliary power? (Y,N) Is water treated? F (Y,N) If yes, complete back of form. If other wells are treated here, which ones? W02 If treated elsewhere, where? If purchase, retreat? [—](Y/N) If yes, complete back of form. DENR 3803 (Revised 9-97) Public Water Supply Section (Review 9-00) P North Carolina Department of Environment, Health, and Natural Resources Division of Environmental Health, Public Water Supply Section SOURCE INFORMATION Date Form Completed GROUND WATER 05/30/08 Owner Assigned Source Code Well Name (If purchase, name of seller) Code G=Ground " - - -- W=Purchase/G j W02 WELL ,2P � � Y=G w/direct influence Z=W w/direct influence If purchase, seller ID# Source Begin Date Direct Influence Date Availability MM - ` YY MM - DID - YY r� P=Permanent � I N E=Emergency I -Interim r — S=Seasonal i O=Other Location of well within the system (If purchase, location of master meter) — APPX. 200' SE OF WELL #1 Latitude (N) Longitude (W) rDeg. Min Sec Deg Min Sec If purchase, use seller's primary source lat/lotig) Vulnerable VOC'slYl N How Determined G=GPS a =Map B=Surveyed y PPS File Name D=Differential GPS MM - DD - YY Assessment Date 01-01-90 ENTRY POINT INFORMATION Owner Assigned Entry Point Code Entry Point Name E01 WELL' #1 Use Code Availability Entry Point Begin Date Entry Point End Date C=Ground/Pennanent P P=Year-round S=Seasonal L_d D=Ground/non-Permanent ❑ E=Emergency I=Interim O=Other MM/YY MM/YY Location: AT WELL SITE Well Site: Owned or controlled? Y ; (Y,N) Control Area (100' radius?) _Y (Y,N) If no, explain: Sources of pollution/distance: NONE NOTED AT TIME OF INSPECTION WITHIN 100' Y Surface water within 200'? �N N If yes, actual distance If yes, bact. samples collected? �' (Y/N) Adequate slope? Y (Y,N) Flooding? N (Y,N) Maintenance: OK M� Well House: Free of stored materials? N/A (Y,N) Properly drained? N/A (Y,N) Locke'd? N (Y,N) Condition of house: FIBERGLASS COVER Type of freeze protection: ; lk Dtamete _4 Type: DRILLED Yield (gpm): UNK Properly sealed? Y (Y,N) a, (If unknown,„ e Properly vented? Y (Y,N) `C�astng�Depth' 275- t..ft put'uNlc') WeI depth 3:OS``' Meter available? Y (Y,N) Concrete slab adequate? Y (Y,N) If no, explain: Size: >3' Size of blow -off: 2" Sample tap?: Before treatment? Y (Y,N) After Treatment? Y (Y,N) Pumps: Capacity: GPM: UNK IJP-IX259Pump intake depth: UNK_ :Auxiliary Power? N (Y,N) Type pump: SUB _ _ Height above floor (pump/casing): SUB / 12" Storage at well site: Elev: I I Hydro: Ground: L If hydro, air volume control? (Y,N) Safety valves: _ (Y,N) Coded?(Y,N) High service pumps: 1. gpm' hp 2. gpm hp 3. gpm hp Auxiliary power? (Y,N) Is water treated? �Y (Y,N) If yes, complete back of form. If other wells are treated here, which ones? If treated. elsewhere, where? WELL #1 _ If purchase, retreat? (Y/N) If yes, complete back of form. I DENR 3803 (Revised 9-97) Public Water Supply Section (Review 9-00) DESIGN T. R.OBrRT LYONS AND ASSOCIATES SHEET CONSULTING ENGINEERS I I c"AnLOTTr, 'NORTH CAROLINA Ei� FOR JOB. NO. CHECK JOB .,I, - -, =--i TIE, ;7 L Y�ao 7P4 �-t 1-5 T, -2- 7Pr 0 PSI g�z e, AYPA Y-15- co tZ Q. Q LLY WYL LemsL 25 4o pr2AW navy tj p su g2pL TD Tmv- NO 0. 4,P il� Le, Z, �y ICJ 1� Th9t ev- V. te'. It We' —ff X ;A. QS2 46,03-0 i"Wpr --- -------- o. IS 0 '44 s s s _ x tit:, .. `p � .a a -' �i �.. � +� �, . � � � ] .a � E� { � i, '�'a `� �' � � ��; I �� ''� ��� �, �S� «• � ,�. ' _ ��� rarr�� . � ;a �'b - • r USA! j- P ry - ` s 'd =us, ' b. _ - s '' • - _ �r, - .. . , �, ,_ � r�• as a .'r , a � - r u � - , y's' ., Asa � 9 .� a+ 1 � t .x ` .� c ' ` >t�s! ` a a "� a � -• I a3 # ��e*' r t:' t i �f` i ., `I i ;t" � � � •fir a4 �V,'°(',�'*+- s, x � .+a a"F - -, .w . `a,. ""� �� --s 's& « ° -;• e x ' a .iy '' 7 . (•�` • € � x a,T, � o t r`. _� $� a $' 8. # c r �, b� ae - �. i m Ago 11 �1 a s.. •,.. .Af«a' .+r ;. a �.all t ,w `�.,r F.. r.. " g "*t, a d i. Lek`'«b k•� et , .! . -a°. �., .'•"* ' ; ,-,B #M. <,. _ + s, +' a J °i a " 4 y' ,. .- atat'� • a?' � _ � Iw• pw4 t ,r . � � 'ar ,�+rY. 1i° i.. i �'A% �i,��'• e.� � �"`� r �� ^,;«;•'* .. e a a e_ • , a � y , �,. •. y �t - „r-ze m.� t r. s. �5;* ��?� —___'ry yi, .s a �� f m;, au..� a,.� a � � , � a • a ��„. s _ " �'�'"'� y'y� a �. i;�ra' r wy '3 ' ,�,: . •� �-s• • _ � x. tit ' >` � 1 � ,� -� .� • ° a �- � �.F' ,Ate , t y. , y,M , ., ,� . , .• � ,.;� Yam, w , t R O� North Carolina Department of Environment,& Natural Resources Division of Water Quality Aquifer Protection Section MONITORING WELL INSPECTION REPORT Well Location: AV -14% - � -;rofrs,9_A1ib C• -- `DateF» Owner: 1,41,1e C e C ��4- Gr �� iCe � WELL.TYPE a /11b Q, Address: 3 Pal i A RA e / s f7iC 9 } County 7& a-04` Road/StreetJlw� j/ f4,s-E-: Quad No. BMW#= (Serial No. ims 0.0 41�� dl7 •Z 'J !Lat to / Long.? , d. /7 We1T onstruction Well Contractor e e e_ %h ja' N e ddress Contractor -Certification# cX G 2 Check Items Meets Min. Standards, ' Remarks Measured Permit Reg uired ? (Y/N) L . , :. Yes No ! i (Permit No.%(!( bog 2b Location - Distance From:........... f I Water Tight Sewage/waste collection 15P A F4 Waste Disposal (septic tank drain field) _ :✓ Other Poll: Source( ) } Other -Poll. Source( 1 . last' Cazbon Galy. St. Other Casing Type ................. .... t yp .. is 5 } s Depth.. ..................: Weight/thickness ..... . ..........e i Height(A.L.S.)................. $ h Other ( ) Grout S 9 ; S Type s ....................... f Thickness .....:............. # Depth ....................... r E Other( ) 3 Screens",. Screened interval 15 — ).a Other( �) a Well Contractor ............ Abandonment g ' Temporary .. s Permanent .......:.......... 4 ? s Cuttinl4s Reports Construction (GW-1) ...... . Abandonment (GW-30) ..... Well Head Completion ........ Access port Water tight pipe entry ... , .. . Well entry :..........'.... . Date Well Constructed ,_ - f A a o t Cheek Items Meets Min. Standards Remarks Measured Yes No. i f INSPECTOR^v Name Office Witness(es) (If Available) Name Address Type Name Address Type r Al,' p15Vy s� ' North Carolina Department of Environment &,Natural Resources Poly Division of Water Quality Aquifer Protection Section, MONITORING WELL INSPECTION REPORT Well Location: w /;�. - /11A/, - • Date JIAJ_ - /� t Owner: e o Q e e ! WELL TYPE /' o fry Address: a' Bry ��� el 2 e / s C ' j County %�} Road/Street Yzv 9 yj Quad No. Serial No —;M y ,y! .� r ,3� • . _ �` Lat Long. e1T , oonstruction 4 .. Well Contractor / e- eZ e Address Contractor Certification# Check Items Meets Min. Standards Remarks Measured Yes No j Permit Required (Y/N) L .... (Permit No. 001?2 Location - Distance From:......... / d Water Tight Sewage/waste collection Waste Disposal (septic tank drain field) i Other Poll. Source( ) i s 8i Other Poll. Source( t � Casing GDCarbon Galy. St: Other Type................... E: Depth.. Weight/thickness ................ / 1 Height A.L.S. ✓ i ' i Other ( ) f s Grout Type............. Thickness .....:....... ... 4 Depth ...............: .. Other( ) Screens i Screened interval ........... x � N C Other(. Well Contractor ............ Abandonment Temporary ................. Permanent ................. s. Z S Cuttings Reports Construction (GW-1) ....... Abandonment (GW-30) ..... Well Head Completion ....... Access port .. ...... ...... . Water tight pipe entry ... , .. . Well entry . ................ . � # �pMeets r �n Check Items Min. Standards � Remarks Measured Yes NoIt yjn' Y } Date Well Constructed 9L— /,4- .16 IN r INSPECTOR- D Ile Name Office e Witness(es� (If Available) Name Address Type Name Address Type 9 North Carolina Department of Environment &,Natural Resources Division of Water Quality 1 Aquifer Protection Section MONITORING- WELL INSPECTION REPORT Nell Location: � us.e / d -� C ;Date Owner° j�e C aaA �b f 4ez-11 1. ROE- ' . ;WELL —PE1a6rdL2(�c, Address: &J ,�,� 'Rs(/ i�d, e/%� �%� o?a' jCounty jRoad/Street 411 "i . :Quad No. 1W #_ ,Serial No.)6, i _s ob 4a� Long. Well" onstructlon 1 Well Contractor /r �-� Na e Address Contractor Certification# f Check Items Meets Min. Standards Remarks Measured Yes No Permit Required ? (Y/N) L .... t (PermitNoW4 Cc/,(70)$ Location - Distance From:........... Water Tight Sewage/waste collection Waste Disposal (septic tank drain field) Other -Poll. Source( ) ► '/- Other Poll. Source( ) F[ F.' ✓ R 1 Casing Plastic Carbon Galy. St. Other Type....................... Depth . .............. Weight/thickness ................. 4 Height (A.L.S.) .. .:........ , Other ( ) # Grout / Type............. ...... V Thickness .....:............. i� 3 a Depth....................... s Other( Screens Screened interval ........... t �s ✓ ` Other( Well Contractor ......... r u. - Abandonment i Temporary .. r Permanent .................. i F Cuttings Reports Construction (GW-1) ........ Abandonment (GW-30) .... . Well Head Completion ....... Access port ................. Water tight pipe entry ... , Well entry ................. Date Well Constructed D D Check Items Meets Min. Standards Remarks Measured Yes No, � Y 4 �• 6 .`t INSPECTOR Name Office (If Available) Name Address Type Name Address Type �,v�. North Carolina fffiii p� Department of Environment &.Natural Resources �,iy Division of Water Quality Aquifer Protection Section MONITORING WELL INSPECTION REPORT ._ Mns.+a.a+wmn.4iw�'.'aif"i+wT�c.+3iaavn•.owm� Well Location: #10 �= % MA-kVQWK% Ale-, Date-TA.-J. 11, Pa/ 0 Owner: 2 I WELL TYPE /t7anlao2 r Address: J,3 ,Q C . ai County e-,-1 j Road/Street h l s Quad No. MW .#=' Serial-5a z / f %. �. % /- 3 0 j Lat.3!5L lo9q lj Long. Well Contractor Cj'ryll,�Y/�C� y�2'.7"h 6'i2d' Name Contractor Certification# oZ /,.I to Permit Required ? (Y/N) I.... . Location - Distance From:.......... . Water Tight Sewage/waste collection Waste Disposal (septic tank drain field) Other,Poll. Source( ) Other Poll. Source( ) Casing , Type....................... Depth. .................. Weight/thickness ................ Height (A.L.S.) ................. Other ( ) Grout Type ............. Thickness .....:............. Depth....................... Other( ) Screens Screened interval ........... Other( ) Well Contractor ............ Abandonment Temporary ................. Permanent ............... Address Check Items Meets Min. Standards Remarks Measured Yes No w I" � (Permit NoW Plastic Carbon Galy. St. Other 6 � c. 1. , zl t� '✓ i CuttinLs Reports Construction (GW-1) ....... Abandonment (GW-30) ... . Well Head Completion ....... Access port .................. Water tight pipe entry :....... Well entry........ ...... . Date Well Constructed Check Items Meets Min. Standards' Remarks Measured Yes No r-' A INSPECTOR e, 0- Name Office Witness(es) (If Available) Name Address Type Name Address Type