WQ0000957_GW Monitoring_20160822

VALLEY PROTEINS , INC.
August 22, 2016 RECEIVED
DEQIDWR
Department of Environment & Natural Resources 2 g ZQ16
Division of Water Resources — Information Processing Unit AUG
1617 Mail Service Center
Raleigh, NC 27699-1617 T4QF0'S
Re: Valley Proteins,Vdoro Division,
Permit #WQO,O47 2w
C-3 V
Enclosed please find the rteTFy 4oring Wells Report for our Wadesboro, North
Carolina Division. o
If you require any additional information or wish to discuss the information' in this report,
please feel free to call me at [phone].
Sincerely,'
Chris Bivans
General Manager
P.O. Box 718
Wadesboro, NC 28170
704-694-3701 Creating Renewable Resources Built on "Tradition
Fax:[phone]
wwwvalleyproteins.com

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES'
GROUNDWATER QUALITY MONITORING:
s
DIVISION OF WATER. QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
617 MAIL SERVICE CENTER, RALEIGH,'NC,27699.1617 'Phone: (919) 733=3221 , •,
FACILITY INFORMATION Please Print
Clearly or Type
PERMIT Number: Expiration Date: 06/30/2018
Facility Name: Valley Proteins
Non -Discharge W00000957 UIC
Permit Name (if different):
NPDES Other
Facility Address: 656 Little Duncan Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Wadesboro NC 28170 County Anson
0 Spray Field ❑ Remediation:
Contact Person: Chris Bivans
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Behind Field #9
No. of wells to be sampled: 8
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW#1
Date sample collected: 07/21/16
FIELD ANALYSES:
WAS
Well Depth: 33 ft.
Well Diameter: 2 in.
pH 7.0 units Temp. 16.9 °C
DRY at
Depth to Water Level: 18.19 ft. below measuring point
Screened Interval: ft.
to
ft. Spec. Cond. µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor No Odor
check
Volume of water pumped/bailed before sampling:
9 gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered: DYES
❑ NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed: 07/21/16 - 07/29/16
Laboratory Name: PACE Analytical
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
" COD mg/I
Nitrite (NO.) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal <1 /100ml
Nitrate (NO3) as N
14.3 mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 1080 mg/I
AI - Aluminum
mg/I
pH (when analyzed) 7.0 units
Ba - Barium
mg/I
TOC 1.4 mg/I
Ca - Calcium
mg/I
Chloride 307 mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 25.8 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance EtMhos
K - Potassium
mg/I
VOC method #
Total Ammonia <• 10 mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen; NH�as N; Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Chris Bivans (General Manager)
Permittee (or Authorized Aqent) Name and Title - Please print or type
GW-59 Rev.1/2007
.V?

aceAnaI cal
www.pacefabs.com
YTICAL RESULTS
Project: Sprayfield Wells
Pace Project No.: 92306020
Parameters Results Units
Field Data
Analytical Method:
Collected By
JJQ 1
Collected Date
7/21116
Collected Time
08:45
Field pH
7.0 Std. Units
Field Temperature
16.9c deg C
Appearance
CLEAR
Field Specific Conductance
1,653 umhos/cm
MBIO 9222D Fecal Coliform CHT
Analytical Method: SM 9222E
Fecal Coliforms
ND CFU/100 m
2540C Total Dissolved Solids
�I
Analytical Method: SM 2540E
Total Dissolved Solids
1080 mg/L
4500H+ pH, Electrometric
I
Analytical Method: SM 4500-1
pH at 25 Degrees C
7.0 Std. Units
300.0 IC Anions 28 Days
Analytical Method: EPA 30 .0
Sulfate
25.8 mg/L
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
ND mg/L I
353.2 Nitrogen, NO2/NO3 pres.
Analytical Method: EPA 3512
Nitrogen, NO2 plus NO3
14.3 mg/L
4500 Chloride
Analytical Method: SM 4500-I
Chloride
307 mg/L
I
5310E TOC
Analytical Method: SM 5310E
Total Organic Carbon
1.4 mg/L
Date: 08/03/2016 08:58: PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
acted: 07/21/16 08:45 Received: 07/21/16 13:15 Matrix: Water
Report Limit DF Prepared Analyzed CAS No. Qual
1
1
1
0.10 1
0.50 1
1
1.0 1
1.0 1
125 1
1.0 1
2.0 1
0.10 1
0.10 5
100 100
1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in"full,
without the written consent of Pace Analytical Services, Inc..
08/01/16 11:36
08/01/16 11:36
08/01/16 11:36
08/01/16 11:36
08/01/16 11:36
08/01/16 11:36
08/01/16 11:36
07/21/16 13:38
07/26/16 10:58
07/25/1613:45 H6
07/28/16 01:33 14808-79-8
07/26/1613:49 7664-41-7
07/26/16 15:33
07/23/16 02:42 16887-00-6 M6
07/29/16 05:01 7440-44-0
Page 5 of 36

c?GEfl1ic31j/i1Cc71 �
Document Name:
Field Data Sheet
Document Issued: April 6, 2015
Page 1 of
,,.-
Document Number:
Issuing Authority:
F-CAP,-FLD-001-rev.00
Pace Huntersville Quality Office
l Field Data Sheet
Client; �L l'�� P` :AL.IV' Location: G{,��c r� p Gv`r r <-_ fir,
l s 6 \1 L Project Name/#: f4tf ; ��._i_. >
Name and Afiliation (Sampler(s):
Name and Affiliation (Inspector): iv ( f�-
Well Information
Well ID:
Well Diameter:
Total Well Depth: ? 3. U 3 ft
Static Water Level: t t_i . 9 q ft
Well Locked: �'ES'; NO
Construction: (EVC Steel Stainless Steel
Multi Factor*: b • I 'J [*(Radius/12)2 x 3.14 x 7.481
Casing Volume: , , `) gallons
Height of Water Column: �� 1 ft Cal. 3 Volumes:"] ; (� gallons
Ptnge Information
r
Date Purged: (�' / % �� / (�' Start Time: C) �1 L' Finish: I U : c7 -f Purge Rate: N
Purging Method: �� c ...( 'r Total Volume Purged: �`�- 0 gallons
Sampling Information j
Date Collected: C (- i 1 I Time Collected:
pm
Sampling Equipment Used:
Bottle Type
Preservation
" rVC. 3 Vo,,� ;LVlvs /i c J D
-.,Zlo .w0,Vf
Field Measurements/Observations
Sample Temp (°C): � �r Time: n `f
Sample pH (s.u.): %: (' Time:
Specific Cond. (uS): (L., `5 3 Time: `t •S
ReDox (mV): `--' Time:
Odor: N 6 t JF_ Time: 0 Z-.: -1 S
General/Weather Observations
Sampler Signature/Date:
Stabilization Test
Analysis Required
fvl # %tea /�:<'! izl i l-Ari
- •.:%erit•t.. rt-vr�t+crud
Turbidity (ntu): Time:
Diss Oxy (mg/L): Time:
Res. Cl (mg/L): Time: —
Other:
Appearance:
_ Time:
Time
Purged
pH (s.u.)
Spec. Cond.
(us)
P,eDox (mV)
Turbidity
(ntu)
Diss Oxy.
(mg/Q
Temp. (°C)
Volume
gemoved
/ / 1.l i c• '>
Other
r�2
Page 29 of

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF. ENVIRONMENT & NATURAL" RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION; OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
617 MAIL°SERVICE CENTER, RALEIGH,`NC 27C99-1617 Phone:-(919)-733 3221 =
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 06/30/2018
Facility Name: Valley Proteins
Non -Discharge WQ0000957 UIC
Permit Name (if different):
NPDES Other
Facility Address: 656 Little Duncan Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Wadesboro NC 28170 County Anson
❑fc Spray Field ❑ Remediation:
Contact Person: Chris Bivans
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Behind Field #4
No. of wells to be sampled: 8
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW#2
Date sample collected: 07/21/16
FIELD ANALYSES:
WAS
Well Depth: 30 ft.
Well Diameter: 2 in.
pH 7.0 units Temp. 18.6 °C
DRY at
Depth to Water Level: 23.08 ft. below measuring point
Screened Interval: ft. to
ft. Spec. Cond. µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor No Odor
check
Volume of water pumped/bailed before sampling:
12 gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered: DYES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 07/21/16 - 07/29/16
Laboratory Name: PACE Analytical
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal <1 /100ml
Nitrate (NO3) as N 9,3 mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 1240 mg/I
Al - Aluminum
mg/I
pH (when analyzed) 7.0 units
Ba - Barium
mg/I
TOC <1 mg/I
Ca - Calcium
mg/I
Chloride 393 mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 6.9 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance EtMhos
K - Potassium
mg/I
VOC method #
Total Ammonia <.10 mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen; NH,as N; Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
, method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Chris Bivans (General Manager)
Permittee (or Authorized Aqent) Name and Title - Please print or type
GW-59 Rev.1/2007
JW

4 Pace Analytical Services, Inc.
1 aceAnalyt�ical ® 2225 Riverside Dr.
Asheville, NC 28804
www.pacelabs.com
[phone]
ANALYTICAL RESULTS
Project: Sprayfield Wells
Pace Project No.: 92306020
Sample: MW-2
Parameters
Lab ID: 92306020002 Collected: 07/21/16 09:40
Results Units Report Limit DF
Received: 07/21/16 13:15 Matrix: Water
Prepared Analyzed CAS No. Qual
Field Data
Analytical Method:
Collected By
JJQ
1
08/01/16 11:36
Collected Date
7/21116
1
08/01/16 11:36
Collected Time
09:40
1
08/01/16 11:36
Field pH
7.0 Std. Units
0.10
1
08/01/16 11:36
Field Temperature
18.6C deg C
0.50
1
08/01/16 11:36
Appearance
CLEAR
1
08/01/16 11:36
Field Specific Conductance
1,970 umhos/cm
1.0
1
08/01/16 11:36
MBIO 9222D Fecal Coliform CHT
Analytical Method: SM 9222D
Fecal Coliforms
NO CFU/100 mL
1.0
1
07/21/16 13:57
2540C Total Dissolved Solids
Analytical Method: SM 2540C
Total Dissolved Solids
1240 mg/L
125
1
07/26/16 10:58
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B
pH at 25 Degrees C
7.0 Std. Units
1.0
1
07/25/16 13:45
H6
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
6.9 mg/L
2.0
1
07/28/16 01:43
14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
NO mg/L
0.10
1
07/26/16 13:51
7664-41-7
353.2 Nitrogen, N021NO3 pros.
Analytical Method: EPA 353.2
Nitrogen, NO2 plus NO3
9.7 mg/L
0.060
3
07/26/16 15:36
M1
4500 Chloride
Analytical Method: SM 4500-CI-E
Chloride
393 mg/L
100
100
07/23/16 02:45
16887-00-6
5310B TOC
Analytical Method: SM 5310B
Total Organic Carbon
ND mg/L
1.0
1
07/29/16 05:11
7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/03/2016 08:58 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 36

Document Name:
Document Issued: April 6, 2015
it
ace'�i1alyllcal_
Field Data Sheet
Page 1 of
Document Number;
Issuing Authority:
f
RCAR-FLD-001-rev.00
Pace Huntersville Quality Office
.0A
1 Field Data Sheet J
Client: `'' -�' � 1��i C I `, % V N Location: GJ Vk f Project Name/#
Name and Affiliation (Sampler(s):
Name and Afiliation (Inspector):
Well Information
Well ID: 11
Well Diameter:
Total Well Depth:
Static Water Level: �(�. �� LI ft
Height of Water Column: ft
Well Locked: C_YES NO
Construction: PVC , Steel Stainless Steel
Multi Factor*: [•(Radius/12)2 x 3.14 x 7.48]
Casing Volume: ) . Z gallons
Cal. 3 Volumes: 1 1' i`f gallons
Purge Information
Date Purged: 2 j- / J v / I (,. Start Time: I 0 • : 'f Finish: 0 � 5 0 Purge Rate: 01
Purging Method: Total Volume Purged: ��� 0 gallons
Sampling Information
Date Collected: I I (r. Time Collected:
pm
Sampling Equipment Used:
Bottle Type
j Lji v v^Y>
1- SC`oYY, L
( 5�tir.L
1-1.) 5 1-1--(
Field Measurements/Observations
Preservation
Analysis Required
P)7 0> A-C ! /7 ' 1 U 6,
_C'( for-i(-(L 5:.-i �( T/{Lnli'Tc1CY71�l i.r��
,A/ 6W
j nS
SAC{{:°--c4alC_( CC)
Sample Temp (°C): { Y Time: 7 `/ `)' V
Sample pH (s.u.): 7 Time:
Specific Cond. (uS): Time:
ReDox (mV): Time:
Odor: NO IQ VTime: 0 c/ `/ ( I
General/Weather Observations
Sampler Signature/Date:
Stabilization Test
Turbidity (ntu): Time:
Diss Oxy (mg/L): Time:
Res. Cl (mg/L): Time:
Other: `'" Time: -
Appearance: C.:_ Ceiv=1
I,'L'IrvI')S S-411,/U•',r)l') 5 �•�n
c I�. 0 7.. /,q 1 l 1
Time
Pur g ed
pH (s.u.)
Spec. Cond.
(us)
P,eDox (mV)
Turbidity
(ntu)
Diss Oxy.
(mg/L)
Temp. (°C)
Volume
Removed
Other
Page 30 of 3

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
IVISION.OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
617'MAIL SERVICE<CENTER, RALEIGH„NC27699-1617 Phone: (919);7333221 •_
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 06/30/2018
Facility Name: Valley Proteins
Non -Discharge W00000957 UIC
Permit Name (if different):
NPDES Other
Facility Address: 656 Little Duncan Road
TYPE OF PERMITTED OPERATION BEING MONITORED
Wadesboro "'" NC 28170 County Anson
❑ Lagoon ❑ Remediation: Infiltration Gallery
K❑ Spray Field ❑ Remediation:
Contact Person: Chris Bivans
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Behind Field #1
No. of wells to be sampled: 8
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW#3
Date sample collected: 07/21/16
FIELD ANALYSES:
WAS
Well Depth: 29.2 ft.
Well Diameter: 4 in.
pH 6.9 units Temp. 18.1 °C
DRY at
Depth to Water Level: 13.48 ft. below measuring point
Screened Interval: ft. to
ft. Spec. Cond. µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor No Odor
check
Volume of water pumped/bailed before sampling:
10 gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered: DYES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 07/21/16 - 07/29/16
Laboratory Name: PACE Analytical
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO.) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal <1 /loom[
Nitrate (NO3) as N 4.1
mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 925 mg/I
Al - Aluminum
mg/I
pH (when analyzed) 6.9 units
Ba - Barium
mg/I
TOC 1.1 mg/I
Ca - Calcium
mg/I
Chloride 315 mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 177 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance ItMhos
K - Potassium
mg/I
VOC method #
Total Ammonia <.10 mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen; NH, as N; Ammonia Nitrogen. Total)
Mn -Manganese
mg/I
,method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: " mg/L VOC Removal%
Chris Bivans (General Manager)
Permittee (or Authorized Aqent) Name and Title - Please print or type
GW-59 Rev.112007
a

ac(eAnal�?ical
i www.pacelabs.com
ANALYTICAL RESULTS
Project: Sprayfield Wells
Pace Project No.: 92306020
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW-3
Lab ID: 92306020003 Collected:
07/21/16 07:45
Received: 07/21/16 13:15 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No. Qual
Field Data
Analytical Method:
Collected By
JJQ
1
08/01/16 11:37
Collected Date
7/21/16
1
08/01/16 11:37
Collected Time
07:45
1
08/01/16 11:37
Field pH
7.0 Std. Units
0.10
1
08/01/16 11:37
Field Temperature
18.1C deg C
0.50
1
08/01/16 11:37
Appearance
CLEAR
1
08/01/16 11:37
Field Specific Conductance
1,873 umhos/cm
1.0
1
08/01/16 11:37
MBIO 9222D Fecal Coliform CHT
Analytical Method: SM 9222D
Fecal Coliforms
ND CFU/100 mL
1.0
1
07/21/16 13:38
2540C Total Dissolved Solids
Analytical Method: SM 2540C
Total Dissolved Solids
925 mg/L
125
1
07/26/16 10:58
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B
pH at 25 Degrees C
6.9 Std. Units
1.0
1
07/25/16 13:45 H6
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
177 mg/L
40.0
20
07/28/16 01:54 14808-79-8 M6
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
ND mg/L
0.10
1
07/26/16 13:52 7664-41-7
353.2 Nitrogen, N021NO3 pres.
Analytical Method: EPA353.2
Nitrogen, NO2 plus NO3
4.1 mg/L
0.020
1
07/26/16 15:42
4500 Chloride
Analytical Method: SM 4500-CI-E
Chloride
315 mg/L
100
100
07/23/16 02:46 16887-00-6
5310E TOC
Analytical Method: SM 5310B
Total Organic Carbon
1.1 mg/L
1.0
1
07/29/16 05:22 7440-44-0
Date: 08/03/2016 08:58 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 36

�) .
Document Name:
Field Data Sheet
Document Issued: April 6, 2015
Page 1 of
... aGe%�atylical
Document Number:
Issuing Authority:
F-CAR-FLD-001-rev.00
Pace Huntersville Quality Office
Field Data Sheet
\ t
Client: `' I e , l c? v Location: �V i �� P c G'i' C�� r� C Project Name/#: =5
Name and Afiliation (Sampler(s);
Name and Afiliation (Inspector):
Well Information
Well ID:
Well Diameter; imC1w5
NR.
Total Well Depth: ft
Static Water Level: ( % ft
Well Locked: :ES ; NO
Construction: Steel Stairdess Steel
Multi Factor*: [*(Radius/12)2 x 3.14 x 7.48]
Casing Volume: 2 • gallons
IIeight of Water Column: r� ft Cal. 3 Volumes: 2 • L gallons
Purge Information
Date Purged: Start Time: Finish: 09 Purge Rate: A%
Purging Method: 13 0 i '' Total Volume Purged: I A (�" . gallons
Sampling Information
Date Collected: 02 1 iT i Time Collected: am) pm
(._<_
Sampling Equipment Used: e.- -
Bottle Type Preservation
jAC:, ititf)
/—.50, 0 1 vv L_ t.'u 7VL
— 15 E-n L
Field Measurements/Observations
Sample Temp (°C): Y 1 Time:
Sample pH (s.u.): . t Time: f �t
Specific Cond. (uS): I? rt ' Time: 0 -7,14S
ReDox (mV): Time:
Odor: Time: C)
General/Weather Observations
Sampler Signature/Date:
Stabilization Test
.analysis Required
.-.t-Gl e
( Lt (c v; Al , SL, i�r:.�. Xr ,V, ko�tvl rpilI "):p,
._rhS
Turbidity (ntu): `—
Time:
Diss Oxy (mg/L):
Time:
Res. Cl (mg/L):
Time:
Other:
Time:
Appearance:
� U` ••., ,i fl 1,.1 I � 4.. i..t
Iai lit:
Time
Purged
pH (s.u.)
Spec. Cond.
(US)
ReDox (mV)
Turbidity
(ntu)
Diss Oxy.
(mg/L)
Temp. (°C)
Volume
Removed
C"N 13
Otiler
Page 31 of 3

SUBMIT FORM ON YELLOW PAPER ONLY
ROUNDWATER QUALITY MONITORING:
OMPLIANCE REPORT FORM
­11 ITV lki CI MAAA' Il kl Please Print Clearly or
Facility Name: Valley Proteins
Permit Name (if different):
Facility Address: 656 Little Duncan Road
Wadesboro NC 28170 County Anson
act Person: Chris Bivans Telephone#: [phone]
Location/Site Name: Behind Pond #1 No. of wells to be sampled: 8
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH', NC,27699.1617 Phone: [phone], _
PERMIT Number: Expiration Date: 06/30/2018
Non -Discharge W00000957 UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
x❑ Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
.L ID NUMBER (from Permit): MW#5 Date sample collected: 07/21/16
Depth: 29.2 ft. Well Diameter: 2 in.
h to Water Level: 10.25 ft. below measuring point Screened Interval: ft. to _ft.
suring Point is ft. above land surface Relative M.P. Elevation: ft.
me of water pumped/bailed before sampling: 9.75 gallons
WELL
FIELD ANALYSES:
pH 6.6 units
Spec. Cond. _
Odor No Odor
Appearance Clear (here: ❑
Temp. 18.7 °C DRY at
Whos I time of
sample analyzed: 07/21/16 - 07/29/16
Laboratory Name: PACE Analytical
Certification No.
IAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal
<1 /100ml
Nitrate (NO3) as N
<,020 mg/I
Zn - Zinc mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
1840 mg/I
Al - Aluminum
mg/I
pH (when analyzed)
6.6 units
Ba - Barium
mg/I
TOC
2.1 mg/I
Ca - Calcium
mg/I
Chloride
354 mg/I
Cd - Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/l
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
33.8 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance
µMhos
K - Potassium
mg/I
VOC method #
Total Ammonia
<• 10 mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
, method #
TKN as N
mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Chris Bivans (General Manager) / 0r_
Permittee (or Authorized Aqent) Name and Title - Please print or type Siqnature of a (or Authorised Aqent)
GW-59 Rev.1/2007
Vr

Al
aceAnalytical
wnw.pacelabs.com
ANALYTICAL RESULTS
Project: Sprayfield Wells
Pace'Project No.: 92306020
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW-5
Parameters
Lab ID: 92306020004 Collected: 07/21/16 10:30
Results Units Report Limit DF
Received: 07/21/16 13:15 Matrix: Water
Prepared Analyzed CAS No. Qual
Field Data
Analytical Method:
Collected By
JJQ
1
08/01/16 11:37
Collected Date
7/21/16
1
08/01/16 11:37
Collected Time
10:30
1
08/01/16 11:37
Field pH
6.6 Std. Units
0.10
1
08/01/16 11:37
Field Temperature
18.7C deg C
0.50
1
08/01/16 11:37
Appearance
CLEAR
1
08/01/16 11:37
Field Specific Conductance
2,512 umhos/cm
1.0
1
08/01/16 11:37
MBIO 9222D Fecal Coliform CHT
Analytical Method: SM 9222D
Fecal Coliforms
ND CFU/100 mL
1.0
1
07/21/16 13:57
2540C Total Dissolved Solids
Analytical Method: SM 2540C
Total Dissolved Solids
1840 mg/L
250
1
07/26/16 10:59
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B
pH at 25 Degrees C
6.6 Std. Units
1.0
1
07/25/16 13:45
H6
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
33.8 mg/L
2.0
1
07/28/16 02:26
14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
ND mg/L
0.10
1
07/26/16 13:54
7664-41-7
353.2 Nitrogen, N021NO3 pres.
Analytical Method: EPA 353.2
Nitrogen, NO2 plus NO3
ND mg/L
0.020
1
07/26/16 15:43
4600 Chloride
Analytical Method: SM 4500-CI-E
Chloride
354 mg/L
20.0
20
07/23/16 02:47
16887-00-6
5310E TOC
Analytical Method: SM 5310B
Total Organic Carbon
2.1 mg/L
1.0
1
07/29/16 09:16
7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/03/2016 08:58 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 36

Document Name:
Document Issued: Aplil6, 2015
' l'8GEA71�?I ICa/
Feld Data Sheet
Page 1 of
Document Number:
Issuing Authority;
P-CAR-FLD-001-rev.00
Pace I-iuntersville Quality Office
j� Field Data Sheet
Client: V Ci C.f.i F � o IC 111i„ Location' 1� c� .c. �;p r'0 rJ C 5 %`� " ` i-
,, _ Project Name/#: f)
Name and Afiliation (Sampler(s):_ t)' �Y — `F�ii
Name and Afiliation (Inspector): _ Wit.
Well Information
Well ID:
Well Diameter: ? 1
Total Well Depth: Ci. 'C3 ft
Static Water Level: I () . ft
Height of Water Column: I`f ft
Well Locked: �ES,' NO
Construction: PVC Steel Stainless Steel
Multi Factor*: �� r(Radius/12)2 x 3.14 x 7.48I
Casing Volume: ( gallons
C7
Cal. 3 Volumes: ?i gallons
Purge Information
Date Purged: / 0 / / i (;) r� � t
�- �` + Start Time: + 1� 7 Finish: Purge Rate: `
Purging Method: Total Volume Purged: i� `') gallons
Sampling Information
Date Collected: -� I " ' l (� ko Time Collected: arri pm
Sampling. Equipment Used: I-, c:., � ..e ,..
Bottle Type
LRU
Field Measurements/Observations
o . r ....�... Time: I Sample Temp (C):
Sample pH (s.u.): (''' ��% Time: i O C-
Specific Cond. (uS): a %' '• Time: ( 0" >' `
ReDox (mV): Time:
Odor: ! Time:
_General/Weather Observations
- Ill, LLI � ✓ �('`.�-7 �' Y-' l,{ -/�K1: 1�.7
Preservation
/V 61 nl 1✓
IV L' A/
Sampler Signature/Date:
Stabilization Test
Analysis Required
j Dc1-'
c-A1*�n"c�� / ��.I+tin(: i; /Vr11_e�e )!Pf//+113
Turbidity (ntu): - Time:
Diss Oxy (mg/L): Time:
Res. Cl (mg/L): - Time:
Other: Time:
Appearance: I'A'-, --
Time
Purged
g
pH (s.u.)
Spec. Cond•
(us)
ReDox (mV)
Turbidity
(ntu)
Diss Oxy.
(mg/L)
Temp..(°C)
Volume
Removek
Other
Page 32 of

SUBMIT FORM ON YELLOW PAPER ONLY
EPARTMENT,OE ENVIRONMENT 8 NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
Mimi
,VlSION'OF.WATERQUALITY-INFORMATION,PROCESSING, UNIT
COMPLIANCE REPORT FORM
617 MAIL SERVICE'CENTER,,RALEIGH NC 27699=1617 Phone'.- {919j'733 3221 , =y:
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 06/30/2018
Facility Name: Valley Proteins
Non -Discharge W00000957 UIC
Permit Name (if different):
NPDES Other
Facility Address: 656 Little Duncan Road
TYPE OF PERMITTED OPERATION BEING MONITORED
Wadesboro NC 28170 County Anson
❑ Lagoon ❑ Remediation; Infiltration Gallery
X1 Spray Field ❑ Remediation:
Contact Person: Chris Bivans
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Behind Field #20
No. of wells to be sampled:
8
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW#6
Date sample collected: 07/21/16
FIELD ANALYSES:
WAS
Well Depth: 45 ft.
Well Diameter: 2
in.
pH 6.2 units Temp. 17.4 °C
DRY at
Depth to Water Level: 11.32 ft. below measuring point
Screened Interval:
ft. to
ft. Spec. Cond. µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor No Odor
check
Volume of water pumped/bailed before sampling:
10.5 gallons
Appearance Cloudy
here: ❑
Samples for metals were collected unfiltered: El YES
❑ NO and field acidified: ❑ YES
❑ NO.
LABORATORY INFORMATION
Date sample analyzed: 07/21/16 - 07/29/16
Laboratory Name: PACE Analytical
Certification No.
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal <1 /100m1
Nitrate (NO3) as N
<,020 mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 128 mg/I
Al - Aluminum
mg/I
pH (when analyzed) 6.2 units
Ba - Barium
mg/I
TOC <1 mg/I
Ca - Calcium
mg/I
Chloride 12.3 mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/l
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 4.8 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance I.LMhos
K - Potassium
mg/I
VOC method #
Total Ammonia <.10 mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
, method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total' VOCs: mg/L VOC Removal%
Chris Bivans (General Manager)
Permittee (or Authorized Aqent) Name and Title - Please print or type
GW-59 Rev.1/2007
Aqent)

L
1 aceAna1j4ca1
www.pacelabs.com
ANALYTICAL RESULTS
Project: Sprayfield Wells
Pace Project No.: 92306020
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW-6
Parameters
Lab ID: 92306020005 Collected: 07/21/16 08:10
Results Units Report Limit DF
Received: 07/21/16 13:15 Matrix: Water
Prepared Analyzed CAS No. Qual
Field Data
Analytical Method:
Collected By
JJQ
1
08/01/16 11:38
Collected Date
7/21116
1
08/01/16 11:38
Collected Time
08:10
1
08/01/16 11:38
Field pH
6.5 Std. Units
0.10
1
08/01/16 11:38
Field Temperature
17.4C deg C
0.50
1
08/01/16 11:38
Appearance
CLOUDY
1
08/01/16 11:38
Field Specific Conductance
158.8 umhos/cm
1.0
1
08/01/16 11:38
MBIO 9222D Fecal Coliform CHT
Analytical Method: SM 9222D
Fecal Coliforms
ND CFU/100 mL
1.0
1
07/21/16 13:38
2540C Total Dissolved Solids
Analytical Method: SM 2540C
Total Dissolved Solids
128 mg/L
25.0
1
07/26/16 11:00
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B
pH at 25 Degrees C
6.2 Std. Units
1.0
1
07/25/16 13:45
H6
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
4.8 mg/L
2.0
1
07/28/16 02:36
14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
ND mg/L
0.10
1
07/26/16 13:55
7664-41-7
353.2 Nitrogen, NO2/NO3 pres.
Analytical Method: EPA 353.2
Nitrogen, NO2 plus NO3
ND mg/L
0.020
1
07/26/16 15:44
4500 Chloride
Analytical Method: SM 4500-CI-E
Chloride
12.3 mg/L
1.0
1
07/23/16 02:52
16887-00-6
5310B TOC
Analytical Method: SM 5310B
Total Organic Carbon
ND mg/L
1.0
1
07/29/16 09:48
7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/03/2016 08:58 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 36

Document Name:
Field Data Sheet
Document Issued: April 6, 2015
Page 1 of 1
,. aceAlnalytical
Document Number:
issuing Authority;
F-CAR-FLD•001-rev.00
Pace Hunters:•ille Quali, Office
c� "+
,r. 1Field Data Sheet :) +, r� •,� ��r,i ,U Client: "U r17Vj-' r'.� 1•(i';��, 'i r Location: ,l i i [; i ' ':7iY C. Project Name/#: t ,') u., . -,!
Name and Afiliation (Sampler(s):
Name and Afiliation (Inspector): N %rl
Well Information
Well ID: 'u,l1v ' �t
Well Diameter: - �l
Total Well Depth: 1-1 ft
Static Water Level: ft
Height of Water Column:
Well Locked: b
Construction: PVC
NO
Steel Stainless Steel
Multi Factor*: % 16
� L [•(Radius/12)2 x 3.14 x 7.481
Casing Volume: 1I7'�. gallons
Cal. 3 Volumes: 1 t-( = gallons
Purge Information
c
Date Purged: / ? / 1 Li Start Time: (U Finish: �' C/`l 3 Purge Rate:
Purging Method: Total Volume Purged: 1)+ i gallons
Samuline Information
77
Date Collected:_ =1-� z1 irY� 1 %�i I Time Collected: 'I V �a_i pm
Sampling Equipment Used: i i, r I. -
Bottle Type
Preservation
LSD, -,IL N"i]>iV
at, 1
; i-C I I)
iv' � rJE
Field Measurements/Observations
Sample Temp (°C): �r�' `L— Time: (% �
Sample pH (s.u.): (.;1 • Time: L 1 U
Specific Cond. (uS): c Time: 0 210
ReDox (mV):
Time: —
Odor: Time: OD 0
n(
Sampler Signature/Date:
Stabilization Test
Analysis Required
c:..E,(dr'ic� � su.l;�lhz: 7'; N,fYat�r',7 %��I1-�•�Ti
i US
Turbidity (ntu): Time: `'
Diss Oxy (mg/L): Time: µ
Res. Cl (mg/L): '- Time: �-
Other: Time: w
Appearance: L
!;"-/. /-)I /1C~
Time
Purged
pH {s.u.)
Spec. Cond.
(us) .�
P,eDox (mV)
Turbidity
(ntu)
Diss Oxy.
(mg/L)
o
Temp. (C)
Volume
Removed
Otilef
Page 33 of 3

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES.
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER QUALITY -INFORMATION PROCESSING=UNIT.'
COMPLIANCE REPORT FORM
617MAIL SERVICE"CENTER,RALEIGH,,NC27699=1617 Phone:•[phone] '.
FACILITY INFORMATION Please Print
Clearty or Type
PERMIT Number: Expiration Date: 06/30/2018
Facility Name: Valley Proteins,
Non -Discharge WQ0000957 UIC
Permit Name (if different):
NPDES Other
Facility Address: 656 Little Duncan Road
TYPE OF PERMITTED OPERATION BEING MONITORED
Wadesboro NC 28170 County Anson
❑ Lagoon ❑ Remediation: Infiltration Gallery
❑x Spray Field ❑ Remediation:
Contact Person: Chris Bivans
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Behind Field #19
No. of wells to be sampled: 8
❑ Water Source Heat Pump ❑ Other:
•
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW#7
Date sample collected: 07/21/16
FIELD ANALYSES:
WAS
Well Depth: 52 ft.
Well Diameter: 2 in.
pH 7.1 units Temp. 18.3 °C
DRY at
Depth to Water Level: 21.2 ft. below measuring point
Screened Interval: ft. to
ft. Spec. Cond. FtMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor No Odor
check
Volume of water pumped/bailed before sampling:
5.5 gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered: ❑YES
El NO and field acidified: []YES El NO
LABORATORY INFORMATION
Date sample analyzed: 07/21/16 - 07/29/16
Laboratory Name: PACE Analytical
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal <1 /l ooml
Nitrate (NO3) as N .12 mg/I
Zn - Zinc mg/I
Coliform: MF Total /loom[
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 309 mg/I
AI - Aluminum
mg/I
pH (when analyzed) 7.1 units
Ba - Barium
mg/I
TOC <1 mg/I
Ca - Calcium
mg/I
Chloride 29.1 mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 5.8 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method #
Total Ammonia <• 10 mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen; NH�as N; Ammonia Nitrogen, Total)
Mn -Manganese
mg/I
,method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Chris Bivans (General Manager)
Permittee (or Authorized Aqent) Name and Title - Please print or type
GW-59 Rev.1/2007

I
l aceAnaly�ical
www.pacelabs.com
ANALYTICAL RESULTS
Project: Sprayfield Wells
Pace Project No.: 92306020
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW-7
Lab ID: 92306020006 Collected:
07/21/16 09:10
Received: 07/21/16 13:15 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
Field Data
Analytical Method:
Collected By
JJQ
1
08/01/16 11:40
Collected Date
7/21/16
1
08/01/16 11:40
Collected Time
09:10
1
08/01/16 11:40
Field pH
7.2 Std. Units
0.10
1
08/01/16 11:40
Field Temperature
18.3C deg C
0.50
1
08/01/16 11:40
Appearance
CLEAR
1
08/01/16 11:40
Field Specific Conductance
514.7 umhos/cm
1.0
1
08/01/16 11:40
MBIO 9222D Fecal Coliform CHT
Analytical Method: SM 9222D
Fecal Coliforms
ND CFU/100 mL
1.0
1
07/21/16 13:57
2540C Total Dissolved Solids
Analytical Method: SM 2540C
Total Dissolved Solids
309 mg/L
25.0
1
07/26/16 11:00
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B
pH at 25 Degrees C
7.1 Std. Units
1.0
1
07/25/16 13:45
H6
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
5.8 mg/L
2.0
1
07/28/16 02:47
14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
ND mg/L
0.10
1
07/26/16 13:57
7664-41-7
353.2 Nitrogen, N021NO3 pres.
Analytical Method: EPA 353.2
Nitrogen, NO2 plus NO3
0.12 mg/L
0.020
1
07/26/16 15:45
4500 Chloride
Analytical Method: SM 4500-CI-E
Chloride
29.1 mg/L
1.0
1
07/23/16 02:53
16887-00-6
5310E TOC
Analytical Method: SM 5310B
Total Organic Carbon
ND mg/L
1.0
1
07/29/16 09:58
7440-44-0
Date: 08/03/2016 08:58 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 10 of 36

Document Name:
Document Issued: April 6, 2015
M1
G@A haMical
Field Data Sheet
Page 1 of
Document Number:
Issuing Authority:
F-CAR-FLD-001-rev.00
Pace Huntersville Qui Office
Field Data Sheet
Client: "x \r%',�:; ' ''r''T: f',� �. Location: i` S L19 'r("t): ; r Project Name/#:
Name and Afiliation (Sampler(s):_ I /;:'c: (, j
Name and Affiliation
Well Information
Well ID: ;u i ,ii - 7
Well Diameter: % i •1:
Total Well Depth: V) 3 ft
Static Water Level: 2 1, ? ft
Height of Water Column: Alt ft
Well Locked: iES
Construction: 'V 1
NO
Steel Stainless Steel
MultiFactor*: D R U_ : Si; [*(Radius/12)2 x 3.14 x 7.481
Casing Volume:. 2 gallons
Cal. 3 Volumes: ! " k' gallons
Purge Information
Date Purged: —) / 7. / ( t -( Start Time: A60 Finish: U 7 Purge Rate:
Purging Method: ,�yud C, r Total Volume Purged: `t 1)" °)gallons
SampIing Information
(1 • r
Date Collected; ���' 1 14� Time Collected: C.1� pm
Sampling Equipment Used:' -
Bottle Type Preservation Analysis Required
;� • yp;� 1.- 'v' ca .;�ilcs Flc� f7 •7Z�C.•
L �i,`� �v L= 6�(i • i ctC Stt I a p• 7 , /Vr 't-6'YYt !f L ;I G
Vill Net
I 1.,5- 1-"t_ Ff�,SE7cr /L'rrtL Aeiji2F:fiie�-
Field Measurements/Observations
Sample Temp (°C): 1 Time: 09' 10
Sample pH (s.u.): Time: -) 9;1
Specific Cond. (uS): `� 1' T� Time: r) ` : I Q
ReDox (mV): --- Time: --
Odor: hi (i ,�L. Time: C r/ 1 L�
Sampler Signature/Date:
Stabilization Test
Turbidity (ntu):
Time:
Diss Oxy (mg/L):
"' Time:
Res. C1(mg/L):
Time:
Other:
Time:
Appearance:
L•f
)7/91
Time
Purged
pH (s.u.)
Spec. Cond.
(us)
ReDox (mV)
Turbidity
(ntu)
Diss Oxy.
(mg/L)
Temp, (oC)
Volume
Removed
�j v-1 ri
Otller
y_�
r
6
_
]
�}V, )teab'/
l
Page 34 of

SUBMIT FORM ON YELLOW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES ..
GROUNDWATER QUALITY MONITORING:
MMC617,MAILSERVICE'C'E'NttR,RALEIGk;NC27699-1617-
IVISION.OF WATER QUALITY-INFORMATIONEROCESSING UNIT : . ,
COMPLIANCE REPORT FORM
Phone: [phone]-
FACILITY INFORMATION Please Print
Clearly or Type
PERMIT Number: Expiration Date: 06/30/2018
Facility Name: Valley Proteins
Non -Discharge W00000957 UIC
Permit Name (if different):
NPDES Other
Facility Address: 656 Little Duncan Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Wadesboro "`""4' NC 28170 County Anson
0 Spray Field ❑ Remediation:
Contact Person: Chris Bivans
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Behind Field #16
No. of wells to be sampled: 8
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW#8
Date sample collected: 07/21/16
FIELD ANALYSES:
WAS
Well Depth: 30 ft.
Well Diameter: 2 in.
pH 6.8 units Temp. 20.8 eC
DRY at
Depth to Water Level: 6.14 ft. below measuring point
Screened Interval: ft. to
ft. Spec. Cond. µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative'M.P. Elevation: ft.
Odor No Odor
check
Volume of water pumped/bailed before sampling:
4 gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 07/21/16 - 07/29/16
Laboratory Name: PACE Analytical
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal <1 /100ml
Nitrate (NO3) as N <.20
mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 428 mg/I
Al - Aluminum
mg/I
pH (when analyzed) 6.8 units
Ba - Barium
mg/I
TOC <1 mg/I
Ca - Calcium
mg/I
Chloride 91.0 mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 8.5 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance I.tMhos
K - Potassium
mg/I
VOC method #
Total Ammonia <-10 mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
, method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Chris Bivans (General Manager)
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.112007

,. aceArialytical
wvtivpacelabs.com
ANALYTICAL RESULTS
Project: Sprayfield Wells
Pace Project No.: 92306020
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW-8
Lab ID: 92306020007 Collected:
07/21/16 11:00
Received: 07/21/16 13:15 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No. Qua[
Field Data
Analytical Method:
Collected By
JJQ
1
08/01/16 11:40
Collected Date
7121/16
1
08/01/16 11:40
Collected Time
11:00
1
08/01/16 11:40
Field pH
6.8 Std. Units
0.10
1
08/01/16 11:40
Field Temperature
20.8C deg C
0.50
1
08/01/16 11:40
Appearance
CLEAR
1
08/01/16 11:40
Field Specific Conductance
607 umhos/cm
1.0
1
08/01/16 11:40
MBIO 9222D Fecal Coliform CHT
Analytical Method: SM 9222D
Fecal Coliforms
ND CFU/100 mL
1.0
1
07/21/16 13:57
2540C Total Dissolved Solids
Analytical Method: SM 2540C
Total Dissolved Solids
428 mg/L
25.0
1
07/26/16 11:01
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B
pH at 25 Degrees C
6.8 Std. Units
1.0
1
07/25/16 13:45 H6
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
8.5 mg/L
2.0
1
07/28/1619:43 14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
ND mg/L
0.10
1
07/26/16 13:58 7664-41-7
353.2 Nitrogen, NO2/NO3 pres.
Analytical Method: EPA 353.2
Nitrogen, NO2 plus NO3
ND mg/L
0.020
1
07/26/16 15:46
4500 Chloride
Analytical Method: SM 4500-CI-E
Chloride
91.0 mg/L
10.0
10
07/23/16 02:54 16887-00-6
5310B TOC
Analytical Method: SM 5310B
Total Organic Carbon
ND mg/L
1.0
1
07/29/16 10:09 7440-44-0
Date: 08/03/2016 08:58 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 11 of 36

Document Name:
Field Data Sheet
Document Issued: April 6, 2015
Pa e 1 of ��__
Document Number:
F-CAR-FLD-001-rev.00
Issuing Authority:
Pace Huntersville Quality Office
j } Field Data Sheet
Client: _ U .(:1.L:1n 11 i l' ; : Location: lr��f;i i�(.i1 cj L . ° = i��
�:. ,Y.. �V' Project Name/#: tr''
Name and AfiliationU(Sampler(s):_ 1'Ar ­'(.)
Name and Afiliation (Inspector):_ ? k1
Well Information
Well ID: A
Well Diameter: l
Total Well Depth: L I `% ft
Static Water Level: I (' • t'+ ft
Height of Water Colun: I- �, L,1
mft
Well Locked:
Construction: I'VC
NO
Steel Stainless Steel
Multi Factor*: t . ( -%C' [*(Radius/12)2 x 3.14 x 7.481
Casing Volume: ). I` gallons
Cal, 3 Volumes: 1 •' t (.D gallons
Purge Information
Date Purged: Z / 0 / (. Start Time: � `> Finish C 3S {Purge Rate: /Q 1A
17)
Purging Method:_.- (.0 Total Volume Purged: �� `r j� gallons
Sampling Information
Date Collected: 1- (2 t I I h Time Collected: pm
Sampling Equipment Used:
> c, , I ?.I
Bottle Type
Preservation
Analysis Required
.PII'! q Ac 1 U
C'
N C/NC
C.1'1 It)r^�ilC'. , fG• l;n�'!tiT• 7'/Vr fY✓��c';�j I�N � ra/3
l- .S
ivoIV,r
-b s
/T'::J_ S0z
Field Measurements/Observations
7VT)+4-
c,
Sample Temp (°C): �U
Time: I I '• 1��
Turbidity (ntu): Time: -
Sample pH (s.u.): (0 • `
Time: 1 1'. 00
Diss Oxy (mg/L): Time:
Specific Cond. uS :
( )
Tune I Wit.%
-
Res. ClCI (mg/L): Time:
ReDox (mV):
Time: 11 O u
Other: Time: _.
Odor:
Time: !,1 ()C'
Appearance: \'ce,
Sampler Signature/Date:
Stabilization Test
('--�'1�;)i1
Time
Purged
pH (s.u.)
Spec. Cond,
(US)
( )
ReDox (mV)
Turbidity
(ntu)
Diss Oxy.
(mg/L)
Temp. (°C)
Volume
Removed
Other
Page =o

SUBMIT FORM ON YELLOW PAPER ONLY
EPARTMENT OF ENVIRONMENTS NATURAL RESOURCES',• -
GROUNDWATER QUALITY MONITORING:
IM6117
[VISION OF WATER QUALITY -INFORMATION PROCESSING UNIT •
COMPLIANCE REPORT FORM
MAILSERVICECENTER,RALEIGH„NC27699-1617 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 06/30/2018
Facility Name: Valley Proteins
Non -Discharge W00000957 UIC
Permit Name (if different):
NPDES Other
Facility Address: 656 Little Duncan Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Wadesboro ""' NC 28170 County Anson
" "'`'r'
Spray Field ❑ Remediation:
Contact Person: Chris Bivans
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Behind Field #14
No, of wells to be sampled: 8
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW#9
Date sample collected: 07/21/16
FIELD ANALYSES:
WAS
Well Depth: 29 ft.
Well Diameter: 2 in.
pH 6.8 units Temp. 17.5 eC
DRY at
Depth to Water Level: 11.35 ft. below measuring point
Screened Interval: ft.
to
ft. Spec. Cond. µMhos
time of
sampling,check
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor No Odor
Volume of water pumped/bailed before sampling:
9 gallons
Appearance Murky
here: ❑
Samples for metals were collected unfiltered: El YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 07/21/16 - 07/29/16
Laboratory Name: PACE Analytical
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/1
Coliform: MF Fecal <1 /100ml
Nitrate (NO3) as N
.41 mg/1
Zn - Zinc mg/1
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/l
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 940 mg/I
Al - Aluminum
mg/I
pH (when analyzed) 6.8 units
Ba - Barium
mg/I
TOC <1 mg/I
Ca - Calcium
mg/I
Chloride 366 mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/1
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 24.4 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method #
Total Ammonia <,10 mg/I
Mg - Magnesium
mg/l
method #
(Ammonia Nitrogen; NH�as N; Ammonia Nitrogen, Total)
Mn -Manganese
mg/1
,method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
GW-59 Rev.1/2007

Z aceAnNjdc'al
mw.pacelabs.com
ANALYTICAL RESULTS
Project: Sprayfield Wells
Pace Project No.: 92306020
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW-9
Lab ID: 92306020008 Collected:
07/21/16 10:05
Received: 07/21/16 13:15 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
Field Data
Analytical Method:
Collected By
JJQ
1
08/01/16 11:42
Collected Date
7/21/16
1
08/01/16 11:42
Collected Time
10:05
1
08/01/16 11:42
Field pH
6.8 Std. Units
0.10
1
08/01/16 11:42
Field Temperature
17.5C deg C
0.50
1
08/01/16 11:42
Appearance
MURKY
1
08/01/16 11:42
Field Specific Conductance
1,725 umhos/cm
1.0
1
08/01/16 11:42
MBIO 9222D Fecal Coliform CHT
Analytical Method: SM 9222D
Fecal Coliforms
ND CFU/100 mL
1.0
1
07/21/16 13:57
2540C Total Dissolved Solids
Analytical Method: SM 2540C
Total Dissolved Solids
940 mg/L -
125
1
07/26/16 11:01
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B
pH at 25 Degrees C
6.8 Std. Units
1.0
1
07/25/16 13:45
H6
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
24.4 mg/L
2.0
1
07/28/1619:57
14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
ND mg/L
0.10
1
07/26/16 14:03
7664-41-7
353.2 Nitrogen, N021NO3 pres.
Analytical Method: EPA 353.2
Nitrogen, NO2 plus NO3
0.41 mg/L
0.020
1
07/26/16 15:47
4500 Chloride
Analytical Method: SM 4500-CI-E
Chloride
366 mg/L
10.0
10
07/23/16 02:54
16887-00-6
5310E TOC
Analytical Method: SM 5310B
Total Organic Carbon
ND mg/L
1.0
1
07/29/16 10:19
7440-44-0
Date: 08/03/2016 08:58 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 12 of 36

Document Name:
Document Issued: April 6, 2015
,.,.-Cel�i7�]IyUC�rl
Field Data Sheet
Page 1 of
Document Number:
Issuing Authority:
F-CAR-FLD-001-rev.00
Pace Huntersville Qualitv Office
Field Data Sheet f/
Client: �,jLt l( `•t- `i,,bt Loca 'on:_iAd^r.r: 12011 i, L- Project Name/#:
Name and Afiliation (Sampler(s);
Name and Afiliation (Inspector):
Well Information 1
Well ID:
Well Diameter: f i>
Total Well Depth: :r' % ft
Static Water Level: �r ft
Height of Water Column: l ft
Well Locked: ES
Construction: 'V
we]
Steel Stainless Steel
Multi Factor*; ) / b? J -6 1*(Radius/12)2 x 3.14 x 7.48]
Casing Volume: 7. = 6
1( gaIons
Cal. 3 Volumes: `f i , t gallons
Purge Information
Date Purged: 7 / 7. 0 / j i 0 Start Time: Finish: GI Purge Rate: N
Purging Method: N ,I i_C V, Total Volume Purged: 1710 gallons
Sampling Information
Date Collected: `f I 1 I �' j Time Collected: (arm; pm
Sampling Equipment Used:
Bottle Type
3•• t(OmLy0,4 J-SzDf'n L
Preservation
d)os 4C i D
,101V E-
ivol U
L- tUCi �_ Sj_ C) -3
iF
la rv1I-
I easuremen s serva ions
Sample Temp (°C): R. G; . Time: i 01 C.>'
Sample pH (s.u.): �." Time: C) J S
Specific Cond. (uS): t7 Time: 100
ReDox (mV):
Odor: r'".' L> n
General/Weather Observations
Sampler Signature/Date:
Stabilization Test
Time:
Time:
Analysis Required
LI C, ))
C� 1 5' IC��. •�, l Ll}=� ( �!'fYCtJlri lr /-/ h � C�
7v.�
'�%3-1'� fl�t�n'IGY1+Cu
Turbidity (ntu):
~-- Time:
Diss Oxy (mg/L):
-'' Time:
Res. Cl (mg/L):
Time:
Other:
Time:
Appearance:
111-"t t; +r k4-1.r
Time
Purged
pH (s.u.)
Spec. Cond.
(us)
ReDox (mV)
Turbidity
(ntu)
Diss Oxy.
(mg/L)
Temp. (°C)
Volume
Removed
Other
t,
,.
{
t
Page 36 of

GW-59A COMPLIANCE REPORT FORM Permit # WQ0000957
(Submit one each monitoring periodwith GW 59 forms.)
1
Enter date monitoring results were due. ( 8/31/2016 ) Will this monitoring report (GW-59 and GW-59A)
YES
NO
be submitted after the established due date?
2
Was any required Information missing on the GW-59 report forms?
YES
NO
IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
identification plate, area overgrown, etc.)2f the answer is "YES", contact to Regional Office for guidance
4
Are any monitoring constituents equal to or above the established standards?
YES
NO
If the answer to question 4 is "NO", skip to section 8.
If the answer to question 4 is "YES'list the affected wells individually with constituents(s) and concentration(s)
exceeding standards in the space provided below:
MW# 1, 2, 3, 5 and 9 exceed ground water standards for Total Dissolved Solids.
MW# 1, 2, 3, 5 and 9 exceed for chlorides.
MW#1 exceeds for nitrate.
MW#6 exceeds for pH.
5
For the same constituents identified in question 4 above, have standards been exceeded previously for the
YES
NO
same constituents s in the same wells s in the last two ears?
If the answer to question 5 is "NO", skip to section 8.
If the answer to question 5 is "YES")ist in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years).
See Report enclosed.
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
If the answer is "YES", a groundwater quality problem may be occuring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly
located; contact the Regional Office
7
Is the permittee implementing previously approved actions required by the Division involving this
YES
NO
groundwater quality problem?
If the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 7 is "NO'l;ontact the Regional Office within 90 days: an evaluation may be
_required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subject the permitteee to a Notice of Violation
fines, and/or penalties.
P(ezometers were placed In the Irrigation fields to determine water quality .
Total Dissolved Solids and Chlorides are naturally high in this area.
Sprinkler heads were purposely capped off near monitoring well #1 as Instructed by Jim Barber (Division of Water Resources)
to see if the nitrate level will change in the well.
Results for nitrates include nitrite due to lab.
8
The Person completing this portion (GW-59A) of the monitoring report should sign below and submit this
form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby acknowledge that the above Information was evaluated and the information submitted In this
report (Compliance Report GW-59A) is true and complete to the best of my knowledge.
Sign ure of Permittee (or Authorized Agent) Dad
GW-59A 121812003