WQ0003698_Groundwater Monitoring Report March 2024_20240430

GW-59A COMPLIANCE REPORT FORM Permit
(Submit one each monitoring period with GW-59 forms.)
# GJQ ©003bR$
1
Enter date monitoring results were due. ( ZO ) Will this monitoring report (GW-59
and GW-59A)
YES
NO
be submitted after the established due date.
\
2
Was any required information missing on the GW-59 report forms?
YES
NO
IF the answer to question I or 2 is "YES, list in the space provided below the well identification
umber(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing
cap, missing
YES
NO
identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Office for guidance.
X
4
Are any monitored constituents equal to or above the established standards?
YE
NO
If the answer to question 4 is "NO", skip to section 8.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and
oncentration(s)
exceeding standards in the space provided below.
5
For the constituents identified in question 4 above, have standards been exceeded previously
for the
YES
NO
same constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is "NO", skip to section 8.
If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s)
exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last
two years).
5-ee,
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
If the answer is "YES", a groundwater quality problem maybe occurring. CONTACT THE
REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly
located; contact the Regional Office.
j
II ,�,,
(Reloll al i CO Af z7�" L
7
Is the yermittee implemebting previously approved actions required by the Division involving
this
YES
NO
groundwater quality problem?
If the answer to question 7 is "YES, describe those actions in the space provided below.
If the answer to question 7 is "NO", contact the Regional Office within 90 days: an evaluation
may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility Failure to do so may subject the permittee to a Notice
of Violation,
fines, and/or penalties.
g
The person completing this portion (GW-59A) of the monitoring report should sign below
and submit this
form with G W-59 forms for required wells to the address provided at the top of the current
G W-59 form.
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rehsac. �teport G -v9...-B no
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GW-59A 12/8/2003

Question #4
LAB DATA WHICH EXCEEDS PERMIT
DATE
MONITORING WELL #
PARAMETER
REPORTED
DATA
3/27/2024
1
pH
5.9
Iron
318 ug/L
2
pH
6.4
Ammonia
5.6 mg/L
Iron
70,700 ug/L
Manganese
1,840 ug/L
3
pH
5.1
Cobalt
1.9
Iron
820 ug/L
Manganese
79.2 ug/L
4
pH
4.85.1
Cobalt
2.3 ug/L
Manganese
128 ug/L

QUESTION #5
LAB DATA WHICH EXCEEDS PERMIT FOR LAST 2 PREVIOUS (YEARS
2 ,02p2
1
pH
5.7
2
Ammonia
6.4 mg/L
Iron
43.9 mg/L
Manganese
1,200 ug/L
pH
6.3
3
Manganese
107 ug/L
4
pH
5.0
Manganese
172 ug/L
pH
5.0
1..3.. �2
1
pH
5.9
2
Ammonia
5.4 mg/L
Iron
27,100ug/L
Manganese
1,250 ug/L
pH
6.4
3
Cobalt
2.5 ug/L
Manganese
98.5 ug/L
pH
5.1
4
Manganese
86 ug/L
pH
4.9
.23 2�3
1
pH
5.9
2
Ammonia
5.9 mg/L
Cobalt
1.1 ug/L
Iron
50,400 ug/L
Manganese
1,310 ug/L
3
pH
5.2
Cobalt
2.2 ug/L
Manganese
70.6 ug/L
4
pH
5
Cobalt
3.3 ug/L
Manganese
126 ug/L
1
pH
5.9
2
pH
6.4
Ammonia
5.6 mg/L
Iron
42,200 ug/L
Manganese
1,530 ug/L
3
pH
5.1
Cobalt
2.8 ug/L
Iron
478 ug/L
Manganese
1 85.8 ug/L
Page 1

4
pH
5
Cobalt
3.0 ug/L
Manganese
124 ug/L
1
pH
5.6
Iron
464 ug/L
2
pH
6.4
Ammonia
4.2 mg/L
Iron
23, 900 ug/L
Manganese
1,490 ug/L
3
pH
5.2
Cobalt
2.4 ug/L
Manganese
85.2 ug/L
4
pH
4.8
Cobalt
2.4 ug/L
Manganese
123 ug/L
1
pH
5.9
Iron
318 ug/L
2
pH
6.4
Ammonia
5.6 mg/L
Iron
70,700 ug/L
Manganese
1,840 ug/L
3
pH
5.1
Cobalt
1.9
Iron
820 ug/L
Manganese
79.2 ug/L
4
pH
4.85.1
Cobalt
2.3 ug/L
Manganese
1 128 ug/L
Page 2

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�ceo
April 11, 2024
Mr. Tim Horton
City of Marion
3982 NC Hwy 226 South
Marion, NC 28752
RE: Project: City of Marion MWs March 2024
Pace Project No.: 92721756
Dear Mr. Horton:
Enclosed are the analytical results for sample(s) received by the laboratory on March 28, 2024. The
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC S
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories
• Pace Analytical Services -Asheville
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Jonathan W Biddix
[e-mail]
704-977-0978
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Its relate only to
ards and the
the Pace Network:
Page 1 of 22

ceo
Project: City of Marion MWs March 2024
Pace Project No.: 92721756
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 22

Pace Analytical Services, LLC
'ace" 2225 Riverside Dr.
Asheville, NC 2880404
[phone]
SAMPLE SUMMARY
Project:
City of Marion MWs March 2024
Pace Project No.:
92721756
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92721756001
MW-1R
Water
03/2712412:20
03/28/2410:15
92721756002
MW-2
Water
03/27/2413:40
03/28/2410:15
92721756003
MW-3
Water
03/27/2417:10
03/28/2410:15
92721756004
MW-4
Water
03/27/2418:00
03/28/2410:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 22

�ceW
SAMPLE ANALYTE COUNT
Project: City of Marion MWs March 2024
Pace Project No.: 92721756
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92721756001
MWA R
EPA 200.8 Rev 5.41994
CRW,
KRL
6
PASI-A
SM 4500-H+B-2011
SMS
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
4
PASI-A
EPA 350.1 Rev 2.0 1993
NCF
1
PASI-A
EPA 351.2 Rev 2.0 1993
M i0
1
PASI-A
EPA 353.2 Rev 2.0 1993
KDF1
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
92721756002
MW-2
EPA 200.8 Rev 5.4 1994
CRW,
KRL
6
PASI-A
SM 4500-H+B-2011
SMS
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
4
PASI-A
EPA 350.1 Rev 2.0 1993
NCF
1
PASI-A
EPA 351.2 Rev 2.0 1993
M i0
1
PASI-A
EPA 353.2 Rev 2.0 1993
KDF1
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
92721756003
MW-3
EPA 200.8 Rev 5.41994
CRW,I
KRL
6
PASI-A
SM 4500-H+B-2011
YEG
I
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
4
PASI-A
EPA 350.1 Rev 2.0 1993
NCF
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
KDF1
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
92721756004
MW-4
EPA 200.8 Rev 5.4 1994
CRW,I
KRL
6
PASI-A
SM 4500-H+B-2011
YEG
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
I
4
PASI-A
EPA 350.1 Rev 2.0 1993
NCF
1
PASI-A
EPA 351.2 Rev 2.0 1993
M
O
1
PASI-A
EPA 353.2 Rev 2.0 1993
KDF1
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 22

(-�Facep
Project: City of Marion MWs March 2024
Pace Project No.: 92721756
Sample: MW-1R
Parameters
200.8 MET ICPMS
Barium
Boron
Cadmium
Cobalt
Iron
Manganese
4500H+ pH, Electrometric
pH at 25 Degrees C
300.0 IC Anions 28 Days
Bromide
Chloride
Fluoride
Sulfate
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, N021NO3 unpres
Nitrogen, Nitrate
Nitrogen, Nitrite
SM4500P-E, Phosphate, Ortho
Orthophosphate as P
Date: 04/11/2024 04:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Lab ID: 92721756001 Collected: 03/27/24 12:20 Received: 03/28/24 10:15 Matrix: Water
Results Units PQL MDL
DF
Prepared
(Analyzed
CAS No.
Analytical Method: EPA 200.8 Rev 5.4 1994 Preparation
Method: EPA 200.8
Rev 5.4 1994
Pace Analytical Services - Asheville
35.4 ug/L 1.0 0.36
1
03/29/24 16:05
03/31/24
22:22 7440-39-3
ND ug/L 50.0 7.5
1
03/2912416:05
041,0112414:24
7440-42-8
ND ug/L 0.10 0.037
1
03/29/24 16:05
03/31/24 22:22 7440-43-9
ND ug/L 1.0 0.14
1
03/29/24 16:05
03/131/24 22:22 7440-48-4
318 ug/L 20.0 3.0
1
03/29/24 16:05
03/31/24 22:22 7439-89-6
9.3 ug/L 2.0 0.24
1
03/29/24 16:05
03/31/24 22:22 7439-96-5
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services - Asheville
6.2 Std. Units 0.10 0.10
1
04104/24
11:39
Analytical Method: EPA 300.0 Rev 2.1 1993
1
Pace Analytical Services - Asheville
ND mg/L 0.10 0.060
1
03/29/24
06:54 24959-67-9
ND mg/L 1.0 0.60
1
03/29/24 06:54 16887-00-6
ND mg/L 0.10 0.050
1
03/29/24 06:54 16984-48-8
ND mg/L 1.0 0.50
1
03/29/24 06:54 14808-79-8
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
ND mg/L 0.10 0.031
1
04/09/2415:51
7664-41-7
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2
Rev 2.01993
Pace Analytical Services - Asheville
ND mg/L 0.50 0.25
1
04/08/24 20:19
04/09/24
05:23 7727-37-9
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Qual
H3
0.048 mg/L 0.020 0.0039 1
03/29/24
09:14 14797-55-8
0.0014J mg/L 0.020 0.0012 1
03/29/24
09:14 14797-65-0 B
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Asheville
0.0191 mg/L 0.050 0.012 1
03/29/24
04:28
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 22

(-�Face"
Project: City of Marion MWs March 2024
Pace Project No.: 92721756
Sample: MW-2
Parameters
`Z1I111li'iI=ki[9;JJi69
Barium
Boron
Cadmium
Cobalt
Iron
Manganese
4500H+ pH, Electrometric
pH at 25 Degrees C
300.0 IC Anions 28 Days
Bromide
Chloride
Fluoride
Sulfate
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
Nitrogen, Nitrite
SM4500P-E, Phosphate, Ortho
Orthophosphate as P
Date: 04/11 /2024 04:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Lab ID: 92721756002 Collected: 03/27/24 13:40 Received: 03/28/2'4 10:15 Matrix: Water
Results Units PQL MDL
DF
Prepared
(Analyzed
CAS No.
Analytical Method: EPA 200.8 Rev 5.4 1994 Preparation
Method: EPA 200.8
Rev 5.4 1994
Pace Analytical Services - Asheville
73.3 ug/L 1.0 0.36
1
03/29/24 16:05
03/31/24
22:26 7440-39-3
46.3J ug/L 50.0 7.5
1
03129/2416:05
04/01/2414:27 7440-42-8
ND ug/L 0.10 0.037
1
03/29/24 16:05
03/31/24 22:26 7440-43-9
0.82.1 ug/L 1.0 0.14
1
03/29/24 16:05
03/31 /24 22:26 7440-48-4
70700 ug/L 200 29.8
10
03/29/24 16:05
04/01/2414:31 7439-89-6
1840 ug/L 20.0 2.4
10
03/29/24 16:05
04/01 /24 14:31 7439-96-5
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services - Asheville
6.4 Std. Units 0.10 0.10
1
04/04/24
11:46
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
0.080.11 mg/L 0.10 0.060
1
03/29/24 07:09 24959-67-9
2.2 mg/L 1.0 0.60
1
03/29/24 07:09 16887-00-6
0.062J mg/L 0.10 0.050
1
03/29/24 07:09 16984-48-8
0.93J mg/L 1.0 0.50
1
03/29/24 07:09 14808-79-8
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
6.6 mg/L 0.10 0.031
1
04/09/2415:52
7664-41-7
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2
Rev 2.0 1993
Pace Analytical Services - Asheville
6.8 mg/L 0.50 0.25
1
04/08/24 20:19
04/09/24
05:24 7727-37-9
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Qual
H3
0.013J mg/L 0.020 0.0039 1 03/29/24 09:21 14797-55-8
0.0016J mg/L 0.020 0.0012 1 03/29/24 09:21 14797-65-0 B
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Asheville
ND mg/L 0.050 0.012 1 03/29/24 04:28
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 22

ace"
Project: City of Marion MWs March 2024
Pace Project No.: 92721756
Sample: MW-3
Parameters
200.8 MET ICPMS
Barium
Boron
Cadmium
Cobalt
Iron
Manganese
4500H+ pH, Electrometric
pH at 25 Degrees C
300.0 IC Anions 28 Days
Bromide
Chloride
Fluoride
Sulfate
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, N021NO3 unpres
Nitrogen, Nitrate
Nitrogen, Nitrite
SM4500P-E, Phosphate, Ortho
Orthophosphate as P
Date: 04/11/2024 04:09 PM
ANALYTICAL RESULTS
Lab ID: 92721766003 Collected: 03/27/24 17:10 Received:
Results Units PQL MDL DF Prepared
Analytical Method: EPA 200.8 Rev 5.4 1994 Preparation Method: EPA 200.8
Pace Analytical Services - Asheville
414 ug/L 3.0
1.1
3
03/29/2416:05
04)
ND ug/L 50.0
7.5
1
03/29/2416:05
04)
0.61 ug/L 0.10
0.037
1
03/29/2416:05
03)
1.9 ug/L 1.0
0.14
1
03/29/2416:05
03)
820 ug/L 20.0
3.0
1
03/29/2416:05
03)
79.2 ug/L 2.0
0.24
1
03/29/2416:05
031
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services - Asheville
5.6 Std. Units 0.10
0.10
1
04)
Analytical Method: EPA 300.0 Rev 2.1
1993
Pace Analytical Services - Asheville
0.097.1 mg/L 0,10
0.060
1
0&
7.6 mg/L 1.0
0.60
1
03J
ND mg/L 0.10
0.050
1
031
ND mg/L 1.0
0.50
1
03)
Analytical Method: EPA 350.1 Rev 2.0
1993
Pace Analytical Services - Asheville
ND mg/L 0.10
0.031
1
04i
Analytical Method: EPA 351.2 Rev 2.0
1993 Preparation
Method: EPA 351.2
Pace Analytical Services -Asheville
ND mg/L 0.50
0.25
1
04/08/24 20:19
041
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services - Asheville
7.1 mg/L 0.10
0.020
5
031
0.0026.1 mg/L 0.020
0.0012
1
031
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Asheville
0.014.1 mg/L 0.050
0.012
1
031
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
10:15 Matrix: Water
CAS No. Qual
5.41994
/2414:39 7440-39-3
/2414:35 7440-42-8
/24 22:30 7440-43-9
/24 22:30 7440-48-4
/24 22:30 7439-89-6
/24 22:30 7439-96-5
t 15:03 H3
t 07:53 24959-67-9
t 07:53 16887-00-6
t 07:53 16984-48-8
t 07:53 14808-79-8
t 15:56 7664-41-7
2.01993
t 05:25 7727-37-9
t 10:39 14797-55-8
t 09:29 14797-65-0 B
t 04:29
Page 7 of 22

(-�Faceo
ANALYTICAL RESULTS
Project: City of Marion MWs March 2024
Pace Project No.: 92721756
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW-4
Lab ID: 92721756004 Collected:
03/27/24 18:00
Received: 03/28/24
10:15 Matrix: Water
Parameters
Results Units PQL
MDL
DF
Prepared
Analyzed CAS No. Qua[
200.8 MET ICPMS
Analytical Method: EPA 200.8 Rev 5.4
1994 Preparation Method: EPA 200.8
Rev 5.4 1994
Pace Analytical Services - Asheville
Barium
61.0 ug/L 1.0
0.36
1
03/29/24 16:05
03/31/24
22:34 7440-39-3
Boron
ND ug/L 50.0
7.5
1
03129/2416:05
04/01/2414:43
7440-42-8
Cadmium
0.10 ug/L 0.10
0.037
1
03/29/24 16:05
03/31/24
22:34 7440-43-9
Cobalt
2.3 ug/L 1.0
0.14
1
03/29/24 16:05
03/31/24
22:34 7440-48-4
Iron
64.8 ug/L 20.0
3.0
1
03/29/24 16:05
03/31/24
22:34 7439-89-6
Manganese
128 ug/L 2.0
0.24
1
03/29/24 16:05
03/31/24
22:34 7439-96-5
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services -Asheville
pH at 25 Degrees C
5.9 Std. Units 0.10
0.10
1
04/08/24
15:07 H3
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1
1993
Pace Analytical Services -Asheville
Bromide
0.16 mg/L 0.10
0.060
1
03/29/24
08:08 24959-67-9
Chloride
2.3 mg/L 1.0
0.60
1
03/29/24
08:08 16887-00-6
Fluoride
ND mg/L 0.10
0.050
1
03/29/24
08:08 16984-48-8
Sulfate
ND mg/L 1.0
0.50
1
03/29/24
08:08 14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg/L 0.10
0.031
1
04/09/24
15:58 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0
1993 Preparation
Method: EPA 351.2
Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Kjeldahl, Total
ND mg/L 0.50
0.25
1
04/08/24 20:19
04/09/24
05:28 7727-37-9
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services - Asheville
Nitrogen, Nitrate
Nitrogen, Nitrite
SM4500P-E, Phosphate, Ortho
Orthophosphate as P
Date: 04/11 /2024 04:09 PM
1.4 mg/L 0.020 0.0039 1 03/29/24 09:31 14797-55-8
0.0031J mg/L 0.020 0.0012 1 03/29/24 09:31 14797-65-0 B
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
0.017J mg/L 0.050 0.012 1 03/29/24 04:29
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 22

ace°
QUALITY CONTROL DATA
Project: City of Marion MWs March 2024
Pace Project No.: 92721756
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QC Batch: 842943
Analysis Method: EPA 200.8 Rev 5.4 1994
QC Batch Method: EPA 200.8 Rev 5.4
1994
Analysis Description: 200.8 MET
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples:
92721756001, 92721756002,
92721756003, 92721756004
METHOD BLANK: 4353368
Matrix: Water
Associated Lab Samples:
92721756001, 92721756002, 92721756003, 92721756004
Blank Reporting
Parameter
Units
Result Limit MDL
Analyzed
Qualifiers
Barium
ug/L
ND 1.0
0.36 03/31/24 20:14
Boron
ug/L
ND 50.0
7.5 03/31/24 20:14
Cadmium
ug/L
ND 0.10 0.037 03/31/2�4 20:14
Cobalt
ug/L
ND 1.0
0.14 03/31/24 20:14
Iron
ug/L
3.3J 20.0
3.0 03/31/24 20:14
Manganese
ug/L
ND 2.0
0.24 03/31/24 20:14
I
LABORATORY CONTROL SAMPLE:
4353369
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits
Qualifiers
Barium
ug/L
50 50.3 101
85-115
Boron
ug/L
50 51.1 102
85-115
Cadmium
ug/L
50 51.4 103
85-115
Cobalt
ug/L
50 52.2 104
85-115
Iron
ug/L
1250 1310 105
85-115
Manganese
ug/L
50 51.5 103
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4353395 4353396
MS MSD
92721431001
Spike Spike MS MSD
MS MSD
% Rec
Max
Parameter
Units
Result
Conc. Conc. Result Result
% Rec % Rec
Limits
RPD
RPD Qua]
Barium
ug/L
ND
50 50 52.0 50.7
104
101 70-130
3
20
Boron
ug/L
ND
50 50 52.6 53.0
104
105 70-130
1
20
Cadmium
ug/L
ND
50 50 52.3 52.2
105
104 70-130
0
20
Cobalt
ug/L
ND
50 50 52.6 52.4
105
105 70-130
0
20
Iron
ug/L
ND
1250 1250 1330 1300
106
103 70-130
2
20
Manganese
ug/L
ND
50 50 52.5 52.0
105
104 70-130
1
20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4353609 4353610
MS MSD
92721792003
Spike Spike MS MSD
MS MSD
% Rec
Max
Parameter
Units
Result
Conc. Conc. Result Result
% Rec % Rec
Limits
RPD
RPD Qual
Barium
ug/L
11.8
50 50 62.3 63.8
101
104 70-130
2
20
Boron
ug/L
ND
50 50 68.0 66.6
107
104 70-130
2
20
Cadmium
ug/L
0.10
50 50 53.0 52.2
106
104 70-130
2
20
Cobalt
ug/L
ND
50 50 53.7 53.5
107
107 70-130
0
20
Results presented on this page are in the units
indicated by the "Units" column except where an alternate unit is presented
to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/11 /2024 04:09 PM
without the written consent of Pace Analytical Services, LLC.
Page 9 of 22

ace"
QUALITY CONTROL DATA
Project: City of Marion MWs March 2024
Pace Project No.: 92721756
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4353609
MS
92721792003 Spike
Parameter Units Result Conc.
Iron ug/L 175 1250
Manganese ug/L 7.6 50
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
4353610
MSD
Spike
MS
MSD
MS MSD
% Rec
Max
Conc.
Result
Result
% Rec % Rec
Limits
RPD RPD Qual
1250
1470
1470
104
104
70-130
0 20
50
60.2
60.8
105
106
70-130
1 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/11/2024 04:09 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 22

Pace Analytical Services, LLC
2225 Riverside Dr.
ace" Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: City of Marion MWs March 2024
Pace Project No.: 92721756
QC Batch: 844278 Analysis Method: SM 4500-H+B-2011
QC Batch Method: SM 4500-H+B-2011 Analysis Description: 4500H+B pH
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92721756001, 92721756002
SAMPLE DUPLICATE: 4360265
92721756002 Dup Max
Parameter Units Result Result RPD RPDi Qualifiers
pH at 25 Degrees C Std. Units 6.4 6.5 1 10 H3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/11 /2024 04:09 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 22

Project: City of Marion MWs March 2024
Pace Project No.: 92721756
QC Batch: 845079
QC Batch Method: SM 4500-H+B-2011
Associated Lab Samples: 92721756003, 92721756004
SAMPLE DUPLICATE: 4364066
Parameter Units
pH at 25 Degrees C Std. Units
SAMPLE DUPLICATE: 4364067
Parameter
pH at 25 Degrees C
QUALITY CONTROL DATA
Analysis Method: SM 4500-H+B-2011
Analysis Description: 4500H+B pH
Laboratory: Pace Analytical Services -
92721761001 Dup M
Result Result RPD RI
7.0 7.5 8
92721780001 Dup
Units Result Result
Std. Units 7.5 7.5
RPD
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/11/2024 04:09 PM without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Qualifiers
10 D6,H3
Qualifiers
10 H3
the right of the result
Page 12 of 22

i
Pace Analytical
Services, LLC
Vaceo
2225 Riverside Dr.
Asheville,
NC 28804
[phone]
QUALITY CONTROL DATA
Project: City of Marion MWs March 2024
Pace Project No.: 92721756
QC Batch: 842670
Analysis Method: EPA 300.0 Rev 2.1 1993
QC Batch Method: EPA 300.0 Rev 2.1
1993
Analysis Description: 300.0 IC Anions
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92721756001, 92721756002, 92721756003, 92721756004
METHOD BLANK: 4352228
Matrix: Water
Associated Lab Samples: 92721756001, 92721756002, 92721756003, 92721756004
Blank Reporting
Parameter
Units
Result Limit MDL Analyzed
Qualifiers
Bromide
mg/L
ND 0.10 0.060 03/28/2 i4
21:45
Chloride
mg/L
ND 1.0 0.60 03/28/24
21:45
Fluoride
mg/L
ND 0.10 0.050 03/28/24
21:45
Sulfate
mg/L
ND 1.0 0.50 03/28/24
21:45
LABORATORY CONTROL SAMPLE:
4352229
Spike LCS LCS % Rec
j
Parameter
Units
Conc. Result % Rec Limits
Qualifiers
Bromide
mg/L
2.5 2.3 92 90-110
Chloride
mg/L
50 49.9 100 90-110
Fluoride
mg/L
2.5 2.4 98 90-110
Sulfate
mg/L
50 49.8 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4352230 4352231
MS MSD
92721739001
Spike Spike MS MSD MS MS,D
% Rec
Max
Parameter Units
Result
Conc. Conc. Result Result % Rec %Rec
Limits
RPD
RPD Qual
Bromide mg/L
ND
2.5 2.5 2.4 2.4 94
97 90-110
2
10
Chloride mg/L
1.8
50 50 51.6 52.8 99
102 90-110
2
10
Fluoride mg/L
ND
2.5 2.5 2.7 2.9 107
116 90-110
8
10 M1
Sulfate mg/L
ND
50 50 49.7 51.0 99
102 90-110
3
10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4352232 4352233
MS MSD
92721756002
Spike Spike MS MSD MS MSD
% Rec
Max
Parameter Units
Result
Conc. Conc. Result Result % Rec % Rec
Limits
RPD
RPD Qua[
Bromide mg/L
0.080J
2.5 2.5 2.5 2.6 96
102 90-110
5
10
Chloride mg/L
2.2
50 50 51.8 54.0 99
104 90-110
4
10
Fluoride mg/L
0.062J
2.5 2.5 2.4 2.5 94
99 90-110
6
10
Sulfate mg/L
0.93J
50 50 51.0 53.3 100
105 90-110
4
10
Results presented on this page are in the units
indicated by the "Units" column except where an alternate unit is presented
I
i
to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/11/2024 04:09 PM
without the written consent of Pace Analytical Services, LLC.
Page 13 of 2;

Pace Analytical ServicesLLC
lAlace-
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: City of Marion MWs March 2024
Pace Project No.: 92721756
QC Batch: 845250 Analysis Method: EPA 350.1 Rev 2.0 1993
QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92721756001, 92721756002, 92721756003, 92721756004
METHOD BLANK: 4364637 Matrix: Water
Associated Lab Samples: 92721756001, 92721756002, 92721756003, 92721756004
Blank Reporting
Parameter Units Result Limit MDL Analyzed
Qualifiers
Nitrogen, Ammonia mg/L ND 0.10 0.031 04/09/2
115:14
LABORATORY CONTROL SAMPLE: 4364638
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits
Qualifiers
Nitrogen, Ammonia mg/L 5 5.1 102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4364639 4364640
MS MSD
92722665003 Spike Spike MS MSD MS MID
% Rec Max
Parameter Units Result Cone. Cone. Result Result % Rec % Rec
Limits RPD RPD Qual
105 90-110 1 10
Nitrogen, Ammonia mg/L ND 5 5 5.3 5.3 106
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4364641 4364642
MS MSD
92721286008 Spike Spike MS MSD MS MSD
% Rec Max
Parameter Units Result Cone. Cone. Result Result % Rec % Rec
Limits RPD RPD Qual
81 90-110 4 10 M1
I
Nitrogen, Ammonia mg/L 202 5 5 198 206 -76
Results presented on this page are in the units indicated by the "Units" column exceptwhere an alternate unit is presented
to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/11/2024 04:09 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 2:

Pace Analytical Services, LLC
2225 Riverside Dr.
ace
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: City of Marion MWs March 2024
Pace Project No.: 92721756
QC Batch: 845172 Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92721756001, 92721756002, 92721756003, 92721756004
METHOD BLANK: 4364338 Matrix: Water
Associated Lab Samples: 92721756001, 92721756002, 92721756003, 92721756004
Blank Reporting
Parameter Units Result Limit MDL Analyzed
Qualifiers
Nitrogen, Kjeldahl, Total mg/L ND 0.50 0.25 04/09/24105:12
LABORATORY CONTROL SAMPLE: 4364339
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits
Qualifiers
Nitrogen, Kjeldahl, Total mg/L 10 10.0 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4364340 4364341
MS MSD
92721766003 Spike Spike MS MSD MS MSD
% Rec Max
Parameter Units Result Cone. Cone. Result Result % Rec % Rec
Limits RPD RPD Qual
Nitrogen, Kjeldahl, Total mg/L ND 10 10 9.9 10.4 97
102 90-110 5 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4364342 4364343
MS MSD
92721756004 Spike Spike MS MSD MS MSD
% Rec Max
Parameter Units Result Cone. Cone. Result Result % Rec % Rec
Limits RPD RPD Qua]
Nitrogen, Kjeldahl, Total mg/L ND 10 10 10.9 10.5 109
105 90-110 4 10
Results presented on this page are in the units indicated by the "Units" column exceptwhere an alternate unit is presented t
the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/11/2024 04:09 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of Z

Pace Analytical Services, LLC
2225 Riverside Dr.
ace@
Asheville, NC 28804
I
[phone]
QUALITY CONTROL DATA
Project: City of Marion MWs March 2024
Pace Project No.: 92721756
QC Batch: 842744 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpre
.
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92721756001, 92721756002, 92721756003, 92721756004
METHOD BLANK: 4352544 Matrix: Water
Associated Lab Samples: 92721756001, 92721756002, 92721756003, 92721756004
Blank Reporting
Parameter Units Result Limit MDL Analyzed
Qualifiers
Nitrogen, Nitrate mg/L ND 0.020 0.0039 03/29/24
08:44
Nitrogen, Nitrite mg/L 0.0024J 0.020 0.0012 03/29/24
08:44
LABORATORY CONTROL SAMPLE: 4352545 1
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits
Qualifiers
Nitrogen, Nitrate mg/L 1.5 1.5 98 90-110
Nitrogen, Nitrite mg/L 1 0.97 97 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4352546 4352547
MS MSD
92721739002 Spike Spike MS MSD MS MSD
% Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec
Limits RPD RPD Qual
Nitrogen, Nitrate mg/L ND 1.5 1.5 1.5 1.5 101
100 90-110 2 10
Nitrogen, Nitrite mg/L ND 1 1 1.1 1.1 108
109 90 110 0 10 1-11
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4352548 4352549
MS MSD
92721739001 Spike Spike MS MSD MS MSD
% Rec Max
Parameter Units Result Conc.Conc. Result Result % Rec % Rec
Limits RPD RPD Qual
Nitrogen, Nitrate mg/L ND 1.5 1.5 1.6 1.5 105
101 90-110 3 10
Nitrogen, Nitrite mg/L ND 1 1 1.1 1.1 107
109 90-110 1 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to
the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/11/2024 04:09 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 2;
'ICI

�ce"
QUALITY CONTROL DATA
Project: City of Marion MWs March 2024
Pace Project No.: 92721756
QC Batch: 842763 Analysis Method: SM 4500-P E-2011
QC Batch Method: SM 4500-P E-2011 Analysis Description: SM450OP-E Phosphorus, Ortho
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92721756001, 92721756002, 92721756003, 92721756004
METHOD BLANK: 4352607 Matrix: Water
Associated Lab Samples: 92721756001, 92721756002, 92721756003, 92721756004
Blank Reporting
Parameter Units Result Limit MDL Analyzed
Orthophosphate as P mg/L ND 0.050 0.012 03/29/24 04:26
LABORATORY CONTROL SAMPLE & LCSD: 4352608
Parameter Units
Orthophosphate as P mg/L
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Qualifiers
4352609
Spike LCS LCSD LCS LCSD % Red Max
Cone. Result Result % Rec % Rec Limits RPD RPD Qualifiers
0.25 0.24 0.25 97 102 90-110 4 10
Results presorted on this page are in the units indicated by the "Units" column except where an alternate unit is
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/11/2024 04:09 PM without the written consent of Pace Analytical Services, LLC.
to the right of the result
Page 17 of 22

�ceo
QUALIFIERS
Project: City of Marion MWs March 2024
Pace Project No.: 92721756
DEFINITIONS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL -Reporting Limit -The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
'Total' may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
B Analyte was detected in the associated method blank.
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H1 Analysis conducted outside the EPA method holding time.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/11 /2024 04:09 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 22

it
l Pace Analytical Services, LLC
/1 / 2225 Riverside Dr.
(-�Fa
1 _ G� Asheville, NC 28804
V [phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: City of Marion MWs March 2024
Pace Project No.: 92721756
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92721756001 MWA R EPA 200.8 Rev 5.4 1994 842943 EPA 200.8 Rev 5.41994 843029
92721756002 MW-2 EPA 200.8 Rev 5.4 1994 842943 EPA 200.8 Rev 5.41994 843029
92721756003 MW-3 EPA 200.8 Rev 5.4 1994 842943 EPA 200.8 Rev 5.41994 843029
92721756004 MW-4 EPA 200.8 Rev 5.4 1994 842943 EPA 200.8 Rev 5.4 1994 843029
92721756001 MW-1R SM 4500-H+B-2011 844278
92721756002 MW-2 SM 4500-H+6-2011 844278
92721756003 MW-3 SM 4500-H+B-2011 845079
92721756004 MW-4 SM 4500-H+B-2011 845079
92721756001 MWA R EPA 300.0 Rev 2.1 1993 842670
92721756002 MW-2 EPA 300.0 Rev 2.1 1993 842670 1
92721756003 MW-3 EPA 300.0 Rev 2.1 1993 842670
92721756004 MW-4. EPA 300.0 Rev 2.1 1993 842670
92721756001 MWA R EPA 350.1 Rev 2.0 1993 845250
92721756002 MW-2 EPA 350.1 Rev 2.0 1993 845250
92721756003 MW-3 EPA 350.1 Rev 2.0 1993 845250
92721756004 MW-4 EPA 350.1 Rev 2.0 1993 845250
92721756001 MWA R EPA 351.2 Rev 2.0 1993 845172 EPA 351.2 Rev 2.0 1993 845339
92721756002 MW-2 EPA 351.2 Rev 2.0 1993 845172 EPA 351.2 Rev 2.0 1993 845339
92721756003 MW-3 EPA 351.2 Rev 2.0 1993 845172 EPA 351.2 Rev 2.0 1993 845339
92721756004 MW-4 EPA 351.2 Rev 2.0 1993 845172 EPA 351.2 Rev 2.0 1993 845339
92721756001 MWA R EPA 353.2 Rev 2.0 1993 842744
92721756002 MW-2 EPA 353.2 Rev 2.0 1993 842744
92721756003 MW-3 EPA 353.2 Rev 2.0 1993 842744
92721756004 MW-4 EPA 353.2 Rev 2.0 1993 842744
92721756001 MWA R SM 4500-P E-2011 842763
92721756002 MW-2 SM 4500-P E-2011 842763
92721756003 MW-3 SM 4500-P E-2011 842763
92721756004 MW-4 SM 4500-P E-2011 842763
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/11/2024 04:09 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 22

:--��ace DC#_Title: ENV-FRM-HUN1-0083 v03 Sample Condition Upon Receipt
I Effective Date: 11/29/2023 4:16:30 PM
Laboratory receiving samples:
Asheville Eden❑ Greenwood ❑ Huntersville // Raleigh❑ Mechanicsville❑ Atlanta[] Kernersvillp l
ConditionSample Client Name: 1 lO# : 912721?%,6
• • � Project #: w r
Courier. / Fed Ex UPS U USPS Client IL'II' II (III' II'I'I'II
❑ Commercial ❑ Pace ❑ Other:
927217SS
Custody Seal Present? ❑Yes � No Seals Intact? ❑Yes E,-� I ❑ ❑No L'JN/A -/
Date/Initials Pe son Examining Contents^ _
Packing Material: ❑ Bubble Wrap ❑Bubble Bags None ❑ Other Bielogical Tissue
Thermometer: _ ❑ Yes ❑ la No N/A
IR Gun ID: Type of ice: Owet ❑Blue ❑None
Correction Factor:
Cooler Temp: f Add/Subtract (°C) Temp should be above freezing to 6°C
i❑Samplesoutoftemp criteria. Samples onice, cooling process
Cooler Temp Corrected (*Q ( has begun
USDA. Regulated Soil ( ff N/A, water sample)
Did samples originate in a gdzarantine zone within the United States: CA, NY, or SC Did samples originate from a foreign source (internationally,
irhar4 mandi l_i Vac ran inrludino Hawaii and Plinrtn WrM7 M Voc 171IU-n
Comments/Discrepancy:
Chain of Custody Present?
�
QY es
❑ No
❑ N/A
1.
Samples Arrived within Hold Time?
Yes
❑ No
❑ N/A
2.
Short Hold Time Analysis (<72 hr.)?
C=1 Yes
❑ No
❑ N/A
3.
Rush Turn Around Time Requested?
❑ Yes
Z No
❑ N/A
4.
Sufficient Volume?
ZYes
❑ No
❑ NIA
5.
Correct Containers Used?
-Pace Containers Used?
es
�' s
[I No
❑ No
❑N/A
❑ N/A
6.
Containers Intact?
Yes
❑ No
❑ N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
❑No
/A
B.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
®'Yes
❑ No
❑ N/A
9.
Headspace in VOA Vials (>5-6mm)?
❑Yes
❑No
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
OYes
❑Yes
❑ No
❑No
QXIA
N/A
11.
COMMENTS/SAMPLE DISCREPANCY
Data Required? ❑ Yes ❑ No
I
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
I
Person contacted: Date/Time:
i
i
Project Manager SCURF Review: Date: i
Project Manager SRF Review: Date:
I
i
I
Qualtrax ID: 69614 Paae 1 Of 2
Page 20 of 22

Effective Date: 11/14/2022
9272 Z 756
*Check mark top half of box if pH and/or dechlorination is verified and Project l# WOE :
within the acceptance range for preservation samples. PM: JWB
Exceptions: VOA, Coliform, TOC, Oil and Grease, DAOI8015 jvoater) DOC. LLHg
CLIENT: 93-MARION
Due Dater 04/11/24
"Bottom half of box is to list number of bottles
• **Check all unpreserved Nitrates for chlorine
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Note. wnenever there is a discrepancy attesting PI or III Carolina compliance simples. a copy of this farm will be sent to the r4arth Carolina DEN Ft Certdication Office. (i L.
Out of hold, incorrect pre6ervotive, out of temp, incorrect containers.
Qualtrax I0:6961 l
Page 2 of 2
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;gate issued Mar, s
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