NC0083887_Report_20240715 (2)

NX Is I )
July 5, 2024
Mr. Jimmy D. Jordan, LG
Environmental Manager
Charlotte Douglas International Airport
5601 Wilkinson Boulevard
Charlotte, North Carolina 28208
Subject: Surface Water Sampling and Analysis Report (Second Quarter)
Former U.S. Airways Maintenance Hangar
NCDEQ UST Section Incident No. 14908
5020 Hangar Road
Charlotte, North Carolina
WSP Project: 6228-24-0007
Dear Mr. Jordan:
WSP USA Environment & Infrastructure Inc. (WSP) is pleased to submit this Surface Water Sampling and Analysis
Report for the above -referenced property in Charlotte, North Carolina. Included in this report is an outline of our
understanding of the project background, description of the sampling activities and results.
Project Background
U.S. Airways, Inc. (U.S. Airways) previously operated an aircraft jet fuel defueling/refueling system at the former
U.S. Airways Maintenance Hangar located at 5020 Hangar Road in Charlotte, North Carolina. The site is located in
the southwest portion of the Charlotte/Douglas International Airport property (Tax Parcel ID 115-211-05).
American Airlines (formerly U.S. Airways) currently leases the maintenance hangar facility from the City of
Charlotte and performs aircraft maintenance at the property. A 1995 release of petroleum occurred at the hangar
location. In December 2018, CLT personnel observed evidence of petroleum seepage from the bank of Coffey
Creek approximately 800 feet north of contaminant source area (Figure 1).
In email correspondence, dated May 13, 2021, Mr. James McDorman informed WSP personnel that Mr. Wes Bell
of the North Carolina Department of Environmental Quality (NCDEQ), Division of Water Resources (DWR)
requested performance of quarterly surface water sampling and analysis of Coffey Creek to assess whether
dissolved petroleum hydrocarbons are present in the stream.
Surface Water Sampling and Analysis
On June 3, 2024, WSP personnel collected one surface water sample (SW-1) from Coffey Creek. The sample was
collected using a stainless -steel cup attached to a stainless -steel rod. This device allows for the water sample to be
dipped from near the center of the stream by the sampler. The sampling cup was decontaminated prior to use by
rinsing with isopropyl alcohol, followed by distilled water.
WSP USA Environment & Infrastructure Solutions Inc.
1001 Morehead Square Drive, Suite 610
Charlotte, North Carolina 28203
NC Geology License: C-247
T: 704-417-5152

Surface Water Sampling and Analysis Report
Former U.S. Airways Maintenance Hangar
WSP Project: 6228-24-0007
July 5, 2024
Sample SW-1 was collected approximately 20 feet downstream of the last petroleum absorbent boom. The
location is shown on Figure 1. The collected sample was poured into laboratory -provided containers with
appropriate preservatives. The sample containers were placed in an ice -filled sample cooler and delivered to
Waypoint Analytical, LLC (Waypoint) in Charlotte, North Carolina for analysis. The sample was maintained under
chain -of -custody protocol. The laboratory analyzed the surface water sample for volatile organic compounds
(VOCs) by EPA Method 6200B including MTBE and semi -volatile organic compounds (SVOCs) by EPA Method
625.1.
Results
The results of the analysis of sample SW-1 identified no detectable concentrations of contaminants of concern. A
table summarizing the current and historical results and the laboratory report are attached. The next surface water
sampling event is planned for September 2024.
Closing
We appreciate your selection of WSP for this project and look forward to assisting you further on this project. If
you have questions, please contact us.
Sincerely,
WSP USA Environment & Infrastructure Inc.
James A Henderson Robert C. Foster, L.G.
Entry Environmental Engineer Geologist
Registered, NC #1335
Cc: Mr. Wes Bell, Senior Environmental Specialist, NCDEQ Division of Water Res©urce���
Mr. Dan Bowser, LG, Hydrogeologist, NCDEQ-DWM; UST Section
1335 '
;
Enclosures

Surface Water Sampling and Analysis Report
Former U.S. Airways Maintenance Hangar
WSP Project: 6228-24-0007
TABLE
July 5, 2024

Table 1
Summary of Surface Water Analytical Results
Charlotte Douglas International Airport
Former U.S. Airways Maintenance Hangar
WSP Project No. 6228-24-0007
SVOCs by EPA 625.1
INN
1. concentrations shown in micrograms Per liter (Pg/B
< value represents no laboraxory dttettion above the Beporting Limit
3. Bold values exceetletl North Carolina 15A 2B Water Quality S[andaMs or Surface Wa[ers (NC 2B) /NortM1 Carolire In -Stream Target Values, July 2021
4. If the NC 2B StandaM was not ertablizned for a mnsbtuent Nortn Carolina In -Stream target Values were usetl in place
B. NE =Not Establisnetl
, NB = Not Reported
].' =15A NCAC 2B antl NortM1 Carolina In -Stream Target Values Frefi Water Aquatic Life values were �wt listeq 15A NCAC 2B Human Heabn values for total PAHs
8. VOCs =volatile Organic CompouiMs
t 0.1=1-Rag, value was deteaed above N,etnod Qetenion Hmit (Mo4 but below raetnod 4uantnation Limb (raQy and is considered an estimate

Surface Water Sampling and Analysis Report
Former U.S. Airways Maintenance Hangar
WSP Project: 6228-24-0007
FIGURE
July 5, 2024

Former Oil Seep Location
Legend
9` groundwater monitor) e
F^
Approximate location of
;�� .. BMW-8,:. ,. � �� MW-6 `•"''`��+,a1�li� '4 � gro monitoring well
Sample Location
Approximateface Water
.... ri
F f f l Creeks/Streams
16
t t f { 4 M W 1
;`.,. ti
MW-5
.. L
WAN
Free Product
.. - ,.✓;?'fir � ..
' , 1
x
*�h � Recov ank I� r
AJAR"
PMW 17
.01
r RW-4
�1RW-5 RW-7
0 75 150
""%,, Feet
PMW-12 -•-*
1 inch = 150 feet
y
FORMER US AIRWAYS
Y + MAINTENANCE HANGAR
i FA r e Greensba
At If 0
North
Carolim
,:; i reenville aC�
A. > Service A16Layer Credits: Mecklenburg County GIS Aerial Imagery 202�2
A1% Columbia
Title: Date: Projection: Figure:
" WSP USA 1/18/2024
Environment &Infrastructure Inc. SITE PLAN NC State Plane (NAD83, feet)
Note: This map is for FORMER U.S. AIRWAYS
2801 Yorkmont Road, Suite 100 reference only. MAINTENANCE HANGAR Project No: File:
Charlotte, NC 28208
[phone] CHARLOTTE, NORTH CAROLINA 6228-24-0007 UMant.Hngarr\13GIS\WorkLinga\WorkngDataaprx 2Da12021\6228-21-0061
AA
Esri, TomTom, Garmin, FAO, NOAA, USGS, EPA, USFWS, Esri, USGS 2021 Drawn hv- KNS - Checked hv, RCF - Date, 1 /1 R/2024

Surface Water Sampling and Analysis Report
Former U.S. Airways Maintenance Hangar
WSP Project: 6228-24-0007
ATTACHMENT
LABORATORY ANALYTICAL REPORT AND CHAIN -OF -CUSTODY FORM
July 5, 2024

Waypointo
ANALYTICAL
6/19/2024
WSP USA Envi. & Infrastructure Inc. (Charlotte)
Rob Foster
2801 Yorkmont Rd. #100
Charlotte, NC, 28208
Ref: Analytical Testing
Lab Report Number: 24-155-0001
Client Project Description: CDIA-Coffey Creek
Project #6228-21-0061.09
Dear Rob Foster:
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Waypoint Analytical, LLC (Charlotte) received sample(s) on 6/3/2024 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 33

Waypoint.0
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State
Program
Lab ID
Expiration Date
North Carolina
State Program
37735
07/31/2024
North Carolina
State Program
402
12/31/2024
South Carolina
State Program
99012
07/31/2024
South Carolina
State Program
99012
12/31/2024
Page 1 of 1 00016/24-155-0001
Page 2 of 33

Waypoint. (2)
449 Springbrook
Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL
www.waypointana lyti ca I som
Sample Summary
Table
Report Number: 24-155-0001
Client Project Description: CDIA-Coffey Creek
Project #6228-21-0061.09
Lab No Client Sample ID Matrix
Date Collected
Date Received Method Lab ID
94697 Sw-1 Aqueous
06/03/2024 11:20
06/03/2024 11:48 6200B
94697 Sw-1 Aqueous
06/03/2024 11:20
06/03/2024 11:48
Pace Analytical - Huntersville, NC, Huntersville, NC
Page 3 of 33

Waypoint.(2)
ANALYTICAL
Project:
Report Number:
CDIA-Coffey Creek
24-155-0001
Client Sample ID Lab Sample ID
Method Parameters
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
Summary of Detected
www.waypointana lytica Isom
Result Units Report Limit Analyzed Qualifiers
No Analytes Detected
Page 4 of 33

Waypointo
ANALYTICAL
Client: WSP USA Envi. & Infrastructure Inc. (Charlotte)
Project: CDIA-Coffey Creek
Lab Report Number: 24-155-0001
Date: 6/19/2024
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
CASE NARRATIVE
625.1 - Base/Neutrals and Acids by GC/MS Method 625.1
Analyte: Benzidine
QC Batch No: V48295/V48269
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: Benzidine
QC Batch No: V48295/V48269
This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this
analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for
a low bias.
Analyte: Chrysene
QC Batch No: V48295/V48269
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: Dibenz(a,h)anthracene
QC Batch No: V48295/V48269
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Page 5 of 33

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01223
WSP USA Envi. & Infrastructure Inc. (Charlotte) Project CDIA-Coffey Creek
Rob Foster
2801 Yorkmont Rd. #100 Information : Project #6228-21-0061.09
Charlotte , NC 28208
Report Date : 06/19/2024
Received : 06/03/2024
Report Number : 24-155-0001 REPOR T OF A NA L YSIS
Lab No : 94697 Matrix: Aqueous
Sample ID: SW-1 Sampled: 6/3/2024 11:20
Analytical Method: 625.1
Prep Method: 625.1 (Prep)
Test Results
1,2-Diphenylhydrazine/Azobenzene <0.554
Hexachlorocyclopentadiene <2.05
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d 14
Surrogate: 2,4,6-Tribromophenol
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
Prep Batch(es): V48269 06/07/24 09:41
Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Ng/L
0.554 2.00
ug/L
2.05 5.00
30.4
Limits: 10-63%
76.8
Limits: 49-118%
45.1
Limits: 22-84%
74.4
Limits: 43-123%
89.8
Limits: 49-151%
106
Limits: 31-144%
1 06/11/24 00:39 AMP V48295
1 06/11/24 00:39 AMP V48295
1
06/11/24 00:39
AMP
625.1
1
06/11/24 00:39
AMP
V48295
1
06/11/24 00:39
AMP
V48295
1
06/11/24 00:39
AMP
V48295
1
06/11/24 00:39
AMP
V48295
1
06/11/24 00:39
AMP
V48295
M Minimum value
Page 6 of 33

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01223
WSP USA Envi. & Infrastructure Inc. (Charlotte) Project CDIA-Coffey Creek
Rob Foster Report Date : 06/19/2024
2801 Yorkmont Rd. #100 Information : Project #6228-21-0061.09 Received : 06/03/2024
Charlotte , NC 28208
Report Number : 24-155-0001 REPOR T OF A NA L YSIS
Lab No : 94697
Matrix: Aqueous
Sample ID: SW-1
Sampled:
6/3/2024 11:20
Analytical Method: 625.1
Prep Batch(es):
V48269
06/07/24 09:41
Prep Method: 625.1 (Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.302
Ng/L
0.302
2.00
1
06/11/24 00:39
AMP
V48295
Acenaphthylene
<0.297
ug/L
0.297
2.00
1
06/11/24 00:39
AMP
V48295
Anthracene
<0.836
Ng/L
0.836
2.00
1
06/11/24 00:39
AMP
V48295
Benzidine
<1.32 M
ug/L
1.32
10.0
1
06/11/24 00:39
AMP
V48295
Benzo(a)anthracene
<0.637
Ng/L
0.637
2.00
1
06/11/24 00:39
AMP
V48295
Benzo(a)pyrene
<1.02
ug/L
1.02
2.00
1
06/11/24 00:39
AMP
V48295
Benzo(b)fluoranthene
<2.49
Ng/L
2.49
5.00
1
06/11/24 00:39
AMP
V48295
Benzo(g,h,i)perylene
<1.01
ug/L
1.01
5.00
1
06/11/24 00:39
AMP
V48295
Benzo(k)fluoranthene
<1.99
Ng/L
1.99
5.00
1
06/11/24 00:39
AMP
V48295
Benzoic Acid
<1.10
ug/L
1.10
10.0
1
06/11/24 00:39
AMP
V48295
Benzyl alcohol
<0.684
Ng/L
0.684
5.00
1
06/11/24 00:39
AMP
V48295
Bis(2-Chloroethoxy)methane
<0.468
ug/L
0.468
5.00
1
06/11/24 00:39
AMP
V48295
Bis(2-Chloroethyl)ether
<1.04
Ng/L
1.04
5.00
1
06/11/24 00:39
AMP
V48295
Bis(2-Chloroisopropyl)ether
<1.08
ug/L
1.08
5.00
1
06/11/24 00:39
AMP
V48295
Bis(2-ethylhexyl)phthalate
<3.46
Ng/L
3.46
10.0
1
06/11/24 00:39
AMP
V48295
4-13romophenyl phenyl ether
<1.11
ug/L
1.11
5.00
1
06/11/24 00:39
AMP
V48295
Butyl benzyl phthalate
<1.83
Ng/L
1.83
5.00
1
06/11/24 00:39
AMP
V48295
4-Chloro-3-methylphenol
<1.18
ug/L
1.18
5.00
1
06/11/24 00:39
AMP
V48295
2-Chloronaphthalene
<7.38
Ng/L
7.38
20.0
1
06/11/24 00:39
AMP
V48295
2-Chlorophenol
<0.938
ug/L
0.938
10.0
1
06/11/24 00:39
AMP
V48295
4-Chlorophenyl phenyl ether
<1.71
Ng/L
1.71
5.00
1
06/11/24 00:39
AMP
V48295
Chrysene
<0.405
ug/L
0.405
2.00
1
06/11/24 00:39
AMP
V48295
Qualifiers/ DF Dilution Factor
M
Minimum value
Definitions MQL Method Quantitation Limit
Page 7 of 33

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01223
WSP USA Envi. & Infrastructure Inc. (Charlotte) Project CDIA-Coffey Creek
Rob Foster Report Date : 06/19/2024
2801 Yorkmont Rd. #100 Information : Project #6228-21-0061.09 Received : 06/03/2024
Charlotte , NC 28208
Report Number : 24-155-0001 REPOR T OF A NA L YSIS
Lab No : 94697
Matrix: Aqueous
Sample ID: SW-1
Sampled:
6/3/2024 11:20
Analytical Method: 625.1
Prep Batch(es):
V48269
06/07/24 09:41
Prep Method: 625.1 (Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Dibenz(a,h)anthracene
<0.434
Ng/L
0.434
2.00
1
06/11/24 00:39
AMP
V48295
Dibenzofuran
<0.856
u9/L
0.856
5.00
1
06/11/24 00:39
AMP
V48295
1,2-Dichlorobenzene
<2.00
Ng/L
2.00
5.00
1
06/11/24 00:39
AMP
V48295
1,3-Dichlorobenzene
<2.00
u9/L
2.00
5.00
1
06/11/24 00:39
AMP
V48295
1,4-Dichlorobenzene
<2.05
Ng/L
2.05
5.00
1
06/11/24 00:39
AMP
V48295
3,3'-Dichlorobenzidine
<1.89
u9/L
1.89
5.00
1
06/11/24 00:39
AMP
V48295
2,4-Dichlorophenol
<1.46
Ng/L
1.46
10.0
1
06/11/24 00:39
AMP
V48295
Diethyl phthalate
<0.745
u9/L
0.745
5.00
1
06/11/24 00:39
AMP
V48295
Dimethyl phthalate
<0.939
Ng/L
0.939
5.00
1
06/11/24 00:39
AMP
V48295
2,4-Dimethylphenol
<1.57
u9/L
1.57
20.0
1
06/11/24 00:39
AMP
V48295
Di-n-butyl phthalate
<2.06
Ng/L
2.06
5.00
1
06/11/24 00:39
AMP
V48295
4,6- Din itro-2-methylphenol
<2.07
u9/L
2.07
10.0
1
06/11/24 00:39
AMP
V48295
2,4-Dinitrophenol
<1.92
Ng/L
1.92
10.0
1
06/11/24 00:39
AMP
V48295
2,4-Dinitrotoluene
<1.11
u9/L
1.11
5.00
1
06/11/24 00:39
AMP
V48295
2,6-Dinitrotoluene
<0.809
Ng/L
0.809
5.00
1
06/11/24 00:39
AMP
V48295
Di-n-Octyl Phthalate
<1.65
u9/L
1.65
5.00
1
06/11/24 00:39
AMP
V48295
Fluoranthene
<0.250
Ng/L
0.250
2.00
1
06/11/24 00:39
AMP
V48295
Fluorene
<0.807
u9/L
0.807
2.00
1
06/11/24 00:39
AMP
V48295
Hexachlorobenzene
<0.979
Ng/L
0.979
5.00
1
06/11/24 00:39
AMP
V48295
Hexachlorobutadiene
<2.73
u9/L
2.73
5.00
1
06/11/24 00:39
AMP
V48295
Hexachloroethane
<1.76
Ng/L
1.76
5.00
1
06/11/24 00:39
AMP
V48295
Indeno(1,2,3-cd)pyrene
<0.477
u9/L
0.477
2.00
1
06/11/24 00:39
AMP
V48295
Qualifiers/ DF Dilution Factor
M
Minimum value
Definitions MQL Method Quantitation Limit
Page 8 of 33

Waypoint.0
ANALYTICAL
01223
WSP USA Envi. & Infrastructure Inc. (Charlotte) Project
Rob Foster
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
CDIA-Coffey Creek
2801 Yorkmont Rd. #100 Information : Project #6228-21-0061.09
Charlotte , NC 28208
Report Number : 24-155-0001
REPORT OF ANAL YSIS
Report Date : 06/19/2024
Received : 06/03/2024
Lab No : 94697
Matrix: Aqueous
Sample ID: SW-1
Sampled: 6/3/2024
11:20
Analytical Method: 625.1
Prep Batch(es):
V48269
06/07/24 09:41
Prep Method: 625.1 (Prep)
Test
Results
Units
MDL
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
Isophorone
<0.444
Ng/L
0.444
5.00
1
06/11/24 00:39 AMP
V48295
1-Methylnaphthalene
<1.14
pg/L
1.14
2.00
1
06/11/24 00:39 AMP
V48295
2-Methylnaphthalene
<0.666
Ng/L
0.666
2.00
1
06/11/24 00:39 AMP
V48295
Naphthalene
<0.728
pg/L
0.728
2.00
1
06/11/24 00:39 AMP
V48295
Nitrobenzene
<0.905
Ng/L
0.905
5.00
1
06/11/24 00:39 AMP
V48295
2-Nitrophenol
<0.493
pg/L
0.493
5.00
1
06/11/24 00:39 AMP
V48295
4-Nitrophenol
<1.23
Ng/L
1.23
10.0
1
06/11/24 00:39 AMP
V48295
N-Nitrosodiphenylamine
<1.10
pg/L
1.10
5.00
1
06/11/24 00:39 AMP
V48295
N-Nitroso-di-n-propylamine
<0.641
Ng/L
0.641
5.00
1
06/11/24 00:39 AMP
V48295
Pentachlorophenol
<1.43
pg/L
1.43
5.00
1
06/11/24 00:39 AMP
V48295
Phenanthrene
<0.428
Ng/L
0.428
2.00
1
06/11/24 00:39 AMP
V48295
Phenol
<0.651
pg/L
0.651
5.00
1
06/11/24 00:39 AMP
V48295
Pyrene
<0.434
Ng/L
0.434
2.00
1
06/11/24 00:39 AMP
V48295
1,2,4-Trichlorobenzene
<2.21
pg/L
2.21
5.00
1
06/11/24 00:39 AMP
V48295
2,4,6-Trichlorophenol
<1.32
Ng/L
1.32
5.00
1
06/11/24 00:39 AMP
V48295
Surrogate: Phenol-d5
30.4
Limits:
10-63%
1 06/11/24 00:39 AMP
625.1
Surrogate: 2-Fluorobiphenyl
76.8
Limits:
49-118%
1 06/11/24 00:39 AMP
V48295
Surrogate: 2-Fluorophenol
45.1
Limits:
22-84%
1 06/11/24 00:39 AMP
V48295
Surrogate: Nitrobenzene-d5
74.4
Limits:
43-123%
1 06/11/24 00:39 AMP
V48295
Surrogate: 4-Terphenyl-d14
89.8
Limits:
49-151%
1 06/11/24 00:39 AMP
V48295
Surrogate: 2,4,6-Tribromophenol
106
Limits: 31-144%
1 06/11/24 00:39 AMP
V48295
Qualifiers/ DF Dilution Factor
M
Minimum value
Definitions MQL Method Quantitation Limit
Page 9 of 33

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
June 18, 2024
Danyale Love
Waypoint Analytical, LLC
449 Springbrook Rd
Charlotte, NC 28217
RE: Project: 24-155-0001
Pace Project No.: 92736919
Dear Danyale Love:
Enclosed are the analytical results for sample(s) received by the laboratory on June 17, 2024. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Sarah Graham
[e-mail]
[phone]
Project Manager
Enclosures
cc: Jerri Dawson, Waypoint Analytical
Angela Overcash, Waypoint Analytical
. V C.
_ REPORT OF LABORATORY ANALYSIS
I This report shall not be reproduced, except in full,
B ;
without the written consent of Pace Analytical Services, LLC.
Page 10 of 33
Page 1 of 16

Project: 24-155-0001
Pace Project No.: 92736919
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 33
Page 2 of 16

SAMPLE SUMMARY
Project: 24-155-0001
Pace Project No.: 92736919
Lab ID Sample ID Matrix Date Collected Date Received
92736919001 SW-1 Water 06/03/2411:20 06/17/2414:22
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 16
Page 12 of 33

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: 24-155-0001
Pace Project No.: 92736919
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92736919001 SW-1 SM 6200B LMB 63 PASI-C
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 16
Page 13 of 33

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 24-155-0001
Pace Project No.: 92736919
Sample: SW-1 Lab ID: 92736919001 Collected: 06/03/24 11:20 Received: 06/17/24 14:22 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical Services
- Charlotte
Benzene
ND
ug/L
0.50
0.079
1
06/17/24 20:06
71-43-2
Bromobenzene
ND
ug/L
0.50
0.14
1
06/17/24 20:06
108-86-1
Bromochloromethane
ND
ug/L
0.50
0.094
1
06/17/24 20:06
74-97-5
Bromodichloromethane
ND
ug/L
0.50
0.17
1
06/17/24 20:06
75-27-4
Bromoform
ND
ug/L
0.50
0.20
1
06/17/24 20:06
75-25-2
Bromomethane
ND
ug/L
5.0
0.22
1
06/17/24 20:06
74-83-9
n-Butylbenzene
ND
ug/L
0.50
0.066
1
06/17/24 20:06
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
0.085
1
06/17/24 20:06
135-98-8
tert-Butylbenzene
ND
ug/L
0.50
0.086
1
06/17/24 20:06
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
0.17
1
06/17/24 20:06
56-23-5
Chlorobenzene
ND
ug/L
0.50
0.085
1
06/17/24 20:06
108-90-7
Chloroethane
ND
ug/L
1.0
0.17
1
06/17/24 20:06
75-00-3
Chloroform
ND
ug/L
0.50
0.069
1
06/17/24 20:06
67-66-3
Chloromethane
ND
ug/L
1.0
0.18
1
06/17/24 20:06
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
0.13
1
06/17/24 20:06
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
0.096
1
06/17/24 20:06
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
0.18
1
06/17/24 20:06
96-12-8
Dibromochloromethane
ND
ug/L
0.50
0.15
1
06/17/24 20:06
124-48-1
1,2-Dibromoethane(EDB)
ND
ug/L
0.50
0.15
1
06/17/24 20:06
106-93-4
Dibromomethane
ND
ug/L
0.50
0.19
1
06/17/24 20:06
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
0.094
1
06/17/24 20:06
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
0.098
1
06/17/24 20:06
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
0.090
1
06/17/24 20:06
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
0.12
1
06/17/24 20:06
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
0.056
1
06/17/24 20:06
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
0.11
1
06/17/24 20:06
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
0.079
1
06/17/24 20:06
75-35-4
cis- 1,2-Dichloroethene
ND
ug/L
0.50
0.11
1
06/17/24 20:06
156-59-2
trans-1 2-Dichloroethene
ND
ug/L
0.50
0.10
1
06/17/24 20:06
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
0.14
1
06/17/24 20:06
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
0.085
1
06/17/24 20:06
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
0.12
1
06/17/24 20:06
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
0.066
1
06/17/24 20:06
563-58-6
cis- 1,3-Dichloropropene
ND
ug/L
0.50
0.090
1
06/17/24 20:06
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
0.13
1
06/17/24 20:06
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
0.072
1
06/17/24 20:06
108-20-3
Ethylbenzene
ND
ug/L
0.50
0.081
1
06/17/24 20:06
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
0.35
1
06/17/24 20:06
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
0.11
1
06/17/24 20:06
98-82-8
Methylene Chloride
ND
ug/L
2.0
1.9
1
06/17/24 20:06
75-09-2
Methyl -tert-butyl ether
ND
ug/L
0.50
0.053
1
06/17/24 20:06
1634-04-4
Naphthalene
ND
ug/L
2.0
0.10
1
06/17/24 20:06
91-20-3
n-Propylbenzene
ND
ug/L
0.50
0.10
1
06/17/24 20:06
103-65-1
Styrene
ND
ug/L
0.50
0.14
1
06/17/24 20:06
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
0.091
1
06/17/24 20:06
630-20-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2024 02:43 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 16
Page 14 of 33

ANALYTICAL RESULTS
Project: 24-155-0001
Pace Project No.: 92736919
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SW-1
Lab ID: 92736919001
Collected:
06/03/24 11:20
Received: 06/17/24 14:22 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
6200B MSV
Analytical
Method: SM 6200B
Pace Analytical Services
- Charlotte
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
0.074
1
06/17/24 20:06
79-34-5
Tetrachloroethene
ND
ug/L
0.50
0.086
1
06/17/24 20:06
127-18-4
Toluene
ND
ug/L
0.50
0.090
1
06/17/24 20:06
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.0
0.12
1
06/17/24 20:06
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
2.0
0.16
1
06/17/24 20:06
120-82-1
1,1,1-Trichloroethane
ND
ug/L
0.50
0.11
1
06/17/24 20:06
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.50
0.096
1
06/17/24 20:06
79-00-5
Trichloroethene
ND
ug/L
0.50
0.17
1
06/17/24 20:06
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.14
1
06/17/24 20:06
75-69-4
1,2,3-Trichloropropane
ND
ug/L
0.50
0.17
1
06/17/24 20:06
96-18-4
1,2,4-Trimethylbenzene
ND
ug/L
0.50
0.031
1
06/17/24 20:06
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
0.50
0.071
1
06/17/24 20:06
108-67-8
Vinyl chloride
ND
ug/L
1.0
0.15
1
06/17/24 20:06
75-01-4
m&p-Xylene
ND
ug/L
1.0
0.094
1
06/17/24 20:06
179601-23-1
o-Xylene
ND
ug/L
0.50
0.14
1
06/17/24 20:06
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
95
%
70-130
1
06/17/24 20:06
17060-07-0
4-Bromofluorobenzene (S)
99
%
70-130
1
06/17/24 20:06
460-00-4
Toluene-d8 (S)
99
%
70-130
1
06/17/24 20:06
2037-26-5
Date: 06/18/2024 02:43 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 16
Page 15 of 33

QUALITY CONTROL DATA
Project: 24-155-0001
Pace Project No.: 92736919
QC Batch: 861984 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200B MSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92736919001
METHOD BLANK: 4445281
Associated Lab Samples: 92736919001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
0.091
06/17/24 16:30
1,1,1-Trichloroethane
ug/L
ND
0.50
0.11
06/17/24 16:30
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
0.074
06/17/24 16:30
1,1,2-Trichloroethane
ug/L
ND
0.50
0.096
06/17/24 16:30
1,1-Dichloroethane
ug/L
ND
0.50
0.056
06/17/24 16:30
1,1-Dichloroethene
ug/L
ND
0.50
0.079
06/17/24 16:30
1,1-Dichloropropene
ug/L
ND
0.50
0.066
06/17/24 16:30
1,2,3-Trichlorobenzene
ug/L
ND
2.0
0.12
06/17/24 16:30
1,2,3-Trichloropropane
ug/L
ND
0.50
0.17
06/17/24 16:30
1,2,4-Trichlorobenzene
ug/L
ND
2.0
0.16
06/17/24 16:30
1,2,4-Trimethylbenzene
ug/L
ND
0.50
0.031
06/17/24 16:30
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
0.18
06/17/24 16:30
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
0.15
06/17/24 16:30
1,2-Dichlorobenzene
ug/L
ND
0.50
0.094
06/17/24 16:30
1,2-Dichloroethane
ug/L
ND
0.50
0.11
06/17/24 16:30
1,2-Dichloropropane
ug/L
ND
0.50
0.14
06/17/24 16:30
1,3,5-Trimethylbenzene
ug/L
ND
0.50
0.071
06/17/24 16:30
1,3-Dichlorobenzene
ug/L
ND
0.50
0.098
06/17/24 16:30
1,3-Dichloropropane
ug/L
ND
0.50
0.085
06/17/24 16:30
1,4-Dichlorobenzene
ug/L
ND
0.50
0.090
06/17/24 16:30
2,2-Dichloropropane
ug/L
ND
0.50
0.12
06/17/24 16:30
2-Chlorotoluene
ug/L
ND
0.50
0.13
06/17/24 16:30
4-Chlorotoluene
ug/L
ND
0.50
0.096
06/17/24 16:30
Benzene
ug/L
ND
0.50
0.079
06/17/24 16:30
Bromobenzene
ug/L
ND
0.50
0.14
06/17/24 16:30
Bromochloromethane
ug/L
ND
0.50
0.094
06/17/24 16:30
Bromodichloromethane
ug/L
ND
0.50
0.17
06/17/24 16:30
Bromoform
ug/L
ND
0.50
0.20
06/17/24 16:30
Bromomethane
ug/L
ND
5.0
0.22
06/17/24 16:30
Carbon tetrachloride
ug/L
ND
0.50
0.17
06/17/24 16:30
Chlorobenzene
ug/L
ND
0.50
0.085
06/17/24 16:30
Chloroethane
ug/L
ND
1.0
0.17
06/17/24 16:30
Chloroform
ug/L
ND
0.50
0.069
06/17/24 16:30
Chloromethane
ug/L
ND
1.0
0.18
06/17/24 16:30
cis-1,2-Dichloroethene
ug/L
ND
0.50
0.11
06/17/24 16:30
cis-1,3-Dichloropropene
ug/L
ND
0.50
0.090
06/17/24 16:30
Dibromochloromethane
ug/L
ND
0.50
0.15
06/17/24 16:30
Dibromomethane
ug/L
ND
0.50
0.19
06/17/24 16:30
Dichlorodifluoromethane
ug/L
ND
0.50
0.12
06/17/24 16:30
Diisopropyl ether
ug/L
ND
0.50
0.072
06/17/24 16:30
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2024 02:43 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 16
Page 16 of 33

QUALITY CONTROL DATA
Project: 24-155-0001
Pace Project No.: 92736919
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 4445281
Associated Lab Samples: 92736919001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed Qualifiers
Ethylbenzene
ug/L
ND
0.50
0.081
06/17/24 16:30
Hexachloro-1,3-butadiene
ug/L
ND
2.0
0.35
06/17/24 16:30
Isopropylbenzene (Cumene)
ug/L
ND
0.50
0.11
06/17/24 16:30
m&p-Xylene
ug/L
ND
1.0
0.094
06/17/24 16:30
Methyl -tert-butyl ether
ug/L
ND
0.50
0.053
06/17/24 16:30
Methylene Chloride
ug/L
ND
2.0
1.9
06/17/24 16:30
n-Butylbenzene
ug/L
ND
0.50
0.066
06/17/24 16:30
n-Propylbenzene
ug/L
ND
0.50
0.10
06/17/24 16:30
Naphthalene
ug/L
ND
2.0
0.10
06/17/24 16:30
o-Xylene
ug/L
ND
0.50
0.14
06/17/24 16:30
sec-Butylbenzene
ug/L
ND
0.50
0.085
06/17/24 16:30
Styrene
ug/L
ND
0.50
0.14
06/17/24 16:30
tert-Butylbenzene
ug/L
ND
0.50
0.086
06/17/24 16:30
Tetrachloroethene
ug/L
ND
0.50
0.086
06/17/24 16:30
Toluene
ug/L
ND
0.50
0.090
06/17/24 16:30
trans- 1 2- Dich loroethene
ug/L
ND
0.50
0.10
06/17/24 16:30
trans- 1,3-Dichloropropene
ug/L
ND
0.50
0.13
06/17/24 16:30
Trichloroethene
ug/L
ND
0.50
0.17
06/17/24 16:30
Trichlorofluoromethane
ug/L
ND
1.0
0.14
06/17/24 16:30
Vinyl chloride
ug/L
ND
1.0
0.15
06/17/24 16:30
1,2-Dichloroethane-d4 (S)
%
94
70-130
06/17/24 16:30
4-Bromofluorobenzene (S)
%
97
70-130
06/17/24 16:30
Toluene-d8 (S)
%
99
70-130
06/17/24 16:30
LABORATORY CONTROL SAMPLE:
4445282
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
20
19.8
99
60-140
1,1,1-Trichloroethane
ug/L
20
20.0
100
60-140
1,1,2,2-Tetrachloroethane
ug/L
20
19.0
95
60-140
1,1,2-Trichloroethane
ug/L
20
20.3
102
60-140
1,1-Dichloroethane
ug/L
20
20.2
101
60-140
1,1-Dichloroethene
ug/L
20
21.0
105
60-140
1,1-Dichloropropene
ug/L
20
20.2
101
60-140
1,2,3-Trichlorobenzene
ug/L
20
19.4
97
60-140
1,2,3-Trichloropropane
ug/L
20
18.3
92
60-140
1,2,4-Trichlorobenzene
ug/L
20
20.1
100
60-140
1,2,4-Trimethylbenzene
ug/L
20
20.3
102
60-140
1,2-Dibromo-3-chloropropane
ug/L
20
16.9
84
60-140
1,2-Dibromoethane (EDB)
ug/L
20
19.9
100
60-140
1,2-Dichlorobenzene
ug/L
20
20.8
104
60-140
1,2-Dichloroethane
ug/L
20
20.2
101
60-140
1,2-Dichloropropane
ug/L
20
20.7
103
60-140
1,3,5-Trimethylbenzene
ug/L
20
20.6
103
60-140
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2024 02:43 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 16
Page 17 of 33

QUALITY CONTROL DATA
Project: 24-155-0001
Pace Project No.: 92736919
LABORATORY CONTROL SAMPLE:
Parameter
4445282
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,3-Dichlorobenzene
ug/L
20
21.5
107
60-140
1,3-Dichloropropane
ug/L
20
19.7
99
60-140
1,4-Dichlorobenzene
ug/L
20
21.0
105
60-140
2,2-Dichloropropane
ug/L
20
18.2
91
60-140
2-Chlorotoluene
ug/L
20
21.1
106
60-140
4-Chlorotoluene
ug/L
20
20.9
105
60-140
Benzene
ug/L
20
20.9
105
60-140
Bromobenzene
ug/L
20
20.7
103
60-140
Bromochloromethane
ug/L
20
20.3
101
60-140
Bromodichloromethane
ug/L
20
19.4
97
60-140
Bromoform
ug/L
20
17.6
88
60-140
Bromomethane
ug/L
20
20.0
100
60-140
Carbon tetrachloride
ug/L
20
20.9
105
60-140
Chlorobenzene
ug/L
20
20.7
104
60-140
Chloroethane
ug/L
20
20.2
101
60-140
Chloroform
ug/L
20
20.0
100
60-140
Chloromethane
ug/L
20
21.3
106
60-140
cis-1,2-Dichloroethene
ug/L
20
20.0
100
60-140
cis-1,3-Dichloropropene
ug/L
20
18.8
94
60-140
Dibromochloromethane
ug/L
20
18.8
94
60-140
Dibromomethane
ug/L
20
21.0
105
60-140
Dichlorodifluoromethane
ug/L
20
24.9
124
60-140
Diisopropyl ether
ug/L
20
18.8
94
60-140
Ethylbenzene
ug/L
20
21.0
105
60-140
Hexachloro-1,3-butadiene
ug/L
20
20.4
102
60-140
Isopropylbenzene (Cumene)
ug/L
20
20.5
103
60-140
m&p-Xylene
ug/L
40
40.9
102
60-140
Methyl -tert-butyl ether
ug/L
20
18.2
91
60-140
Methylene Chloride
ug/L
20
17.8
89
60-140
n-Butylbenzene
ug/L
20
20.5
102
60-140
n-Propylbenzene
ug/L
20
20.8
104
60-140
Naphthalene
ug/L
20
18.8
94
60-140
o-Xylene
ug/L
20
20.5
103
60-140
sec-Butylbenzene
ug/L
20
21.0
105
60-140
Styrene
ug/L
20
20.5
102
60-140
tert-Butylbenzene
ug/L
20
18.1
90
60-140
Tetrachloroethene
ug/L
20
20.6
103
60-140
Toluene
ug/L
20
20.7
104
60-140
trans- 1 2- Dich loroethene
ug/L
20
20.4
102
60-140
trans- 1 3- Dich loropropene
ug/L
20
18.8
94
60-140
Trichloroethene
ug/L
20
21.7
108
60-140
Trichlorofluoromethane
ug/L
20
22.4
112
60-140
Vinyl chloride
ug/L
20
20.7
104
60-140
1,2-Dichloroethane-d4 (S)
%
92
70-130
4-Bromofluorobenzene (S)
%
98
70-130
Toluene-d8 (S)
%
98
70-130
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2024 02:43 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 16
Page 18 of 33

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 24-155-0001
Pace Project No.: 92736919
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4445283
MS
92736920001 Spike
Parameter Units Result Conc.
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-
chloropropane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Chlorotoluene
4-Chlorotoluene
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Dichlorodifluoromethane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene
(Cumene)
m&p-Xylene
4445284
MSD
Spike MS MSD MS MSD % Rec
Conc. Result Result % Rec % Rec Limits
ug/L
ND
200
200
209
215
105
107
60-140
ug/L
ND
200
200
236
245
118
122
60-140
ug/L
ND
200
200
228
227
114
114
60-140
ug/L
ND
200
200
214
213
107
107
60-140
ug/L
ND
200
200
212
220
106
110
60-140
ug/L
ND
200
200
208
220
104
110
60-140
ug/L
ND
200
200
249
257
124
128
60-140
ug/L
ND
200
200
252
264
126
132
60-140
ug/L
ND
200
200
222
223
111
112
60-140
ug/L
ND
200
200
244
260
122
130
60-140
ug/L
ND
200
200
238
253
119
126
60-140
ug/L
ND
200
200
229
228
114
114
60-140
Max
RPD RPD Qual
3 30
4 30
0 30
0 30
4 30
5 30
3 30
5 30
1 30
7 30
6 30
0 30
ug/L
N D
200
200
237
244
118
122
60-140
3
30
ug/L
N D
200
200
233
244
116
122
60-140
5
30
ug/L
N D
200
200
223
232
111
116
60-140
4
30
ug/L
N D
200
200
200
199
100
100
60-140
0
30
ug/L
N D
200
200
243
254
122
127
60-140
4
30
ug/L
N D
200
200
229
243
115
122
60-140
6
30
ug/L
N D
200
200
240
244
120
122
60-140
2
30
ug/L
N D
200
200
234
241
117
120
60-140
3
30
ug/L
N D
200
200
232
242
116
121
60-140
4
30
ug/L
N D
200
200
248
259
124
130
60-140
5
30
ug/L
N D
200
200
241
253
121
126
60-140
5
30
ug/L
1530
200
200
1670
1630
68
48
60-140
2
30 M1
ug/L
N D
200
200
222
240
111
120
60-140
8
30
ug/L
N D
200
200
210
225
105
113
60-140
7
30
ug/L
N D
200
200
231
226
116
113
60-140
2
30
ug/L
N D
200
200
185
187
92
94
60-140
1
30
ug/L
N D
200
200
173
191
87
95
60-140
9
30
ug/L
N D
200
200
249
249
125
124
60-140
0
30
ug/L
N D
200
200
230
232
115
116
60-140
1
30
ug/L
N D
200
200
173
186
87
93
60-140
7
30
ug/L
N D
200
200
210
225
105
112
60-140
7
30
ug/L
N D
200
200
231
243
115
121
60-140
5
30
ug/L
N D
200
200
213
223
107
111
60-140
4
30
ug/L
N D
200
200
190
190
95
95
60-140
0
30
ug/L
N D
200
200
199
204
99
102
60-140
2
30
ug/L
N D
200
200
223
224
112
112
60-140
0
30
ug/L
N D
200
200
212
233
106
116
60-140
9
30
ug/L
107
200
200
313
332
103
112
60-140
6
30
ug/L
17.6
200
200
256
263
119
123
60-140
3
30
ug/L
N D
200
200
247
257
123
129
60-140
4
30
ug/L
17.5
200
200
252
260
117
121
60-140
3
30
ug/L
N D
400
400
470
485
118
121
60-140
3
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2024 02:43 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 16
Page 19 of 33

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 24-155-0001
Pace Project No.: 92736919
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4445283
4445284
MS
MSD
92736920001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Methyl-tert-butyl ether
ug/L
1800
200
200
2140
2200
174
202
60-140
3
30 E
Methylene Chloride
ug/L
38.3
200
200
207
220
85
91
60-140
6
30
n-Butylbenzene
ug/L
ND
200
200
254
271
127
135
60-140
6
30
n-Propylbenzene
ug/L
5.3
200
200
250
262
122
128
60-140
5
30
Naphthalene
ug/L
122
200
200
394
425
136
151
60-140
8
30 M1
o-Xylene
ug/L
ND
200
200
243
239
121
119
60-140
2
30
sec-Butylbenzene
ug/L
ND
200
200
247
265
123
132
60-140
7
30
Styrene
ug/L
ND
200
200
232
235
116
117
60-140
1
30
tert-Butylbenzene
ug/L
ND
200
200
199
209
99
104
60-140
5
30
Tetrachloroethene
ug/L
ND
200
200
254
263
127
131
60-140
4
30
Toluene
ug/L
ND
200
200
214
216
107
108
60-140
1
30
trans-1,2-Dichloroethene
ug/L
ND
200
200
218
229
109
115
60-140
5
30
trans-1,3-Dichloropropene
ug/L
ND
200
200
185
183
93
92
60-140
1
30
Trichloroethene
ug/L
ND
200
200
252
246
126
123
60-140
2
30
Trichlorofluoromethane
ug/L
ND
200
200
216
215
108
108
60-140
0
30
Vinyl chloride
ug/L
ND
200
200
199
208
100
104
60-140
4
30
1,2-Dichloroethane-d4 (S)
%
101
101
70-130
4-Bromofluorobenzene (S)
%
102
102
70-130
Toluene-d8 (S)
%
96
94
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2024 02:43 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 16
Page 20 of 33

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: 24-155-0001
Pace Project No.: 92736919
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
E Analyte concentration exceeded the calibration range. The reported result is estimated.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2024 02:43 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 16
Page 21 of 33

Project: 24-155-0001
Pace Project No.: 92736919
Lab ID Sample ID
92736919001 SW-1
Date: 06/18/2024 02:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
QC Batch Method QC Batch Analytical Method
SM 6200B 861984
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
Page 13 of 16
Page 22 of 33

DC#_Title: ENV-FRM-HUN1-0083 04-
Sample Condition Upon Receipt
ace
Effective Date: 4/26/2024 10:14:05 AM
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville [f Raleigh❑ Mer$innir-c%AIIal-1 a*inintn I KarnprcvillpF�
Sample Condition Upon Receipt Client Name; Project #tWO# : 92736919
f� n
Courier: LJ Fed Ex OLIPS LJ Lis Ps Client 111111111111
❑ Commercial ❑ Pace ❑ Other: _ 92736919
Custody Seal Present? El Yes ElNo Seals intact? ❑Yes ❑No I5 N/A
Date/Initials Person Examining Contents:
Packing Material: El Bubble Wrap ❑ Bubble Bags ❑None z Other Biological Tissue IFien? 6-17- zY
Thermometer:
I {R Gun ID: ` ,,r
Type of Ice: Wet ❑Blue
Correction Factor:
Cooler Temp: Add/Subtract (°C) L�
Cooler Temp Corrected 1 �,1+
USDA Regulated Soil ( [?N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC
(check maps)? ❑Yes ❑ No
Chain of Custody Present?
I"Yes
❑ NO
:1 N/A
Samples Arrived within Hold Time?
R es
❑ No
❑ N/A
Short Hold Time Analysis (<7Z hr.)?
❑ Yes
GVNo
❑ N/A
Rush Turn Around Time Requested?
❑ Yes
1KNQ
❑ N/A
Sufficient Volume?
MCS
❑ No
❑ N/A
Correct Containers Used?
Yes
❑ No
❑ N/A
-Pace Containers Used?
Vies
❑ No
❑ N/A
Containers Intact?
EVYes
❑ No
❑ N/A
Dissolved analysis: Samples Field Filtered?
❑ Yes
❑ No
1 /A
Sample Labels Match COC?
ZKes
❑ No
❑ N/A
-Includes Date/Time/1D/Analysis Matrix:
Headspace in VDA Vials (>5-6mm)?
El Yes
VNo
❑NIA
Trip Blank Present?
❑Yes
�]'Na
❑N/A
Trip Blank Custody Seals Present?
❑ Yes
MINZ
❑ N/A
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
S.
6.
❑ Yes ❑ No IJ N/A
❑ None
Temp should be above freezing to 6'C
❑ Samples out of temp criteria. Samples on ice, cooling process
has begun
Did samples originate from a foreign source (internationally,
including Hawaii and Puerto Rico)? I] Yes ❑ No
Comments/Discrepancy:
Lot ID of split Containers:
Date/Time:
Date:
Date:
Field Data Requlred? ❑Yes ❑ No
Qualtrax ID: 69614
Page 23 of 33
Pace 1 of 2 Page 14 of 16

DC#_Title: ENV-FRM-HUN1-0083 v04-
Sample Condition Upon Receipt
ace
Effective Date: 4/26/2024 10:14:05 AM
*Cheek mark top half of box If pH and/or dechlorination is verified and within the
acceptance range far preservation samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottles
***Check all unpreserved Nitrates for chlorine
Pra,e� # WO# : 92736919
PM: SMG Due Date: 05/19/24
CLIENT: 92-Prism
J
Laboratory Receiving Location: Asheville ❑ Eden❑ Greenwood El Huntersville ❑ Raleigh[_I Mechanicsvil[e❑ Atlanta❑ Kernersvillel]
Client Profile Number Notes
r�
■
WOMEN
mow■
PH Adjustment Log for Preserved Samples
Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative Lot #
adjusted added
Note: Wheneverthere is a discrepancy affeuUng North Carolina compliance samples, a copy ofthis form will besenttothL NorthCarolina DENR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Qualtrax ID: 69614
Page 24 of 33
Paae 2 of 2 Page 15 of 16

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Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: WSP USA Envi. & Infrastructure Inc. (Charlotte)
Project Description: CDIA-Coffey Creek
Report No: 24-155-0001
QC Prep: V48269 QC Analytical Batch(es): V48295
QC Prep Batch Method: 625.1 (Prep) Analysis Method: 625.1
Analysis Description: 625.1 - Base/Neutrals and Acids by GC/MS
Lab Reagent Blank LRB-V48269 Matrix: AQU
Associated Lab Samples: 94697
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
Acenaphthene
pg/L
<0.302
0.302
2.00
06/10/24 21:49
Acenaphthylene
pg/L
<0.297
0.297
2.00
06/10/24 21:49
Anthracene
pg/L
<0.836
0.836
2.00
06/10/24 21:49
Benzidine
pg/L
<1.32
1.32
10.0
06/10/24 21:49
Benzo(a)anthracene
pg/L
<0.637
0.637
2.00
06/10/24 21:49
Benzo(a)pyrene
pg/L
<1.02
1.02
2.00
06/10/24 21:49
Benzo(b)fluoranthene
pg/L
<2.49
2.49
5.00
06/10/24 21:49
Benzo(g,h,i)perylene
pg/L
<1.01
1.01
5.00
06/10/24 21:49
Benzo(k)fluoranthene
pg/L
<1.99
1.99
5.00
06/10/24 21:49
Benzoic Acid
pg/L
<1.10
1.10
10.0
06/10/24 21:49
Benzyl alcohol
pg/L
<0.684
0.684
5.00
06/10/24 21:49
Bis(2-Chloroethoxy)methane
pg/L
<0.468
0.468
5.00
06/10/24 21:49
Bis(2-Chloroethyl)ether
pg/L
< 1.04
1.04
5.00
06/10/24 21:49
Bis(2-Chloroisopropyl)ether
pg/L
<1.08
1.08
5.00
06/10/24 21:49
Bis(2-ethylhexyl)phthalate
pg/L
<3.46
3.46
10.0
06/10/24 21:49
4-Bromophenyl phenyl ether
pg/L
<1.11
1.11
5.00
06/10/24 21:49
Butyl benzyl phthalate
pg/L
<1.83
1.83
5.00
06/10/24 21:49
4-Chloro-3-methylphenol
pg/L
<1.18
1.18
5.00
06/10/24 21:49
2-Chloronaphthalene
pg/L
<7.38
7.38
20.0
06/10/24 21:49
2-Chlorophenol
pg/L
<0.938
0.938
10.0
06/10/24 21:49
4-Chlorophenyl phenyl ether
pg/L
<1.71
1.71
5.00
06/10/24 21:49
Chrysene
pg/L
<0.405
0.405
2.00
06/10/24 21:49
Dibenz(a,h)anthracene
pg/L
<0.434
0.434
2.00
06/10/24 21:49
Dibenzofuran
pg/L
<0.856
0.856
5.00
06/10/24 21:49
1,2-Dichlorobenzene
pg/L
<2.00
2.00
5.00
06/10/24 21:49
1,3-Dichlorobenzene
pg/L
<2.00
2.00
5.00
06/10/24 21:49
1,4-Dichlorobenzene
pg/L
<2.05
2.05
5.00
06/10/24 21:49
Date:
06/19/2024 02:14 PM
Page 1 of 6
Page 26 of 33

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: WSP USA Envi. & Infrastructure Inc. (Charlotte)
Project Description: CDIA-Coffey Creek
Report No: 24-155-0001
QC Prep: V48269 QC Analytical Batch(es): V48295
QC Prep Batch Method: 625.1 (Prep) Analysis Method: 625.1
Analysis Description: 625.1 - Base/Neutrals and Acids by GC/MS
Lab Reagent Blank LRB-V48269 Matrix: AQU
Associated Lab Samples: 94697
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
3,3'-Dichlorobenzidine
pg/L
<1.89
1.89
5.00
06/10/24 21:49
2,4-Dichlorophenol
pg/L
<1.46
1.46
10.0
06/10/24 21:49
Diethyl phthalate
pg/L
<0.745
0.745
5.00
06/10/24 21:49
Dimethyl phthalate
pg/L
<0.939
0.939
5.00
06/10/24 21:49
2,4-Dimethylphenol
pg/L
<1.57
1.57
20.0
06/10/24 21:49
Di-n-butyl phthalate
pg/L
<2.06
2.06
5.00
06/10/24 21:49
4,6- Din itro-2-methylphenol
pg/L
<2.07
2.07
10.0
06/10/24 21:49
2,4-Dinitrophenol
pg/L
<1.92
1.92
10.0
06/10/24 21:49
2,4-Dinitrotoluene
pg/L
<1.11
1.11
5.00
06/10/24 21:49
2,6-Dinitrotoluene
pg/L
<0.809
0.809
5.00
06/10/24 21:49
Di-n-Octyl Phthalate
pg/L
<1.65
1.65
5.00
06/10/24 21:49
Fluoranthene
pg/L
<0.250
0.250
2.00
06/10/24 21:49
Fluorene
pg/L
<0.807
0.807
2.00
06/10/24 21:49
Hexachlorobenzene
pg/L
<0.979
0.979
5.00
06/10/24 21:49
Hexachlorobutadiene
pg/L
<2.73
2.73
5.00
06/10/24 21:49
Hexachlorocyclopentadiene
pg/L
<2.05
2.05
5.00
06/10/24 21:49
Hexachloroethane
pg/L
<1.76
1.76
5.00
06/10/24 21:49
Indeno(1,2,3-cd)pyrene
pg/L
<0.477
0.477
2.00
06/10/24 21:49
Isophorone
pg/L
<0.444
0.444
5.00
06/10/24 21:49
1-Methylnaphthalene
pg/L
<1.14
1.14
2.00
06/10/24 21:49
2-Methylnaphthalene
pg/L
<0.666
0.666
2.00
06/10/24 21:49
Naphthalene
pg/L
<0.728
0.728
2.00
06/10/24 21:49
Nitrobenzene
pg/L
<0.905
0.905
5.00
06/10/24 21:49
2-Nitrophenol
pg/L
<0.493
0.493
5.00
06/10/24 21:49
4-Nitrophenol
pg/L
<1.23
1.23
10.0
06/10/24 21:49
N-Nitrosodiphenylamine
pg/L
<1.10
1.10
5.00
06/10/24 21:49
N-Nitroso-di-n-propylamine
pg/L
<0.641
0.641
5.00
06/10/24 21:49
Date:
06/19/2024 02:14 PM
Page 2 of 6
Page 27 of 33

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: WSP USA Envi. & Infrastructure Inc. (Charlotte)
Project Description: CDIA-Coffey Creek
Report No: 24-155-0001
QC Prep: V48269 QC Analytical Batch(es): V48295
QC Prep Batch Method: 625.1 (Prep) Analysis Method: 625.1
Analysis Description: 625.1 - Base/Neutrals and Acids by GC/MS
Lab Reagent Blank LRB-V48269 Matrix: AQU
Associated Lab Samples: 94697
Blank
MDL
MQL
Analyzed
%
% Rec
Parameter
Units
Result
Recovery
Limits
Pentachlorophenol
pg/L
<1.43
1.43
5.00
06/10/24 21:49
Phenanthrene
pg/L
<0.428
0.428
2.00
06/10/24 21:49
Phenol
pg/L
<0.651
0.651
5.00
06/10/24 21:49
Pyrene
pg/L
<0.434
0.434
2.00
06/10/24 21:49
1,2,4-Trichlorobenzene
pg/L
<2.21
2.21
5.00
06/10/24 21:49
2,4,6-Trichlorophenol
pg/L
<1.32
1.32
5.00
06/10/24 21:49
2-Fluorobiphenyl (S)
06/10/24 21:49
77.4
49-118
2-Fluorophenol (S)
06/10/24 21:49
51.8
22-84
Nitrobenzene-d5 (S)
06/10/24 21:49
81.2
43-123
4-Terphenyl-d14 (S)
06/10/24 21:49
95.4
49-151
2,4,6-Tribromophenol(S)
06/10/24 21:49
105
31-144
Phenol-d5(S)
06/10/24 21:49
34.8
10-63
Laboratory Control Sample & LCSD
LCS-V48269 LCSD-V48269
Spike
LCS
LCSD
LCS LCSD
% Rec
Parameter
Units
Conc.
Result
Result
%Rec a/o Rec
Limits
RPD
Max
RPD
Acenaphthene
pg/L
50.0
40.1
38.5
80.2 77.0
47-145
4.0
20.0
Acenaphthylene
pg/L
50.0
41.5
41.3
83.0 82.6
33-145
0.4
20.0
Anthracene
pg/L
50.0
44.9
42.6
89.8 85.2
27-133
5.2
20.0
Benzidine
pg/L
50.0
5.55
4.00
11.1* 8.0*
15-150
32.4*
20.0
Benzo(a)anthracene
pg/L
50.0
41.2
40.1
82.4 80.2
33-143
2.7
20.0
Benzo(a)pyrene
pg/L
50.0
48.2
47.2
96.4 94.4
17-163
2.0
20.0
Benzo(b)fluoranthene
pg/L
50.0
39.5
40.2
79.0 80.4
24-159
1.7
20.0
Benzo(g,h,i)perylene
pg/L
50.0
48.6
43.3
97.2 86.6
10-219
11.5
20.0
Benzo(k)fluoranthene
pg/L
50.0
49.1
45.3
98.2 90.6
11-162
8.0
20.0
Benzoic Acid
pg/L
50.0
30.8
27.8
61.6 55.6
10-125
10.2
20.0
* QC Fail Date: 06/19/2024 02:14 PM Page 3 of 6
Page 28 of 33

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: WSP USA Envi. & Infrastructure Inc. (Charlotte)
Project Description: CDIA-Coffey Creek
Report No: 24-155-0001
QC Prep: V48269 QC Analytical Batch(es): V48295
QC Prep Batch Method: 625.1 (Prep) Analysis Method: 625.1
Analysis Description: 625.1 - Base/Neutrals and Acids by GC/MS
Laboratory Control Sample & LCSD LCS-V48269 LCSD-V48269
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
Benzyl alcohol
pg/L
50.0
38.1
36.5
76.2
73.0
16-107
4.2
20.0
Bis(2-Chloroethoxy)methane
pg/L
50.0
37.5
36.4
75.0
72.8
33-184
2.9
20.0
Bis(2-Chloroethyl)ether
pg/L
50.0
32.7
30.5
65.4
61.0
12-158
6.9
20.0
Bis(2-Chloroisopropyl)ether
pg/L
50.0
33.0
31.4
66.0
62.8
36-166
4.9
20.0
Bis(2-ethylhexyl)phthalate
pg/L
50.0
48.9
47.0
97.8
94.0
10-158
3.9
20.0
4-Bromophenyl phenyl ether
pg/L
50.0
42.2
41.4
84.4
82.8
53-127
1.9
20.0
Butyl benzyl phthalate
pg/L
50.0
46.8
45.2
93.6
90.4
10-152
3.4
20.0
4-Chloro-3-methyl phenol
pg/L
50.0
41.4
40.4
82.8
80.8
22-147
2.4
20.0
2-Chloronaphthalene
pg/L
50.0
36.4
35.8
72.8
71.6
60-118
1.6
20.0
2-Chlorophenol
pg/L
50.0
35.4
34.7
70.8
69.4
23-134
1.9
20.0
4-Chlorophenyl phenyl ether
pg/L
50.0
39.3
39.0
78.6
78.0
25-158
0.7
20.0
Chrysene
pg/L
50.0
37.8
27.5
75.6
55.0
17-168
31.5*
20.0
Dibenz(a,h)anthracene
pg/L
50.0
23.4
15.1
46.8
30.2
10-227
43.1*
20.0
Dibenzofuran
pg/L
50.0
41.7
41.8
83.4
83.6
39-114
0.2
20.0
1,2-Dichlorobenzene
pg/L
50.0
29.5
25.1
59.0
50.2
32-129
16.1
20.0
1,3-Dichlorobenzene
pg/L
50.0
28.2
23.9
56.4
47.8
20-124
16.5
20.0
1,4-Dichlorobenzene
pg/L
50.0
27.2
22.5
54.4
45.0
20-124
18.9
20.0
3,3'-Dichlorobenzidine
pg/L
50.0
44.4
43.8
88.8
87.6
10-262
1.3
20.0
2,4-Dichlorophenol
pg/L
50.0
41.1
42.2
82.2
84.4
39-135
2.6
20.0
Diethyl phthalate
pg/L
50.0
43.5
41.6
87.0
83.2
10-114
4.4
20.0
Dimethyl phthalate
pg/L
50.0
45.4
43.6
90.8
87.2
10-112
4.0
20.0
2,4-Dimethyl phenol
pg/L
50.0
50.0
48.3
100
96.6
32-119
3.4
20.0
Di-n-butyl phthalate
pg/L
50.0
47.1
45.1
94.2
90.2
10-118
4.3
20.0
4,6- Din itro-2-methylphenol
pg/L
50.0
53.2
53.7
106
107
10-181
0.9
20.0
2,4-Dinitrophenol
pg/L
50.0
58.8
58.1
118
116
10-191
1.1
20.0
2,4-Dinitrotoluene
pg/L
50.0
56.0
54.9
112
110
39-139
1.9
20.0
* QC Fail Date: 06/19/2024 02:14 PM Page 4 of 6
Page 29 of 33

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: WSP USA Envi. & Infrastructure Inc. (Charlotte)
Project Description: CDIA-Coffey Creek
Report No: 24-155-0001
QC Prep: V48269 QC Analytical Batch(es): V48295
QC Prep Batch Method: 625.1 (Prep) Analysis Method: 625.1
Analysis Description: 625.1 - Base/Neutrals and Acids by GC/MS
Laboratory Control Sample & LCSD LCS-V48269 LCSD-V48269
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
2,6-Dinitrotoluene
pg/L
50.0
56.7
54.8
113
110
50-158
3.4
20.0
Di-n-Octyl Phthalate
pg/L
50.0
45.4
44.1
90.8
88.2
10-146
2.9
20.0
Fluoranthene
pg/L
50.0
43.8
42.4
87.6
84.8
26-137
3.2
20.0
Fluorene
pg/L
50.0
41.2
40.8
82.4
81.6
59-121
0.9
20.0
Hexachlorobenzene
pg/L
50.0
46.4
43.2
92.8
86.4
10-152
7.1
20.0
Hexachlorobutadiene
pg/L
50.0
32.7
29.6
65.4
59.2
24-116
9.9
20.0
Hexachlorocyclopentadiene
pg/L
50.0
26.6
25.4
53.2
50.8
32-117
4.6
20.0
Hexachloroethane
pg/L
50.0
25.6
21.9
51.2
43.8
40-113
15.5
20.0
Indeno(1,2,3-cd)pyrene
pg/L
50.0
45.8
42.0
91.6
84.0
10-171
8.6
20.0
Isophorone
pg/L
50.0
32.9
32.0
65.8
64.0
21-196
2.7
20.0
1-Methylnaphthalene
pg/L
50.0
34.9
33.3
69.8
66.6
40-135
4.6
20.0
2-Methylnaphthalene
pg/L
50.0
35.1
33.0
70.2
66.0
18-121
6.1
20.0
Naphthalene
pg/L
50.0
32.0
30.0
64.0
60.0
21-133
6.4
20.0
Nitrobenzene
pg/L
50.0
36.4
34.4
72.8
68.8
35-180
5.6
20.0
2-Nitrophenol
pg/L
50.0
44.2
43.7
88.4
87.4
29-182
1.1
20.0
4-Nitrophenol
pg/L
50.0
26.5
25.8
53.0
51.6
10-132
2.6
20.0
N-Nitrosodiphenylamine
pg/L
50.0
54.7
52.9
109
106
69-152
3.3
20.0
N-Nitroso-di-n-propylamine
pg/L
50.0
41.3
39.7
82.6
79.4
10-230
3.9
20.0
Pentachlorophenol
pg/L
50.0
56.0
54.1
112
108
14-176
3.4
20.0
Phenanthrene
pg/L
50.0
43.8
41.0
87.6
82.0
54-120
6.6
20.0
Phenol
pg/L
50.0
17.4
16.8
34.8
33.6
10-112
3.5
20.0
Pyrene
pg/L
50.0
45.1
43.5
90.2
87.0
52-115
3.6
20.0
1,2,4-Trichlorobenzene
pg/L
50.0
31.3
28.2
62.6
56.4
44-142
10.4
20.0
2,4,6-Trichlorophenol
pg/L
50.0
43.4
42.5
86.8
85.0
37-144
2.0
20.0
2-Fluorobiphenyl (S)
80.4
75.2
49-118
2-Fluorophenol (S)
49.3
45.6
22-84
Date: 06/19/2024 02:14 PM Page 5 of 6
Page 30 of 33

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: WSP USA Env!. & Infrastructure Inc. (Charlotte)
Project Description: CDIA-Coffey Creek
Report No: 24-155-0001
QC Prep: V48269
QC Prep Batch Method: 625.1 (Prep)
QC Analytical Batch(es): V48295
Analysis Method: 625.1
Analysis Description: 625.1 - Base/Neutrals and Acids by GC/MS
Laboratory Control Sample & LCSD
LCS-V48269 LCSD-V48269
Spike LCS LCSD
LCS
LCSD
% Rec
Parameter Units
Conc. Result Result
%Rec
% Rec
Limits RPD
Nitrobenzene-d5 (S)
77.8
72.4
43-123
4-Terphenyl-d14 (S)
89.0
82.4
49-151
2,4,6-Tribromophenol (S)
105
97.2
31-144
Phenol-d5 (S)
33.1
31.5
10-63
Date: 06/19/2024 02:14 PM Page 6 of 6
Page 31 of 33

WayPAoint.
NALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 01223
Customer Name: WSP USA Envi. & Infrastructure Inc. (Charlotte)
Report Number: 24-155-0001
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other:
0 UPS 0 Client 0 Courier Thermometer ID:
IRT15 5.3C
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
0 Yes
0 No
# Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
# Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample Iabel(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
U Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
U Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
0 Not Present
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
U Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
0 N/A
Trip Blanks received with VOAs
0 Yes
* No
0 N/A
Soil VOA method 5035 — compliance criteria met
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
Special precautions or instructions included?
Comments:
0 Yes 0 No U N/A
F Low concentration EnCore samplers (48 hr)
Low conc pre -weighed vials (Sod Bis -14 d)
0Yes ONo
Signature: Angelo Norvell
Date & Time: 06/03/2024 12:00:00
Page 32 of 33

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Page 33 of 33