WQ0003626_Monitoring - 03-2024_20240717

Monitoring Report Submittal
Permit Number#*
Name of Facility:*
Month: * March
WQ0003626
Campbell Soup Supply Co., LLC
Report Information
Type *
Revised - NDMR, NDAR-1, NDAR-2, NDMLR
Year:* 2024
Upload Document*
NDMR Report ReSubmittal March w Labs.pdf 5.46MB
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59).
Confirmation Email Address: * [e-mail]
Name of Submitter: * Liz Ward
Signature:
1-6&-lird
Date of submittal: 7/17/2024
This will be filled in automatically
Initial Review
Reviewer: Wanda.Gerald

Is the project number correct?* WQ0003626
Is the monitoring report accepted?* Yes No
Regional Office* Fayetteville
Reviewer: _anonymous
Review Date: 7/17/2024

FORM: NDMR 08-11 NON -DISCHARGE MONITORING REPORT (NDMR) Page _1_ of _3
Permit No.: W00003626
Facility Name: Campbell Soup Supply Company, LLC
County: Robeson
Month: March
Year: 2024
PPk 001
Flow Measuring Point: ❑influent 0 Effluent ❑ No Flow generated
Parameter Monitoring Point: ❑ InFluent O Effluent ❑Groundwater Lowering El Surface Water
Parameter Code -►
50050
00400
00310
00610
00530
00665
00620
00625
00916
01027
01042
00929
00927
01067
01092
1 WQ09
>
E
~
c
0
v
O
°
LL
O
m
M
E
E
Q
o
3
`
o
f0
z
1�
c
V
°
n
E
z
m o
_a
>Q zO
24-1hr
hrs
GPD
su
mg/L
mq/L
mg/L
mg/L
mg/L
mg/L
mg/L
mq/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
1
07:00
24
2,664,200
4.7
2
07:00
24
1,900.900
3
07:00
24
2.144.400
4
07:00
24
2,392,300
6
5
07:00
24
2,335,800
4.2
1240
<2.50
344
5.54
<0.100
33.2
2.98
<0.002
0.0298
78.4
3.36
00128
0.394
13.28
6
07:00
24
2,025,400
42
7
07:00
24
2,250,200
4.2
8
07:00
24
1.860,600
4.6
9
07:00
24
2,076,800
10
07:00
24
825.700
11
07:00
24
1.801,500
4.7
12
07:00
24
1,882.900
38
1170
3.14
283
465
<0.100
31.8
4
<0.002
0.0132
101
4.9
0.0104
0.424
13.03
13
07:00
24
1.689.600
4
14
07:00
24
1.904.800
4
15
07:00
24
1.969.000
4
16
07:00
24
1,439,600
17
07:00
24
1,573,500
18
07:00
24
2,249,700
4.5
19
07:00
24
2,044,000
4
20
07:00
24
2,202,200
4.1
21
07:00
24
2,199,600
4
22
07:00
24
1,925,400
4
23
07:00
24
1,097,800
24
07:00
24
862,000
25
07:00
24
1,866,600
61
26
07:00
24
1.975.800
4
27
07:00
24
2.035.7001
4.1
28
07:00
24
1,924,6001
4.3
29
07:00
24
471,000
4.3
30
07:00
24
481,200
31
07:00
24
0
Average:
1,744,284
1.205.00
3.14
313.50
5.10
32.50
3.49
0.02
89.70
4.13
0.01
0.41
13.16
Daily Maximum:
2,664,200
6.10
1.240.00
3.14
344.00
5.54
33.20
4.00
0.03
101.00
4.90
0.01
0.42
13.28
Daily Minimum:
0
3.80
1.170.00
3.14
283.00
465
31.80
2.98
0.01
78.40
3.36
0.01
0.39
13.03
Sampling Type:
Recorder
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Calculated
Monthly Limit:
4,000,000
Daily Limit:
Sample Frequency:
Daily
5/Week
Bimonthly I
Bimonthly
Bimonthly
Bimonthly
Bimonthly
Bimonthly
Bimonthly
Bimonthly
Bimonthly
Bimonthly
Bimonthly
Bimonthly
Bimonthly
Bimonthly

FORM: NDMR 08-11 NON -DISCHARGE MONITORING REPORT (NDMR) Page _2 of 3
Permit No.: W00003626
Facility Name: Campbell Soup Supply Company, LLC
County: Robeson
Month: March
Year: 2024
PI 001
Flow Measuring Point: ❑ influent O Effluent ❑ No flow generated
Parameter Monitoring Point: ❑ influent 0 Effluent ❑ Groundwater Lowering ❑ Surface Water
Parameter Code - 0
50050
00931
00940
31616
00600
70300
Of0
m
m
Q
Q
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c
O
d
Ed
fn
U
O
3
LL
=
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rn o
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OR
W—m
U
co
O 2
Z
CD_
N O
N Cn
E
24-hr
hrs
GPD
Ratio
mq/L
#/100 mL
mq/L
mg/L
1
07:00
24
2,664.200
2
07:00
24
1.900.900
3
07:00
24
2,144,400
4
07:00
24
2,392,300
5
07:00
24
2,335,800
736
68.9
208,000
33.2
6
07:00
24
2,025,400
7
07:00
24
2.250,200
8
07:00
24
1,860.600
9
07:00
24
2.076.800
10
07:00
24
825.700
11
07:00
24
1,801,500
12
07:00
24
1,882,900
7.96
111
<2,000
31.8
13
07:00
24
1,689,600
14
07:00
24
1,904,800
15
07:00
24
1,969,000
16
07:00
24
1,439,600
17
07:00
24
1,573,500
18
07:00
24
2,249,700
19
07:00
24
2,044.000
20
07:00
24
2.202.200
21
07:00
24
2,199,600
22
07:00
24
1,925,400
23
07:00
24
1,097,800
24
07:00
24
862,000
25
07:00
24
1,866,600
26
07:00
24
1.975,800
27
07:00
24
2.035.700
28
07:00
24
1.924.600
29
07:00
24
471,000
30
07:00
24
481,200
311
07:00 1
24
0
Average:
1.744,284
766
89.95
32.50
Daily Maximum:
2,664,200
7.96
111.00
###✓#
33.20
Daily Minimum:
0
7.36
68.90
31.80
Sampling Type:
Recorder
Calculated
Grab
Grab
Grab
Monthly Limit:
4,000,000
Daily Limit:
Sample Frequency:
Daily
Bimonthly

FORM: NDMR 08-11 NON -DISCHARGE MONITORING REPORT (NDMR) Page _3_ of 3
Sampling Person(s) Certified Laboratories
Name:
Thomas Ammons (Environmental Hydrological Consultants)
Name:
Pace Analytical Lab/TBL
Name:
Jeff Scott
Name:
Campbell Soup Supply Company
Does all monitoring data and sampling frequencies meet the requirements in Attachment A of your permit? ❑ Compliant O Non -Compliant
If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective
action(s) taken. Attach additional sheets if necessary.
certification page for March 2024 DMR to check Non -Compliant vs Compliant as TDS was not specified to be analyzed during March sampling in error by our consultant.
Operator in Responsible Charge (ORC) Certification
Permittee Certification
ORC: Allan Baldwin
Permittee: Camppbell Soup Supply Company, LLC
Certification No.: 27196
Signing Official: Mark Rogers
Grade: 4 Phone Number: [phone]
Signing Official's Title: Associate VP - Site Operations
Has the ORC changed since the previous NDMR? ❑ yes O No
Phone Number: [phone] Permit Expiration: 4/30/2030
Signature Date
Signature Date
By this signature, I certify that this report is accurrate and complete to the best of my knowledge
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information
submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete I am
aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations
Mail Original and Two Copies to:
Division of Water Quality
Infunuatiun Prucessing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617

PaceAnalytical
ANALYTICAL REPORT
March 13, 2024
EHC, Inc.
Sample Delivery Group
Samples Received:
Project Number:
Description:
Site:
Report To:
L1712150
03/06/2024
17-M I0100-1
Campbell Soup Spray Effluent
MAXTON, NC
Mr. Thomas Ammons
PO Box 902
Red Springs, NC 28377
Entire Report Reviewed By: 4�41
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ,
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
I
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ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EHC, Inc. 17-MI0100-1 L1712150 03/13/24 08:10 1 of 18

TABLE OF CONTENTS
Cp: Cover Page
1
FP1
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
FSS
BI-MONTHLY (1ST) MAR L1712150-01
5
rqn
Qc: Quality Control Summary
7
Gravimetric Analysis by Method 2540 D-2015
7
Fr]
Wet Chemistry by Method 350.1
8
Wet Chemistry by Method 351.2
9
FQ Cl
Wet Chemistry by Method 365.4
11
GI
Wet Chemistry by Method 5210 B-2016
12
Wet Chemistry by Method 9056A
13
rAl
Metals (ICP) by Method 6010D
15
GI: Glossary of Terms
16
FC
Al: Accreditations & Locations
17
Sc: Sample Chain of Custody
18
ACCOUNT: PROJECT: SDG:
DATE/TIME:
PAGE:
EHC, Inc. 17-MI0100-1 L1712150
03/13/24 08:10
2 of 18

SAMPLE SUMMARY
Collected by
Collected date/time
Received date/time
BI-MONTHLY (1ST) MAR L1712150-01 GW
Thomas Ammons
03/05/2409:52
03/06/2409:00
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
Calculated Results
WG2241134
1
03/08/24 00:32
03/08/24 00:32
LDT
Mt. Juliet, TN
Gravimetric Analysis by Method 2540 D-2015
WG2243899
1
03/11/2414:38
03/11/2416:13
DLS
Mt. Juliet, TN
Wet Chemistry by Method 350.1
WG2241151
10
03/07/2412:58
03/07/2412:58
LAS
Mt. Juliet, TN
Wet Chemistry by Method 351.2
WG2241134
2
03/06/24 20:28
03/08/24 00:32
LDT
Mt. Juliet, TN
Wet Chemistry by Method 365.4
WG2242290
2
03/06/24 20:28
03/10/2418:11
LDT
Mt. Juliet, TN
Wet Chemistry by Method 5210 B-2016
WG2240852
10
03/06/2414:54
03/11/2414:14
MEL
Mt. Juliet, TN
Wet Chemistry by Method 9056A
WG2241044
1
03/06/24 21:18
03/06/24 21:18
GEB
Mt. Juliet, TN
Metals (ICP) by Method 6010D
WG2241619
1
03/07/2413:39
03/07/2418:02
ZSA
Mt. Juliet, TN
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EHC, Inc.
17-MI0100-1
L1712150
03/13/2408:10
3 of18
FP1
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
Heather J Wagner
Project Manager
FP1
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ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EHC, Inc. 17-MI0100-1 L1712150 03/13/24 08:10 4 of 18

BI-MONTHLY (1ST) MAR SAMPLE RESULTS - 01
Collected date/time: 03/05/24 09:52 L1712150
Additional Information - Results for field analyses are not accredited to ISO 17025
Analyte
pH (On Site)
Temperature (on -site)
Calculated Results
Result Units
3.7 su
52 Deg. C
Result Qualifier RDL
Analyte mg/I mg/I
Total Nitrogen 33.2 0.100
Gravimetric Analysis by Method 2540 D-2015
Result Qualifier RDL
Analyte mg/I mg/I
Suspended Solids 344 50.0
Wet Chemistry by Method 350.1
Result Qualifier RDL
Analyte mg/I mg/I
Ammonia Nitrogen ND 2.50
Sample Narrative:
L1712150-01 WG2241151: dilution due to sample matrix
Wet Chemistry by Method 351.2
Dilution Analysis Batch
date / time
1 03/08/2024 00:32 WG2241134
Dilution Analysis Batch
date / time
1 03/11/202416:13 WG2243899
Dilution Analysis Batch
date / time
10 03/07/202412:58 WG2241151
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I mg/I date / time
Kjeldahl Nitrogen, TKN 33.2 0.500 2 03/08/2024 00:32 WG2241134
Wet Chemistry by Method 365.4
Result Qualifier
RDL
Dilution
Analysis
Batch
Analyte mg/I
mg/I
date / time
Phosphorus,Total 5.54
0.200
2
03/10/202418:11
WG2242290
Wet Chemistry by Method 5210 B-2016
Result Qualifier
RDL
Dilution
Analysis
Batch
Analyte mg/I
mg/I
date / time
BOD 1240 K8 K9
2.00
10
03/11/202414:14
WG2240852
Wet Chemistry by Method 9056A
Result
Qualifier RDL
Analyte mg/I
mg/I
Chloride 68.9
1.00
Nitrate N D
0.100
Nitrite N D
0.100
Metals (ICP) by Method 6010D
Analyte
Cadmium
Calcium
Copper
Magnesium
Nickel
Sodium
ACCOUNT:
EHC, Inc.
Dilution Analysis
Batch
date / time
1 03/06/2024 21:18
WG2241044
1 03/06/2024 21:18
WG2241044
1 03/06/2024 21:18
WG2241044
Result
Qualifier RDL Dilution
Analysis
Batch
mg/I
mg/I
date / time
ND
0.00200 1
03/07/202418:02
WG2241619
2.98
1.00 1
03/07/202418:02
WG2241619
0.0298
0.0100 1
03/07/202418:02
WG2241619
3.36
1.00 1
03/07/202418:02
WG2241619
0.0128
0.0100 1
03/07/202418:02
WG2241619
78.4
3.00 1
03/07/202418:02
WG2241619
PROJECT:
SDG:
17-MI0100-1
L1712150
DATE/TIME: PAGE:
03/13/24 08:10 5 of 18
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SAMPLE RESULTS - 01
L1712150
BI-MONTHLY (1ST) MAR
Collected date/time: 03/05/24 09:52
Metals (ICP) by Method 6010D
Analyte
Zinc
Result Qualifier RDL
mg/I mg/I
0.394 0.0500
Dilution Analysis
date / time
1 03/07/202418:02
Batch
W62241619
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ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EHC, Inc. 17-MI0100-1 L1712150 03/13/24 08:10 6 of 18

WG2243899
Gravimetric Analysis by Method 2540 D-2015
Method Blank (MB)
(MB) R4044468-1 03/11/2416:13
MB Result MB Qualifier MB MDL
Analyte mg/I mg/1
Suspended Solids U 2.50
L1712118-03 Original Sample (OS) • Duplicate (DUP)
MB RDL
mg/I
2.50
QUALITY CONTROL SUMMARY
L1712150-01
(OS) L1712118-03 03/11/2416:13 • (DUP) R4044468-3 03/11/2416:13
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I % %
Suspended Solids 21.6 19.2 1 11.8 P1 10
L1712150-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1712150-01 03/11/2416:13 • (DUP) R4044468-4 03/11/2416:13
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I % %
Suspended Solids 344 356 1 3.43 10
Laboratory Control Sample (LCS)
(LCS) R4044468-2 03/11/2416:13
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I % %
Suspended Solids 773 788 102 85.0-115
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ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EHC, Inc. 17-MI0100-1 L1712150 03/13/24 08:10 7 of 18

WG2241151 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 350.1 L1712150-01
Method Blank (MB)
(MB) R4042900-1 03/07/2412:49
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/I mg/1 mg/I
Ammonia Nitrogen U 0.117 0.250
L1711683-15 Original Sample (OS) • Duplicate (DUP)
(OS) L1711683-15 03/07/2412:52 • (DUP) R4042900-3 03/07/2412:53
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I % %
Ammonia Nitrogen ND ND 1 0.000 10
L1712188-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1712188-02 03/07/2413:13 • (DUP) R4042900-7 03/07/2413:14
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I % %
Ammonia Nitrogen 0.712 0.776 1 8.60 10
Laboratory Control Sample (LCS)
(LCS) R4042900-2 03/07/2412:50
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I % %
Ammonia Nitrogen 7.50 7.48 99.7 90.0-110
L1711683-15 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1711683-15 03/07/2412:52 • (MS) R4042900-4 03/07/2412:55 • (MSD) R4042900-5 03/07/2412:56
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
Analyte mg/I
mg/I
mg/I
mg/I % % % %
Ammonia Nitrogen 5.00
ND
4.95
4.97 99.1 99.5 1 90.0-110 0.423
L1712188-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1712188-01 03/07/2413:10 • (MS) R4042900-6 03/07/2413:11
Spike Amount Original Result MS Result MS Rec.
Analyte mg/I mg/I mg/I %
Ammonia Nitrogen 5.00 ND 5.01 100
ACCOUNT:
EHC, Inc.
RPD Limits
10
Dilution Rec. Limits MS Qualifier
1 90.0-110
PROJECT: SDG: DATE/TIME: PAGE:
17-MI0100-1 L1712150 03/13/24 08:10 8 of 18
— I
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WG2241134
QUALITY CONTROL SUMMARY
Wet Chemistry by Method 351.2
L1712150-01
Method Blank (MB)
(MB) R4043060-1 03/07/24 22:30
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/I mg/I mg/I
Kjeldahl Nitrogen, TKN U 0.140 0.250
L1712O05-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1712005-01 03/07/24 22:32 • (DUP) R4043060-3 03/07/24 22:33
Original Result DUP Result Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I %
%
Kjeldahl Nitrogen, TKN 0.428 0.336 1 24.1
P1 20
L1712199-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1712199-01 03/07/24 22:51 • (DUP) R4043060-6 03/07/24 22:53
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I % %
Kjeldahl Nitrogen, TKN ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R4043060-2 03/07/24 22:31
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I % %
Kjeldahl Nitrogen, TKN 12.3 13.1 107 80.0-120
L1712O05-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1712005-01 03/07/24 22:32 • (MS) R4043060-4 03/07/24 22:35 • (MSD) R4043060-5 03/07/24 22:36
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
Analyte mg/I mg/I mg/I mg/I % % % %
Kjeldahl Nitrogen, TKN 5.00 0.428 2.13 6.79 34.0 127 1 90.0-110 J3 J5 104
Sample Narrative:
MS: Spike failure due to matrix interference
MSD: Spike failure due to matrix interference
RPD Limits
20
- I
Cp
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FSS
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FSr
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EHC, Inc. 17-MI0100-1 L1712150 03/13/24 08:10 9 of 18

WG2241134 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 351.2 L1712150-01
L1712199-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1712199-01 03/07/24 22:51 • (MS) R4043060-7 03/07/24 22:54
Spike Amount Original Result MS Result MS Rec.
Analyte mg/I mg/I mg/I %
Kjeldahl Nitrogen, TKN 5.00 ND 5.55 111
Sample Narrative:
MS: Spike failure due to matrix interference
Dilution Rec. Limits MS Qualifier
of
90.0-110 J5
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EHC, Inc. 17-MI0100-1 L1712150 03/13/24 08:10 10 of 18

WG2242290
Wet Chemistry by Method 365.4
Method Blank (MB)
(MB) R4043763-1 03/10/2417:38
MB Result MB Qualifier MB MDL
Analyte mg/I mg/I
Phosphorus,Total U 0.0350
L1712O05-01 Original Sample (OS) • Duplicate (DUP)
MB RDL
mg/I
0.100
QUALITY CONTROL SUMMARY
L1712150-01
(OS) L1712005-01 03/10/2417:41 • (DUP) R4043763-3 03/10/2417:42
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I _ % %
Phosphorus,Total 1.50 1.63 1 8.31 20
Sample Narrative:
OS: unknown matrix problem with ms, but sample confirmed with dup
L1712199-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1712199-01 03/10/2418:05 • (DUP) R4043763-5 03/10/2418:09
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I % %
Phosphorus,Total ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R4043763-2 03/10/2417:39
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I % %
Phosphorus,Total 1.81 1.73 95.8 85.0-115
L1712O05-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1712005-01 03/10/2417:41 • (MS) R4043763-6 03/10/2418:31 • (MSD) R4043763-4 03/10/2417:45
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
Analyte mg/I mg/I mg/I mg/I % % % %
Phosphorus,Total 2.50 1.50 1.13 2.51 0.000 40.4 1 90.0-110 J6 J3 J6 75.8
Sample Narrative:
OS: unknown matrix problem with ms, but sample confirmed with dup
MS: unknown matrix problem with ms, but sample confirmed with dup
RPD Limits
20
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EHC, Inc. 17-MI0100-1 L1712150 03/13/24 08:10 11 of 18

WG2240852
Wet Chemistry by Method 5210 B-2016
Method Blank (MB)
(MB) R4044135-1 03/11/2410:27
MB Result MB Qualifier MB MDL
MB RDL
Analyte mg/I mg/1
mg/I
BOD U 0.200
0.200
L1712O33-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1712033-01 03/11/2413:49 • (DUP) R4044135-3 03/11/2413:53
Original Result DUP Result Dilution DUP RPD
Analyte mg/I mg/I
BOD ND ND 1 0
L1712188-03 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1712150-01
DUP Qualifier DUP RPD
Limits
o�
30
(OS) L1712188-03 03/11/2415:06 • (DUP) R4044135-4 03/11/2415:08
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I % %
BOD ND ND 1 0 30
Laboratory Control Sample (LCS)
(LCS) R4044135-2 03/11/2413:15
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I % %
BOD 198 242 122 84.6-115 J+
Laboratory Control Sample (LCS)
(LCS) R4044135-5 03/11/2415:37
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I %
30D 198 213 107
Rec. Limits LCS Qualifier
o�
84.6-115
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EHC, Inc. 17-MI0100-1 L1712150 03/13/24 08:10 12 of 18

WG2241044
Wet Chemistry by Method 9056A
Method Blank (MB)
(MB) R4042828-3 03/06/24 08:42
MB Result
Analyte
mg/I
Chloride
U
Nitrate
U
Nitrite
U
MB Qualifier MB MDL
MB RDL
Mg/1
mg/I
0.379
1.00
0.0480
0.100
0.0420
0.100
L1712122-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1712150-01
(OS) L1712122-01 03/06/2418:05 • (DUP) R4042828-5 03/06/2418:44
Original Result
DUP Result
Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
Analyte
mg/I
mg/I
%
%
Chloride
15.9
16.0
1 0.590
15
Nitrate
ND
ND
1 1.06
15
Nitrite
ND
ND
1 11.8
15
L1712199-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1712199-01 03/06/24 21:56 • (DUP) R4042828-8 03/06/24 22:09
Original Result
DUP Result
Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
Analyte
mg/I
mg/I
%
%
Chloride
244
244
1 0.206
E 15
Nitrate
3.01
3.03
1 0.590
15
Nitrite
ND
ND
1 0.000
15
Laboratory Control Sample (LCS)
(LCS) R4042828-4 03/06/24 08:54
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
%
%
Chloride 40.0
39.5
98.8
80.0-120
Nitrate 8.00
7.69
96.1
80.0-120
Nitrite 8.00
8.04
100
80.0-120
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EHC, Inc. 17-MI0100-1 L1712150 03/13/24 08:10 13 of 18

WG2241044 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9056A L1712150-01
L1712122-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1712122-01 03/06/2418:05 • (MS) R4042828-6 03/06/2418:57 • (MSD) R4042828-7 03/06/2419:10
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
Chloride
40.0
15.9
53.2
52.9
93.3
92.6
Nitrate
8.00
ND
7.55
7.52
93.4
93.1
Nitrite
8.00
ND
8.01
7.93
99.2
98.2
L1712199-01 Original Sample (OS) • Matrix Spike (MS)
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
1 80.0-120 0.481
1 80.0-120 0.363
1 80.0-120 1.00
(OS) L1712199-01 03/06/24 21:56 • (MS) R4042828-9 03/06/24 22:22
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/I mg/I mg/I % %
Nitrate 8.00 3.01 10.3 91.3 1 80.0-120
Nitrite 8.00 ND 8.48 106 1 80.0-120
RPD Limits
15
15
15
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EHC, Inc. 17-MI0100-1 L1712150 03/13/24 08:10 14 of 18

WG2241619
Metals (ICP) by Method 6010D
Method Blank (MB)
(MB) R4042981-1 03/07/2417:15
MB Result
MB Qualifier MB MDL
Analyte mg/I
mg/I
Cadmium U
0.000479
Calcium U
0.0793
Copper U
0.00368
Magnesium U
0.0853
Nickel U
0.00161
Sodium U
0.504
Zinc U
0.00652
Laboratory Control Sample (LCS)
(LCS) R4042981-2 03/07/2417:17
Spike Amount
LCS Result
LCS Rec.
Analyte mg/I
mg/I
%
Cadmium 1.00
0.957
95.7
Calcium 10.0
9.58
95.8
Copper 1.00
1.05
105
Magnesium 10.0
10.3
103
Nickel 1.00
0.921
92.1
Sodium 10.0
9.76
97.6
Zinc 1.00
0.959
95.9
QUALITY CONTROL SUMMARY
L1712150-01
MB RDL
mg/I
0.00200
1.00
0.0100
1.00
0.0100
3.00
0.0500
Rec. Limits LCS Qualifier
°/
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
L1712129-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1712129-03 03/07/2417:18 • (MS) R4042981-4 03/07/2417:22 • (MSD) R4042981-5 03/07/2417:23
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
Cadmium
1.00
ND
1.00
1.01
100
101
Calcium
10.0
227
236
235
92.8
81.8
Copper
1.00
ND
1.04
1.05
103
104
Magnesium
10.0
103
111
111
82.2
77.7
Nickel
1.00
ND
0.990
0.988
98.5
98.3
Sodium
10.0
950
949
951
0.000
3.35
Zinc
1.00
ND
0.993
0.991
99.3
99.1
Dilution Rec. Limits
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
MS Qualifier MSD Qualifier RPD RPD Limits
0.791 20
0.469 20
0.865 20
0.412 20
0.199 20
V V 0.176 20
0.203 20
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EHC, Inc. 17-MI0100-1 L1712150
DATE/TIME:
03/13/24 08:10
PAGE:
15 of18

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
E
The analyte concentration exceeds the upper limit of the calibration range of the instrument established by the initial
calibration (ICAL).
J3
The associated batch QC was outside the established quality control range for precision.
J5
The sample matrix interfered with the ability to make any accurate determination; spike value is high.
J6
The sample matrix interfered with the ability to make any accurate determination; spike value is low.
J+
The associated batch QC was outside the upper control limits; associated data has a potential positive bias.
K8
Glucose/glutamic acid BOD/CBOD was above method acceptance levels.
K9
Test replicates show more than 30% difference between high and low values.
P1
RPD value not applicable for sample concentrations less than 5 times the reporting limit.
v
The sample concentration is too high to evaluate accurate spike recoveries.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EHC, Inc. 17-MI0100-1 L1712150 03/13/24 08:10 16 of 18

ACCREDITATIONS & LOCATIONS
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama
40660
Nebraska
NE-OS-15-05
Alaska
17-026
Nevada
TN000032021-1
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TN002
California
2932
New Mexico
TN00003
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolinas
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhodelsland
LA000356
Kentucky16
KY90010
South Carolina
84004002
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee' °
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas'
LAB0152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TN003
Vermont
VT2006
Michigan
9958
Virginia
110033
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A21-A
A21-A — ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A21-A — ISO 17025 s
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
Drinking Water 2 Underground Storage Tanks 'Aquatic Toxicity ° Chemical/Microbiological 'Mold 6 Wastewater n/a Accreditation not applicable
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
FP1
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ACCOUNT: PROJECT: SDG: DATE/TIME:
EHC, Inc. 17-MI0100-1 L1712150 03/13/24 08:10
PAGE:
17 of 18

-.
TBL
Shipping: Mailing-,
2401 W. 5th St. PO Box 589
Lumberton NC 28358 Lumberton, NC 28359
EHC ENVIRONMENTAL
PO BOX 902
RED SPRINGS, NC 28377
ATTN: THOMAS AMMONS
SAMPLE NUMBER - 40775
DATE SAMPLED - 3-5-24
DATE RECEIVED- 3-5-24
TIME RECEIVED - 0951
PAGE 1 OF 1
FINAL REPORT OF ANALYSES
Phone: [phone]
Fax: [phone]
Email: pam.hester-
[e-mail]
PROJECT NAME:CAMPBELL SOUP
REPORT DATE: 3-6-24
SAMPLE ID - BI-MONTHLY FECAL
SAMPLER - THOMAS AMMONS
DELIVERED BY - CLIENT
SAMPLE MATRIX - WW
TIME SAMPLED - 0902
RECEIVED BY - THK
QUAL
DET.
ANALYSIS
METHOD DATE
RESULT
UNITS CODE
LIMIT
BIOCHEMICAL OXYGEN DEMAND
SM5210-B
N/R
MG/L
2.0
TOTAL SUSPENDED SOLIDS
SM2540D
N/R
MG/L
AMMONIA NITROGEN
SM4500NH3D
N/R
MG/L
0.1
FECAL COLIFORM
SM9222D 3/5/2024
208,000
COL/100ML
1
CONDUCTIVITY
SM2510B
N/R
UMHOS/CM
10
CHEMICAL OXYGEN DEMAND
SM5220D
N/R
MG/L
30.0
PH
SM4500 H+B
N/R
STD UNITS
0.1
VOLATILE SUSPENDEDSOLIDS
SM2540E
N/R
MG/L
500
N/R = ANALYSIS NOT REQUESTED
LABORATORY DIRECTOR
NCDENR DWQ # 37, NCDENR DW # 37781

T B L ENVIRONMENTAL Bllllnngg Information:_.
Ana lysIslContainerlPreservative-
�f'1 l- t�- N tJ t �CO►.1 l��'
LABORATORY, INC.
2401 W. 5TH STREET d s was NC Z-937
LUMBERTON, NC 28358
[phone] mall [a: e�,tG f'�1+�+CctJS
rna��Co
P mj act ity/Sate
otectzd
Description: li.(-; AC�
�}
Phone: Client Project#: ESC Key:
FAX:
Collected by: � SltelFacllily ID#: P.0.#:
p
Collect d b slgnalure Rush? ( Lab MUST Be Notified) Date Results Needed;
Same Day ....... 200% No.
Next Day........ 100% Emalf? �No' Yes
N
CoCode (lab use only)
TemplatelPrelogln
Two Day .........50% of
Immediate eked on Ice N o FAX? _No Yes
Shipped Via:
Cntrs
Sample ID Camp/Grab Matrix' Depth Date Time
Remadhslconiaminant Sample # (lab only)
l t4L(QAMai.
09 r,4b
InS (�.�
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*Matrix. SS-SoIVSolid GW-Groundwaler VIMI-WasteWater DW-Drinking Water DT-Other pH Temp
marks:
Flow Other
Re quls d b . tgnalure)
Date:
�L
Recelved b ' J�� Samples returned via: ❑ UPS
❑ FedEx ❑ Courier ❑
Condition: (lab use only)
}
Re lin ed b SI nalure
Y� { g. )
.r
Received by: {Signature} _ Temp: Bottles Received:
Dale:
Time:
CoC Seals Intact: _ Y � N NA
Relinquished by: (Signature)
Date:
Time:
Recelved for lab by: (Signature) Dale:
Time:
pH Checked:
NCF:

Company Name/Address:
Billing Information: $
Analv�ic
/ fnntainar / Pracarvativa
Chain of Custody Page of_
EHC, Inc.
_
Accounts Payable Pres
PO Box 902 Chk
PO Box 902
Red Springs, NC 28377
% ���.�
�+
Red Springs, NC 28377
PEDVLE ADVANCING SCIENCE
tt4
?
MT JULIET, TN
Report to:
Email To: [e-mail]
Mr. Thomas Ammons
a
}
a
12065 Lebanon Rd Mount Juliet, TN 37122
Submitting a sample via this chain of custody
constitutes acknowledgment acceptance of the
R p
Project Description:
Cit State
Y/
Please Circle:
Campbell Soup Spray Effluent
Collected:
PT MT CT ET
°
UJ
ti
g
,
Vac Terms and Cond eons found at.
http // fo pacelabs com/hubf,/pas-standard-
term .pdf
Phone:[phone]
Client Project #
Lab Project #
#1yg71
17-M10100-1
ENVHYD-09-Mi1024-3
M
0SDG
0
0
C193
Collected by (print):
Site/Facility ID #
,�
nn
P.O. #1
Z
tt t
"dmas' i'tt^�+tio
S
MAXTON, NC
1
CL
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ttr
1
Acctnum: ENVHYD
Collected by (signature):
Rush? (Lab MUST Be Notified) Quote # L1
0
z
0
Template:T61121
Same Day _ Five Day »
.,
4
z`
Immediately
_ Next Day 5 Day (Rad only) Date Results Needed .
"
i
`"J
PreloRin: P1057141
_ Two Day _ to Day (Rad only) No alr'
PM: 873 —Heather J Wagner
Packed on Ice N _ Y
_ Three Day
of
`"3
Comp/Grab Matrix * Depth Date Time ntrs
I
�
Q
_!
11
�
f,AEG
edSample
p via: FGround
P
ID
- 0
�• _/ GW
Remarks Sample R (lab only)
/
.� 3'�' �l t6Z 5 X
JAL ��. - 1.� .�,�-
X
X
X
X
_...... - --..... _... —...... .... _ ..............................
* Matrix emarks:Metals = Cd, Ca, Cu, Mg, Ni, Na, Zn p �L� �j Q sample Recerpc �tlecri'tst
SS - Soil AIR - Air F- Filter i PH � Temp Coe seal Present 12..r,cl . NA Y N
GW- Groundwater B- Bioassay IOC. Sign ed/Accurat.e: :;y —_ N`
WW -Wastewater Flow Other Bottles arrive intact: >Y -._N.
DW- Drinking Water correct bottles used: Y N'
Samples returned via: efficient volumesent: Y N
OT - ther Tracking # � fi' if A1plicable
UPS ; )
FedEx _ Courier y
VOA Zero Headspa._e. Y N -
lank ed::""" o, P eservit ion Corre t./Checiked: Y N
Relin uis d by : (Sig re) Date: Time: Received by: (Signature) Trip Blank Received: Yes J No — ---
// - KZ�U Scrc _n <0.5
�.��.,� j� ,t/ HCl / MeoH
Relinqu ed by : (Signature)
Date:
Time:
Received by: (Signature) Temp:, °C Bottles Received: If pre PH-toeeHSozi iRc' 23 2 5" !?F.-1 Time
I CR6-20221 V
a
Relinquished by : (Signature)
Date:
Time:
Received for lfb by: (Signat a Cate Time: tf©id:--)nditlon:

PaceAnalytical
ANALYTICAL REPORT
March 25. 2024
EHC, Inc.
Sample Delivery Group
Samples Received:
Project Number:
Description:
Site:
Report To:
L1714532
03/13/2024
17-M I0100-1
Campbell Soup Spray Effluent
MAXTON, NC
Mr. Thomas Ammons
PO Box 902
Red Springs, NC 28377
Entire Report Reviewed By: 4�41
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ,
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
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EHC, Inc. 17-MI0100-1 L1714532 03/25/24 09:28 1 of 18

TABLE OF CONTENTS
Cp: Cover Page
1
FP1
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
FSS
MARCH BI-MONTHLY-2ND L1714532-01
5
rqn
Qc: Quality Control Summary
6
Gravimetric Analysis by Method 2540 D-2015
6
Fr]
Wet Chemistry by Method 350.1
7
Wet Chemistry by Method 351.2
8
FQ Cl
Wet Chemistry by Method 365.4
10
GI
Wet Chemistry by Method 5210 B-2016
11
Wet Chemistry by Method 9056A
12
rAl
Metals (ICP) by Method 6010D
14
GI: Glossary of Terms
16
FC
Al: Accreditations & Locations
17
Sc: Sample Chain of Custody
18
ACCOUNT: PROJECT: SDG:
DATE/TIME:
PAGE:
EHC, Inc. 17-MI0100-1 L1714532
03/25/24 09:28
2 of 18

SAMPLE SUMMARY
MARCH BI-MONTHLY-2ND L1714532-01 GW
Collected by
Thomas Ammons
Collected date/time
03/12/2412:50
Received date/time
03/13/2408:45
Method
Batch
Dilution Preparation
Analysis
Analyst
Location
date/time
date/time
Calculated Results
WG2247242
1 03/22/2416:34
03/22/2416:34
CAT
Mt. Juliet, TN
Gravimetric Analysis by Method 2540 D-2015
WG2247709
1 03/19/2411:57
03/19/2415:35
DLS
Mt. Juliet, TN
Wet Chemistry by Method 350.1
WG2246081
1 03/14/2414:01
03/14/2414:01
LAS
Mt. Juliet, TN
Wet Chemistry by Method 351.2
WG2247242
2 03/15/2413:30
03/22/2416:34
CAT
Mt. Juliet, TN
Wet Chemistry by Method 365.4
WG2251809
1 03/15/2413:30
03/22/2418:51
CAT
Mt. Juliet, TN
Wet Chemistry by Method 5210 B-2016
WG2245649
10 03/13/2413:12
03/18/2410:28
MEL
Mt. Juliet, TN
Wet Chemistry by Method 9056A
WG2245737
1 03/13/2416:36
03/13/2416:36
DLH
Mt. Juliet, TN
Metals (ICP) by Method 6010D
WG2246497
1 03/15/2416:33
03/17/2412:45
ZSA
Mt. Juliet, TN
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EHC, Inc.
17-MI0100-1
L1714532
03/25/24 09:28
3 of 18
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
Heather J Wagner
Project Manager
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EHC, Inc. 17-MI0100-1 L1714532 03/25/24 09:28 4 of 18

MARCH BI-MONTHLY-2ND SAMPLE RESULTS - 01
Collected date/time: 03/12/24 12:50 L1714532
Additional Information - Results for field analyses are not accredited to ISO 17025
Analyte
pH (On Site)
Temperature (on -site)
Calculated Results
Result Units
3.19 su
60 Deg. C
Result Qualifier RDL
Analyte mg/I mg/I
Total Nitrogen 31.8 0.100
Gravimetric Analysis by Method 2540 D-2015
Dilution Analysis Batch
date / time
1 03/22/202416:34 WG2247242
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I mg/I date / time
Suspended Solids 283 41.7 1 03/19/202415:35 WG2247709
Wet Chemistry by Method 350.1
Result
Qualifier RDL
Dilution Analysis
Batch
Analyte mg/I
mg/I
date / time
Ammonia Nitrogen 3.14
0.250
1 03/14/202414:01
WG2246081
Wet Chemistry by Method 351.2
Result
Qualifier RDL
Dilution Analysis
Batch
Analyte mg/I
mg/I
date / time
Kjeldahl Nitrogen, TKN 31.8
0.500
2 03/22/202416:34
WG2247242
Wet Chemistry by Method 365.4
Result
Qualifier
RDL
Dilution
Analysis
Batch
Analyte mg/I
mg/I
date / time
Phosphorus,Total 4.65
0.100
1
03/22/202418:51
WG2251809
Wet Chemistry by Method 5210 B-2016
Result
Qualifier
RDL
Dilution
Analysis
Batch
Analyte mg/I
mg/I
date / time
BOD 1170
K5
2.00
10
03/18/202410:28
WG2245649
Wet Chemistry by Method 9056A
Result
Qualifier
RDL
Dilution
Analysis
Batch
Analyte mg/I
mg/I
date / time
Chloride 111
1.00
1
03/13/202416:36
WG2245737
Nitrate ND
0.100
1
03/13/202416:36
WG2245737
Nitrite ND
0.100
1
03/13/202416:36
WG2245737
Metals (ICP) by Method 6010D
Result
Qualifier
RDL
Dilution
Analysis
Batch
Analyte mg/I
mg/I
date / time
Cadmium ND
0.00200
1
03/17/202412:45
WG2246497
Calcium 4.00
1.00
1
03/17/202412:45
WG2246497
Copper 0.0132
0.0100
1
03/17/202412:45
WG2246497
Magnesium 4.90
1.00
1
03/17/202412:45
WG2246497
Nickel 0.0104
0.0100
1
03/17/202412:45
WG2246497
Sodium 101
3.00
1
03/17/202412:45
WG2246497
Zinc 0.424
0.0500
1
03/17/202412:45
WG2246497
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
EHC, Inc.
17-MI0100-1
L1714532
03/25/24 09:28 5 of 18

WG2247709
Gravimetric Analysis by Method 2540 D-2015
Method Blank (MB)
(MB) R4047801-1 03/19/2415:35
MB Result MB Qualifier MB MDL
Analyte mg/I mg/1
Suspended Solids U 2.50
MB RDL
mg/I
2.50
QUALITY CONTROL SUMMARY
L1714532-01
L1714532-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1714532-01 03/19/2415:35 • (DUP) R4047801-3 03/19/2415:35
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I % %
Suspended Solids 283 277 1 2.38 10
L1714558-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1714558-01 03/19/2415:35 • (DUP) R4047801-4 03/19/2415:35
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I % %
Suspended Solids 35.0 29.0 1 18.8 P1 10
Laboratory Control Sample (LCS)
(LCS) R4047801-2 03/19/2415:35
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I %
Suspended Solids 773 796 103
Rec. Limits LCS Qualifier
85.0-115
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EHC, Inc.
PROJECT: SDG: DATE/TIME: PAGE:
17-MI0100-1 L1714532 03/25/24 09:28 6 of 18

WG2246081
Wet Chemistry by Method 350.1
Method Blank (MB)
(MB) R4045699-1 03/14/2413:41
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/I mg/1 mg/I
Ammonia Nitrogen U 0.117 0.250
L1714560-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1714560-01 03/14/2414:10 • (DUP) R4045699-3 03/14/2414:11
Original Result DUP Result Dilution DUP RPD
Analyte mg/I mg/I %
Ammonia Nitrogen 1.20 1.20 1 0.167
L1714569-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1714532-01
DUP Qualifier DUP RPD
Limits
10
(OS) L1714569-01 03/14/2414:23 • (DUP) R4045699-6 03/14/2414:25
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I % %
Ammonia Nitrogen ND ND 1 0.000 10
Laboratory Control Sample (LCS)
(LCS) R4045699-2 03/14/2413:43
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I % %
Ammonia Nitrogen 7.50 7.33 97.7 90.0-110
L1714560-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1714560-01 03/14/2414:10 • (MS) R4045699-4 03/14/2414:13 • (MSD) R4045699-5 03/14/2414:14
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec.
Analyte mg/I mg/I mg/I mg/I % %
Ammonia Nitrogen 5.00 1.20 6.15 6.18 99.0 99.5
L1714569-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1714569-01 03/14/2414:23 • (MS) R4045699-7 03/14/2414:26
Spike Amount Original Result MS Result MS Rec.
Analyte mg/I mg/I mg/I %
Ammonia Nitrogen 5.00 ND 4.79 95.8
ACCOUNT:
EHC, Inc.
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
1 90.0-110 0.438
RPD Limits
10
Dilution Rec. Limits MS Qualifier
1 90.0-110
PROJECT: SDG: DATE/TIME: PAGE:
17-MI0100-1 L1714532 03/25/24 09:28 7 of 18
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WG2247242
Wet Chemistry by Method 351.2
Method Blank (MB)
(MB) R4048959-1 03/22/2415:25
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/I mg/I mg/I
Kjeldahl Nitrogen, TKN U 0.140 0.250
L1714383-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1714383-01 03/22/2416:30 • (DUP) R4048959-3 03/22/2415:30
Original Result DUP Result Dilution DUP RPD
Analyte mg/I mg/I %
Kjeldahl Nitrogen, TKN 0.588 0.883 1 40.1
L1714392-02 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1714532-01
DUP Qualifier DUP RPD
Limits
P1 20
(OS) L1714392-02 03/22/2415:55 • (DUP) R4048959-6 03/22/2415:57
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I % %
Kjeldahl Nitrogen, TKN 0.371 0.342 1 8.13 20
Laboratory Control Sample (LCS)
(LCS) R4048959-2 03/22/2415:26
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I % %
Kjeldahl Nitrogen, TKN 12.3 12.8 104 80.0-120
L1714387-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1714387-04 03/22/2415:43 • (MS) R4048959-4 03/22/2415:44 • (MSD) R4048959-5 03/22/2415:45
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec.
Analyte mg/I mg/I mg/I mg/I % %
Kjeldahl Nitrogen, TKN 5.00 0.796 6.59 6.65 116 117
Sample Narrative:
MS: Spike failure due to matrix interference
MSD: Spike failure due to matrix interference
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
1 90.0-110 0.906
RPD Limits
20
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W G2247242
Wet Chemistry by Method 351.2
QUALITY CONTROL SUMMARY
L1714532-01
L1714483-02 Original Sample (OS) • Matrix Spike (MS)
(OS) L1714483-02 03/22/2415:59 • (MS) R4048959-7 03/22/2416:00
Spike Amount Original Result MS Result MS Rec.
Analyte mg/1 mg/1 mg/I %
Kjeldahl Nitrogen, TKN 5.00 1.20 6.30 102
Dilution Rec. Limits MS Qualifier
o/1
1 90.0-110
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WG2251809 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 365.4 L1714532-01
Method Blank (MB)
(MB) R4049004-1 03/22/2417:57
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/I mg/I mg/I
Phosphorus,Total U
0.0350 0.100
L1714383-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1714383-01 03/22/2418:00 • (DUP) R4049004-3 03/22/2418:01
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I _ mg/I % %
Phosphorus,Total ND ND 1 0.000 20
L1714392-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1714392-02 03/22/2418:48 • (DUP) R4049004-12 03/22/2418:49
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I % %
Phosphorus,Total ND ND 1 0.836 20
Laboratory Control Sample (LCS)
(LCS) R4049004-2 03/22/2417:58
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I % %
Phosphorus,Total 1.81 1.67 92.5 85.0-115
L1714387-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1714387-04 03/22/2418:43 • (MS) R4049004-10 03/22/2418:44 • (MSD) R4049004-11 03/22/2418:45
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
Analyte mg/I mg/I mg/I mg/I % % % %
Phosphorus,Total 2.50 ND 0.966 0.971 35.9 36.1 1 90.0-110 0.516
Sample Narrative:
MS: spike failed due to sample matrix
MSD: spike failed due to sample matrix
RPD Limits
20
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EHC, Inc. 17-MI0100-1 L1714532 03/25/24 09:28 10 of 18

WG2245649
Wet Chemistry by Method 5210 B-2016
Method Blank (MB)
(MB) R4046842-1 03/18/24 09:29
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/I mg/1 mg/I
BOD 0.373 B1 0.200 0.200
L1714294-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1714294-01 03/18/2410:01 • (DUP) R4046842-3 03/18/2410:04
Original Result DUP Result Dilution DUP RPD
Analyte mg/I mg/I %
BOD 14.6 14.7 1 0.547
L1714393-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1714532-01
DUP Qualifier DUP RPD
Limits
o�
30
(OS) L1714393-01 03/18/2410:19 • (DUP) R4046842-4 03/18/2410:21
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I % %
BOD ND ND 1 0 30
Laboratory Control Sample (LCS)
(LCS) R4046842-2 03/18/24 09:39
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I %
BOD 198 210 106
Laboratory Control Sample (LCS)
Rec. Limits LCS Qualifier
84.6-115
(LCS) R4046842-5 03/18/2411:01
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I % %
BOD 198 216 109 84.6-115
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WG2245737
Wet Chemistry by Method 9056A
Method Blank (MB)
(MB) R4046849-1 03/13/2410:41
MB Result
Analyte mg/I
Chloride U
Nitrate U
Nitrite U
MB Qualifier MB MDL
MB RDL
Mg/1
mg/I
0.379
1.00
0.0480
0.100
0.0420
0.100
L171120O-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1714532-01
(OS) L1711200-01 03/13/2413:00 • (DUP) R4046849-3 03/13/2413:12
Original Result
DUP Result
Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
Analyte
mg/I
mg/I
%
%
Chloride
189
188
1 0.279
15
Nitrate
5.01
4.91
1 2.02
15
Nitrite
ND
ND
1 0.000
15
L1714539-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1714539-01 03/13/2417:15 • (DUP) R4046849-6 03/13/2417:27
Original Result
DUP Result
Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
Analyte
mg/I
mg/I
%
%
Chloride
1.24
1.22
1 1.65
15
Nitrate
ND
ND
1 0.000
15
Nitrite
ND
ND
1 0.000
15
Laboratory Control Sample (LCS)
(LCS) R4046849-2 03/13/2410:54
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
%
%
Chloride 40.0
39.3
98.2
80.0-120
Nitrate 8.00
7.80
97.5
80.0-120
Nitrite 8.00
7.78
97.3
80.0-120
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EHC, Inc. 17-MI0100-1 L1714532 03/25/24 09:28 12 of 18

WG2245737 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9056A L1714532-01
L17112OO-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1711200-01 03/13/2413:00 • (MS) R4046849-4 03/13/2413:25 • (MSD) R4046849-5 03/13/2413:38
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
Chloride
40.0
189
191
190
6.20
4.50
Nitrate
8.00
5.01
11.9
11.9
85.8
85.8
Nitrite
8.00
ND
7.76
7.76
97.0
97.0
Sample Narrative:
MS: Cl/SO4 spike failed due to sample matrix
MSD: Cl/SO4 spike failed due to sample matrix
L1714539-01 Original Sample (OS) • Matrix Spike (MS)
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
1 80.0-120 V V_ 0.357
1 80.0-120 0.0168
1 80.0-120 0.0696
(OS) L1714539-01 03/13/2417:15 • (MS) R4046849-7 03/13/2417:40
Spike Amount
Original Result
MS Result
MS Rec.
Dilution Rec. Limits MS Qualifier
Analyte
mg/I
mg/I
mg/I
%
%
Chloride
40.0
1.24
41.5
101
1 80.0-120
Nitrate
8.00
ND
8.78
110
1 80.0-120
Nitrite
8.00
ND
8.09
101
1 80.0-120
RPD Limits
15
15
15
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EHC, Inc. 17-MI0100-1
SDG: DATE/TIME: PAGE:
L1714532 03/25/24 09:28 13 of 18

WG2246497
Metals (ICP) by Method 6010D
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1714532-01
(MB) R4046565-1 03/17/2411:10
MB Result
MB Qualifier MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
Cadmium U
0.000479
0.00200
Calcium U
0.0793
1.00
Copper U
0.00368
0.0100
Magnesium U
0.0853
1.00
Nickel U
0.00161
0.0100
Sodium U
0.504
3.00
Zinc U
0.00652
0.0500
Laboratory Control Sample (LCS)
(LCS) R4046565-2 03/17/2411:13
Spike Amount
LCS Result
LCS Rec.
Rec. Limits
LCS Qualifier
Analyte
mg/I
mg/I
%
%
Cadmium
1.00
1.01
101
80.0-120
Calcium
10.0
10.2
102
80.0-120
Copper
1.00
0.979
97.9
80.0-120
Magnesium
10.0
10.2
102
80.0-120
Nickel
1.00
1.01
101
80.0-120
Sodium
10.0
9.91
99.1
80.0-120
Zinc
1.00
1.03
103
80.0-120
L1714458-06 Original Sample
(OS) • Matrix
Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1714458-06
03/17/2411:16 • (MS) R4046565-4 03/17/2411:21 • (MSD)
R4046565-5
03/17/2411:24
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec. Dilution
Rec. Limits
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
%
Cadmium
1.00
ND
0.994
0.997
99.4
99.7 1
75.0-125
Calcium
10.0
39.6
48.9
48.8
93.5
92.2 1
75.0-125
Copper
1.00
ND
0.998
0.988
99.5
98.5 1
75.0-125
Magnesium
10.0
6.40
16.1
16.2
97.2
97.6 1
75.0-125
Nickel
1.00
ND
1.00
1.00
100
100 1
75.0-125
Sodium
10.0
ND
11.6
11.7
96.9
97.8 1
75.0-125
Zinc
1.00
ND
1.05
1.05
102
102 1
75.0-125
MS Qualifier
MSD Qualifier RPD
0.280
0.261
0.919
0.218
0.0742
0.710
0.0915
RPD Limits
20
20
20
20
20
20
20
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ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EHC, Inc. 17-MI0100-1 L1714532 03/25/24 09:28 14 of 18

WG2246497 QUALITY CONTROL SUMMARY
Metals (ICP) by Method 6010D L1714532-01
L1714460-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1714460-05 03/17/2411:27 • (MS) R4046565-6 03/17/2411:29 • (MSD) R4046565-7 03/17/2411:32
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
Cadmium
1.00
ND
1.01
0.999
101
99.9
Calcium
10.0
42.2
51.6
51.7
94.2
94.8
Copper
1.00
ND
1.00
0.997
99.4
99.0
Magnesium
10.0
6.60
16.5
16.4
98.6
98.4
Nickel
1.00
ND
1.01
1.00
101
100
Sodium
10.0
ND
12.0
11.8
99.1
97.5
Zinc
1.00
0.0526
1.08
1.07
103
101
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
1 75.0-125
1.00
20
1 75.0-125
0.117
20
1 75.0-125
0.378
20
1 75.0-125
0.142
20
1 75.0-125
0.936
20
1 75.0-125
1.38
20
1 75.0-125
1.17
20
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EHC, Inc. 17-MI0100-1 L1714532 03/25/24 09:28 15 of 18

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
131
The blank depletion was greater than the recommended maximum depletion of 0.2mg/L.
J5
The sample matrix interfered with the ability to make any accurate determination; spike value is high.
J6
The sample matrix interfered with the ability to make any accurate determination; spike value is low.
K5
The Dilution water D.O. depletion was > 0.2 mg/L.
P1
RPD value not applicable for sample concentrations less than 5 times the reporting limit.
v
The sample concentration is too high to evaluate accurate spike recoveries.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EHC, Inc.
17-MI0100-1 L1714532 03/25/24 09:28 16 of 18

ACCREDITATIONS & LOCATIONS
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama
40660
Nebraska
NE-OS-15-05
Alaska
17-026
Nevada
TN000032021-1
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TN002
California
2932
New Mexico
TN00003
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolinas
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhodelsland
LA000356
Kentucky16
KY90010
South Carolina
84004002
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee' °
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas'
LAB0152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TN003
Vermont
VT2006
Michigan
9958
Virginia
110033
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A21-A
A21-A — ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A21-A — ISO 17025 s
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
Drinking Water 2 Underground Storage Tanks 'Aquatic Toxicity ° Chemical/Microbiological 'Mold 6 Wastewater n/a Accreditation not applicable
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
FP1
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ACCOUNT: PROJECT: SDG: DATE/TIME:
EHC, Inc. 17-MI0100-1 L1714532 03/25/24 09:28
PAGE:
17 of 18

Shipping: Mailin :
2401 W. 5th St. PO Box 589
Lumberton NC 28358 Lumberton, NC 28359
TBL
EHC ENVIRONMENTAL
PO BOX 902
RED SPRINGS, NC 28377
ATTN: THOMAS AMMONS
SAMPLE NUMBER - 40884
DATE SAMPLED - 3-12-24
DATE RECEIVED- 3-13-24
TIME RECEIVED - 1412
PAGE 1 OF 1
FINAL REPORT OF ANALYSES
Phone: [phone]
Fax: [phone]
Email:pam.hester-
tbi hotmaiI.com
PROJECT NAME:CAMPBELL SOUP
REPORT DATE: 3-13-24
SAMPLE ID - BI-MONTHLY FECAL
SAMPLER - THOMAS AMMONS
DELIVERED BY - CLIENT
SAMPLE MATRIX - WW
TIME SAMPLED - 1300
RECEIVED BY - THK
QUAL
DET.
ANALYSIS
METHOD DATE
RESULT
UNITS CODE
LIMIT
BIOCHEMICAL OXYGEN DEMANDSM5210-B
N/R
MG/L
2.0
TOTAL SUSPENDED SOLIDS
SM2540D
N/R
MG/L
AMMONIA NITROGEN
SM450ONH30
N/R
MG/L
0.1
FECAL COLIFORM
SM9222D 3/12/2024
<2,000
COL/1001VIL
1
CONDUCTIVITY
SM25103
N/R
UMHOS/CM
10
CHEMICAL OXYGEN DEMAND
SM5220D
N/R
MG/L
30.0
PH
SM4500 H+B
N/R
STD UNITS
0.1
VOLATILE SUSPENDED SOLIDS
SM2540E
N/R
MG/L
500
N/R = ANALYSIS NOT REQUESTED
LABORATORY DIRECTOR �—
NCDENR DWQ # 37, NCDENR DW # 37781

TB L ENVIRONMENTAL
LABORATORY, INC.
2401 W. 5T" STREET
LUMBERTON, NC 28358
910 370-0371
91111ng Information:._
(P6 la� qGz
Rom- 5?0`55 z3
AnalysislContalnerlPreservative
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Project 1 j
Description: l gt �,0�1\
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Phone:
FAX: 4D -IA 3 -T
Client Project #:
ESC Key:
Collected by:
wtr++ax/ t
SltelFacllity ID#:
CoCode (lab use only)
Shipped Via:
Cootedylgna e):
on Ice N Y
Rush? ( Lab MUST Be Notified)
Same Day.......200%
Next Day........ 100%
Two Day .........50%
°
Date Results Needed:
No.
ofimcked
Email? No_YesTemplatelPrelogin
—
FAX? No Yes
Sample ID
Comp/Grab
Matrix`(
Depth
Date
Time
Cntrs
Remarks/Contaminant
Sample it (lab only)
off,
"Matrix. SS - Soll/Solid GW - Groundwater WW - WasteWater DW - Drinking Water OT - Other•
RerParks:
PH Temp
Flow Other
[Rel Ishe lure)
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€Zelinq is by: (Slgnalure)
Dale:
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Receive gn u Samples returned via: El UPS
❑ FedEx ❑ Courier ❑
Received by: (Slgnalure) Temp: Bottles Received:
Condition: (lab use only)
Date:
Time:
CoC Seals Intact: _ Y _ N NA
Relinquished by: (Signature)
Dale:
Time:
Received for lab by: (Signature) Dale:
Time:
pH Checked:
NCF:

Coc,pdny Name/Address:
EHC Inc..
Billing Information
n vci
/ f nntaina Pra<anrativa
Chain of Custody Page _ of
—
'
Accounts Payable Pres
PO Box 902 Chk
PO Box 902
Red Springs, NC 28377
ace,
Red Springs, NC 28377
PEOPLE ADVANCING SCIENCE
MT JULIET, TN
Report to:
Email To: [e-mail] _
Mr. Thomas Ammons
X
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et
QJ
,
j
12065 Lebanon Rd Mount Juliet, TN 37122
Submitting a sample via th s cha n of custody
constitutes acknov,ledgmentand acceptanceofthe
Project Description:
City/State
Please Circle:
Campbell Sou Spray Effluent
P P P Y
Collected:
PT MT CT ET
@
Pace Terms and Condtion, round at
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(
hops // nfo pacelabs.com/hubf,/pas standard
terms pdf
Client
Phone: [phone]
Project #
Lab Project #
SDG# /
17-M10100-1
ENVHYO 09 M11024 3
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Collected by (print):
Site/Facie±y !D #
P.O. # W
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MAXTON, NC
m `
A cctnum:ENVHYD
Collec e by (signature):
Rush? (Lab MUST Be Notified) Quote #
(
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Template:T61121
Same Day Five Day M2.
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_ Next Day _ 5 Day (Bad Only) Date Results Needed r
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PM 873 - Heather i Wagner
_ y
_ ThreeDay o' q 1
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Shipped via: FJdEX'Ground
Sample ID
Remarks Sample If (lab only)
'
Gw 3_j2-Z'i `Z;'Sz, 5 x
-- --
x
x
x
x_
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- ---- ---- .....
_
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• Matrix: emarks:Metals = Cd, Ca, Cu, Mg, Ni, Na, Zn ,jQ 5ampLe Re�F1pc �he< xL fist
SS -Soil AIR -Air F-Filter t;.'�1 3.�e Temp �e� X
pH COC seal Present/intact. tan I
GW- Groundwater B- Bioassay COC Signed/Accurate: r N
i
WW •Wastewater Flow Other Bottles arriverntact: � __N'
Correct bottl_.r used: 'y N
DW- Drinking Water —N
Samples returned via: Sufficient volulle sent: 'I
OT - Oth r Tracking #
z f �J 1 cat: le
UPS FedEx Courier V0A Zero
Headspane. y N
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Relinq •shed : (Signature)
Date:
Time:
Received by: (Signature)
_
Temp, oC Bottles Received: If preservation required by Login: Date/Time
Relinquished by : (Signature)
Date:
Time:
Received for lab by:,(Signa e)
Date: Time Hold: Condltlon:NCF