NC0074268_More Information (Received)_20240424

Action History (UTC-05:00) Eastern Time (US & Canada)
Submit by Anonymous User 4/24/2024 11:54:13 AM (Supplemental Submittal)
Submit by bradley.bennett 7/10/2024 3:00:35 PM (Supplemental Info Submittal)
• The task was assigned to Wren.Thedford, bradley.bennett 4/24/2024 11:54:14 AM
• bradley.bennett assigned the task to bradley.bennett 7/10/2024 2:57:50 PM

Initial Review Information
.........
Updated ID#: * IMPORTANT: REVIEWER SHOULD VERIFY and revise here if necessary.
NCO074268
How should this project be handled? *
File Discard
Information Submitted on 4/24/2024
Submitter Information
Name: David Shellenbarger
Who is submitting the information?
Email Address:* [e-mail]
Submittal Information
The Division of Water Resources (DWR) is providing this site to allow for the upload of required supplemental information
associated with discharge monitoring reports (DMR). All DMR data is required to be submitted electronically through
the eDMR system and should not be submitted here. Division staff will review all uploaded documents and will only
maintain required information. Documents such as laboratory reports are not required to be submitted and will not be
maintained in the system.
Project Information:
Please supply the permit number for this project.
...............................................................................................................................
Existing ID#* Permit Number
NCO074268
Examples: NCxxxxxxx or NCGxxxxxx
Facility Name: * Crowders Creek WWTP
County: Gaston
Please upload all files that need to be submited. *
Click the upload button or drag and drop files here to attach document
DMR-PPA-1 Crowders Creek WWTP NC0074268.pdf 25.02MB
Only pdf files are accepted.
Please provide descriptive comments about the attached information.
Please find the attached results for the 2024 Priority Pollutant Analysis analyzed on effluent from the City of Gastonia's
Crowders Creek WWTP.
* By checking the box and signing box below, I certify that:
o I have given true, accurate, and complete information on this form;

• I agree that submission of this Supplemental Information form is a "transaction" subject to Chapter 66, Article 40 of the
NC General Statutes (the "Uniform Electronic Transactions Act')
• I agree to conduct this transaction by electronic means pursuant to Chapter 66, Article 40 of the NC General Statutes
(the "Uniform Electronic Transactions Act');
• I understand that an electronic signature has the same legal effect and can be enforced in the same way as a written
signature; AND
• I intend to electronically sign and submit the Supplemental Information form."
Full Name: David Shellenbarger
Signature:
Date Submitted: 04/24/2024

Annual Monitoring and Pollutant Scan
Permit No. NCO074268 Month June
Outfall 001 Year 2023
Facility Name Crowders Creek WWTP ORC Thomas Carlos Lopez
Date of sampling 3 / 19 / 2024 Phone [phone]
Analytical Laboratory City of Gastonia - Crowders Creek Laboratory(#210), Pace Analytical Services - Asheville (#40)
Pace Analytical Services - Charlotte (#12), Pace Analytical Services - Columbia (#329)
ara .e, e �
_.A.-.
" ar, stark
Cade
arniile p
_ ��
�., �na � t�ca Nf tlCicrd
. Qu ntitatiioWu,
eve
,
� Urits:af
ensure en
. .. _
Ammonia (as N)
C0610
Composite
SM4500 NH3 D
0.2
0.4,
mg/L
Chlorine (total residual, TRC)
50060
Grab
SM4500 CL G
20
<20
ug/L
Dissolved Oxygen
00300
Grab
SM 4500 O G
0.1
10.2
mg/L
Nitrite plus Nitrate Total (as N)
00630
Composite
SM4500 NO3 F-NO2
0.5
5
mg/L
Total Kjeldahl Nitrogen
00625
Composite
SM4500 NORG C
1.0
3.8
mg/L
Oil and Grease
00556
Grab
1664 B
4.8
<4.8
mg/L
Total Phosphorus
C0665
Composite
SM4500 P E
0.05
0.3
mg/L
Total Dissolved Solids
70295
Composite
SM2540C
50
356
mg/L
Hardness
00900
Composite
EPA 200.7
662
61,400
ug/L
eta st taleo�erae varzd
Antimony
a tQ
01097
e�no
Composite
EPA 200.8
1.0
1.4
ug/L
Arsenic
01002
Composite
EPA 200.8
1.0
<1.0
ug/L
Beryllium
01012
Composite
EPA 200.8
1.0
<1.0
ug/L
Cadmium
01027
Composite
EPA 200.8
0.5
<0.5
ug/L
Chromium
01034
Composite
EPA 200.8
1.0
<1.0
ug/L
Copper
01042
Composite
EPA 200.8
1.0
1.8
ug/L
Lead
01051
Composite
EPA 200.8
1.0
<1.0
ug/L
Mercury (Method 1631E)
COMER
Grab
EPA 1631 E
1.0
1.1
ng/L
Nickel
01067
Composite
EPA 200.8
1.0
5.6
ug/L
Selenium
01147
Composite
EPA 200.8
1.0
<1.0
ug/L
Silver
01077
Composite
EPA 200.8
1.0
<1.0
ug/L
Thallium
01059
Composite
EPA 200.8
1.0
<1.0
ug/L
Zinc
01092
Composite
EPA 200.8
10.0
44.4
ug/L
Cyanide
00720
Grab
SM4500-CN
10
<10
ug/L
Total phenolic compounds
32730
Grab
EPA 420.4
0.050
<0.050
mg/L
,
Acrolein*
34210
Grab
EPA 624.1
5.0
<5.0
ug/L
Acrylonitrile*
34215
Grab
EPA 624.1
, .0
<5.0
ug/L
Benzene
34030
Grab
EPA 624.1
1.0
<1.0
ug/L
Bromoform
32104
Grab
EPA 624.1
2.0
<2.0
ug/L
Carbon Tetrachloride
32102
Grab
EPA 624.1
2.0
<2.0
ug/L
Chlorobenzene
34301
Grab
EPA 624.1
2.0
<2.0
ug/L
Chlorodibromomethane
34306
Grab
EPA 624.1
2.0
<2.0
ug/L
Chloroethane
85811
Grab
EPA 624.1
2.0
<2.0
ug/L
2-chloroethyl vinyl ether
34576
Grab
EPA 624.1
5.0
<5.0
ug/L
Chloroform
32106
Grab
EPA 624.1
2.0
6.7
ug/L
Dichlorobromomethane
32101
Grab
EPA 624.1
2.0
<2.0
ug/L
1,1-dichloroethane
34496
Grab
EPA 624.1
2.0
<2.0
ug/L
1,2-dichloroethane
32103
Grab
EPA 624.1
2.0
<2.0
ug/L
Trans-1,2-dichloroethylene
34546
Grab
EPA 624.1
2.0
<2.0
ug/L
1,1-dichloroethylene
34501
Grab
EPA 624.1
2.0
<2.0
ug/L
1,2-dichloropropane
34541
Grab
EPA 624.1
2.0
<T0
ug/L
1,3-dichloropropylene
77163
Grab
EPA 624.1
4.0
<4.0
ug/L
Ethylbenzene
34371
Grab
EPA 624.1
1.0
<1.0
ug/L
Methyl Bromide
34413
Grab
EPA 624.1
2.0
<2.0
ug/L
Methyl Chloride
34418
Grab
EPA 624.1
2.0
<2.0
ug/L
Methylene Chloride
34423
Grab
EPA 624.1
2.0
<2.0
ug/L
1,1,2,2-tetrachloroethane
81549
Grab
EPA 624.1
2.0
<2.0
ug/L
Form - DMR- PPA-1 Page 1

Annual Monitoring and Pollutant Scan
Permit No. NCO074268 Month June
Outfa11001 Year 2023
,t.,
Parameter; <..
v. �ga:,*f*.'>F'r. UN
.Pararne�er
Gode�
-1 "t :,, :� fi�
�x
Sam le;T e
P - YP
rF `l,q�`'`t"�i3`�� e, # xrz'3^
A 'al : cal�Method
Yt .
k'StiA �+"�'�"i&''axe �' }:�..`s
uantitatiari
Q:� �:xP
Le. -
3.''S�. �,.
IN Sam: le
Resu tMeasu
Units -of
erim�ent
Tetrachloroethylene
34475
Grab
EPA 624.1
2.0
<2.0
ug/L
Toluene
34010
Grab
EPA 624.1
1.0
<1.0
ug/L
1, 1, 1 -trichloroethane
34506
Grab
EPA 624.1
2.0
<2.0
ug/L
1,1,2-trichloroethane
34511
Grab
EPA 624.1
2.0
<2.0
ug/L
Trichloroethylene
39180
Grab
EPA 624.1
2.0
<2.0
ug/L
Vinyl Chloride
39175
Grab
EPA 624.1
2.0
<2.0
ug/L
cis-1,2 Dichloroethene **
Grab
EPA 624.1
2.0
<2.0
ug/L
Trichlorofluoromethane **
Grab
EPA 624.1
2.0
<2.0
ug/L
`�a - • ' ct e4 oma�xcls
P-chloro-m-creso
34452
Composite
EPA 625.1
5.0
<5.0
ug/L
2-chlorophenol
34586
Composite
EPA 625.1
5.0
<5.0
ug/L
2,4-dichlorophenol
34601
Composite
EPA 625.1
5.0
<5.0
ug/L
2,4-dimethylphenol
34606
Composite
EPA 625.1
10.0
<10.0
ug/L
4,6-dinitro-o-cresol
34657
Composite
EPA 625.1
10.0
<10.0
ug/L
2,4-dinitrophenol
34616
Composite
EPA 625.1
50.0
<50.0
ug/L
2-nitrophenol
34591
Composite
EPA 625.1
5.0
<5.0
ug/L
4-nitrophenol
34646
Composite
EPA 625.1
10.0
<10
ug/L
Pentachlorophenol
39032
Composite
EPA 625.1
10.0
<10
ug/L
Phenol
34694
Composite
EPA 625.1
5.0
<5.0
ug/L
2,4,6-trichlorophenol
34621
Composite
EPA 625.1
10.0
<10.0
ug/L
Acenaphthene
34205
Composite
EPA 625.1
5.0
<5.0
ug/L
Acenaphthylene
34200
Composite
EPA 625.1
5.0
<5.0
ug/L
Anthracene
CO220
Composite
EPA 625.1
5.0
<5.0
ug/L
Benzidine
39120
Composite
EPA 625.1
50.0
<50.0
ug/L
Benzo(a)anthracene
34526
Composite
EPA 625.1
5.0
<5.0
ug/L
Benzo(a)pyrene
34247
Composite
EPA 625.1
5.0
<5.0
ug/L
3,4 benzofluoranthene
34230
Composite
EPA 625.1
5.0
<5.0
ug/L
Benzo(ghi)perylene
34521
Composite
EPA 625.1
5.0
<5.0
ug/L
Benzo(k)fluoranthene
34242
Composite
EPA 625.1
5.0
<5.0
ug/L
Bis (2-chloroethoxy) methane
34278
Composite
EPA 625.1
10.0
<10.0
ug/L
Bis (2-chloroethyl) ether
34273
Composite
EPA 625.1
5.0
<5.0
ug/L
Bis (2-chloroisopropyl) ether
34283
Composite
EPA 625.1
5.0
<5.0
ug/L
Bis (2-ethylhexyl) phthalate
39100
Composite
EPA 625.1
5.0
<5.0
ug/L
4-bromophenyl phenyl ether
34636
Composite
EPA 625.1
5.0
<5.0
ug/L
Butyl benzyl phthalate
34292
Composite
EPA 625.1
5.0
<5.0
ug/L
2-chloronaphthalene
34581
Composite
EPA 625.1
5.0
<5.0
ug/L
4-chlorophenyl phenyl ether
34641
Composite
EPA 625.1
5.0
<5.0
ug/L
Chrysene
34320
Composite
EPA 625.1
5.0
<5.0
ug/L
Di-n-butyl phthalate
39110
Composite
EPA 625.1
5.0
<5.0
ug/L
Di-n-octyl phthalate
34596
Composite
EPA 625.1
5.0
<5.0
ug/L
Dibenzo(a,h)anthracene
34556
Composite
EPA 625.1
5.0
<5.0
ug/L
1,2-dichlorobenzene
34536
Grab
EPA 624.1
2.0
<2.0
ug/L
1,3-dichlorobenzene
34566
Grab
EPA 624.1
2.0
<2.0
ug/L
1,4-dichlorobenzene
34571
Grab
EPA 624.1
2.0
<2.0
ug/L
3,3-dichlorobenzidine
34631
Composite
EPA 625.1
10.0
<10.0
ug/L
Diethyl phthalate
34336
Composite
EPA 625.1
5.0
<5.0
ug/L
Dimethyl phthalate
34341
Composite
EPA 625.1
5.0
<5.0
ug/L
2,4-dinitrotoluene
34611
Composite
EPA 625.1
5.0
<5.0
ug/L
2,6-dinitrotoluene
C0626
Composite
EPA 625.1
5.0
<5.0
ug/L
1,2-diphenylhydrazine
34346
Composite
EPA 625.1
5.0
<5.0
ug/L
Fluoranthene
C0376
Composite
EPA 625.1
5.0
<5.0
ug/L
Fluorene
34381
Composite
EPA 625.1
5.0
<5.0
ug/L
Hexachlorobenzene
C0700
Composite
EPA 625.1
5.0
<5.0
ug/L
Hexachlorobutadiene
39702
Composite
EPA 625.1
5.0
<5.0
ug/L
Hexachlorocyclo-pentadiene
34386
Composite
EPA 625.1
10.0
<10.0
ug/L
Hexachloroethane
34396
Composite
EPA 625.1
5.0
<5.0
ug/L
Indeno(1,2,3-cd)pyrene
34403
Composite
EPA 625.1
5.0
<5.0
ug/L
Isophorone
34408
Composite
EPA 625.1
10.0
<10.0
ug/L
Form - DMR- PPA-1 Page 2

Annual Monitoring and Pollutant Scan
Permit No. NC0074268 Month June
Outfall 001 Year 2023
Parameter .,,.-
Parameter
��'
Code..
F
=Sample. Type
, >��': �n
•Amyl real Method
fQuaritation =
-
levelResu
Sasn le ''
t
Units ;uf
<t _;
A Neasurem , t
Naphthalene
34696
Composite
EPA 625.1
5.0
<5.0
ug/L
Nitrobenzene
34447
Composite
EPA 625.1
5.0
<5.0
ug/L
N-nitrosodi-n-propylamme
34428
Composite
EPA 625.1
5.0
<5.0
ug/L
N-nitrosodimethylamme
34438
Composite
EPA 625.1
5.0
<5.0
ug/L
N-nitrosodiphenylamine
34433
Composite
EPA 625.1
10.0
<10
ug/L
Phenanthrene
34461
Composite
EPA 625.1
5.0
<5.0
ug/L
Pyrene
34469
Composite
EPA 625.1
5.0
<5.0
ug/L
1,2,4,-trichlorobenzene
34551
Composite
EPA 625.1
5.0
<5.0
ug/L
* Analysis conducted outside of EPA hold time.
** Additional parameters run per method 624.
Sampling should be conducted as specified in 40 CFR Part 136.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who managed the system, or those persons directly responsible for gathering the information, the information submitted is, to the best
of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Thomas. LopEz, ORC- Crowders Creek WWTP
Author' ed R resentative name
Date
Form - DMR- PPA-1 Page 3

ace"
April 17, 2024
Susan Copeland
Two Rivers Utilities
5642 South York Highway
Gastonia, NC 28054
RE: Project: CR EFFLUENT PPA-Revised Report
Pace Project No.: 92720685
Dear Susan Copeland:
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on March 22, 2024. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
Revision 1 - This report was reissued April 17, 2024. Data for Benzidine has been reported
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Ariel S Fitzgerald
[e-mail]
704-977-0945
Project Manager
Enclosures
cc: Jennifer Kirby, Two Rivers Utilities
David Shellenbarger, Two Rivers Utilities
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 14

cem
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: CR EFFLUENT PPA-Revised Report
Pace Project No.: 92720685
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 14

acem
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: CR EFFLUENT PPA-Revised Report
Pace Project No.: 92720685
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92720685001 CREFFLUENT EPA625.1 PKS 59 PASI-C
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 14

(-�Face"'
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: CR EFFLUENT PPA-Revised Report
Pace Project No.: 92720685
Sample: CR EFFLUENT
Lab ID: 92720685001 Collected:
03/19/24 07:42
Received: 03/22/24 11:44 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared Analyzed
CAS No.
Qual
625 RVE
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
Acenaphthene
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
83-32-9
Acenaphthylene
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
208-96-8
Anthracene
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
120-12-7
Benzidine
ND
ug/L
50.0
1
03/26/24 01:45 03/28/24 03:03
92-87-5
Benzo(a)anthrace ne
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
56-55-3
Benzo(a)pyrene
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
50-32-8
Benzo(b)fluoranthene
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
191-24-2
Benzo(k)fluoranthene
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
207-08-9
4-Bromophenylphenyl ether
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
101-55-3
Butylbenzyl phtha late
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
85-68-7
4-Chloro-3-methylphenol
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1
03/26/24 01:45 03/28/24 03:03
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
111-44-4
2-Chloronaphthalene
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
91-58-7
2-Chlorophenol
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
7005-72-3
Chrysene
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
10.0
1
03/26/24 01:45 03/28/24 03:03
91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
120-83-2
Diethyl phtha late
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
84-66-2
L1,M0
2,4-Dimethylphenol
ND
ug/L
10.0
1
03/26/24 01:45 03/28/24 03:03
105-67-9
L1
Dimethylphthalate
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
131-11-3
L1,M0
Di-n-butylphthalate
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
84-74-2
M1
4,6-Dinitro-2-methylphenol
ND
ug/L
10.0
1
03/26/24 01:45 03/28/24 03:03
534-52-1
R1
2,4-Dinitrophenol
ND
ug/L
50.0
1
03/26/24 01:45 03/28/24 03:03
51-28-5
2,4-Dinitrotoluene
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
606-20-2
Di-n-octylphthalate
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
117-84-0
bis(2-Ethylhexyl)phthalate
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
117-81-7
Fluoranthene
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
206-44-0
Fluorene
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
87-68-3
Hexachlorobenzene
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
118-74-1
Hexachlorocyclopentad iene
ND
ug/L
10.0
1
03/26/24 01:45 03/28/24 03:03
77-47-4
Hexachloroethane
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
193-39-5
Isophorone
ND
ug/L
10.0
1
03/26/24 01:45 03/28/24 03:03
78-59-1
Naphthalene
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
91-20-3
Nitrobenzene
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
98-95-3
2-Nitrophenol
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
88-75-5
4-Nitrophenol
ND
ug/L
10.0
1
03/26/24 01:45 03/28/24 03:03
100-02-7
R1
N-Nitrosodimethylamine
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
1
03/26/24 01:45 03/28/24 03:03
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
03/26/24 01:45 03/28/24 03:03
86-30-6
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced, except in
full,
Date: 04/17/2024 03:32 PM
without the written consent of Pace Analytical Services, LLC.
Page 4 of 14

ce",
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: CR EFFLUENT PPA-Revised Report
Pace Project No.: 92720685
Sample: CR EFFLUENT Lab ID: 92720685001 Collected: 03/19/24 07:42 Received: 03/22/24 11:44 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 RVE
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical
Services - Charlotte
2,2'-Oxybis(1-chloropropane)
ND
ug/L
5.0
1
03/26/24 01:45
03/28/24 03:03
108-60-1
Pentachlorophenol
ND
ug/L
10.0
1
03/26/24 01:45
03/28/24 03:03
87-86-5
Phenanthrene
ND
ug/L
5.0
1
03/26/24 01:45
03/28/24 03:03
85-01-8 M1
Phenol
ND
ug/L
5.0
1
03/26/24 01:45
03/28/24 03:03
108-95-2
Pyrene
ND
ug/L
5.0
1
03/26/24 01:45
03/28/24 03:03
129-00-0 M1
1,2,4-Trichlorobenzene
ND
ug/L
5.0
1
03/26/24 01:45
03/28/24 03:03
120-82-1
2,4,6-Trichlorophenol
ND
ug/L
10.0
1
03/26/24 01:45
03/28/24 03:03
88-06-2
Surrogates
Nitrobenzene-d5 (S)
81
%
10-120
1
03/26/24 01:45
03/28/24 03:03
4165-60-0
2-Fluorobiphenyl (S)
79
%
15-120
1
03/26/24 01:45
03/28/24 03:03
321-60-8
Terphenyl-d14 (S)
92
%
11-131
1
03/26/24 01:45
03/28/24 03:03
1718-51-0
Phenol-d6 (S)
43
%
10-120
1
03/26/24 01:45
03/28/24 03:03
13127-88-3
2-Fluorophenol (S)
56
%
10-120
1
03/26/24 01:45
03/28/24 03:03
367-12-4
2,4,6-Tribromophenol (S)
82
%
10-137
1
03/26/24 01:45
03/28/24 03:03
118-79-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/17/2024 03:32 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 14

(-�Face-
Project: CR EFFLUENT PPA-Revised Report
Pace Project No.: 92720685
QC Batch: 841687
QC Batch Method: EPA 625.1
Associated Lab Samples: 92720685001
QUALITY CONTROL DATA
Analysis Method: EPA 625.1
Analysis Description: 625 MSS
Laboratory: Pace Analytical Services - Charlotte
METHOD BLANK: 4347188
Associated Lab Samples: 92720685001
Parameter
Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
1,2,4-Trichlorobenzene
ug/L
ND
5.0
03/27/24 19:22
2,2'-Oxybis(1-chloropropane)
ug/L
ND
5.0
03/27/24 19:22
2,4,6-Trichlorophenol
ug/L
ND
10.0
03/27/24 19:22
2,4-Dichlorophenol
ug/L
ND
5.0
03/27/24 19:22
2,4-Dimethyl phenol
ug/L
ND
10.0
03/27/24 19:22
2,4-Dinitrophenol
ug/L
ND
50.0
03/27/24 19:22
2,4-Dinitrotoluene
ug/L
ND
5.0
03/27/24 19:22
2,6-Dinitrotoluene
ug/L
ND
5.0
03/27/24 19:22
2-Chloronaphthalene
ug/L
ND
5.0
03/27/24 19:22
2-Chlorophenol
ug/L
ND
5.0
03/27/24 19:22
2-Nitrophenol
ug/L
ND
5.0
03/27/24 19:22
3,3'-Dichlorobenzidine
ug/L
ND
10.0
03/27/24 19:22
4,6-Dinitro-2-methylphenol
ug/L
ND
10.0
03/27/24 19:22
4-Bromophenylphenyl ether
ug/L
ND
5.0
03/27/24 19:22
4-Chloro-3-methylphenol
ug/L
ND
5.0
03/27/24 19:22
4-Chlorophenylphenyl ether
ug/L
ND
5.0
03/27/24 19:22
4-Nitrophenol
ug/L
ND
10.0
03/27/24 19:22
Acenaphthene
ug/L
ND
5.0
03/27/24 19:22
Acenaphthylene
ug/L
ND
5.0
03/27/24 19:22
Anthracene
ug/L
ND
5.0
03/27/24 19:22
Benzidine
ug/L
ND
50.0
03/27/24 19:22
Benzo(a)anthracene
ug/L
ND
5.0
03/27/24 19:22
Benzo(a)pyrene
ug/L
ND
5.0
03/27/24 19:22
Benzo(b)fluoranthene
ug/L
ND
5.0
03/27/24 19:22
Benzo(g,h,i)perylene
ug/L
ND
5.0
03/27/24 19:22
Benzo(k)fluoranthene
ug/L
ND
5.0
03/27/24 19:22
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
03/27/24 19:22
bis(2-Chloroethyl) ether
ug/L
ND
5.0
03/27/24 19:22
bis(2-Ethylhexyl)phthalate
ug/L
ND
5.0
03/27/24 19:22
Butyl benzylphthalate
ug/L
ND
5.0
03/27/24 19:22
Chrysene
ug/L
ND
5.0
03/27/24 19:22
Di-n-butylphthalate
ug/L
ND
5.0
03/27/24 19:22
Di-n-octylphthalate
ug/L
ND
5.0
03/27/24 19:22
Dibenz(a,h)anthracene
ug/L
ND
5.0
03/27/24 19:22
Diethylphthalate
ug/L
ND
5.0
03/27/24 19:22
Dimethylphthalate
ug/L
ND
5.0
03/27/24 19:22
Fluoranthene
ug/L
ND
5.0
03/27/24 19:22
Fluorene
ug/L
ND
5.0
03/27/24 19:22
Hexachloro-1,3-butadiene
ug/L
ND
5.0
03/27/24 19:22
Hexachlorobenzene
ug/L
ND
5.0
03/27/24 19:22
Qualifiers
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/17/2024 03:32 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 14

Pace Analytical Services, LLC
ace 2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: CR EFFLUENT PPA-Revised Report
Pace Project No.: 92720685
METHOD BLANK: 4347188
Associated Lab Samples: 92720685001
Parameter
Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed Qualifiers
Hexachlorocyclopentadiene
ug/L
ND
10.0
03/27/24 19:22
Hexachloroethane
ug/L
ND
5.0
03/27/24 19:22
Indeno(1,2,3-cd)pyrene
ug/L
ND
5.0
03/27/24 19:22
Isophorone
ug/L
ND
10.0
03/27/24 19:22
N-Nitroso-di-n-propylamine
ug/L
ND
5.0
03/27/24 19:22
N-Nitrosodimethylamine
ug/L
ND
5.0
03/27/24 19:22
N-Nitrosodiphenylamine
ug/L
ND
10.0
03/27/24 19:22
Naphthalene
ug/L
ND
5.0
03/27/24 19:22
Nitrobenzene
ug/L
ND
5.0
03/27/24 19:22
Pentachlorophenol
ug/L
ND
10.0
03/27/24 19:22
Phenanthrene
ug/L
ND
5.0
03/27/24 19:22
Phenol
ug/L
ND
5.0
03/27/24 19:22
Pyrene
ug/L
ND
5.0
03/27/24 19:22
2,4,6-Tribromophenol (S)
%
73
10-137
03/27/24 19:22
2-Fluorobiphenyl (S)
%
74
15-120
03/27/24 19:22
2-Fluorophenol (S)
%
65
10-120
03/27/24 19:22
Nitrobenzene-d5 (S)
%
79
10-120
03/27/24 19:22
Phenol-d6 (S)
%
51
10-120
03/27/24 19:22
Terphenyl-d14 (S)
%
79
11-131
03/27/24 19:22
LABORATORY CONTROL SAMPLE:
Parameter
4347189
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2,4-Tdchlorobenzene
ug/L
50
43.3
87
44-142
2,2'-Oxybis(1-chloropropane)
ug/L
50
56.0
112
36-166
2,4,6-Trichlorophenol
ug/L
50
56.6
113
37-144
2,4-Dichlorophenol
ug/L
50
54.9
110
1-191
2,4-Dimethylphenol
ug/L
50
63.5
127
32-119 L1
2,4-Dinitrophenol
ug/L
250
326
130
1-181
2,4-Dinitrotoluene
ug/L
50
60.6
121
39-139
2,6-Dinitrotoluene
ug/L
50
61.5
123
50-158
2-Chloronaphthalene
ug/L
50
55.1
110
60-118
2-Chlorophenol
ug/L
50
55.2
110
23-134
2-Nitrophenol
ug/L
50
55.9
112
29-182
3,3'-Dichlorobenzidine
ug/L
100
111
111
1-262
4,6-Dinitro-2-methylphenol
ug/L
100
124
124
1-181
4-Bromophenylphenyl ether
ug/L
50
54.7
109
53-127
4-Chloro-3-methylphenol
ug/L
100
111
111
22-147
4-Chlorophenylphenyl ether
ug/L
50
59.6
119
25-158
4-Nitrophenol
ug/L
250
198
79
1-132
Acenaphthene
ug/L
50
56.8
114
47-145
Acenaphthylene
ug/L
50
59.2
118
33-145
Anthracene
ug/L
50
54.3
109
1-166
Benzidine
ug/L
100
13.9J
14
10-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/17/2024 03:32 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 14

(-�Face"
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: CR EFFLUENT PPA-Revised Report
Pace Project No.: 92720685
LABORATORY CONTROL SAMPLE:
4347189
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Benzo(a)anthracene
ug/L
50
54.0
108
33-143
Benzo(a)pyrene
ug/L
50
57.6
115
17-163
Benzo(b)fluoranthene
ug/L
50
58.3
117
24-159
Benzo(g,h,i)perylene
ug/L
50
59.2
118
1-219
Benzo(k)fluoranthene
ug/L
50
56.7
113
11-162
bis(2-Chloroethoxy)methane
ug/L
50
56.4
113
33-184
bis(2-Chloroethyl) ether
ug/L
50
56.5
113
12-158
bis(2-Ethylhexyl)phthalate
ug/L
50
64.0
128
8-158
Butylbenzylphthalate
ug/L
50
55.0
110
1-152
Chrysene
ug/L
50
53.5
107
17-168
Di-n-butylphthalate
ug/L
50
59.0
118
1-118
Di-n-octylphthalate
ug/L
50
57.7
115
4-146
Dibenz(a,h)anthracene
ug/L
50
59.7
119
1-227
Diethylphtha late
ug/L
50
59.5
119
1-114 L1
Dimethylphthalate
ug/L
50
59.3
119
1-112 L1
Fluoranthene
ug/L
50
57.7
115
26-137
Fluorene
ug/L
50
59.1
118
59-121
Hexachloro-1,3-butadiene
ug/L
50
40.0
80
24-116
Hexachlorobenzene
ug/L
50
54.7
109
1-152
Hexachlorocyclopentadiene
ug/L
50
48.8
98
25-150
Hexachloroethane
ug/L
50
37.4
75
40-113
Indeno(1,2,3-cd)pyrene
ug/L
50
58.7
117
1-171
Isophorone
ug/L
50
57.0
114
21-196
N-Nitroso-di-n-propylamine
ug/L
50
61.5
123
1-230
N-Nitrosodimethylamine
ug/L
50
49.1
98
25-150
WIN itrosodiphenylamine
ug/L
50
56.4
113
25-150
Naphthalene
ug/L
50
47.6
95
21-133
Nitrobenzene
ug/L
50
54.0
108
35-180
Pentachlorophenol
ug/L
100
120
120
14-176
Phenanthrene
ug/L
50
55.1
110
54-120
Phenol
ug/L
50
36.5
73
5-112
Pyrene
ug/L
50
56.0
112
52-115
2,4,6-Tribromophenol (S)
%
101
10-137
2-Fluorobiphenyl (S)
%
98
15-120
2-Fluorophenol (S)
%
77
10-120
Nitrobenzene-d5 (S)
%
96
10-120
Phenol-d6 (S)
%
60
10-120
Terphenyl-d14 (S)
%
92
11-131
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
4347190
4347191
MS
MSD
92720685001 Spike
Spike MS
MSD
MS MSD % Rec
Parameter Units
Result Conc.
Conc. Result
Result
% Rec % Rec Limits RPD Qua[
1,2,4-Trichlorobenzene ug/L
ND 50
50 41.3
38.8
83 78 44-142 6
2,2'-Oxybis(1-chloropropane) ug/L
ND 50
50 49.5
50.5
99 101 36-166 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/17/2024 03:32 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 14

Pace Analytical Services, LLC
2225 Riverside Dr.
(-�ace© Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: CR EFFLUENT PPA-Revised Report
Pace Project No.: 92720685
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4347190
MS
92720685001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
4347191
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
2,4,6-Trichlorophenol
ug/L
ND
50
50
53.7
46.9
107
94
37-144
14
2,4-Dichlorophenol
ug/L
ND
50
50
51.0
47.1
102
94
1-191
8
2,4-Dimethylphenol
ug/L
ND
50
50
59.4
57.5
119
115
32-119
3
2,4-Dinitrophenol
ug/L
ND
250
250
44.8J
ND
18
9
1-181
2,4-Dinitrotoluene
ug/L
ND
50
50
59.0
57.6
118
115
39-139
2
2,6-Dinitrotoluene
ug/L
ND
50
50
59.8
58.1
120
116
50-158
3
2-Chloronaphthalene
ug/L
ND
50
50
51.6
48.7
103
97
60-118
6
2-Chlorophenol
ug/L
ND
50
50
48.5
48.1
97
96
23-134
1
2-Nitrophenol
ug/L
ND
50
50
52.4
50.5
105
101
29-182
4
3,3'-Dichlorobenzidine
ug/L
ND
100
100
124
130
124
130
1-262
5
4,6-Dinitro-2-methylphenol
ug/L
ND
100
100
74.3
51.3
74
51
1-181
37 R1
4-Bromophenylphenyl ether
ug/L
ND
50
50
60.6
54.3
121
109
53-127
11
4-Chloro-3-methylphenol
ug/L
ND
100
100
108
101
108
101
22-147
7
4-Chlorophenylphenyl ether
ug/L
ND
50
50
57.7
56.0
115
112
25-158
3
4-Nitrophenol
ug/L
ND
250
250
115
69.4
46
28
1-132
49 R1
Acenaphthene
ug/L
ND
50
50
53.8
51.7
108
103
47-145
4
Acenaphthylene
ug/L
ND
50
50
56.3
54.5
113
109
33-145
3
Anthracene
ug/L
ND
50
50
59.9
57.4
120
115
1-166
4
Benzidine
ug/L
ND
100
100
46AJ
49.3J
46
49
10-130
Benzo(a)anthrace ne
ug/L
ND
50
50
63.1
62.6
126
125
33-143
1
Benzo(a)pyrene
ug/L
ND
50
50
63.5
62.8
127
126
17-163
1
Benzo(b)fluoranthene
ug/L
ND
50
50
64.0
62.3
128
125
24-159
3
Benzo(g,h,i)perylene
ug/L
ND
50
50
63.4
64.9
127
130
1-219
2
Benzo(k)fluoranthene
ug/L
ND
50
50
63.8
64.4
128
129
11-162
1
bis(2-Chloroethoxy)methane
ug/L
ND
50
50
52.1
51.0
104
102
33-184
2
bis(2-Chloroethyl) ether
ug/L
ND
50
50
49.5
50.6
99
101
12-158
2
bis(2-Ethylhexyl)phthalate
ug/L
ND
50
50
73.1
64.3
146
129
8-158
13
Butylbenzylphthalate
ug/L
ND
50
50
66.0
65.3
132
131
1-152
1
Chrysene
ug/L
ND
50
50
67.8
68.8
136
138
17-168
2
Di-n-butylphthalate
ug/L
ND
50
50
65.7
63.6
131
127
1-118
3 M1
Di-n-octylphthalate
ug/L
ND
50
50
66.5
67.4
133
135
4-146
1
Dibenz(a,h)anth racene
ug/L
ND
50
50
63.0
65.1
126
130
1-227
3
Diethylphthalate
ug/L
ND
50
50
60.1
57.7
120
115
1-114
4 MO
Dimethylphthalate
ug/L
ND
50
50
57.8
55.0
116
110
1-112
5 MO
Fluoranthene
ug/L
ND
50
50
64.8
61.7
130
123
26-137
5
Fluorene
ug/L
ND
50
50
57.2
55.7
114
111
59-121
3
Hexachloro-1,3-butadiene
ug/L
ND
50
50
38.6
35.8
77
72
24-116
8
Hexachlorobenzene
ug/L
ND
50
50
61.5
56.6
123
113
1-152
8
Hexachlorocyclopentadiene
ug/L
ND
50
50
45.2
41.2
90
82
25-150
9
Hexachloroethane
ug/L
ND
50
50
35.0
33.6
70
67
40-113
4
Indeno(1,2,3-cd)pyrene
ug/L
ND
50
50
63.9
65.2
128
130
1-171
2
Isophorone
ug/L
ND
50
50
52.5
50.5
105
101
21-196
4
N-Nitroso-di-n-propylamine
ug/L
ND
50
50
52.7
55.2
105
110
1-230
5
N-Nitrosodimethylamine
ug/L
ND
50
50
42.0
41.5
84
83
25-150
1
N-Nitrosodiphenylamine
ug/L
ND
50
50
63.8
59.8
128
120
25-150
6
Naphthalene
ug/L
ND
50
50
44.8
43.4
90
87
21-133
3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/17/2024 03:32 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 14

(A`qace0
QUALITY CONTROL DATA
Project: CR EFFLUENT PPA-Revised Report
Pace Project No.: 92720685
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
4347190
MS
92720685001 Spike
Parameter
Units
Result Conc.
Nitrobenzene
ug/L
ND 50
Pentachlorophenol
ug/L
ND 100
Phenanthrene
ug/L
ND 50
Phenol
ug/L
ND 50
Pyrene
ug/L
ND 50
2,4,6-Tribromophenol (S)
%
2-Fluorobiphenyl (S)
%
2-Fluorophenol (S)
%
Nitrobenzene-d5 (S)
%
Phenol-d6 (S)
%
Terphenyl-d14 (S)
%
4347191
MSD
Spike
MS
MSD
Conc.
Result
Result
50
49.4
47.7
100
103
82.6
50
60.8
58.2
50
35.1
31.2
50
65.4
66.9
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
99
95
35-180
4
103
83
14-176
22
122
116
54-120
4 M1
70
62
5-112
12
131
134
52-115
2 M1
99
81
10-137
83
70
15-120
61
49
10-120
82
70
10-120
51
40
10-120
97
89
11-131
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/17/2024 03:32 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 14

Pace Analytical Services, LLC
2225 Riverside Dr.
(-`*ace Asheville, NC 28804
[phone]
QUALIFIERS
Project: CR EFFLUENT PPA-Revised Report
Pace Project No.: 92720685
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/17/2024 03:32 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 14

�ceo
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: CR EFFLUENT PPA-Revised Report
Pace Project No.: 92720685
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92720685001 CR EFFLUENT EPA 625.1 841687 EPA 625.1 842070
Date: 04/17/2024 03:32 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 12 of 14

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DC# —Title: ENV-FRM-HUN1-0083 v02—Sarnple Condition Upon Receipt
Effective Date: 11/14/2022
*Check mark top half of box if pH and/or dechlorination Is verified and Projec-i
within the acceptance range for preservation samples,
Exceptions: VOA, CoUforrn,TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottles
***Check all unpreserved Nitrates for chlorine
wo#:9272068
pli: ASF Due Date: 03/28/24
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Qualtrax ID: 69614 Page 2 of 2 Page 14 of 14

(-�Face�
April 11, 2024
Susan Copeland
Two Rivers Utilities
5642 South York Highway
Gastonia, NC 28054
RE: Project: CR EFFLUENT PPA-Revised Report
Pace Project No.: 92720687
Dear Susan Copeland:
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on March 22, 2024. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
Revision 1 - This report was reissued April 11, 2024. Data for Acrolein and Acrylonitrile has been reported
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Ariel S Fitzgerald
[e-mail]
704-977-0945
Project Manager
Enclosures
cc: Jennifer Kirby, Two Rivers Utilities
David Shellenbarger, Two Rivers Utilities
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 15

(-�Face�
Project: CR EFFLUENT PPA-Revised Report
Pace Project No.: 92720687
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cart. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water#: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 15

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
CR EFFLUENT PPA-Revised Report
92720687
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92720687001
CR EFFLUENT
EPA 624.1
SAS
34
PASI-C
EPA 624.1
SAS
5
PASI-C
EPA 624 By SIM
JJK
3
PASI-C
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 15

(-�Face-
Project: CR EFFLUENT PPA-Revised Report
Pace Project No.: 92720687
Sample: CR EFFLUENT
Parameters
624 Volatile Organics
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1, 3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Methylene Chloride
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluo romethane
Vinyl chloride
Surrogates
4-Bromofluorobenzene (S)
Toluene-d8 (S)
1,2-Dichloroethane-d4 (S)
624 Volatile Organics Acrolein
Acrolein
Acrylonitrile
Surrogates
4-Bromofluorobenzene (S)
Toluene-d8 (S)
1,2-Dichloroethane-d4 (S)
Date: 04/11/2024 03:31 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Lab ID: 92720687001 Collected: 03/19/24 07:44 Received: 03/22/24 11:44 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 624.1
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
6.7
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
98 %
101 %
102 %
Analytical Method: EPA 624.1
Pace Analytical Services - Charlotte
ND ug/L
ND ug/L
102 %
103 %
102 %
1.0
1
03/27/24 13:40
71-43-2
2.0
1
03/27/24 13:40
75-27-4
2.0
1
03/27/24 13:40
75-25-2
2.0
1
03/27/24 13:40
74-83-9
2.0
1
03/27/24 13:40
56-23-5
2.0
1
03/27/24 13:40
108-90-7
2.0
1
03/27/24 13:40
75-00-3
2.0
1
03/27/24 13:40
67-66-3
2.0
1
03/27/24 13:40
74-87-3
2.0
1
03/27/24 13:40
124-48-1
2.0
1
03/27/24 13:40
95-50-1
2.0
1
03/27/24 13:40
541-73-1
2.0
1
03/27/24 13:40
106-46-7
2.0
1
03/27/24 13:40
75-34-3
2.0
1
03/27/24 13:40
107-06-2
2.0
1
03/27/24 13:40
75-35-4
2.0
1
03/27/24 13:40
156-59-2
2.0
1
03/27/24 13:40
156-60-5
2.0
1
03/27/24 13:40
78-87-5
2.0
1
03/27/24 13:40
10061-01-5
2.0
1
03/27/24 13:40
10061-02-6
1.0
1
03/27/24 13:40
100-41-4
2.0
1
03/27/24 13:40
75-09-2
2.0
1
03/27/24 13:40
79-34-5
2.0
1
03/27/24 13:40
127-18-4
1.0
1
03/27/24 13:40
108-88-3
2.0
1
03/27/24 13:40
71-55-6
2.0
1
03/27/24 13:40
79-00-5
2.0
1
03127/2413:40
79-01-6
2.0
1
03/27/24 13:40
75-69-4
2.0
1
03/27/24 13:40
75-01-4
70-130 1
70-130 1
70-130 1
5.0 1
5.0 1
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
03/27/24 13:40 460-00-4
03/27/24 13:40 2037-26-5
03/27/24 13:40 17060-07-0
04/05/2417:33 107-02-8 H1
04/05/2417:33 107-13-1 H1
04/05/2417:33 460-00-4
04/05/2417:33 2037-26-5
04/05/24 17: 33 17060-07-0
Page 4 of 15

ace"
ANALYTICAL RESULTS
Project: CR EFFLUENT PPA-Revised Report
Pace Project No.: 92720687
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: CR EFFLUENT
Parameters
Lab ID: 92720687001 Collected: 03/19/24 07:44
Results Units Report Limit DF
Received: 03/22/24 11:44 Matrix: Water
Prepared Analyzed CAS No. Qua]
624 Volatiles by SIM
Analytical Method: EPA 624 By SIM
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L
2.0
1
03/26/24 17:07
123-91-1
Surrogates
Toluene-d8 (S)
124 %
70-130
1
03/26/24 17:07
2037-26-5
1,2-Dichloroethane-d4 (S)
104 %
70-130
1
03/26/24 17:07
17060-07-0
Date: 04/11/2024 03:31 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 15

�ceo
QUALITY CONTROL DATA
Project: CR EFFLUENT PPA-Revised Report
Pace Project No.: 92720687
QC Batch: 842114 Analysis Method: EPA 624.1
QC Batch Method: EPA 624.1 Analysis Description: 624 MSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92720687001
METHOD BLANK: 4349202
Associated Lab Samples: 92720687001
Parameter
Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
1,1,1-Trichloroethane
ug/L
ND
2.0
03/27/24 11:35
1,1,2,2-Tetrachloroethane
ug/L
ND
2.0
03/27/24 11:35
1,1,2-Trichloroethane
ug/L
ND
2.0
03/27/24 11:35
1,1-Dichloroethane
ug/L
ND
2.0
03/27/24 11:35
1,1-Dichloroethene
ug/L
ND
2.0
03/27/24 11:35
1,2-Dichlorobenzene
ug/L
ND
2.0
03/27/24 11:35
1,2-Dichloroethane
ug/L
ND
2.0
03/27/24 11:35
1,2-Dichloropropane
ug/L
ND
2.0
03/27/24 11:35
1,3-Dichlorobenzene
ug/L
ND
2.0
03/27/24 11:35
1,4-Dichlorobenzene
ug/L
ND
2.0
03/27/24 11:35
Benzene
ug/L
ND
1.0
03/27/24 11:35
Bromodichloromethane
ug/L
ND
2.0
03/27/24 11:35
Bromoform
ug/L
ND
2.0
03/27/24 11:35
Bromomethane
ug/L
ND
2.0
03/27/24 11:35
Carbon tetrachloride
ug/L
ND
2.0
03/27/24 11:35
Chlorobenzene
ug/L
ND
2.0
03/27/24 11:35
Chloroethane
ug/L
ND
2.0
03/27/24 11:35
Chloroform
ug/L
ND
2.0
03/27/24 11:35
Chloromethane
ug/L
ND
2.0
03/27/24 11:35
cis-1,2-Dichloroethene
ug/L
ND
2.0
03/27/24 11:35
cis-1,3-Dichloropropene
ug/L
ND
2.0
03/27/24 11:35
Dibromochloromethane
ug/L
ND
2.0
03/27/24 11:35
Ethylbenzene
ug/L
ND
1.0
03/27/24 11:35
Methylene Chloride
ug/L
ND
2.0
03/27/24 11:35
Tetrachloroethene
ug/L
ND
2.0
03/27/24 11:35
Toluene
ug/L
ND
1.0
03/27/24 11:35
trans- 1,2-Dichloroethene
ug/L
ND
2.0
03/27/24 11:35
trans- 1,3-Dichloropropene
ug/L
ND
2.0
03/27/24 11:35
Trichloroethene
ug/L
ND
2.0
03/27/24 11:35
Trichlorofluoromethane
ug/L
ND
2.0
03/27/24 11:35
Vinyl chloride
ug/L
ND
2.0
03/27/24 11:35
1,2-Dichloroethane-d4 (S)
%
102
70-130
03/27/24 11:35
4-Bromofluorobenzene (S)
%
96
70-130
03/27/24 11:35
Toluene-d8 (S)
%
101
70-130
03/27/24 11:35
LABORATORY CONTROL SAMPLE: 4349203
Qualifiers
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,1,1-Trichloroethane ug/L 20 22.0 110 70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/11 /2024 03:31 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 15

�ceo
QUALITY CONTROL DATA
Project: CR EFFLUENT PPA-Revised Report
Pace Project No.: 92720687
LABORATORY CONTROL SAMPLE:
Parameter
4349203
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,2,2-Tetrachloroethane
ug/L
20
21.2
106
70-130
1,1,2-Trchloroethane
ug/L
20
21.3
107
70-130
1,1-Dichloroethane
ug/L
20
20.3
101
70-130
1,1-Dichloroethene
ug/L
20
21.6
108
69-131
1,2-Dichlorobenzene
ug/L
20
22.7
113
70-130
1,2-Dichloroethane
ug/L
20
22.3
111
70-130
1,2-Dichloropropane
ug/L
20
21.4
107
70-130
1,3-Dichlorobenzene
ug/L
20
22.4
112
70-130
1,4-Dichlorobenzene
ug/L
20
21.8
109
70-130
Benzene
ug/L
20
22.0
110
65-135
Bromodichloromethane
ug/L
20
21.3
106
70-130
Bromoform
ug/L
20
21.8
109
70-130
Bromomethane
ug/L
20
18.0
90
41-148
Carbon tetrachloride
ug/L
20
22.9
114
70-130
Chlorobenzene
ug/L
20
21.1
105
70-130
Chloroethane
ug/L
20
22.6
113
41-157
Chloroform
ug/L
20
22.3
111
70-130
Chloromethane
ug/L
20
22.1
110
59-141
cis- 1,2-Dichloroethene
ug/L
20
20.0
100
70-130
cis- 1,3-Dichloropropene
ug/L
20
23.1
115
70-130
Dibromochloromethane
ug/L
20
22.1
110
70-130
Ethylbenzene
ug/L
20
21.5
108
70-130
Methylene Chloride
ug/L
20
19.9
100
62-130
Tetrachloroethene
ug/L
20
21.6
108
70-130
Toluene
ug/L
20
21.9
109
70-130
trans- 1,2-Dichloroethene
ug/L
20
20.6
103
70-130
trans- 1,3-Dichloropropene
ug/L
20
22.5
113
70-130
Trichloroethene
ug/L
20
22.8
114
70-130
Trichlorofluoromethane
ug/L
20
24.4
122
57-130
Vinyl chloride
ug/L
20
22.2
111
66-140
1,2-Dichloroethane-d4 (S)
%
90
70-130
4-Bromofluorobenzene (S)
%
97
70-130
Toluene-d8 (S)
%
102
70-130
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
4349204
4349205
MS
MSD
92721300001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qua]
1,1,1-Trichloroethane
ug/L
ND
20
20
27.7
29.6
138
148
70-150
7
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
25.6
26.9
128
135
66-144
5
1,1,2-Trichloroethane
ug/L
ND
20
20
26.1
28.9
130
144
70-142
10 M1
1,1-Dichloroethane
ug/L
ND
20
20
25.3
27.9
126
139
67-150
10
1,1-Dichloroethene
ug/L
ND
20
20
26.8
28.7
134
143
64-162
7
1,2-Dichlorobenzene
ug/L
ND
20
20
24.3
27.3
122
137
70-142
12
1,2-Dichloroethane
ug/L
ND
20
20
26.9
28.9
134
144
58-145
7
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/11/2024 03:31 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 15

(-�Face°
QUALITY CONTROL DATA
Project: CR EFFLUENT PPA-Revised Report
Pace Project No.: 92720687
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4349204
Parameter
1,2-Dichloropropane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis- 1,3-Dichloropropene
Dibromochloromethane
Ethylbenzene
Methylene Chloride
Tetrachloroethene
Toluene
trans- 1,2-Dichloroethene
trans- 1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
MS
92721300001 Spike
Units
Result Conc
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
4.7
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
4349205
MSD
Spike
MS
MSD
Conc.
Result
Result
20 20
27.6
28.5
20 20
24.2
27.5
20 20
23.1
26.3
20 20
28.0
30.0
20 20
28.4
30.4
20 20
27.3
28.8
20 20
34.2
37.5
20 20
26.9
30.2
20 20
26.8
27.6
20 20
29.4
34.7
20 20
29.7
33.8
20 20
28.2
30.1
20 20
25.7
28.2
20 20
27.4
30.2
20 20
26.9
29.7
20 20
27.4
28.4
20 20
23.5
25.6
20 20
26.9
28.2
20 20
27.0
29.3
20 20
25.4
27.9
20 20
27.6
29.7
20 20
28.3
30.1
20 20
29.7
30.7
20 20
28.3
29.9
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
MS
MSD
% Rec
% Rec
% Rec
Limits
RPD Qual
138
142
70-144
3
121
137
70-142
13
116
131
70-140
13
140
150
70-142
7 M1
142
152
70-139
7 M1
136
144
64-140
5
171
187
28-192
9
135
151
70-140
12 M1
134
138
70-141
3
147
173
58-191
16
125
145
70-138
13 M1
141
151
43-162
7
129
141
70-143
9
137
151
68-151
9 M1
135
148
70-144
10 M1
137
142
70-143
4
117
128
70-144
8
135
141
70-143
5
135
146
69-144
8
127
139
70-151
9
138
149
70-139
7 M1
142
150
70-142
6
148
154
62-146
4 M1
141
150
61-162
6
95
105
70-130
102
99
70-130
102
101
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/11 /2024 03:31 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 15

cem
Project: CR EFFLUENT PPA-Revised Report
Pace Project No.: 92720687
QC Batch: 844694
QC Batch Method: EPA 624.1
Associated Lab Samples: 92720687001
METHOD BLANK: 4362220
Associated Lab Samples: 92720687001
Parameter
Acrolein
Acrylonitrile
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
QUALITY CONTROL DATA
Analysis Method:
Analysis Description:
Laboratory:
Matrix: Water
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
EPA 624.1
624 MSV with Acrolein
Pace Analytical Services - Charlotte
Units
Blank
Result
Reporting
Limit
Analyzed
ug/L
ND
5.0
04/05/2410:09
ug/L
ND
5.0
04/05/2410:09
%
110
70-130
04/05/2410:09
%
97
70-130
04/05/2410:09
%
102
70-130
04/05/2410:09
LABORATORY CONTROL SAMPLE:
4362221
Spike
LCS LCS
Parameter
Units
Conc.
Result % Rec
Acrolein
ug/L
100
107 107
Acrylonitrile
ug/L
100
101 101
1,2-Dichloroethane-d4 (S)
%
98
4-Bromofluorobenzene (S)
%
102
Toluene-d8 (S)
%
100
Qualifiers
% Rec
Limits Qualifiers
60-140
70-130
70-130
70-130
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
4362222
4362223
MS
MSD
92722471002 Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
Acrolein
ug/L
ND 100
100
76.5
66.3
77
66
40-160 14 H1
Acrylonitrile
ug/L
ND 100
100
126
113
126
113
59-155 11 H1
1,2-Dichloroethane-d4(S)
%
113
107
70-130
4-Bromofluorobenzene (S)
%
103
106
70-130
Toluene-d8 (S)
%
102
101
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/11 /2024 03:31 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 15

ace",
QUALITY CONTROL DATA
Project: CR EFFLUENT PPA-Revised Report
Pace Project No.: 92720687
QC Batch: 841650 Analysis Method: EPA 624 By SIM
QC Batch Method: EPA 624 By SIM Analysis Description: 624 MSV Volatiles by SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92720687001
METHOD BLANK: 4347083
Matrix: Water
Associated Lab Samples: 92720687001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
1,4-Dioxane(p-Dioxane)
ug/L
ND 2.0
03/26/2410:59
1,2-Dichloroethane-d4(S)
%
97 70-130
03/26/2410:59
Toluene-d8 (S)
%
108 70-130
03/26/24 10:59
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE: 4347084
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane(p-Dioxane) ug/L 20 21.7 108 60-140
1,2-Dichloroethane-d4(S) % 97 70-130
Toluene-d8 (S) % 105 70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4347085
4347086
MS
MSD
92720768001 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane(p-Dioxane)
ug/L ND 20
20 19.6
20.4 98
102
63-136 4
1,2-Dichloroethane-d4(S)
%
105
105
70-130
Toluene-d8 (S)
%
123
125
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/11/2024 03:31 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 15

�ceo
QUALIFIERS
Project: CR EFFLUENT PPA-Revised Report
Pace Project No.: 92720687
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
H1 Analysis conducted outside the EPA method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/11 /2024 03:31 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 15

(-�Face-
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: CR EFFLUENT PPA-Revised Report
Pace Project No.: 92720687
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
92720687001
CR EFFLUENT
EPA 624.1
842114
92720687001
CR EFFLUENT
EPA 624.1
844694
92720687001
CR EFFLUENT
EPA 624 By SIM
841650
Date: 04/11/2024 03:31 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
Page 12 of 15

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' fV` DC#Ttler ENV-FRM-HUNI-0083 v02_Sample Condition Upon Receipt
ace
%­�'r:,q':
Effective Date 11/1412022
*Check mark top half of box if pH and/or dechlorination is verified and Project
within the acceptance range for preservation samples,
Exceptions: VOA, Coliform, TOG, Oil and Grease, 011018015 (water) DOC, Lft
**Bottom half of box into list number of bottles
***Check all unpreserved Nitrates for chlorine
PM: ASF Due Date: 03/28/24
CLIENT: 93-TwoRivers
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PR Adjustment Log for Preserved Samples
Sample I
Type of Preservative
pH upon receipt
fate preservation adjusted
Time preservatiDn
adjusted
Amount of Preservative
added
tat —it
Note: Whenever there is a discrepancyratfecting North Carolina cornplid(Ices amples, a copy of this form vrill btesent to the @larch Carolina DM Cert[ficfrtion OMiice li:e.
Out of hold incorrect preservative, out of temp, incorrect containers.
Qualtrax ID: 69614 Page 2 of 2 Page 14 of 15

e-v,,
f I j
Trans-1,2-dwwornelhylene
34546
Bis (2-ahloreethyl) ether
1,1-dichloroethylet a
34501
Bis (2-chloroisopropyl) ether
34273
42-dichlompropane
C0541
"is (2-cth the
y xy plyl
43-dichloropropyle'ne
7719
ethte
4-6rorrcophcnylpkenylelher
CG1100
Ethylbeozene
34371
Butyl bamylphthalate
3dG3G
Methyl bromide
34413
2-ahlamiwpkthalene
34292
Methyl chiQrlde
34419
4-ch(omphenylphenyl ether
34531
Mcthylone Chloride
34423
Ckrysane
34641
lrW-tetracbloroethane
81549
Dl-a-butylpklh,6te
34320
Tetraahloroethylerie
3447
T)-n-actylphlhalatie
39110
Toluene
34010
))rbcnzQ(a,h)nntlrracene
34596
"
—
1,1,14xiohloroothane
34506
1,?-dichlorahauzei�e
34556
1,1,2-trichloroathane
34511
i,3-dichlorobeozeae
34536
Trichlamethylene
39180
1.4-dichlorobeozene
34566
%Hoyt chlaride
39175
3,3-dichlorabeczldltte
34571
tlefde!eEraerahlaersmnatradd
Diothyl phthalate
3463t
firen�rA— —
P-chlnrQ m-cresQl
3 p 1S2
Dimethplphthalate
343336
2-ckloraphenot
34586
2,4-di di otoluene
3434i
2,4-dichlorapheaal
34601
2 ,6 d nitrQWlnzne
34611
2,4-dimetbylplzenol
4,6-dinitrC-o-crtsol
346t76
i?-dpkanylhydrazine
C0526
34344
2,4-dinitroghQrn1
34657
34616
Fluomathene
C0376
2-nNrophenol
34591
Fluarzuc
Hexachlarobe=a,!
34381
1!alarlfe arrrtrrlc carttrrourrdr•
4 nilropitztzol
PortWhlorophenol
34646
l exaahlCrobutadiene
C0700
C070Z
Acrolain
34210
Phenol
39032
FlexaclltarQeycla-pentadiczta
3438E
Aarylonitrte
34215
2,4,frtrichlaroplrenol
34694
FIexaciiloroethanc
3434E
Berizole
34030
BrsEralca
Mm
34621
Iud=C(12,3.cd)pyrene
34403
Bromo£Qrm
-
Aceanihee
Isophorone32104
34408
Carbon tetmchlaride
32102
Aaenaphthy[ete
34205
Napbtbaleac
34696
Chlorabznzene
34301
Antbrncene
34200
Nitrobenzene
34447
Chlomd bromomediale
34306
CO220
N-nitrosodl-n-propylamine
34418
ChIaroetbaae
858E1
Benz (,r)H
Hcnza{a)anthracene
39t20
N-nitrowdlmerhylamine
�44,39
)-ah(aroethylvinylether
34S76
Bon�(a}pyrene
C0526
K-nitrosodiphcuylaminc
34433
Cldoratorm
32106
3,4 benroitaorantkene
34247
PkcnantLrene
34461
17iohlarabromamefhaca
321.01
Benzo(9hi)peryleae
34230
Pyrenz
34469
l,t diahlaroerhane
34496
3enco(1<)0uoeanthen
34521
1„ 4 t ckiorolrenxeti
CpSSI
l,2-dlchloroetlaant
v
32103
His (2-eWor-thoay) mclt ace
4 r
''—`�
34278
► D►cXanc
Page 15 of 15

ace°
March 29, 2024
Susan Copeland
Two Rivers Utilities
5642 South York Highway
Gastonia, NC 28054
RE: Project: CR EFFLUENT
Pace Project No.: 92720682
Dear Susan Copeland:
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on March 22, 2024. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Ariel S Fitzgerald
[e-mail]
704-977-0945
Project Manager
Enclosures
cc: Jennifer Kirby, Two Rivers Utilities
David Shellenbarger, Two Rivers Utilities
44
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 11

(-�Face-
Project: CR EFFLUENT
Pace Project No.: 92720682
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
VirginiaNELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 11

(' AO�a c e 0
Project: CR EFFLUENT
Pace Project No.: 92720682
Lab ID Sample ID
92720682001 CR EFFLUENT
92720682002 CR EFFLUENT
PASI-A = Pace Analytical Services -Asheville
PASI-C = Pace Analytical Services - Charlotte
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Method
Analysts
Analytes
Reported
Laboratory
EPA 1664B
YY
1
PASI-C
EPA 200.7 Rev 4.4 1994
SBW
1
PASI-A
SM 2540C-2015
MDW
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 11

(-�Faceo
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: CR EFFLUENT
Pace Project No.: 92720682
Sample: CR EFFLUENT
Lab ID: 92720682001 Collected: 03/19/24 07:41
Received: 03/22/24 11:44 Matrix: Water
Parameters
Results Units Report Limit DF
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
Oil and Grease
ND mg/L 4.8 1
03/27/24 14:30
Sample: CR EFFLUENT
Lab ID: 92720682002 Collected: 03/19/24 07:41
Received: 03/22/24 11:44 Matrix: Water
Parameters
Results Units Report Limit DF
Prepared Analyzed CAS No. Qua]
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services -Asheville
Hardness, Total(SM 23406)
61400 ug/L 662 1
03/26/2413:00 03/27/24 15:11
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2015
Pace Analytical Services -Asheville
Total Dissolved Solids
356 mg/L 50.0 1
03/25/24 23:42
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2024 10:15 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 11

(-�Faceo
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: CR EFFLUENT
Pace Project No.: 92720682
QC Batch: 842095
Analysis Method:
EPA 1664B
QC Batch Method: EPA 1664E
Analysis Description:
1664 HEM, Oil and Grease
Laboratory:
Pace Analytical Services - Charlotte
Associated Lab Samples: 92720682001
METHOD BLANK: 4349099
Matrix: Water
Associated Lab Samples: 92720682001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Oil and Grease
mg/L
ND 5.0 03/27/24 14:30
LABORATORY CONTROL SAMPLE: 4349100
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Oil and Grease
mg/L
40 32.9
82 78-114
MATRIX SPIKE SAMPLE: 4349101
92720175002 Spike
MS MS % Rec
Parameter
Units
Result Conc.
Result % Rec Limits Qualifiers
Oil and Grease
mg/L
16.9 38.5
47.4 79 78-114
SAMPLE DUPLICATE: 4349102
92720514002 Dup
Parameter
Units
Result Result
RPD Qualifiers
Oil and Grease
mg/L
21.0 21.7 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2024 10:15 AM without the written consent of Pace Analytical Services, LLC, Page 5 of 11

(-�Face�
QUALITY CONTROL DATA
Project: CR EFFLUENT
Pace Project No.: 92720682
QC Batch: 841758 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92720682002
METHOD BLANK: 4347380
Associated Lab Samples: 92720682002
Parameter Units
Hardness, Total(SM 2340B) ug/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 662 03/27/2413:44
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE: 4347381
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Hardness, Total(SM 2340B) ug/L 33100 32500 98 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4347382 4347383
MS MSD
92720628001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Hardness, Total(SM 2340B) ug/L 9.6 33100 33100 39000 39900 89 92 70-130 2
mg/L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4347417 4347418
MS MSD
92720882001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Hardness, Total(SM 2340B) ug/L 29500 33100 33100 61400 64600 96 106 70-130 5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2024 10:15 AM without the written consent of Pace Analytical Services, LLC.
Page 6 of 11

ace"
QUALITY CONTROL DATA
Project: CR EFFLUENT
Pace Project No.: 92720682
QC Batch: 841674 Analysis Method: SM 2540C-2015
QC Batch Method: SM 254OC-2015 Analysis Description: 2540C Total Dissolved Solids
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92720682002
METHOD BLANK: 4347142
Associated Lab Samples: 92720682002
Parameter Units
Total Dissolved Solids mg/L
LABORATORY CONTROL SAMPLE: 4347143
Parameter Units
Total Dissolved Solids mg/L
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 25.0 03/25/24 23:42
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 256 102 90-110
SAMPLE DUPLICATE: 4347144
92719925006 Dup
Parameter Units Result Result
Total Dissolved Solids mg/L 4440 4460
RPD Qualifiers
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2024 10:15 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 11

(A"ga ce°
QUALIFIERS
Project: CR EFFLUENT
Pace Project No.: 92720682
I2747fkW11@H69
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
'Total' may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2024 10:15 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 11

cem
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
CR EFFLUENT
Pace Project No.:
92720682
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method Batch
92720682001
CR EFFLUENT
EPA1664B
842095
92720682002
CR EFFLUENT
EPA 200.7 Rev 4.4 1994
841758 EPA 200.7 Rev 4.4 1994 841898
92720682002
CR EFFLUENT
SM 2540C-2015
841674
Date: 03/29/2024 10:15 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 11

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ace"
April 10, 2024
Susan Copeland
Two Rivers Utilities
5642 South York Highway
Gastonia, NC 28054
RE: Project: CR EFFLUENT PPA
Pace Project No.: 92720681
Dear Susan Copeland:
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on March 22, 2024. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
� <J�
Ariel S Fitzgerald
[e-mail]
704-977-0945
Project Manager
Enclosures
cc: Jennifer Kirby, Two Rivers Utilities
David Shellenbarger, Two Rivers Utilities
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 16

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DC#_Title; ENV-FRM-HUNI-0083 02_Sample Condition Upon Receipt
Effective Date: 11/14/2022
*Cheek mark tole half of box if pH and/or dechlorination is verified and
within the acceptance range for preservation samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, ORO/8415 twatori DOC, LLHU
**Bottom half of box is to list number of bottles
***Check all unpreserved Nitrates for chlorine
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Mote: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form tvzll he sent to the North Carolina DENR Certification Office (Le,
Out of hold, incorrect preservative, out of temp, incorrect containers.
Qualtrax ID: 69614 Page 2 of 2 Page 3 of 16

aceAnalytical
Report of Analysis
Pace Analytical Services, LLC
9800 Kincey Avenue
Suite 100
Huntersville, NC 28078
Attention: Ariel Fitzgerald
Project Name: CR Effluent PPA
Project Number: 92720681
Lot Number:ZC28034
Date Completed:04/09/2024
04/10/2024 1:59 PM
Approved and released by:
Project Coordinator 1: Jenna S. Holliday
P
4W.
ANSI Nalional Aceradltalioa Board
A C C R E D I T E D
e
/ TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 4 of 16
Page 1 of 13

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Pace Analytical Services, LLC
Lot Number: ZC28034
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 166413, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM
2320 B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011,
Fecal Coliform Colilert-18. If you have any questions regarding this report, please contact the Pace
Project Manager listed on the cover page.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
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PACE ANALYTICAL SERVICES, LLC
Sample Summary
Pace Analytical Services, LLC
Lot Number: ZC28034
Project Name: CR Effluent PPA
Project Number: 92720681
Sample Number Sample ID Matrix Date Sampled Date Received
001 CR EFFLUENT Aqueous 03/19/2024 0747 03/28/2024
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
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Page 3 of 13

PACE ANALYTICAL SERVICES, LLC
Sample Sample ID
(0 detections)
Detection Summary
Pace Analytical Services, LLC
Lot Number: ZC28034
Project Name: CR Effluent PPA
Project Number: 92720681
Matrix Parameter
Method Result Q Units Page
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 16
Page 4 of 13

Inorganic non-metals
Client: Pace Analytical Services, LLC Laboratory ID:ZC28034-001
Description: CR EFFLUENT Matrix: Aqueous
Date Sampled:03/19/2024 0747 Project Name: CR Effluent PPA
Date Received:03/2812024 Project Number: 92720681
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Phenolics) 9065 1 04/04/2024 1731 DMA 99429
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Phenolics 9065 ND 0.0050 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 16
Page 5 of 13

QC Summary
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: ZC28034
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 16
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Inorganic non-metals - MB
Sample ID: ZQ99429-001 Matrix: Aqueous
Batch: 99429
Analytical Method: 9065
Parameter Result Q Dil LOQ Units Analysis Date
Phenolics ND 1 0.0050 mg/L 04/04/20241722
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: ZC28034
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 16
Page 7 of 13

Inorganic non-metals - LCS
Sample ID: ZQ99429-002 Matrix: Aqueous
Batch: 99429
Analytical Method: 9065
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Phenolics 0.050 0.050 1 101 90-110 04/04/20241726
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: ZC28034
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 16
Page 8 of 13

Inorganic non-metals - MS
Sample ID: ZC28034-001 MS
Batch:99429
Analytical Method: 9065
Matrix: Aqueous
Sample Spike
Amount Amount Result %Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Phenolics ND 0.050 0.049 1 98 90-110 04/04/20241735
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
* = RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: ZC28034
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 16
Page 9 of 13

Inorganic non-metals - MSD
Sample ID: ZC28034-001MD
Batch: 99429
Analytical Method: 9065
Matrix: Aqueous
Sample Spike
Amount Amount Result %Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Phenolics ND 0.050 0.049 1 98 0.86 90-110 20 04/04/20241740
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
* = RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: ZC28034
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 13 of 16
Page 10 of 13

Chain of Custody
m7 re
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 14 of 16
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone]
www.pacelabs.com
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Page 15 of 16
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PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 16 of 16
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