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HomeMy WebLinkAboutNC0024201_Permit renewal application_20111231October 5, 2011 Dear Mr. Brown: Sincerely, cc: Beverly Eaves Perdue Governor Dee Freeman Secretary Subject: Receipt of permit renewal application NPDES Permit NC0024201 Roanoke Rapids WWTP Halifax County’ 1517 Mail Service Center, Raleigh, North Carolina 27699-1517 Location: 512 N. Salisbury St Raleigh, North Carolina 27604 Phone 919-807-6300 \ FAX 919-807-64921 Customer Service: 1-877-623-6748 Internet ww.ncwaterquality org An Equal OpportunityAffirmative Action Employer » Dina Sprinkle Point Source Branch R DANIELEY BROWN PE CHIEF EXECUTIVE OFFICER ROANOKE RAPIDS SANITARY DISTRICT PO BOX 308 ROANOKE RAPIDS NC 27870 If you have any additional questions concerning renewal of the subject permit, please contact Gil Vinzani at (919) 807-6395. CENTRAL FILES Raleigh Regional Office/Surface Water Protection NPDES Unit ^07} .... ocr. North CarolinaNaturally NCDENR North Carolina Department of Environment and Natural Resources Division of Water Quality * Coleen H. Sullins Director The NPDES Unit received your permit renewal application on October 4, 2011. A member of the NPDES Unit will review your application. They will contact you if additional information is required to complete your permit renewal. You should expect to receive a draft permit approximately 30-45 days before your existing permit expires. Roanoke Rapids Sanitary District September 30. 2011 RE: Dear Ms. Sprinkle, Renewal ofNPDES Permit Number NC0024201 Roanoke River Waste Treatment Plant P.O. Box 308 1000 Jackson Street Roanoke Rapids, NC 27870 (252) 537-9137 Fax: (252)537-3064 w^'w.rrsd.o.rg RRSD respectfully requests that the following issues be addressed in this permit renewal: • We request that Footnote 1 remain in the permit unaltered. • We are in the process of identifying a new downstream sampling location. Our current downstream sampling location is at U.S. 158 crossing the Roanoke River. Traffic has increased significantly on U.S. 158, and we are concerned for the safety of our staff. Our intention is to send a letter to the Division in the next few weeks that will outline the reason for our request. We will identify the location of the proposed and current downstream sampling locations in this correspondence. • We request that Footnote 2 - Monthly average effluent CBOD§ and TSS concentrations shall not exceed 15% of the respective influent value (i.e., 85% removal is required.) - be removed from the permit. We believe that the additional percentage removal limitation is not warranted as the facility continuously meets the monthly and weekly average permit limit. If Footnote 2 is not removed, we request that the language be modified to make an exception for low influent suspended solids and CBOD events. Our facility has difficulty­ meeting this percent removal requirement when influent suspended solids and CBOD concentrations are extremely low. Thus, we request that Footnote 2 be modified, as follows: Monthly average effluent CBOD5 and TSS concentrations shall not exceed. 15% The Roanoke Rapids Sanitary District (RRSD) is permitted to discharge treated effluent to the Roanoke River. The permit expires on March 31, 2012. Tire enclosed application is for ren ewal of the referenced permit. In accordance with the requirements of North Carolina G.S. 143.215.1(c), we are submitting one signed original and two copies of the completed application package. The application package includes the following: 1. Completed permit application form, EPA Form 2 A, with figures. 2. Attachment A: Priority Pollutant Scan Analyses (five scans). 3. Attachment B: Second Species Toxicity Tests (four tests). 4. Attachment C: Biosolids Management Description. "i “ff r /A Ms. Dina Sprinkle NC DENR, Division of Water Quality, NPDES Unit 1617 Mail Service Center Raleigh, North Carolina, 27699-1617 2/Month1/Week11.1%0726.5 25"6 1/Week3/Week4.2%1.06 2/Month1/Week24.9%3.9115.7 1/Month0.0120.009 1/Month0.0720.058Zinc o o o o <u cn 2 o> E 5 O)S* C O) O E 4.9 Parameter_______ Dissolved Oxygen (June, _Julyx August, September) Dissolved Oxygen (October through May)__ " Temperature (June, July, August, September)___ Temperature (October through May)__ ’Copper 25 30‘ 6.7 "184 3.50 “f3.8 T84 2.03 OXKSS “1,88 3.T0_ 0.69 29.4% 0.21% 53_8% 22.4% 37.5% 28% 61% 5/week 5/week 5/week _ 1/mpnJh 1/month Data reported from Long Term Monitoring Plan Data reported from Long Term Monitoring Plan 2/week............... 3/week ........... ~1/week___ 1/quarter_____ i/quarter c o §s Q cts T5 E 12 __co 0.37 CBO_D _ _ TSS Ammonia total Phosphorus cu O) 2 a>>*•£ E £ a ?! o a> ^_Q=. o c o .2 E 13 o •£ O rc O > 7.6% The monitoring data indicates that our discharge is routinely in compliance with pennit limits. The coefficient of variation is less than 40% for all of our samples except for ammonia. The low coefficient of variation indicates nominal variability in our effluent. Our conclusions from the MBR analysis are as follows: We request a reduction in the frequency of upstream and downstream stream sampling events for dissolved oxygen and temperature from 3/week to 1/week in June, July, August, and September. We also request a reduction in the upstream and downstream sampling events from October through May to be reduced from 1/week to 2/roonth. Reduce the CBOD? monitoring frequency from daily sampling to 2/week. Reduce the TSS monitoring frequency from daily sampling to 3/week Reduce the ammonia monitoring frequency from daily sampling to 1/week. o E 0> *! E S'-? <5 ill E ^2 go § O <D Q-‘c Q- 1/Week Table 1: Summary of Monitoring Burden Reduction Analysis ** s E 0) a. >» It ofthB respective influent value (U., 85% removal is required). This requirement shall he waived if influent TSS concentrations are less than 150 mg/l and/or influent CBOD is less than 100 mg/l. . Wc request an increase in the Total Residual Chlorine permit limit from 28 pg/L to 50 u.g/L pursuant to the DWQ Point Source Branch correspondence dated May 1, 2008. • We request a reduction in monitoring frequency for several parameters. We performed a Monitoring Burden Reduction (MBR) analysis on our effluent monitoring data for the last two years as recommended in tire EPA Guide for Performance Based Reductions of NPDHS Permit Monitoring Frequencies (April 1996). A summary of these results is presented in Table I. on RRSD Effluent Monitoring Data >» u E V 3 ♦s ofs* E i E 5 o>“ ^.e-e >2 S t E B* 3 ° J- cj 5 S 3/Week o o o o Attachments cc: We very much appreciate the time and effort of the NPDES Unit to consider our requests for this permit renewal. Please do not hesitate to call myself (252-537-9137) or Mary Sadler with Hazen and Sawyer (919-755-8560) if you have any questions. Gregg-Camp. ORC RRSD Wastewater Treatment Plant Jeff Poupart. DWQ, Point Source Branch Chief Tom Belnick. DWQ, NPDES Unit Supervisor Maty Sadler. Hazen and Sawyer File A copy of the permit Fact Sheet. Documentation for any methodology, data, and assumptions used in any permit modification, including Reasonable Potential Analyses, if applicable. A copy of any comments that are received from the public regarding this permit renewal, if applicable. Reduce the total nitrogen and total phosphorous monitoring frequency from monthly sampling to once per quarter. Remove the monthly effluent composite sampling for copper and zinc. Our Discharge Monitoring Report (DMR) data shows negligible amounts of these pollutants in our effluent. These monitoring frequencies were originally required in the former NPDES permit allowing a discharge to Chockoyotte Creek. The results of these metals tests will continue to be transferred from our Long Term Monitoring Plan and reported on our DMR quarterly and monthly during Year 5 of the Long Term Monitoring Plan, as required. Reduce the chronic toxicity sampling (Cer io daphnia) from quarterly to annually. We have been conducting chronic toxicity testing since April 1993. All of our toxicity tests have passed, including the second species testing with Fathead Minnow. • We request the following information as part o f the draft permit preparation: o o We would like to offer a final consideration regarding the timing of our draft NPDES pennit. We understand that there are several outstanding technical issues that the Division is in the process of resolving, e.g. language revisions to permit standard conditions, the proposed EPA impaired -water status for mercury over the entire state of North Carolina, the North Carolina Water Quality Association's (NCQWA) request for reduced sampling and monitoring, and the issues associated with the Triennial Review. We would like to request that these technical issues be resolved prior to our draft permit being issued. We would continue to operate under our current permit until such time a draft NPDES is prepared by the Division and the final permit is issued. Sincerely, Roanoke Rapids Sanitary District R. Danieley Brown, P.E. Chief Executive Officer BASIC APPLICATION INFORMATION Roanoke River Waste Treatment Plant Facility Name Mailing Address 135 Aqueduct Road Weldon, North Carolina 27890 A. Gregg CampContact Person uOCTOperator in Responsible ChargeTitle 0 ^1— (252) 536-4884Telephone Number 135 Aqueduct RoadFacility Address Weldon, North Carolina 27890 (not P.O. Box) A.2. Applicant Information. If the applicant is different from the above, provide the following: Roanoke Rapids Sanitary District Applicant Name 1000 Jackson Street. PO Box 308 Mailing Address Roanoke Rapids. North Carolina 27870 R. Danieley BrownContact Person Chief Executive OfficerTitle (252) 537-9137Telephone Number Is the applicant the owner or operator (or both) of the treatment works? El operator NPDES NC00242Q1 Other Stormwater Permit - General NCG110000 UIC Other Land Application Permit WQ0001989 RCRA Other Collection System Permit WQCSQ0027 PSD municipalities and areas served by the facility. Provide the name and population of each Name Population Served Type of Collection System Ownership Roanoke Rapids 17.000 Separate Sanitary District Gaston 1,650 Separate Sanitary District Halifax & Northampton County 336 Separate County Total population served 18,986 EPA Form 3510-2A (Rev. 1-99). Replaces ERA forms 7550-6 & 7550-22.Page 2 of 22 RIVER BASIN: Roanoke NC DENR Raleigh Re^onal Office _________•______ PERMIT ACTION REQUESTED: Standard Renewal Indicate whether correspondence regarding this permit should be directed to the facility or the applicant. facility E applicant - --------------------------------#______________ FACILITY NAME AND PERMIT NUMBER: Roanoke River WWTP, NC0024201 El owner PART A. BASIC APPLICATION INFORMATION FOR ALL APPLICANTS: All treatment works must complete questions A.1 through A.8 of this Basic Application Information Packet A.1. Facility Information. E C E 0 W E [r^-------1- . 0ENR-WATFR QUALITY TOINT SOURCE BfVWCH A.3. Existing Environmental Permits. Provide the permit number of any existing environmental permits that have been issued to the treatment works (include state-issued permits). A.4. Collection System Information. Provide information on r _..J---------------- - U1C 11Q111C ailu (JU(JU,ailuII entity and, if known, provide information on the type of collection system (combined vs. separate) and its ownership (municipal, private, etc.). A.5. Indian Country. Is the treatment works located in Indian Country?a. Yes 3 No b. Yes E3 No A.6. Design flow rate 8.34a.mgd Two Years Ago Last Year This Year b.Annual average daily flow rate 4.1 MGD 4,1 MGD 3.2 MGD Maximum daily flow ratec.13.7 MGD 4.1 MGD 12.9 MGD A.7. Collection System. Indicate the type(s) of collection system(s) used by the treatment plant. Check all that apply. Also estimate the percent contribution (by miles) of each. 0 Separate sanitary sewer 100 % Combined storm and sanitary sewer N/A % A.8. Discharges and Other Disposal Methods. Does the treatment works discharge effluent to waters of the U.S.?S Yesa. No If yes, list how many of each of the following types of discharge points the treatment works uses: i.Discharges of treated effluent 1 ii.Discharges of untreated or partially treated effluent 0 iii.Combined sewer overflow points 0 iv.Constructed emergency overflows (prior to the headworks)0 Other N/Av.0 b. that do not have outlets for discharge to waters of the U.S.?0 No If yes, provide the following for each surface impoundment: Location:N/A N/A mgd Does the treatment works land-apply treated wastewater?c. Yes 0 No If yes, provide lhe following for each land application site: Location:N/A Number of acres:0 0 mgd Is land application intermittent? d. Yes 0 No EPA Form 3510-2A (Rev. 1-99). Replaces ERA forms 7550-6 & 7550-22.Page 3 of 22 Does the treatment works discharge or transport treated or untreated wastewater to another treatment works? Annual average daily volume applied to site: continuous or Annual average daily volume discharge to surface impoundment(s) Is discharge continuous or intermittent? PERMIT ACTION REQUESTED: Standard Renewal RIVER BASIN: Roanoke __________________• FACILITY NAME AND PERMIT NUMBER: Roanoke River WWTP, NC0024201 Does the treatment works discharge effluent to basins, ponds, or other surface impoundments “ - Yes Does the treatment works discharge to a receiving water that is either in Indian Country or that is upstream from (and eventually flows through) Indian Country? Flow. Indicate the design flow rate of the treatment plant (i.e., the wastewater flow rate that the plant was built to handle). Also provide the average daily flow rate and maximum daily flow rate for each of the last three years. Each year's data must be based on a 12-month time period with the 12 month of “this year" occurring no more than three months prior to this application submittal. N/A If transport is by a party other than the applicant, provide: Transporter Name N/A Mailing Address N/A N/A Contact Person N/A Title N/A Telephone Number N/A For each treatment works that receives this discharge, provide the following: Name N/A Mailing Address N/A N/A Contact Person N/A Title N/A Telephone Number N/A If known, provide the NPDES permit number of the treatment works that receives this discharge N/A Provide the average daily flow rate from the treatment works into the receiving facility.N/A mgd e. Yes El No Description of method (including location and size of site(s) if applicable): N/A N/A intermittent?or EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.Page 4 of 22 Annual daily volume disposed by this method: Is disposal through this method continuous Does the treatment works discharge or dispose of its wastewater in a manner not included in A.8. through A.8.d above (e.g., underground percolation, well injection): If yes, provide the following for each disposal method: __________•_______ PERMIT ACTION REQUESTED: Standard Renewal RIVER BASIN: Roanoke FACILITY NAME AND PERMIT NUMBER: Roanoke River WWTP, NC0024201 If yes, describe the mean(s) by which the wastewater from the treatment works is discharged or transported to the other treatment works (e.g., tank truck, pipe). WASTEWATER DISCHARGES: A.9. Description of Outfall. Outfall number 001a. b.Location (State) Distance from shore (if applicable)c.N/A ft. d.Depth below surface (if applicable)N/A ft. Average daily flow ratee.3.8 mgd f.Does this outfall have either an intermittent or a periodic discharge? Yes 0 No (gotoA.9.g.) If yes, provide the following information: Number f times per year discharge occurs:N/A Average duration of each discharge:N/A Average flow per discharge:N/A mgd Months in which discharge occurs:N/A Is outfall equipped with a diffuser?g- Yes 0 No A.10. Description of Receiving Waters. Name of receiving watera.Roanoke River b.Name of watershed (if known)Roanoke River and Tributaries United States Soil Conservation Service 14-digit watershed code (if known):03010107070010 Name of State Management/River Basin (if known): Roanoke River Basinc. United States Geological Survey 8-digit hydrologic cataloging unit code (if known):03010107 d.Critical low flow of receiving stream (if applicable) 1172 cfs (7Q10) acute cfs chronic cfs Total hardness of receiving stream at critical low flow (if applicable): unknowne.mg/l of CaCO3 ERA Form 3510-2A (Rev. 1-99). Replaces ERA forms 7550-6 & 7550-22.Page 5 of 22 27890 (Zip Code) RIVER BASIN: Roanoke _____________ FACILITY NAME AND PERMIT NUMBER: Roanoke River WWTP, NC0024201 _________ PERMIT ACTION REQUESTED: Standard Renewal Weldon_____________ (City or town, if applicable) Halifax (County) 36° 26' 13" (Latitude) 77° 36' 37" (Longitude) If you answered lYes” to question A.8.a, complete questions A.9 through A.12 once for each outfall (including bypass points) through which effluent is discharged. Do not include information on combined sewer overflows in this section. If you answered “No” to question AJTa, go to Part B, "Additional Application Information for Applicants with a Design Flow Greater than or Equal to 0.1 mgd.” RIVER BASIN: Roanoke A.11. Description of Treatment a. □ Advanced Describe: b. Design BODS removal or Design CBOD5 removal 90 % Design SS removal 90 % Design P removal N/A % Design N removal N/A % Other N/A N/A % What type of disinfection is used for the effluent from this outfall? If disinfection varies by season, please describe:c. Sodium Hypochlorite If disinfection is by chlorination is dechlorination used for this outfall?El Yes □ No Does the treatment plant have post aeration?□ Yes 0 No minimum, effluent testing data must be based on at least three samples and must be no more than four and one-half years apart. Outfall number:001 MAXIMUM DAILY VALUE AVERAGE DAILY VALUEPARAMETER Value Units Value Units pH (Minimum)6.9 s.u. pH (Maximum)6.5 s.u. Flow Rate 5.66 MGD 3.76 MGD 5 Temperature (Winter)13.95 °C 11.9 °C 4 26.9 °C 25.5 °C 5 AVERAGE DAILY DISCHARGE POLLUTANT ML/MDL Cone.Units Cone.Units CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS BODS CBOD5 6.8 Mg/I 5.6 Mg/I 5 SM5210B 2 mg/l FECAL COLIFORM 60 16 5 SM9222D 1/100ml TOTAL SUSPENDED SOLIDS (TSS)27.4 Mg/I 11.4 Mg/I 5 SM2540 2.5 mg/l EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.Page 6 of 22 END OF PART A. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE PERMIT ACTION REQUESTED: Standard Renewal Colon! es/100 ml Number of Samples ANALYTICAL METHOD BIOCHEMICAL OXYGEN DEMAND (Report one) FACILITY NAME AND PERMIT NUMBER: Roanoke River WWTP, NC0024201 Colonies /100ml Temperature (Summer) * For pH please report a minimum and a maximum daily value MAXIMUM DAILY DISCHARGE Number of Samples What level of treatment are provided? Check all that apply. S Primary S Secondary □ Other. Indicate the following removal rates (as applicable): A.12. Effluent Testing Information. All Applicants that discharge to waters of the US must provide effluent testing data for the following parameters. Provide the indicated effluent testing required by the permitting authority for each outfall through which effluent is discharged. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. At a BASIC APPLICATION INFORMATION PART B. B.1. b. c. d. e. f. B.3. B.4. N/A N/AMailing Address: N/A N/ATelephone Number: N/AResponsibilities of Contractor: B.5. b. EPA Form 3510-2A (Rev. 1-99). Replaces ERA forms 7550-6 & 7550-22.Page 7 of 22 contractor? Yes If yes, list the name, address, pages if necessary). Name: ___ft__ PERMIT ACTION REQUESTED: Standard Renewal RIVER BASIN: Roanoke List the outfall number (assigned in question A.9) for each outfall that is covered by this implementation schedule. N/A _______ft____ FACILITY NAME AND PERMIT NUMBER: Roanoke River WWTP, NC0024201 gpd Briefly explain any steps underway or planned to minimize inflow and infiltration. The District continues SSES for I & I in the collection system; Collection System Master Plan has been developed; Sub­ Basin, A & B have been rehabbed; Belmont Area SSES in progress; Comprehensive SSES for Basin I budgeted. Indicate whether the planned improvements or implementation schedule are required by local, State, or Federal agencies. N/A Yes No Scheduled improvements and Schedules of Implementation. Provide information on any uncompleted implementation schedule or uncompleted plans for improvements that will affect the wastewater treatment, effluent quality, or design capacity of the treatment works. If the treatment works has several different implementation schedules or is planning several improvements, submit separate responses to question B.5 for each. (If none, go to question B.6.) a. ADDITIONAL APPLICATION INFORMATION FOR APPLICANTS WITH A DESIGN FLOW GREATER THAN OR EQUAL TO 0.1 MGD (100,000 gallons per day). All applicants with a design flow rate £ 0.1 mgd must answer questions B.1 through B.6. All others go to Part C (Certification). Inflow and Infiltration. Estimate the average number of gallons per day that flow into the treatment works from inflow and/or infiltration. 1,410,000 Operation/Maintenance Performed by Contractor(s). Are any operational or maintenance aspects (re^ted t0 wastewater treatment and effluent quality) of the treatment works the responsibility of a telephone number, and status of each contractor and describe the contractor’s responsibilities (attach additional B.2. Topographic Map. Attach to this application a topographic map of the area extending at least one mile beyond facility property boundaries. This map must show the outline of the facility and the following information. (You may submit more than one map if one map does not show the entire area.) See Attached Figure a. The area surrounding the treatment plant, including all unit processes. The major pipes or other structures through which wastewater enters the treatment works and the pipes or other structures through which treated wastewater is discharged from the treatment plant. Include outfalls from bypass piping, if applicable. Each well where wastewater from the treatment plant is injected underground. Wells, springs, other surface water bodies, and drinking water wells that are: 1) within ’/« mile of the property boundaries of the treatment works, and 2) listed in public record or otherwise known to the applicant. Any areas where the sewage sludge produced by the treatment works is stored, treated, or disposed. If the treatment works receives waste that is classified as hazardous under the Resource Conservation and Recovery Act (RCRA) by truck, rail, or special pipe, show on the map where the hazardous waste enters the treatment works and where it is treated, stored, and/or disposed. Process Flow Diagram or Schematic. Provide a diagram showing the processes of the treatment plant, including all bypass piping and all backup power sources or redunancy in the system. Also provide a water balance showing all treatment units, including disinfection (e.g., chlorination and dechlorination). The water balance must show daily average flow rates at influent and discharge points and approximate daily flow rates between treatment units. Include a brief narrative description of the diagram. See Attached Figure c. d. Schedule Actual Completion Implementation Stage MM/DD/YYYY MM/DD/YYYY - Begin Construction ///I - End Construction /I /I - Begin Discharge I I // - Attain Operational Level /I I e.□ Yes □ No B.6. Outfall Number: 001 AVERAGE DAILY DISCHARGE POLLUTANT MUMDL Cone.Units Cone.Units 3.76 Mg/I 1.9 Mg/I 5 SM4500F O.lmg/I <15 Ug/I <11.4 Ug/I 5 HACK 10014 <10ug/l DISSOLVED OXYGEN 5.9 Mg/I 5.12 Mg/I 5 SM4500-OG NA 8.99 Mg/I 4.16 Mg/i 5 ERA 351.1 0.2mg/l 15.9 Mg/I 12.7 Mg/I 5 ERA 353.2 0.1mg/l OIL and GREASE <5 Mg/I <5 Mg/I 5 ERA1664A 5mg/l PHOSPHORUS (Total)4.08 Mg/I 2.16 Mg/I 5 ERA 200.7 0.02mg/l 391 Mg/I 280.8 Mg/I 5 SM2540C 10mg/l OTHER NA ERA Form 3510-2A (Rev. 1-99). Replaces ERA forms 7550-6 & 7550-22.Page 8 of 22 J TOTAL DISSOLVED SOLIDS (TDS) TOTAL KJELDAHL NITROGEN (TKN) NITRATE PLUS NITRITE NITROGEN CHLORINE (TOTAL RESIDUAL, TRC) END OF PART B. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE MAXIMUM DAILY DISCHARGE PERMIT ACTION REQUESTED: Standard Renewal Number of Samples ANALYTICAL METHOD RIVER BASIN: Roanoke FACILITY NAME AND PERMIT NUMBER: Roanoke River WWTP, NC0024201 If the answer to B.5.b is "Yes," briefly describe, including N/A CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS AMMONIA (as N) new maximum daily inflow rate (if applicable). Provide dates imposed by any compliance schedule or any actual dates of completion for the implementation steps listed below, as applicable, -or improvements planned independently of local, State, or Federal agencies, indicate planned or actual completion dates as applicable. Indicate dates as accurately as possible. N/A 2 __ Have appropriate permits/clearances concerning other Federal/State requirements been obtained? Describe briefly: N/A EFFLUENT TESTING DATA (GREATER THAN 0.1 MGD ONLY). Applicants that discharge to waters of the US must provide effluent testing data for the following parameters. Provide the indicated effluent testing required by the permitting authority for each outfall through which effluent is discharged. Do not Include information on combine sewer overflows in this section. All Information reported must be based on data collected through analysis conducted • Parl 136 methods- ln addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. At a minimum effluent testing data must be based on at least three pollutant scans and must be no more than four and on-half years old. BASIC APPLICATION INFORMATION PARTC. CERTIFICATION ALL APPLICANTS MUST COMPLETE THE FOLLOWING CERTIFICATION. Name and official title Signature Telephone number (252) 537-9137 Date signed works or identify appropriate permitting requirements. SEND COMPLETED FORMS TO: 27699-1617 EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.Page 9 of 22 PERMIT ACTION REQUESTED: Standard Renewal RIVER BASIN: Roanoke _____e> FACILITY NAME AND PERMIT NUMBER: Roanoke River WWTP, NC0024201 NCDENR/ DWQ Attn: NPDES Unit 1617 Mail Service Center Raleigh, North Carolina R. Danieley Brown, Chief Executive Officer, Roanoke Rapids Sanitary District 21; 2oi I_____________________________ Upon request of the permitting authority, you must submit any other information necessary to assure wastewater treatment practices at the treatment AH applicants must complete the Certification Section. Refer to Instructions to determine who is an officer for the purposes of this certification. All applicants must complete all applicable sections of Form 2A, as explained in the Application Overview. Indicate below which parts of Form 2A you have completed and are submitting. By signing this certification statement, applicants confirm that they have reviewed Form 2A and have completed all sections that apply to the facility for which this application is submitted. Indicate which parts of Form 2A you have completed and are submitting: El Basic Application Information packet Supplemental Application Information packet: El Part D (Expanded Effluent Testing Data) EJ Part E (Toxicity Testing: Biomonitoring Data) El Part F (Industrial User Discharges and RCRA/CERCLA Wastes) □ Part G (Combined Sewer Systems) I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information, the information is. to the best of my knowledge and belief true accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment RIVER BASIN: Roanoke River WWTP. NC0024201 Standard Renewal Roanoke SUPPLEMENTAL APPLICATION INFORMATION PART D. EXPANDED EFFLUENT TESTING DATA Refer to the directions on the cover page to determine whether this section applies to the treatment works. The five required Priority Pollutant Scans are Attachment A to this NPDES Permit Application. Outfall number:001 (Complete once for each outfall discharging effluent to waters of the United States.) MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE POLLUTANT ML/MDL Cone.Units Mass Units Cone.Units Mass Units METALS (TOTAL RECOVERABLE). CYANIDE, PHENOLS, AND HARDNESS. ANTIMONY ARSENIC BERYLLIUM CADMIUM CHROMIUM COPPER LEAD MERCURY NICKEL SELENIUM SILVER THALLIUM ZINC CYANIDE HARDNESS (as CaCO3) Use this space (or a separate sheet) to provide information on other metals requested by the permit writer EPA Form 3510-2A (Rev 1-99). Replaces ERA forms 7550-6 & 7550-22.Page 10 of 22 FACILITY NAME AND PERMIT NUMBER: ____________•)__________ PERMIT ACTION REQUESTED: TOTAL PHENOLIC COMPOUNDS Number of Samples ANALYTICAL METHOD Effluent Testing: 1.0 mgd and Pretreatment Works. If the treatment works has a design flow greater than or equal to 1 0 mgd or it has (or is required to have) a pretreatment program, or is otherwise required by the permitting authority to provide the data, then provide effluent testing data for the following pollutants. Provide the indicated effluent testing information and any other information required by the permitting authority for each outfall through which effluent is discharged. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected through analyses conducted using 40 CFR Part 136 methods. In addition, these data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. Indicate in the blank rows provided below any data you may have on pollutants not specifically listed in this form. At a minimum, effluent testing data must be based on at least three pollutant scans and must be no more than four and one-half years old. PERMIT ACTION REQUESTED:RIVER BASIN: Roanoke River WWTP, NC0024201 Standard Renewal Roanoke Outfall number: 001 AVERAGE DAILY DISCHARGE POLLUTANT ML/MDLCone.Units Mass Units Cone.Units Mass Units VOLATILE ORGANIC COMPOUNDS ACROLEIN ACRYLONITRILE BENZENE BROMOFORM CHLOROBENZENE CHLOROETHANE CHLOROFORM 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE ETHYLBENZENE METHYL BROMIDE METHYL CHLORIDE METHYLENE CHLORIDE TOLUENE EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22 Page 11 of 22 ___________________ FACILITY NAME AND PERMIT NUMBER: (Complete once for each outfall discharging effluent to waters of the United States.) MAXIMUM DAILY DISCHARGE Number of Samples ANALYTICAL METHOD TETRACHLORO­ ETHYLENE 1,1,2.2-TETRA- CHLOROETHANE TRANS-1.2-DICHLORO- ETHYLENE DICHLOROBROMO­ METHANE 1,1-DICHLORO- ETHYLENE 1,3-DICHLORO- PROPYLENE 2-CHLOROETHYLVINYL ETHER CARBON TETRACHLORIDE CHLORODIBROMO­ METHANE FACILITY NAME AND f’ERMIT NUMBER:PERMIT ACTION REQUESTED:RIVER BASIN: Roanoke River WWTP, NC0024201 Standard Renewal Roanoke Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.) MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE POLLUTANT ML/MDLCone.Units Mass Units Cone.Units Mass Units TRICHLOROETHYLENE VINYL CHLORIDE Use this space (or a separate sheet) to provide information on other volatile organic compounds requested by the permit writer ACID-EXTRACTABLE COMPOUNDS P-CHLORO-M-CRESOL 2-CHLOROPHENOL 2,4-DICHLOROPHENOL 2,4-DIMETHYLPHENOL 4,6-DINITRO-O-CRESOL 2,4-DINITROPHENOL 2-NITROPHENOL 4-NITROPHENOL PENTACHLOROPHENOL PHENOL Use this space (or a separate sheet) to provide information on other acid-extractable compounds requested by the permit writer BASE-NEUTRAL COMPOUNDS ACENAPHTHENE ACENAPHTHYLENE ANTHRACENE BENZIDINE BENZO(A)ANTHRACENE BENZO(A)PYRENE Page 12 of 22EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22 Number of Samples ANALYTICAL METHOD 2,4.6- TRICHLOROPHENOL 1.1.1- TRICHLOROETHANE 1,1,2- TRICHLOROETHANE FACILITY NAME AND PERMIT NUMBER:PERMIT ACTION REQUESTED:RIVER BASIN: Roanoke River WWTP, NC0024201 Standard Renewal Roanoke Outfall number: 001 AVERAGE DAILY DISCHARGE POLLUTANT ML/MDLCone.Units Mass Units Cone.Units Mass Units BENZO(GHI)PERYLENE CHRYSENE DI-N-BUTYL PHTHALATE DI-N-OCTYL PHTHALATE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1.4-DICHLOROBENZENE DIETHYL PHTHALATE DIMETHYL PHTHALATE 2,4-DINITROTOLUENE 2.6-DINITROTOLUENE EPA Form 3510-2A (Rev 1-99) Replaces EPA forms 7550-6 & 7550-22.Page 13 of 22 Number of Samples 1,2-DIPHENYL- HYDRAZINE 2-CHLORO- NAPHTHALENE BENZO(K) FLUORANTHENE ANALYTICAL METHOD DIBENZO(A.H) ANTHRACENE 3,3-DICHLORO- BENZIDINE 4-CHLORPHENYL PHENYL ETHER 4-BROMOPHENYL PHENYL ETHER BIS (2-ETHYLHEXYL) PHTHALATE BUTYL BENZYL PHTHALATE BIS (2-CHLOROISO- PROPYL) ETHER BIS (2-CHLOROETHOXY) METHANE BIS (2-CHLOROETHYL)- ETHER 3,4 BENZO­ FLUORANTHENE ----- (Complete once for each outfall discharging effluent to waters of the United States.) MAXIMUM DAILY DISCHARGE FACILITY NAME AND PERMIT NUMBER:PERMIT ACTION REQUESTED:RIVER BASIN: Roanoke River WWTP, NC0024201 Standard Renewal Roanoke Outfall number: 001 MAXIMUM DAILY DISCHARGE POLLUTANT ML/MDLCone.Units Mass Units Cone.Units Mass Units FLUORANTHENE FLUORENE HEXACHLOROBENZENE HEXACHLOROETHANE ISOPHORONE NAPHTHALENE NITROBENZENE PHENANTHRENE PYRENE Use this space (or a separate sheet) to provide information on other base-neutral compounds requested by the permit wnter Use this space (or a separate sheet) to provide information on other pollutants (e g , pesticides) requested by the permit wnter EPA Form 3510-2A (Rev 1-99). Replaces EPA forms 7550-6 & 7550-22 Page 14 of 22 1.2.4- TRICHLOROBENZENE (Complete once for each outfall discharging effluent to waters of the United States.) AVERAGE DAILY DISCHARGE END OF PART D. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE Number of Samples ANALYTICAL METHOD N-NITROSODI- METHYLAMINE N-NITROSODI- PHENYLAMINE N-NITROSODI-N- PROPYLAMINE INDENO(1,2,3-CD) PYRENE HEXACHLORO­ BUTADIENE HEXACHLOROCYCLO- PENTADIENE SUPPLEMENTAL APPLICATION INFORMATION PART E. TOXICITY TESTING DATA E.1.Required Tests. Test number: Test number: Test number: Test Species & test method number Age at initiation of test Outfall number Dates sample collected Date test started Duration Manual title Edition number and year of publication Page number(s) Give the sample collection method(s) used. For multiple grab samples, indicate the number of grab samples used.c. 24-Hour composite Grab d.Indicate where the sample was taken in relation to disinfection. (Check all that apply for each Before disinfection After disinfection After dechlorination EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.Page 15 of 22 PERMIT ACTION REQUESTED: Standard Renewal RIVER BASIN: Roanoke FACILITY NAME AND PERMIT NUMBER: Roanoke River WWTP, NC0024201 Indicate the number of whole effluent toxicity tests conducted in the past four and one-half years. chronic acute required to have one under 40 CFR Part 403); or 3) POTWs required by the permitting authority to submit data for these parameters. ’ thes® retUl,S f™81 indude <luarter1y testin9 for a 12-month period within the past 1 year using multiple species (minimum of two Show no aOnnrhAriTh|U tS froT/four.t®s,f. Performed at least annually in the four and one-half years prior to the application, provided the results ’ 10 a^jtion. submit the results of any other whole effluent toxicity tests from the past four and one-half years. If a whole effluent toxicity test t^dtyr^luct^on evaluate 30(1 006 hal cted revealed toxicity' Provide anY information on the cause of the toxicity or any results of a • If you have already submitted any of the information requested in Part E, you need not submit it again. Rather, provide the information requested in question E.4 for previously submitted information. If EPA methods were not used, report the reasons for using alternate methods, it test summaries are available that contain all of the information requested below, they may be submitted in place of Part E. comptete Onit°rin9 d3ta 'S reqUired’ d° nOt comPlete Par1 E Refer to the Application Overview for directions on which other sections of the form to • Quarterly Ceriodaphnia WET results are on file with the Division. • Four second species toxicity tests are submitted as Attachment B to this NPDES Permit Application. E.2. Individual Test Data. Complete the following chart for each whole effluent toxicity test conducted in the last four and one-half years Allow one column per test (where each species constitutes a test). Copy this page if more than three tests are being reported. a. Test information. b Give toxicity test methods followed. RIVER BASIN: Roanoke Test number:Test number:Test number: Describe the point in the treatment process at which the sample was collected.e. Sample was collected: f. For each test, include whether the test was intended to assess chronic toxicity, acute toxicity, or both Chronic toxicity Acute toxicity g. Provide the type of test performed. Static Static-renewal Flow-through Source of dilution water. If laboratory water, specify type; if receiving water, specify source.h. Laboratory water Receiving water i. Type of dilution water. If salt water, specify "natural" or type of artificial sea salts or brine used. Fresh water Salt water Give the percentage effluent used for all concentrations in the test series.j- k. Parameters measured during the test. (State whether parameter meets test method specifications) pH Salinity Temperature Ammonia Dissolved oxygen I.Test Results. Acute: %%% LCso %95% C.l.% % Control percent survival %% % Other (describe) ERA Form 3510-2A (Rev 1-99). Replaces ERA forms 7550-6 & 7550-22 Page 16 of 22 PERMIT ACTION REQUESTED: Standard Renewal FACILITY NAME AND PERMIT NUMBER: Roanoke River WWTP, NC0024201 Percent survival in 100% effluent RIVER BASIN: Roanoke Chronic: NOEC %%% %%% Control percent survival %%% Other (describe) m. Quality Control/Quality Assurance. Is reference toxicant data available? ////// Other (describe) E.3. Toxicity Reduction Evaluation. Is the treatment works involved in a Toxicity Reduction Evaluation? Yes No If yes, describe: //Date submitted:(MM/DD/YYYY) Summary of results (see instructions) ERA Form 3510-2A (Rev 1-99). Replaces ERA forms 7550-6 & 7550-22 Page 17 of 22 PERMIT ACTION REQUESTED: Standard Renewal FACILITY NAME AND PERMIT NUMBER: Roanoke River WWTP, NC0024201 E.4. Summary of Submitted Biomonitoring Test Information. If you have submitted biomonitonng test information, or information regarding the cause of toxicity, within the past four and one-half years, provide the dates the information was submitted to the permitting authority and a summary of the results. Was reference toxicant test within acceptable bounds? END OF PART E. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE. What date was reference toxicant test run (MM/DD/YYYY)? IC25 FACILITY NAME AND PERMIT NUMBER:PERMIT ACTION REQUESTED:RIVER BASIN: Roanoke River WWTP, NC0024201 Standard Renewal Roanoke SUPPLEMENTAL APPLICATION INFORMATION PART F. INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES GENERAL INFORMATION: F.1.Pretreatment program. Does the treatment works have, or is subject to, an approved pretreatment program? S Yes No Number of non-categorical SIUs. a. Number of CIUs.1b. SIGNIFICANT INDUSTRIAL USER INFORMATION: F.3. Kennametal, Inc. Name: 100 Kennametal Road Mailing Address: Weldon, NC 27890 Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge.F.4. Machine tool accessory manufacturing F.5. Principal product(s):Tungsten carbide and ceramic cutting tool inserts Tungsten carbide and ceramic powdersRaw material(s): Flow Rate.F.6. a. intermittent)continuous or X C b. intermittent)continuous or N/Agpd(N/AN/A Pretreatment Standards. Indicate whether the SIU is subject to the following:F.7. NoEl YesLocal limitsa. El Yes NoCategorical pretreatment standardsb. If subject to categorical pretreatment standards, which category and subcategory? Page 18 of 22EPA Form 3510-2A (Rev 1-99). Replaces EPA forms 7550-6 & 7550-22. All treatment works receiving discharges from significant industrial users or which receive RCRA.CERCLA, or other remedial wastes must complete part F. F.2. Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (CIUs). Provide the number of each of the following types of industrial users that discharge to the treatment works. 7147 gpd Non-process wastewater flow rate. Indicate the average daily volume of non-process wastewater flow discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. Significant Industrial User information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU s discharge. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and provide the information requested for each SIU. F.8. N/A RCRA HAZARDOUS WASTE RECEIVED BY TRUCK, RAIL, OR DEDICATED PIPELINE: RCRA Waste. Does the treatment works receive or has it in the past three years received RCRA hazardous waste by truck, rail or dedicated pipe?F.9. S No (go to F. 12)□ Yes Waste transport. Method by which RCRA waste is received (check all that apply): N/AF.10. □ Dedicated Pipe□ Rail□ Truck UnitsAmount N/AN/AN/A N/A N/A N/AN/A S No F.13. N/A N/A F.15. Waste Treatment Is this waste treated (or will be treated) prior to entering the treatment works?a. 0 No□ Yes If yes, descnbe the treatment (provide information about the removal efficiency): N/A b. □ Intermittent□ Continuous N/A Page 19 of 22EPA Form 3510-2A (Rev 1-99). Replaces EPA forms 7550-6 & 7550-22. FACILITY NAME AND PERMIT NUMBER: Roanoke River WWTP, NC0024201 END OF PART F. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e g., upsets, interference) at the treatment works in the past three years? □ Yes 0 No If yes, describe each episode. Is the discharge (or will the discharge be) continuous or intermittent? If intermittent, describe discharge schedule. PERMIT ACTION REQUESTED: Standard Renewal RIVER BASIN: Roanoke □ Yes (complete F.13 through F.15.) Waste Origin. Describe the site and type of facility at which the CERCLA/RCRA/or other remedial waste originates (or is excepted to origniate in the next five years). F.14. Pollutants. List the hazardous constituents that are received (or are expected to be received). Include data on volume and concentration, if known. (Attach additional sheets if necessary.) CERCLA (SUPERFUND) WASTEWATER, RCRA REMEDIATION/CORRECTIVE ACTION WASTEWATER, AND OTHER REMEDIAL ACTIVITY WASTEWATER: F.12. Remediation Waste. Does the treatment works currently (or has it been notified that it will) receive waste from remedial activities? F.11. Waste Description. Give EPA hazardous waste number and amount (volume or mass, specify units). EPA Hazardous Waste Number RIVER BASIN: Roanoke SUPPLEMENTAL APPLICATION INFORMATION PART F. INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES GENERAL INFORMATION: Pretreatment program. Does the treatment works have, or is subject to, an approved pretreatment program?F.1. □ No□ Yes F.2. Number of non-categorical SIUs. a. 1Number of CIUs.b. SIGNIFICANT INDUSTRIAL USER INFORMATION: F.3. Reser's Fine Foods Name: 11251 Hwy 903 Mailing Address: Halifax. NC 27839 Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge.F.4. Food processing F.5. Cold salads, baked beans, meal saladsPrincipal product(s): Potatoes, pastas, cabbage, salad dressings Raw material(s): Flow Rate.F.S. a. intermittent)continuous or b. intermittent)N/A(N/A continuous or9PdN/A Pretreatment Standards. Indicate whether the SIU is subject to the following:F.7. E] Yes □ NoLocal limitsa. □ Yes 13 NoCategorical pretreatment standardsb. If subject to categorical pretreatment standards, which category and subcategory? Page 18 of 22EPA Form 3510-2A (Rev 1-99) Replaces EPA forms 7550-6 & 7550-22 FACILITY NAME AND PERMIT NUMBER: Roanoke River WWTP, NC0024201 All treatment works receiving discharges from significant Industrial users or which receive RCRA.CERCLA, or other remedial wastes must complete part F. Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (CIUs). Provide the number of each of the following types of industrial users that discharge to the treatment works. PERMIT ACTION REQUESTED: Standard Renewal 123 752 gpd (X Non-process wastewater flow rate. Indicate the average daily volume of non-process wastewater flow discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. one SIU discharges to the treatment works, copy questions F.S through F.S and Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU’s discharge Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. Supply the following information for each SIU. If more than provide the information requested for each SIU. F.8. N/A RCRA HAZARDOUS WASTE RECEIVED BY TRUCK, RAIL, OR DEDICATED PIPELINE: RCRA Waste. Does the treatment works receive or has it in the past three years received RCRA hazardous waste by truck, rail or dedicated pipe?F.9. S No (go to F. 12) Yes F.10. Waste transport Method by which RCRA waste is received (check all that apply): N/A Dedicated Pipe Rail Truck UnitsAmount N/AN/AN/A N/AN/A N/A N/AN/AN/A No N/A F.14. N/A F.15. Waste Treatment Is this waste ireated (or will be treated) prior to entering the treatment works?a. El No Yes If yes. describe the treatment (provide information about the removal efficiency): N/A b. Continuous N/A Page 19 of 22EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. FACILITY NAME AND PERMIT NUMBER: Roanoke River WWTP, NC0024201 END OF PART F. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE Pollutants. List the hazardous constituents that are received (or are expected to be received). Include data on volume and concentration, if known. (Attach additional sheets if necessary.) Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e g., upsets, interference) at the treatment works in the past three years? Yes No If yes, describe each episode. Is the discharge (or will the discharge be) continuous or intermittent? Intermittent If intermittent, describe discharge schedule. PERMIT ACTION REQUESTED: Standard Renewal RIVER BASIN: Roanoke Yes (complete F.13 through F.15.) F.13. Waste Origin. Describe the site and type of facility at which the CERCLA/RCRA/or other remedial waste originates (or is excepted to origniate in the next five years) CERCLA (SUPERFUND) WASTEWATER, RCRA REMEDIATION/CORRECTIVE ACTION WASTEWATER, AND OTHER REMEDIAL ACTIVITY WASTEWATER: F.12. Remediation Waste. Does the treatment works currently (or has it been notified that it will) receive waste from remedial activities? F.11. Waste Description. Give EPA hazardous waste number and amount (volume or mass, specify units). EPA Hazardous Waste Number FACILITY NAME AND PERMIT NUMBER:RIVER BASIN: Roanoke River WWTP. NC0024201 Roanoke SUPPLEMENTAL APPLICATION INFORMATION PART F. INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES GENERAL INFORMATION: Pretreatmont program. Does the treatment works have, or is subject to, an approved pretreatment program?F.l. NoE Yes Number of non-categorical SIUs.2 a. Number of CIUs.b. SIGNIFICANT INDUSTRIAL USER INFORMATION: F.3. Rosemary Power Station Name: 120 West 12'n Street Mailing Address: Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge.F.4. Power generation F.5. Principal product(s):Electricity Natural gas. No 2 fuel oil, and waterRaw material(s): F.6.Flow Rate. a. intermittent)continuous or X 18765 C b. intermittent)continuous or N/Agpd(N/AN/A Pretreatment Standards. Indicate whether the SIU is subject to the following:F.7. 0 Yes NoLocal limitsa. Yes 0 NoCategorical pretreatment standardsb. If subject to categorical pretreatment standards, which category and subcategory? Page 18 of 22EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. PERMIT ACTION REQUESTED: Standard Renewal All treatment works receiving discharges from significant Industrial users or which receive RCRA.CERCLA, or other remedial wastes must complete part F. F.2. Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (CIUs). Provide the number of each of the following types of industrial users that discharge to the treatment works. gpd Non-process wastewater flow rate. Indicate the average daily volume of non-process wastewater flow discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU’s discharge. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. Supply the following Information for each SIU. If more than one SIU discharge* to the treatment works, copy question* F.3 through F.8 and provide the Information requested for each SIU. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Roanoke Rapids, NC 27870 F.8. N/A F.10. F.11. Units N/A N/A N/A N/A N/A N/A a. b. If intermittent, describe discharge schedule. N/A L EPA Form 3510-2A (Rev 1-99).Rep.’aces EPA forms 7550-6 & 7550-22 Page 19 of 22 RIVER BASIN: Roanoke PERMIT ACTION REQUESTED: Standard Renewal waste is received (check all that apply). N/A Dedicated Pipe lous waste number and amount (volume or mass, specify units). Amount F.15. Waste Treatment IS this waste treated (or will be treated) prior to entering the treatment works? Yes (3 No If yes. describe the treatment (provide information about the removal efficiency): N/A Yes S No (go to F 12) a2a,d0US was,e b* fell or dedicated pipe? Waste transport Method by which RCRA Truck Q Raj| Waste Description. Give EPA hazard. EPA Hazardous Waste Number N/A TTO THE — or contributed to any problems (e g., Is the discharge (or will the discharge be) continuous or intermittent? Continuous Q intermittent FACILITY NAME AND PERwFFMUMBER: Roanoke River WWTP, NC0024201 hy «» SIU- Has the SIU caused Yes ra No i* If yes, describe each episode. sen notified that it will) receive waste from remedial activities? known. (Attach additional sheet^neiTsarJ1)31 reCe,Ved (or are expected to be received). Include data on volume and concentration, if N/A F.iz ^emodlatlon WastoTDoesIhekeatrnentwork7currentiy^orhas^tb& Yes (complete F.13 through F.15.) No N/A G.1. c. species potentially affected by CSOs. G.2. e. a. b.Location (City or town, if applicable) (Zip Code) (County) (State) (Latitude) (Longitude) c. ft. d. ft.e. ! J CSC frequency b. hours (□ actual or approx.) Page 20 of 22 ---------------------- -------------events (□ actual or approx.) Give the average duration per CSO event. PERMIT ACTION REQUESTED: Standard Renewal c. d. RIVER BASIN: Roanoke a. b. Give the number of CSO events in the last year FACILITY NAME AND PERMIT NUMBER: ~ ------ Roanoke River WWTP. NC0024201 SUPPLEMENTAL APPLICATION INFORMATION A Form 3510-2A (Rev. 1-99). Replaces ERA forms 7550-6 & 7550-22 System Map. Provide a. b. Distance from shore (if applicable) Depth below surface (if applicable) Which of the following were monitored during the last year7r this CSO? □ Rainfall q CSO pollutant concentrations CSO flow volume D Receiving water quality f- How many storm events were monitored during the last year? G.4. CSO Events. N/A p A RTG. COMBIN E D S E WE RSYSTEMs --------------------- --------=--------------- -- ---------------------- — ----------- outstanding natural r^X watered CS°S (e 9 ' beaCheS’ drinkin9 water supplies, shellfish beds, sensitive aquatic ecosystems, and Waters that support threatened and endangered Includes the rollawing ^XX^N/A8'^maP PraVided* “ 3 Separa,e *•*<>■ «W> “mbined sewer collection system that Location of major sewer trunk lines, both combined and separate sanitary Locations of points where separate sanitary sewers feed into the combined sewer system Locations of in-line and off-line storage structures. Locations of flow-regulating devices. Locations of pump stations. OUTFALLS? G.3. Description of Outfall. N/A ---------- ------------------------------------------------------- ------ Outfall number c. d. G.5.Description of Receiving Waters. N/A Name of receiving water:a. b. c. Page 21 of 22 RIVER BASIN: Roanoke _____» PERMIT ACTION REQUESTED: Standard Renewal EPA Form 3510-2A (Rev. 1-99). Replaces ERA forms 7550-6 & 7550-22. FACILITY NAME AND PERMIT NUMBER: ’ Roanoke River WWTP. NC0024201 Give the average volume per OSO event. —------------------million gallons (□ actual or approx.) Give the minimum rainfall that caused a OSO event in the last year ----------Inches of rainfall Name of watershed/river/stream system: United State Soil Conservation Service 14-digit watershed code (if known): Name of State Management/River Basin. United States Geological Survey Miglt hydrologic cataloging unit code (if known): G.6. CSO Operations. N/A “e Attached Figures Topographic Map Plant Site Plan Plant Flow Schematic Process Narrative Attachments Attachment A: Attachment B: NPDES FORM 2A Additional Information Priority Pollutant Scan Analysis Second Species Toxicity Test Results Attachment C: Biosolids Program Description A ) Add,t,onal information, if proved, wiil appear on the foiiowmg pages. Attached Figures NPDES FORM 2A Additional Information -J Roanoke Rapids Sanitary District - NC0024201 Not to Scale USGS Quad Name: Weldon Receiving Stream: Roanoke River Stream Class: C Subbasin: Roanoke - 030208 Lat: 36°26’10” Long: 77°36’04” Facility Location I ? ,Weldoii, Outfall 001 stow as Mft OUIfKl 3 siuoct SUTfUMIW ORMWl oaiew mtw kos suFWurmi SIHRMTMIo o LEGEND PLAN I HOiV SCHEMATIC >«>W O-IWOH WIPWHEHT CftWCH &ARCADIS DGtSTEO SLUDGE OaSTFD SIUKE VM41A OAR SCWfN AERAION TANKS ROANOKE RAPIDS SANITARY DISTRICT WASTEWATER TREATMENT PLANT □OCKOYOTTE CREEK OVTFAll CMRSiOl «JX DMSSJON TO ROANOKE OVfPflOW TO ROANOKE RMH 2 FR UART AHAEROEC DCrSTERS PHttiARv ClAWfRS :rcklwg MTEW ■US PUMP swot EML CLARTfRS ClSCEiARGl TO RfJANW’ RfVER GMT CHAMBERS 1 SaCOMJARY AMAERCW DCESTER DfSCMRGE TO ROANOKE fMR J s n h h 1 « I ftooo “’.IIP SIATKW 1 “WS PITER Kcscjunx ?JUP SIAIOH 3 PVUPS m< iifiufnT w surw < .•".'UPS I S1A911ZATCN FACILITY | KlUEW EOUMIZATION [ CIILCRNAIIQN/ | ' iXCHOftWiON | •AS SRAWTr | THICKENERS I WAS HJMP STATON ’ POURS I PPiMAffr SLUDGE I I PUMP STATION | Wri.UEMT PUMP STATION 4 PIMPS UHU (WCAIVIi I MOEMHC I Q oasrfu SWWWAMI i O ORAJMtt FROM DWNC BEDS •> Process Narrative The solids handling process description is provided in Attachment C. Influent flow enters the Roanoke River Waste Treatment Plant via two outfalls: the Chockoyotte Creek Outfall and the Roanoke River Outfall. Both outfalls combine in a collection box prior to mechamcal screening and grit removal. Influent flow may be routed to influent equalization when necessary. The influent wastewater is lifted via an influent pump station to primary clarifiers. Primary clarified effluent gravity flows to trickling filters. Trickling filter effluent is pumped to aeration basins for further secondary treatment. The mixed liquor then flows to final clarifiers. Clarified effluent is then chlorinated and dechlorinated. Effluent flow is measured prior to discharge to the Roanoke River. An effluent flood pump station is used to pump to the Roanoke River when flow by gravity may not be achieved. NPDES FORM 2A Additional Information Attachment A: Priority Pollutant Scan Analysis Scan Sanitary District Page 1 _1 1 <50 <3 50 3 Permit No. _NC002 Outfall__001 Sample Result Month _July. Year _2007 Quantitation Level Units of Measurement 1 1 1 1 "T i i i i T~ T" i i i i i i i i i T i i i T~ T~ Composite Composite Composite Composite Composite Composite Composite Composite Composite Composite Composite Composite Composite Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Sample Type Composite Grab Composite Composite Composite Composite Composite Grab Grab EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 Analytical Method ~EPA 350,2~ EPA 360,2 EPA 300,0 ~EPA 351,3 ' EPA 365,3 ' EPA 160,1 EPA 130,2 ~ EPA 330,5 EPA 1664 ug/L ug/L llg/E ug/L ug/l ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L mg/L m8/L mg/L mg/L mg/L mg/L mg CaCO3/L mg/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/1 ug/L ug/L ug/L ug/L ug/L ug/L ug/L Number of samples 1 1 ~ 1 1 1 1 ~ 1 1 1 100 100 5.0 5,0 5,0 5,0 5.0 10 10 5.0 5.0 5.0 5.0 5.0 0.2 2 2 2 10 0.0005 5 3 5 50 2 5 5 0.20 n/a 0,300 1.00 0.250 10 1 15 5 3,76 4,2 12,281 8,99 1,61 218 48 <15 <5 <100 <100 <5,0 2,4 <5.0 <5,0 3 <10 <10 <5.0 <5.0 <5.0 <5.0 <5.0 <0,2 <2 <2 11 <10 0.0165 <5 <3 <5 <50 53 7 10 Parameter Ammonia (as N) Dissolved oxygen Nitrate/Nitrite ~ Total Kjeldahl nitrogen Total Phosphorus Total dissolved solids Hardness Chlorine (total residual, TRC) Oil and grease Metals (total recoverable). Antimony Arsenic ^B)i Beryllium Cadmium Chromium [Copper Lead Mercury ~ Nickel " Selenium Silver Thallium Zinc Cyanide Total phenolic compounds Volatile organic compounds Acrolein ~ Acrylonitrile Benzene Bromoform Carbon tetrachloride ’ Chlorobenzene Chlorodibromomethane Chloroethane 2-chloroethylvinyl ether Chloroform Dichlorobromome thane 1.1- dichloroethane 1.2- dichloroethane Trans-1,2-dichloroethylene Form - DMR- PPA-1 _____ cyanide and total phenols ' ~EPA 200,7 | EPA 206,2 ’ EPA 200,7 ~EPA 200,7 ~ EPA 200,7 ~ EPA 200,7 EPA 200,7 ~ EPA 1631E~ EPA 200,7 ~ EPA 270.2 ~ EPA 200,7 ~ EPA 200,7 ~ EPA 200.7 ~ EPA 335,2 ~ EPA 420,1 ~ Faculty Name: Roanoke Rapids _uuuyu,stnct 0Rc Date of sampling: 07/10/2007 —A-Gregg Camp___ Analytical Laboratory: Microbac Labs / Southern Testing Divis^nCTRL^S^^p4884- _______ 8 division olRL#7624 and RRSD-WWTP NC70 Annual Monitoring and Pofl^ c Scan ! Parameter Sample Result Month_July. Year 2007 Number of samples Units of Measurement EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624~ EPA 624 ' EPA 624 ~ EPA 624 EPA 624 EPA 624 EPA 624 10 10 10 50 10 10 10 10 10 10 10 10 10 10 10 10 10 20 10 10 10 50 50 10 50 50 10 10 <20 <10 <10 <10 <50 <50 <10 <50 <50 <10 <10 ug/L ug/L ug/L ug/L ug/L ug/l ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ____1 ____1 ____1 ____1_ ____1 ____1 ____1 ___1_ ___1 ___1 ___1_ ___1_ 1 ___1 ___1_ 1 ___1 Page 2 1 1 1 1 1 1 1 1 T" i~ i i i i i i i i i i i i T~ i 5,0 5.0 10 5.0 10 10 10 5.0 5.0 5.0 5.0 5.0 5.0 10 <10 <10 <10 <50 <10 <10 1.7/<1.6* <10 <10 <10 <10 <10 3.7/2.2* <10 <10 <10 <10 <5.0 <5,0 <10 <5.0 <10 <10 <10 <5.0 <5.0 <5.0 <5.0 <5.0 <5,0 <10 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Sample _____ _____________Type Volatile organic compounds (Cont.) 1.1- dichloroethylene 1.2- dichloropropane 1.3- dichloropropylene Ethylbenzene Methyl bromide Methyl chloride Methylene chloride 1,1,2,2-tetrachloroeth an e Tetrachloroethylene Toluene 1.1.1- trichloroethane 1.1.2- trichloroethane Trichloroethylene Vinyl chloride Acid-extractable compounds P-chloro-m-creso 2-chlorophenol 2.4- dichlorophenol 2.4- dimethylphenol 4.6- dinitro-o-cresol 2.4- dinitrophenol 2-nitrophenol 4-nitrophenol Pentachlorophenol Phenol 2.4.6- trichlor op he no 1 Base-neutral compounds Acenaphthene Acenaphthylene Anthracene Benzidine Benzo(a)anthracene Be nzo(a) pyrene 3,4 benzofluoranthene Benzo(ghi)perylene Benzo(k)fluoranthene Bis (2-chloroethoxy) methane Bis (2-chloroethyl) ether Bis (2-chloroisopropyl) ether Bis (2-ethylhexyl) phthalate 4-bromophenyl phenyl ether Butyl benzyl phthalate 2-chloronaphthalene 4-chlorophenyl phenyl ether ” Form - DMR- PPA-1 Quantitation I Level a/ Permit No. _NC0024201_ Outfall 001 Analytical Method Parameter Form - DMR- PPA-1 Signature Page 3 Permit No. _NC002 Outfall 001 Quantitation Level Sample Result Number of samples Sample Type Month July. Year,2007_____ Units of Measurement Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab > EPA 625 » EPA 625 EPA 625 EPA 625 _ EPA 625 EPA 625 EPA 625 EPA 625 __ EPA 625 __ EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 __ EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 __ EPA 625 ~~ EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 analyzed by the The sample 10 10 10 10 10 10 10 50 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 lo 10 10 To ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/l ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L <10 <10 2.1/<1,1* <10 <10 <10 <10 <50 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 contract laboratory' was i Both sets of data have been reported where differing sample data 1 1 1 1 1 1 1 ~T ~T i i i i i T" i T~ ~T~ T" T" T~ T" T~ i T~ T" i T ______F~ on 7/18/07. The Laboratory re-analyzed on 7/ 19/07, out of holding i resulted. __I Base-neutral compounds (cont.) Chrysene Di-n-butyl phthalate Di-n-octyl phthalate Dibenzo(a,h)anthracene 1.2- dichlorobenzene 1.3- dichlorobenzene 1.4- dichlorobenzene 3.3- dichlorobenzidine Diethyl phthalate Dimethyl phthalate 2.4- dinitrotoluene 2,6-dinitro toluene 1,2-diphenylhyd razine Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclo-pentad i en e Hexachloroethane Indeno( 1,2,3-cd)pyrene Isophorone Naphthalene Nitrobenzene N-nitrosodi-n-propylamine N-nitrosodimethylamine N-nitrosodiphenylamine Phenanthrene Pyrene 1,2,4,-trichlorobenzene *Semi-volatile organics compounds were Control Sample (LCS) failed to meet the QC limits, but with passing QC. Authorized Representative name certify under penalty of law that this document and all attachments were prepared under my direction and supervision m accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons that manage the system, or those persons directly responsible for gathering the information the mformation submitted is, to the best of my knowledge and belief, true, accurate and complete I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Annual Monitoring and Pol^^ t Scan Analytical I Method Parameter 1 1 1 Grab Form - DMR- PPA-1 Page 1 Permit No. _NC002 Outfall _001_. Analytical Method Sample Result Number of samples Quantitation Level Month _October_ Year__2008 Units of Measurement 1 7 i 7 7 7 SM 4500 SM 4500 EPA 300.0 SM 4500 EPA 365,3 SM 2540C SM2340C SM 4500 _______________________EPA 1664A Metals (total recoverable), cyanide and total phenols Composite Composite Composite Composite Composite Composite Composite Composite Composite Composite Composite Composite Composite Grab Grab Sample Type Composite Grab Composite Composite Composite Composite Composite Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 " EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 SM 3113B SM 3113B EPA 200.7 EPA 200.7 EPA 200.7 EPA 200,7 EPA 200.7 EPA 1631E EPA 200.7 SM 3113B EPA 200.7 EPA 279.2 EPA 200.7 SM 4500 EPA 420.1 0.25 0.6 0.2 2 2 2 10 0.0005 5 0.6 5 0.2 2 5 5 0.20 N/A 1.3 1.00 0.2 10 2.0 13.5 5 14,9 3.46 1.44 256 46 <13.5 <5 mg/L mg/L mg/L mg/L mg/L mg/L mg CaCO3/L ug/1 mg/L ug/L ug/L ug/L ug/L Ug/L ug/L ug/L Ug/L Ug/L ug/L ug/l ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/1 ug/L ug/L ug/L ug/L ug/L ug/L ug/L 1 1 1 T 1 T 1 1 T i 7" i i 7" i "7 "7 1 i 1 i i i T T~ i 7" i i 100 100 5.0 5.0 5.0 5.0 5.0 10 10 5.0 5.0 5.0 5.0 5.0 1.61 5.7 Ammonia (as N) Dissolved oxygen Nitrate/Nitrite Total Kjeldahl nitrogen Total Phosphorus Total dissolved solids Hardness Chlorine (total residual, TRC) Oil and grease <100 <100 <5.0 <5.0 <5.0 <5.0 1.1 <10 <10 2.6 2.3 <5.0 <5.0 <5.0 <0.25 0.9 <0.2 <2 2 11 <10 0.0173 <5 1.1 <5 0.25 39 <5 <5 Antimony Arsenic Beryllium Cadmium Chromium Copper Lead Mercury Nickel Selenium Silver Thallium Zinc Cyanide Total phenolic compounds Volatile organic compounds Acrolein Acrylonitrile Benzene Bromoform Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane 2-chloroethylvinyl ether Chloroform Dichlorobromomethane 1,1 -dichloroethane 1,2-dichloroe thane Trans-1,2-dichloroethylene Annual Monitoring and Pol^^ ; Scan Facility Name: Roanoke Rapids Sanitary District OrC: _a Gregg Camp. Date of sampling: 10/14/08 Phone: ____252-536-4884____ Analytical Laboratory: Microbac Labs / Southern Testing Division STRL#7624 and RRSD-WWTP NC 70 compounds Form - OMR- PPA-1 Page 2 Permit No. _NCOO Outfall _001_ Analytical Method Quantitation Level Sample Result Number of samples Units of Measurement Sample Type Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 10 10 10 50 10 10 10 10 10 10 10 10 10 10 10 10 To~ 20 10 10 10 50 50 10 50 50 10 10 5.0 5.0 10 5.0 10 10 10 5.0 5.0 5.0 5.0 5.0 5.0 10 <20 <10 <10 <10 <50 <50 <10 <50 <50 <10 <10 <5.0 <5.0 <10 <5.0 <10 <10 <10 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <10 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 1 1 1 1 1 T i "T" 1 T" i T" 7" i T~ T~ 1 i i i i i i i T i i i 1 1 1 i i i i T T i i T~ i <10 <10 <10 <50 <10 <10 <10 <10 <10 <10 <10 <10 4.9 <10 <10 <10 <10 EPA 624 |— EPA 624 ~~ EPA 624 EPA 624 ~ EPA 624 ~ EPA 624 ~~ EPA 624 ~ EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 Parameter Volatile organic compounds (Cont.) 1 ■ 1 -dichloroethylene 1.2- dichloropropane 1 >3-dichloropropylene Ethylbenzene Methyl bromide Methyl chloride Methylene chloride 1.1.2.2- tetrachloroethane Tetrachloroethylene Toluene 1,1,1 -trichloroethane 1.1.2- trichloroethane Trichloroethylene Vinyl chloride Acid-extractable P-chloro-m-creso 2-chlorophenol 2.4- dichlorophenol 2.4- dimethylphenol 4.6- dinitro-o-cresol 2.4- dinitrophenol 2-nitrophenol 4-nitrophenol Pentachlorophenol Phenol 2.4.6- trichlorophenol Base-neutral compounds Acenaphthene Acenaphthylene Anthracene Benzidine Benzo(a)anthracene Benzo(a) pyrene 3,4 benzofluoranthene Benzo(ghi)perylene Bcnzo(k)fluoranthene Bis (2-chloroethoxy) methane Bis (2-chloroethyl) ether Bis (2-chloroisopropyl) ether Bis (2-ethylhexyl) phthalate 4-bromophenyl phenyl ether Butyl benzyl phthalate 2 chloronaphthalene 4-chlorophenyl phenyl ether Scan Month _October_ _______ Year 2008. Signature Form - DMR- PPA-1 Page 3 Permit No. _NC00 J Outfall 001 Quantitation Level Sample Result Number of samples Sample Type Analytical Method Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab EPA 625 EPA 625 ~ EPA 625 ~~ EPA 625 ~ EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 ’ EPA 625 EPA 625 EPA 625 EPA 625 __10 ~__10 __10 __10_ 10 10 10 50 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10__ 10 10__ 10__ 10 <10 <10 <10 <10 <10 <10 <10 <50 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 1.2 <10 ug/L ug/L ug/L Ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ___1 ___1_ 1 __1_ __1 __1 __1 __1_ 1 1 1 1 1 1 1 1 1 1 1 i: i i i i _i 1 1 1 i a? Parameter | Base-neutral compounds (cont.) Chrysene Di-n-butyl phthalate Di-n-octyl phthalate ~ Dibenzo(a,h)anthracene ~ 1.2- dichlorobenzene 1.3- dichlorobenzene 1.4- dichloro benzene 3.3- dichlorobenzidine Diethyl phthalate Dimethyl phthalate 2.4- dinitrotoluene 2,6-dinitrotoluene 1,2-diphenylhydrazine Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclo-pentadiene Hexachloroethane Indeno( 1,2,3-cd)pyrene Isophorone Naphthalene Nitrobenzene N-nitrosodi-n-pr o py 1 a m i n e N-nitrosodimethylamine N-nitrosodiphenyla mine Phenanthrene Pyrene 1.2,4,-trichlorobenzene ' gather and evaluate the information subnX Xd qUaliried PCrSOnnel ProPerlv Authorized Representative name Annual Monitoring and Po^l Scan Month .October__ Year __2008 Units of Measurement : ScanAnnual Monitoring and Poll [Trans-1,2-dichloroethyle n e Grab EPA 624 5 <5 ug/1 1 Form - DMR- PPA-1 Page 1 Month_January_____ Year____2009____ Sample Result 1 T T i T T T T T T~ F EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 "EPA 624 ~EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Composite Composite Composite Composite Composite Composite Composite Composite Composite Composite Composite Composite Composite Grab Grab SM 3113B SM 3113B EPA 200.7 EPA 200.7 EPA 200.7 EPA 200,7 EPA 200.7 EPA 163 IE EPA 200.7 SM 3113B EPA 200.7 EPA 279.2 EPA 200.7 SM 4500 EPA 420.1 20 10 1 2 5 2 10 0.0005 10 10 50 50 2 5 5 100 100 5 5 5 5 5 10 10 5 5 5 5 0.2 N/A 1.3 0.5 0.2 10 2 11.5 5 and RRSD-WWTP NC70 Units of Measurement mg/l mg/l mg/1 mg/l mg/l mg/l mg/l ug/1 mg/l ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 Ug/1 Number of samples 1 1 1 1 1 1 1 1 1 1 T T T T T i T i i T~ T" T~ i Parameter Ammonia (as N) Dissolved oxygen Nitrate/Nitrite Total Kjeldahl nitrogen Total Phosphorus Total dissolved solids Hardness Chlorine (total residual, TRC) Oil and grease Analytical Method ~SM 4500~ SM 4500 EPA 300.0 SM 4500 ~ EPA 365.3 SM 2540C SM 2340C HACH 10014| ' EPA 1664A <20 <10 <1 <2 <5 8.5 <10 0.00656 <10 <10 <50 <50 39 <5 <5 0.46 5.4 12 <0.5 1.26 391 62 <11.5 <5 ORC _A. Gregg Camp______ Phone 252-536-4884___ Microbac Labs/Southern Testing Division STRL#9752 Sample Type Composite Grab Composite Composite Composite Composite Composite Grab ________________Grab Metals (total recoverable), cyanide and total phennlw Antimony Arsenic ~ Beryllium Cadmium Chromium Copper Lead Mercury Nickel Selenium Silver Thallium Zinc Cyanide Total phenolic compounds Volatile organic compounds Acrolein Acrylonitrile Benzene Bromoform Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane 2-chloroethylvinyl ether Chloroform Dichlorobromomethane 1,1 -dichloroethane 1,2-dichloroe thane <100 <100 <5 <5 <5 <5 <5 <10 <10 <5 <5 <5 <5 Facility Name _Roanoke Rapids Sanitary District Date of sampling: 1/13/2009 Analytical Laboratory_ W) Permit No. _NC002420I_ Outfall__001__ antitation Level Annual Monitoring and Pol^^^ t Scan Parameter 1 _____1 Page 2 Month__January_____ Year_____2009_____ Analytical Method Quantitation Level Sample Result Number of samples Units of Measurement --------------- ------- EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/I ug/1 ug/1 ug/1 Ug/1 1 ~T 1 1 1 T T T i i i i Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 10 10 10 50 10 10 10 10 10 10 10 10 10 10 10 10 10 20 10 10 10 50 10 10 50 50 10 10 5 5 5 5 10 10 5 5 5 5 5 5 5 10 <10 <10 <10 <50 <10 <10 <10 <10 <10 <10 <10 <10 1.9 <10 <10 <10 <10 <20 <10 <10 <10 <50 <10 <10 <50 <50 <10 <10 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 Ug/1 ug/1 Ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 Ug/1 ug/1 ug/1 ug/1 Ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 Ug/1 ug/1 ug/1 ug/1 1 2? 1 ~T T 1 T T T T~ T~ T~ T~ T"r~ 1 T T T 1 T T T T T~ <5 <5 <5 <5 <10 <10 <10 <5 <5 <5 <5 <5 <5 <10 Permit No. _NC002^^1_ Outfall 00 I_ Sample ___ ________________Type Volatile organic compounds (Cont.) 1,1 -dichloroe thy len e 1.2- dichloropropane 1.3- dichloropropylene Ethylbenzene Methyl bromide Methyl chloride Methylene chloride ' 1.1.2.2- tetrachloroethane Tetrachloroethylene Toluene 1,1,1 -trichloroethane 1.1.2- trichloroe than e T richloroethylene Vinyl chloride Acid-extractable compounds P-chloro-m-creso 2-chlorophenol 2.4- dichlorophenol 2.4- dimethylphenol 4.6- dinitro-o-cresol 2.4- dinitrophenol 2-nitrophenol 4-nitrophenol Pentachlorophenol Phenol 2.4.6- trichlorophenol Base-neutral compounds Acenaphthene Acenaphthylene Anthracene Benzidine Benzo(a)anthracene Benzo(a)pyrene 3,4 benzofluoranthene Benzo(ghi)perylene Benzo(k)fluoranthene Bis (2-chloroethoxy) methane Bis (2-chloroethyl) ether Bis (2-chloroisopropyl) ether Bis (2-ethylhexyl) phthalate 4-bromophenyl phenyl ether Butyl benzyl phthalate 2-chloronaphth a le n e 4-chlorophenyl phenyl ether Form - DMR- PPA-1 ScanAnnual Monitoring and Poll Parameter Signature Form - DMR- PPA-1 Date Page 3 Quantitation Level Sample Result Units of Measurement Number of samples Analytical Method Month__January Year______2009 Sample Type Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab EPA 625 EPA 625 P EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 10 10 10 10 10 10 10 50 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 Toi 10 10 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 Ug/1 __1 1 F r :i :i i i ~T ~T ~T~ i i T~ ~T~ i i i T~ T~ T T T T T 1 ~ I <10 <10 <10 <10 <10 <10 <10 <50 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 1.2 <10 Permit No. _NC0024^^ Outfall___001_ Base-neutral compounds (cont.) Chrysene Di-n-butyl phthalate ~ Di-n-octyl phthalate ~ Dibenzo(a,h)anthracene ~ 1.2- dichloro benzene 1.3- dichlorobenzene — 1.4- dichlorobenzene 3.3- dichlorobenzid ine Diethyl phthalate Dimethyl phthalate 2.4- dinitrotoluene 2,6-dinitrotoluene 1,2-diphenylhydrazine Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclo-pentadiene Hexachloroethane Indeno( 1,2,3-cd)pyrene Isophorone Naphthalene Nitrobenzene N-nitrosodi-n - propylamine N-nitrosodimethylamine N-nitrosodiphenylamine Phenanthrene Pyrene 11,2,4,-trichlorobenzene Authorized Representative name mformanon submxtted is , to the best of my knowledge and belief, true, accurate and complete I am aware hat there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Form - DMR- PPA-1 Page 1 Permit No. _NCOO Outfall 001_ units oi Measurement Month __June_ Year___2010. VUUDLiLation —; Level oainpie Result EPA 200.8 ' SM3113B' EPA 200.8~ SM3U3B SM3113B EPA 200,8 SM3113B EPA 1631 EPA 200.8 SM3113B SM3113B EPA 200,8 SM3113B SM4500CN EPA420.1 Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab oampie Type Composite Grab Composite Composite Composite Composite Composite Grab Grab EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 snuiyiicai Method ~SM4500NH3' SM4500-QG~ EPA 300 SM4500N-org ~SM4500PF~ SM2540C SM2340C Hack 10014 EPA 1664 0.01 0.01 0.001 0.001 0.001 0.001 0.001 0.002 0.002 0.001 0.001 0.001 0.001 b.ooi 0.006 0.002 0.001 0.002 0.002 0.01 0.001 0.0005 0.01 0.002 0.001 0.005 0.01 0.005 0.001 <0.01 <0.01 <0.001 <0.001 <0.001 <0.001 <0.001 <0.002 <0.002 <0.001 <0.001 <0.001 <0.001 <0.001 mg/l mg/1 mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l ng/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l ug/1 mg/l uinoer oi samples i i i i i i ir i i “T i i 1 i T i T T T“ T~ T" i- i i i "T i i i T" i i i T“ i T~ i o.i NA 0.02/0.03 0.01 0.05 5 1 7 5 <0.006 <0.002 <0.001 <0.002 <0.002 0.01 <0.001 0.0398 <0.010 <0.002 <0.001 <0.005 0.045 <0.005 <0.0100 3.45 5.9 8.27 6.51 2.4 247 56.2 <7 <5.0 Parameter Ammonia (as N) Dissolved oxygen Nitrate/Nitrite Total Kjeldahl nitrogen Total Phosphorus Total dissolved solids Hardness Chlorine (total residual, TRC) Oil and grease Metals (total recover^bUTcyanlde and total phenes' Composite Composite Composite Composite Composite Composite Composite Composite Composite Composite Composite Composite Composite Grab Grab Antimony Arsenic Beryllium Cadmium Chromium Copper Lead Mercury Nickel Selenium Silver Thallium Zinc ' Cyanide Total phenolic compounds Volatile organic compounds Acrolein Acrylonitrile Benzene Bromoform Carbon tetrachloride Chlorobenzene Chlorodi bromomethane Chloroethane 2-chloroethylvinyl ether Chloroform Dichlorobromomethane 1.1- dichloroethane 1.2- dichloroe thane Trans-1,2-dichloroethylene Facility Name .Roanoke Rapids Sanitary District ORC A e Date of sampling April 15, 2010 - ■ Gregg Camp---- Ana^cal laboratory _Microbac'^7^93 and RRSDTOncvo252’536'4884 Parameter Form - DMR- PPA-1 Page 2 Permit No. _NC002 Outfall___001__ Analytical Method Quantitation Level Sample Result Month __June_ Year___2010. Units of Measurement Number of samples Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 0.0098 0.0098 0.0098 0.049 0.0098 0.0098 0.0098 0.0098 0.0098 0.0098 0.0098 "0.0098 0.0098 0.0098 0.0098 0.0098 0.0098 0.02 0.0098 0.0098 0.098 0.049 0.049 0.0098 0.049 0.049 0.0098 0.0098 0.001 0.001 0.002 0.001 0.002 0.002 0.002 0.001 0.001 0.001 0.001 0.001 0.001 0.002 <0.001 <0.001 <0.002 <0.001 <0.002 <0.002 <0.002 <0.001 <0.001 0.0046 <0.001 <0.001 <0.001 <0.002 mg/1 mg/l mg/1 mg/I mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 T 1 T T i i T T T i T i i T i i i i T i i i F i i 1 i i i i i T T T i i T“ <0.0098 <0.0098 <0.0098 <0.049 <0.0098 <0.0098 <0.0098 <0.0098 <0.0098 ”<0.0098 <0.0098 <0.0098 <0.0098 <0.0098 <0.0098 <0.0098 <0.0098 <0.02 <0.0098 <0.0098 <0.0098 —<0.049 <0.049 <0.0098 <0.049 ~<0.049 <0.0098 <0.0098 Sample _________________Type Volatile organic compounds (Cont.) 1,1 -dichloroethylen e 1.2- dichloropropane 1 >3-dichloropropylene Ethylbenzene Methyl bromide Methyl chloride Methylene chloride 1.1.2.2- tetrachloroethane Tetrachloroethylene Toluene 1,1,1 -trichloroethane 1.1.2- trichloroe thane Trichloroethylene Vinyl chloride Acid-extractable compounds P-chloro-m-creso 2-chlorophenol 2.4- dichloroph enol 2.4- dimethylphenol 4.6- dinitro-o-cresol 2.4- dinitroph enol 2-nitrophenol 4-nitrophenol Pentachlorophenol Phenol 2.4.6- trichlorophenol Base-neutral compounds Acenaphthene Acenaphthylene Anthracene Benzidine Benzo(a)anthracene Benzo(a)pyrene 3,4 benzofluoranthene Benzo(ghi)perylene Benzo(k)fluoran thene Bis (2-chloroethoxy) methane Bis (2-chloroethyl) ether Bis (2-chloroisopropyl) ether Bis (2-ethylhexyl) phthalate 4-bromophenyl phenyl ether Butyl benzyl phthalate 2-chloronaphthalene 4-chlorophenyl phenyl ether annual monitoring ana rouutant scan Annual monitoring ana ro at scan ■ Signature Form - DMR- PPA-1 Page 3 * Permit No. _NCOO Outfall___001__ Analytical Method Quantitation Level Sample Result Number of samples Sample Type Units of Measurement Month __June_ Year___2010. Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 " EPA 625 0.0098 0.0098 0.0098 0.0098 0.0098 0.0098 0.0098 0.049 0.0098 0.0098 0.0098 0.0098 0.0098 0.0098 0.0098 0.0098 0.0098 0.0098 0.0098 0.0098 0.0098 0.0098 0.0098 0.0098 0.0098 0.0098 0.0098 0.0098 0.0098 <0.0098 <0.0098 <0.0098 <0.0098 <0.0098 <0.0098 <0.0098 <0.049 <0.0098 I <0.0098 ~ <0.0098 <0.0098 <0.0098 <0.0098 <0.0098 <0.0098 <0.0098 <0.0098 <0.0098 <0.0098 <0.0098 <0.0098 <0.0098 " <0.0098 ~ <0.0098 <0.0098 <0.0098 <0.0098 <0.0098 mg/l ___mg/1 mg/1 mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l _2. 1 __1_ __1_ 1 1 1 1 1 __1 1 1 1 1 1 1 1 ~T i _i i ~i i: i' _i i ~i i T [Parameter Base-neutral compounds (cont.) Chrysene T Di-n-butyl phthalate Di-n-octyl phthalate r Dibenzo(a,h)anthracene 1.2- dichlorobenzene 1.3- dichlorobenzene 1.4- dichlorobenzene ~ 3.3- dichlorobenzidine Diethyl phthalate Dimethyl phthalate 2.4- dinitrotoluene 2,6-dinitrotoluene ~ 1,2-diphenylhydrazine ~ Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclo-pent adiene Hexachloroethane Indeno( 1,2,3-cd)pyrene Isophorone Naphthalene Nitrobenzene N-nitrosodi-n-propylamine N-nitrosodimethylamine N-nitrosodiphenylamine Phenanthrene Pyrene 11,2,4,-trichlorobenzene Authorized Representative name Annual Monitoring and Poll Scan Parameter 0.2 1 4.4 1 0.1 1 1 1 1 1 1 Grab Grab Grab Grab Grab Grab Grab Grab Form - DMR- PPA-1 Page 1 0.025 0.010 Antimony Arsenic Composite Composite Grab Grab 4,08 292 15.9 T.32 1 I 0.1 NA 10 T <0.025 <0.010 Permit No. _NC0024 Outfall___001______ ORC _A. Gregg Camp____ Phone _252-536-4884 NC 165 and RRSD WWTP NC 70 Analytical Method Quantitation Level Sample Result Units of Measurement Number of samples Facility Name _Roanoke Rapids Sanitaiy District. Date of sampling _July 17, 2011_ Analytical Laboratory _Meritech, Inc. Sample Type Month__July Year 2011 1 T EPA 350.1 SM4500Q G EPA 353.2~ EPA 351,1 EPA 200,7 SM 2540C SM 2340B HACK10014 ______________________EPA 1664A Metals (total recoverable), cyanide and total phenols EPA 200.7 EPA 200.7 Composite Composite Composite Composite Composite Composite Composite Composite Composite Composite Composite Grab Grab Composite Grab Composite Composite Composite Composite Composite Grab Grab Grab Grab Grab Grab EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 200,7 EPA 200.7 EPA 200.7~ EPA 200.7 EPA 200.7 EPA1631 EPA 200,7 EPA 200,7 EPA 200,7 EPA 200,7~ EPA 200.7 EPA 335.4 EPA 420.1 <50,0 <10.0 <1.00 <1.00 <1.00 <1.00 <1.00 <5.00 <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 0.005 0.002 0.005 0.010 0.010 0.001 0.010 0.010 0.005 0.020 0.010 0.005 0.010 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 mg/1 mg/1 mg/l mg/1 mg/l mg/l mg/l ug/1 mg/l 1 1 T T i T i T T i T T i F i T T T i T T T i F F i F Acrylonitrile Benzene Bromoform Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane 2-chloroethylvinyl ether Chloroform Dichlorobromomcthane 1.1- dichloroethane 1.2- dichloroe thane [Trans-1,2-dichloroethylene Beryllium Cadmium Chromium Copper Lead Mercury Nickel Selenium Silver Thallium Zinc Cyanide Total phenolic compounds Volatile organic compounds Acrolein Ammonia (as N) Dissolved oxygen Nitrate/Nitrite Total Kjeldahl nitrogen Total Phosphorus Total dissolved solids Hardness Chlorine (total residual, TRC) Oil and grease 0.2 0.02 10 <0.005 <0.002 <0.005 0.010 <0.010 0.00467 <0.010 <0.010 <0.005 <0.020 0.029 <0.005 0.017 60.8 <10 <5.0 <50.0 <10.0 <1.00 3.79 <1.00 <1.00 5.73 <5.00 <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 mg/l mg/l mg/l mg/l mg/l mg/l mg/l ug/1 mg/l mg/l mg/l mg/l mg/l mg/l mg/l Parameter Form - DMR- PPA-1 Page 2 Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Analytical Method Sample Result Units of Measurement Month__July Year____2011 Number of samples Quantitation Level EPA 624 EPA 624 ' EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab EPA 625 EPA 625 EPA 625 ~ EPA 625 EPA 625 EPA 625 ~ EPA 625 EPA 625 ~ EPA 625 ' EPA 625 EPA 625 ’ EPA 625 ' EPA 625 EPA 625 EPA 625 ' EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 <1.00 <1.00 <1.00 <1.00 <5.00 <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <5.00 <10 <10 <10 <10 <50 <50 <10 <50 <50 <10 <10 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 1 ~T ^7 1 T 1 T T T T T T T~ r 1 1 T 7 1 1 7 7 7 i T~ i i i i i i i 7 i i i T F i <10 <10 <10 <50 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <50 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <1.00 <1.00 <1.00 <1.00 <5.00 <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <5.00 <10 <10 <10 <10 <50 <50 <10 <50 <50 <10 <10 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 Permit No. _NC0024^^__ Outfall 001 Annual Monitoring and Poll]^^ t Scan Sample __ Type Volatile organic compounds (Cont.) 1,1 -dichloroethylene 1.2- dichloropropane 1.3- dichloropropylene Ethylbenzene Methyl bromide Methyl chloride Methylene chloride 1.1.2.2- tetrachloroeth a ne Tetrachloroethylene Toluene 1,1,1 -trichloroethane 1.1.2- trichloroe thane Trichloroethy le n e Vinyl chloride Acid-extractable compounds P-chloro-m-creso 2-chlorophenol 2.4- dichlorophenol 2.4- dimethyl phenol 4.6- dinitro-o-cresol 2.4- dinitrophenol 2-nitrophenol 4-nitrophenol Pentachlorophenol Phenol 2.4.6- trichlorophenol Base-neutral compounds Acenaphthene Acenaphthylene Anthracene Benzidine Benzo(a)anthracene Benzo(a)pyrene 3,4 benzofluoranthene Benzo(ghi)perylene Benzo(k)fluoranthene Bis (2-chloroethoxy) methane Bis (2-chloroethyl) ether Bis (2-chloroisopropyl) ether Bis (2-ethylhexyl) phthalate 4-bromophenyl phenyl ether Butyl benzyl phthalate 2-chloronaphthalene Parameter j am Signature Date Form - DMR- PPA-1 Page 3 EPA 625 Analytical Method <10 Sample Result 1 Number of samples <10 Quantitation Level Grab Sample Type Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab I EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 _ EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 ~ EPA 625 ~ EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 EPA 625 <10 <10 <10 <10 <10 <10 <10 <50 <10 <10 <10 <10 <10 <10 <10 <10 <10 <50 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 ug/1 ug/1 ug/1 ug/1 ug/I ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/I ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 1 1 __1_ 1 1 1 1 1 1 1 1 1 ~T~ ~T~ 1 ~T~ 1 T~ T" 1 T“ 1 T“ 1 1 ~1 1 7 i <10 <10 <10 <10 <10 <10 <10 <50 <10 <10 <10 <10 <10 <10 <10 <10 <10 <50 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 Base-neutral compounds (cont.) Chrysene Di-n-butyl phthalate Di-n-octyl phthalate Dibenzo(a,h)anthracene 1.2- dichlorobenzene ~ 1.3- dichlorobenzene 1.4- dichloro benzene 3.3- dichloro benzidine Diethyl phthalate Dimethyl phthalate 2.4- dinitrotoluene 2,6-dinitrotolu ene 1,2-diphenylhyd razin e Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclo-pentadiene Hexachloroethane Indeno( 1,2,3-cd)pyrene Isophorone Naphthalene Nitrobenzene N-nitrosodi-n-propylamine N-nitrosodimethylamine ~~ N-nitrosodiphenylamine Phenanthrene Pyrene 1.2,4,-trichlorobenzene Permit No. _NC0024^^ Outfall 001 4-chlorophenyl phenyl ether Annual Monitoring and Poll^fe| : Scan Authorized Representative name I certify under penalty of taw that this document and all attachments were prepared under my direction anage the system, or those persons directly responsibel for gathering the information, the mformatron subm.tted is , to the best of my knowledge and belief, true, accurate and complete I War?‘h ' an! SI8nlficant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Month_July Year____2011 ~ ug/1 Units of ] Measurement NPDES FORM 2A Additional Information Attachment B: Second Species Toxicity Test Results Effluent Toxicity R Form-Chronic Fathead Minnow Mui Date:8/2/2011ncentration Test Facility: Roanoke Rapids Sanitary District NPDES # NCOO 24201 Pipe #: County: Halifax Comments |Laboratory: Meritech, Inc. x Signature of Operator in Responsible Charge x Signature of Laboratory Supervisor MAIL ORIGINAL TO: Test Initiation Date/Time 7/19/2011 3’55 PM Avg Wt/Surv. ControlF ]0.595 Test Organisms % Survival[97.5 Avg Wt (mg)[0.581 Hatch Date:7/18/11 % Survival[97.5 Hatch Time:3:00 PM Avg Wt (mg)[ 0.552 % Survival[J95.0 Avg Wt (mg)[ 0.583 1.1 % Survivalf 92.5 Avg Wt (mg)[ 0.551 [2.2 % Survival[97.5 Avg Wt (mg)[0.533 % Survivalf J97.5 Avg Wt (mg)[0.562 - n\A/(~> Pnrm AT.H f1/riA\ 1 7/18/2011 Water Quality Data Control pH (SU) Init/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin Sample Collection Start Date Grab Composite (Duration) Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) Chlorine(mg/L) Temp at Receipt (’C) | 4.4 | Surviving # Original # Wt/original (mg) | 0.275 | Surviving # Original # Wt/original (mg) | 0.55 | Surviving# Original # Wt/original (mg) High Concentration pH (SU) Init/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin 1 Surviving # Original # Wt/original (mg) 1 Surviving # Original # Wt/original (mg) r Cultured In-House P Outside Supplier Dilution H2O Batch # Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) Normal Hom. Var. NOEC LOEC ChV Method Environmental Sciences Branch Division of Water Quality NC DENR 1621 Mail Service Center Raleigh, NC 27699-1621 0 7 91 / 8 06 7 24 / 7 20 25.8 / 24 3 0 8.18 / 8.17 7 17 / 7 40 25.8 / 24 3 9 10 0.511 10 10 0.545 9 10 0.510 9 10 0.575 9 10 0.610 560 48 58 220 561 46 59 216 1 8 24 / 7 76 7 45 / 6 82 25 8 / 24 2 1 8.33 / 7 94 7 49 / 7 03 25 8 / 24 2 2 7/20/2011 10 10 0.560 10 10 0.540 9 10 0.572 10 10 0.594 9 10 0.596 2 10 10 0 594 2 8 23 / 8.08 7 55 / 7 20 24 3 / 24 3 2 8.16 / 8 04 7 39 / 7 35 24 3 / 24 3 9 10 0.528 10 10 0.538 10 10 0.539 10 10 0.487 10 10 0.588 3 10 10 0.576 10 10 0.616 10 10 0.542 9 10 0.584 10 10 0.571 4 9 10 0.524 Survival Critical 10 10 10 10 10 5 8.23 / 7.97~ 7 46 / 7.30 25.6 / 24.3 Calculated 18 16 14 18 18 6 8.21 / 7 84 7 57 / 7.04 25 6 / 24 4 559 48 58 217 1 10 10 0.629 3 7/21/2011 10 10 0.516 Stats Cone. 0.275 0 55 1.1 2.2 4.4 4 8.34 / 7.91~ 7 65 / 7.20 24 7 / 24 3 6 8.17 / 784 7.58 / 7,17 25 6 / 24 4 % Eff. Repl. [Control | Sun/iving # Original # Wt/original (mg) 23.9 54 81 405 <0.1 1.7 24.7 52 77 626 <0.1 1.6 24.1 59 76 567 <0.1 1 8 4 8.23 / 7.89' 7 55 / 7.24 Survival FB FP 44 >4.4 >4 4 Steel's Growth Fl* Fk 4 4 >4.4 >4,4 Dunnet's Growth Critical Calculated 2.41 1.0971 2.41 -0.0662 2.41 1.1160 2.41 1 8159 2.41 0.6999 5 8 20 / 7 96 7.54 / 7 36 25.6 / 24 3 3 8.23 / 8.11 7 62 / 7 42 25 0 / 24 5 [ 24 7 / 24 3 Overall Result ChV [ >4 4 Day 3 8.30 / 8.02 7.39 / 7 34 25 0 / 24 5 Date:4/29/2011 NPDES # NCOO 24201 Pipe #: County: CommentslLaboratory: Meritech, Inc. x Signature of Operator in Responsible Charge x Signature of Laboratory Supervisor MAIL ORIGINAL TO: Avg Wt/Surv. Control[Test Initiation Date/Time 3:10 PM 0.636 Test Organisms4/19/2011 % Survival [100.0 Avg Wt (mg)[Hatch Date:4/18/110.636 % Survival [Hatch Time: 3:00 pm CT100.0 Avg Wt (mg)[0.648 % Survival[100.0 Avg Wt (mg)[0.671 % Survival [100.01.1 JAvg Wt (mg)[0.670 % Survival [95.0 Avg Wt (mg)[j0.649 % Survival[100.0[4.4 JAvg Wt (mg)[0.665 DWQ Form AT-5 (1/04) 1 4/18/2011 r Cultured In-House Outside Supplier Water Quality Data Control pH (SU) Init/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin | 0.275 | Surviving # Original # Wt/original (mg) | 0.55 I Surviving # Original # Wt/original (mg) 2.2 | Surviving # Original # Wt/original (mg) High Concentration pH (SU) Init/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin 1 | Surviving # Original # Wt/original (mg) 1 Surviving # Original # Wt/original (mg) Sample Collection Start Date Grab Composite (Duration) Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) Chlorine(mg/L) Temp, at Receipt (’C) Dilution H2O Batch# Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) % Eff. Repl. [Control | Surviving # Original # Wt/original (mg) Environmental Sciences Branch Division of Water Quality NC DENR 1621 Mail Service Center Raleigh, NC 27699-1621 Normal Hom. Var. NOEC LOEC ChV Method 540 48" 59 221 10 10 0.658 10 10 0.638 10 10 0.685 8 10 0.545 10 10 0.666 1 10 10 0.594 541 46 57 224 1 8.22 / 7.81 7.50 / 6 75 25.7 / 24.2 1 8.16 / 7.78 7.42 / 6.50 25 7 / 24 2 2 4/20/2011 10 10 0.617 10 10 0.647 10 10 0.710 10 10 0.671 10 10 0.616 2 10 10 0.665 543 48 60 230 2 8.25 / 7.97 7.57 / 7.10 25.8 / 24.3 2 8.17 / 7 99 7 47 / 7 20 25 8 / 24 3 10 10 0.580 10 10 0.652 10 10 0.622 10 10 0.720 10 10 0.706 3 10 10 0.627 10 10 0.747 10 10 0.663 10 10 0.659 10 10 0.673 10 10 0.736 Survival Critical 10 10 10 10 10 Calculated _ 18 18 18 16 18 6 8.24 / 8.18 7.40 / 7 25 25.5 / 24 5 6 8 22 / 8.12 7 36 / 7.18 25.5 / 24 5 Calculated -0.3249 -0 9543 -0.9272 -0.3519 -0.7986 0 8.16 / 8.07 7.38 / 7.37 25.8 / 24.2 0 8.06 / 7 99 7 45 / 7.25 25 8 / 24 2 542 48 58 218 3 4/21/2011 4 10 10 0.657 4 8.29 / 7.88 7.33 / 6.97 24.7 / 24.3 5 8.29 / 8.01 7 44 / 7.10 24 9 / 24.2 23 8 48 20 388 <0.1 0.5 23 8 50 79 491 <0.1 0.6 23.7 50 91 498 <0.1 1.1 Stats Cone. 0.275 0.55 1.1 2.2 4.4 Effluent Toxicity Rep^^Form-Chronic Fathead Minnow Multi-(j|^pentration Test Facility: Roanoke Rapids Sanitary District Growth Critical 2.41 2.41 2.41 2.41 2.41 Growth Fl Fl 4.4 >4.4 >4.4 Dunnet's Survival Fl Fl 4.4 >4 4 >4 4 Steel's 3 8.24 / 8.14 7 47 / 7.19 24 3 / 24 2 5 8 14 / 7 98 7 35 / 6 99 24 9 / 24 2 4 8.28 / 7.89 7 31 / 6 98 24 7 / 24 3 Overall Result ChV | >4 4 Day 3 ~ 8.26 / 8.17 7.48 / 7 21 24.3 / 24.2 Date: 1/28/2011 NPDES# NC00 24201 Pipe # County: Comments|Laboratory: Meritech, Inc. x Signature of Operator in Responsible Charge x Signature of Laboratory Supervisor MAIL ORIGINAL TO: Avg Wt/Surv. Control^Test Initiation Date/Time 2:50 PM1/18/2011 0.619 Test Organisms % Survival[100.0 Avg Wt (mg)r 0.619 Hatch Date:1/17/11 % Survival[100.0 Hatch Time: 3:00 pm CT Avg Wt (mg)[0.632 % Survivalf 100.0 Avg Wt (mg)[0.631 % Survival[1.1 100.0 Avg Wt (mg)[0.591 % Survival[100.0 Avg Wt (mg)[ 0.606 % Survival F 97.54.4 Avg Wt (mg)r 0.607 Day DWO Form AT-.5 /1/04) 1 1/17/2011 Water Quality Data Control pH (SU) Init/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin Sample Collection Start Date Grab Composite (Duration) Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) Chlorine(mg/L) Temp, at Receipt (°C) [ 2 2 | Surviving# Original # Wt/original (mg) | 0.275 | Surviving# Original # Wt/original (mg) | 0.55 I Surviving # Original # Wt/original (mg) High Concentration pH (SU) Init/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin 1 Surviving # Original # Wt/original (mg) 1 | Surviving # Original # Wt/original (mg) F Cultured In-House F Outside Supplier Dilution H2O Batch # Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) Environmental Sciences Branch Division of Water Quality NC DENR 1621 Mail Service Center Raleigh, NC 27699-1621 Normal Hom. Var. NOEC LOEC ChV Method 523 48 60 225 10 10 0 621 10 10 0.648 10 10 0.642 10 10 0.692 10 10 0.586 1 10 10 0.607 524 48 62 232 525 48 58 227 10 10 0.620 10 10 0.610 10 10 0 607 10 10 0.652 2 10 10 0.627 10 10 0.698 2 8.13 / 8 11 7.71 / 7.60 24.7 / 24 4 2 8.05 / 8.09 7.63 / 7 60 24 7 / 24.4 3 1/20/2011 9 10 0.614 10 10 0.543 10 10 0 562 10 10 0.623 10 10 0.634 3 10 10 0.617 10 10 0.560 10 10 0.584 10 10 0.588 10 10 0 559 10 10 0.620 4 8.23 / 7.75 7.75 / 6.60 24.5 / 24 2 4 8.18 / 7 76 7.79 / 6.40 24 5 / 24 2 Survival Critical 10 10 10 10 10 5 8.22 / 8 12 7 58 / 7.56 24.3 / 24 2 5 8.30 / 8.05 7.63 / 7.60 24 3 / 24 2 Calculated 18 18 18 18 16 6 8 20 / 7 85 7 90 / 7.15 24 6 / 24 2 6 8.21 / 7.85 7 90 / 7.17 24.6 / 24 2 Critical 2.41 2.41 241 2.41 2.41 0 8 23 / 7 96 7 59 / 7 29 24 6 / 24 3 0 8.23 / 8.08 7 65 / 7 47 24 6 / 24 3 1 8.24 / 7.84' 7 55 / 7,32 24 9 / 24 3 1 8.15 / 782 7.51 / 7 10 24 9 / 24 3 2 1/19/2011 3 8.26 / 7 68 7.82 / 6.05 24 2 / 24.3 4 10 10 0.623 Stats Cone. 0.275 0.55 1.1 2.2 4 4 % Eff. Repl. [Control | Surviving # Original # Wt/original (mg) 23.1 44 22 374 <0.1 0.2 24.1 50 45 380 <0.1 0.3 23.9 58 72 412 <0.1 0.3 Effluent Toxicity Rei^^Form-Chronic Fathead Minnow Multi-] Facility: Roanoke Rapids Sanitary District Growth Calculated -0.4780 -0.4264 0 9771 0.4441 0 4264 Survival Fl Fl 4 4 >4 4 >4 4 Steel's Growth Fl Fl 4 4 >4.4 >4.4 Dunnet's ^centration Test 3 8.23 / 7 74 7 81 / 7.51 24 2 / 24 3 Overall Result ChV | >4 4 Effluent Toxicity Re,Date: 10/22/2010 Facility: Roanoke Rapids Sanitary District NPDES # NC00 24201 Pipe # County: Laboratory: Meritech, Inc.Comments! x Signature of Operator in Responsible Charge cX Signature of Laboratory Supervisor MAIL ORIGINAL TO: Test Initiation Date/Time Avg Wt/Surv. Controlf10/12/2010 4.00 PM 0.537 Test Organisms % Survival[97 5 Avg Wt (mg)[0.524 Hatch Date:10/11/10 % Survival[100.0 Hatch Time: 3:00 pm CT Avg Wt (mgjF 0 552 % Survival[100.0 Avg Wt (mg)[0.535 % SurvivalF1.1 97.5 Avg Wt (mgH 0.518 % SurvivalF 100.0 Avg Wt (mg)[0.540 % SurvivalF4.4 97.5 Avg Wt (mg)[0.534 Day J DWQ FormAT-5 (1/04) 1 10/11/2010 F Cultured In-House Outside Supplier Water Quality Data Control pH (SU) Imt/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin Dilution H2O Batch # Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) Sample Collection Start Date Grab Composite (Duration) Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) Chlorine(mg/L) Temp, at Receipt (“C) | 0.275 | Surviving # Original # Wt/original (mg) | 0.55 | Surviving # Original # Wt/original (mg) High Concentration pH (SU) Init/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin 1 Surviving # Original # Wt/original (mg) 1 Surviving # Original # Wt/original (mg) 2.2 | Surviving # Original # Wt/original (mg) Normal Hom. Var. NOEC LOEC ChV Method Environmental Sciences Branch Division of Water Quality NC DENR 1621 Mail Service Center Raleigh, NC 27699-1621 % Eff. Repl. [Control | Surviving # Original # Wt/original (mg) 495 48 62 212 0 8.22 / 8.13 7.36 / 7.32 25 7 / 25 4 0 8.14 / 8.12 7.30 / 7 28 25 7 / 25 4 10 10 0.551 10 10 0.548 10 10 0.523 10 10 0.509 10 10 0.545 1 8.29 / 8.04 7.45 / 7 41 25 5 / 25.1 2 10/12/2010 10 10 0.562 10 10 0.498 10 10 0.545 10 10 0 577 2 10 10 0.516 2 8.26 / 8.17 7 55 / 7 48 25 0 / 24 4 3 10/14/2010 10 10 0.560 10 10 0.570 9 10 0.486 10 10 0.562 10 10 0.542 3 10 10 0.554 3 8.23 / 8.14 7 58 / 7.33 24.1 / 25.0 9 10 0.463 10 10 0.544 10 10 0.517 10 10 0.546 10 10 0 545 4 10 10 0 547 Survival Critical 10 10 10 10 10 5 8 25 / 8.01 7 77 / 7 56 25 2 / 24 1 Calculated 20 20 18 20 18 6 8 18 / 7 80' 7 67 / 6 83 24.3 / 24 5 6 8.20 / 7.87 7.69 / 6.93 24 3 / 24 5 1 9 10 0 477 496 48 66 216 497 40 54 216 1 8 26 / 8 07 7 45 / 7 40 25 5 / 25 1 24 7 44 41 397 <0.1 1 0 10 10 0.521 498 48 54 208 2 8 23 / 8 19 7 57 / 7 54 25 0 / 24 4 Stats Cone. 0.275 0.55 1.1 2.2 4.4 4 8.26 / 8 15 7 55 I 7 56 24 7 / 25 0 4 8.28 / 8.14 7.66 / 7.60 24 7 / 25.0 5 8 28 / 8.03 7 77 / 7 50 25.2 I 24 1 24.1 44 25 360 <0 1 0.1 23.7 '44 ■79 ■444 <0.1 1.2 Growth Critical Calculated 2.41 -1.3018 2.41 -0 4981 T41 0 2604 2.41 I -0.7471 2 41 -0 4755 Growth Fl Fl 4 4 M4 >4 4 Dunnet's Survival ri n 4 4 >44 >4 4 Steel's 3 8.30 / 8 22 7 60 / 7 43 24 1 / 25.0 ^Form-Chronic Fathead Minnow Multi^j^centration Test Overall Result ChV | >4 4 Attachment C: Biosolids Program Description NPDES FORM 2A Additional Information ATTACHMENT C Roanoke Rapids Sanitary District At present, the District has permitted approximately 3,100 acres of private farmland of which 91 acres of self owned land for residual application. Approximately 2,600,000 gallons of ~5% solids is applied to an estimated 226 acres per year. Soil pH is adjusted to achieve a soil pH as specified by permit conditions. Synagro Southeast, Inc. manages Land application of residuals. The Roanoke Rapids Sanitary District holds the land application permit and provides a licensed ORC and back-up ORC as required. Synagro Southeast, Inc. provides transport and application equipment and personnel. District personnel perform all treatment of residuals. Pathogen and VAR reduction for Waste Activated Sludge (WAS) is accomplished by lime stabilization, mixing, and a holding system to maintain proper pH control. Primary solids are treated through three anaerobic digesters with solids either stored for liquid application or dried on drying beds. Storage (holding) of treated solids is provided by an above ground 1.0 million gallon (MG) tank and backed-up by two retrofitted clarifiers adding 0.375 MG each to provide a total of 1.75 MG storage in an emergency. Biosolids Program Roanoke Rapids Sanitary District NPDES Permit No. NC0024201 Land Application Permit No. WQ0001989 The District utilizes final alkaline stabilization of waste activated sludge and anaerobic digested primary sludge in order to meet pathogen and vector reduction requirements. The alkaline stabilization process and anaerobic digested primary sludge meets all requirements for pathogen and vector attraction reduction (VAR) for Class B biosolids. R. Danieley Bro(vn, P.E. Chief Executive Officer Subject: Dear Mr. Camp, Sincerely, cc: RRO files Beverly Eaves Perdue Governor Raleigh Regional Office 1628 Mail Service Center Vicki Webb Environmental Specialist Phone (919) 791-4200 FAX (919) 788-7159 Dee Freeman Secretary The aquatic toxicity test using 24-hr composite samples of effluent discharged from Roanoke Rapids WWTP has been completed. Roanoke Rapids WWTP has an effluent discharge permitted that is 8.34 million gallons per day (MGD) entering Roanoke River (7Q10 of 1172 CFS). Whole effluent samples were collected on March 15 and March 17 by Vicki Webb and Tom Ascenzo for use in a chronic Ceriodaphnia dubia pass-fail toxicity test. The test using these samples resulted in a pass. Toxicity test information follows. Whole effluent toxicity test results Roanoke Rapids WWTP NPDES Permit # NC0024201/001 Halifax County North Carolina Division of Water Quality Raleigh Regional Office Surface Water Protection Internet: www.ncwaterquality.org 1628 Mail Service Center Raleigh, NC 27699-1628 An Equal Opportunity/Affirmative Action Employer - 50% Recycled/10% Post Consumer Paper Mr. Gregg Camp 135 Aqueduct Rd. Weldon, NC 27890 Test Type Test Concentrations Test Result Control Survival Control Mean Reproduction Test Treatment Survival Treatment Mean Reproduction First Sample pH First Sample Conductivity First Sample Total Residual Chlorine Second Sample pl 1 Second Sample Conductivity Second Sample Total Residual Chlorine 3-Brood Ceriodaphnia dubia chronic pass fail 1.1% Pass 100% 22.4 neonates 92% 23.6 neonates 7.11 SU 409 micromhos/cm <0.10 ing/L 7.08 SU 429 micromhos/cm <0.10 me/L OneNorthCarolina — Naturally Customer Service 877-623-6748 If you have any questions concerning the toxicity sampling or results, please contact me either by phone at (919) 791-4200 or email at vicki.webb@ncdenr.gov. HCDENR North Carolina Department of Environment and Natural Resources Division of Water Quality Coleen H. Sullins Director May 13,2011 EPA NPDES NC0024201 INI66I Permit Effective DateEntry Time/Date 07/07/0111/03/1409:00 AM Roanoke Rapids WWTP Permit Expiration DateExit Time/Date135 Aqueduct Rd 12/03/3111/03/14Weldon NC 27890 03:00 PM Other Facility Data Name, Address of Responsible Official/Title/Phone and Fax Number Camp,P0 Box 308 Roanoke Rapids NC 27870//252-536-4884/Gregg Section C: Areas Evaluated During Inspection (Check only those areas evaluated) Other Section D: Summary of Finding/Comments (Attach additional sheets of narrative and checklists as necessary) (See attachment summary) Agency/Office/Phone and Fax NumbersName(s) and Signature(s) of Inspector(s) RRO WQ///Vicki Webb RRO WQ//919 791-4200/tom ascenzo Page #1 3l United States Environmental Protection Agency Washington, D C. 20460 yr/mo/day 11/03/14 Contacted No Date Form Approved. OMB No. 2040-0057 Approval expires 8-31-98 Name(s) of Onsite Representative(s)/Titles(s)/Phone and Fax Number(s) /// Inspection Work Days 671 I 69 77 7 EPA Form 3560^3 (Rev 9-94) Previous editions are obsolete. QA 72Ld Facility Self-Monitoring Evaluation Rating 70U J11 Fac Type 20U ____________________________________________Section B: Facility Data______ Name and Location of Facility Inspected (For Industrial Users discharging to POTW, also include POTW name and NPDES permit Number) Inspector 19QJ Inspection Type 18UIJ1712l Transaction Code 1 w 2 111 Remarks 21l I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I 73l I I74 -----Reserved--------------------- 75| I I I I I I I 80 Bl71 u Water Compliance Inspection Report Section A: National Data System Coding (i.e., PCS) ' / Agency/Officp/Phone anti Fax Numbers DateSignature of Management Q A Reviewer Permit: NC0024201 Inspection Date: 03/14/2011 Yes No NA NEOther Comment:Tox test ran the week of March 14, 2011. Facility passed 3Page # Owner - Facility: Roanoke Rapids WWTP Inspection Type: Bioassay Compliance