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HomeMy WebLinkAboutWI0500180_Documentation of compliance actions_20240627 June 27, 2024 Michael Hall North Carolina Department of Environmental Quality Division of Water Resources, Raleigh Regional Office 1628 Mail Service Center Raleigh, North Carolina 27699 Subject: 102 City Hall Plaza and 200 North Mangum Street Durham, Durham County, North Carolina Permit No. WI0500180 Mid-Atlantic Job No. R3791.02 Dear Mr. Hall: Mid-Atlantic Associates, Inc. (Mid-Atlantic) is pleased to submit this summary of environmental services performed at the 102 City Hall Plaza and 200 North Mangum Street site on behalf of NP Loden Durham, LLC. Included in this report are the action items requested by the North Carolina Department of Environmental Quality (NCDEQ), Division of Water Resources (DWR), Raleigh Regional Office (RRO) following the site inspection and sampling activities in August and October 2023 and a summary of the activities completed to satisfy these action items. Project Background Information The Subject Property is located at 102 City Hall Plaza and 200 North Mangum Street in Durham, North Carolina. The site is identified by Durham County PIN number 0821-12-97-6353, consists of 0.42 acres, and is currently developed with two multi-tenant retail/commercial buildings totaling approximately 33,000 square feet. The site was issued Permit No. WI0500180 on December 12, 2023 for the continued operation of three geothermal heating/cooling water return wells. Prior to issuance, the NCDEQ DWR, RRO completed an inspection of the site on August 8, 2023 and returned to the site on October 27, 2023 to inspect and sample the three geothermal well systems. Groundwater test results indicated that concentrations of fecal and total coliform were above North Carolina Groundwater Quality Standards (NCGQS) in all samples analyzed. On January 16, 2024, the RRO requested the following items be achieved and documented within 90 days of permit issuance:  Contact the RRO and verify the correct nomenclature of the wells and their locations;  Identify and label all the wells and their sample ports and provide the RRO with proof (photograph of the wells) that this has been done; 102 City Hall Plaza and 200 North Mangum Street June 27, 2024 Durham, North Carolina Page 2  Have a licensed well driller inspect the vault and well seal for W2, make repairs as necessary, and provide a written verification to the RRO summarizing these repairs and affirming that the vault and well seal are sound;  Ensure that the vault for W1 is readily accessible; and  Take steps to verify the laboratory analytical results for coliform. If the wells and geothermal systems are found to contain coliform, have a licensed well driller disinfect the wells and geothermal systems, and verify that the seals for all the wells are sound, and do not allow infiltration of surface water. Summary of Field Activities Mid-Atlantic confirmed the nomenclature of the well systems and their locations during a visit to the site on February 28, 2024. Mid-Atlantic sent a site map via email to NCDEQ on March 5, 2024 to verify the correct locations of the well systems. Trademasters Service, Inc. was contracted by NP Loden Durham, LLC to label each well and their sampling ports. Mid-Atlantic sent photographs of the properly labeled wells and their sampling ports via email to NCDEQ on March 5, 2024. N.W. Poole Well and Pump Co. was contracted by NP Loden Durham, LLC to inspect the vault and seal for W2. N.W. Poole Well and Pump Co. replaced the well cap with a new aluminum well cap and replaced the seal for W2 on April 9, 2024. During the site visit on April 9, 2024, Mid-Atlantic confirmed that W1 is readily accessible. The well cover is properly labeled and visible. On April 9, 2024, N.W. Poole Well and Pump Co. disinfected each of the three well systems in response to the presence of fecal and total coliform in each well during the October 2023 sampling performed by NCDEQ. Following chlorination, the well systems were run for approximately 8 hours until chlorine was no longer detected in the systems. Due to technical issues with well system W2 following disinfection, Mid-Atlantic delayed sampling for fecal and total coliform until repairs were complete. On June 20, 2024, Mid-Atlantic collected a total of six water samples from the three geothermal well systems. Mid-Atlantic collected samples from the supply ports (W1-I, W2-I, and W3-I) and from the return ports (W1-E, W2-E, and W3-E) of each well system. Each sample was analyzed for fecal coliform (Method IDEXX Coliform) and total coliform (Method SM 9223B). Neither fecal nor total coliform were detected in the well systems. 102 City Hall Plaza and 200 North Mangum Street June 27, 2024 Durham, North Carolina Page 3 Conclusions The activities described herein address the requested items outlined in the letter to NP Loden Durham, LLC from the RRO dated January 16, 2024. Sincerely, MID-ATLANTIC ASSOCIATES, INC. Daniel H. Nielsen, PE Madeline Hook Principal Engineer Staff Scientist Attachments: Site Map Geothermal Well Photo Log Laboratory Analytical Report and Chain of Custody Record DRAWN BY:DATE: ENG. CHECK: JOB NO:DRAFTCHECK: GIS NO: ´ 1 inch = 65 feet 0 100 20050Feet REFERENCES: 1. 2021 AERIAL IMAGERY FROM NC ONEMAP2. COUNTY INFORMATION FROM DURHAM COUNTY GIS3. MID-ATLANTIC FIELD NOTES SITE MAP102 CITY HALL PLAZADURHAM, NORTH CAROLINA APPROVAL: MARCH 2024 DWG NO: 1 R3791.02 Legend #*Location of Well Subject Site Parcel Boundaries 05G-R3791.02-1 MRH #* #*#* W3 W2 W1Approximate Location of Sampling Ports for W1 and W2 Approximate Location of Sampling Ports for W3 102 City Hall Plaza and 200 North Mangum Street Durham, North Carolina 1 Geothermal Well Photo Log Photo 1 - Well 1 and 2 Heat Exchanger Photo 2 - Well 1 Return Port 102 City Hall Plaza and 200 North Mangum Street Durham, North Carolina 2 Photo 3 – Well 1 Supply Port Photo 4 – Well 1 Vault 102 City Hall Plaza and 200 North Mangum Street Durham, North Carolina 3 Photo 5 – Well 2 Return Port Photo 6 - Well 2 Supply Port 102 City Hall Plaza and 200 North Mangum Street Durham, North Carolina 4 Photo 7 – Well 2 Vault Photo 8 – New Seal on Well 2 102 City Hall Plaza and 200 North Mangum Street Durham, North Carolina 5 Photo 9 – New Well Cap on Well 2 Photo 10 – Well 3 Heat Exchanger 102 City Hall Plaza and 200 North Mangum Street Durham, North Carolina 6 Photo 11 – Well 3 Supply and Return Ports Photo 12 – Well 3 Vault ANALYTICAL REPORT PREPARED FOR Attn: Madeline Hook Mid-Atlantic Associates 409 Rogers View Court Raleigh, North Carolina 27610 Generated 6/24/2024 8:58:16 AM JOB DESCRIPTION 102 City Hall Plaza JOB NUMBER 752-21068-1 See page two for job notes and contact information. Cary NC 27511 Suite A 104 Woodwinds Industrial Court Eurofins Raleigh Page 1 of 17 1 2 3 4 5 6 7 8 9 10 11 12 13 14 Eurofins Raleigh Eurofins Raleigh is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies Job Notes This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project Manager. Authorization Generated 6/24/2024 8:58:16 AM Authorized for release by Nikita Kuruganty, Project Manager Nikita.Kuruganty@et.eurofinsus.com (912)354-7858 Page 2 of 17 6/24/2024 1 2 3 4 5 6 7 8 9 10 11 12 13 14 Table of Contents Client: Mid-Atlantic Associates Project/Site: 102 City Hall Plaza Laboratory Job ID: 752-21068-1 Page 3 of 17 Eurofins Raleigh 6/24/2024 Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1 Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3 Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5 Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6 Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9 QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10 Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11 Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .14 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .15 Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16 Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .17 1 2 3 4 5 6 7 8 9 10 11 12 13 14 Definitions/Glossary Job ID: 752-21068-1Client: Mid-Atlantic Associates Project/Site: 102 City Hall Plaza Glossary These commonly used abbreviations may or may not be present in this report. ¤Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MCL EPA recommended "Maximum Contaminant Level" MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative / Absent POS Positive / Present PQL Practical Quantitation Limit PRES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count Eurofins Raleigh Page 4 of 17 6/24/2024 1 2 3 4 5 6 7 8 9 10 11 12 13 14 Job Narrative 752-21068-1 Analytical test results meet all requirements of the associated regulatory program listed on the Accreditation/Certification SummaryPage unless otherwise noted under the individual analysis. Data qualifiers are applied to indicate exceptions. Noncompliantquality control (QC) is further explained in narrative comments. Matrix QC may not be reported if insufficient sample or site-specific QC samples were not submitted. In these situations, todemonstrate precision and accuracy at a batch level, a LCS/LCSD may be performed, unless otherwise specified in themethod. Surrogate and/or isotope dilution analyte recoveries (if applicable) which are outside of the QC window are confirmedunless attributed to a dilution or otherwise noted in the narrative. ReceiptThe samples were received on 6/20/2024 10:15 AM. Unless otherwise noted below, the samples arrived in good condition, and,where required, properly preserved and on ice. The temperature of the cooler at receipt time was 12.0°C. BiologyNo additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Case Narrative Client: Mid-Atlantic Associates Job ID: 752-21068-1 Project: 102 City Hall Plaza Eurofins Raleigh Job ID: 752-21068-1 Eurofins Raleigh Page 5 of 17 6/24/2024 1 2 3 4 5 6 7 8 9 10 11 12 13 14 Detection Summary Job ID: 752-21068-1Client: Mid-Atlantic Associates Project/Site: 102 City Hall Plaza Client Sample ID: W1-I Lab Sample ID: 752-21068-1 No Detections. Client Sample ID: W1-I Lab Sample ID: 752-21068-2 No Detections. Client Sample ID: W1-E Lab Sample ID: 752-21068-3 No Detections. Client Sample ID: W1-E Lab Sample ID: 752-21068-4 No Detections. Client Sample ID: W2-I Lab Sample ID: 752-21068-5 No Detections. Client Sample ID: W2-I Lab Sample ID: 752-21068-6 No Detections. Client Sample ID: W2-E Lab Sample ID: 752-21068-7 No Detections. Client Sample ID: W2-E Lab Sample ID: 752-21068-8 No Detections. Client Sample ID: W3-I Lab Sample ID: 752-21068-9 No Detections. Client Sample ID: W3-I Lab Sample ID: 752-21068-10 No Detections. Client Sample ID: W3-E Lab Sample ID: 752-21068-11 No Detections. Client Sample ID: W3-E Lab Sample ID: 752-21068-12 No Detections. Eurofins Raleigh This Detection Summary does not include radiochemical test results. Page 6 of 17 6/24/2024 1 2 3 4 5 6 7 8 9 10 11 12 13 14 Client Sample Results Job ID: 752-21068-1Client: Mid-Atlantic Associates Project/Site: 102 City Hall Plaza Lab Sample ID: 752-21068-1Client Sample ID: W1-I Matrix: Drinking WaterDate Collected: 06/20/24 09:10 Date Received: 06/20/24 10:15 Method: SM 9223B - Coliforms, Total, and E.Coli (Colilert - Presence/Absence) RL MDL ABSENT NONE 06/20/24 15:11 1 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier Escherichia coli NONE 06/20/24 15:11 1ABSENTColiform, Total Lab Sample ID: 752-21068-2Client Sample ID: W1-I Matrix: WaterDate Collected: 06/20/24 09:10 Date Received: 06/20/24 10:15 Method: IDEXX Coliform - Coliforms, Fecal RL MDL ND 1.0 MPN/100mL 06/20/24 14:13 1 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier Coliform, Fecal Lab Sample ID: 752-21068-3Client Sample ID: W1-E Matrix: Drinking WaterDate Collected: 06/20/24 09:15 Date Received: 06/20/24 10:15 Method: SM 9223B - Coliforms, Total, and E.Coli (Colilert - Presence/Absence) RL MDL ABSENT NONE 06/20/24 15:11 1 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier Escherichia coli NONE 06/20/24 15:11 1ABSENTColiform, Total Lab Sample ID: 752-21068-4Client Sample ID: W1-E Matrix: WaterDate Collected: 06/20/24 09:15 Date Received: 06/20/24 10:15 Method: IDEXX Coliform - Coliforms, Fecal RL MDL ND 1.0 MPN/100mL 06/20/24 14:13 1 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier Coliform, Fecal Lab Sample ID: 752-21068-5Client Sample ID: W2-I Matrix: Drinking WaterDate Collected: 06/20/24 09:20 Date Received: 06/20/24 10:15 Method: SM 9223B - Coliforms, Total, and E.Coli (Colilert - Presence/Absence) RL MDL ABSENT NONE 06/20/24 15:11 1 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier Escherichia coli NONE 06/20/24 15:11 1ABSENTColiform, Total Lab Sample ID: 752-21068-6Client Sample ID: W2-I Matrix: WaterDate Collected: 06/20/24 09:20 Date Received: 06/20/24 10:15 Method: IDEXX Coliform - Coliforms, Fecal RL MDL ND 1.0 MPN/100mL 06/20/24 14:13 1 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier Coliform, Fecal Lab Sample ID: 752-21068-7Client Sample ID: W2-E Matrix: Drinking WaterDate Collected: 06/20/24 09:25 Date Received: 06/20/24 10:15 Method: SM 9223B - Coliforms, Total, and E.Coli (Colilert - Presence/Absence) RL MDL ABSENT NONE 06/20/24 15:11 1 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier Escherichia coli Eurofins Raleigh Page 7 of 17 6/24/2024 1 2 3 4 5 6 7 8 9 10 11 12 13 14 Client Sample Results Job ID: 752-21068-1Client: Mid-Atlantic Associates Project/Site: 102 City Hall Plaza Lab Sample ID: 752-21068-7Client Sample ID: W2-E Matrix: Drinking WaterDate Collected: 06/20/24 09:25 Date Received: 06/20/24 10:15 Method: SM 9223B - Coliforms, Total, and E.Coli (Colilert - Presence/Absence) (Continued) RL MDL ABSENT NONE 06/20/24 15:11 1 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier Coliform, Total Lab Sample ID: 752-21068-8Client Sample ID: W2-E Matrix: WaterDate Collected: 06/20/24 09:25 Date Received: 06/20/24 10:15 Method: IDEXX Coliform - Coliforms, Fecal RL MDL ND 1.0 MPN/100mL 06/20/24 14:13 1 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier Coliform, Fecal Lab Sample ID: 752-21068-9Client Sample ID: W3-I Matrix: Drinking WaterDate Collected: 06/20/24 09:00 Date Received: 06/20/24 10:15 Method: SM 9223B - Coliforms, Total, and E.Coli (Colilert - Presence/Absence) RL MDL ABSENT NONE 06/20/24 15:11 1 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier Escherichia coli NONE 06/20/24 15:11 1ABSENTColiform, Total Lab Sample ID: 752-21068-10Client Sample ID: W3-I Matrix: WaterDate Collected: 06/20/24 09:00 Date Received: 06/20/24 10:15 Method: IDEXX Coliform - Coliforms, Fecal RL MDL ND 1.0 MPN/100mL 06/20/24 14:13 1 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier Coliform, Fecal Lab Sample ID: 752-21068-11Client Sample ID: W3-E Matrix: Drinking WaterDate Collected: 06/20/24 09:05 Date Received: 06/20/24 10:15 Method: SM 9223B - Coliforms, Total, and E.Coli (Colilert - Presence/Absence) RL MDL ABSENT NONE 06/20/24 15:11 1 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier Escherichia coli NONE 06/20/24 15:11 1ABSENTColiform, Total Lab Sample ID: 752-21068-12Client Sample ID: W3-E Matrix: WaterDate Collected: 06/20/24 09:05 Date Received: 06/20/24 10:15 Method: IDEXX Coliform - Coliforms, Fecal RL MDL ND 1.0 MPN/100mL 06/20/24 14:13 1 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier Coliform, Fecal Eurofins Raleigh Page 8 of 17 6/24/2024 1 2 3 4 5 6 7 8 9 10 11 12 13 14 QC Sample Results Job ID: 752-21068-1Client: Mid-Atlantic Associates Project/Site: 102 City Hall Plaza Method: Coliform - Coliforms, Fecal Client Sample ID: DuplicateLab Sample ID: 752-21071-A-2 DU Matrix: Water Prep Type: Total/NA Analysis Batch: 7695 Coliform, Fecal ND ND MPN/100mL NC 25 Analyte DU DU DUnitResult Qualifier Sample Result Sample Qualifier LimitRPD RPD Eurofins Raleigh Page 9 of 17 6/24/2024 1 2 3 4 5 6 7 8 9 10 11 12 13 14 QC Association Summary Job ID: 752-21068-1Client: Mid-Atlantic Associates Project/Site: 102 City Hall Plaza Biology Analysis Batch: 7689 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Drinking Water SM 9223B752-21068-1 W1-I Total/NA Drinking Water SM 9223B752-21068-3 W1-E Total/NA Drinking Water SM 9223B752-21068-5 W2-I Total/NA Drinking Water SM 9223B752-21068-7 W2-E Total/NA Drinking Water SM 9223B752-21068-9 W3-I Total/NA Drinking Water SM 9223B752-21068-11 W3-E Total/NA Analysis Batch: 7695 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water Coliform752-21068-2 W1-I Total/NA Water Coliform752-21068-4 W1-E Total/NA Water Coliform752-21068-6 W2-I Total/NA Water Coliform752-21068-8 W2-E Total/NA Water Coliform752-21068-10 W3-I Total/NA Water Coliform752-21068-12 W3-E Total/NA Water Coliform752-21071-A-2 DU Duplicate Total/NA Eurofins Raleigh Page 10 of 17 6/24/2024 1 2 3 4 5 6 7 8 9 10 11 12 13 14 Lab Chronicle Client: Mid-Atlantic Associates Job ID: 752-21068-1 Project/Site: 102 City Hall Plaza Client Sample ID: W1-I Lab Sample ID: 752-21068-1 Matrix: Drinking WaterDate Collected: 06/20/24 09:10 Date Received: 06/20/24 10:15 Analysis SM 9223B CB1 7689 EET RAL Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 06/20/24 15:11 - 06/21/24 11:12 ¹ Client Sample ID: W1-I Lab Sample ID: 752-21068-2 Matrix: WaterDate Collected: 06/20/24 09:10 Date Received: 06/20/24 10:15 Analysis Coliform ME1 7695 EET RAL Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 06/20/24 14:13 - 06/21/24 11:10 ¹ Client Sample ID: W1-E Lab Sample ID: 752-21068-3 Matrix: Drinking WaterDate Collected: 06/20/24 09:15 Date Received: 06/20/24 10:15 Analysis SM 9223B CB1 7689 EET RAL Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 06/20/24 15:11 - 06/21/24 11:12 ¹ Client Sample ID: W1-E Lab Sample ID: 752-21068-4 Matrix: WaterDate Collected: 06/20/24 09:15 Date Received: 06/20/24 10:15 Analysis Coliform ME1 7695 EET RAL Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 06/20/24 14:13 - 06/21/24 11:10 ¹ Client Sample ID: W2-I Lab Sample ID: 752-21068-5 Matrix: Drinking WaterDate Collected: 06/20/24 09:20 Date Received: 06/20/24 10:15 Analysis SM 9223B CB1 7689 EET RAL Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 06/20/24 15:11 - 06/21/24 11:12 ¹ Client Sample ID: W2-I Lab Sample ID: 752-21068-6 Matrix: WaterDate Collected: 06/20/24 09:20 Date Received: 06/20/24 10:15 Analysis Coliform ME1 7695 EET RAL Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 06/20/24 14:13 - 06/21/24 11:10 ¹ Client Sample ID: W2-E Lab Sample ID: 752-21068-7 Matrix: Drinking WaterDate Collected: 06/20/24 09:25 Date Received: 06/20/24 10:15 Analysis SM 9223B CB1 7689 EET RAL Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 06/20/24 15:11 - 06/21/24 11:12 ¹ Eurofins Raleigh Page 11 of 17 6/24/2024 1 2 3 4 5 6 7 8 9 10 11 12 13 14 Lab Chronicle Client: Mid-Atlantic Associates Job ID: 752-21068-1 Project/Site: 102 City Hall Plaza Client Sample ID: W2-E Lab Sample ID: 752-21068-8 Matrix: WaterDate Collected: 06/20/24 09:25 Date Received: 06/20/24 10:15 Analysis Coliform ME1 7695 EET RAL Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 06/20/24 14:13 - 06/21/24 11:10 ¹ Client Sample ID: W3-I Lab Sample ID: 752-21068-9 Matrix: Drinking WaterDate Collected: 06/20/24 09:00 Date Received: 06/20/24 10:15 Analysis SM 9223B CB1 7689 EET RAL Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 06/20/24 15:11 - 06/21/24 11:12 ¹ Client Sample ID: W3-I Lab Sample ID: 752-21068-10 Matrix: WaterDate Collected: 06/20/24 09:00 Date Received: 06/20/24 10:15 Analysis Coliform ME1 7695 EET RAL Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 06/20/24 14:13 - 06/21/24 11:10 ¹ Client Sample ID: W3-E Lab Sample ID: 752-21068-11 Matrix: Drinking WaterDate Collected: 06/20/24 09:05 Date Received: 06/20/24 10:15 Analysis SM 9223B CB1 7689 EET RAL Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 06/20/24 15:11 - 06/21/24 11:12 ¹ Client Sample ID: W3-E Lab Sample ID: 752-21068-12 Matrix: WaterDate Collected: 06/20/24 09:05 Date Received: 06/20/24 10:15 Analysis Coliform ME1 7695 EET RAL Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 06/20/24 14:13 - 06/21/24 11:10 ¹ ¹ This procedure uses a method stipulated length of time for the process. Both start and end times are displayed. Laboratory References: EET RAL = Eurofins Raleigh, 104 Woodwinds Industrial Court, Suite A, Cary, NC 27511, TEL (919)467-3090 Eurofins Raleigh Page 12 of 17 6/24/2024 1 2 3 4 5 6 7 8 9 10 11 12 13 14 Accreditation/Certification Summary Client: Mid-Atlantic Associates Job ID: 752-21068-1 Project/Site: 102 City Hall Plaza Laboratory: Eurofins Raleigh Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below. Authority Program Identification Number Expiration Date North Carolina (DW)State 37724 07-31-24 The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which the agency does not offer certification. Analysis Method Prep Method Matrix Analyte Coliform Water Coliform, Fecal Eurofins Raleigh Page 13 of 17 6/24/2024 1 2 3 4 5 6 7 8 9 10 11 12 13 14 Method Summary Job ID: 752-21068-1Client: Mid-Atlantic Associates Project/Site: 102 City Hall Plaza Method Method Description LaboratoryProtocol IDEXXColiformColiforms, Fecal EET RAL SMSM 9223B Coliforms, Total, and E.Coli (Colilert - Presence/Absence)EET RAL Protocol References: IDEXX = IDEXX Laboratories SM = "Standard Methods For The Examination Of Water And Wastewater" Laboratory References: EET RAL = Eurofins Raleigh, 104 Woodwinds Industrial Court, Suite A, Cary, NC 27511, TEL (919)467-3090 Eurofins Raleigh Page 14 of 17 6/24/2024 1 2 3 4 5 6 7 8 9 10 11 12 13 14 Sample Summary Client: Mid-Atlantic Associates Job ID: 752-21068-1 Project/Site: 102 City Hall Plaza Lab Sample ID Client Sample ID Matrix Collected Received 752-21068-1 W1-I Drinking Water 06/20/24 09:10 06/20/24 10:15 752-21068-2 W1-I Water 06/20/24 09:10 06/20/24 10:15 752-21068-3 W1-E Drinking Water 06/20/24 09:15 06/20/24 10:15 752-21068-4 W1-E Water 06/20/24 09:15 06/20/24 10:15 752-21068-5 W2-I Drinking Water 06/20/24 09:20 06/20/24 10:15 752-21068-6 W2-I Water 06/20/24 09:20 06/20/24 10:15 752-21068-7 W2-E Drinking Water 06/20/24 09:25 06/20/24 10:15 752-21068-8 W2-E Water 06/20/24 09:25 06/20/24 10:15 752-21068-9 W3-I Drinking Water 06/20/24 09:00 06/20/24 10:15 752-21068-10 W3-I Water 06/20/24 09:00 06/20/24 10:15 752-21068-11 W3-E Drinking Water 06/20/24 09:05 06/20/24 10:15 752-21068-12 W3-E Water 06/20/24 09:05 06/20/24 10:15 Eurofins Raleigh Page 15 of 17 6/24/2024 1 2 3 4 5 6 7 8 9 10 11 12 13 14 Pa g e 1 6 o f 1 7 6/ 2 4 / 2 0 2 4 1234567891011121314 Login Sample Receipt Checklist Client: Mid-Atlantic Associates Job Number: 752-21068-1 Login Number: 21068 Question Answer Comment Creator: Barnes, Sara List Source: Eurofins Raleigh List Number: 1 TrueRadioactivity wasn't checked or is </= background as measured by a survey meter. TrueThe cooler's custody seal, if present, is intact. TrueSample custody seals, if present, are intact. TrueThe cooler or samples do not appear to have been compromised or tampered with. TrueSamples were received on ice. TrueCooler Temperature is acceptable. TrueCooler Temperature is recorded. TrueCOC is present. TrueCOC is filled out in ink and legible. TrueCOC is filled out with all pertinent information. TrueIs the Field Sampler's name present on COC? TrueThere are no discrepancies between the containers received and the COC. TrueSamples are received within Holding Time (excluding tests with immediate HTs) TrueSample containers have legible labels. TrueContainers are not broken or leaking. TrueSample collection date/times are provided. TrueAppropriate sample containers are used. TrueSample bottles are completely filled. TrueSample Preservation Verified. TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs TrueContainers requiring zero headspace have no headspace or bubble is <6mm (1/4"). TrueMultiphasic samples are not present. TrueSamples do not require splitting or compositing. TrueResidual Chlorine Checked. Eurofins Raleigh Page 17 of 17 6/24/2024 1 2 3 4 5 6 7 8 9 10 11 12 13 14