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Home My WebLink AboutNCG080626_DMR and Lab Data_20240202 k January 30, 2024 APEX yO� a�aFb NC DEMLR Mooresville Regional Office oP ems"<R 610 East Center Avenue, Suite 301 9i�oaic�o Mooresville, NC 28115 RE: NCG 080000 Discharge Monitoring Report Southeastern Freight Lines—HIC 3065 Kelly Boulevard Claremont, North Carolina 28610 Permit No. NCGO80626 To whom it may concern: Apex Companies, LLC (Apex) has prepared the attached Discharge Monitoring Report (DMR) on behalf of Southeastern Freight Lines for samples collected at the above referenced facility in Q4 2023. Samples were collected for pH, Total Suspended Solids, and Oil & Grease analysis. Analysis of samples collected indicated no exceedances of benchmark values. A copy of the DMRs is included as Attachments 1 8r 2. The laboratory report has been included as Attachment 3, and a photo log showing the pH measurement for these samples has been included as Attachment 4. Apex understands that NC DEMLR has implemented electronic reporting systems and DMRs are to be submitted via these systems. Earlier this month, Apex coordinated with Southeastern Freight Lines to register with NC eDMR and Southeastern Freight Lines has submitted the applicable eDMR registration forms to DEMLR. Registration for this facility is still pending, therefore Apex has prepared a hard-copy DMR to ensure that DEMLR has been provided with monitoring reports as required per the permit. If you have any questions regarding this matter, please contact Apex at(813) 248-8558. Sincerely, Apex Companies, LLC Josh McClintic Engineer 2 Attachments: Attachment 1 — Outfall 1 DMR Attachment 2—Outfall 2 DMR Attachment 3—Laboratory Report Attachment 4— Photo Log Apex Companies,LLC-5909 Breckenridge Pkwy,Suite E Tampa,FL 33610.T 813.248.8558-ApexCos.com Discharge Monitoring Report—NCG080626 January 30, 2024 Southeastern Freight Lines—HIC Page 2 Attachment 1 Outfall 1 DMR Apex Companies,LLC 5909 Breckenridge Pkwy,Suite E-Tampa,FL 33610-T 813,248.8558 ApexCos.com PERMITTEENANIVADDRESS (Indude Fadlity Namerl tionif Different) NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM (NPOES) Form Approved DISCHARGE MONITORING REPORT (DMR) ONE No.2U4 000,1 NAME Southeastem Freight Lines NCGO80626 2023-04-01 ADDRESS 462+Reegt3n•Brlvet{'(.t;Do.JrcF'Q PERMIT NUMBER DISCHARGENUMBER GhRROR21'NC4BEg6 1 Leul+ykon5e 2-9013 MONITORING PERIOD FACILITY Southeastern Freight Lines-HIC YEAR MO DAY YEAR MO DAY LOCATION 3055 Kelly Boulevard FROM 2023 10 0t TO 2023 12 31 Claremont,NC 28610 NOTE:Read instructions before QUANTITY OR LOADING QUALITYORCONCENTRATON NO FREQUENCY SAMPLE PARAMETER EX OF AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS ANALYSIS TYPE SAMPLE 6.8 6.8 S.U. 0 1/90 grab pH PERMIT REQUIREMENT 6.0 9.0 0 1/90 grab SAMPLE <2.5 0 1/90 grab TSS PERMIT 100 mg/L 0 1/90 grab REQUIREMENT SAMPLE <1.5 mg/L 0 1/90 grab Oil St Grease PERMIT 15 0 grab REQUIREMENT 1/90 SAMPLE 0.41 1/90 Rainfall PERMIT In _ 1/90 — REQUIREMENT SAMPLE 0 gal/ 1/90 NCOIL PERMIT _ month — 1/90 REQUIREMENT SAMPLE PERMIT REQUIREMENT SAMPLE PERMIT REQUIREMENT NAMERITLE PRINCIPAL EXECUTIVE OFFICER I rend,under penalty or law Mat this document and all attachment were papered under my arecmn an TELEPHONE DATE superv¢lon In ecwMence MM aeptemdeeigned b assure Metqualifiedpemonnelproper,ge erandwwuat Me kdarmauab whmmed. Barred on my,ty by m Me peep or pa000•who mi ne>,e Maori or Moae ( � persorm nrecdy responsible mr gathenng Me tMrmabon.Me MMrmawn euemined t.M Me beat of my kno dedp �Lic'04�1 � and belied,bee,aeanm.and complete. ,am aware Mat Mere are aledficam pename•Mr•nom lies raise 76Lf )Z j�q v�j a / 3/ irmaimmor adunng me poesialSy or fine and lmpdommenl for kna.Nng vid ne abo . 810NATURE RINCIPALE%ECUTNE J a.G 2.71 TYPED OR PRINTED OFFICER OR AUTHORIZED AGENT AREA NUMBER YEAR MO DAY COMMENT AND EXPLANATION OF ANY VIOLATIONS (Reference all attachments here) EPA Form 3320-1(Rev.03-99) Previous edib'ons may be used. This is a 4-part form PAGE 1 OF 2 Discharge Monitoring Report—NCG080590 January 30, 2024 Southeastern Freight Lines—HIC Page 3 Attachment 2 Outfall 2 DMR PERMITTEENAMEIADDRESS (InGude Facility NamelLBcafionit Oillennnt) NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM (NODES) Form Approved DISCHARGE MONITORING REPORT (DMR) OMB No.2040-0004 NAME Southeastern Freight Lines NCGO80626 2023-04-02 ADDRESS 4524-Reelyalat Spi4f2c:) rtcfL. PERMIT NUMBER DISCHARGE NUMBER trL�E� C�s1�13 MONITORING PERIOD FACILITY Southeastern Freight Lines-HIC YEAR MO DAY YEAR MO DAY LOCATION 3055 Kelly Boulevard FROMI 2023 1 10 1o1 TO 1 2023 1 12 31 Claremont,NC 28610 NOTE:Read instructions before QUANTITY OR LOADING QUALITY OR CONCENTRATION NO FREQUENCY SAMPLE PARAMETER OF AVERAGEEX MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS ANALYSIS TYPE SAMPLE 7.0 7.0 0 1/90 grab pH PERMIT S•U• 6.0 9•0 0 1/90 grab REQUIREMENT SAMPLE <2.5 0 1/90 grab TSS PERMIT 100 mg/L 0 1/90 grab REQUIREMENT SAMPLE <1.5 mg/L 0 1/90 grab Oil & Grease PERMIT 15 0 1/90 grab REQUIREMENT Rainfall SAMPLE 0.41 - 1/90 - PERMIT to 1/90 REQUIREMENT SAMPLE 0 gal/ - 1/90 - NCOIL PERMIT - month - 1/90 - REQUIREMENT SAMPLE PERMIT REQUIREMENT SAMPLE PERMIT REQUIREMENT NAMEITQLE PRINCIPAL EXECUTIVE OFFICER I ready under penalty of lax mat mu aoamem and an anechmmm xem petered under my arrested or TELEPHONE BATE aup—am In accordancewrite srytem deamedloaumemtlqualifiea peladnnelpromm,emmmendevelurle me mlwmetbn aubmltled Based on my bquty of me pelaon o�persons x110 manepe Me system,or Mou /�7f pmepnef."a,reapmate and elefor complete.. Iamba4re that Marc are aronsubmilyd ormicash wfmyMWledg ] �(/} Qn ��`�� inlmmaand ltidn MWanB me posslEllltyof(neend lmpdaontmemfi(m bereerp NoleEotnaeneltles lm whmXdnp la eIONFTUR PRI L COTVE Zc�/ 3L3°26�} �� I �/ TYPED OR PRINTED OFMCER OR AUTHORI GEM AREA NUMBER YEAR M10 DAY COMMENT AND EXPLANATION OF ANY VIOLATIONS (Reference all attachments here) EPA Form 3320-1(Rev.03-99) Previous editions maybe used. This is a 4-pan form PAGE 2 OF 2 Discharge Monitoring Report—NCG080590 January 30, 2024 Southeastern Freight Lines—HIC Page 4 Attachment 3 Laboratory Report tiff eurofins 0 Environment Testing ANALYTICAL REPORT F PREPARED FOR Attn: Kevin Cooke °9ysP<� Apex Companies LLC 5900 Northwoods Business Pkwy °F Suite 5900-0 Charlotte, North Carolina 28269 Generated 12/28/2023 3:47:57 AM JOB DESCRIPTION Hickory JOB NUMBER 752-14492-1 Eurofins Raleigh • • Notes This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. I The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the methodology, with any exceptions noted. This report shall not be reproduced except in full,without the express written approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project Manager. Authorization Generated WOMA) 12/28/2023 3:47:57 AM Authorized for release by Heather Trotter,Project Manager Heather Trotter(�et.eurofinsus.mm (912)354-7858 Eurofins Savannah is a laboratory within Eurolms Environment Testing Southeast,LLC,a company within Eurofins Environment Testing Group of Companies Page 2 of 17 12/28/2023 Client:Apex Companies LLC Laboratory Job ID:752-14492-1 Project/Site: Hickory Table of Contents Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8 QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9 Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10 Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13 Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14 Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16 Eurofins Raleigh Page 3 of 17 12/28/2023 Definitions/Glossary Client:Apex Companies LLC Job ID:752-14492-1 Project/Site: Hickory Qualifiers General Chemistry Qualifier Qualifier Description `+ LCS and/or LCSD is outside acceptance limits,high biased. HF Parameter with a holding time of 15 minutes.Test performed by laboratory at client's request.Sample was analyzed outside of hold time. Glossary Abbreviation These commonly used abbreviations may or may not be present in this report. n Listed under the"D'column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio(normalized absolute difference) Dil Fac Dilution Factor OIL Detection Limit(DoD/DOE) OIL,RA,RE,IN Indicates a Dilution,Re-analysis,Re-extraction,or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration(Radiochemistry) EDL Estimated Detection Limit(Dioxin) LOD Limit of Detection(DoD/DOE) LOQ Limit of Quantitalion(DoD/DOE) MCL EPA recommended"Maximum Contaminant Level" MDA Minimum Detectable Activity(Radiochemistry) MDC Minimum Detectable Concentration(Radiochemistry) MDL Method Detection Limit ML Minimum Level(Dioxin) MPN Most Probable Number MQL Method Quantilation Limit NC Not Calculated NO Not Detected at the reporting limit(or MDL or EDL if shown) NEG Negative/Absent POS Positive/Present PQL Practical Quenlitabon Limit PRIES Presumptive QC Quality Control RER Relative Error Ratio(Radiochemistry) RL Reporting Limit or Requested Limit(Radiochemistry) RPD Relative Percent Difference,a measure of the relative difference between two points TEF Toxicity Equivalent Factor(Dioxin) TEQ Toxicity Equivalent Quotient(Dioxin) TNTC Too Numerous To Count Eurofins Raleigh Page 4 of 17 12/28/2023 Case Narrative =` ` e d N7 C " °r Job ID: 752-14492-1 Client:Apex Companies LLC q2 p i Project: Hickory P c G m.2m _, tr\ � Job ID: 752-14492-1 d�� Ourofins Raleigh Job Narrative 752-14492-1 Analytical test results meet all requirements of the associated regulatory program listed on the Accreditation/Certification Summary Page unless otherwise noted under the individual analysis. Data qualifiers are applied to indicate exceptions. Noncompliant quality control(QC)is further explained in narrative comments. Matrix QC may not be reported if insufficient sample or site-specific QC samples were not submitted. In these situations,to demonstrate precision and accuracy at a batch level,a LCS/LCSD may be performed, unless otherwise specified in the method. Surrogate and/or isotope dilution analyte recoveries(if applicable)which are outside of the QC window are confirmed unless attributed to a dilution or otherwise noted in the narrative. Regulated compliance samples(e.g.SDWA,NPDES)must comply with the associated agency requirements/permits. Receipt The samples were received on 12/11/2023 8:18 AM. Unless otherwise noted below,the samples arrived in good condition, and, where required,properly preserved and on ice. The temperature of the cooler at receipt time was 3.3°C General Chemistry Method 254OD:The laboratory control sample(LCS)for analytical batch 752-5521 recovered outside acceptance limits for Total Suspended Solids. There was insufficient sample to perform a re-extraction or re-analysis;therefore,the data have been reported. No additional analytical or quality issues were noted,other than those described above or in the Definitions/Glossary page. Eurofins Raleigh Page 5 of 17 12/28/2023 Detection Summary Client:Apex Companies LLC Job ID: 752-14492-1 Project/Site: Hickory Client Sample ID: Outfall 01 Lab Sample ID: 752-14492-1 Cnalyte Result Qualifier RL RL Unit oil Fac D Method Prep Type Temperature 19.6 HF 0.5 0.5 Celsius 1 SM 4500 H+B Total/NA pH 6.8 HF 1.0 1.0 SU i SM 4500 H+B Total/NA Client Sample ID: Outfall 02 Lab Sample ID: 752-14492-2 Analyte Result Qualifier RL RL Unit DII Fac D Method Prep Type Temperature 18.9 HF 0.5 0.5 Celsius 1 SM 4500 H+B Total/NA pH 7.0 HF 1.0 1.0 SU 1 SM 4500 H+B Total/NA This Detection Summary does not include radiochemical test results. Eurofins Raleigh Page 6 of 17 12/28/2023 Client Sample Results Client:Apex Companies LLC Job ID: 752-14492-1 Project/Site: Hickory Client Sample ID: Outfall 01 Lab Sample ID: 752-14492-1 Date Collected: 12110123 11:24 Matrix:Water Date Received:12/11/23 08:18 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed oil Fac SGT-HEM(1664B) <1.5 5.3 1.5 mg/L — 12/27/2313,54 12/2712316:24 1 Analyte Result Qualifier RL RL Unit D Prepared Analyzed oil Fac Total Suspended Solids(SM 2540D) <2.5 •+ 2.5 2.5 mg/L 12/13/23 09:38 1 Temperature(SM 4500 H+B) 19.6 HF 0.5 0.5 Celsius 12/27/23 1573 1 pH(SM 4500 H+B) 6.8 HF 1.0 1+0 SU 12/27/23 15:13 1 Client Sample ID: Outfall 02 Lab Sample ID: 752-14492-2 Date Collected:12110123 11:38 Matrix:Water Date Received:12111/23 08:18 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed oil Fac SGT-HEM(16648) <Is 5.4 1.5 mg/L 12/27/2313:54 12/2712316:24 1 Analyte Result Qualifier RL RL Unit D Prepared Analyzed oil Fac Total Suspended Solids(SM 2540D) <2.5 •+ 2.5 2.5 mg/L 12/13/23 09:38 1 Temperature(SM 4500 H+B) 18.9 HF 0.5 0.5 Celsius 12/27/23 15:13 1 pH(SM 4500 H+B) 7.0 HF 1.0 1.0 SU 12127/2315:13 1 Eurofins Raleigh Page 7 of 17 12/28/2023 QC Sample Results Client:Apex Companies LLC Job ID:752-14492-1 Project/Site: Hickory Method: 1664B - HEM and SGT-HEM Lab Sample ID: MB 680-81539711-A Client Sample ID:Method Blank Matrix:Water Prep Type:Total/NA Analysis Batch:815431 Prep Batch: 815397 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac SGT-HEM <1.4 5.0 1.4 mg/L 12/27/2313:54 12/27/2316.24 1 Lab Sample ID: LCS 680-815397/2-A Client Sample ID: Lab Control Sample Matrix:Water Prep Type:Total/NA Analysis Batch:815431 Prep Batch:815397 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits SGT-HEM 20.0 15.80 mg/L 79 64-132 Lab Sample ID: LCSD 680-815397/3-A Client Sample ID: Lab Control Sample Dup Matrix:Water Prep Type:Total/NA Analysis Batch:815431 Prep Batch:815397 Spike LCSD LCSD %Rec RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit SGT-HEM 20.0 14.80 mg/L 74 64-132 7 34 Method: SM 2540D -Solids, Total Suspended (TSS) Lab Sample ID: MB 752-5521/1 Client Sample ID:Method Blank Matrix:Water Prep Type:TotaUNA Analysis Batch: 5521 MB MB Analyte Result Qualifier RL RL Unit D Prepared Analyzed oil Fac Total Suspended Solids -2.5 2.5 2.5 mg/L 1211 312 3 0 9:38 1 Lab Sample ID: LCS 752-552112 Client Sample ID: Lab Control Sample Matrix:Water Prep Type:Total/NA Analysis Batch:5521 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Total Suspended Solids 100 130 '+ mg/L 130 80-120 Method: SM 4600 H+ B - pH Lab Sample ID:752-14492-1 DU Client Sample ID: Outfall 01 Matrix:Water Prep Type:Total/NA Analysis Batch:5669 Sample Sample DU DU RPD Analyte Result Qualifier Result Qualifier Unit D RPD Limit Temperature 19.6 HF 19.7 Celsius 0.5 pH 6.8 HF 6.8 SU 0.4 10 Eurofins Raleigh Page 8 of 17 12/28/2023 QC Association Summary Client:Apex Companies LLC Job ID:752-14492-1 Project/Site:Hickory General Chemistry Analysis Batch: 55211 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 752-14492-1 Outfall 01 Total/NA Water SM 2540D 752-14492-2 Outfall 02 Total/NA Water SM 2540D MB 752-5521/1 Method Blank Total/NA Water SM 25400 LCS 752-5521/2 Lab Control Sample Total/NA Water SM 2540D Analysis Batch: 5669 Lab Sample to Client Sample ID Prep Type Matrix Method Prep Batch 752-14492-1 Outfall 01 Total/NA Water SM 45o0 H+B 752-14492-2 Outfall 02 Total/NA Water SM 4500 H+B LCS 752-5669/2 Lab Control Sample Total/NA Water SM 4500 H+B 752-14492-1 DU Outfall 01 Total/NA Water SM 4500 H+B Prep Batch:815397 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 752-14492-1 Ouvall 01 Total/NA Water 1664B 752-14492-2 Outfall 02 Total/NA Water 16648 MB 680-81539711-A Method Blank Total/NA Water 16648 LCS 680-815397/2-A Lab Control Sample Total/NA Water 1664E LCSD 680-815397/3-A Lab Control Sample cup Total/NA Water 1664B Analysis Batch: 815431 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 752-14492-1 Outfall 01 Total/NA Water 166413 815397 752-14492-2 Outfall 02 Total/NA Water 1664B 815397 MB 680-815397/1-A Method Blank Total/NA Water 1664E 815397 LCS 680.815397/2-A Lab Control Sample Total/NA Water 1664E 815397 LCSD 680-81539713-A Lab Control Sample Dup Total/NA Water 1664B 815397 Eurofins Raleigh Page 9 of 17 12/28/2023 Lab Chronicle i _ Client:Apex Companies LLC Job ID:752-14492-1 Project/Site: Hickory Client Sample ID: Outfall 01 Lab Sample ID: 752-14492-1 Date Collected: 1 211 0/23 11:24 Matrix:Water Date Received:12111/23 08:18 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number Analyst Lab or Analyzed Total/NA Prep 1664E 815397 TD EET SAV 12/27/23 13:54 Total/NA Analysis 1664B 1 815431 TD EET SAV 12/27/2316:24 Total/NA Analysis SM 2540D 1 5521 CB EET ESC 12/13/2309:38 Total/NA Analysis SM 4500 H+B 1 5669 ME EET ESC 12/27/23 15:13 Client Sample ID: Outfall 02 Lab Sample ID: 752-14492.2 Date Collected:1211012311:38 Matrix:Water Date Received: 12/11/23 08:18 `• Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number Analyst Lab or Analyzed Total/NA Prep 1664B 815397 TD EET SAV 12/27/2313:54 Total/NA Analysis 1664E 1 815431 TD EET SAV 1212712316:24 Total/NA Analysis SM 2540D 1 5521 CB EET ESC 12/13/23 09:38 Total/NA Analysis SM 4500 H+B 1 5669 ME EET ESC 12/27/23 15:13 Laboratory References: EET ESC=Eurofins Raleigh,102-A Woodwinds Industrial Court,Cary,NC 27511,TEL(919)677-1669 EET SAV=Eurofins Savannah,5102 LaRoche Avenue,Savannah,GA 31404,TEL(912)354-7858 Eurofins Raleigh Page 10 of 17 12/28/2023 Accreditation/Certification Summary Client:Apex Companies LLC Job ID:752-14492-1 Project/Site: Hickory Laboratory: Eurofins Raleigh Unless otherwise noted,all analytes for this laboratory were covered under each accreditation/certification below. Authority Program Identification Number Expiration Date North Carolina(WW/SW) State 591 12-31-23 The following analytes are included in this report,butthe laboratory is not certified by the governing authority. This list may include analytes for which the agency does not offer certification. Analysis Method Prep Method Matrix Analyte SM 4500 H+6 Water Temperature Laboratory: Eurofins Savannah The accredhations/certifications listed below are applicable to this report. Authority Program Identification Number Expiration Date North Carolina(WW/SW) State 269 12-31-23 Eurofins Raleigh Page 11 of 17 12/28/2023 Method Summary Client:Apex Companies LLC Job ID:752-14492-1 Project/Site: Hickory Method Method Description Protocol Laboratory 1664E HEM and SGT-HEM 1664B EET SAV SM 2540D Solids,Total Suspended(TSS) SM EET ESC SM 4500 H+B pH SM EET ESC 1664E HEM and SGT-HEM (Aqueous) 1664E EET SAV I _ Protocol References: 1664B=EPA-821-98-002 SM="Standard Methods For The Examination Of Water And Wastewater' Laboratory References: EET ESC=Eurofins Raleigh,102-A Woodwinds Industrial Court,Cary,NC 27511.TEL(919)677-1669 EET SAV=Eurofins Savannah,5102 LaRoche Avenue,Savannah,GA 31404,TEL(912)354-7858 I Eurofins Raleigh Page 12 of 17 12/28/2023 Sample Summary Client:Apex Companies LLC Job ID:752-14492-1 Project/Site: Hickory Lab Sample 10 Client Sample to Matrix Collected Received 752-14492-1 Outfall 01 Water 12/1012311:24 12/11/2308:18 752-14492-2 Outfall 02 Water 12/10/2311:38 12/11/2308:18 C Eurofins Raleigh Page 13 of 17 12/28/20 g3 Eurofins Raleigh 102-AwoodMnds IndusbW Court Chain of Custody Record eurofins Cary NC27511 Environment Toting Phone:919-M 16M 1 1�C7t Client Information "TOIWA, A, lac Pec aaNn r'*uv^s No(sY GOCN1: 1 Gaines,Pmanda 752-11 4 7 4 3 24 4.1 uwC Ppv.: cc.nn amai Sute of Peat Kevin Cooke ��ptl 19-3 amaMa,gaines®eteumfingue,com Paget of GompeNy PwsIG: ba Apex Companies LLC Analysis Requested Addesa: D.pas.Rp W: 'i Preservation Codes: 5900 NorftvDWs Business Pkwy Suite Sato-o A Ha M Cay. TAT Raqueabd ms,y 6 NaOH N Na. Charlotte C Lf Amtrb P Ne20aa SUM,as D f0tft d G Neros NC,28269 CempOa.Prole Ay. A" E N.H R N229Y03 a. F MWH a H2SO4 G A r 980474-4220(Tel) Purchase Order not required H As Gmid T TSPobeeanyenne Em t MM I IM U Acsroro V KaJin.COpke@ep IaxCOS.COm s_ K EDI.A J 01 w*w W pH off dd Pm)ect Name: ReMne. R L EM Y 7d Hickory 752M78 e A 752-14492 COC z ° fv..M F SL'Fl- - hyd Apt .A.0 saoWe other� a Zsbb tW2 ple Mabbt e 1Z ynp, o...saSam le Identifleation Sam le Dateab eM1r1s..AWS lei InstructlonsMofl: y(`64-sm_�H L• -ttL water0 1\(1 IAM J_F4t_ ( ,� b2jwater Calfwateruw.�2(GZ N`I�_ NN to Dt OU -24at, -ASS t Possible HaerdlrlendAcaeon SaI-m—pIle Dfaposal(Afae maybe Hsamples are reteinedlomld then lmorrtb) M Non-Hazard M Flammable �Sldn IMUnt C]Poisons �Unimown CO Radrpl "Return To Client Disposal Leb 7 Amh(ve For Months Deliverable Requested:1 II III,N Other(specify) Special InsbuctionvOC Requirements: Empty Kit Relinquished by Date: Time: I Iswtbae of M*Mw RMbqubaW by Detdrene: Compsm Compem CIA, jovlzI,hj Vier Cr ce i ll 23 ReNtrgNaned ty. m./flma RecNved bv: paE✓iNNe: cempam N N Rebq�Ybd by 0a1dtNNe Campem ReeaNWq DamTrt.: Comvm N O Custody Sealslmact Custody Seal Na ��prt p Cooler Tempendu")CarAOtlNar Renadu: 211 r 'i w b Yes b No �Wl lCZ :l �I t- C'7"---j 3 7 "0610812011 Eurofins Raleigh rAe• 102-A WooCeinds IndusMal Court ;j eurofins Cary NC 27511 Chain of Custody Record Enalmnment Testing Phony.919.6"1669 smpM- Lab Pw: 4rtbrTxwng NO(a): COC NO: Client Information Sub Contract Lab Gaines,Amanda 75z-19971 Shipp riXt PAab: E-maa: abm WOaroU Page: SNppirglRecMing amanda.gaines®aLeumBnsus.mm North Carolina page 1 of 1 Cbnpn/. 'a Re*e (aae nay.): e: Eu Ains Environment Testing Southeast, Stale North Cerolina(WWfSW) 752-14492.1 Adeetc Owe Me Reawealed: P16 rnmee Codes: 5102 LaRoche Avenue, 1227t2023 Analysis Requested IF CL 1eGM. TAT RKw (dryah m0H HSBwannah I.=.i n Attd4 P 14 2bAdSGaA,3� R Ha Ca aOH a912,35s-7858Rep 912-352-01S5(FU) � T iSP DOdehVaR WNer VFrole4 Wma: PrgeA DTA W gApes Companies 75202378M 2 °tl1°`(°P°�Ir 3� 6 SaMatrix T Sample ccSam IeldamMeation CliiemlD bID Sam Ie Date Time GS sew lnstruetioarmote: outfen 01(752-14492-1) 12=23 11:24 water x Outfag 02(76ZI4492.2) iviw 3 11.38 Water x raftm Hob:fwnw bbwretmyxvadvgav an aWJegmClbMe.EbOr ErM,OmbnlTaalYq Seumeor,liF wOO.eeanaYYF of R4e,Od.aNa'baa0ve6btlon wrimearrn awn ov.i0cmo-atxmen.44w.'ma HinDb NlPnanie krabdeeuMerdWnoMabOy.atlb 4bbamry dove mI t+drMOy mebmin emedb6M meb Bob W 04gb Whd abcn IOfineF/1SIlnblmatrbbong arbyuw.me aelryba nvrtbe r1,4ge0 Wtl,m eb Eam4m Emlronnba Taaa,g SWdbut. Iabam,YMOrbrimbadav wTlOewoHded.Ama»rdes b aaaeNttlim soon ebaleae OroyMb Euorm BrdtbvneMTaWfq 9oumaert tLDalbnEen Rbmdlnat/.H ae�e0uamd wxmurbb w bmeidb dY9,bwvn4,e elaMd cmm of Wmdy aau0iq 10 aN0 ox npnarxa m EWMna EmawbienlTedmg 8oWeaet LLG PoselbleltmardidendNoaaon Sam Is Disposel(A fxmaybeassaa ;fsa.piesanreWnediongw Man l month) UnCongnned nRe(um ro Caen Dispose/ Leb AMMe For monthe Deliverable Requested:I,II,ill,N Other fspecly) Ptlmary,Deliverable Rank 2 Special InsKILtions/OCIRequirements. Empty YOl Relinquished by Date Time: Mesiba oisabnbwt Rare qubMd GunDaM RaoeM1aO / me� � + C....J DomP RNtrWiPaM ry. a oOr01u0' aeuheeK camv.m RNm4uaMd M. OaMbb: ngbwan RadaeO by Date/rwrir. (?anOariY CusWdy SOTNIAtaet Cuatgdy Seal No. CoderTempebb+efa)°C anb OlMrRemeda: e vas o v..rwnanm Page 15 of 17 12/28/2023 Login Sample Receipt Checklist Client:Apex Companies LLC Job Number:752-14492-1 Login Number:14492 List Source:Eurofins Raleigh List Number:1 Creator:Yonish,Rachel Question Answer Comment Radioactivity wasn't checked or is</=background as measured by a survey True meter. The cooler's custody seal,if present,is intact. True Sample custody seals,if present,are intact. True The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Samplers name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time(excluding tests with immediate True m HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. True There is sufficient vol.for all requested analyses,incl.any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is True <6mm(1/4"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. True Eurofins Raleigh Page 16 of 17 12/28/2023 Login Sample Receipt Checklist Client:Apex Companies LLC Job Number:752-14492-1 Login Number:14492 List Source:Eurofins Savannah List Number:2 List Creation:12/12/23 01:34 PM Creator:Harley,Tynisha Question Answer Comment Radioactivity wasn't checked or is</=background as measured by a survey N/A meter. The cooler's custody seal,if present,is intact. True Sample custody seals,if present,are intact. True The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COG is present. True COG is filled out in ink and legible. True COG is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COG. True Samples are received within Holding Time(excluding tests with immediate True HTs) \� Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. NIA There is sufficient vol.for all requested analyses,Incl.any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is N/A <6mm(1/4'). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. N/A Eurofins Raleigh Page 17 of 17 12128/2O23 Discharge Monitoring Report—NCGO80590 January 30, 2024 Southeastern Freight Lines—HIC Page 5 Attachment 4 Photo Log Site Photographs - 12/10/2023 3055 Kelly Blvd Claremont , NC 28610 Photograph 1 _ Description: Outfa 1101 MI1IN Photograph; 2 Description: Outfal101 ti w.. � -- ^^^^ i11111119 Photograph 3 Description: Outfa 1101 �:" � EIIIIIIIR APEX Site Photographs - 12/10/2023 3055 Kelly Blvd Claremont, NC 28610 Photograph, 4 Description: Outfa I102 -- ._ ..a. nmeie Photograph, 5 Description: Outfa I IO2 MOW: IIIIIIIIR Photograph, 6 Description: OutfaII02 c i 1 y t .4d UNION APEX