WQ0041666_Modification_20240522

Initial Review
Reviewer nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
Permit Number (IR) * WQ0041666
Applicant/Permittee EMA Resources, Inc.
Applicant/Permittee Address 755 Yadkinville Rd, Mocksville, NC 27028
Is the owner in BIMS? Yes No Is the facility in BIMS?
Owner Type
Facility Name
County
Fee Category Major
Is this a complete application?*
Yes No
Signature Authority
Signature Authority Title
Signature Authority Email
Document Type (if non -application)
Email Notifications
Organization
EMA Resources Class A Residuals Program
Wilkes
Does this need review by the hydrogeologist? * Yes No
Regional Office
CO Reviewer
Admin Reviewer
Fee Amount
Complete App Date
05/22/2024
Yes No
$528
Below list any additional email address that need notification about a new project.
Email Address
Comments to be added to email notfication
Comments for Admin
Comments for RO

Comments for Reviewer
Comments for Applicant

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Brent Collins
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
3363993646
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0041666
Has Current Existing permit number
Applicant/Permittee*
EMA Resources Inc.
Applicant/Permittee Address*
755 Yadkinville Rd, Mocksville, NC 27028
Facility Name*
EMA Resources Class A Residuals Program
Please provide comments/notes on your current submittal below.
Re -submitting as the first check that was sent was for the wrong amount.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
EMA Resources Permit Modification - WQ0041666.pdf 9.35MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date
fftafe&lala rd
5/17/2024

Division of Water Resources
Water Quality Permitting Section
Non -Discharge Permitting Unit
1617 Mail Services Center
Raleigh, NC 27699-1617
RE: Permit Modification — WQ0041666
To Whom it May Concern:
EMA Resources is submitting the included permit modification for the EMA Resources
Inc. — DCAR Permit WQ0041666. We are asking to have the City of Durham — Brown
WTP Facilities' dry tons increased from 1500 to 2500. During 2023, we land applied
more than anticipated and this increase should account for any increases in production. A
check for $348.00 is being mailed today along with the submission confirmation.
If you have any questions concerning this modification, please contact Brent Collins —
Director of Technical Services
Z_de
Director of Technical Services
brcnt,(11oH�ns(
[phone]
Phone 336o75191441 — Fax [phone]
755 Yadkinville Rd — Mocksville, NC 27028

I=
Prepared. By-
EMA Resources Inc.
755 Yadkinville Road
Mocksville, NC 27028
336-751-1441
April 17'h,2024
Phone 336o75191441 — Fax [phone]
755 Yadkinville Road — Mocksville, NC 27028

ROY COOFIER
Governor
ELIZABE'lli S, BISER
See'relaq
S. DANIEL SMUTI-i
Dh ector
ERfK BLANKENS111P— PRESIDENT
EMA RESOURCES, INC.
755 YADKINVILLE ROAD
MOCKSVILLE, NORTH CAROUNA 27028
Dear Mr. Blankenship:
t4ORIH CAROUIN�A
E'nidrommenralQuality,
Subject: Ise it No. WQ0041666
EMA Resources Class A
Residuals Program
Attachment A Certification
Davie County
In accordance with your pennit major modification request received December 22, 2021, we are
forwarding herewith a modified Attachment A certified March 10, 2022, to EMA Resources, Inc. for the
subject residuals management program.
Modifications to the subject Attachment are as follows: Addition of the Wade G. Brown WTI
(NC0332010 — P01) as an approved residuals source with a pennitted dry tonnage of 1,500 dry tons per
year (DT/yr).
The modified Attachment A shall be effective from the date of certification until January 31, 2027
(i.e., expiration date of the current pennit), shall void Attachment A of Ise it No. WQ0041666 issued July
16, 2020 that was previously certified on March 25, 2021, and shall be subject to the conditions and
limitations as specified therein, as well as those specified in the above -referenced pennit. Please replace
Attachment A of Ise it No. WQ0041666 that was certified on March 25, 2021 with the modified
Attachment A. Please note that the Permittee shall submit a renewal application no later than August
4,2026.
If any parts, requirements or limitations contained in this certification are unacceptable, the
Pennittee has the right to request an adjudicatory hearing upon written request within 30 days following
receipt of this pennit. This request shall be in the fonu of a written petition, conforming to Chapter 150B
of the North Carolina General Statutes, and filed with the Office of Administrative Hearings at 6714 Mail
Service Center, Raleigh, NC 27699-6714. Otherwise, this certification shall be final and binding.
If you need any additional infonnation concerning this matter, please contact Erick Saunders at
[phone] or p.(den rgi„v.
' e�1111
Lest
S. Daniel Smith, Director
Division of Water Resources
IOV
W Wrlh Sahsbury Sirect l K:0 Mailll So Oce CeinumI Ral6gh, North (�ardUna 27699 1617
(07079000

Mr. Erik Blankenship
March 10, 2022
Page 2 of 2
cc: Durham County Health Department (Electronic Copy)
Raleigh Regional Office, Water Quality Regional Operations Section (Electronic Copy)
Winston-Salem Regional Office, Water Quality Regional Operations Section (Electronic Copy)
Brent Collins — EMA Resources, Inc. (Electronic Copy)
Laserfiche File (Electronic Copy)
Digital Permit Archive (Electronic Copy)

fflvnn�
In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as
amended, and other applicable Laws, Rules, and Regulations
PERMISSION IS HEREBY GRANTED TO
E
Davie County
operation of a residuals management program for EA Resources, Inc. and consisting of the distribution
of Class A residuals generated by the approved facility listed in Attachment A, with no discharge of wastes
to surface waters, pursuant to the application received May 5, 2020, and in conformity with other supporting
data subsequently filed and approved by the Department of Environmental Quality and considered a part
of this pennit. The disposal of residuals is regulated under Title 40 Code of Federal Regulations Part 503.
This pennit does not exempt the Pennittee from complying with Federal Regulation 40 CFR Part 503.
This pennit shall be effective from the date of issuance through January 31, 2027, and shall be subject to
the following conditions and limitations:
1. SCHEDULES
1. The Pennittee shall request renewal of this permit on Division -approved forms no Later than August 4,
2026. [15ANCAC' 02T'.0105(b),02T'.0109]
The Pennittee shall maintain and operate the subject residuals management program so there is no
discharge to surface waters, nor any contravention of groundwater or surface water standards. In the
event the residuals management program fails to perfonu satisfactorily, including the creation of
nuisance conditions due to improper operation and maintenance, the Pennittee shall immediately cease
distributing residuals, take immediate corrective actions, and contact the Winston-Salem Regional
Office supervisor. [15ANCACO2T'.0108(b)(1)(A)i
2. This permit shall not relieve the Permittee of their responsibility for damages to groundwater or surface
water resulting from the operation of this residuals management program. [ 15A NC AC 02T
.0108(b)(1)(A)i
3. Only residuals generated by the facility listed in Attachment A are approved for distribution in
accordance with this pennit. [15ANCACO2T'.1101]
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4. Pollutant concentrations in distributed residuals shall not exceed the following Ceiling Concentrations
or Monthly Average Concentrations, on a dry weight basis:
Ceiling Concentration
Monthly Average
Parameter
Concentration
(m,91W
Arsenic
75
41
Cadmium
85
39
Copper
4,300
1,500
Lead
840
300
Mercury
57
17
Molybdenum
75
N/A
Nickel
420
420
Selenium
100
100
Zinc
7,500
2,800
[15A NC AC 02T. I 105(a), 02T.1105(c)]
5. Class A biological residuals shall meet the pathogen reduction requirements in 15A NC AC 02T
.1 106(a). Exemptions to this requirement shall be specified in Attachment A. [15A NCAC 02T
.1 106(a), 02T.1106(d) I
6. Class A biological residuals shall meet one of the vector attraction reduction alternatives in 15A NC AC
02T.1107(a). Exemptions to this requirement shall be specified in Attachment A. [15ANCACO2T
.1 107(a), 02T. I 107(c) I
7. The facilities and sites herein were permitted per the following setbacks:
a. Setbacks for Class A land application sites are as follows (all distances in feet):
Liquid Cake
Residuals Residuals
i. Each private or public water supply source:
100 100
ii. Surface waters such as intermittent and perennial streams, perennial
100 25
waterbodies, and wetlands:
in. Surface water diversions such as ephemeral streams, waterways, and
25 0
ditches:
iv. Groundwater lowering ditches where the bottom of the ditch
25 0
intersects the SHWT
v. Each well with exception of monitoring wells:
100 100
vi. Bedrock outcrops:
25 0
Unless otherwise noted in Attachment A, "cake" residuals are those that have greater than 15%
solids by weight and can be stacked without flowing, as well as can be handled, transported
and spread as a solid (e.g., using a backhoe, front end loader, stinger spreader, broadcast
spreader or other equipment designed for handling solid materials) without leaving any
significant liquid fraction behind.
[15A NC AC 02T. I 108(b) I
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H. Residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in exceedance of
agronomic rates. Appropriate agronomic rates shall be calculated using expected nitrogen requirements
based on the detennined Realistic Yield Expectations (RYE) using any of the following methods:
a. Division's pre -approved site specific historical data for specific crop or soil types by calculating
the mean of the best three yields of the last five consecutive crop harvests for each field.
b. North Carolina Historical Data for specific crop and soil types as provided by North Carolina State
University Department of Soil Science I
U _ L). A copy
shall be kept on file and reprinted every five years in accordance with Condition IV. 6.
c. If the RYE cannot be detennined using methods (a) or (b) above, the Permittee may use the RYE
and appropriate nutrient application rates reported in any of the following documents:
i. Crop management plan as outlined by the local Cooperative Extension Office, the North
Carolina Department of Agriculture and Consumer Services, the Natural Resource
Conservation Service, or other agronomist.
ii. Waste Utilization Plan as outlined by the Senate Bill 1217 Interagency Group - Guidance
Document: Chapter I
(h F --) o 100 1 09.4?Ljl).
lul ---------- -
in. Certified Nutrient Management Plan as outlined by the Natural Resources Conservation
Services (NRCS). These plans must meet the USDA-NRCS 590 Nutrient Management
Standards (11j,
d. If the RYE and appropriate nutrient application rates cannot be determined, the Permittee shall
contact the Division to determine necessary action.
[15A NCAC 02T. I 109(a)(1)(K) I
9. Prior to distributing Class A residuals that have a sodium adsorption ratio (SAR) of 10 or higher, the
Pennittee shall obtain and implement recommendations from at least one of the following: the local
Cooperative Extension Office; the Department of Agriculture and Consumer Services; the Natural
Resource Conservation Service; a North Carolina Licensed Soil Scientist or an agronomist. The
recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a
mechanism for maintaining site integrity and conditions conducive to crop growth. The Permittee shall
maintain written records of these recommendations and details of their implementation. The Permittee
shall notify third -party entities of the effects of a high SAR content residuals on their receiving sites.
[15A NC AC 02T.0108(b)(1)(A)l
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1. The Pennittee shall operate and maintain the residuals management program as a non -discharge system.
[15A NCAC 02T.1100]
2. The Pennittee shall maintain a Division -approved Operation and Maintenance Plan that shall include:
a. Description of the program, and associated facilities and equipment, in sufficient detail to show
what operations are necessary for the program to function and by who the functions are to be
conducted-,
b. Description of anticipated maintenance of facilities and equipment associated with the program-,
c. Include provisions for safety measures, including restriction of access to sites and equipment-,
d. Spill control provisions:
i. Response to upsets and bypasses including control, containment, and remediation; and
ii. Contact infonnation for plant personnel, emergency responders, and regulatory agencies-,
e. Detailed inspection procedures:
i. Names or titles of personnel responsible for conducting inspections-,
ii. Frequency and location of inspections, and procedures to assure that the selected locations and
inspection frequency are representative of the residuals management program; and
in. Description of record keeping and actions to be taken by the inspector in the event that
noncompliance is observed-,
f. Detailed sampling and monitoring procedures:
i. Names or titles of personnel responsible for conducting sampling and monitoring-,
ii. Description of monitoring procedures including parameters to be monitored" and
in. Sampling frequency and procedures to assure that representative samples are collected.
Fluctuation in temperature, flow, and other operating conditions can affect the quality of the
residuals gathered during a particular sampling event. The sampling plan shall account for any
foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to
meet pathogen and vector attraction reduction requirements.
[15A NCAC 02T. I I 10(a)]
3. Upon the Water Pollution Control System Operators Certification Commission's (WPCSOCC)
classification of the residuals management program, the Permittee shall designate and employ a
certified operator in responsible charge (ORC), and one or more certified operators as back-up ORCs.
The ORC or their back-up shall visit the facilities in accordance with 15A NCAC 08G 0204 and shall
comply with all other requirement in 15A NCAC 08G 0204. [15A NCAC 02T.0 117, 08G .0204]
4. The Pennittee shall ensure that a copy of this permit and the Division -approved Operation and
Maintenance Plan is available when land applying bulk Class A residuals. [15ANCAC 02T'.1110(b)]
5. The Pennittee shall ensure that spill control provisions are available when transporting or land applying
bulk Class A residuals. [15ANCACO2T'.1110(a)(4)]
6. Class A residuals may be staged at the land application site for up to 30 days for biological residuals
and 60 days for non -biological residuals. Class A residuals shall be stored or staged in a manner to
prevent runoff of leachate and other wastewaters generated. [15A NCAC 02T . I I I 0(c), 02T . I I I 0(d) I
7. Adequate measures shall be taken to prevent wind erosion and runoff from the bulk Class A residual
land application sites. [15A NCAC 02T'.0108(b)(1)(A)i
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H. Bulk Class A residuals shall not be land applied under the following conditions:
a. If the residuals are likely to adversely affect a threatened or endangered species listed under section
4 of the Endangered Species Act or its designated critical habitat-,
b. If the application causes nuisance conditions-,
c. Ifthe land fails to assimilate the bulk residuals orthe application causes the contravention of surface
water or groundwater standards"
d. If the land is flooded, frozen, or snow-covered, or is otherwise in a condition such that runoff of
the residuals would occur;
e. Within the 100-year flood elevation, unless the residuals are injected or incorporated within a 24-
hour period following a residuals land application event-,
f. During precipitation events, or within 24 hours following a rainfall event of 0.5 inches or greater
in a 24-hour period-,
g. If the slope of the land is greater than 10% when liquid residuals are surface applied, or if the slope
of the land is greater than 18% when liquid residuals are injected or incorporated-,
h. If the land does not have an established vegetative cover crop unless the land is a Division -approved
no -till site, or the residuals are injected, or incorporated within a 24-hour period following the
application of residuals-,
i. If the vertical separation of the seasonal high water table and the depth of residuals application is
less than one foot-,
J . If the vertical separation of the depth to bedrock and the depth of residuals application is less than
one foot-,
k. If the application exceeds agronomic rates; or
L If the land application sites are located within a DVS -I watershed pursuant to 15A NCAC 0213.0212
or within the Critical Area of a WS-II pursuant to Sub -Item (4)(g) of Rule 15A NCAC 02B .0212,
or within the Critical Area of a WS-111 or S-IV watershed pursuant to Sub -Item (4)(h) of Rules
15A NC AC 02B.0215, and.0216.
15A NCAC 02T. I 109(a)(1), 02T. I 109(b)
9. The Pennittee shall notify all third -party entities receiving bulk Class A residuals that land application
activities occurring on the third-party's property shall meet the requirements in 15A NCAC 02T
.1108(b) and 02T .1109(a)(1) (i.e., Conditions 11.7.a. and 111.8., respectively). [15A NCAC 02T
.1103 (a)(4), 02T. 1103 (a)(5)]
10. Bagged or other container Class A residuals shall have an affixed label or an information sheet provided
to the person receiving the Class A residuals. The label or information sheet shall contain the following:
a. The name and address of the person who prepared the residuals-,
b. A statement that residual land application is prohibited except in accordance with the instructions
on the label or infonnation sheet-,
c. A statement that the residuals shall be applied at agronomic rates and recommended rates for its
intended use.
15A NCAC 02T. I 109(c)
11. The Pennittee shall not distribute bulk Class A residuals to any person or entity known to be applying
residuals contrary to the conditions of this permit. The Pennittee shall report to the Winston-Salem
Regional Office any person or entity known to be applying residuals contrary to the conditions of this
pennit. [15A NCAC 02T.0 108(b)(1)(A) I
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The Pennittee shall conduct and report any Division required monitoring necessary to evaluate this
program's impact on groundwater and surface water. [15ANCACO2T'.0108(c)]
2. The residuals from each source generating facility shall be analyzed to demonstrate they are non-
hazardous under the Resource Conservation and Recovery Act (RCRA). Residuals that test or are
classified as a hazardous or toxic waste under 40 CFR Part 261 shall not be land applied. The analyses
(i.e., corrosivity, ignitability, reactivity, and toxicity characteristic leaching procedure (T'CLP)) shall be
performed at the frequency specified in Attachment A, and the Pennittee shall maintain these results
for five years. Any exemptions from the requirements in this condition shall be specified in Attachment
A. The TCLP analysis shall include the following parameters, and the Federal regulatory level (mg/L)
is in parentheses:
Arsenic (5.0) 1,4-Dichlorobenzene (7.5) Nitrobenzene (2.0)
Barium (100.0) 1,2-Dichloroethane (0.5) Pentachlorophenol (100.0)
Benzene (0.5) I,I-Dichloroethylene (0.7) Pyridine (5.0)
Cadmium (1.0) 2,4-Dinitrotoluene (0.13) Selenium (1.0)
Carbon tetrachloride (0.5) Endrin (0.02) Silver (5.0)
Heptachlor (and its epoxide)
Chlordane (0.03) Tetrachloroethylene (0.7)
Chlorobenzene (100.0) Flexachlorobenzene (0.13) Toxaphene (0.5)
Chloroform (6.0) Flexachlorobutadiene (0.5) Trichloroethylene (0.5)
Chromium (5.0) Flexachloroethane (3.0) 2,4,5-T'richlorophenol (400.0)
m-Cresol (200.0) Lead (5.0) 2,4,6-T'ri chi orophenol (2.0)
o-Cresol (200.0) Lindane (0.4) 2,4,5-T'P (Silvex) (1.0)
p-Cresol (200.0) Mercury (0.2) Vinyl chloride (0.2)
Cresol (200.0) Methoxychlor (10.0)
2,4-D (10.0) Methyl ethyl ketone (200.0)
Once the residuals have been monitored for two years at the frequency specified in Attachment A, the
Pennittee may submit a permit modification request to reduce the frequency of this monitoring
requirement. In no case shall the monitoring frequency be less than once per pennit cycle.
[15A NCAC 13A .0 102(b), 02T. 110 1, 02T .11051
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3. The residuals from each source generating facility shall be analyzed at the frequency specified in
Attachment A, and the Pennittee shall maintain the results for a minimum of five years. Each analysis
shall include the following parameters:
Aluminum
Mercury
Potassium
Ammonia -Nitrogen
Molybdenum
Selenium
Arsenic
Nickel
Sodium
Cadmium
Nitrate -Nitrite Nitrogen
SodiuAdsorption Ratiom
(SCR)
Calcium
Percent Total Solids
TKN
Copper
pH
Zinc
Lead
Phosphorus
Magnesium
Plant Available Nitrogen
(by calculation)
15A NCAC 02T.I101]
4. Residuals shall be monitored for compliance with pathogen and vector attraction reduction
requirements at the frequency specified in Attachment A. The monitoring results shall specify the
stabilization process utilized, and demonstrate compliance with the Class A pathogen reduction
requirements in 15A NC AC 02T .1 106(a), and one vector attraction reduction requirement in 15A
NCAC 02T .1 107(a) shall be met. Any exemptions from the requirements in this condition shall be
specified in Attachment A. [15ANCACO2T'.1106(a),02T'.1107(a),02T'.1111(c)I
5. Representative samples of residuals that are prepared for distribution shall be collected and analyzed.
[15A NC AC 02T. I I I l(a)]
6. The Pennittee shall maintain records for all bulk Class A residual distribution events. These records
shall include the following:
a. Residuals source (as listed in Attachment A),-
b. Date of distribution-,
c. Name and address of residuals recipient-,
d. Volume of residuals distributed toeach recipient; and
e. Intended use of residuals.
[15A NC AC 02T'.0108(c)]
7. One hard copy and one electronic copy of an annual report shall be submitted on or before March I".
The annual report shall meet the requirements described in the Instructions for Residuals Application
AnnualReportingForms. Instructions for reporting and annual report forins are available at
h
n �iUre io �ai ng: 16 rni s, or can be obtained by contacting the Ion -Discharge Branch
directly. The annual report shall be submitted to the following address:
Division of Water Resources
Inforination Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
15A NC AC 02T. I I I I (d) I
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H. Noncompliance Notification
The Pennittee shall report to the Winston-Salem Regional Office, telephone number [phone],
within 24 hours of first knowledge of the:
a. Any process unit failure (e.g., mechanical, electrical, etc.) rendering the facility incapable of
adequate residual treatment.
b. Any failure resulting in a discharge to surface waters.
c. Any time self -monitoring indicates the program has gone out of compliance with its permit
limitations.
d. Distribution of residuals abrionnal in quantity or characteristic.
e. Any discharge from a vehicle or piping system transporting residuals.
Emeroencies requiring reporting outside normal business hours shall call the Division's Emergency
tn tn
Response personnel at telephone number [phone], [phone], or [phone]. All
noncompliance notifications shall file a written report to the Winston-Salem Regional Office within
five days of first knowledge of the occurrence, and this report shall outline the actions proposed or
taken to ensure the problem does not recur. [15ANCACO2T'.0108(b)(1)(A)i
V. INSPECTIONS
1. The Pennittee shall perforin inspections and maintenance to ensure proper operation of the Pertnittee's
storage and distribution facilities. [15ANCACO2'1'.1110(f)]
2. The Pennittee shall inspect the Pernuttee's residuals processing, storage, and transport facilities to
prevent malfunctions, facility deterioration, and operator errors that may result in discharges of wastes
to the environment, threats to human health, or public nuisances. The Pennittee shall maintain an
inspection log that includes the date and time of inspection, observations made, and maintenance,
repairs, or corrective actions taken. The Pennittee shall maintain this inspection log for a period of five
years from the date of inspection, and this log shall be made available to the Division upon request.
[15A NCAC 02T.0108(b)(1)(A), 02T. 11 10(f)]
3. Division authorized representatives may, upon presentation of credentials, enter and inspect any
property, premises, or place related to the distribution sites or facilities permitted herein at any
reasonable time for detennining compliance with this permit. Division authorized representatives may
inspect or copy records maintained under the to and conditions of this pennit, and may collect
groundwater, surface water, or leachate samples. [G.S. 143-215.3(a)(2)]
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MONO
I . Failure to comply with the conditions and limitations contained herein may subject the Pennittee to a
Division enforcement action. [G.S. 143-215.6A, 143-215.613, 143-215.6C]
2. This pennit is effective only with respect to the nature and volume of wastes described in the permit
application, and Division -approved plans and specifications. [G.S. 143-215. l(d)]
3. Unless specifically requested and approved in this permit, there are no variances to administrative codes
or general statutes governing the construction or operation of the facilities permitted herein. [15A
NCAC 02T'.0105(n)]
4. The issuance of this permit does not exempt the Permittee from complying with all statutes, rules,
regulations, or ordinances that other jurisdictional government agencies (e.g., local, state, and federal)
may require. [15ANCACO2T'.0105(c)(6)]
If the permitted residuals program change ownership, or the Permittee changes their name, the
Pennittee shall submit a pennit modification request on Division -approved forms. The Permittee shall
comply with all to and conditions of this permit until the pennit is transferred to the successor -
owner. [G.S. 143-215.1(d3)]
6. This permit is subject to revocation or modification upon 60-day notice from the Division Director, in
whole or part for:
a. violation of any terms or conditions of this pennit or Administrative Code Title 15A Subchapter
02T',-
b. obtaining ape nnitby misrepresentation or failure to disclose all relevant facts-,
c. the Perin ittee's refusal to allow authorized Department employees upon presentation of'credentials:
i. to enter the Permittee's premises where a system is located or where any records are required
to be kept;
it. to have access to any permit required documents and records-,
in. to inspect any monitoring equipment or method as required in this pennit'- or
iv. to sample any pollutants-,
d. the Pertnittee's failure to pay the annual flee for administering and compliance monitoring; or
e. a Division determination that the conditions of this permit are in conflict with North Carolina
Administrative Code or General Statutes.
[15A NCAC 02T.01 10]
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7. Unless the Division Director grants a variance, expansion of the facilities pennitted herein shall not
occur if any of the following apply:
a. The Pennittee or any parent, subsidiary, or other affiliate of the Pennittee has been convicted of
environmental crimes under G.S. 143-215.613, or under Federal law that would otherwise be
prosecuted under G.S. 143-215.613, and all appeals of this conviction have been abandoned or
exhausted.
b. The Pennittee or any parent, subsidiary, or other affiliate of the Permittee has previously abandoned
a wastewater treatment facility without properly closing the facility.
c. The Pennittee or any parent, subsidiary, or other affiliate of the Pennittee has not paid a civil
penalty, and all appeals of this penalty have been abandoned or exhausted.
d. The Pennittee or any parent, subsidiary, or other affiliate of the Permittee is currently not compliant
with any compliance schedule in a permit, settlement agreement, or order.
e. The Pennittee or any parent, subsidiary, or other affiliate of the Pennittee has not paid an annual
fee.
15A NC AC 02T. 0 120(b), 02T.0120(d)]
H. This permit shall not be renewed if the Pennittee or any affiliation has not paid the required annual fee.
[15A NC AC 02T. 0 120(c) I
Kermit issued this the 16 1h day of July 2020
NORTH CAROLINA ENVIRONMENTAL MANAGEMESIT COMMIS SION
­7
S. Daniel Smith, Director
Division of Water Resources
By Authority of the Environmental Management Commission
Permit Number WQ0041666
WQ0041666 Version 1.0 Shefl Version 200201 Page 10 of 10

IZOY COOPEIZ
Govemoe
DIONNE DE]AA-GATTI
Secrelat y
S. DANIEL. SMITH
D�recror
EmK BiANKENSHIP - PRESIDENT
EMA RESOURCES, INC.
755 YADK INVILLE Rom)
MOCKSVILLE, Noin'ij CAiwuNA 27028
Dear Mr. Blankenship:
P40RTH CARU INA
Env ironmenatal Qualfty
Subject: Ise it No. WQ0041666
EMA Resources DC AR
Attachment A Certification
Davie County
In accordance with your pennit major modification request received February 25, 2021, we are
forwarding herewith a modified Attachment A certified March 25, 2021, to EMA Resources, Inc. for the
subject residuals management program.
Modifications to the subject Attachment are as follows: Addition of the John J. Ili W`1'P (Permit
No. NC0087866) as a residuals source, with an approved dry tonnage of 1,035 dry tons/yr (DT/yr).
The modified Attachment A shall be effective from the date of certification until January 31,
2027 (i.e., expiration date of the current permit), shall void Attachment A of he it No. WQ0041666
issued July 16, 2020, and shall be subject to the conditions and limitations as specified therein, as well as
those specified in the above -referenced pennit. Please replace Attachment A of Ise it No. WQ0041666
that was issued July 16, 2020 with the modified Attachment A. Please note that the Permittee shall
submit a renewal application no later than August 4, 2026.
If any parts, requirements or limitations contained in this certification are unacceptable, the
Pennittee has the right to request an adjudicatory hearing upon written request within 30 days following
receipt of this pennit. This request shall be in the form of a written petition, conforining to Chapter 150B
of the North Carolina General Statutes, and filed with the Office of Administrative Hearings at 6714 Mail
Service Center, Raleigh, NC 27699-6714. Otherwise, this certification shall be final and binding.
If you need any additional inforination concerning this matter, please contact Erick Saunders at
[phone] or
S. Daniel Smith, Director
Division of Water Resources J,
cc: Davie County Health Department (Electronic Copy)
Randolph County Health Department (Electronic Copy)
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State of North Carolina
e epart Dmnt ®f Environmental Quality
,)WR Division of Water Resources
Division, of Water Resources 15A NCAC 02T.1 100 — DISTRIBUTION OF CLASS A RESIDUALS
FORM: DCAR 06-16
I. APPLICANT INFORMATION:
1. Applicant's name: EMA Resources Inc.
Applicant type: El Individual E Corporation E] General partnership El Privately -Owned public Utility
E] Federal [_1 State E] Municipal E] County
Signature authority's name per 15A NCA C 021' 0 106: Erik LflankcnshiR Title: president
Applicant's mailing address: 755 Yadkinville Rd
City: Mocksville State: NC Zip: 27028-
'I'elephone number: [phone] Email Address: erik.blankeiisliin()ei-ntresourcesine.com
2. Consultant's name: License Number (for P.E.):
Affiliation: El On Staff El Retained (Finn:
Consultant's mailing address:
City: — State: Zip:
'I'elephone number: Email Address:
3. Fee submitted: $348 (See Instruction B)
1. Application is for (check all that apply): [:] new, 0 modified, n renewed pen -nit
2. Ifthis application is being submitted to renew or modify in existing pen -nit, provide the following:
Pennit number: WQ0041 000
Date of host -recently issued permit: 11/15/2022
Date of host -recently certified Attachment A (if different than the pen -nit): 11/15/2022
III. FACILITY INFORMATION:
1. Name of'residuals processing facility: Wade G. Brown WIT
City: Durham
Coordinates: Latitude: 36" 05' 29"
Datum: NAD83
Method of'measurement: GPS
State: NC Zip: 27701
Longitude: 78-'52'21 "
Level of accuracy: nearest second
County where facility is located: Durham
2. Facility contact (person familiar with residuals preparation):
Name: 'I'om Lucas Title: WIT ORC
Mailing address: I0 I City Hall Plaza
City: Durham State: NC Zip: 27701
'I'elephone number: (2-19) 560-4362 E-mail address: tomyi.lLu[ct,,,Ca)clurlitiyiiic gov
Wi
FORM: DCAR 06-16 page I ol'3

3. Is the residual process facility also the generator? 0 Yes- , El No
If'Na, please specify delivery frequency and quantity of'residual to be processed:
4. Length of'residuals storage at facility: Source Specific days (Note: the Division requires minimum 30 days storage in units that
are separate from treatment system, i.e. not in clarifiers, aeration basins, etc.)
IV. RESIDUALS QUALITY INFORMATION:
I . Specify how these residuals will be distributed:
El sold or given away in bags or other containers-, El lawn (bulk)-, F-1 home garden (bulk)-,
other (explain)- Residuals will be - land -applied -by-l-�,MA-Resources -Inc. at -agronomic rate,,,
Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a
load capacity of'one metric ton or less.
2. Complete the fallowing if'residuals are to be mixed with other materials:
Type of'Materials Amounts to be added
_—T ex
)er 1.0 ton of'residuals (drtoi�i) I ()d
3. Approximate amounts ol'the residuals received and processed at the facility: 2500 dry tons per year.
4. Approximate amounts ol'the final product (processed residuals) to be distributed: 2500 dry tons per year.
5. Provide a description of the onsite storage management plan far the treated residuals (including estimated average and
maximum storage times prior to distribution): Source Specific
6. Does the facility have a ston-nwater management plan? R Yes-, No
Explain whether the treatment and storage areas are under roof or how ston-nwater runoff will be handled: Source Specific
V. RESIDUALS SOURCE INFORMATION: (Required far all new, renewed, or modified residuals source)
Complete and submit the attached Residuals Source Certification and all associated documentation.
RSC 06-16.doc
FORM: DCAR 06-16 Page 2 of'3

Professional Engineer's Certification: (Application Involving New or Changes to 'treatment or Storage Units)
attest that this application for
has been reviewed by me and is accurate and complete to the best of'my knowledge. I further attest that to the best of'my knowledge
the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal package
may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have reviewed
this material and have judged it to be consistent with the proposed design.
North Carolina professional Engineer's Seal, Signature, and Date:
Applicant's Certification:
The applicant or any affiliate has not been convicted ol'an environmental crime, has not abandoned a wastewater facility without proper
closure, does not have in outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active
compliance schedule, and do not have any overdue annual fees under Rule 15A N(,'A(,' 02T 0 105.
0 Yes E:1 No, Explain-,
Erik Blankenshila President
(SignatureAuthority's Name — PLEASE PRINT) (Title)
attest that this application for EMA Resources Inc.
(Facility Name)
has been reviewed by me and is accurate and complete to the best of'my knowledge. I understand that the Division of Water Resources
may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically
granted in the pen -nit. Further, any discharge of'residuals to surface waters or the land will result in in immediate enforcement action,
which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water
Resources should a condition of this pen -nit be violated. I also understand that il'all required parts of this application are not completed
and that if all required supporting ird'on-nation and attachments are not included, this application package will be returned to me as
incomplete.
Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.613, any person who knowingly makes any false
statement, representation, or certification in any application shall be guilty ol'a Class 2 misdemeanor, which may include a fine not to
exceed $10,000 as well as civil penalties up to $25,000 per violation.
Signature: I q, "'pir
FORM: DCAR 06-16 Page 3 of'3

o
o
rL
am

DWR
State of North Carolina
Department of Environmental Quality
Division of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
1. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: Ci
ty of 1) urharn — Brown Wf 1)
2. Facility pen -nit holder is: El Federal, F] State,
Facility pen -nit issued by: Z Div. of'Water Resource
or F-1 Other (explain:
3. Facility contact person and title: Tan Lucas — WIT ORC
Complete mailing address: 10-1- City Hall Plaza
City: Durham State: NC
0 Local Government, or F] private.
s. [:] Div. of'Environmental Health,
Zip: 27701-
'I'elephone number: (219) 5604302 E-mail address: toimn.lLu[cat,,,fa)clurliii-niie gov
4. Facility physical address: 7297 Adarns 1, ard Rd
City: Durham State: NC Zip: 27712-
Coordinates: Latitude: 36" 05'29" Longitude: 78" 52'21
Datum: NAD83 Level of accuracy: nearest second
Method of'measurement MAP
5. purpose of the facility:
E] treatment of'municipal wastewater, E] treatment of'100% domestic wastewater,
Z treatment of'potable water, [:] treati-nentof'100% industrial wastewater,
❑ treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: — % industrial and % domestic)
❑ other (explain: _).
6. Does the facility have in approved pretreatment program: R Yes Z No
7. Facility pennitted/design flow: 30 M(ID and facility average daily flow: 213(both Wf Ps) M(ID
8. Average amount of'residuals being generated at this facility 2200 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
'type and volume of'residuals treatment: Water treatin
'type and volume of'residuals storage (i.e., outside of'residuals treatment units): AD roximatCly '/2 acre covered storaL3cTad
It. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if'residuals are regulated under:
El 40 Cl, R part 503 or Z 40 Cl R part 257.
Note: Only residuals that are generated during domestichnunicipal wastewater treatment processes are regulated under 40
Cl, R part 503, otherwise, the residuals are regulated under 40 Cl, R part 257.
2. Specify if'residuals are defined under 15A N(,',A(,' 021' 1 102(�2� as:
[:] Biological Z Non -Biological
FORM: RSC 06-16 page 1 of, 5

Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the fallowing to demonstrate that the residuals are non -hazardous under
IZCRA: (Note - this item does not have to be completed far facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 Cl, R 6261.31-6261.33: F-I yes 0 no.
ll'yes, list the number(s):
b. Specify whether or not the residuals exhibit any ol'the characteristics defined by 40 Cl, R §261.21 -
261.24: F-I yes 0 no.
Fill in the fallowing tables with the results ol'the latest toxicity characteristic leaching procedure (TC1,11) analysis as well
as those far corrosivity, ignitability, and reactivity:
Laboratory: and Date ol'analysis: 1/10/24
Passed corrosivity test: Z yes F-I no. pH: s. u. (2 < pH < 12.5)
Passed ignitability test: Z yes n no. 1, lashpoint: >170 'T' (> 140°F)
Passed reactivity test: Zyes [:]no.fICN:0.478mg/lcg(<250)&fl2S:<-/5mg/lcg(<500)
TCLP Parameter
Limit
Result
TCLP Parameter
Limit
Result
(M 9/1)
(M9/1)
(M9/1)
(M9/1)
Arsenic
5.0
ND
flexachlorobenzene
0.13
ND
Barium
100.0
0.474
fl ex achl oro - I , 3 -B utadi en e
0.5
ND
Benzene
0.5
ND
flexachloroethane
3.0
ND
Cadmium
1.0
ND
Lead
5.0
ND
urban n Tetrachloride
0.5
ND
1,indane
0.4
ND
Chlordane
0.03
ND
Mercury
0.2
ND
Chlorobenzene
100.0
ND
Methoxychlor
10.0
ND
Chlorol'on,n
6.0
ND
Methyl Ethyl Ketone
200.0
ND
Chromium
5.0
ND
Nitrobenzene
2.0
ND
m-Cresol
200.0
ND
Pentachlorophenol
100.0
ND
o-Cresol
200.0
ND
Pyridine
5.0
ND
p-Cresol
200.0
ND
Selenium
1.0
ND
Cresol
200.0
ND
Silver
5.0
ND
2,4-D
10.0
ND
Tetrachloroethylene
0.7
ND
I .4-Dichlorobenzene
7.5
ND
Toxaphene
0.5
ND
I .2-Dichloroethane
0.5
ND
Trichloroethylene
0.5
ND
I , I -Dichloroethylene
0.7
ND
2.4.5-Trichlorophenol
400.0
ND
2.4-Dinitrotoluene
0.13
ND
2.4.6-Trichlorophenol
2.0
ND
Endrin
0.02
ND
2.4.5-'I'll (Silvex)
1.0
ND
Heptachlor and its Hydroxide
0.008
ND
Vinyl Chloride
0.2
ND
FORM: RSC 06-16 page 2 of, 5

] Metals Determination: Complete one ol'the fallowing tables (i.e., as applicable) to demonstrate that the residuals do not violate
the ceiling concentrations for metals regulated under 15A N(,'A(,' 02T 1105.
a. For DistributionlLand jRL�ficqtion: Fill in the fallowing table with the results ol'the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Waypoint Anal ytcical and Date ol'analysis: 03/04/2024
—
Parameter
Ceiling
Monthly Average
Result
Concentration Limits
Concentration Limits
(ClassA & ClassB)
(Class A Only)
(mglkg)
(mglkg)
(mglkg)
Arsenic
75
41
6.16
Cadmium
85
39
5.91
Copper
4,300
1,500
216
Lead
840
300
<4.93
Mercury
57
17
<0. 112
Molybdenum
75
n/a
6.26
Nickel
420
420
30.1
Selenium
100
100
<8.62
Zinc
7,500
2,800
68
b. for_,Vur ace Disposal Unit land W latest analyses (i.e., on a dry weight
L ..... ........ Fill in the fallowing table with the results of 1,
basis) for the following metal parameters
Laboratory: — and Date ol'analysis:
Distance from Disposal
Arsenic
Chromium
Nickel
Unit to Boundary to
Closest Property Line
(meters, check one)
(m9l'k9)
(m9l'k9)
(m91'k9)
E] > 0 but < 25
30
200
210
El > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but< 100
46
300
320
❑ > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg1kg)
FORM: RSC 06-16 page 3 of,

5. Nutrient/Micronutrient Determination: Complete the fallowing:
a. Total solids: 20.3 %.
b. Fill in the fallowing table with the results ol'the latest analyses (i.e., on a dry weight basis) far the fallowing nutrient and
micronutrient parameters:
Waypoint
Laboratory: hit Analytical and Date ol'analysis: 03/04/2024
T
Parameter
Result
(mglkg)
Aluminum
20700
Ammonia -Nitrogen
626
Calcium
<956
Magnesium
460
Nitrate -Nitrite Nitrogen
49.1
pH (Standard Unit)
5.2
Phosphorus
1110
potassium
380
Sodium
<3 20
Total K�jeldahl Nitrogen
7140
c. Using the results listed in Item 11. 5b. above, calculate the sodium adsorption ration (SAR): 0.96
[Note: 11'residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department ol'Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or in agronomist, prior to land application of'residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism far maintaining site integrity and
conditions conducive to crop growth].
d. Specify themineralization rate to be used in calculating the plant available nitrogen (PAN) ol'the residuals: 10%. This rate
is a (check one): Z default value, or 1:1 actually established.
If the residuals are not generated from the treatment of'municipal or domestic wastewater, explain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
e. Calculate the PAN far the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method First (15t) Year PAN Five -Year
Maximum Adjusted PAN
(mOkO (mOkO
Surface 1,014 1,404
I qj ection/In corporation 1,327 1,717
h Other Pollutants Determination: Specify whether or not there are any other pollutants of'concern in the residuals and provide
the results ol'the latest analyses:
FORM: RSC 06-16 Page 4 of,

7. Pathoguen Reduction: Per 15A N(,',A(,' 02T 1 106, specify how residuals will meet the pathogen reduction requirements:
a. For DistribufionlLandjL)L)fication (P L 'Clays A or Equivalent.
Q . . . . . _
E] A fecal colif'on-n density that is demonstrated to be less than I ,000 MIIN per grain ol'total dry solids,
or
E] A salmonellasl). density that is demonstration to be less than 3 MIIN per 4 grains ol'total dry solids.
AND one ol'the followings (except for non -biological residuals):
El Alternative I [15A NCAC 02T.1 106(b)(3)(A)l - Time/Temperature Compliance.
E] Alternative 2 [15A NCAC 02T. 1 106(b)(3)(B)l - Alkaline Treatment.
El Alternative 3 [15A NCAC 02T. 1 106(b)(3)(C)l - Prior Testing for Enteric Virus/Viable flelminth Ova.
El Alternative 4 [15A NCAC 02T. 1 106(b)(3)(D) No Prior Testing for Enteric Virus/Viable flelminth Ova.
Ej Alternative 5 [15A NCAC 02T. 1 106(b)(3)(E)-(K)l - Process to Further Reduce Pathogens (111, RP).
Specify one: El composting, F-] heat drying, E] heat treatment,
F] then-nophilic aerobic digestion, E] beta ray irradiation,
❑ gamma ray irradiation, or E] pasteurization.
b. For LandA wfication of'Clays B:
E] Alternative I [ISA NCAC 02T. 1 106(c)(1) Fecal Colifon-n Density Demonstration.
❑ Alternative 2 [15A NCAC 02T. 1 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: El aerobic digestion, R air drying, E] anaerobic digestion,
R composting, or El lime stabilization.
c. for Vur ace DisLmsal:
L ..... _
El Select One ol'the Class A or Equivalent Pathogen Reduction Alternatives in Item 11. 7a. above.
El Select One ol'the Class B or Equivalent Pathogen Reduction Alternatives in Item 11. 7b. above.
El Exempt - JI'Daily Cover Alternative is chosen in Item 11.8. below [I 5A NCAC 02T.1 106(a)(2)1.
El Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Vect®r Attracti®n Deducti®n LVAR1: Per 15A NC A(,'02'11107 mm specify how residuals will meet the VAR requirements:
E] Alternative I [15A NCAC 02T.1 107(a)(I)l - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
❑ Alternative 2 [15A NCAC 02T. 1 107(a)(2)1 - 40-Day Bench Scale Test (Anaerobic Digestion).
❑ Alternative 3 [15A NCAC 02T. 1 107(a)(3)1 - 30-Day Bench Scale Test (Aerobic Digestion).
❑ Alternative 4 [15A NCAC 02T. 1 107(a)(4)1 - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
❑ Alternative 5 [15A NCAC 02T. 1 107(a)(5)1 - 14-Day Aerobic Processes.
❑ Alternative 6 [15A NCAC 02T. 1 107(a)(6)1 - Alkaline Stabilization.
El Alternative 7 [15A NCAC 02T. 1 107(a)(7)1 - Drying of'Stabilized Residuals.
El Alternative 8 [15A NCAC 02T. 1 107(a)(8)1 - Drying ol'Unstabilized Residuals.
El Alternative 9 [15A NCAC 02T. 1 107(a)(9)1 - Injection.
El Alternative 10 [1 5A NCAC 02T. 1 107(a)(I 0) 1 - Incorporation.
El Alternative for Surface Disposal Units Only - Soil/Other Material Cover [I 5A NCAC 02T. 1 107(b)(2)
Z Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur
when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of, 5

Standard Operating Procedure and Operation
3 Maintenance
r r/
a. Ensure the requirements of EMA Resources Inc. Permit# WQ 041000 are
met.
a. The following is a list of personnel in order they are to be contacted when
information needs to be shared.
i. EMA Resources Inc.
1. David Ackley —Project Manager — 419-212-3699
2. Brent Collins — Director of Technical Services — 336-399-3646
3. Roy Whitaker— Director or Marketing — 336-909-171
4. Mike Collins — Director of Operations — 336-399-0070
ii. City of Durham
1. Tarn Lucas — WTP ORC — 919-560-4362 x35207
a. The operational function of this project will involve trucking cake residuals
to agronomic sites. It is going to be spread at agronomic rates that are
determined using the Realistic `Geld Expectations (RYE) as outlined in the
permit, the amount of other nutrient sources the landowner and operator
has applied, and the residuals nutrient and metal sample that is current for
that monitoring period. It is going to be spread with a cake applicator that
will use an auger and paddles to spread the material in such a way as to

achieve a consistent spread pattern. The material is going to be land
applied on fields that have a crop grooving on them that are going to either
be grazed or cut for animal feed. Application rates will be reduced by 25%
on fields that are primarily used for grazing in accordance with USDA- RCS
590. Grazed fields will be determined by the farmers and EMA project
managers.
a
Maintenance Schedule
a. EMA Resources Inc. will follow the maintenance schedule as recommended
by the EMA Resources Director of Operations (Bike Collins) for the
equipment necessary to complete thejob.
S. Safety Measures
a. City of Durham -Brown WTP and EMA Resources Inc. believe in operating in
a safety conscious manner and all employees participate in safety training
that is designed to help employees recognize safety issues and take steps
to prevent accidents from occurring. In addition, EMA Resources employees
have the authority to stop operations if they think any aspect of the
operation is going to cause environmental or personal harm.
a
Spill Response Plan
a. In the unlikely event of a spill, the following action shall be taken
immediately.
i. n ill Clean-up c ivi i ® The EMA Resources
Project Manager shall take immediate charge and initiate clean-up
activities. EMA Resources labor and equipment is to be utilized. In
the event additional labor and equipment is required, assistance may
be requested from the City of Durham, The NC Department of
Transportation, and other private contractors as necessary.
ii. Halt the Source the -Spill: Such as a ruptured container or
damaged transport unit.
iii. Contain S ill® Form a barrier. Sufficient quantities of straw shall
be used for such purposes. Earthen barriers may be constructed to
augment the straw bale containment area of the spill. The
Operations Manager or the person in charge on the spill site will
advise the clean-up personnel where to get the straw, lime, and other

items necessary to complete the clean-up operation. ie. local farmers,
farm supply centers, nurseries.
iv. Initial lean Employ front-end loaders, vacuum equipment,
sludge application vehicles, and/or local septic tank service to
remove as much of the spilled material as possible. Straw and/or
sand should be scattered in the spill area to soak up the remaining
material. The straw and sand soaked material will be collected and
removed to a disposal area approved by representatives of the state
regulatory agency.
v. finall Clean::W. Employ rotary brush sweeper if needed and apply
lime to the spill area upon the approval of the clean-up efforts by the
state regulatory representative. If the event occurs on private
property, the clean-up will be completed to the satisfactory of the
property owner and state regulatory representatives. The ultimate
goal will be restore the spill area to its original condition if possible.
vi. Notification: As soon as possible after the spill occurs, the EMA
Resources Project Manager or designee will notify the City of Durham
and the EMA Resources main office. EMA Resources office staff are
then responsible for notifying other key EMA Resources personnel.
vi i. rtin - EMA Resources staff will notify the Raleigh Regional
office of NCDENR by telephone [phone] as soon as possible,
but not more than 24 hours after, or on the next working day
following the occurrence. The EMA Project Manager shall provide a
written report within 48 hours of the spill to the EMA Resources
Director of Technical Services and City of Durham staff. The report
shall list all relative information and actions taken. With the
assistance of EMA Resources personnel, and City of Durham
personnel, a written report will be filed with the Raleigh Regional
office within 5 days of the occurrence. For after-hours reporting, the
Division's emergency number shall be called to report all incidences
[phone].
7. Inspection Plan
a. Inspection for the land application of residuals will be conducted on a
minimum of a weekly basis at the land application site during land
application activities. The inspection frequency is based on the time frame

that it is going to take to complete the project and the amount of dry tans
to be land applied from this facility. The inspections will consist of
inspecting a current field that is being applied as well as inspecting random
fields that have been completed. Inspections will be conducted by David
Ackley — Project Manager. These inspections will consist of the following:
i. Verifying the application rates for each field that plan on receiving
material.
ii. Checking the calculated loads to ensure the correct amount of
residuals are being land applied.
iii. Ensure that all manned equipment has a copy of the permit and the
operation and maintenance plan.
iv. Ensure that the field has been flagged properly and that all buffers
are being adhered to.
v. Verify that the proper number of samples of the residuals have been
taken and that it meets the criteria for land application.
vi. The records will be kept in the EMA Resources project fibs in the
main office.
vii. EMA Resources and City of Durham staff will immediately inform the
other party if any of the following conditions are noted.
1. Any occurrence with the distribution program resulting in the
land application of significant amounts of material that is
abnormal in quantity or characteristics.
2. Any failure of the distribution system that results in the release
to surface waters.
3. Any time that self -monitoring indicates that the facility has
gone out of compliance with the permit.
4. Any process failure that results in the system not adequately
treating the residuals.
5. Any spill or discharge from a vehicle or piping system during
residuals transportation.
0. Any release that requires immediate reporting outside normal
business hours shall be called in by EMA Resources staff to
DE R at (00) 5 -030 . This number is to be called in the
event of a release to surface waters or imminent failure of a

storage system when the event occurs outside of normal
business hours.
8. Sampling and Monitoring Plan
a. Sampling for this project consists of sampling the residuals prior to land
application occurring in order to ensure that the residuals are suitable for
land application.
b. The samples will be collected from the storage pad that holds the residuals
c. David Ackley, Brent Collins, Roy Whitaker or other designee will be
responsible for sample collection for nutrient and metal, TCLP, and soil
samples.
d. Nutrient, metal and TCLP sample aliquots will be collected randomly and
consist of at Fast 7 individual aliquots mixed together in order to get the
composite sample for these parameters.
e. The residuals will be sampled annually for TCLP including the RCIls.
f. fetal and nutrient parameters will be collected and analyzed based on the
requested dry ton numbers in the permit application.
a. The environmental impacts for residuals may be affected by this procedure.
b. This procedure helps assure that land application is conducted in a safe and
efficient manner whip ensuring compliance with the laws and regulations
and to minimize exposure, negative environmental impacts and public
relation concerns.

Program Information
1. Provide a narrative explaining the following:
a. flow will the materials be handled and transported from where the residuals were
produced to where it will be treated?
The residuals are produced through non -biological water treatment processes at the
Brown WI'. See process flow. Liquid material from the Williams WTP is trucked to the
Brown WTP and corningled before being pressed using their belt filter press. Once the
residuals have been dewatered, they will be stored at the on -site pad. When the residuals
are ready to be land applied, they will be taken to agricultural sites by EMA Resources
and land applied at agronomic rates.
ba flow will the residuals be processed/treated?
See Process flow diagram and narrative.
c. Where will the residuals be stored until processing?
The residuals will be stored at their approximately 1/2, acre covered cake storage pad.
da flow will the final product be distributed?
The residuals will be delivered to local farmers via end dump trailers. Each load will be
off-loaded to a high flotation applicator for application on a receiver site (grassland or
row crop).

Brown WTP Marketability Statement
Residuals will be given to local farmers for crop production. EMA Resources Inc. will land apply the
material for the local farmers who have chosen to receive the product. Cake spreaders will be utilized
to spread the material in a consistent and even manner. The material will be applied to fields that have
a cover crop growing, either grass for hay production, pasture, or row crops. Agronomic rates will be
determined using the Realistic Yield Website through NC State.

The residuals that are land applied are produced at the Brown WTP at: 1615 Infinity Road, Durham, NC
27712. Mr. Tom Lucas, Brown Water Treatment (}RCis the preparerofthe residuals and responsible for
the plant operations.
The residuals from the Brown WTP will be land applied at agronomic rates based on the Realistic Yield
Expectation rate for the fields and crops to6egrown. The VVTPresiduals will not 6eapplied tofrozen,
snow covered or flooded fields. The fields will be flagged with the following buffers tohelp prevent
runoff from the applied fields.
Cake Residuals
Each private or public water supply source: 100
Surface waters such as intennittent and perennial streams, perennial
waterbodies, and wetlands: 25
Surface water diversions such as ephemeral streams, waterways, and
ditches: 0
Groundwater lowering ditches where the bottom of the ditch intersects
Each well with exception of monitoring wells: 100
Bedrock outcrops: 0
Residuals produced by the Brown WTP will be applied to agricultural fields in bulk and will be land
applied according to this label as well as following all permit conditions listed in the land application
permit WQ0041666.
Adequate procedures will be followed to prevent surface runoff from carrying any disposed or stored

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11111111 111111 t 1111111��111;i--Itiii I I I 1 1 1 11 11 lgri i
2=11
City of Durham — Brown WTP
Requested Permitted Rate:
We are requesting a permitted dry tonnage rate of 2500 dry tons of water plant
residuals. This number is based on past data and an expected increase in their
production. In 2023, EMA Resources land applied 2,247 which was higher than our
currently permitted amount. This number includes the contributions from the Williams
WTP material that is comingled and pressed at the Brown WTP.

2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ` Fax [phone]
www.waypointaiial,ytical.coni
wMaDEW
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 24-066-0042
Client Project Description: Brown WTP
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 3/6/2024 for the analyses presented in the following report.
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a' -'symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
MGM=
H r �
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 10

Waypoeint.o
ANALYTICAL
27g0Whitten Roadl,Memphis, TN 38133
Main �901.21@.24U0"Fax 901.2I3.2440
unwmw.waypoNmtanelytiomU,corn
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical,LLC.,Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2025
Arkansas
State Program
88'0650
02/07/2025
California
State Program
2904
06/30/2024
Florida
State Program
NELAP
E871157
06/30/2024
Georgia
State Program
C044
11/14/2025
Georgia
State Program
04015
06/30/2024
Illinois
State Program
NELAP
200078
10/31/2024
Kentucky
State Program
80215
06/30/2024
Kentucky
State Program
KY90047
12/31/2024
Louisiana
State Program
NELAP
LA037
12/31/2024
Louisiana
State Program
NELAP
04015
06/30/2024
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/31/2024
North Carolina
State Program
415
12/31/2024
Pennsylvania
State Program
NELAP
68'03195
05/31/2024
South Carolina
State Program
84002
06/30/2024
Tennessee
State Program
02027
11/14/2025
Texas
State Program
NELAP
T184704188
09/30/2024
Virginia
State Program
00106
06/30/2024
Virginia
State Program
NELAP
460181
09/14/2024
Page of 0000/24-06S-0042
Page 2 of 10

Sample Summary Table
Report Number- 24-066-0042
Client Project Description: Brown WTP
Lab No Client Sample ID Matrix Date Collected
85737 Brown VVTP Solids 03/04/2024 12:15
03/06/2024
Page 3 of 10

y� * to
PA L
Client: EMA Resources Inc
Project Brown V\fTP
Lab Report Number: 24-066-0042
Date: 3/20/2024
OXMAN
Main 901.213.2400 0 Fax [phone]
www.waypoir�tanalytical.com
CASE NARRATIVE
Block Digestion and FIA Method 4500NORGD-2011
Analyte: Total Kjeldahl Nitrogen
QC Batch No: L737601/L737301
Matrix spike recovery outside of control limits. Acceptable LCS recovery indicates the system was in control, but
the reported result could be affected by matrix interference.
Metals Analysis Method 6010D
Sample 85735 (North Durham)
Analyte: Aluminum
QC Batch No: L737815/L737486
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 85737 (Brown WTP)
Analyte: Aluminum
QC Batch No: L737815/L737486
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 85737 (Brown VVTP)
Analyte: Arsenic
QC Batch No: L737815/L737486
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 85737 (Brown WTP)
Analyte: Calcium
QC Batch No: L737815/L737486
This analyte was analyzed at a dilution due to IBC interference/matrix interference.
Sample 85737 (Brown WTP)
Analyte: Cadmium
QC Batch No: L737815/L737486
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 85737 (Brown VVTP)
Analyte: Chromium
QC Batch No: L737815/L737486
This analyte was analyzed at a dilution due to IBC interference/matrix interference,
Sample 85737 (Brown WTP)
Analyte: Copper
QC Batch No: L737815/L737486
This analyte was analyzed at a dilution due to IBC interference/matrix interference.
Sample 85735 (North Durham)
Analyte: Iron
Page 4 of 10

Way� * to
PA L
QC Batch No: L737B15/L737486
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 8S737(Brown VVTP)
*na/yte: Iron
QCBatch No: L737815/L73748G
This analyte was analyzed at a dilution due to IEC interference/matrix interference,
Sample B5737(Brown VVTP)
Analyte: Potassium
QC Batch No: L737815/L737486
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 85735(North Durham)
Analyte: Potassium
QC Batch No: L737958/L737486
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. Nomatrix interference im
suspected.
Sample 85737(Brown VVTP)
Anolyte:KAagnesium
QC Batch No: L737815/L737488
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 8S737(Brown VVTP
Analyte:ManQaneme
(3CBatch No: L737815/L737486
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 85737 (Brown VVTP)
*nalyte: Molybdenum
QC Batch No: L737815/L737488
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 85737(Brown VVTP)
Analyte: Sodium
C)CBatch No: L737815/L73748B
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 8S737(Brown VVTP)
Analyte: Nickel
QC Batch No: L737815/L737486
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample B5735(North Durham)
Anolyte:Phoaphonua
[3CBatch No: L737815/L737486
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. Nomatrix interference iususpected.
Sample 85737 (Brown VVTP)
Page 5 of 10

Way� * to
PA L
Analyte:Phosphorus
QC Batch No: L737B15/L737486
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 8S737(Brown VVTP)
Analyte: Lead
QC Batch No: L737815/L737486
This analyte was analyzed at a dilution due to IEC interference/matrix interference,
Sample B5737(Brown VVTP)
Analyhe: Sulfur
QC Batch No: L737815/L737486
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 85737 (Brown VVTP)
Analyte: Selenium
QC Batch No: L737815/L737486
This analyte was analyzed at a dilution due to IEC interference/matrix interference,
Sample 85737 (Brown VVTP)
*naxyne: Zinc
QCBatch No: L737815/L73748S
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Page 6 of 10

Waypoint.(D
ANALYTICAL
46245
BMAResources Inc
Mr. Brent Collins
755Yadk|mAUeKd
MmckmviUe, NC 27028
Project BrowWTP
Information :
27g0Whitten Roadl,&MernphUs,TN 38133
Main �901.21@.24U0oFax 901-2I3.2440
unwmvv.waypoNmtanelytiomU,cann
Report Date 03/20/2024
Received03/06/2024
; .xeh�
ConnieCook
Report Number : 24-066-0042
REPORT OFANAL YSIS
Project
Manager
Lab No: 85737
Matrix:
Solids
Sample ID : Brown WTP
Sampled: 3/4/2024 12:15
Test
Results
Units
MDL
MQL
DF
Date/Time
By
Analytical
Analyzed
Method
Moisture
79~7
96
0.010
0.010
1
03/07/24 14:10
CAN
SW-DRY0V7
Ammonia Nitrogen
626
mg/Kg-drK
70.0
493
1
03/19/2415:40
]PJ
450ONH][-2011
Nitnytc+Nitrite-N
49,1
mg/Kg-dry
23.9
25.3
1
03/18/24 11:05
]RZ
450ONO3F-2016
Organic N
6500
mg/Kg-dry
936
1760
1
03/00/24 13:26
CALCULATION
pH
5,2
S.U.
1
03/08/24 16:00
CNB
9045D
Total Solids
20,3
96
0.010
0.010
1
03/07/2414:10
[AH
254DG-2011
Total Kjddah| Nitrogen
7140
mg/Kg-dry
1760
1
03/08/24 13:26
ANH 4500NORGD-2011
Phosphorus
1110
mg/Kg-dry
09.0
123
5
03/11/24 12:39
BKN
6010Q
Aluminum
20700
mg/Kg-dry
115
123
S
03/11/24 12:39
BKN
6010D
Arsenic
6,163
mg/Kg-drK
8.18
12.3
5
03/11/2412:39
8KN
6010D
Cadmium
5,91
mg/Kg-dry
1.23
2.46
S
03/11/24 12:39
BKN
6010D
Calcium
<956
mg/Kg-drK
958
1230
5
03/11/24 12:39
8KN
6010D
Chromium
21,0
mg/Kg-dry
6.16
6.16
S
03/11/24 12:39
BKN
6010D
Copper
216
mg/Kg-drK
7.39
12.3
5
03/11/24 12:39
8KN
6010D
Iron
345000
mg/Kg-dry
421
493
10
03/11/24 12:23
BKN
6010D
Lead
<4.93
mg/Kg-dry
4.93
7.39
5
03/11/24 12:39
8KN
6010Q
Magnesium
460
mg/Kg dry
64.0
123
5
03/11/2412:39
BKN
6010D
Manganese
2630
mg/Kg-dry
8.62
12.3
5
03/11/24 12:39
8KN
6010D
Mercury
<0.112
mg/Kg-dry
0.113
0.931
1
03/13/2112:32
FDS
7471A
Molybdenum
6,26
mg/Kg-dry
3.69
6.16
5
03/11/24 12:39
8KN
6010D
Nickel
30,1
mg/Kg-dry
3.69
6.16
5
03/11/24 12:39
BKN
6010D
Potassium
380
mg/Kg -dry
153
248
5
03/11/24 12:39
BKN
6010D
Selenium
<W.GZ
mg/Kg -dry
8.62
12.3
5
03/11/24 12:39
BKN
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method QuanUtationLimit
I Estimated value
Page 7 of 10

o
ANALYTICAL
46245
EMA Resources Inc
Project Brown WTP
Mr, Brent Collins
755 Yadkinville Rd
Information
Mocksville , NC 27028
Report Number : 24-066-0042
Lab No : 85737
Sample ID : Brown WTP
Test
2790 Whitten Roadl, Mernplils, TN 38133
Main 901.213.2400 " Fax [phone]
wwwar. waypohita nalyticall. corn
REPORT OFANAL YSITS
Results Units MDL
Report Date 03/20/2024
Received 03/06/2024
11�eh—
Connie Cook
Project Manager
Matrix: Solids
Sampled: 3/4/2024 12:15
MQL DF Date / Time By Analytical
Analyzed Method
Sodium
<320
rng/Kg - dry
320
616
5
03/11/24 12:39 BKN
6010D
Zinc
68.0
mg/Kg - dry
20.9
30.8
5
03/11/24 12:39 BKN
6010D
Sulfur
3870
rng/Kg - dry
128
246
5
03/11/24 12:39 BKN
6010D
Sodium Absorption Ratio
<0.01
Ratio
0.01
0.01
5
03/11/24 12:39
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
I Estimated value
Page 8 of 10

2790 Whitten RodmphiTN a, Mes, 38,133
Wa y p, dia n t, Main 901.233.2400 ' Fax 901.213,2440
ANALYTICAL www.waypo�tanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 24-066-0042
Shipping Method
400 Fed Ex 0 US Postal 0 Lab 0 Other:
................................................................. . . . . . . . . . . . . . . . 0 UPS 0 Client 0 Courier Thermometer ID: 'T1 37
Shipping container/cooler uncomprornised? Yes 0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No Not Present
Custody seals intact on sample bottles?
0 Yes
0 No Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
Yes
0 No
COC properly completed
Yes
0 No
Samples in proper containers?
Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Yes
0 No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved
Water - VOA vials free of headspace
Trip Blanks received with VOAs
Soil VOA method 5035 — compliance criteria met
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Special precautions or instructions included?
0 Yes
0 No
# N/A
0 Yes
0 No
# N/A
0 Yes
0 No
# N/A
0 Yes 0 No # N/A
Low concentration EnCore samplers (48 hr)
Low conc pre -weighed vials (Sod Bis -14 d)
0 Yes # No
Comments: — I
Signature: FC—adlee -------------------- ] Date &Time: [0-3/0
Page 9 of 10

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Page 10 of 10

�wwuwu
aREPORT
ceAnalytical ANALYTICAL
January 24, 2024
EMA Resources
Sample Delivery Group: L1695669
Samples Received: 01/11/2024
Project Nurriber:
Description: Sludge
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27025
Entire Report Reviewed By
Reagan Johnson
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall riot be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0062. Where sampling conducted by the customer, results relate to the accwacy of the inforrnation provided,
and as the samples are received.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1695669 01/24/24 09:55 1 of 21

TABLE OF CONTENTS
To ANe of Cr. Mr
So Samol Summary
Cn: Case Narrative
Sn SamWe ReWs
RROWN W PP 1...1n695669...01
On chmmy cammd swummy
Wet Wm=y by Mebod SQU 13
Wet by 9034
Wet by 90,45ll)
Wet by 193"/l0)lRD)A
MoTwry by MeToci 7470A
MeWs Pm FJ by !Aehodi 6011aIC)
VoAUW Chgarime CompowWs (Gj(�"JVS) by Vk��H-tocA E,,2(5()H�`,7)
Ack,]i Hmtkides XKJ by MeUnd BVAA
PeMkides NMI by MeNod BOWidl3,
Semi WaMe (Alonk; Compawds ((3(�,IVS) by
G11: Glossary of'Tenms
A[ & Ii
sc slnllllll:fle Chnllll of ll`Ustlody
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
IMA Resources L1695669 004n4 0955 2021

IWARNMENEXEMMORIN
SAMPLE SUMMARY
:( , I ll( '( j 'd by
oll I( �(I "d � 1, 1 '( , trrri�
" ( (, ( '1v( ' I J, I k '411' I'l
3PC)VVN VV .16%069 01 VVas� e
'Irf�1'10 ftI11111"
31110124 10.00
01111124 (N 00
.................
Method
Batch
Dilution Prepmation
...............
Analysis
Analyst
Location
date/time
date/time
Preparation by Method 1311
WG2207860
1 01/19/24 12:41
01/19/24 12:41
BTP
Mt. Juliet, TN
Preparation by Method 1311
WG2208021
1 01/17/24 13:40
01/17/24 13:40
BTP
Mt. Juliet, TN
Wet Chemistry by Method 9012 B
WG2206160
1 01/12/24 13:14
01/12/24 17:08
UNP
Mt. Juliet, TN
Wet Chemistry by Method 9034-9030B
WG2205204
1 01/14/24 09:47
01/14/24 10:17
DMA
Mt. Juliet, TN
Wet Chemistry by Method 9045D
WG2206462
1 01/13/24 09:47
01/13/24 11:50
KRB
Mt. Juliet, TN
Wet Chemistry by Method D93/1010A
WG2208644
1 01/18/24 15:15
01/18/24 15:15
ARV
Mt. Juliet, TN
Mercury by Method 7470A
WG2209772
1 01/20/2410:55
01/20/2415:26
AKB
Mt. Juliet, TN
Metals (ICP) by Method 6010D
WG2209813
1 01/21/2410:14
01/21/2413:58
D-S
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG2208740
1 01/18/24 15:11
01/18/2415:11
JCP
Mt. Juliet, TN
Chlorinated Acid Herbicides (GC) by Method 8151A
WG2209661
1 01/21/24 07:50
01/21/2419:26
AMM
Mt. Juliet, TN
Pesticides (GC) by Method 8081B
WG2209670
1 01/21/24 09:44
01/21/24 17:49
NWH
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG2209666
1 01/21/24 09:43
01/23/24 19:27
JRM
Mt. Juliet, TN
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
IMA Resources L169 5669 01/24/24 09:55 3 of 21

CASE N/\RR/\Tl\/E
All sample a|iquOLSwere received atthe correct temperature, |nthe proper nta| .withthe
appropriate preservatives, and within method specified holding tirries, unlessqualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOO) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the E],
quality of the data have been identified by the laboratory, and no infon-nation or data have been
knowingly withheld that would affect the quality of the data. M
�IE
R e a g a n J o h n s o n
Project Manager | ,� U
Project Narrative E]
All Reactive cyanmeresults reported m[he a«aclheuieponwere determined matomlsusing method eo12 D.
All Reactive Sulfide resulls reported in the altached reportweie delermined as rotals using nneffiod 9024-902013.
xccouwr pROuscr cma: nxremmE: pxss:

BROWN WTP
SAMPLE RESULTS - 01
Collected date/time:
01/10/24 10:00
L1695669
Pir(---apeiirahon oy
1-311
Result
Qualifier Prep
Batch
Analyte
date / time
TO P Extraction
1/19/202412:41:30 PM
WG2207860
TCLP 71-IF Extraction
-
1/17/20241:40:13 PM
WG2208021
Initial pH
6.47
1/19/202412:41:30 RIM
WG2207860
Final PH
4.97
1/19/2024 12:41:30 RIM
WG2207860
WeL Ch(,-.ai,rdsUry Ibyr IVI Ahud 9012 1. . .3
Result Qualifier
RDL
Dilution
Analysis Batch
Analyte mg/kg
mg/kg
date / time
Reactive Cyfinide 0.478 J6
&250
1
Y1117 _IA60
01/12/2024 17:08 V G2?06160
WeL Ch(,iTflsUry by VkAhod 9034-903GE"I
Result Qualifier
RDL
Dilution
Analysis Batch
Analyte mg/kg
mg/kg
date / time
Reactive Sulfide ND
75.0
1
01/14/2024 10:17 11VG2?05204
WeL Chernsl.ry Ibyr IMcthod 9045[
Result Qualifier
Dilution
Analysis , , , , s , , , , , , , , , , , , , ,
, , , , , , , , , , , , , , , , , , , , , , , , , , , Batch
Analyte Su
date / time
Corrosivity by pH 6.06 1
1
01/13/2024 11:50
1111G2206462
Sample Narrative:
L1695669-01 WG2206462: 6.06 at 20.7C
WeL ChernIsUry by Mcth()d )93/1010A
Result Qualifier
Dilution
Analysis
Batch
Analyte Deg. F
date / time
Igniftability DNI at 170
1
01/18/2024 15:15
11VG22026-,14
Mercury Ibyr Medhod 7470A
Result Qualifier
RDL
Limit
Dilution Analysis
Batch
Analyte mg/l
mg/l
mg/l
date/time
Mercury ND
0.0100
0.20
1 01/20/2024 15:26
1NG2209772
Metals (10PI) by IIMIexl.hod 6010[')
Result Qualifier
RDL
Limit
Dilution Analysis
Batch
Analyte mg/l
mg/l
mg/l
date/time
Arsenic ND
0.100
5
1 01/21/2024 13:58
WG2209r',13
Barium 0.474
0.100
100
1 01/21/2024 13:58
\NG2209813
Cadmium ND
0.100
1
1 01/21/2024 13:58
WG2209rn,13
Chromium ND
0.100
5
1 01/21/2024 13:58
\NG2209813
Lead ND
0.100
5
1 01/21/2024 13:58
WG2209rn,13
Selenium ND
0.100
1
1 01/21/2024 13:58
\NG2209813
Silver ND
0.100
5
1 01/21/2024 13:58
WG2209rn,13
Volable (Dirgaitc Coirn�30L,flnds (GC;/MS) by Meflhod
826GE)
Result Qualifier
RDL
Limit
Dilution Analysis
Batch
Analyte mg/l
mg/l
mg/l
date/time
Benzene ND
0.0500
0.50
1 01/18/2024 15:11
WG2208740
Carbon tetrachloride ND
0.0500
0.50
1 01/18/2024 15:11
1NG2208740
Chlowbenzene ND
0.0500
100
1 01/18/2024 15:11
WG2208740
Chloroform ND
0.250
6
1 01/18/2024 15:11
1NG2208740
1,2-Dichloroethane ND
0.0500
0.50
1 01/18/2024 15:11
WG2208740
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
FIMA Resources
L169 5669
01/24/24 09:55 5 of 21

BROWN WTP
SAMPLE RESULTS
m 01
Collected dateltime: 01110/24 10:00
L1695669
qtul
A4IsiMle olieu.nl'1It .. irq,")O
,lI'1d s (�":7�...A`V S)i .1':,f" E�,Pflhod 82.60E)
Result
Qualifier RDII
Limit
Di lotion
Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
1,1-Dichloioethene
ND
0.0500
0.70
1
01/18/202415:11
1NG 2(l8740
2-Butanone (MEK
ND
0.500
200
1
01/18/202415:11
WG2208740
Tetrachloroethene
ND
0.0500
0.70
1
01/18/202415:11
1NG2208740
Trichloroethene
ND
0.0500
0.50
1
01/18/202415:11
WG2208740
Vinyl chloride
ND
0.0500
0.20
1
01/18/202415:11
1NG2208740
(S) Toluene-d8
84.4
80.0-120
011181202415:11
1NG;2208740
(S)4-Bromofluorobenzene
86.8
77.0-126
011181202415:11
1NG;2208740
(S)12-Dichloroethcrne-d4
81.5
70.0-130
011181202415:11
1NG;22CkkG740
1.,IrnIIG:iJin,-He d Acid (GC') IL:y
I Ic.-JIlu.-d 8151/
Res It
Qualifier RDEI,
Dilution
Analysis
Batch
Analyte
mg/
mg/
LiLimit
g/l
date tlrne,,,,
2,4,5-TP (Silvex)
ND
0.00200
1
01/21/202419:26
1NGi2209661
2,4-D
ND
0.00200
1
01/21/202419:26
1NG;2209661
(S) 2,4-Dichlor©phenyl Acetic Acid
80.0
14.0-158
011211202419:26
1NGi2209661
'Ie sV C:IICIIE:: Cn (GC) by 4'IIV,"7'` hod 8081B
Rpsult
Qualifier R DLLimit
Dilution
Analysis
Batch.,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,.
Analyte
mg/I
mg/I
mg/I
date/time
Chlordane
ND
0.00500
0.03
1
01/21/202417:49
1NG2209670
Endrin
ND
0.00500
0.02
1
01/21/202417:49
1NG2209670
Heptachlor
ND
M0500
0.0080
1
01/21/202417:49
1NG2209670
I-leptachlor epoxide
ND
0.00500
0.0080
1
01/21/202417:49
1NG2.209670
Lindane
ND
M0500
0.40
1
01/21/202417:49
1NG2209670
Methoxychlor
ND
0.00500
10
1
01/21/202417:49
1NG,2209670
Toxaphene
ND
0.0100
0.50
1
01/21/202417:49
1NG,i2209670
(S) Decochlorobiphenyl
56.7
10.0-128
01121120241749
1NG,2209670
S)Tetrochloro-m-xylene
68.6
10.0-127
01121120241749
1NG,i2209670
>e:"ntllVolla'tIIle Organic C.:ol"npoulrnds
(GUMS) by II\Iel':Ihod 8270::
Result
Qualifier RDL
Limit
Dilution
Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
1,4-Dichlorobenzene
ND
0.100
7.50
1
01/23/202419:27
1NG2209666
2,4-Dinitrotoluene
ND
0.100
0.13
1
01/23/202419:27
1NG2209666
Hexachloiobenzene
ND
0.100
0.13
1
01/23/202419:27
1NGi2209666
I-lexachloro-13-butadierie
ND
0.100
0.50
1
01/23/202419:27
1NG2209666
Hexachloioethane
ND
0.100
3
1
01/23/202419:27
1NGi2209666
Nitrobenzene
ND
0.100
2
1
01/23/202419:27
1NG2209666
Pyridine
ND
0.100
5
1
01/23/202419:27
1NGi2209666
3&4-Methyl Phenol
ND
0.100
400
1
01/23/202419:27
1NG2209666
2-Methylphenol
ND
0.100
200
1
01/23/202419:27
1NGi2209666
Pentaclilorophenol
ND
0.100
100
1
01/23/202419:27
1NG2209666
2,4,5-Trichlorophenol
ND
0.100
400
1
01/23/202419:27
1NGi2209666
2,4,6-Triclilorophenol
ND
0.100
2
1
01/23/202419:27
1NG2209666
(5) 2-Fluorophenol
22.3
10.0-120
011231202419:27
1NGi2209666
(S) Phenol-d5
15.0
10.0-120
011231202419:27
1NG2209666
S) Nitrobenzene-d5
62.0
10.0-127
011231202419:27
1NGi2209666
(S) 2-Fluorobiphenyl
60.2
10.0430
011231202419:27
1NG2209666
S) 2,4,6-Tribronrophenol
38.4
10.0-155
011231202419:27
1NGi2209666
(S) p-Terpheny1-d14
52.3
10.0-128
011231202419:27
1NG2209666
ACCOUNT:
PROJECT:
SDG:
DATE/TME: PAGE:
LIMA Resources
L1695669
01/24/24 09:55 6 of 21

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94-2

GLOSSARY OF TERMS
Guide to Reading
and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive
explanation, and if you have additional questions please contactyour project representative_
Results Disclaimer - Information
that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix,
Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results
relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Defection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical of by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name of the Particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample May be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target %. recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful OC Sample analysis will target all analytes recovered 01
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. TI'm Original sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifler
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossaiy and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty Confidence level of 2 sigma.
(Radiochemistry)
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn) observed either at sarriple receipt by the laboratory frorn the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc) analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being periormed on your samples typically, but on laboratory generated material.
This is the clOCUrrient created in the field when your samples were initially collected. This is used to verity the tirrie and
Sample Chain of date of collection, the person collecting the saimples, and the analyses that the laboratory is requested to perform. This
Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
sarriples from the time of collection until delivery to the laboratory for analysis.
This section Of your report Will provide the results of all testing performed an your samples. These results are provided
Sample Results (Sr) by sample ID and are separated by the analyses performed on each sarnple. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
J3
J6
T8
Description
The analyte conce n fro Lion exceeds the upper limit of the calibration range of the instrument established by the initial
calibration (ICAL).
The identification of the analyte is acceptable, the reported value is an estimate.
The associated batch QC was outside the established quality control range for precision.
The sample matrix interfered with the ability to make any accurate determination-, spike value is low.
RPD between the primary and confirmatory analysis exceeded 40%.
Sample(s) received past/too close to holding time expiration.
ACCOUNT:
LIMA Resources
PROJECT: SDG: DATE/TIME: PAGE:
L169 5669 01/24/24 09:55 19 of 21

ACCREDITATIONS & LOCATIONS
Cdr11 I () I I \4 c), i i-(ihe, I'N
Alabama
40660
Nebraska
NE-05-15-05
Alaska
17-026
Nevada
TNO00032021-1
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jeisey—NELAP
TN002
California
2932
New Mexico
TN00003
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina
DW21704
Georgia
NEIAP
North Carolina
41
Georgia
923
North Dakota
R-140
Idaho
TNO0003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode island
LA000356
Kentucky
KY90010
South Carolina
84004002
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee
2006
Louisiana
I A018
Texas
T104704245-20-18
Maine
TN00003
Texas'
LAB0152
Maryland
324
Utah
TNO00032021-11
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
110033
Minnesota
047-999-305
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A2LA
A21 A — 150 17025
1461.01
AIHA-1 APJ I C EMI AP
100789
A21-A — ISO 17025
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TNO0003
Drinking Water 2 Underground Storage Tanks ' Aquatic Toxicity 4 Chernical/Microhiological ' Mold ' Wastewater Wa Accreditation not applicable
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope ofaccreditation held by Pace Analytical.
ACCOUNT: PROJECT: SDG: DATE/TIME:
11VA Resources LI695669 01/24/24 09:55
PAGE:
20 of 21

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WQ0041111666
Final Audit Report
Created: 2024-04-17
By: Brent Collins ([e-mail])
Status: Signed
Transaction ID: CBJCHBCAABAAcOIPXZ6nxeFz7PFIXY-OgRqs_iji5f2Y
Document created by Brent Collins ([e-mail])
2024-04-17 - 12:59:32 PM GMT- IP address: 206.85.202.26
jiii Document emailed to Erik Blankenship (erik.blankenship Ca)emaresourcesinc.com) for signature
2024-04-17 - 12:59:49 PM GMT
Email viewed by Erik Blankenship ([e-mail])
2024-04-17 - 1:20:57 PM GMT- IP address: 206.85.202.92
Document e-signed by Erik Blankenship ([e-mail])
Signature Date: 2024-04-17 - 1:21:49 PM GMT - Time Source: server- IP address: 206.85.202.92
Agreement completed.
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