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HomeMy WebLinkAboutWQ0007798_GW Monitoring_20050429i IN UL 'l-1 I-ANI IN( CONTRACTORS AND CONSULTANTS CIVIL • GEOTECHNICAL • ENVIRONMENTAL ; RESULTS OF GROUND WA rR _t!.tivr-u _ SAMPLING EVENT JAN 20 2006 -`- (NOVEMBER 2005) 1 DENR-FAYEffEVILLEREGIOML0fCl PERMIT No. WQ0007798 TOASTMASTER, INC. - INGRAHAM TIME PRODUCTS FACILITY GROUND WATER REMEDIATION PROJECT LAURINEURG, NORTH CAROLINA PREPARED FOR: NORTH CAROLINA DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES DIVISION OF WATER QUALITY RALEIGH, NORTH CAROLINA DECEMBER 18, 2005 PREPARED BY: GULFSTREAM ENVIRONMENTAL, INC. 8633 VINTAGE CLUB DRIVE WILMINGTON, NC 28411 (910)612-4853 Pt GULFSTREAM Environmental, Inc. 8633 Vintage Club Drive Wilmington, NC 28411 ♦ Environmental ♦ Geotechnical ♦ Materials Testing December 18th, 2005 North Carolina Department of Environment and Natural Resources Division of Water Quality P.O. Box 29578 Raleigh, North Carolina 27626-0535 RECEIVED JAN 2 0 2006 DEAR -FAYErULLE REGIONAL OFFICE Re: Results of November 2005 Ground Water Sampling Toastmaster, Inc.- Ingraham Time Products Facility (Permit No. WQ0007798) Ground Water Remediation Project Laurinburg, North Carolina Dear Sir or Madam: In accordance with the new permits issued February 15, 2005, we are forwarding the enclosed monitoring report outlining the results of the November 2005 Ground Water Sampling event conducted on November 7th, 2005 at Toastmaster, Inc.- Ingraham Time Products Facility in Laurinburg, NC. Following, you will find: Appendix I .......... GW-59-A Appendix 11......... GW-69 Compliance Monitoring Forms Appendix III........ Laboratory Analysis If you have any questions, or if we may be of assistance, please contact us at 910-612-4853. Sincerely, Rudy A. Smithwick, P.G. President cc: Mr. Larry Clark/Mr. Mike Kraus, Toastmaster, Inc. APPENDIX I GROUNDWATER QUALITY MONITORING COMPLIANCE REPORT ]FORM GW-59A GW-59A COMPLUNCP REPORT &ORIIM Permit # W 4CJooZ7g8 ' (Submit one each hminftoring period with GfY--59 forms.) 1 Enter date monitoring results were due. Will this monitoring report (GW-59 and GW-59A) YES NO be submitted after the established due date? ` 2 Was any required information -missing on the GW-59 report forms? YES NO IF the answer to question t or 2 is OYES', list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged coring, unlocked or missing cap, missing YES NO identification plate, area overgrown, eta)? Ifthe answer.fs "Yes", contact the Regional Offecefor guidance. 4 Are any monitored constituents equal to or above the established standards? 'M NO If the answer to question 4 is'NO , sidp to section & If the answer to question 4 is "YES" list the affected wells individually with constituents) and concentiation(s) exceeding standards in the space provided below. 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is "NO', skip to section B. If the answer to question 5Is "YES" list in the space provided below, each well with constituent(s) exceeding standards, concentrations) reported, and sample collection date for each occurrence (for the last two years). 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer is "YES", a groundwater qualfty problem maybe occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELYFOR GUIDANCE ffthe answeris "NO" monitoring wells maybe improperly located; contact the Regional Office. 7 Is the pennittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is TES, describe those actions in the space provided below. If the answer to question 7 is "NO" contact the Regional Office within 90 days., an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the vermittee to a Notice of Violation, fines, andforpenalties. g The person completing this portion (G W-59A) of the monitoring report should sign below and submit this ' form with GW49 forms for required wells to the address provided at the top of the current GW-59 form. 1 helebyacknowledgrththe above"InforrtaLonuas evarua(ed and themformation submitted in tjhls` rtporE (Ggmpl(apce Repor,C;GW59q)'is,tiue,arid:cogiptete to"thebest of my knowledge � �:: � � `: - Signature of Pe dtee (or Authorized Agent) Date GW-59A 12/8/2003 NIA V/A APPENDIX II GROUNDWATER QUALITY MONITORING COMPLIANCE REPORT FORMS GW-59 SUSMlr FORM ON YELLOW PAPER ONLY GROUNDWATER 014ALITY € ONETOR'IN ear Type FacI iiy Pemil Gast4;Cc4Petson:S>i'd"-i;-1 c_c,wmctc. -:.. Telemone4;Y Satifeit. Letcdao& Site Name' _ -, No. of iNells toLn c.- Weli Cepft fl- Well Diameter:— in. etc Coo � Influent Inlwval:,.�.,.._.: it to ft. Depth to Water Level: !O . -O fL 9 Foi below measuring ni. � cif€uent Measurfng Point (M.P.) is: W ft. above land surface. Relative M.P. Cievation In fL:r Gellons of water ptamPeftaFfedbefore sampling: Qata-sample collwed: ,,�- Feid analysis: pH 5-2-9 Specific Conductances uMhos Temp. i 8. 3._ °C, Odor - Appamnpe — PERMIT9: EXPiRA iCiM DATE: Ncn-012sehar€1e_W_Q 00037 NPOES TYPE 4F PERMITTED OPERATION BSING MONITORED --.. Lagoon RekndaliorrInfittration Gallery Spray Field _ Rc ate: rs_ F3�4asyr@?slr�utar.,�,�,-Lanvw�Lsatiaa ai.Siu5o2 �'-' . 45ther - NOTE and d0801mat concentrations. Date sample analyzed: i � �, as €:aSoeato°yDame: e L-. _ A516M_VQF4„fS Cermcationmo._f#st - 2iiaLM9=(Samples for metalstvere oolfeoted unfl Sexed —YES —NO and field soidiffr-d .—YES ^ Nq COD m`O Nitrate (NO2) as N mgA Ni - Nickel Colafoam. MF Fecal 1100mi Nitrate (bf0a) as N fragl➢ P® - Lead _ melt Coliiform: fit€!" Total _ lmflmS Phosphorus: Total as A___._— m,gA Zn - Zinc MgA (Notc- Vw WN method Sar htnhl;r turbid mmglem) Orthophosphate m9A Ammonia Nitrogen ,,.. rrign Dissolited Solids. Total mgii Al - Aluminum mgA father {Specify Con grounds and Concentration to hs} pH (w when analyzed) 5. 33 units Be - Baratdt*t faagli i OC MgA tea - Calcium ing/I [C chioride _ rngfi Cd - Cadmium Arsenic mgA Chromium: Total Grease and Oils mgA Cu - Copper mgA Phena€ Sulfate _ mgA Mg Fe - Iran mg/i €%tg - Mercury I' L�TE ;� M411 OFfiGANIC$- (GC,GCtM8,HPLC) test Spe0ffl0C0rtdttctanCe:.a.._ _.. uFr hos K- Potassium MWI (Specify and methad 4. At£ach lab mpa, t.) Reportftac d? fss✓(t} Nc,____(Q) Total Aumm-ovila.,.�- -..�.� ti - Meg iers1 �'Ht"iY I y. -.f` � VCbC #= C3-G{:ten f T KN as N ._ mgl Mn - Manganese - ing/1. method F Permit Name (if Well Localictlt SU9MI i" i�. RM ON YELLOW PAPER ONLY County Telephone ts73 No. a' Webs is be or Type e t a r PESZIT R: ruetn ruerevin.4uotx evm uGr;tmm reiE79t7f;, tc w — F07 gpry 4'Cst�f TreaPtttetit SpSteiri3 :'del!Depth: ft WOUDIameter: - in. Giw^M.tlna: tatfitzenf {9S) Sareanetd Interval: IL to ft. ZWfftuent (99) Depths to Wafer l ev2(:, (2.� . below measuring point. Measuring Point (M.P.) [g:— ft. etfove land surface. Relative M.P. Elevation In If.: Gaffons of water ipumped ailed before sampfing: Date r,,jmpta eoflectad; 1 O � Maid analysis; H 5 SpeciffoConduclarica uMhos Tean�`G, Odor - Appearanaa -- - oEPARTmEur of, crmalotmtw, 6,iiATumt tiasouncEs WATER QUALM oiVI510%, GROUNI 1YATER SECTIOU EXPIRATION RATE: - NP®ES____ - _ TYPE GF PERMITTED OPERATION BEING MONITORrED f-aaoon X Remdatfan:tififrationGallery Sptay Feld _ Ramsdiafbi: _ Rotary Distributor ,........ Lad Agpacafton of:Siudoaz Other, r - NGTE- Values should refloat dissolved and . L� colloidal concentraUares. Bats sample analyzed: '71 05 Gti Laboratory Name: �4a�IG�}�wttt cLaOif P-16S Certifloation No.. get, _ P9RAIUI %OC (Samples for motals were collected unfliterezl_____YES —NO and field acidtffed co~ �I mgtl Nitrite (NO2) as N mgA Colifo= MF Fecal �pl00mf Nitrate (NO3) as N lmglt Colfforntl MP Total /100ml Phosphorus: Total as P - mgfl twa� It" "PH mew d Ca9r n=Qrx f, eure¢a umvt«a} Orthophosphate Mgii OW —Dived Solids, Total mgli Al -.Aluminum zngll phi (when analyzed)- 5 a$ unfits Ba- at7tr l ettgfl TOO M0,1f Ca- Calcium mgA Ohio de _ - - mfgn Cd - Cadm°aut,a rmgA Aiwrdc mgA Chromium: Total - mg/i Grease and Oils mgll Gu - copper m9A Phenol mgA Pe - Iran m511 Sulfate _ . mgA t%g - Mercury mgo Spediflo conductance -umhos K - Potasslum rrrgf( Total Ammonia mWI Mg - Magnesrelm rr+tigti T KN as N — mgA Mn -Manganese ,__YES fd'C) Ni - Rlickel Pb - Lead _ m9n Zn - Zinc _ mgfi Ammonia Nitrogen mgfl, Other (Specify compounds and Concentration Unla') cg - f_ ORGANICS. (Gc.ccfms,HPLc) (Specify test and tflathod>9. Attach lab rouort.) Repoit Att>ached2 +`e (9) No _-(a) VOC method Q =y -;21 1 J method 0 = Facility Name Permit Hame Weii LomtfW Site SUBMIT FORM ON YEi.I PAPER ONLY County Tctepieone bt:��� No. of Weis to brf or Type ­11 ei r-ct natg... 4=1 FGP Ga°oW3vtrst:Y Tre2prt2rt4Sy IE1r;:� Well Depth. fl dYeil Diameter: I in, Check C A%® Influent (98) Screened fntervai; _ t. to R. E1 Effluent (99) Depth to Water Level:,�drf. below measuiiog paint. hlaasurrV Paint (M.P4Ig:5• I ft. above farad surface: Relative .1,01 P. Elevation to ft.: CW7onS o9 water p€anyped/' died sampling,: f . 5 D�atm sartpYs collected: u ,� o� I"ieldanaiy53S: F{ (7 Spa Ific cowtictance' iFi1 107. p Terip.l OCR Odor AppearaitCS ENV'IRONREM & NATURAL RESOURCES PERMIT 9: EXPIRATION DATE: N0rftDisehargeWQ00(Q7j 795 Uti _` TYPE OF PERMITTED OPERATION BEING MONITORED Eagoon X Re nedietirir. Infiltration Csa.G;<y Spray Flow _.F>Msi 1ft Hotary Disuitiutas —:Land Ataptseaflon of Sludge other, WM' Values should reflect dissolved and . colloidal concentrations. W Date sample analy ed: d' 11 2,1 0-5 M Laboalory Name: V.—A IQ m_AMAU CAI A86i=@ g§ Gefitiraticn Na. SA AAR62FI 01,4 (Samples for metals wore reflected unfiltered_____ YES —NO and field nofdifled COD mgA Nitrite (NO2) as N mgA Collfo¢m: MF Focal ___ 1100ml Nitrate (NOS) as N vrsgh Cofiform: MF Total /100mi Phosphorus: Total as P. mgA tracsr~v= to" MetEe+dfor w4bipruresd.Imnfacy Orthophosphate mgA Dissolved solids: Torsi mg(i Al - Aluminum mgA' p;H (wit*.en analyzed) y - A 9�� unties Sa - Barium mgA TOC. mg/i Ca -Calcium mgA Chloride mgli Cd- Cadmium— mgA {arsenic rlrgA Chromium: Total mg/I (grease and Oils mgA Cu - Copper mg/I Phenol. mgA Fe - Iron mg/I Sulfate mg/I Hg-.Memury MqA Specific Conductance uMhos K - Potassium - mgri Total Ammonia mg/I Mg - Magnesium mg/I TKN as N mgrl Mn - Manganese - _ mgfl — YES i NO) Ni - Nickel _ mgti Pb - Lead._ _ m9A Zn - Zinc _ mg/I Ammonia Nitrogen.._.,_ _ mgfl Other (5pecit'y compounds and concentration unhs) g. ORGANIC$: (GsC,CaC MS;I1fiLC) (Specify test and m€ tthod a. Attach dab r porl.) Repot Atfthed? Yes 11i Ito __ (a) V00 : method 9 = &C Con I : medrod r s method 0 SuStei? EORPA ON Y 'L n €°ACER 0mLY GROUNDWATER QUALITY MONITORING: or Type racillty Same: - Permit Name (If ContactPersort cr -- __. Telepfronafc` S-SOS-3617-: m t( 4yelE L�a9iofci Site Name, Pif-3V75io; No. of WalL- to bo Sampied 49a Weil ldentiiicatitrtNumber (from Permit): M.1X_S � ForGromd—st'? rz�lrnnBSy:t�re Weft Depth: ? 1. O fL Well Diameter: :I-. Mecb, 01 . � influent (98) Effluent (99) Depth to Water Level: �5f N. below measuring Measuring Point W.P.) W-1 I ft. above land surface. Relative MP. Elevation In fi.' Gmons or Irate! pum�� d1balled before sampling: 2• o Date sample cctllecfeef: QS Meldarcalgsis: pI'l. Y• �.�L�._ SPBCjiiCCOmd6!eti3mCe. uia5ftilr: Temp. ��°G, Odor Appearance t7EPARTW EWOF MVIRONYIMT @: HAWRAL RRSO 1ACES WATER CiiALRY DIM10H, Ut'�fYJ.'J`WATER sEGTIOU 1'"MkEi.. Gfd:1PFCE C^'cFdTEm U. II t'ERhiff #: EXPIRATiOM DATE: -- Nen-Disrtargewoc-)Op22-95 u3 —_ _ NPDES TYPE OF PERN11 1) OPERATION BEING A$Oh'ITORED Lagoon X R2[rio-otallominfiara0unGallery spicy Field Rr imfoa: c_ Rotary Distributor — L€anct E :a>.ton of $tud,;la 6:fh:r_ t pUQM3 Values ;should reflect disscNad and . s"3 colloidal ccesces4traYtmns, Lute sample analyzed: i !' MI 05 LaboratoryP3arme: cAt. I..AB R1(SS CeriitEostictl lac. �%k�l. . PARAPJI RS (Samples far metals were collected unfittered— YES _NO and field acidified —YES —110) con mgfl 1900ml Nitrite (NOa) as N Nitrates (NOS) as N mgA mg/l Ni - Nickel mgfi Conform: MF Fecal — Pb - Lead- _ rngA Conform: MFTotal /100mi Phosphorus: Tonal as Fes, mqA Zn - Zinc _ moil (Note;tlx:MPNmethod fbehighivhlrbwamplea) Orthophosphate moil Ammonia Nitrogen —mo Dissolved Solids: Total mg/l Al - Aluminum mgtl Other (spec14f compounds and ConcentratIan unita} p..4 (when analyzed) PT. I I unhs Ba - Fsarfurri mg/1 tngli co - Calcium mgA Chloride, ____ mg/l Cd - Cadmium— mg/l Arsenic mgli Chromium: Total mgA Crease and Oils. __ mgA Cu - Copper_ - mgil Phenol mgA Fe - lion mg(f ORGANICS: (GG,GORa S,HPLC,) Sulfate mgli utillhos Hg - Merrury K- Potassium mg/l rng/f (Sreaify test and method E. Aft,ch lob sport.) RepartAttachad? Yeses: "(t) No_—(0) Specific Conductance - - Total Ammonia mg/1 Wig - Magnesium mglt VOC method P -_ Cd1D l TKN as €tl ,mgA Mn - Manganese mgA method a method 0 = Facility Name:..l Permit Hams (if Well Local rifSite SUBMIT PORM ON YELLOW PAPER ONLY Tdephone a -:'a PAS No. of Wells to be or Tjfpe Well ldentiiiatior~ Number (from Perttttt); M VV - le r Grou Meta* Tr@atmeimS SAS€cam wen Depth: 35. O et: Wen D etec Z__a_O m. CYter.YiOn„: ® fstfluent (SS) Screened t Water ft. b S�� it. 0 Effluent (99) Depth to Warr Levrfi° ft. below measuring pain[. Measuring Point(KLP.) l9. • A ft. above land surface. Relative M.P, Elevation in ft.- Gailonsof water Baum, ��rb4ied before sampling, LOB Data; sample collected; (I o S Feldanatysis; pH_reSI I Specific Conductance u9dihos Temp, 2�L°C, Odor— Appearance DEPARTKAMOF ENWU30NR LME NATURAL RESOURCES WATER QUALM 01mloij, GP.aUNSWATM SSM0f1 -laAll.sytcee�taTEA .�`i PERMITIP EXPIRAT90NDA.TE:� Non-DischargeWO-0-0 i1i9 NPDES_ TYPE E EBMyrj.rp OPERATION BEING MONITORED Lagoon X Rernadlalion: infiftratlan Gallery Rotary Mstrbutar - _ _. Lane Aitpteallon LI' Sfucgs, Other: r NOTE: Valuer should reflect dissoived and E3 colloidal concentrations, c� Vale,.aample analyzed: Laboratory Name: 10rrmn_ANAWInCAL A69@M_S SS Cettlti,;attor! iVff. ��f. - PARAMEFERS (Samples for metalswere collected unfiltered —YES _NO and field-aotdtfled — YES _ NO) COD m9A Nltdte V02) as N mgA Ni - Nickel— _ m9Ji Coliform: MF Fecal !t ODMI Nitrate (NO3) as N rngA Pb - Lead w_ _ - mg/1 Colfform: MF Total �1100mi Phosphorus: Total as P mgA Zn - Zinc - mgA grrozE: tuc 10H method Far mortis turbid t;arrpiesj Orthophosphate mgft Ammonia Nitrogen O -MO Dissolved Soltds, Total rmgft Al - Aluminum mg/I Other (SpecaYCcmpottnds and Concentration urns) p; t (kvhen analyzed) 5 2 7 units Ba - Bariun m9A TCC mg/9 Ca - Calcium mgA TC (. g Chloride mg/I Cd - Cadmium— -- mgA Arsenio mgA Chromium: Total rngfl Grease and Coils mgA Cu - Copper F g/I - - Phenol mgA Fe - lion mqA ORGANICS: (GC,CCtmS,HPLC) Sulfate mgA h(g - Mercury rmg/I (Specify test end method ft. Attach lab report.) SpecificCondaletance umhos K-Potassium - mrgfl PepaftAftched? Yes!(7j Nis—(C) TOW Ammonia _—_ o____ mgfl Mg - Magnesium mgh VOC : method 9 _ TKN as i t mg/l Mn - Manganese mgtl : method P+ -fi:Lfa_ method 0 - CP SUBMIT FORM ON Yam- t V PAPER ONLY Facility Name:_ Perm i name (if _f... wo w,Fsul6+? Count}t.��rCs-�•tD contact Person:L Y GLA '�zg' '*' (ZVI Telephone Wets LcoatfaniSite Nama't.R�-Wq'l' No. of Wells to W Sampled: .._._------------_ io is -. _ ET 4 r - - ln.m r:arinu). Zvi .v— GrL`td;?dwaleer TP-,ritmEtil Systwis INLA Depth 25.0 4L WellDiameter:2• D In. Ch Gnat ® Influent (98) Scrowed Interval: 2 • S ft. to !Si D ft. ®�dffueatt (33� Depth €oVlraierLsaeE:IS. S fiWowmeasuring,point.. Nteasuring Pvint CM.P.) is:_ ft. above land surface, Relative M.P. Elevation to 4P:: _ Gallons of water pumped ted before sampling: (c D Data sample collaefed: oS Field analysis pl ! specific Conductance umhos Temp; °C, OdoP Appearance 'HATER & 14A UR,AL RESOTIRCES vDWATc-R SECTIOR PERMIT d: EXPIRA`nON DATE: __ Non-DischargewQ000-1 95 Ulo - - NPDBS, _ _._,. TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon X Re nlern Inf4Rrallan Gallery Spray Field _ Heir diabw Rotary fNsirbutcr Land aweatiaa of sluegs . Cttwr, i NOTE; Values should reflect dissolved and - colloidal concentrations. Date sample analyzed: Laboratory Name: A Mrn AMiiLY-n l. I-ASOWMIZiSS - Centitcation fvo:.. kill . t5 EARAMETEFS41 (Samples for metals were collected unfiltered —YES —NO and field aoidified COO) mgA Nitrite (NO2) as N mgA Coifforrri: MF Fecal 1100mi Nitrate (NOS) as H emg/f Coliform: MF Total 1100mi Phosphorus. Total as Pam, mgA 04V=PAMMethod °urtdshtYXUrbidaiMpt") Orthophosphate mgtl Dissolved SdIds: Total ._ rngff Al - Aluminum mga pH (When analyzed) t-[_ - Ia u; iifs tia - Barium mgA TOG rngfl Ca - Calcium mqA Chloride mgA Cd - Cadmium_ - mgA Arsenic mgA Chromium: Total fmgft Grease and Oils mgR Cu - Capper rng/i Phenol mgA Fe - lion mg/l Sulfate mgA Hg - Mercury mg/I Specific Conductance utdlf os K - Potassium t-mgdl TotalAmttonk - mgdt Fig -Magnesium rng/I TKN as N mgfl Mn - Manganese mgA .._.._YES — NO) NJ - Nickel— - - mgn Pb - Lead- _ mgA Zn - Zinc - mgli Ammonia Nitrogen _mrsfi Other ($peclty Compounds and C©ncentratlun UdMl ORGANIC$: (GG,GCx j, 1FLC# (Specify test and method 4. At'tach tab rq;;rcrl ) RepertAtta&ied? YP.s✓(1) Na_®(Gi) VOC ; method rat : method 0 Facitily Nam: Permit Name well 5USMIT MRM ON YF4l<Uq PAPERO,\tLy County _� Telephone 4:573 No. of Wells; to be Waft Identification Number (from Permit): M-w l Q � far Groam�'72terTre3YSl:eljS Systc Wall Depth 25. C- It Well Dlametec in. Meakft;0 Influent (g&j ,osac-reed tntvruac..Z.,��€#_ to 2-5 - o it. t� �tfttserlY (9g} Depth to Water Leval: .f L ft. below measuring point. Measuring Point W.P.p ts: 25 it. above land surface. Relative M.P. Elevation In It.: Gallons of Water pumpedlballe i belorazampti r 33. o Oatn sample! collected: 1 a Fmld analysis: ptiq,9 0 Specific Oonductanco—uIusycs TemP,!Q' 3 °C, 0(for Appearance OEPARTrr F Ir OF &AWRONtsr°3`Y`+ 6 NATURAL i,csOURCEs WATER CUAUN DWMION, GROUNDWATER SEMI= a�sefeaft,seaTVlLscE�ER Elul. NPDES Splay Field Rotary D'rstrijauter .,� other. EXPIRATION DATE, WERATION BEING MONITORED _.Retnetlia3iore:Mfil[rztionGailvry Lend Ao%slim oI Slu.-g- . NOTE Values should raftsat dissawcd end colloidal concentrations, f)Ate sarmla AnKlvrM- l.I f 1.7.1os Laboratory Name: certification No. PABC MRTLM (Samples for metals were o0ilacted unflitered—YES —NO and Field acidlfIPd COD mg/I Nitrite (NO2) as N rngA Collform: MF Fecal /100ml Nitrate 0403) as N mg/i Coliform: fYIF Total 1100ml Phosphorus: petal as Fes., magi! 0402=TJUR!'WtnethodI=hlghlytUrbldaantplatj Orthophosphate Mg/i Ulssolved Solids: Total rng/I Al - Aluminum nab P-Li (saflari a aalyesd) H - S units Ba - Barium mgi i 0C MVI Ca - calcium mg/1 "Waride Trig/! Cd- Cadmium mQ_A Arsenic rnglt Chromium: Total mg/I (crease and Oils rngll Cu - Copper rngfl Phenol ✓rag/! Fe - lion mg/1 Sulfate mgA tig - Mercury M&I SpaciEIC CandVGlanre_ _ uMhcs K- Potasslurn mvi Total Amrrlcnia €ng/f Mg - Magnesium mgEl TKN as €V mgI Mn - Manganese mgfl t.� —YES l 10) Ni. Nickel mg/1 Pb - Lead_._._ _ mg>i Zn - Zinc _ Aig/I Ammonia Nitrogen _ MO Other (specify Compounds and Concentrallun Units) _TC • 1 _19 111 f RGANBCS (GG GC/MS,HFL0) (Specify test and method P. Attach lab mport.) ReportAtteahed? No-_(0) VOC method 9 = I method A = mm1?,nrl �:- GROUNDWATER QUALITY MONITORING: : Permit Name (if Wall Lccatita€tj Site SUBt1MF-ORM ON MLIatV PAPER ONLY County �T4 Telephone 5:5"P3 No. c: Welts I t)e -- tFrrGmunftt: ,TMatmmm tSptarcw 1 of oeptfr ZS _Oft. Wall Dlameter: `f ,O in. cted,One; 0 Influent (98) Weaned Inteml [,, o it to 2S` 0it. ® fftueni (99} Depth to WWater Lae2L f & Z A, below measuring point. MeaSurh9 Paint (M,P.) ft. abova land surface. Relative M.P, Elevation in ft.: Gallons of water pumpedRrafted taefore sampling: L •a Data sample collected: (� Field analysis: pH H - q 1 Specific Conductance a4h rs Temp. �K °C, Odor Appaarance DEPARTR'Ear OF WATE.4 QUALM I PERMIT €: EXPIRATION DATE: Nen•Dischrarga�QQ001'79b uiC NPOES Ty=PEOF PE_8MJTTED OPERA'r ION MNG MONITORED Lagoon.2f._.-..R�m2dialfan:infiltration Gallery Spray Freid IierrediatDtY Rotary Distributor Land Appkatiiar, of Stud�a r_ KMZ '4faiueu Should reflect dissolved ano' . C,y colloidal concentrations. � Orate sample analyzed: 6S , L boratory Name: aflr�lG t e 1 a$�Ft� &S Cetwicalion No.. Yet - f1_A_RAfffM(Samples far metals were collected van€itterecF______YES ____NO and fieldacIdified '0D mg/I Nitrite (NO2) as N mgtt Conform: MF Fecal /j aft Nitrate Ma) as N mg/t Colffarm: MFTotal 1100ml Phosphorus: Total as P .- rr o (Haze -Use rAt"neth6d Faz high§Y rssrtkr armpits) Orthophosphate. _ mg1l Dissolved Solids: Total mg/l Al - Aluminum mgll pi(whenana(y7ed) 5 O units Ba-Barium MCA 'C Ca- Calcium mill Chloride -- - mgA Cd- Cadmium mg/l Arsenic mg/l Chromium: Total,, mg/I Grease and fails-- _-- rngn Cu - Copper— mg/1 Phenol mg/i Fe - iron _ tng/I Sulfate _ mg/( Hg - Mercury - - _ mgA Specific Condu=nce ui hos if - PotassiuTrr mo Total Ammonia €ng/I Mg - Mag msium _ mg/1 TKN as N mg/l Mn - Manganese mg/l ____ YES NO) Ni - Nickel Mg/f Pb - Lead _ mgA Zn - Zinc _ mg/1 Ammonia Nitrogen__— m9h Other (Specify Compotuids and Concentration Uni s) Z241 UgrL ORGANICS. (G0,GCAA1iS,HPL0) (Specify test and rrrothod 9. Attach lair mp arf.) RepadA'ttached? Ye,,/(1) No_(0) WOC method f iaa I metftod meifusd Gt = Facility Name:J PePrnit game (if Well 1.00eff n! Site SUBMIT FORM ON YQELLQV PAPER ONLY TatepRorie t: No. Cf'wells 'to eueit Dept fn,ssovix rvudrwut (er[3ii: Well . Main at ER...m.. rTrL*nta tt Systrum e€t tiffs 3fa• O fL Weil f3fameFer..4 r? (R €nfluent (98) Screened'Intendat. (e• O ft. to BD. O ft. Effluent (99) Depth to Water LovehILU[,_ff, batowmeaswing point. Measudng. POInt (Rt,P.) W b—_Z- ft above land surface. Re s71ve tA.P. EPe eauon !n ft.: Oaflan5 of cuafee porn ed/baAe6 before sdmplirtg 3c1. D Data tsampls Collected: UM �a� fiietdanalysts: pH i Specific Conductance Umhos Tom. Zv' 'G, Odor Appearance OF EMIRONIFAi a HAIVRAL:RZSOUiCES rY DiVISION, GAOUNDWATER St"F Off Yic.E Ci:t=Sm-M ROW PERMIT tf: EXPIRATION DATE Non-€3ischargew-G OOt7 -1�U10 NPDES TYP_OF PERMITTED OPERATION eEfNG MONITORED Ea000z. ._.,Remedfaiiom InfiRratfon Galtory Sprays efd �Ratnadiafen: Rotary Di3lnbulor —Land A ttcallono!SUdge -r 4ttwr,__ _.. NOTE Values should rePde-cE dissAtvec3 CRct.. c.5 colloidal concontratiorm "o V� Date sample anallozed: i l P R.1 as iabo:atoryNasnN.Aiyipjor e�,6,YaacRR et8a c0 E5 Certification No.:Ast . P VIE9PS (Sasnpleo for metals Were collected unfiltered YM _-___NO and field acidified Cori M94 Nitrite (NOz) as N mg/1 Coliform: MF Fecal _ -- !t OOml Nitrate (NO3) as N mg/f Colifdrm Total 1100ml Phosphorus: Total as P — - - _- mgll Val= U=f1w" Methodrw hkhly turbW=(West Clithfl os hater m f Dissolved Scifds: Total mgn Al - Aluminum mgA analyzed) S" E I pPi units Ba - Baduin MgA nwhen mg/t Ca - calcium m9A Chtor€de mgii Cd - Cadmium mgn Arsenio mgn Chromium: Total mg/! Grease and Offs mgA Cu - Copper. mg/i Phenol mgA FP - Iron mg/t Sulfate. mgli Fig - Mercury mglt Specific ConductanCe uMhns K -Pofzwium_ mgA Total Ammonia mg/! Mg, -Magnesium mg/€ TKN as N — mgA Mn - Manganese mgfl YES —,NO) Ni - Nickel— _ Ing/i Pb - Lead _ mgii Zn - Zfnc _ ntg(€ Ammonia Nitrogen_ _mo Other (Specify compounds and cmcerltrallon Units) _ Uj G ORGANICS: (eC,o ln° ;KRac) (specify test end Method n. Attorh &Eb report.) RepodAttached? Yes✓(t) No_®(Q VOC method ". metPtQd 9s m�lhad N APPENDIX III LABORATORY ANALYTICAL RESULTS PARADIGM ANALYTICAL LABORATORIES, INC. 5500 Business Drive Wilmington, North Carolina 28405 (910) 350-1903 Fax (910) 350-1557 Mr. Rudy Smithwick Toastmaster, Inc. 8633 Vintage Club Dr. Wilmington NC 28411, Report Number: G420-55 . Client Project: Toastmasster Laurinburg Dear Mr. Smithwick: Enclosed are the results of the analytical services performed under the referenced project. The samples are certified to meet the requirements of the National Environmental LaboratoryAccreditation Conference Standards -Copies of this report and supporting data will be retained in our files for a period of five years -in the event they are required for future reference. Any samples submitted to our laboratory will will be retained for a maximum of thirty (30) days from the date of this report unless other arrangements are requested. If there are any questions about the report or the services performed during this project, please call Paradigm at (910) 350-1903. We will be happy to answer any questions or concerns which you may have. Thank you for using Paradigm Analytical Labs for your analytical services. We look forward to working with you again on any additional analytical needs which you may have. Sincerely, J. RAtrick Weaver Laboratories, Inc. N.C. Certification #481 S.C. Certification #99029 1 of 26 r PARADIGM ANALYTICAL LABORATORIES, INC. Results for Volatiles by GC 601 Client Sample ID: Effluent Analyzed By: MJC ` Client Project ID: Toastmaaster Laurinburg Date Collected: •1119/05 0:00 Lab Sample ID: G420-55-1A Date Received: 11/10/05 ' Lab Project ID: G420-55 Matrix: Water I ' Analyte Result RL Dilution Date uprL uglL Factor Analyzed ' Bromodichloromethane BQL 1.00 1 11/16/05 ` Bromoform BQL 2.00 1 11/16/05 Bromomethane BQL 1.00 1 11/16/05 Carbon tetrachloride BQL 1.00 1 11/16/05' Chlorobenzene BQL 1.00 1 1,1/16/05 Chloroethane BQL, 1.00 1 11/16/05 Chloroform BQL 1.00 1 11/16/05 Chloromethane BQL 1.00 1 11/16/05 Dibromochloromethane BQL 1.00 1 11/16/05 1,2-Dibromoethane (EDB) BQL 1.00 1 11/16/05 1,2-Dichlorobenzene BQL 1.00 1 11/16/05 1,3-Dichlorobenzene BQL 1.00 1 11/16/05 1,4-Dichlorobenzene BQL 1.00 1 11/16/05 1,1-Dichloroethane BQL 1.00 1 11/16/05 1,2-Dichloroethane BQL 1.00 1 11/16/05 1,1-Dichloroethene BQL 1.00 1 11/16/05 cis-1,2-Dichloroethene 1.08 1.00 1 11/16/05 trans-1,2-Dichloroethene BQL 1.00 1 11/16/05 1,2-Dichloropropane BQL 1.00 1 11/16/05 cis-1,3-Dichloropropene BQL 1.00 1 11/16/05 trans-1,3-Dichloropropene BQL 1.00 1 11/16/05 - Methylene Chloride BQL 5.00 1 11/16/05 1,1,2,2-Tetrachloroethane BQL 1.00 1 11/16/05 Tetrachloroethene BQL 1.00 1 11/16/05 1, 1, 1 -Trichloroethane BQL 1.00 1 11/16/05 1,1,2-Trichloroethane BQL 1.00 1 11/16/05 Trichloroethene 11.5 1.00 1 11/16/05 Trichlorofluoromethane BQL 1.00 1 11/16/05 Vinyl Chloride BQL 1.00 1 11/16/05 - Surrogate Spike Recoveries Spike Spike Percent Added Result . Recovery I 1,4-Dichlorobutane 40 39.4 98.4 1 Comments: All values corrected for dilution. BQL = Below quantitation limit. Reviewed By: GCL-UMSV?0'12 of 26 N.C. Certification #481 S.C. Certification #99029 PARADIGM ANALYTICAL LABORATORIES, INC. Results for Voiatiles by GC 601 Client Sample ID: Influent Analyzed By: MJC Client Project ID: Toastmaaster Laurinburg Date Collected: 11/9/05 0:00 Lab Sample ID: G420-55-2A Lab Project ID: G420-55 Analyte Date Received: 11/10/05 Matrix: Water Result RL ugiL ug/L Dilution Date Factor Analyzed Bromodichloromethane BQL 50.0 50 11/17/05 Bromoform BQL 100 50 11/17/05 Bromomethane BQL 50.0 50 11/17/05 Carbon tetrachloride BQL 50.0 50 11/17/05 Chlorobenzene BQL 50.0 50 11/17/05 Chloroethane BQL 50.0 50 11/17/05 Chloroform BQL 50.0 50 11/17/05 Chloromethane BQL 50.0 50 11/17/05 Dibromochloromethane BQL 50.0 50 11/17/05 1,2-Dibromoethane (EDB) BQL 50.0 50 11/17/05 1,2-Dichlorobenzene BQL 60.0 50 11/17/05 1,3-Dichlorobenzene BQL 50.0 50 .11/17/05 1,4-Dichlorobenzene BQL 50.0 50 11/17/05 1,1-Dichloroethane BQL 50.0 50 11/17/05 1,2-Dichloroethane BQL 60.0 50 11/17/05 1,1-Dichloroethene BQL 50.0 50 11/17/05 cis-1,2-Dichloroethene BQL 50.0 50 11/17/05 trans-1,2-Dichloroethene BQL 50.0 50 11/17/05 1,2-Dichloropropane BQL 50.0 50 11/17/05 cis-1,3-Dichloropropene BQL 50.0 50 11/17/05 trans-1,3-Dichloropropene BQL 50.0 50 11/17/05 Methylene Chloride BQL 250 50 11/17/05 1,1,2,2-Tetrachloroelhane BQL 60.0 50 11/17/05 Tetrachloroethene BQL 50.0 50 11/17/05 1, 1, 1 -Trichloroethane BQL 50.0 50 11/17/05 1,1,2-Trichloroethane BQL 50.0 50 11/17/05 Trichloroethene 505 50.0 50 11/17/05 Trichlorofluoromethane BQL 50.0 50 11/17/05 Vinyl Chloride BQL 50.0 50 11/17/05 Surrogate Spike Recoveries Spike Spike Percent Added Result Recovery 1,4-Dichlorobutans 40 37.7 94.3 Comments: All values corrected for dilution. BQL = Below quantitation limit. Reviewed By: cc uM _n "m 3 of 26 N.C. Certification #481 S.C. Certification #99029 PARADIGM ANALYTICAL LABORATORIES, INC. Results for Volatiles by GC 601 Client Sample ID: RWA Analyzed By: MJC . Client Project ID: Toastmaaster Laurinburg Date Collected:, 11/9/05 0:00 Lab Sample ID: G420-55-3A Date Received: 11/10/05 Lab Project ID: G420-65 Matrix: Water Analyte Result RL ug/L ug/L Dilution Date Factor Analyzed Bromodichloromethane BQL 50.0 50 11/17/05 Bromoform BQL 100 50 11/17/05 Bromomethane BQL 50.0 50. 11/17/05 Carbon tetrachloride BQL 50.0 50 11/17/05 Chlorobenzene BQL 50.0 50 11/17/05 Chloroethane BQL 50.0 50 11/17/05 Chloroform BQL 50.0 50 .11/17/05 Chloromethane BQL 56.0 50 1.1/17/05 Dibromochloromethane BQL 50.0 50 11/17/05 1,2-Dibromoethane (EDB) BQL 50.0 50• 11/17/05 1,2-Dichlorobenzene BQL 50.0 50 11/17/05 1,3-Dichlorobenzene BQL 50.0 50 11/17/05 1,4-Dichlorobenzene BQL 50.0 50 11/17/05 1,1-Dichloroethane BQL 50.0 50 11/17/05 1,2-Dichloroethane BQL 50.0 50 11/17/05 1,1-Dichlaroethene BQL 50.0 50, 11/17105. cis-1,2-Dichloroethene BQL 50.0 50 11/17/05 trans-1,2-Dichloroethene BQL 50.0 50 11/17/05 1,2-Dichloropropane BQL 50.0 50 11/17/05 1 cis-1,3-Dichloropropene BQL 50.0 50 11/17/05 trans-1,3-Dichloropropene BQL 50.0 50 11/17/05 Methylene Chloride BQL 250 50 11/17/05 1;1,2,2-Tetrachloroethane BQL 50.0 50 11/17/05 Tetrachloroethene BQL 50.0 50 11/17/05 1, 1, 1 -Trichloroethane BQL 50.0 50 11/17/05 1,1,2-Trichloroethane BQL 50.0 50 11/17/05 Trichloroethehe 480 50.0 50 11/17/05 Trichlorofluoromethane BQL 50.0 5o 11/17/05 Vinyl Chloride BQL 50.0 50 11/17/05 Surrogate Spike Recoveries Spike Spike Percent Added Result Recovery 1,4-Dichlorobutane 40 37.5 93.7 / Comments: All values corrected for dilution. BQL = Below quantitatlon limit. i L Reviewed By:ccu4.of 26 N.C. Certification #481 S.C. Certification #99029 PARADIGM ANALYTICAL LABORATORIES, INC. Results for Volatiles by GC 601 Client Sample ID: RW-2 Analyzed By: MJC Client Project ID: Toastmaaster Laurinburg Date Collected: 11/9/05 0:00 Lab Sample ID: G420-55-4A Date Received: 11/10/05 Lab Project ID: G420-55 Matrix: Water Analyte Result RL uglL uglL Dilution Date Factor Analyzed Bromodichloromethane BQL 50.0 50 11/17/05 Bromoform BQL 100 50 11/17/05 Bromomethane BQL 50.0 50 11/17/05 Carbon tetrachloride BQL 50.0 50 11/17/05 Chlorobenzene BQL 50.0 50 11/17/05 Chloroethane BQL 50.0 I 50 11/17/05 Chloroform BQL .50.0 50 11/17/05 Chloromethane BQL 50.0 50 11/17/05 Dibromochloromethane BQL 50.0 50 11/17/05 1,2-Dibromoethane (EDB) BQL 50.0 50 11/17/05 1,2-Dichlorobenzene BQL 50.0 50 11/17/05 1;3-Dichlorobenzene BQL 50.0 50 11/17/05 1,4-Dichlorobenzene BQL 50.0 50 11/17/05 1,1-Dichloroethane BQL 50.0 50 11/17/05 1,2-Dichloroethane BQL 50.0 50 11/17/05 1,1-Dichloroethene BQL 50.0 50 11/17/05 cis-1,2-Dichloroethene BQL 50.0 50 11/17/05 trans-1,2-Dichloroethene BQL 50.0 50 11/17/05 1,2-Dichloropropane BQL 50.0 50 11/17/05 cis-1,3-Dichloropropene BQL 50.0 50 11/17/05 trans-1,3-Dichloropropene BQL 50.0 50 11/17/05 Methylene Chloride BQL 250 50 11/17/05 1,1,2,2-Tetrachloroethane BQL 50.0 50 11/17/05 Tetrachloroethene BQL 50.0 50 11/17/05 1, 1, 1 -Trichloroethane BQL 50.0 50 11/17/05 1,1,2-Trichloroethane BQL 50.0 50 11/17/05 Trichloroethene 472 50.0 50 11/17/05 ' Trichlorofluoromethane BQL 50.0 50 11/17/05 Vinyl Chloride BQL 50.0 50 11/17/05 Surrogate Spike Recoveries Spike Spike Percent Added Result Recovery 1,4-Dichiorobutane 40 36.6 96.4 Comments: All values corrected for dilution. BQL = Below quantitation limit. Reviewed By:11W cc u _ve"5 of 26 N.C. Certification #481 S-C. Certification #99029 `i PARADIGM ANALYTICAL LABORATORIES, INC. Results for Volatiles by GC 601 Client Sample ID: MW-3 Analyzed By: MJC Client Project ID: Toastmaaster Laurinburg Date Collected: 1119/05 0:00 Lab Sample ID: G420-55-6A Date Received: 11/10/05 Lab Project ID: G420-55 Matrix: Water 1, Analyte Result RL ug[L ug1L Dilution Date Factor Analyzed Bromodichloromethane BQL 10.0. 10 11/17/05 Bromoform BQL 20.0 10 11/17/05 Bromomethane BQL 10.0 10 11/17/05 Carbon tetrachloride BQL 10.0 10 11/17/05 Chlorobenzene BQL 10.0 10 11/17/05 Chloroethane BQL 10.0 10 11/17/05 Chloroform BQL 10.0 10 11/17/05 Chloromethane BQL 10.0 10 *11/17/05 Dibromochloromethane BQL 10.0 10 11/17/05 1,2-Dibromoethane (EDB) BQL 10.0 _ 10 11/17/05 1,2-Dichlorobenzene BQL 10.0 10 11/l7/05 1,3-Dichlorobenzene BQL 10.0 10 11/17/05 1,4-Dichlorobenzene BQL 10.0 10 11/17/05 1,1-Dichloroethane BQL 10.0 10 11/17/05 1,2-Dichloroethane BQL 10.0 10 11/17/05 1,1-Dichloroethene BQL 10.0 10 11/17/05 cis-1,2-Dichloroethene BQL 10.0 10 11/17/05 trans-1,2-Dichloroethene BQL 10.0 10 11/17/05 1,2-Dichloropropane BQL 10.0 10 11/17/05 cis-1,3-Dichioropropene BQL 10.0 10 11/17/05 trans-1,3-Dichloropropene BQL 10.0 10 11/17/05 Methylene Chloride BQL 50.0 10 11/17/05 1,1,2,2-Tetrachloroethane BQL 10.0 10 11/17/05 Tetrachloroethene BQL 10.0 10 11/17/05 1, 1, 1 -Trichloroethane BQL 10.0 10 11/17/05 1,1,2-Trichloroethane BQL 10.0 10 11/17/05 Trichloroethene 77.1 10.0 . 10 11/17/05 Trichlorofluoromethane BQL 10.0 10 11/17/05 Vinyl Chloride BQL 10.0 10 11/17/05 Surrogate Spike Recoveries Spike Spike Percent Added Result Recovery 1,4-Dichlorobutane 40 36.3 90.7 Comments: All values corrected for dilution. BQL = Below quantitation limit. Reviewed By- GCJ ye.0'16 of 26 N.C. Certification #481 S.C. Certification #199029 PARADIGM ANALYTICAL LABORATORIES, INC. ' Results for Volatiles by GC 601 - Client Sample ID: MW-5 Analyzed By: MJC Client Project ID: Toastmaaster Laurinburg Date Collected: 11/9/05 0:00 Lab Sample ID: G420-55-12A Date Received: 11/10/05 Lab Project ID: G420-55 Matrix: Water Analyte Result RL Dilution Date -, / u611. ugli. Factor Analyzed " Bromodichloromethane BQL 1.00 1 11/16105 .. Bromoform BQL 2.00 1 11/16/05 Bromomethane BQL 1.00 1 11/16/05 Carbon tetrachloride BQL 1.00 1 11/16/05 Chlorobenzene BQL 1.00 1 11/16/05 n Chloroethane BQL 1.00 1 11/16/05 Chloroform BQL 1.00 1 11/16/05 Chloromethane BQL 1.00 1 11/16/05 Dibromochloromethane BQL 1.00 1 11/16/05 1,2-Dibromoethane (EDB) BQL 1.00 1 11/16/05 1,2-Dichlorobenzene BQL 1.00 1 11/16/05 1,3-Dichlorobenzene BQL 1.00 1 11/16/05 1,4-Dichlorobenzene BQL 1.00 1 11/16/05 1,1-Dichloroethane BQL 1.00 1 11/16/05 1,2-Dichloroethane BQL 1.00 1 11/16/05 J M-Dichloroethene BQL 1.00 1 11/16/05 cis-1,2-Dichloroethene BQL 1.00 1 11/16/05 :- trans-1,2-Dichlaroethene BQL 1.00 1 11/16/05 1,2-Dichloropropane BQL 1.00 1 11/16/05 cis-1,3-Dichloropropene BQL 1.00 1 11/16/65 -. trans-1,3-Dichloropropene BQL 1.00 1 11/16/05 Methylene Chloride BQL 5.00 1 11/16/05 1,1,2,2-Tetrachloroethane BQL., 1.00 1 111.16/05 Telrachloroethene BQL 1.00 1 11/16/05 1,1,1-Trichloroethane BQL 1.00 1 11/16/05 1,1,2-Trichloroethane BQL 1.00 1 11/16/05 - Trichlorbethene 6.28 1.00 1. 11/16/05 Triohlorolluoromethane BQL 1.00 1 11/16/05 Vinyl Chloride BQL 1.00 1 11/16/05 Surrogate Spike Recoveries 1,4-Dichlorobutane Comments: All values corrected for dilution. BQL = Below quantitation limit. Spike Spike Added Result 40 36.9 Percent Recovery 92.3 Reviewed By: sc_ures- zox�sl1 of 26 J N.C. Certification #481 S.C. Certification #99029 J i PARADIGM ANALYTICAL LABORATORIES, INC. Results for Volatiles by GC 601 Client Sample ID: MW-6 Analyzed By: MJC Client Project ID: Toastmaaster Laurinburg Date Collected: 11/9/05 0:00 Lab Sample ID: G420-55-7A Date Received: 11/10/05 Lab Project ID: G420-55 Matrix: Water Analyte Result RL uglL uglL Dilution Date Factor Analyzed Bromod(chloromethane BQL 20.0 20 11/17/05 Bromoform BQL 40.0 20 11/17/05 Bromomethane BQL 20.0 20 11/17/05 Carbon tetrachloride BQL 20.0 20 11/17/05 Chlorobenzene BQL 20.0 20 11/17/05 Chloroethane BQL 20.0 20 11/17/05 Chloroform BQL 20.0 20 11/17/05 Chloromethane BQL 20.0 20 11/17/05 Dibromochloromethane BQL 20.0 20 11/17/05 1,2-Dibromoethane (EDB) BQL 20.0 20 _ 11/17/05 1,2-Dichlarobenzene BQL 20.0 20 11/17/05 1,3-Dichlorobenzene BQL 20.0 20 11/17/05 1,4-Dichlarobenzene BQL 20.0 20 11/17/05 1,1-Dichloroethane BQL 20.0 20 11/17/05 1,2-Dichloroethane BQL 20.0 20 11/17/05 1,1-Dichloroethene BQL 20.0 20 11/17/05 cis-1,2-Dichloroethene BQL 20.0 20 11/17/05 trans-1,2-Dichloroethene BQL 20.0 20 11/17/05 1,2-Dichloropropane BQL 20.0 20 11/17/05 cis-1,3-Dichloropropene BQL 20.0 20 11/17/05 trans-1,3-Dichloropropene BQL 20.0 20 11/17/05 Methylene Chloride BQL 100 20 11/17/65 1,1,2,2-T.etrachloroethane BQL 20.0 20 11/17/05 Tetrachloroethene BQL 20.0 20 11/17/05 1, 1, 1 -Trichloroethane BQL 20.6 20 11/17/05 1,1,2-Trichloroethane BQL 20.0 20 11/17/05 Trichloroethene 184 20.0 20 11/17/05_ Trichlorofluoromethane BQL 20.0 20 11/17/05 Vinyl Chloride BQL 20.0 20 11/17/05 Surrogate Spike Recoveries Spike Spike Percent Added Result Recovery. 1,4-Dichlorobutane 40 37.8 94.5 Comments: All values corrected for dilution. BQL = Below quantitation limit. Reviewed By:11 W GCuM _J " 7 of 26 N.C. Certification #481 S.C. Certification #99029 PARADIGM ANALYTICAL LABORATORIES, INC. Results for Volatiles by GC 601 Client Sample ID: MW-9 Analyzed By: MJC Client Project ID: Toastmaaster Laurinburg Date Collected: 11/9/05 0:00 Lab Sample ID: G420-55-13A Date Received: 11/10/05 Lab Project ID: G420-55 Matrix: Water / Analyte Result RL ug/L ug/L Dilution Date Factor Analyzed Bromodichloromethane BQL 1.00 1 11/17/05 Bromoform BQL 2.00 1 11/17/05 Bromomethane BQL 1.00 1 11/17/05 Carbon tetrachloride BQL 1.00 1 11/17/05 Chlorobenzene BQL 1.00 1 11/17/05 Chlorcethane BQL 1.00 1 11/17/05 Chloroform BQL 1.00 1 11/17/05 Chloromethane BQL 1.00 1 11/17/05 Dibromochloromethane BQL 1.00 1 11/17/05 1,2-Dibromoethane (EDB) BQL 1.00 1 11/17/05 1,2-Dichlorobenzene BQL 1.00 1 11/17/05 1,3-Dichlorobenzene BQL 1.00 1 11/17/05 1,4-Dichlorobenzene BQL 1.00 1 11/17/05 1,1-Dichloroethane BQL 1.00 1 11/17/05 1,2-Dichloroethane BQL 1.00 1 11/17/05 1,1-Dichloroethene BQL 1.00 1 11/17/05 cis-1,2-Dichloroethene BQL 1.00 1 11/17/05 trans-1,2-Dichloroethene BQL 1.00 1 11/17/05 1,2-Dichloropropane BQL 1.00 1 11/17/05 cis-1,3-Dichloropropene BQL 1.00 1 11/17/05 trans-1,3-Dichloropropene BQL 1.00 1 11/17/05 Methylene Chloride BQL 5.00 1 11/17/05 1,1,2,2-Tetrachloroethane BQL 1.00 1 11/17/05 Tetrachioroethene BQL 1.00 1 11/17/05 1,1,1-Trichloroethane BQL 1.00 1 11/17/05 1,1,2-Trchloroethane BQL 1.00 1 11117/05 Trichloroethene 3.20 1.00 1 11/17/05 Trichlorofluoromethane BQL 1.00 1 11/17/05 Vinyl Chloride BQL 1.00 1 11/17/05 Surrogate Spike Recoveries Spike Spike Percent Added Result Recovery 1,4-Dichlorobutane 40 39.3 98.3 Comments: All values corrected for dilution. BQL = Below quantitation limit. Reviewed By ccL-012 of 26 N.C. Certification #481 S.C. Certification #99029 9 PARADIGM ANALYTICAL LABORATORIES, INC. Results for Volatiles by GC 601 Client Sample ID: MW=10 Analyzed By: MJC Client Project ID: Toastmaaster Laurinburg Date Collected: 11/9/05 0:00 Lab Sample ID: G420-55-9A Lab Project ID: G420-55 Analyte Date Received: 11/10/05 Matrix: Water Result RL uglL uglL Dilution Date Factor Analyzed Bromodichloromethane BQL 10.0 10 11/17/05 Bromoform BQL 20.0 10 11/17/05 Bromomethane BQL 10.0 10. 11/17/05 Carbon tetrachloride BQL 10.0 10 11/17/05 Chlorobenzene BQL 10.0 10 11/17/05 Chlorcethane BQL 10.0 10 11/17/05 Chloroform BQL 10.0 10 11/17/05 Chloromethane BQL' 10.0 10 11/17/05 Dibromochloromethane BQL 10.0 10 11/17/05 1,2-Dibromoethane (EDB) BQL 10.0 10 11/17/05 1,2-Dichlorobenzene BQL 10.0 10 11/17/05 1,3-Dichlorobenzene BQL 10.0 10 11/17/05 1,4-Dichlorobenzene BQL 10.0 10 11/17/05 1,1-Dichloroethane BQL 10.0 10 11/17/05 1,2-Dichloroethane BQL 10.0 10 11/17/05 1,1-Dichloroethene BQL 10.0 10 11/17/05 cis-1,2-Dichloroethene BQL 10'.0 10 11/17/05 trans-1,2-Dichloroethene BQL 10.0 10 11/17/05 1,2-Dichloropropane BQL 10.0 10 11/17/05 cis-1,3-Dlchloropropene BQL 10.0 10 11/17/05 trans-1,3-Dichloropropene BQL 10.0 10 11/17/05 Methylene Chloride BQL 50.0 10 11/17/05 1,1,2,2-Tetrachloroethane BQL 10.0 10 11/17/05 Tetrachloroethene BQL 10.0 10 11/17/05 1,1,1-Trichloroethane BQL 10.0 10 1Ill 7/05 1,1,2-Trichloroethane BQL 10.0 10 11/17/05 Trichloroethene 72.1 10.0 10 11/17/05 Trichlorofluoromethane BQL 10.0 10 11/17/05 Vinyl Chloride BQL - 10.0 10 11/17/05 Surrogate Spike Recoveries Spike Spike Percent Added Result Recovery 1,4-Dichlorobutane 40 39.2 98.1 Comments: All values corrected for dilution. BQL = Below quantitation limit. Reviewed By: Gc Lu+no.xt of 26 N.C. Certification #481 S.C. Certification #99029 19 PARADIGM ANALYTICAL. LABORATORIES, INC. Results for Volatiles by GC 601 Client Sample ID: MWA 1 Analyzed By: MJC Client Project ID: Toastmaaster Laurinburg Date Collected: 1119/05 0:00 Lab Sample ID: G420-55-10A Date Received: 11/10/05 Lab Project ID: G420-55 Matrix: Water Analyte Result RL ug/L uglL Dilution Data Factor Analyzed Bromodichloromethane BQL 32.0 32 11/17/05 Bromoform BQL 64.0 32 11/17/05 Bromomethane BQL 32.0 32 11/17/05 Carbon tetrachloride BQL 32.0 32 11/17/05 Chlorobenzene BQL 32.0 32 11/17/05 Chioroethane BQL 32.0 32 11/17/05 Chloroform BQL 32.0 32 11/17/05 Chloromethane BQL 32.0 32 11/17/05 Dibromochloromethane BQL 32.0 32 11/17/05 1,2-Dibromoethane (EDB) BQL 32.0 32 11/17/05 1,2-Dichlorobenzene BQL 32.0 32 11/17/05 1,3-Dichlorobenzene BQL - 32.0 32 11/17/05 1,4-Dichlorobenzene BQL 32.0 32 11/17/05 1,1-Dichloroethane BQL 32.0 32 1lil7/05 1,2-Dichloroethane BQL 32.0 32 11/17/05 11,1-Dichloroethene BQL 32.0 32 11/17/05 cis-1,2-Dichloroethene BQL 32.0 32 11/17/05 trans-1,2-Dichloroethene BQL 32.0 32 11/17/05 1,2-Dichloropropane BQL 32.0 32 11/17/05 cis-1,3-Dichloropropene BQL 32.0 .32 11/17/05 trans-1,3-Dichloropropene BQL 32.0 32 11/17/05 Methylene Chloride BQL 160 32 11/17/05 1,1,2,2-Tetrachlaroethane BQL 32.0 32 11/17/05 Tetrachloroelhene BQL 32.0 32 11/17/05 1, 1, 1 -Trichloroethane BQL 32.0 32 11/17/05 1,1,2-Trichloroethane BQL 32.0 32 11/17/05 Trichloroethene 294 32.0 32 11/17/05 Trichlorofluoromethane BQL 32.0 32 11/17/05 Vinyl Chloride BQL 32.0 32 11117/05 Surrogate Spike Recoveries Spike Spike Percent Added Result Recovery 1,4-Dichlorobutane 40 36.3 90.9 Comments: All values corrected for dilution. BQL = Below quantitation limit. Reviewed By cc_ums- .ms9 of 26 N.C. Certification #481 S.C. Certification #99029 . _ �i PARADIGM ANALYTICAL LABORATORIES, INC. Results for Volatiles .l by GC 601 Client Sample ID: MW-14 Analyzed By: MJC Client Project ID: Toastmaaster Laurinburg Date Collected: 1119105 0:00 Lab Sample ID: G420-55-11A Date Received: 11/10/05 ' Lab Project ID: G420-55 Matrix: Water Analyte Result RL Dilution Date uga ug/L Factor Analyzed Bromodichloromethane BQL 1.00 1 11/16/05 - Bromoform BQL 2.00 1 11/16/05 Bromomethane BQL 1.00 1 11/16/06 Carbon tetrachloride BQL 1.00 1 11/16/05 Chlorobenzene BQL 1.00 1 11/16/05 Chloroethane BQL 1.00 1 11/16/05 Chloroform BQL 1.00 1 11/16/05 Chloromethane BQL 1.00 1 11/16/05 Dibromochloromethene BQL 1.00 1 11/16/05 1,2-Dibromoethene (EDB) BQL 1:00 1 11/16/05 1,2-Dichlorobenzene BQL- 1.00 1 11/16/05 1;3-Dichlorobenzene BQL 1.00 1 11/16/05 1,4-Dichlorobenzene BQL 1.00 1 11/16/05 1,1-Dichloroethane ,' BQL 1.00 1 11/16/05 1,2-Dichloroethane BQL 1.00 1 11/16/05 1 1,1-Dichloroethene BQL 1.00 1 11/16/05 cis-1,2-Dichloroethene 4.28 1.00 1 11/16/05 trans-1,2-Dichloroethene BQL 1.00 1 11/16/05 1,2-Dichloropropane BQL 1.00 1 11/16/05 cis-1,3-Dichloropropene BQL 1.00 1 11/16/05 trans-1,3-Dichloropropene BQL 1.00 1 11/16/05 - Methylene Chloride BQL 5.00 1 11/16/05 r 1,1,2,2-Tetrachloroelhane BQL 1.00 1 11/16/05 Telrachloroethene BQL '1.00 1 11/16/05 1,1,1-Trichloroethane BQL 1.00 1 11/16/05 - 1,1,2-Trichloroethane BQL 1.00 1 11/16/05 Trichloroethene 19.6 1.00 1 11/16/05 Trichlorofluoromethane BQL 1.00 1 11/16/05 Vinyl Chloride BQL 1.00 1 11/16/05 Surrogate Spike Recoveries Spike Spike Percent Added Result, Recovery J 1,4-Dichlorobutane 40 38.9 97.3 Comments: All values corrected for dilution. BQL = Below quantitation limit. Reviewed By: 4 GC�-LUSQ0'10of26 N.C. Certification #481 S.C. Certification #99029 PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: Effluent Client Project ID: Toastmaaster Laurinburg Lab Sample ID: G420-55-1D Lab Project ID: G420-55 Parameter Result Units pH 6.86 S.U. Temperature 22.4 °C Analyzed By: RML Date Collected: 11-09-2005 00:00 Date Received: 11-10-2005 00:00 Matrix: Water Procedure Date Analyzed 150.1 11-23-2005 16:00 r Comments: Samples analyzed out of 15 minute hold time. Reviewed By:IA� 13 of 26 N.C. Certification #481 S.C. Certification #99029 PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: Influent Client Project ID: Toastmaaster Laurinburg Lab Sample ID: G420-55-20 Lab Project ID: G420-55 Parameter Result Units pH 5.22 S.U. Temperature 22.7 OC Comments: Samples analyzed out of 15 minute hold time. Analyzed By: PSW Date Collected: 11-09-2005 00:00 Date Received: 11-10-2005 00:00 Matrix: Water Procedure Date Analyzed 150.1 11-23-2005 16:10 f N.C. Certification #481 S.C. Certification #99029 Reviewed By:L PN urns w 1 14 of 26 PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: RW-1 Analyzed By: PSW Client Project ID: Toastmaaster Laurinburg Date Collected: 11-09-2005 00:00 Lab Sample ID: G420-55-3D Date Received: 11-10-2005 00:00 Lab Project ID: G420-55 Matrix: Water Parameter Result Units Procedure Date Analyzed pH 5.37 S.U. 150.1 11-23-2005 16:14 Temperature 22.8 °C Comments: Samples analyzed out of 15 minute hold time. Reviewed ByVMS�.W 15 of 26 N.C. Certification #481 S.C. Certification #99029 PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: RW-2 Analyzed By: PSW Client Project ID: Toastmaaster Laurinburg Date Collected: 11-09-2005 00:00 Lab Sample ID: G420-55-41) Date Received: 11-10-2005 00:00 Lab Project.ID: G420-55 Matrix: Water Parameter Result Units Procedure Date Analyzed pH 5.08 S.U. 150.1 11-23-2005 16:16 n Temperature 22.7 °C 1 Comments: Samples analyzed out of 15 minute hold time. Reviewed By: °e_ ims w I 16 of 26 N.C. Certification #481 S.C. Certification #99029 PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: MW-3 Analyzed By: PSW Client Project ID: Toastmaaster Laurinburg Date Collected: 11-09-2005 00:00 Lab Sample ID: G420-55-6D Date Received: 11-10-2005 00:00 7: Lab Project ID: G420-55 Matrix: Water y Parameter Result Units Procedure Date Analyzed pH 5.37 S.U. 150.1 11-23-2005 16:17 Temperature 22.7 °C i Comments: Samples analyzed out of 15 minute hold time. Reviewed By:LIMS o_ 17 of 26 N.C. Certification #481 S.C. Certification #99029 PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: MW-5 Analyzed By: PSW Client Project ID: Toastmaaster Laurinburg Date Collected: 11-09-2005 00:00 Lab Sample ID: G420-55-12D Date Received:, 11-10-2005 00:00 .Lab Project ID: G420-55' . Matrix: Water Parameter Result Units Procedure Date Analyzed pH 5.11 S.U. 150.1 11-23-2005 16:24 Temperature 22.6 °C Comments: Samples analyzed out of 15 minute hold time. Reviewed By: pH_ ms_w i 22 of 26 N.C. Certification #481 S.C. Certification #99029 PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: MW-6 Analyzed By: PSW Client Project ID: Toastmaaster Laurinburg Date Collected: 11-09-2005 00:00 Lab Sample ID: G420-55-71) Date Received: 11-10-2005 00:00 Lab Project ID: G420-55 Matrix: Water Parameter. Result Units Procedure Date Analyzed pH 5.07 S.U. 150.1 11-23-2005 16:18 Temperature 22.4 °C comments: Samples analyzed out of 15 minute hold time. Reviewed By: pLUMS 18 of 26 N.C. Certification #481 S.C. Certification #99029 PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: MW-9 Analyzed By: PSW Client Project ID: Toastmaaster Laurinburg Date Collected: 11-09-2005 00:00 Lab Sample ID: G420-55-13D Date Received: 11-10-2005 00:00 Lab Project ID: G420-55 Matrix: Water Parameter Result Units Procedure Date Analyzed J pH 4.96 S.U. 150.1 11-23-2005 16:26 Temperature 22.6 °C Comments: Samples analyzed out of 15 minute hold time. Reviewed By: pH-,ms;;, 23 of 26 N.C. Certification #481 S.C. Certification #99029 PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: MW-10 Client Project ID: Toastmaaster Laurinburg Lab Sample ID: G420-55-91) Lab Project ID: G420-55 Parameter Result Units pH 4.59 S.U. Temperature 22.7 0C . Comments: Samples analyzed out of 15 minute hold time. Analyzed By: PSW Date Collected: 11-09-2005 00:00 Date Received: 11-10-2005 00:00 Matrix: Water Procedure Date Analyzed 150.1 11-23-2005 16:19 Reviewed By: PLms-vo,- 19 of 26 N.C. Certification #481 S.C. Certification #99029 j 1 PARADIGM ANALYTICAL LABORATORIES, INC. Results for lnorganlcs Client Sample ID: MW-11 Client Project ID: Toastmaaster Laurinburg Lab Sample ID: G420-55-1 OD Lab Project ID: G420-55 Parameter Result Units pH 5.07 S.U. Temperature 22.6 °C Comments: Samples analyzed out of 15 minute hold time. Analyzed By: PSW Date Collected: 11-09-2005 00:00 Date Received: 11-10-2005 00:00 Matrix: Water Procedure Date 150.1 N.C. Certification #481 S.C. Certification #99029 Analyzed 11-23-2005 16:21 Reviewed By: PH- 20 of 26 PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: MW-14 Client Project ID: Toastmaaster Laurinburg Lab Sample ID: G420-55-11 D Lab Project ID: G420-55 Parameter Result Units pH 5.51 S.U. Temperature 22.6 °C Comments: Samples analyzed out of 15 minute hold time. l Analyzed By: PSW Date Collected: 11-09-2005 00:00 Date Received: 11-10-2005 00:00 Matrix: Water Procedure Date Analyzed 150.1 11-23-2005 16:22 Reviewed By: v pH_IMSy01 21 of 26 N.C. Certification #481 S.C. Certification #99029 PARADIGM ANALYTICAL LABORATORIES, INC. List of Reporting Abbreviations and Data Qualifiers B = Compound also detected in batch blank BQL = Below Quantitation Limit DF = Dilution Factor Dup = Duplicate D = Detected, but RPD is > 40% between results in dual column method. E = Estimated concentration, exceeds calibration range. J = Estimated concentration, below calibration range and above MDL LCS(D) = Laboratory Control Spike (Duplicate) MDL = Method Detection Limit MS(D) = Matrix Spike (Duplicate) PQL = Practical Quantitation Limit RL = Reporting Limit RPD = Relative Percent Difference mg/kg = milligram per kilogram, ppm, parts per million ug/kg = micrograms per kilogram, ppb, parts per billion mg/L = milligram per liter, ppm, parts per million ug/L =micrograms per liter, ppb, parts per billion • Rec = Percent Recovery • soilds = Percent Solids Special Notes: 1) Metals and mercury samples are digested with a hot block, see the standard operating procedure document for details. 2) Uncertainty for all reported data is less than or equal to 30 percent. M134.092205.2 N.C. Certification #481 S.C. Certification #99029 24 of 26 N N rAKAUIUMAINALY•11UAL LABORATORIES, INC. .52432 0 coC# 5500 Business Drive, Wilmington, NC 28405 Chain -of Custody Record &Analytical Request "' N Phone:(910)--350-1903 FAX:(910)-350-1557 Page of Client: IBLtSTyV�STt/' Project T \[r ��y1�Dt /�1oy �� �'` O;�ReportTo: v� ��"41LJC Address: �iso �' rGdAlr«: Contact: S4+ i j 1,Lvi L�� Tamaround: STr,n,;4rof Addrem:_CA/J.."bviS NIO 4 b33VanK I CIv6 1, Phone: �J I D �p 17- �P S"S3 Job Number: W i (n, (V C- a, g � I � Quote A Fax: n n %T... V... F A . n,ii=. ,� �✓ 1, III' Inu I�, LLYI 1 1 :Y 1 I9 111 � - 1 1 I I I ti 1 HE�1������� - ■ill■ 11��� 11011������. IN MEN IM MEN M1 11 1 111: I.:I � - �i ��✓����/��� III • � .:�� - III I111 ' � 1 W. 1 1 1 11 I %. 1 -NC SC Other SEE REVERSE , TERMS a 24 UNIUMAL PARADIGM ANALYTICAL LABORATORIES, INC. COc# 5 2 4 31CS 5500 Business Drive, Wilmington, NC 28405 Chain of Custody Record & Analytical Request cc Phone:(910)-350-1903 FAX:(910)-350-1557 Page-2—,- of ?-- Client: -169.2iv00 Project ID: 100f&f Yxf i J tI v /,n &JJ(Date: ��� t D J Report To: Address: Contact: k;6, G1 ti.: Or Turnaround: Address: Phone: Job Number: Quote A Fax: P.O. Number: Invoice To: �� 5:11:•.•.. 1 II II I l P:YI :11 1 :Y 11 IfIN 1SEEREVERSEFOR i.4 �.Ilih.l:;li� is In 'LY•l: �� n 11 Y. I ✓. /11 '11:. 1 TERMS AND CONDMONS SUBMIT FORM ON Y L t O P,qpFER ONLY Facittty Nami Permit. Name Well LooatiordSite Nama — - t 1' Se• .ti Telephone p:573- SoS- 3sl7_ No. of Wells to bo Sampled: P. Wepltlen6fication Number (tram Pemrlt): / W � WeilgepUt: Z5. Weliblameten?'.0 For Growdwater7reatmentSkins Screened.tnterval: 5. o Itto 2S.o ft. Checkenc p Influent (91)) Depth to Water Level: f 3• (o fL below measuring point 01 Effluent `(99) Measuring Point (M•P-') is: Z_S (L abbV. land surface. Relative M.P. Elevation In. ft.: Gallons of water pumped/baljed before sampling: fa • S Dato sample collected >_ z l OS Feld analysis: pH-5 (p8_ SpeGiicConductance T+p• ^C; Odor ulNhos Appearance PARAMETERS (Samples for tnetois,Were collected pn4llered_YE$, COp. mgA. Coflform: MFTotxl-----,_/100ml Coliform: MF Total Nitrite (NO2) as N Nitrate (NO3) as _ _�`1100mt (Mot--Uao MFN Method' forhightyturbld Sam pnej Dissolved Solld T Phosphorus: Total Orthophosphate PERMIT#: & NATURAL RESOURCES VDWATER SECUoN DATE: --�� �"� �s 1UPERAMN BEING MONITORED Lagoon . X Remedialiorc Infiltration Gallery Spray Field _-Redled ft. � Rotary Disuitiuta �—.Land Application at Sludge - .. Omer NQT.S: Values should reflect dissolved and N• , Colloidal concentrations. - Date sample analyzed: - ILI z z I0q CLn 3 ` Laboratory Name.. v L L oP�M1tD Certification No. —491 _ t, and fieldaofdified __YES —N0) ' mgA Ni - Nicke N mgA Pb - Lear! m� as P. mgA Zn - Zinc mqA H S• oral------mgA TOG hen analyz@dj -- --_units A(- Aluminum. -Barium mgA mgA Ammonia Nitrogen Other (Spedy C �pOendLs and Concentration Chloride gA Ca Ca - Calcium mgA m TGE qs Units) Arsenic Grease and Oils mgA mgA Cd-Cadmium Chromium: Total mg/I m%i Phenol mgA Cu - Copper fron M911 lfate HtcConductance��_uMhosK ital mg Hg - Merou mgg�/II m ORGANICS: {Gc,GCIMS,HPLC} Ammonia mgA - Potarcur Mg - magnesium mg/I (SpeCffy test and method 0. Attach lab repoit) ' Report Attached? Yerz✓(1) No TKN as N - mg/l Mri -Manganese mgA mgA _(0) VOC method a SUBMIT FORM ON YFt t nW pppER ONLY GROUNDWATER QUALITY. -MONITORING: • nIPARTMENTOF.ENVIRONE4@7r6NATTIAAIRESOUzj COMPLIANCE. LEYFREPORT RU'F?1Vl FltGit-fFY tNFURKATI(1ta . - WATER OIfA1 TiY DNMfON,GROUNDWATER SECTION 1a!?6UUL SEAVICscum n 1,ce(-I. —r "�' Facifity, Name- tL} I8S E(Z ( K_L KG(�gt} wnl Please PrinrG(eaNy or Typo hit' vrs � • • ALNG NC 2769•r63a phi 19 . PERMIT PERMischarge�pO0i7 Permit Name (if different). Facillty Address M: . �PIRA710NDATE:_�_ UIC 0/!D wart. ug 0 28352 -- Cdnfact Person:l.$R�Y_ 11: " County �M1,-A 0 NPDES . TYPE OF PEnMtTrpn OPERA770N BEING MONfTOAED Weft LOW. n/Sito Name °47 s�, ro r o Telephone ff:`�73� f3D� 6- 3S� Z NO- of Wolfs to be Sampled: . Lagoon LC _temediatjm mrsuenn Qartery . ' Spray F-w1d Wag tdentificatiat Number {fmm Perro): W 2 "" • Welt Depth: 3o,O ForGruartmierTmatatent terns R _-gamedwdon - notary Disc -,&Aar __Land AppBaatlon at Sludge ---- �_ Wep'Diameterl.2S Screened Interval. Ito _ 3p. o �. in, Q=kOne CI Influent (98} Other. r� Depth to W. rLavel S° 2 N befOW'measuring point 0 Effluent. (99) Measuring UQM- Values should reflect dissolved and Point (M.P) Ls: 1. 30 it above land surface. Gallons Of Water pumpad/baded.before o Relative M.P. Elevation In ft..Colloidal' . concentration. j sampling: I • Field an alysis: pH' 5• && Speq(fcConductance Data sample crodeeled L 2-1 S Data sample analyzed: rLj 1.z I Oq ro F Temp,l(e.0 .0 odor ultitiros Appearance ` Laboratory Name; �+zflotyrr, Atwtc c oRATI a ec Cerdflcaton'No._16 _ cn PAriAM ET(Samples farmeiaTs,rierocollecteduntiflered COD. m Coliform MF Fecal _��100m1 l YES _NO Nftdte (NO2) as N and'fleldabtdiffed _.,YES rzo m9A -- r Coliform: MF Total �100mi (Not= Usa Nitrate O (I`r 3) as N' Phosphorus: Total aSP Ni -Nickel mgA Pb - Leap 91 m MPN methodTarhlghty turbid sampr11flJ Solids: Total mgA PH (W Orthophosphate '-'�'— Al mgA Zn -Zinc Mgt! mgA Ammonia Nitrogen �_ en PH (when analyzed). y t units Toc' - Aluminum 13a - l3arittm ' Other (Specuycompounds and Units) Chloride mgA Arsenic mg/I Ca - Calcium Cd - Cadmium m9 rngA 0 L Grease and 01s mgft Chromium: Total' m� m !I Phenol mgA Sulfate Cut- Copper (Mercury ron m. mg Conductance Sptal Hg - m9�1 ORGANICS: (Ge°GC/MS,HPLC) mg/1 �uMhOS Ar TKNat mania mg11 K - Potassium Mg -Magnesium (Speelfy test and method k Attach lab repoit.)' gA ReportAttaebed2 Yes, --(I) No'_(0}. mgll Mn -Manganese Mg/1 9 VOC . method R r�'lTT1111fRfIT fMlwnw.er�wsl --�-----: Methodll_ D�•-^u�oRap mraa°Pleona Rev. 0312006,111meeOrdAggwBq prn orrypeIn• ., fDwlet Well Location/ SUBMIT FORhI ON V O " FgpER ONLY Telephone 11:572 No- of Wells to be Well Depth: 6D.0 -- l.zs For GmttndviatertM&tlnentSystems ----�._..n. WeIYOlamet' S=e.netr_`Inonc O Influent (88) d. Depth to 1Mervah fL:to . Water Level l I • ±- fL below measuring point 13 .Effluent, (99) Measuring Point (M-m) is: S_} it ati0ve tandsudace. Relative M.P. Elevadonln H.: Galbrts of water pumped/balled before sampling: (5 Data taampla leva collected: i -z z I os Fietdanalysis: pH 5 30 , Specific. Conductance Temp. �D• 1 eC Oder. Mhos . Appearance OEPARMENroP ENVIAONNFNL Ei NATURAL RESOURCES WATER QUALITY ONLSION. GROUNDWATER SECTIou 4!lt61AtLSEAVICECENiER I;(PI-I E RMFTp-RATION DATE: n-DischargeW400077 9_UDES TYPE OF PERM n ----- 1T7�_ OPERATION BEING MONtTOREO Lagoon �,Rerne?ietlorc "11ratlon gallery 33 Spray Field aemtxraAon: nr. Rotary Dislributor ,_Land Appfi=Uon of Sfudge NQM-. Values should reflect dissolved and colloidal concentrations. s- Dale sample analyzed- I'L12z l Oq o Laboralory'Name- cn AaADl6m ANgLrncnL t ter, Certification No. _OV0I PQRQ- (samples,for metals; Were collected urifittered__YES ei COD. Colilorin: MF Fecal --- -- _ ,_1100mf ti-ul'" mg(i _NO Nitrite (NO2) as N Nitrate (NO.) N And fieldabldlffed m A g -AYES Ni -Nickel MF Total-----1100m1 (Note iu samprYeJ e MPSollds- as Phosphorus: Total as P —'—'---�-- mgfi mgn m Pb -Lead g/I Zn - Zi m l Tohlyhrytur6[d Dissolved Solids: Total -----__ (When'analyzed} mg/l Orthophosphate At - Aluminum Mgt' mg/1 Ammonia Nitrogen mgn cl, TO TOC units 6a -Barium Other (SPecllyCom tends and Concentration Po ) Chloride m9n Ca - Calcium - m m9n 94 :Arsenic mgn Cd - Cadmium m (U Grease and O1s mO Chromium: Total mg l Phenol Sulfate m9n Cti - Copper mg/l Specff(c Conductance Tots! mg uMhos Hg-Iron Mercu K - Potassl I mg/I . mgn ORGANICS:(oQ.GnC;-lS,IiPLC) (Speofty, toll and method R. Attach " Ammonia TKN as N mg/1 Mg - Magnesium m9n. mgn lab report.) Report Attached? yes ✓(1) No _(01 VOA^: m9/1 Mn - Manganese mgn method q ._ :method s Ml1�1I111T1f}4trw w.� ru4Y7li54Q='[7T1TIRlfRi1'T'�rT}!ll�L�1AM4eliw�elu�si method N _ GW59 -r- -n .•nnwu�a rma.rempintorrype 6ev. astz000 • �8aatumrl Porialtee (oi nAlAxtrcea n Facility Nema Permit Name Well Location! SUBMIT FORM ON Telephone p572 No- of Welts to be Well Depth: I .... L W04)lamekterl•as • �ci1=dvtaert1eetnntsy#= ScmenedlntCheck One: Inftue,:iL to IL nf {98} Depth to Water Level: I t: 4 'g, betrnv measuring point. Effluent (99) :_ ft. abd'va land surface. Relative M.P. Elevation in h Meastidng Polet (M.P_} is GatiOns of water prmtped@alled before sampling. I. 5 Dato Sam to collected: '2_ OS Fialdarrdlysi@: pH S. 12 . SenrJar rt P PAPER ONLY DVARTMEWOF ENwRONMHri 6 NATURAL RESOURCES WATER QUALM DrASIoN, GFyO�UN,WA7'ER SECTION Me-MML SER1110E CENfE,R RAI _Y u.a...-..-- _ [NPOSS n-Dischargo�000-179Py rIHATIONDATE:�_ UIP OF PEpt"t n OPERATION BEING MONITORED Lagoon X_Remediatrorc Infidnitlon Gallery Spray Reid _qd arron: Rotary D stnbutas __LWd Appecattan ct Sludge � other. p NOTE. Values should reflect dissolved and r colloidal concentrations. C:) Datesamplsanalyzed. Sj27.jOq cit Laboratory Name- 2ADl6m A Certitication No.--f91 nS(sainptesiermetats.Werecollectedurifittered COD = COD.._NO Collform: MF Fecal mgA YES Nitrite (NO2) as N and field acldiffed m9A _1 YES Coliform: IVIF Total ''-"—fit --�-_1100ml tHo�:v.�Mnttmeurodrarnr9nryremtds,mpr.ei 00� Nitrate (NO.) as N Phosphorus: Total mgA Ni - Nicke Pb - Lead— m , gg Dissolved Solids Total` as P Orthophosphate ""--mgA mgA Zn-zmc m m oCwhen'analyzed)_s. 01 .. mgA units Al - Aluminum Ba - Barium mgA Ammonia Nitrogen �%ther (speclty.Compounds a s) Chforide Arsenic mgA Ca-`Caloium - Cd-Cadmium mg�lt - TC E fxt Grease and Oils m9n gA Chromium: Total mgA mgI Phenoi Sulfate mglt M94911 Cu - Copper - Iron mgii Specific Conductance mos H9 -Mercury mg/I mgll. ORGANICS: (Gc.GC/Ms HPl C) Total mania TKN uMhos mgA . K-Potassium Mg - Magnesium mg/I (specuy test and method ft. Attach lab Report Attached? Ye ✓�) No as N mgA Mn -Manganese mgA mgn VOC={1� -- �": method IY Ik C !� method 9 a IIfAlfnllRPlt• t•Irr _ _ w..aM1—.. r-------.---^. GW59 Rev. 0aMM FORM ON YELLO " PAPER ONLY 19130UND.WATE8 Facility Name Permit Name c'"' - �aokD4 t County oTLy4Np Con�actPetson;l $R �L! gRIGt 8 P Tele hone #:573- SOS- 361 z. WeiRocat;aN$ite.Namo•t�-�`4Tsb.e t.o No_ of Wells to be Sampled: Weil Idenfihcattdn h6mber (from ParMit): rl W S WeHDepth: 2`i_ O _ft yy60jName ter,1,25 in ��d��TreeimenfSystems Screened Imervab fL. i0 .2-4 , o it. Check One: E tnfludnt (88) Depth to WH. belowme Water Level: 5 asuring point O EfftuenL (99) 9 . �1 Measuring Potnt (M.P:) Es 3Z it. ab6vd land surface. Relative M.P. Elevation in a - Galldrts of water pumperllbafled.before sampling; 2,. O pato sample collected ZI Fieidanalysis; pH- `t •5�3 g046-Conductance ui Temp. 22. h RESOURCES PERMIT#: EXPIRATION DATE: Non-Disrdiargewp00779f} uIC NPDES TYPE OF PERM17TEQ OPERATION BEING MONfTORED LaB°°c-Z_Remedieub a Inraration Gallery Spray field Rotary,Disir"buter —_Land Application of Sludge NOTE- Values should renect dissolved and . 3 colloidal concentrations. -ac Datesampiaanalyzod• 1LI7.7.10q Laboratory Name: .$R_LIDIC+m ptrHtYTGat LA3oRATes� Certification No. —alu1 _ —�— PARAM R (Samples a. collected ariffttered _YES COD. —NO COD. Coliform: N Fecal m9A Nitrite (NO2) as N andfleldaolditled mgA —YES —NO) CO (farm: MF Total r—/I ---- wohn ase D0MI 1100ml Nitrate (NO.) as N Phosphorus: Total as P mgA ' Ni - Nickel Pb -Lead mgA mg4 MP" method' Ibrhightyturbid samprotJ Dissolved d Solids: Total ly_ mg4 Orthophosphate Al m mgA g� Zn-Zinc Ammonia Nitrogen mg/l TOGwhen analyzed) N . A4 units , -'Aluminum Ba . Barium m� _�_ m Other (speciiycompounds.and Concenhagonr mg/1 Chloride Arsenic mill mgn Ga - Calcium Cd-Cadmium m TGe s aa-! Grease and 01s mgA Chromium: Total m� mil Phenol mg4 Cu-Copper Fe *lMercu m 1 Sulfate Specftlo Conductance�`_uMhos mg Hg- mg/1 mgn ORGANICS: (6c.GWS,HPLC) Ammonia K - Potassium Mg -Magnesium �— m9A (Speolfy test and Method A. Attach lab repoit:) Report Attached? yes Mo_(0) TOW s Nmg/l mgA Mn - Manganese mgn L✓(1) �O—� : method mefhad N Rwhwwttai mefhod 0 -_... GW59^1d=•nvonwe110119e.eieaaeprMorrype I Rev. 0312000 Un�Q OO Y AA�Oh _ `j' zq I D �'"^ eoi Porml C• _ . SUBMIT FORM ON VEI i Facility Name Permit Name F Tale hone tt 573 Well LotaBoN$ite:Name*e47.51e `" p No_ of Wells to be Wall Depth: 35. o RrGroundwater Tmatmiltsletterns tt Wep Diameter, Z. in CheckOnc: CI Influent 98 Screened latervat:_ Iq.t� eta. S.o R. ( ) Depth to Water Leval: -13.5 ry• below measuring polnL O Effluent. (99) MaasUrhV Paint (M.m) is:q•? It. ab6Oland surface. Relative M.P. Elevation in R: Gaeons of water pumpedlballed before sampling: O. O Date sample collected: Z 21 fiietdanalysis: pH S• IZ Specific Conductance uathos Temp. zo.' t _ "C; Odor Appearance.' ONLY DEPARTmsurOF ENVIRONMENT 6 NATURAL RESOURCES WATER QUAUTY'DIMON, GgoUNDWATER SECnON 1"ll-MAIL SERV1ca c6'Nrsrt IJ 0 I -1 rnnme i n: EXPIRATION DATE.• Non -Discharge WQp0017g8 UIC NPOES TYPE OF PERM D OPERATION BEING MONITORED Lagoon _Remediallom infiltration Gallery, e 5prayField __Ramegft,: n Rotary Muibutor __LandApptkationofSludge Otber._ c NOTE, Values should reflect dissolved and. N colloidal concentrations. . Jr Date Sample analyzed.• 'L12z 10q L11 td Laboratory Name: ¢RpIGm A.�LYTIcgL LAII--em;ag Certification Nm— 10t _ PARAMEr _R (Samples tormetais;wera collected uriifftered COD, mgA. _YES —NO Nitrite (NO2) as N Nitrate (NO3) as N and field acldltled mgA _YES _ NO) Ni - NickelmgA Colitorm: MF Fecal --�_/10Dml Coliform: MF%tai —� _/iDOml (Note: Use MPkMethod 'for highly nrrOltl sampray ..Phosphorus: Total as P Orthophosphate mgA mgA Pb - Lean 9R Zn - Zinc m - mg/l Dissolved Solids: Total PH (when analyzed) S. vz mgA units AI - Alumfnum $a -Barium mgA m� Ammonia Nitrogen__ Other (-Specify and Concentration Uniits) Chloride mgA Ca - Calcitmt mg/I L Arsenic mgA Cd - Cadmium Chromium: Total mg/1 1 I Grease and OilsmgA Phenol mgA Cu -Copper mgA 1719/1 Sulfate mgA m A 9 Fe • Iron H 9 - Mercury m9/l . ORGANICS: (GC,GCjm$,HPLC) Speciilo Conductance uMhos K - Potass(um mgA (specify test and method 0. Attach lab ro oil p } Total Ammonia TKN as N m 9A Mg - Magnesium — mgJl mg/1 ReportAttached? Yet,L✓ 1 VOC () ( } mgA : Mn - Manganese mgA : method N - mefhad B = method N = GW-59 ACV, 0312000 1 Facility Narnr PemtitName well Welt Depth: 35 . c Screened lnterv&. I Depth to WaterLevei:_ Measuring Point (M.P,) Gallons Of water pumpi Fralda'nalysit pH 5 SUBMIT FORM ON County1-� Telephone 8:5 No_ of Weirs to -% PAPER ONLY • a OEPART6tENTOP ENMONMEM 6NATURAL RESOURCES WATER QUAE! ONlStdiN, G OUH7nYATER SECTtpN - PERMIT R: EXPIRATION DATE. Non-OischargeW�0007798 UIG TYPE OF PERMnTPn OPERATION BEING MONITORED Lagoon CL_Remedi xwc IMdUation Gallery Ca spray RoI'd �Rers+ed�ata;: - e -. Rotary Mtr4lWor - L*nd Appfi Mnof Studge ... Other- t� NM, Vafuesshould .reflect 'dissolved and , colloidal concentrations. Dafesampieanafyzed: rL17.7-loq Laboratory Name: $ Aetyn; ArJAUYTICAL I 69Km ets c Certification No. - a _ PAOAM£TFR (Samples for metalsWere oollected unffttered YE$ D.' CO_NO and fieldeoldtf. mg/I Nitrite (NO2) as N m COtifaml: MF Fecal --r_/1 DOml Nitrate O gq Gtliifarm: tvlF Total (NOS) as N mgq -- /100ml Phosphorus: Total as P4_ mgq ttgo:c v� lxatt mau:op rornfyMY turbld s mpr,q Orthophosphate q Df I ' Itta-=-_"" CheckanrU Influent (98) -35 Z� ft. below measuring point I O Effluent (99) 6z above land surfaceRelative M.P. Elevation in ft- hefore sampling 1 `f . O bate sample conected ZI . 8pesific Conductance umhos sso ved Solids. Total analyzed) mgq units TOihen Chloride mgq Arsenic mg/l mgq Crease and Oils mgq. Phenol m Sulfate mqfi Specific Conductance uMhos Total Attimania mgq TKN as N mgq GW69 Rev, 0 12M Al -.Aluminum mg mgq Ba - Barium, Ca - Caloium m gq Cd - Cadmium mgq Chromium: Total- Cu -Copper mg I Fe -Iron mg Hg -Mercury mgn K - Potassium Mg - Magnesium - mgl Mn - Manganese mgq - - YES - _ NO) Ni - Nickel mglt Pb - Leap mgq Zn - Zinc ,Ammonia Nitrogen .11191 Other (�cifycompsa Unfls)- i a l0rae e, I- ORGANICS: (GG.GGM3,HPLG) (Speolty test and Method 8. Attach lab repoit.) Rep rtAttac$8d2 Ye:;✓(1) , NO_ -(a) method P (rG C r1 I method 8 method 8 = ORGANICS: (GG.GGM3,HPLG) (Speolty test and Method 8. Attach lab repoit.) Rep rtAttac$8d2 Ye:;✓(1) , NO_ -(a) method P (rG C r1 I method 8 method 8 = GR.CIUND.WAT08- Facility Name Permit Name Well Wet Qapth: Depth to Water Messudrig Point Gallons of water rieldanalysH:' I SUBMIT FORM ON YELL PAPER ONLY County I-A-0 I Telephone #:573 No. of Wefts to be a rvumuer prom rerm,gy (vtvv� FOt GreundentterTreatment Spit= 5. o ftr won.Dfameter,2_o in. C beckOne: t7 Influent (98) th z • S IL:ta - 25 `d IL p Effluent (99) Level: 5 . ft, below measuring point (M.P:) Is:_ it. ibmvg tend surface. Relative M.P. Elevation in N.: ptrmpe#balfed before sampling: G •U Dato sample coffecfed:Z �4 (5 Appearance DEPARTMENT OF ENVIRONMENT 6 NATURAL RESOURCES WATER GUALTrY We-AMDECENTER l�NLSION, GF("I OUNDWATER SECTION LSERVIC( PERMIT e: EXPIRATION DATE: Non-DischargeW0000'/iG8 UIC NPOES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon _Remedialion: Inrittrallon Gallery Spray Frew ' _. Rame mfi n: -Rotary Distributor ;_Land Application of8tudge tV NOM, Values should reflect dissolved and. colloidal concentrations. Data sample analyzed: o Laboratory Name:11RR016rri nin_ eAL LA6oRRTJRaeS Certification No. AL_ _ _ - � Lit PARAMETERS (Samples formetals were collected unfiltered _'YES _NO and field abldiffed _YES _ NO) CQD, mgA Nitrite (NO2) as N mgA Ni - Nickel mgA Coliform: MF Fecal /1 DDml Nitrate (NO3) PS N mgA Pb - Lean mgA Coliform: MF Total 1100mt Phosphorus: Total as P mgA Zn - Zinc mgA (more: Use MPH method'ler highry turbid sampraay Orthophosphate mgA Ammonia Nitrogen mgn. Dissolved Solids: Total mgA At - Aluminum mgA Other (Speclty Compounds and Concentration units) pH (when analyzed) 41 • 6R units Ba - Barium mgA TOO mgA Ca - Calcium mgA Chloride mgA Cd - Cadmium mgA Arsenio mgA Chromium: Total mgA Grease and Oils mgA Cu - Copper mg/I Phenol mgA Fe - Iron mg/I ORGANICS: (GC,GCAAS,HPLC) Sulfate mgA Hg - Mercury mgA (Specify test and method A. Attach lab' repoit) Specific Conductance uMhos K- Potass(um mg/I RepoltAttached? Yes ✓(1) No_(0) Total Ammonia mgA Mg - Magnesium mgA VOC : method # = 6, , r n I TKN as N mgA Mn - Manganese mgA : method x. SUBMIT FORM ON YeL4-Qldr RAPER ONLY' R: Facility Address: PLAN.T QOAiDD NPDES LAU121WBUW-.., ts`Ytrc 7-8357- County SCO-1-.-ANO TYPE OF PERMITTED OPERATION BEING MONITORED CcriiaocPetson:i tP YGl ARKS°tVm 'S73-8Oe,-38iz Lague _RemeSiAITOMInfaralionGagery 7, 5� Telephone a: Weft LocabonlSite Nam . r" a No. nl Welfs to be Sampled: a Spray Field _Rernedmrmtr Rotary Mtribular _Land Application ofShfte Wep7denthfmation:Number (from Perml!};�lWl[� �GrDtmdwaterTt MDtSystpnsm Well Depth: 2_5 • O k Weil`Didmeten,, 4,0 in. ru—t,^ Gl Influent {9$} - Screened Interval,_I__ 5 ft:ta •2' O fi 3 Eiftuent (99) NoIrE: Values should reflect dissolved and . Depth to Water Level:�'R, below measuring point colloidal concentrations.ldreflectdissolved y Measuring Polht (M:P:) Is:3.25 fL above lands ace. Relative M.P. Elevallon inn : Gallons of water pumpedlbaReq before eampling 3•. O Date sample collected? 05 Data sample analyzed 'Z; Zz O� En, f ietdanalysis: pH � , Speci(Ic Conductance umh(A Laboratory Name: $2AD16m ANAGYnc,�u LA6oPRTaORte9 Certification No. -� l _ i DEPARTIOW OF ENVIRONMENT 6 NATURAL RESOURCES - WATER OUALIiY DIVISION. (I O�UNDWATER SECTION - iefthktL5ERVICEt:ENTER (�IQI1 - EXPiRATION DATE: PARAMETERS (Samples forrmetals Were collected uritlitered YES _NO and field ObIdtffed COD. mgA Nitrite (NO2) as N mgA Co(iform: MFFecal /100m1 Nitrate.(NOS) as N mgA Col'tforrh, MF Total 1100ml Phosphorus: Total as P mgA (Note: Use MPH method rerhtghlyrurbid sanpres) Orthophosphate mgA. ❑issolved-Sollds' Total Soli 9A mgA Aluminum - Al - Alumt mgA H. whed P ( yzed) `-%�1 _ .. units Ba - Barium mgA `TOO m Ca - Calcium m9/1 Chloride mgA _ Cd- Cadmium mgA Arsenic mgA Chromium: Total mg/I Grease and Oils mgA Cu -Copper ' mgA Phenol mgA Fe -Iron mg/1 Sulfate mgA Hg - Mercury mgA Specific Conductance uMhos K - Potasslum mg/I Total Ammonia mg/i Mg - Magnesium mgA TKN as N mgA Mn - Manganese mgA nor. vwcuwr ____.YES —NO) Ni - Nickel mgA Pb - Lead mgA Zn - Zinc mgA Ammonia Nitrogen mgA Other (SpecifyCompounds and Concentration Units) -_2C E I �• to DCE 4.7.1 1 OIL ORGANICS: (GO,GCAOS,HPLC) (Speeily test and method P. Attach lab repoit.) ReportAttachedT Yes✓(1) No (0) - VOC : method a = (rC. G n 1 : methods = : method a = SUBMIT FORM ON MELLOw PAPER ONLY GR.OUNb..WAT58 QUAL[TY.MONITORING- ' ' WATE OUAT I IMON, GROUN N0.7111Ip1.nESOUACES SECTION _ LUSMCECENTER COMPUANGE'REPORT FORM 4!! -UA i,CQ (-1WAIEFt RALEtGK NC 2769"06 Phone 19 7334 - t .EACIt:ISY INFORMA`ti79N- Please fir)M Gleaily or Type Facility Narne� TEf2 l (v4rS KG fb9HAm ME �(OPLtCTS �ACt LI TY P6 D1Te: EXPIRATION DATE. Non-DischargeW0000-/'798 Permit Name (if different): Facilltyff Address: -PLANT OAD . NPDES TYPE OFPERMITTED OPERATION BEING MONITORED A' ... _LA afl6uwrp tom`" 6 28352 County SL0-rG-Atb -P-Y CdnT&Petscn:�fl�K' TelephoneR573-BO6-3817- 47' sre, �H _Reme?�altorklnHilr6 lion Gallery Well LocatlordSite Name . No_ cf Webs to bo Sampled: Spray Field Re"Tation: — 4 ,� Rotary D)eidwor _Lend Appacalle n,of Sludge I Oiher._ t tNel! Identtffcation Number fmitt Pandit : r 1 I I ( ) Ali_ For Groundwater Treatment Syshm 25 D Wd Depth- tL VJe11`btameter, O h CheckOnw influent {9$) Screened Interval: f - : o . IL:to —5 • a R 1] Effluent (99) . NOTE, Vetues should reflect dissolved and , o I I q Depth to Water Level• 0 (L below'measuring point colloidal concentrations to Messudng Potnt (M.P.) tt abdva tand surface. Relative M.P. Elevallon !n ft: '7;� . Gallons of water pumpa�aH ed before sampling. Z9•o Date sample collected: zlzl OS Date sample analyzed Zz Feld analysis: pH �t•YI SpecllleConductance ufiAttos Laboratory Name:>MADI6m ANALYTICAL LAt3oKN1QL4eS Temp. • 1 "t; Odor Appearance Certification No.��f91 - PARAMETERS (Samples for metals Were collected urififtered YES -_NO and field aoldttfed ,_; YES _ NO) CO,D. mgll Write (0402) as N mg/l N! - Nickel mgR Cotltorm: MF Fecal /100ml Nitrate (NO3) as N mg/I Pb - Lead mgil Coliform: MF Total /100ml Phosphorus: Total as P mg/I Zn - Zinc mg/l (Noteritam MPH method' for highly turbid samp6s) Orthophosphate mgR Ammonia Nitrogen rrtgfl, Dissolved solids: Total mgn AI - Aluminum mgll Other (Specify Compounds and GoncemratietiUnits) pH.(when'analyzed} 4.95 units Sat -Barium risgll TOC mgp Ca - Calcium mgll -rrC E ?j I f p ()ckL Chloride mg/I Cd-Cadmium mg/I Arsenic mg/l Chromium: Total mg/I Grease and Oils mgn., Cu - Copper mg/l Phenol mg/I Fe'- Iron mg/l ORGANICS: (GC,GCIMS,HPLC) Sulfate mg/l i mg (Spa tact and method If. Attach lab repoiL) Specific Conductance uMhos K- Potass(um mg/I Report Attached? YesL✓(1) No_(0) Total Ammonia - mg/l Mg - Magnesium mg/l VOC method a = G-C, c p I TKN as N mgA . Mn - Manganese mg/I ; method N I SUBMIT FORM ON OROUNDINATE8 Facility Name VASiMlASTEIt l twf 1IYGryI({AM It hIF_ i ((DPlw T r'y1U L I TY Permit Name (ifdifferent): Facility Address: -PLANT QOAD LAy211J1WI2,Co tom" V6 28352 County Stoll RNQ ""' l 2YC_LARK "' °' S73-SDS-351z Contact PetsoR: Telephone 4f LRT 'J}°µ7' 5t�. Weft LocaUoN$ite:Name� _ No. aF Webs to 6e Sampled: � ° Wellldent>ficationNumber(froiiPerntlt): MW12 Foicroundwaterireetmentsystems Well Depth: ZG iL We!Diameter2'0 irL Check One. 0 Influent (98) screened lntervakli.to'�-0 R ❑ Effluent (99) Depth to Water Level: IZ, q5 ft beloW'measudng point Measuring Point (M.m) is -Zs (L aboYa tend surface. Relative M.P. Elevation In iL: Gallons of water pumpedlb�ited before sampling S Dato sampl® collected: ZI Y75 Fieldenalysis, pH. `. SpeafitiConductance uMhos Temp. il--_"C, Odor Appearance F-R ONLY . 6EPAaTMENr, OF . WAT It MIAMI( _90 MAIL SERVIL RALEIGH. NC 27 PERMIT W: )NrdENr 6NA'[UNA},flESOtlflCEs - ! - ROTATm sECnON, I Is (�, PhD=1979) 733 3227 iRAT10N DATE. TYPE OF PERMITTED.OPERATION BEING MONITORED Lagoon X Remediation: Inriltfallon Gallery S Spray Frew _Remedia6otl Rotary Disidbufor',Land Appeaallcn cf Stodge •. Other Ili: Values should reflect dissolved and , ry colloidal concentrations. 0 .Date sample analyzed: en LaboreforyNama: UitAD(Gm A L c L lAr30FKMF4eSf Certification No. —LIS1 _ PARAMETERS (Samples formeta,lewere collected unfiltered YES _NO and field acld(ffed COd. mgfl Nitrite (NO2) as N mgA Coliform: MF Feral /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as P mgA (Note: Use MPH method`forhlgbty turbld sampr e) OfthophOsphate mgA Dissolved Solids: Total mgA AI - Aluminum mgA pH (when analyzed) . 5. 00 units Ba - Barium mgA mgA Ca - Calcium mgA Chloride mgA Cd-Cadmium mgA Arsenic mgA Chromium: Total mg/I Grease and Oils mgA Cu - Copper mgA Phenol mgA Fe . Iron -mg/I Sulfate mgA Hg - Mercury mgA Specific Conductance uMhos K - Potassl mg/I Total Ammonia mgA Mg - Magnesium mgA TKN as N' mgA Mn > Manganese mgA —YES _NO) Ni - Nickel m Pb - Lead m o zn -Zinc lvej, N Ammonia Nitrogen •�., Other (SpecifyCompounds and Concentration Unils� t 12-P, � ORGANICS: (G0,GC/MS,HPLC) (Specify test'end method#. Attach lab report.) Report Attached? Yea ✓(1) -No _(0) VOC Y method # = (Krr) I method 9 method M = SUBMIT FORM ON YELLOW PAPER ONLY a oEPARTmemr. of ENVIRONMENT d, NATURAL. RESOURCES OROUND.Wyh').9R QUALt.7Y.MONfTOR1NG: WATEROUAUTY0NR10N,G OUNDWAMRsECNoN COMPLIANCE REPORT'FORN RAALEGter NO 27699463% �1211 Phoa¢e 1e 7a1aa1 .MOLITYINFORMAT(oN - Please PriatClearlyorTypa Facility Name ILMEMAS�� I ���KO m�IM£ �(OpIIas f^Ut.(TY PERMIT a: EXPIRATIONDATE: Permit.Name(ifdlfferenl): NOn-Diseharge! .QQQO. 798 UIC 0_rM•AJJ........'�r-.�inrr r)AO NPDES — Well Telephone No_ of Wells to be Wait Depth: It. WeliDiameter—in. CherkOrte:E] Influent (98} Screened Interval: l0o`• . ' It. p Effluent (991 Depth to Wptef Level: Q tt below measuring point Meastiring Paint (M.P.) is:— IL above land surface. Relative M.P. Elevation In fl.: Geitdns of water pumpedlba!!ed before.sampling: Date sample collected: 2 2i pS Flaidanelysit; pH S' Z Speel(icCondoctance ufmos Appearance OPERATION BEING MONITORED Lagoon LRemediatiorc Infiltration Gallery Spray Field _. Romafiallin: cns ... Rotary Distributor _Land Application of Sludge a<•. m Other NOTE: Values should raftect dissolved and. colloldnl concentrations. p Date sample analyzed.• cn rl;IZ7.10q Laboratory Name: UP I&M {a<NAGY1148 W eSil Certilication No. 3 a l _ PARAMETERS (Samples for nielalswero collected untlitered_YES NO and field eoldified —YES _ NO) COD. . mgA Nitrite (NO2) 85 N mgA Ni - Nickel mg/i Coliform: MF Fecal /100ml Nitrate (NO3) as N mgA Pb - Lead mgA Coliform: MF Total 1100ml Phosphorus: Total as P mgFl Zn -Zinc— (Nore:Uw MPH method farhighlyturbid sampNe) Orthophosphate _ mg/I Ammonia Nitrogen Dissolved Solids• Total mgA At - Aluminum mgA Other (Specify Compounds and Concentrafto. Uruls) = pH (when 'analyzed) S- 39 units . Ba - Barium mgli � r -7 TOG tngn Ca - Calcium mg/I • 2 1 i ° 1 0 `" 6. Chloride mgA Cd -Cadmium mgA ( Cn LL Arsenic mgA Chromium: Total mg/I p °° Grease and Oils Phenol mg/I mgA Cu - Copper Fe -Iron mg/I mg/I ORGANICS: (GC,GC/MS,HPLO) I �� " Sulfate mg/I Hg - Mercury Mg/1 (so city test and method 0. Attach lab rept Specific Conductaride uMhos K- Potassium mg/I Report Attached? Yes ✓✓(1) No (0) as Total Ammonia mgA Mg -Magnesium mgA VOG ; method a = TKN as N mgA Mn - Manganese mgA: method 8 method 0 GROUN COMPL tN Faciety Name Permit Name Facility Addre LAyOf fJ. Congo'tPeM Well Location Well ltlentifici Welt Depth: _ Screenedinu Depth to Web Fialdanalysis: pH 5-'10 Temp o.3 SUBMIT FORM PAPER ONLY ... .Telephone #:� la- YSOtS- brit Z �°4Tse.ro - Na of Wells to be Sampled: . ermlt}: For t;raimdwaterTrnatmentSysttaas Wep'biameter, in. checkdnr.0 Influent (98) to', 0- 0 iG El below=measuring point Effluent (99) . abgvs land surface. Relative M.P. Elevation In it: tote sa 1 piinW. 2 D Date sample collected •Z-i 05 Appearance ERMONMENT 6 NATURAL RMURCES DNISIOM GROMM ATER SECTION gemcnill VC-1 PERMIT#:- EXPIRATION DATE. Non- DIse haegaWDDD j_j9S UIC NPOES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Llienietfial'rorc In6t(ra#on Qaller Os Spray Field _RentetliatbrL -2 _ Rotary Distributor _Land Appticaron of shatoe Other.-97 ' o ° NDIE: Values should reflect dissolved and rs colloidal concentrations. Date sample analyzed: Laboratory Name: RaAPl�!cc wuNTlcAi LAI3o%1TUW eS CertiticatlonNo. -4SI. _ PapAM6TERS (Samples for metals -Were collected uiitittered,_YES _NO and field abldiffed —YES _ NO) COD, mgA Nitrite (NO12) as N mgA Ni - Nickel mgft Coliform: MF Fecal Coliform: MF Total /100ml, 100mi Nitrate (NO3) as N Phosphorus: Total as P. mgA mgA _ Pb -Lea-Learf mq, Zn - Zinc mg/( (No re:v=Wit Method Whish,yWrnroSaMphts) Orthophosphate mgA Ammonia Nitrogen_ mg/t^• Dissolved Solids: Total mgA Ai -Aluminum _m9A Other ymo c'i rd n urais) . pHHCarhen'analyied) s. 5 io units Ba - Barium- - mgtF o I s mgli Ca - Cafo€um mgA E. TL14 QQ I - Chloride mgA Cd - Cadmium mgA � w Arsenic mgA Chromium: Total mg/I 9 1 Grease and Oils mgA Cu -Copper mg/I.I Pheno! mgA Fe • Iron mg/l ORGANICS: (Gc,GctmS,HP Nc) { Sulfate mgA N9 -Mercury mgA (Specify test and rrfethod r). A ch lab rapoitf�i Specific Conductance uMhos K - Potassirmr= mg/I _ ,ReportAttached? Yet;✓ 1to tea) Total Ammonia mgA Mg - magnesium mg/f - VOC : mattiod N (rG C., n I` TKN as N mgA , Mn - Manganese mg/l : method if s SUBMIT FORM ON Y I 1 nw PAPER ONLY W DEPARTMENT OF EMONMEM B NATURAL RESOURCES GROUND..WAT Ft QUALITY MONITORING: WATER caALiTY OM510N, CgOUNDWATER SEcnoH 'r **MAIL SERVICE CENTER ou l-I - GaMPUP(I�lCE'REPORT.'t=•OXfM RALEIG NO 27699-ICS Phone: 19 73 1 FIS UT'YINF-orI1MA*ngtj - pleasePr/niC/eadyoi'TyJeI7_ Facility Name' l Ott I Kh(10,PIMAM IIlli= ROIALM FA U Ll PERMtTn: EXPIRATION DATE: PermiENams(ifdgerent); Non-Disctt.W00007798 UIC Facility Address: -PLAI\r 01lD NPDES I-AUl21 JBUUCe Is""A 2.8352 Coon Sr oTt RNOTYPE OF PERMITTED OPERATION BEING MONITORED Con acfperson RY U ARK '� 41 Telephone #573- S3o13- Lague �_Remedialion: Infiltration Gallery III' LAT-3y° 7'sl�. Slimy Feld '—Riindafma; .r; Well LoCatltuti $Ile. N 1me� N0.'of Wolfs to 68 Sampled:flotary Distnbutor _Land Apprnation of ShldgeWag Identification'Ne mber (from Pemtlt): j2W I t a 1 „Tmarmnth.- v Well Depth: % Wellbiameter,__.___in. Check One:❑ Influent (98) Screened Iittetval: IL.to , � R. ❑ Effluent. (99) NOTE' Values should reflect dissolved and Depth to Water Level; _ fl, below'measuring point. colloidal concentrations. Measuring Point (M,P:) Is:_ If. at Vii land surface. Relative M.P. Elevation In r�i1 Gallons of water pI mpedlbaRed before sampling, Date sample collected: E i 5 Date sample analyzed.• Field analysis: 'pH��Sr{ Sp6elfieConduclanee u[tiilios LaboratoryNama;�IGm {�nrn�rncnL LgCio�Ti Wes Temp. �_°C,Oda, Appearance CenhlcatidnNo. -�$L = PARAMETERS (Samples for metals Were collected uriff tered YES: _NO and field acidified YES , —NO) COD, mgA Nitrite (NO2) as N mgA Ni - Nickel rngn Colitorm: MF Fecal /100ml Nitrate (NO3) as N mgA Pb - Learl mgA Collform: MF Total /100m1 Phosphorus: Total as P mgA Zn - Zinc amg/l ' (Note: Use MPH method 'tarMghty turbidsampNsj Orthophosphate mgA Ammonia' Nitrogen mgA (E Dissolved` Solids Total mgA AI - Aluminum mgA Other (Speciycorrpounds and Con tration Urns s)E When analyzed) 5. 3s units Be - Barium mgA L TOG mgA Ca - Calcium mgA TCiz- 7-&4 wit l I?c.-t o Chloride mgA Cd - Cadmium mgA . t =, Arsenic mgA Chromium: Total mgA I Grease and Oils mgA Cu - Copper mg/1 t -► Phenol mgA mgA Fe - Iron Hg -Mercury mg/I mgA ORGANICS: (GC,GC/MS,HPLC) report.) Sulfate (Specify test and method A. Attach Is SpecillcConductance uMhos K- Potasslum m9/1 .. ReportAtteched? YerL✓(1) N _(o} Total Ammonia mgA Mg - Magnesium mgA VOC : method 0 - TKN as N mgA Mn - Manganese mgA : method e = method if - SUBMIT FORM ON YFI t ow PAPER ONLY G OMUNDWAT913 QUALITY MONITORING- • • : 09PARTMWCF MIRONMEUi 6 NATURAL RESOURCES ,. WAMQUALtrYnMSION G OUNOWQTER SECilON � COMPLIANCE REPORT— FORM - RALOGHSF0276 CENTER (2i 1 Phorre l -. - - t - .[ FACILITY INFORMATION. I • -... .. Please Print Cfest or Type .. FaailiryName• IL7STMI5TEtZ IK(3;06ib HAY'AllMf-p(0{xkTS �cILITY. PERMITt<: EXPIRAT7pNDATE: Non-DischargeVdOD00'7-19B UIC PennitName(ifdllferenl}: ' Facility Address: -fPLA NPDES LfttGU2ftJBU{zC� 'S "iIIG 2.8357- County 5LoTLa4N0 TYPE OF PERMITTED OPERATION BEING MONITORED Con oliperson:i CLARK. ' ' 'Se•� Teleplwhe#573-SoS-3517- .. Lagoon ;LRemedWdorcInfiftrarronGallery - LriT-'Jt°47 Well LoealioNS'ite.Namo� NOofWells to be Sampled: SptayFe[tl �Remsd'mtan+ . .. - . Rotary Disln'butor _Land Application of sludge- , other . "T:i , t , -• eo - . Ydeptdent�caGCiiiftumber.(rrarnPormi}: For frcundwaterTreatment $y e= Well Depth: >L WepDiameler,—in.. greckone:Cl Influent (98) -c Screened Interval ftRr • - h. I] Values should reflect dissolved and . Depth to Water Leval: fL below measuring point Measurfi Point (M P.) Is:_ ft abdve land surface. ` Relative M.P. Elevation In t1,, colloidal concentrations. g Og Date "Z 12Z 0� Gaiters of water pum Defore sampling Date sample collected, sample analyzed: -Red i ieldanalYsis: pH ` pedfic-Conduclance utvlhos Laboratory Narr>a G t oWiTv 43l �s Temp. "C, Odor l Appearance: CerGGeaGon Nc _ .PARAMETERS (Samples for metalawere collectedunllttered_YES _NO and field acidified YE9 _ NO) COD, ` mgA Nitrite (NO2) as N mgA Ni - Nickel mgA Coflform: MF Fecal 1100ml Nitrate (NO3) as N ntg/l Pb - Lead mg/I_r Collform: MF Total /100ml Phosphorus: total as P mg!! Zn - Zinc mg/l 01*1=thm MPA method for highly turbid sMiphiq Orthophosphate mgA Ammonia Nitrogen t ' aw - Dissolved Solids: Total mgA At - Aluminum mgA Other (Specify compounds and �c`n� as units) _ pH.(when'analyzed) units Sa-Barium '' mgA®: �_ J TOC mgA Ca - Calcium rngA -EILI � P I -Chloride mgA Cd - Cadmium I t€ mgA 17C F� 1 7 -in �' z s—a Arsenic mgA Chromium: Total' mg/I T Grease and Oils mgA Cu - Copper mg/I ' Phenol, mg/f Fe -Iron mg/I ORGANICS: (GO,GC/MS,WPLQ R5 . '. Sulfate rngA - Hg -Mercury _ mgA. , (specify test and method 0. ana atsreporta SpecificConduaance -- - ul K-Potasslum mgA ReportAttached2 Ye&_✓(1) . No —(a) Total Ammonia - mgA Mg - Magnesium - mgA VOC' method #'. (rG G, n TKN as N mgA Mn -,Manganese mgA. : method rr method 8 ; 'nvv, VJJLWY - _ to JUN 13 V05 OENR-FAYEifENLlERE010MlOFFlCE 5 AEN-VI- L. 7 I CONTRACTORS r. AND CONSU6LTANT y �acjyxd 9$CIVIL * GEOTECHNICALO RESULTS OF 1st TRIMESTER GROUND WATER SAMPLING `(2005) PERMIT No. WQ0007798 TOASTMASTER, INC. — INGRAHAM TIME PRODUCTS FACILITY i GROUND WATER INFILTRATION GALLERY SCOTLAND COUNTY LAURINBURG, NORTH CAROLINA PREPARED FOR: NORTH CAROLINA DEPARTMENT OF ENVIRONMENT & i NATURAL RESOURCES DIVISION OF WATER QUALITY RALEIGH, NORTH CAROLINA - cn ++ =� rn"7 1 -om CD March 25, 2005 s m C=) o . NO n PREPARED BY: GULFSTREAM ENVIRONMENTAL, INC. 8633 VINTAGE CLUB DRIVE WILMINGTON, NC 28411 (910) 612-4853 GULFST'MAM ENVIRONMENTAL, INC. 8633 Vintage Club Drive Wilmington, NC 28411 910-612-4853 ♦ Environmental ♦ Geotechnical ♦ Construction Materials Testing March 25, 2005 North Carolina Department of Environment and Natural Resources Division of Water Quality P.O. Box 29578 Raleigh, North Carolina 27626-0535 Re: Results of 1st Trimester Ground Water Sampling, (2005) Permit No. WQ0007798 Toastmaster, Inc: Ingraham Time Products Facility Laurinburg, Scotland County, North Carolina DearSir or Madam: Please find enclosed the monitoring report outlining the results of the 1st Trimester Ground Water Sampling event conducted in February 2005 at Toastmaster, Incorporated's Ingraham Facility. Within this report, you will find: • Ground Water Pump & Treat Remediation Site Data Sheet, Part A (App. I) • Table 1 -- Ground Water Level Data (App.11) • Table 2 -- Laboratory Analytical Results - Trichloroethene (App. H) • Table 3 -- pH and Temperature Data — Ground Water (App. H) • Tables 4A/4B—Remediation System Pressure/Volume Readings (App. H) • Graphs - Ground Water Monitoring Data Trends (App. III) • GW-59 Forms (App. IV)Laboratory Analytical Results (App. V) If you have any questions, or if we may be of assistance, please do not hesitate to contact us at 910-612-4853. Sincerely, 4It�f-�� Rudy A. Smithwick, P.G. President cc: Mr. Larry Clark /Mike Kraus, Toastmaster, Inc. r APPENDIX I GW-79 GROUNDWATER PUMP & TREAT REMEDIATION SITE DATA SHEET 0 I NORTH CAROLINA DEPARTMENT OF MWIRuNmE Yr, HEALTH AND NATURAL RESOURCES . Division of Environmental Management, Groundwater Section GROUNDWATER PUMP & TREAT REMEDIATION SITE DATA SHEET PART A (To be completed Background with each submission) ` 1� Site Name: .I(1Q9YMC1StffSflC •��(1G fftiil fl T YYl I)I �l- Incident No: r Location: I)�I('Ayi Region: PO.y3k4PV1Ite County: Date Release Identified: 4 . Responsible Party:-TO—OSi-MC Syef --rnc. Date CAP. Completed: L r I F Fr PART B (To be completed for,initial report or to update information -previously provided) Hydrogeology Description of Aquifer Lithology: Is bedrock aquifer/fractured saprolite impacted? Describe. Average Hydraulic Conductivity (ft./day): Average Groundwater Gradient (t): _ How were above determined? Major Pumping Influences Which may Affect*GW Flow: Distance from Site: Pumping Rate- Location and Distance from Site of Nearest Supply Well(s): Description of Release Type of Product: Estimated Volume Released: Average Plume Dimensions (ft.)--Width: Length: Depth Interval: Ranges of Concentrations from CSA: 'Emergency Response/Initial Remedial Actions - Date Source Removed/Repaired: Free Product Recovered (gal.): Soil Excavation (tons): Average Contaminant Concentration (mg/kg).: Type of Treatment or Disposal: Remediation Goals of Remediation: Description of Treatment System: Pilot test conducted? (Type) Date: Method of System Effluent Disposalm: No. of Monitoring Wells: Monitoring Schedule: Date GW'System Started: No. of Recovery Wells: Recovery Well Flowrate Drawdown Radius of GPM (ft-) Influence(ft.) Pump Type/ Capacity Are any other remediation systems used in conjunction with Pump & Treat? Describe. GW-79/S-94 APPENDIX II TABLES TABLE 1(Page 1 of 4) Ground Water Level Data 1st Trimester Sampling Event -2005 Toastmaster, Inca Ingraham Time Products Facility Laurinbur , North Carolina Well ID Date Top of Casing Elevation Depth to Ground Water Ground Water Table Elevation Monitoring Well MW-1 1/30/01 116.41 14.87 101.54 6/25/01 ,116.41 15.30 101.11 915101 116.41 16.00 100.41 1/25/02 116.41 17.00 99.41 6/28/02 116.41 15.70 100.71 9/17/02 116.41 18.00 98.41 1/28/03 116.41 14.30 102.11 5/7/03 116.41 5.30 111.11, 9/23/03 116.41 14.00 10141 1/13/04 116.41 14.30 102.11 5/13/04 116.41 14.00 102.41 2/21/05 116.41 13.60 102.81 MW-2 6/25/01 113.76 16.70 97.06 9/5/01 113.76 14.21 99.55 1/25/02 113.76 16.96 96.80 6/28/02 113.76 16.80 96.96 9/17/02 113.76 19.00 94.76 1/28/03 113.76 16.00 97.76 5/7/03 113.76 , 12.40 101.36 9/23/03 113.76 16.00 97.76 1/13/04 113.76 15.30 98.46 5/13/04 113.76 17.20 96.56 2/21/05 113.76 15.20 98.56 MW-3 6/25/01 112.34 13.20 99.14 9/5/01 112.34 11.95 100.39 1/25/02 112.34 15.99 96.35 6/28/02 112.34 13.00 99.34 9/17/02 112.34 14.91 97.43 1/28/03 112.34 12.05 100.29 5/7/03 112.34 9.00 103.34 9/23103 112.34 12.10 100.24 Note: * - No Data Available BQL - Below Quantitation Limit - -New Well Not Surveyed at Time of this Report 1/13/04 112.34 11.80 100.50 . 5/13/04 112.34 12.50 99.84 2/21/05 112.34 11.60 100.74. TABLE 1,(Page 2 of 4) Ground.Water Level Data 1st Trimester Sampling Event -2005 Toastmaster, Inc. Ingraham Time Products Facility Laurinbur , North Carolina Well ID • Date Top of Casing Elevation Depth to Ground Water Ground Water Table Elevation MW-4 6/25/01 115.12 15.40 99.72 9/5/01 115.12 14.44 100.68 1 /25/02 115.12 14.00 101.12 6/28/02 115.12 13.23 101.89 9/17/02 115.12 15.19 99.93 1/28/03 115.12 16.01 99.11 5/7/03 115.12 7.80 107.32 9/23/03 115.12 12.20 102:92 1/13/04 115.12 12.21 102.91 5/13/04 115.12, 12.60 102.52 2/21/05 115.12 11.40 103.72 MW-5 6/25/01 119.78 10.60 109.18 9/5/01 119.78 11.50 108.28 1 /25/02 119.78 10.10 109.68 6/28/02 119.78 13.00 106.78 9/ 17/02 119.78 13.81 105.97 1/28/03 119.78 9.68 113.10 5/7/03 119.78 6.03 113.75, 9/23/03 119.78 8.90 110.88 1/13/04 119.78 9.35 110.43 5/13/04 119.78 9.04 110.74 2/21/05 119.78 9.59 110.19 MW-6 6/25/01 112.94'. 15.10 97.84 9/5/01. 112.94. • 13.53 99.41 1/25/02 112.94 15.83 . 97.11 6/28/02 112.94 .15.00 97.94 9117/02 112.94 16.97 95.97 1/28/03' 112.94 13.82 99.12 5/7/03 112.94 TO-.801 102.14 9/23/03 112.94 14.06 - 98.88 Note: ' - No Data Available . BQL-Below Quantitation Limit - -New Well Not Surveyed at Time of this Report 1/13/04 112.94 13.43 99.51 5/13/04 112.94 14.83 98.11 2/21/05 112.94 13.50 99.44 MW-7 1 /3 0/01 120.81 15.50 105.31 6/25/01 . 120.81 15.71 105.10 9/5/01 120.81 15.70 105.11 -TABLE 1(Page 3 of 4) Ground Water Level Data 1st Trimester Sampling Event -2005 Toastmaster, Inc. Ingraham Time Products Facility Laurinbur , North Carolina Well ID Date Top of Casing Elevation . Depth to Ground Water Ground Water Table Elevation AM-7 cont'd 1/25/02 . 120.81 17.50 103.31 6/28/02 -120.81 16.30 104.51 9/ 17/02 120.81 19.10 101.71 1/28/03 120.81 14.75 106.06 5/7/03* 120.81 9.02 111.79 9/23/03 120.81 14.34 106.47 1/13/04 120.81 15.14 105.67 5/13/04- 120:81 14.10. 106.71 2/21/05 120.81 14.10 106.71 MW-9 6/25/01. 117.15 16.20 100.95 9/5/01 117.15 15.94 101.21 1/25/02 117.15 17.10 100.05 6/28/02 117.15 16.90 100.25 9/17/02 117.15 17.50 99.65 1/28/03 117.15 15.80 101.35 5/7/03 117.15 15.00 102.15 9/23/03 117.15 15.70 101.45 1 / 13 /04 117.15 15.13 102.02 5/13/04 117.15 15.20 101.95 2/21/05 117.15 15.40 101.75 MW-10 6/25/01 110.83 11.50 99.33 9/5/01 110.83 12.80 98.03 1/25/02 110.83 13.00 97.83 6/28/02 110.83 12.41 98.42 9/ 17/02 110.83 14.81 96.02 1/28/03 110.83 11.13 99.70 5/7/03 110.83' 5.03 105.80 Note: ' - No Data Available BQL - Below Quantitation Limit - New Well Not Surveyed at Time of this Report 9/23/03 110.83. 11.04 99.79 1/13/04 110.83 10.54 100.29 5/13/04 110.83 10.30 100.53 2/21/05 110.83 10.30 100.53 MW-11 6/25/01 117.57 15.60 10.1.97 9/5/01 117.57 13.50 104.07 1/25/02 117.57 14.17 . 103.40 6/28/02 . 117.57 13.75 103.82 9/ 17/02 117.57 16.10 101.47 TABLE1 (Page 4 of 4) Ground Water Level Data " 1st Trimester Sampling Event - 2005 Toastmaster, Inc. Ingraham Time Products Facility Laurinbur , North. Carolina Well ID Date Top of Casing Elevation Depth to Ground Water Ground . Water Table Elevation _ MW-11cont'd 1/28/03 117.57 12.97 104.60 5/7/03 117.57 6.85 110.72 9/23/03 117.57 11.61 105.96 1/13/04 117.57 12.26 105.31 5/13/04 117.57 11.85 105.72 2/21/05 117.57 11.90 105.67 MW-12 6/25/01- 112.34 10.80- 101.54 9/5/01 112.34 9.10 103.24 1/25/02 112.34 10.85 101.49' 6/28102 112.34 11.87 100.47 9/17/02 112.34 16.10 96.24 1/28/03 112.34 12.61 99.73 5/7103. 1.12.34 7.22 105.12 9/23/03 112.34 9.94 102.40 1/13/04 112.34 9.50 102.84 5/13/04 1.12.34 10.44 101.90 2/21/05 112.34 12.45. 99.89 MW-13 6/25/01 120.35 , 26.40 93.95 .9/5/01. 120.35 .24.91 95.44 1/25/02 120.35 23.10 97.25 6/28/02 _ 120.35 22.40 97.95 9/17/02 120.35 31.00 89.35 1/28/03 120.35 24.41 95.94 5/7/03 120.35 15.00 105.35 Note:' - No Data Available BQL - Below Quantitation Limit - -New Well Not Surveyed at Time of this Repoli 9/23/03 120.35 ` 24.92 95.43 1113/04 120.35 NM 5/13/04 120.35 15.92 104.43 2/21/05 120.35 30.75 89.60 MW-14 1/25/02 119.03 16.00 103.03 .6/28/02 119.03 15.12 103.91 9/17/02 119.03 18.41 100.62 1 /28/03 119.03 13.15 105.88 5/7/03 119.03 7.53 111.50 9/23 /03 119.03 12.75 106.28 1 / 13 /04 119.03 12.35 106.68 5/13/04 119.03 8.73 110.30 2/21 /05 119.03 12.30 106.73 TABLE 2 (Page 1 of 5) Laboratory Analytical Results for Trichloroethene- Ground Water EPA Method 601 1st Trimester Sampling Event - 2005 Toastmaster, Inc. Ingraham Time Products Facility Laurinbur , North Carolina Well ID Date Trichloroethene (ppb) C Standard-2.8) Monitoring Well MW-1 6/25/01 BQL 9/5/01 260 1/25/02 100 6/28/02 120 9/17/02 86 1/28/03 91 5/7/03 BQL 9/23/03 16 1/13/04 26 5/13/04 76.0 2/22/05 95.7 MW-2 6/25/01 610 9/5/01 490 1/25/02 17 6/28/02 520 9/17/02 380 Note:' - No Data Available. BQL -Below Quantitation Limit - -New Well Not Surveyed at Time of this Report 1/28/03 260 5/7/03 260 9/23/03 150 1/13/04 440 5/13/04 337 2/12/05 289 MW-3 6/25/01 46 9/5/01 130 1/25/02 82 6/28/02 78 9/17/02 83 1/28/03 140. 5/7/03 77 9/23/03 71 1/13/04 .88 5/13/04 70.5 2/22/05 87.6 TABLE 2 (Page 2 of 5) Laboratory Analytical Results for Trichloroethene— Ground Water EPA Method 601 1st Trimester Sampling Event — 2005 Toastmaster, Inc. Ingraham Time Products Facility Laurinbur , North Carolina Well ID Date Trichloroethene (ppb) C Standard — 2.8 MW-4 6/25/01 610 9/5/01 330 9/17/02 350 1/28/03 630 5/7/03 290 9/23/03 410 1/13/04. 390 5/13/04 235 2122/05 209 MW-5 6/25/01 110 9/5/01 64 1/25/02 10 6/28/02 19 9/17/02 15 . 1/28/03 15 Note: ' - No Data Available BQL — Below Quantitation Limit — -New Well Not Surveyed at Time of this Report 5/7/03 5.8 9/23/03 12 1/13/04 9 5/13/04 13.3 2/22/05 5.94 MW-6 6/25/01 290 9/5/01 220 1/25/02 140 6/28/02 170 9/17/02 150 1/28/03 230 5/7/03 260 9/23/03 340 1/13/04 210 5/13/04 215 2/22/05 145 MW-7 1/30/01 1600 6/25/01 1800 9/5/01 99 1/25/02 320 , 6/28/02 570 TABLE 2 (Page 3 of 5) Laboratory Analytical Results for Trichloroethene— Ground Water EPA Method 601 1st Trimester Sampling Event — 2005 Toastmaster, Inc. Ingraham Time Products Facility Laurinbur , North Carolina Well ID Date Trichloroethene (ppb) (NC Standard — 2.8) MW-7 cont'd 9/17/02 BQL 1/28/03 640 5/7/03 5400 9/23/03 800 1/13/04 76 5/13/04 356 2/22/05 106 MW-9 6/25/01 5 9/5/01 8 1/25/02 32 6/28/02 BQL 9/17/02 8 . Note: s - No Data Available BQL —Below Quantitation Limit — -New Well Not Surveyed at Time of this Report 1/28/03 BQL 5/7/03 BQL 9/23/03 13 1/13/04. 4.9 5/13/04 9.15 - 2/22/05 BQL MW-10 6/25/01 70 9/5/01 1000 1/25/02 1300 6/28/02 1500 9/17/02, 1300 1/28/03 1100 5/7/03 13 9/23/03 28 1/13/04 _ 12 5/13/04 6.48 2/22/05 17.6 MW-11 9/5/01 620 1/25/02 930 6/28/02 780 9/17/02 740 1/28/03 460 5/7/03 130 TABLE 2 (Page 4 of 5) Laboratory Analytical Results for Trichloroethene — Ground Water EPA Method 601 1st Trimester Sampling Event — 2005 Toastmaster, Inc. Ingraham Time Products Facility Laurinbur , North Carolina Well ID Date Trichloroethene (ppb) C Standard — 2.8 " MW-11 cont'd 9/23/03 190 1/13/04 280 5/15/04 328 2/22/05 316 MW-12 6/25/01 ' 4 9/5/01 190 1125/02 15 6/28/02 130 9/17/02 590 1/28/03 250 Note: • - No Data Available BQL — Below Quantitation Limit -- -New Well Not Surveyed at Time of this Report 5/7/03 6.5 9/23/03 110 1/13/04 330 5/13/04 8.33 2/22/05 128 MW-13 6/25/01 35 9/5/01 86 1/25/02. 90 6/28/02 110 9/17/02 74 , 1/28/03 86 5/7/03 86 9/23/03 75 5/13/04 60.1 2/22/05 7.82 MW-14 . 6/25/01 16 9/5/01 39 1/25/02 90 6/28/02 20 9/17/02 22 1/28/03 28 5/7/03 2.6 9/23/03. 8 1/13/04 6.8 '5/13/04 3:55 2/22/05 3.94 TABLE 2 (Page 5 of 5) Laboratory Analytical Results for Trichloroethene — Ground Water EPA Method 601 1st Trimester Sampling Event — 2005 Toastmaster, Inc. Ingraham Time Products Facility Laurinbur , North Carolina Well ID Date Trichloroethene (ppb) C Standard — 2.8 Influent 5/23/00 750 9/26/00 630 1/30/01 600 6/25/01 660 9/5/01 570 1/25/02. 550 6/28/02 590 Note: ' - No Data Available BQL —Below Quautitatio¢ Limit - -New Well Not Surveyed at Time of this Report f 9/17/02 550 1/28/03 780 5/7/03 .630 9/23/03 560 1/13/04 600 5/13/04 581 2/22/05 374 Effluent(Trench) 5/23/00 BQL 9/26/00 BQL 1/30/01 1 6/25/01 BQL 9/5/01 39 (Note: sample collected from system effluent not trench) 1/25/02 130 6/28/02 BQL 9/17/02 BQL 1/28/03 45 5/7/03 BQL 9/23103 BQL 1/13/04 3.6 5/13/04 26.9 2/22/05 10.8 Note: _ - No Data Available' BQL —Below Quantitation-Limit — -New Well Not Surveyed at Time of this Report Table 3 pH and Temperature Data - Ground Water 1st Trimester Sampling Event - 2005 Toastmaster, Inc. Ingraham Time Products Facility Laurinbur ,North Carolina Well ID pH - Laboratory Measurement pH - Field Measurement Temperature -Field (Celsius) Wells -Monitoring MW-1 5.77 5.68 16.1 MW-2 5.41 5.63 16.8 MW-3 5.24 5.30 20.1 MW-4 5.01 5.12 20.6 MW-5 4.84 4.58 22.0 MW-6 5.02 5.12 20.1 MW-7 5.23 5.00 17.9 MW-9 4.88 - MW-10 -4.31 4.59 19.4 MW-11 4.95 4.41. 16.6 MW-12 5.08 4.54 17.1 MW-13 5.39 5.12 18.9 NM-14 5.56 5.40 20.34 EFFLUENT (rMNCIR) 6.08 5.19 19.6 INFLUENT 1 5.22 4.60 14.8 Note: s -No Data Available BQL - Below Quantitation Limit - -New Well Not Surveyed at Time of this Report Table 4A Ground Water Remediation System Pressure Readings 1st Trimester Sampling Event — 2005 Toastmaster, Inc. Ingraham Time Products Facility Laurinbur ,North Carolina Location Reading Blower Pressure 46 in. of H2O Carbon Bank 1 Not collected . Carbon Bank 2 Not collected Carbon Bank 3 Not collected Table 413 Ground Water Remediation System Volume Readings 1st Trimester Sampling Event.— 2005 Toastmaster, Inc. Ingraham Time Products Facility Laurinbur ,North Carolina Location Reading Influent RW-1 14360587 gal. Influent RW-2 00704947 gal. Influent RW-3 04147352 gal. Effluent Totalizer '. 239054.31 Note: ' - No Data Available BQL — Below Quantitation Limit — -New Well Not Surveyed at Time of this Report APPENDIX III GRAPHS 300 250 200 H a a 100 50 0 Graph 10 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NG MW-1 Monitoring Data -- Trichloroethene 5/23/00 9126/06 1/30/01 6/25/01 9/5/01 1/25/02 6/28/02 9/17/02 1/28/03 5/7/03 9/23/03 1/13/04 2/22/05 Date Sampled --+-- series1 900 800 700 600 a a c 500 0 1 r 400 c+ 0 0 U 300 200 100 0 Graph 2 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NC MW-2 Monitoring Data -- Trichloroethene 5/23/00 9/26/00 1/30/01 .6/25/01 9/5/01 1/25/02 6/28102 9/17/02 1/28/03 5/7/03 9/23/03 1/13/04 2/22/05 Date Sampled —Seriesl 160 140 120 a 100 a a c 0 ' 80 c d u 0 0 0 60 '40 20 0 Graph 3 - Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NC MW-3 Monitoring -Data -- Trichloroethene 5/23/00 9/26/00 1/30/01 6/25/01 9/5/01 1/25/02 6/28/02 9/17/02 1/28/03 5/7/03 9123/03 1/13/04 2122/C Date Sampled tSeriesl Graph 4 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NC MW-4 Monitoring Data -- Trichloroethene 1200 1000 200 n 5/23/00 9/26/00 1130/01 6/25/01 9/5/01 1/25/02 6128/02 9/17/02 1/28/03 5/7/03 9/23/03 1/13/04 2/22/05 Date Sampled —Seriesl Graph 5 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NC MW-5 Monitoring Data -- Trichloroethene rig M 500 a a °' 400 c 0 1! c c07+ 300 c 0 U 200 100 0 5/23/00 ' 9/26/00 1/30/01 6/25/01 9/5/01 1/25/02 6/28/02 9/17/02 1/28/03 5/7/03 9/23/03 1113/04 2/22/( Date Sampled t Series1 1000 900 800 700 a 600 a e 0 500 c m u 0 400 U 300 200 950 720 Graph 6 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NC MW-6 Monitoring Data -- Trichloroethene 50 340 100 p , 5/23/00 9/26/00 1/30/01 6/25/01 9/5/01 1125/02 6/28/02 9117/02 1/28/03 5/7/03 9/23/03 1/13/04 2/22/05 Date Sampled t Series1 Graph 7 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NC MW-7 Monitoring• Data*-- Trichloroethene 16000 14000 12000 g 10000 a CL 0 8000 c m u 0 o 6000 4000 2000 0 5/23/00 9/26/00 1/30/01 6/25/01 9/5101 1/25/02 6/28/02 9/17/02' 1/28/03 5/7/03 9/23/03 1/1W04 2/22/05 Date Sampled -+-Series1 Graph 8 80 70 60 n 50 a - <.a o' 0 40 c m u c V 30 20 10 0 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NC MW-9 Monitoring Data -- Trichloroethene 5/23/00 .9/26100 1/30101 6/25/01 9/5/01 1/25/02 6/28/02 9/17/02 1/28/03 5/7/03 9/23/03 1/13/04 2/22/05 . Date Sampled s Seriesl Graph 9 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NC MW-10 Monitoring Data -- Trichloroethene 1800 1700 . 1600 1400 1200 Ca a 1000 0 ari 800 u e o• U 600 400 200 0 5/23/00 9/26/00 1/30/01 1 6126/01 9/5/01 1/25/02 6128/02 9/17/02 1/28/03 5/7/03 9/23/03 1/13/04 2/22105 Date Sampled tSeriesl 1000 900 800 700 c 600 a a a° �a 500 e u o 400 v 300 200 100 Graph 10 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NC MW-11 Monitoring Data -- Trichloroethene 930 80 740 620 460 350 31 9 0 40 130 q 23/00 9/26/00 1/30/01 6/25/01' 915/01 1125/02 6/28/02. 9/17/02 1/2b1U3 of{iUa WIZIUa 111o1u'+ zJA Date Sampled -+-Series1 700 600 500 a a a 400 c 0 e01i 300 0 O U 200 100 0 urapn i i Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NC MW-12 Monitoring Data -- Trichloroethene 5/23/00 9/26/00 1/30/01 6/26/01 9/5/01 1/25/02 6/28102 9117/02 1/28/03 5/7/03 9/23/03 1/13/04 2/22 Date Sampled t seriesl 180 160 140 120 a a a 100 0 80 u e 0 U 60 4C 2C C 170 M Graph 12 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NC MW-13 Monitoring Data -- Trichloroethene �R 110 75 7.82 5/23/00 9/26/00 1/30/01 6/25/01 9/5/01 1/25/02 6/28/U2 9/1/NZ 'II[oiva ginuo aicoiw 41441u Date Sampled Seriesl 100 90 80 70 a 60 0. c 0 A 50 e d c+ 0 40 U 30 20 10 0 Graph 13 Toastmaster, Inc. ' Ingraham Time Products Facility Laurinburg, NC ' MW-14 Monitoring Data-- Trichloroethene —-Seriesl 28 2 . 16 3.9 6 1/30/01. 6/25/01 9/5/01 1125/02 .6/28/02 9/17/02 1128/03 5/7103 9/23/03' .1/13/04 2/2. Date Sampled Graph 14 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NC. RW-1 Monitoring Data -- Trichloroethene 1000 900 800 700 a 600 0 m 500 c d 0 400 U 300 20C 10C !6/00 6/25/01 9/5/01 1/26/02 6/28102 9/17/02 1128/03 5/7/03 9/23/03 9/13N4 ZIG; Date Sampled �—Series1' 1200 1000 800 A a a c 0 600 e d u e 0 U 400 .200 C Graph 15 Toastmaster,Inc. Ingraham Time Products Facility Laurinburg, NC 9/26/00 6/25/01 9/5/01 1/25/0.2 6/28/02 9/17/02 1128/03. 517/03 9/23/03 1/13104 2/22105 Date Sampled PARADIGM ANALYTICAL LABORATORIES, INC. M00 Business Drive Wilmington, North Carolina 28405 (910) 350-1903.. Fax.(910) 350-1557 Mr. Rudy Smithwick Toastmaster, Inc. 8633 Vintage Club Dr. Wilmington NC 28411 Report Number: G420-46 Client Project: Toastmaster Laurinburg Dear Mr. Smithwick: Enclosed are the results of the analytical services performed under the referenced . project. The samples are certified to meet the requirements of the National Environmental Laboratory Accreditation Conference Standards. Copies of this report and supporting data will be retained in our files for a period of five years in the event they are required for future reference. Any samples submitted to our laboratory will will be retained fora maximum of thirty (3b) days from the date of this report unless other arrangements are requested. If there are any questions about the report'or the services performed during this project, please call Paradigm at (910) 350-1903. We will be happy to answer any questions or concerns which you may have. -Thank you for using Paradigm Analytical Labs for your analytical services. We look forward to working with you again on any additional analytical needs which you may have. Sincerely, Laboratories, Inc. J. Patrick Weaver 1. of 39 N.C. Certification #481 S.C. Certification #99029 I YAKAJJ1li1V1 AIVAL111l:A1, LAISVKAIVKIL,, 11V1:. Results for Volatiles by GC 601 Client Sample ID: MW-1 Analyzed By: DCS Client Project ID: Toastmaster Laurinburg Date Collected: 2/22/2005 0:00 Lab Sample ID: G42046-1A Date Received: 2/25/2005 Lab Project ID: G420-46 Matrix: Water Analyte Result RL ug/L ug/L Dilution Date Factor Analyzed Bromodichloromethane BQL 10.0 10 312/2005 Bromoform BQL 20.0 10 312/2005 Bromomethane BQL 10.0 10 3/2/2005 Carbon tetrachloride BQL 10.0 10 3/2/2005 Chlorobenzene BQL 10.0 10 3l2/2005 Chloroelhane BQL 10.0 10 3/2/2005 Chloroform BQL 10.0 10 312/2005 Chloromethane BQL 10.0 10 3/2/2005 Dibromochloromethane BQL 10.0 10 312/2005 1,2-Dibromoethane (EDB) BQL 10.0 10 312/2005 1,2-Dichlorobenzene BQL 10.0 10 312/2005 1,3-Dichlorobenzene BQL 10.0 10 312/2005 1,4-Dichlorobenzene BQL 10.0 10'. 3/212005 1,1-Dichloroethane BQL 10.0 10 3/2/2005 1,2-Dichloroethane BQL 10.0 10 3/2/2005 1,1-Dichloroethene BQL 10.0 10 312/2005 cis-1,2-Dichloroethene BQL 10.0 10 312/2005 trans-1,2-Dichloroethene BQL 10.0 10 312/2005 1,2-Dichloropropane BQL 10.0 10 312/2005 cis-1,3-Dichloropropene BQL 10.0 10 3/2/2005 trans-1,3-Dichloropropene BQL 10.0 10 3/2/2005 Methylene Chloride BQL 50.0 10 312/2005 1,1,2,2-Tetrachloroethane BQL 10.0 10 312/2005 Tetrachloroethene BQL 10.0 10 .312/2005 1,1,1-Trichloroethane BQL 10.0 10 312/2005 1,1,2-Trichloroethane BQL 10.0 10 3/2/2005 Trichloroethene ' 95.7 10.0 10 312/2005 Trichiorofluoromethane BQL 10.0 10 3/212005 Vinyl Chloride BQL 10.0 10 312/2005 Surrogate Spike Recoveries Spike Spike Percent Added Result Recovery 1,4-Dichlorobutane 40 41.1 103 Comments: All values corrected for dilution. BQL = Below quantitation limit. Reviewed By:, 2 of 39 N.C. Certification #481 S.C. Certification #99029 PARADIGM ANALYTICAL LABORATORIES, INC. Results for Volatiles by GC 601 Client Sample ID: MW-2 Analyzed By: JTF Client Project ID: Toastmaster Laurinburg Date Collected: 2/22/2005 0:00 Lab Sample ID: G420-46-2A Date Received: *2/25/2005 Lab Project ID:.G420-46 i Matrix: Water ' Analyte Result. ` RL Dilution Date i ugn. ugrL Factor Analyzed Bromodichloromethane BQL 20.0 20 3/2/2005 Bromoform BQL 40.0 20 3/2/2005 Bromomethane BQL, 20.0 20 312/2005 Carbon tetrachloride BQL 20.0 20 3/212005 Chlorobenzene BQL" 20.0 20 312/2005 Chloroethane BQL 20.0 20 3/2/2005 Chloroform BQL 20.0 20 312/2005 Chloromethane BQL 20.0 20 3/2/2005 Dibromochloromethane BQL 20.0 20 312/2005 1,2-Dibromoethane (MB) BQL 20.0 20 3/212005 1,2-Dichlorobenzene BQL 20.0 20 312/2005 1,3-Dichlorobenzene BQL 20.0 20 3/2/2005' 1,4-Dichlorobenzene BQL 20.0 20 3/2/2005 1,1-Dichloroethane BQL 20.0 20 3/2/2005 1,2-Dichloroethane BQL 20.0 20 3/2/2005 1,1-Dichloroethene BQL 20.0 20 312/2005 cis-1,2-Dichloroethene BQL 20.0 20 3/2/2005 trans-1,2-Dichloroethene BQL 20.0 20 3/212005 1,2-Dichloropropane BQL 20.0 20 312/2005 cis-1,3-Dichloropropene' BQL 20.0 20 3/2/2005 trans-1,3-Dichloropropene BQL 20.0 20 31212005 Methylene Chloride BQL 100 20 31212005 1,1,2,2-Tetrachloroethane BQL 20.0 20 3/2/2005 Tetrachloroethene BQL 20.0 20 3/212005 1,1,1-Trichloroethane BQL 20.0 20 3/212005 1,1,2-Trichloroethane BQL 20.0 20 312/2005 Trichloroethane 289 20.0 20 3/212005 Tdchlorotluoromethane _BQL 20.0 20, 3/212005 Vinyl Chloride BQL.' 20.0 20 3/212005 Surrogate Spike Recoveries Spike Spike Percent Added Result Recovery 1,4-Dichlorobutane 40 41.7 104. Comments:' All values corrected for dilution. BQL= Below quantitation limit. 0 Reviewed By:/-,f7 3 of 39 N.C. Certification #481 S.C. Certification #99029 PARADIGM ANALYTICAL LABORATORIES, INC. Results for Volatiles by GC 601 Client Sample ID: MW-3 Analyzed By: JTF Client Project ID: Toastmaster Laurmburg Date Collected: 2/22/2005 0:00 Lab Sample ID: G420-46-3A Date Received: 2/25/2005 Lab Project ID: G420-46 Matrix: Water Analyte . Result RL Dilution Date 1 ugu. uglr. Factor Analyzed Bromodichloromethane BQL 5.00 5. 311/2005 .. i Bromoform BQL 10.0 5 3l1/2005 Bromomethane BQL 5.00 5 3/1/2005 .. Carbon tetrachloride BQL 5.00 5 .. 3/1/2005 Chlorobenzene BQL 5.00 5 311/2005 1 Chlorcethane BQL 5.00 5 311/2005 Chloroform BQL 5.00 5 31.1/2005 Chloromethane BQL 5.00 5 311/2005 Dibromochloromethane BQL 5.00 5 311/2005 1,2-Dibromoeihane (EDB) BQL 5.00 5 3/1/2005 1,2-Dichlorobenzene BQL 5.00 5 3/1/2005 f 1,3-Dichlorobenzene BQL 5.00 5 311/2005 1,4-Dichlorobenzene BQL 5.00 5 311/2005 1,1-Dichloroethane BQL 5.00 5 31112005 1,2-Dichloroethane BQL 5.00 5 3/1/2005 1 1,1-Dichloroethene BQL 5.00 5 311/2005 cis-1,2-Dichloroe(hene BQL 5.00 5 311/2005 trans-1,2-Dichlorcethene BQL 5.00 5 311/2005 1,2-Dichloropropane BQL 5.00 5 31112005 cis-1,3-Dichloropropene . BQL 5.00 5 3/1/2005 trans-1,3-Dichloropropene BQL 5.00 5 311/2005 Methylene Chloride BQL 25.0 5 311/2005 1,1,2,2-Tetrachloroethane BQL 5.00 5 3/112005 Telrachloroethene BQL 5.00 5 31112005 1,1,1-Trichloroethane BQL 5.00 5 3/1/2005 1,1,2-Trichloroethane BQL 5.00 5 811/2005 Trichloroethene 81.6 5.00 5 3/1/2005 Trichlorofluoromethane BQL 5.00 5 3/1/2005 Vinyl Chloride BQL 5.00 5 3/112005 ' Surrogate Spike Recoveries Spike Spike Percent Added Result Recovery 1,4-Dichlorobutane 40 41.3 .103 Comments: . All values corrected for dilution. BQL = Below quantitation limit. Reviewed By:/IE 4 of 39 N.C. Certification #481 S.C.' Certification #99029 n PARADIGM ANALYTICAL LAB11RA1.•URIES, INC. Results for Volatiles by GC 601 Client Sample ID: MW-4 Client Project ID: Toastmaster Laudnburg Lab Sample ID: G420-46-4A Lab Project ID: G420-46 Analyzed By: JTF Date Collected: 2/22/2005 0:00 Date Received: 2/25/2005 Matrix: Water Analyte Result RL Dilution Date t uglL ug1L Factor Analyzed Bromodichloromethane BQL 10.0 10 312/2005 Bromoform BQL 20.0 10 3/212005 Bromomethane BQL 10.0 10 312/2005 Carbon tetrachloride BQL 10.0 10 312/2005 Chlorobenzene BQL 10.0 10 312/2005 Chloroethane BQL 10.0 10 312/2005 Chloroform BQL 10.0 10 3/2/2005 Chloromethane BQL 10.0 10 3/2/2005 Dibromochloromethane BQL 10.0 10 302005 1,2-Dibromoethane(EDB) BQL 10.0 10 312/2005 1,2-Dichlorobenzene BQL 10.0 10 3/212005 1,3-Dichlorobenzene BQL. 10.0 . 10 -312/2005 1,41Dichlorobenzene BQL 10.0 10 3/212005 1,1-Dichloroethane BQL 10.0 10 31212005 1,2-Dichloroethane BQL 10.0 10 312/2005 1,1-Dichloroethene BQL 10.0 10 .312/2005 cis-1,2-Dichloroethene 75.0 10.0 10 302005 trans-1,2-Dichloroethene BQL 10.0 10 312/2005 1,2-Dichioropropane BQL . 10.0 10 312/2005 cis-1,3-Dichloropropene BQL 10.0 10- 3/212005 trans-1,3-Dichloropropene BQL 10.0 10 31212005 Methylene Chloride BQL 50.0 10 3/212005 1,1,2,2-Tetrachloroethane BQL 10.0 10 312/2005 Tetrachloroethene BQL 10.0 10 3/212005 1,1,1-Trichloroethane BQL 10.0 10 3/212005 1,1,2-Trichloroethane BQL 10.0 10 3/212005 Trichloroethene 209 10.0 10 31212005 Trichlorofluoromethane BQL 10.0 10, 312/2005 Vinyl Chloride BQL 10.0 10 3/212005 Surrogate Spike Recoveries Spike Spike Percent Added Result Recovery 1,4-Dichlorobutane 40 41.4 103 Comments: All values corrected for dilution. BQL=Below quantitation limit. Reviewed By:A, 5 of 39 N.C. Certification #481 S.C. Certification #99029 PARADIGM ANALYTICAL LABORATORIES, INC. Results for Volatiles by GC 661 Client Sample ID: MW-5 Analyzed By: JTF Client Project ID: Toastmaster Laurinburg Date Collected: 2/22/2005 0:00 Lab Sample ID: G420-46-5A Date Received: 2/25/2006 Lab Project ID: G420-46 Matrix: Water Analyte Result RL Dilution Date i ugn. ugrL Factor Analyzed Bromodichloromethane BQL 1.00 1 311/2005 Bromoform BQL 2.00 1 3/1/2005 1 Bromomelhane BQL 1.00 1 311/2005 Carbon tetrachloride BQL 1.00 1 31//2005 Chlorobenzene BQL 1.00 1 311/2005 Chloroethane BQL 1.00 1 311/2005 Chloroform BQL 1.00 1 3/1/2005 Chloromelhane BQL 1.00 1 311/2005 Dibromachloromethane BQL 1.00 1 311/2005 1,2-Dibromoethane (EDB) BQL 1.00 1 311/2005 1,2-Dichlorobenzene BQL 1.00 1 311/2005 1,3-Dichlorobenzene BQL 1.00 1 .311/2005 1,4-Dichlorobenzene BQL 1.00 1 3/1/2005 1,1-Dichloroethane BQL 1.00 1 311/2005 1,2-Dichloroethane BQL 1.00 1 311/2005 1,1-Dichloroethene BQL 1.00 1 3/1/2005 cis-1,2-Dichloroethene BQL 1.00 1 311/2005 trans -1,2-Dichloroethene BQL 1.00 1 311/2005 1,2-Dichloropropane BQL 1.00 1 3/1/2005 cis-1,3-Dichloropropene BQL 1.00 1 3/1/2005 trans-1,3-Dichloropropene BQL 1.00 1 . 3/112005 Methylene Chloride BQL 5.00 1 31112005 • 1,1,2,2-Tetrachloroethane BQL 1.00 1 3l1/2005 Tetrachloroethene BQL 1.00 1 31112005 1,1,1-Trichloroethane BQL 1.00 1 311/2005 1,1,2-Trichloroethane BQL 1.00 1 311/2005 Trichloroethene 5.94 1.00 1 3/1/2005 Trichlorofluoromethane BQL 1.00 1 31112005 Vinyl Chloride BQL 1.00 1 311/2005 Surrogate Spike Recoveries Spike Spike Percent Added Result Recovery 1,4-Dichlorobuhane 40 40.9 102 Comments: All values corrected for dilution. BQL = Below quantitation limit. Reviewed By:,-AF 6 of 39 N.C. Certification #491 S.C. Certification #99029 PARADIGM ANALYTICAL LABORATORIES, INC. Results for Volatiles by GC 601 Client Sample ID: MW-6 Analyzed By: DCS Client Project ID: Toastmaster Laurinburg Date Collected: 2/22/2005 0:00 Lab Sample ID: G420-46-6A Date Received: 2/25/2005 Lab Project lb: G42046 Matrix: Water Analyte Result RL uglL uglL Dilution Date Factor Analyzed Bromodichloromethane BQL 10.0 10 3/2/2005 Bromoform BQL 20.0 10 -3/212005 Bromomethane BQL 10.0 10 312/2005 Carbon tetrachloride BQL 10.0 10 31212005 Chlorobenzene BQL 10.0 10 3/212005 Chlomethane BQL 10.0 10 312/2005 Chloroform BQL 10.0 10 3/2/2005 Chloromethane BQL 10.0 10 3/2/2005 Dibromochloromethane BQL 10.0 10 312/2005 1,2-Dibromoethane(EDB) BQL 10.0. 10 3/2/2005 1,2-Dichlorobenzene BQL 10.0 10 3/2/2005 1,3-Dichlorobenzene BQL 10.0 10 3/2/2005 1,4-Dichlorobenzene BQL 10.0- 10 3/2/2005 1,1-Dichloroethane BQL 10.0 10 3P2/2005. 1,2-Dichloroethane BQL 10.0 10 312/2005 1,1-01chloroethene BQL 10.0 10 3/2/2005 cis-1,2-Dichloroethene 21.1 10.0 10. 312/2005 trans-1,2-Dichloroethene BQL 10.0 10 31212005 1,2-Dichloropropane BQL 10.0 10 3/2/2005 cis-1,3-Dichloropropene BQL 10.0 10 312/2005 trans-1,3-Dichloropropene BQL 10.0 10 W212005 Methylene Chloride BQL 50.0 10 312/2005 1,1,2,2-Tetrachloroethane BQL 10.0 10 3/212005 Tetrachloroethene BQL 10.0 10 3/212005 1,1,1-Trichloroelhane BQL 10.0 10 31212005 1,1,2-Trichlbroethane BQL 10.0 10 31212005 Tiichloroethene 145 10.0 10 312/2005 Trichlorofluoromethane BQL 10.0 10 31212005 Vinyl Chloride - BQL 10.0 10 3/212005 Surrogate Spike Recoveries Spike Spike Percent Added Result Recovery 1,4-Dichlorobutane 40 41.8 104 Comments: All values corrected for dilution. BQL = Below quantitation limit. Reviewed By: 7 of 39 N.C. Certification #481 - S.C. Certification #99029 YAHAMUM ANALY'1'1GAL LABUKAWKILJ, INN. Results for Volatiles by GC 601 Client Sample ID: MW-7 Analyzed By: JTF Client Project ID: Toastmaster Laurinburg Date Collected: 2/22/2005 0:00 Lab Sample ID: G420-46-7A Date Received: 2125/2005 Lab Project ID: G420-46 Matrix: Water Analyte Result RL Dilution Date uglL ugn. Factor Analyzed Bromodichloromethane BQL 8.00 8 3/2/2005 Bromoform BQL 16.0 8 3/212005 Bromomethane BQL 8.00 8 3/2/2005 Carbon tetrachloride BQL 8.00 8 3/2/2005 Chlorobenzene BQL 8.00 8 3/2/2005 Chlorcethane BQL 8.00 8 3/2/2005 Chloroform BQL 8.00 8 312/2005 Chloromethane 8QL 8.00 8 3/2/2005 Dibromochloromethane BQL 8.00 8 312/2005 1,2-Dibromoethane (EDB) BQL 8.00 8 3/2/2005 1,2-Dichlorobenzene BQL 8.00 8 3/2/2005 1,3-Dichlorobenzene BQL 8.00 8 31212005 1,4-Dichlorobenzene BQL 8.00 8 312/2005 1,14)ichloroethane BQL 8.00 8 3/2/2005 1,2-Dichloroethane BQL 8.00 8 3/2/2005 1,1-Dichloroethene BQL 8.00 8 3/2/2005 cis-1,2-Dichloroethene BQL 8.00 8 312/2005 trans-1,2-Dichloroethene BQL 8.00 8 3/2/2005 1,2-Dichloropropane BQL 8.00 8 312/2005 cis-1,3-Dichloropropene BQL 8.00 8 3/2/2005 tra6s-1,3-Dichloropropene BQL 8.00 8 3/212005 Methylene Chloride BQL 40.0 8 3/212005 1,1,2,2-Tetrachloroelhane BQL 8.00 8 312/2605 Tetrachloroethene 17.9 8.00 8 3/212005 1,1,1-Trichloroethane BQL 8.00 8 3/212005 1,1,2-Trichloroethane BQL 8.00 8 312/2005 Trichloroethene 106 8.00. 8 312/2005 Trichlorofluoromethane BQL . 8.00 8 312/2005 Vinyl Chloride BQL 8.00 8 3/212005 Surrogate Spike Recoveries Spike Spike Percent Added Result Recovery 1,4-Dichlorobutane 40 41.5 104 Comments: All values corrected for dilution. BQL= Below quantitation limit. Reviewed By: 8 of 39 N.C. Certification #481 S.C. Certification #99029 PARADIGM ANALYTICAL LABORATORIES, INC. Results for Volatiles by GC 601 Client Sample ID: MW-9 Analyzed By: JTF Client Project ID: Toastmaster Laurinburg Date Collected: 2/22/2005 0:00 Lab Sample ID: G420-46-BA Date Received: 2/25/2005 Lab Project ID: 6420-46 Matrix: Water Analyte Result RL Dilution Date ug/L uglL Factor Analyzed Bromodichloromethane BQL 1.00 1 3/1/2005 Bromoform BQL 2.00 1 3/1/2005 Bromomethane BQL 1.00 1 3/1/2005' Carbon tetrachloride BQL 1.00 1 311/2005 Chlorobenzene BQL 1.00 1 311/2005 Chloroethane BQL 1.00 1= 311/2005 Chloroform BQL 1.00 1 3/1/2005 Chloromethane. BQL I,00 1 3/1/2005 Dibromochloromethane BQL 1.00 1 311/2005 1,2-Dibromoethane (EDB) BQL 1.00 1 3/112005 1,2-Dichlorobenzene BQL 1.00 1 311/2005 1,3-Dichlorobenzene BQL 1.00 1 3/1/2005 ' 1,4-Dichlorobenzene BQL 1..00 1 3/112005 1,1-Dichloroelhane BQL 1.00 1 3/112005 1,2-Dichloroethane BQL 1.00 1 3/1/2005 1,1-Dichlor6ethene BQL 1.00 1 3/1/2005 cis-1,2-Dichloroethene BQL 1.00 1. 311/2005 trans-1,2-Dichloroethene BQL 1.00 1. 3/1/2005 1,2-Dichloropropane' BQL 1.00 1 311/2005 c7is-1,3-Dichloropropene BQL 1.00 1 311/2005 trans-1,3-Dichloropropene BQL 1.00 1 311/2005 Methylene Chloride BQL 5.00 1 3/1/2005 1,1,2,2-Tetrachloroethane BQL 1.00 1 311/2005 Tetrachloroethene BQL 1.00 1 3/1/2005 1,1,1-Trichloroethane BQL 1.00 1 3/112005 1,1,2-Trichloroethane BQL 1.00 1 311/2005 Trichloroethene BQL 1.00 1 3/112005 Trichlorofluoromethane BQL 1.00 1 3/1/2005 Vinyl Chloride . BQL 1.00 1 3/1/2005 Surrogate Spike Recoveries Spike Spike Percent Added Result Recovery 1,4-Dichlorobutane 40 40.5 101 Comments: All values corrected for dilution. BQL= Below quantitation limit. Reviewed By:,ff— 9 of 39 N.C. Certification #481 S.C. Certification #99029 PARADIGM ANALY'1'IUAL LABURAIU1(1E6, 1NU. Results for Volatiles by GC 601 Client Sample ID: MW-10 Analyzed By: DCS Client Project ID: Toastmaster Laurinburg Date Collected: 2/22/2005 0:00 Lab Sample ID: G420-46-9A Date Received: 2/25/2005 Lab Project ID: G420-46 Matrix: Water Analyte Result RL Dilution Date ' ug1L - ug/L Factor Analyzed Bromodichloromethane BQL 1.00 1 3/1/2005 Bromoform BQL. 2.00 1 3/1/2005 Bromomethane BQL, 1.00 1 3/1/2005 Carbon tetrachloride BQL 1.00 1 3/1/2005 Chlorobenzene BQL 1.00 1 .3/112005 Chloroethane BQL 1.00 1 3/112005 Chloroform BQL 1.00 1 3/112005 Chloromethane BQL 1.00 1 3/1/2005 Dibromochloromethane BQL 1.00 1 3/1/2005 1;2-Dibromoethane(EDB) BQL 1.00 1 3/1/2005 1,2-Dichlorobenzene BQL 1.00 1 3/1/2005 1,3-Dichlorobenzene BQL 1.00 1 3/1/2005 1,4-Dichlorobenzene BQL 1.00 1 3/1/2005 1,1-Dichloroethane _ BQL 1.00 1 3/112005 1,2-Dichloroethane BQL 1.00 1 3/112005 1,1-Dichloroethene BQL 1.00 1 3/112005 cis-1,2-Dichloroethene 4.21 1.00 1 M/2005 trans-1,2-Dichloroethene BQL 1.00 1 3/112005 1,2-Dichloropropane BQL 1.00 1. 3/1/2005 cis-1,3-Dichloropropene BQL 1.00 1 31112005 trans+l,3-Dichloropropene BQL 1.00 1 3/112005 Methylene Chloride BQL 5.00 1 311/2005 1,1,2,2-Tetrachlor6ethane BQL 1.00 1 3/112005 Tetrachloreethene BQL 1.00 1 3/1/2005 1,1,1-Trichloroethane BQL 1.00 1 31112005 1,1,2=Trichloroethane BQL. 1.00 1 3/112005 Trichloroethene 17.6 1.00 1 3/1/2005 Trichlorofluoromethane BQL' 1.00 1 311/2005 Vinyl Chloride BQL 1.00 1 ,3/112005 Surrogate Spike Recoveries Spike Spike Percent Added Result Recovery 1,4-Dichlorobutane 40 41.2 103 Comments: All values corrected for dilution. BQL = Below quantitation limit. Reviewed By: 10 of 39 N.C. Certification #481 S.C. Certification #99029, , YPYKHL1b1V1 H1VHL111l+HL 1.HDV1cHlVxcic,�; uva,. Results for Volatiles by GC 601 Client Sample ID: MW-11 Analyzed By: JTF . Client Project ID: Toastmaster Laurinburg Date Collected: 2/22/2005 0:00 . i Lab Sample ID: G420-46-10A Date Received: 2/25/2005 Lab Project ID: G420-46 Matrix: Water Analyte Result RL Dilution Date egg _ uglL Factor Analyzed Bromodichloromethane BQL 20.0 20 3/212005 Bromoform BQL 40.0 20 312/2005 Bromomethane BQL 20.0 20 3/212005 - Carbon tetrachloride BQL 20.0 20 3/2/2005 Chlorobenzene BQL 20.0 20 31212005 Chloroethane BQL 20.0 20 31212005 Chloroform BQL 20.0 20 3/212005 Chforomethane BQL 20.0 20 31212005 Dibromochloromethane BQL 20.0 20 312/2005 ' 1,2-Dibromoethane (EDB) BQL 20.0 20 312/2005 1,2-Dichlorobenzene BQL 20.0 20 312I2005 1,3-Dichlorobenzene BQL 20.0 20 312/2005 . 1,4-Dichlorobenzene BQL 20.0 .20 3/2I2005 1,1-Dichloroethane BQL 20.0 20 312/2005 1,2-Dichloroethane BQL 20.0 20 312/2005 1,1-Dichloroethene BQL • 20.0 20 312/2005 cis-1,2-Dichloroethene BQL 20.0 20 3/2/2005 trans-1,2-Dichloroethene BQL 20.0 20 3/2/2005 1,2-Dichloropropane BQL 20.0 20 3/212005 cis-1,3-Dichloropropene BQL 20.0 20 312/2005 trans-1,3-Dichloropropene BQL 20.0 20 312/2005 Methylene Chloride BQL 100 20 3/2/2005 1,1,2,2-Tetrachloroethane BQL 20.0 20 31212005 Tetrachloroethene BQL 20.0 20 312/2005 1,1,1-Trichloroethane BQL 20.0 20 312/2005 j 1,1,2-Trichloroethane ' .. BQL 20.0 20 31212005 Trichloroethene 316 20.0 20 31212005 Trichlorofluoromethane BQL 20.0 20 .312/2005 Vinyl Chloride BQL 20.0 20 312/2005 Surrogate Spike Recoveries Spike Spike Percent Added Result Recovery 1,4-Dichlorobutane 40 41.2 103 Comments:. All values corrected for dilution. BQL= Below quantitation limit. Reviewed By 11 of 39 N.C. Certification #481 S.C. Certification #99029 PARADIGM ANALYTICAL LABORATORIES, INC. Results for Volatiles by GC 601 Client Sample ID: MW-12 Analyzed By: JTF Client Project ID: Toastmaster Laurinburg Date Collected: 2/22/2005 0:00 Lab Sample ID; G42046-11A Date Received: 2/25/2005 Lab Project ID: G42046 Matrix: Water Analyte Result RL Dilution Date ' ug/L ug[L Factor Analyzed Bromodichloromethane BQL 4.00 4 3/1/2005 Bromoform BQL 8.00 4 3/1/2005 Brdmomethane BQL 4.00 4 311/2005 Carbon tetrachloride BQL 4.00 4 3l1/2005 Chlorobenzene BQL 4.00 4 .311/2005 Chloroethane BQL 4.00 4 311/2005 Chloroform BQL 4.00 4 3/1/2005 Chloromethane BQL 4.00 4 3/1/2005 Dibromochloromethane BQL 4.00 4 3/1/2005 1,2-Dibromoethane (EDB) BQL 4.00 4 3/1/2005 1,2-Dichlorobenzene BQL 4.00 4 3/1/2005 1,3-Dichlorobenzene BQL 4.00 4 311/2005 1,4-016hlorobenzene BQL 4.00 4 3/1/2005 1,1-Dichloroethane BQL 4.00 4 ' 3/1/2005 1,2-Dichloroethane BQL 4.00 4 3/1/2005 1,1-01chloroethene BQL 4.00 4. .3/1/2005 cis-1,2-Dichloroethene 7.39 4.00 4 3/1/2005 trans-1,2-Dichloroethene BQL 4.00 4 3/1/2005 1,2-Dichloropropane BQL 4.00 4 3/1/2005 cis-1,3-Dichloropropene BQL 4.00 4 3/1/2005 trans-1,3-Dichloropropene BQL 4.00 4 3/1/2005 Methylene Chloride BQL 20.0 4 3/1/2005 1,1,2,2-Tetrachloroethane BQL 4.00 4 3/1/2005 Tetrachloroethene BQL 4.00 4 3/1/2005 1,1',1-Trichloroethane BQL 4.00 4 3/112005 1,1,2-Trichloroethane BQL 4.00 4 3/1/2005 Trichloroethene 128 • 4.00 4 311/2005 Trichlorofluoromethane BQL 4.00 4 3/1/2005 Vinyl Chloride BQL 4.00 4 3/1/2005 Surrogate Spike Recoveries Spike Spike Percent Added Result Recovery 1,4-Dichlorobutane 40 40.8 102 Comments: All values corrected for dilution. BQL = Below quantitation limit. Reviewed By: cc ums -42 of 39 N.C. Certification #481 S.C. Certification #99029 I PARADIGM ANALYTICAL LABORATORIES, INC. Results for Volatiles by GC 601 Client Sample ID: MWA3 Analyzed By: DCS Client Project ID: Toastmaster Laurinburg Date Collected: 2/22/20,05 0:00 Lab Sample ID: G420-46-12A Date Received: 2/25/2005 Lab Project ID: G42046 Matrix: Water Analyte B ro m o d i c h l o ro m e th a n e Bromofomn Bromomethane Carbon tetrachloride Chlorobenzene Chloroelhane Chloroform Chloromethane . D ibromochlo romethane 1,2-Dibrom6ethane (EDB) 1,2-01chlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroelhene cis-1, 2-Dichloroethene trans-1,2-Dichloroeth ene 1,2-Dichloropropane cis-1,3-Dichloropropene . trans-1,3-Dichloropropene Methylene Chloride 1,1,2,2-Tetrachloroethane Tetrachloroethene 1,1,1-Trichloroethane 1,12-Trichloroethane Trichloroethene Tri chlorofluorometh ane Vinyl Chloride Surrogate Spike Recoveries 1,4-Dichlorobutane Comments: All values corrected for dilution. BQL = Below quantitation limit. Result ug/L BQL BQL BQL BQL BQL BQL BQL BQL. BQL BQL ' BQL BQL .BQL BQL BQL BQL 1.48 BQL BQL BQL BQL BQL BQL BQL BQL BQL 7.82 BQL . BQL RL ug/L 1.00 2.00 1.00 1.00 1.00. 1.00 1.00 1.00 1.06 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 5.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 Spike Added 40 Dilution Factor Spike Result 41:4 Data Analyzed 311/2005 31112005 311/2005 3/1/2005 311/2005 3/1/2005 311/2005 311/2005 .311/2005 3/1/2005 311/2005 311/2005 311/2005 311/2005 3/1/2005 3/1/2005 311/2005 311/2005 3/1/2005 311/2005 311/2005 311/2005 3/1/2005 311/2005 311/2005 311/2005 311/2005 3/1/2005 .311/2005 Percent Recovery 10.4 ,J Reviewed By� 13 of 39 N.C. Certification #481 S.C. Certification #99029 YARAVIUM AIVALY�l1l;AL LABUKAlURIEb, INN. Results for Volatiles by GC 601 Client Sample ID:, MW-14 Analyzed By: JTF Client Project ID:,Toastmaster Laurinburg Date Collected: 2/22/2005 0:00 Lab Sample ID: G42046-13A Date Received: 2/25/2005 Lab Project ID: G420-46 Matrix: Water it 1 Analyte Result RL Dilution . Date uga ugrL Factor Analyzed Bromodichloromethane BQL 1.00 1 3/1/2005 i Bromoform BQL 2.00 1 311/2005 Bromomethane BQL 1.00 1 3/1/2005 Carbon tetrachloride BQL 1.00 1 91112005 { Chlorobenzene BQL 1.00 1 3/112005 Chloroethane BQL 1.00 1 311/2005 Chloroform BQL 1.00 1 31112005 Chloromethane BQL, 1.00 1 311/2005 Dibromochloromethane BQL 1.00 1 3/1/2005 1,2-Dibromoethane (EDB) BQL 1.00 1 3/1/2005 1,2-Dichlorobenzene BQL 1.00 1 3/1/2005 1,3-Dichlorobenzene BQL 1.00 1 311/2005 1,4-Dichlorobenzene BQL. 1.00 1 3/1/2005 1,1-Dichloroethane BQL 1.00 1 311/2005 1,2-Dichloroethane BQL 1.00 1 3/112005 1,1-Dichloroeth6ne BQL 1.00 1 3/112005 cis-1,2-Dichloroethene BQL 1.00 1 3/1/2005 trans-1,2-Dichloroethene BQL 1:00 1 311/2005 1,2-Dichloropropane BQL .1.00 1 311/2005 cis-1,3-Dichlorepropene BQL 1.00 1 3/1/2005 trans-1,3-Dichloropropene BQL 1.00 1 311/2005 Methylene Chloride BQL 5.00 1 3/11/2005 1,1,2,2-Telrachloroethane. BQL 1.00 1 3/1/2005 I Tetrachloroethene BQL 1.00 1 3/1/2005, 1,1,1;Trichloroethane BQL 1.00 1 3/112005 1,1,2-Trichloroethane BQL 1.00 1 311/2005 Trichlorcethene 3.94 1.00 1 3/1/2005 Trichlorofluoromethane BQL 1.00 1 3/112005 Vinyl Chloride BQL 1.00 1 3/1/2005 Surrogate Spike Recoveries Spike Spike Percent Added Result Recovery 1,,4-Dichiorobutane 40 41.5 104 Comments: All values corrected for dilution. BQL = Below quantitation limit. Reviewed By:. 14 of 39 N.C. Certification #481 S.C. Certification #99029 PARADIGM ANALYTICAL LASURArURI S, INC. Results for Volatiles by GC 601 Client Sample ID: RWA 'Client Project ID: Toastmaster Laurinburg Lab Sample ID: G420-46-14A Lab Project ID: G420-46 Analyte Result ug/L Bromodichloromethane BQL Bromoform BQL Bromomethane BQL Carbon tetrachloride BQL Chlorobenzene BQL Chloroethane - BQL Chloroform BQL Chlorome thane BQL 1)ibromochloromethane BQL 1,2-Dibromoethane (EDB) BQL 1,2-Dichlorobenzene BQL 1,3-Dichlorobenzene BQL 1,4-Dichlorobenzene BQL 1,1-Dichloroethane BQL 1,2-Dichloroethane BQL 1',1-Dichloroethene BQL ' cis-1,2.Dichloroethene BQL trans-1,2-Dichloroethene BQL 1,2-01chloropropane BQL cis-1,3-Dichloropropene BQL trans-1,3-Dichloropropene BQL Methylene Chloride BQL 1,1,2,2-Tetrachloroethane BQL Tetrachloroethene . , BQL 1,1,1-Trichloroethane BQL 1,1,2-Trichloroethane BQL, Trichloroethene 264 Trichlorofluoromethane BQL Vinyl Chloride BQL Surrogate Spike Recoveries . 1,4-Dichlorobutane Comments: All values corrected for dilution. BQL = Below quantitation limit. Analyzed By: JTF Date Collected: 2/22/2005 0:00 Date Received: 2/2512005 Matrix: Water RL ugn- 20.0 40.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 160 20.0 20.0 20.0 20.0 20.0 20.0 20.0 Spike Added 40 . Dilution Date Factor Analyzed 20 312/2005 20 3l2/2005 20 312/2005 20 312/2005 20 312/2005 20 3/2/2005 ' 20 3/212005 20 3/2/2005 20 312/2005 20 3/2/2005 20 312/2005 20 3/2/2005 20 3/2/2005 20 3/212005 20 3/2/2005 20 .3/2/2005 20 3/212005 20 312/2005 20 31212005 20 312/2005 20 3/212005 20 3/212005 20 3/212005 20 3/212005 20 3/2/2005 20 31212005 20 302005 20 3/212005 20 3/2/2005 Spike Percent Result Recovery 41.3 103 Reviewed By: 15 of 39 N.C. Certification #481 S.C. Certification #99029 PARADIGM ANALYTICAL LABORATORIES, INC. ` Results for Volatlles by GC 601 Client Sample ID: RW-2 Analyzed By: JTF Client Project ID: Toastmaster Lauririburg Date Collected: 2/22/2005 0:00 Lab Sample ID: G42046-15A Date Received: 2/25/2005 Lab Project ID: G420-46 Matrix: Water i , ' Analyte Result RL Dilution Date uga ug/L Factor Analyzed Bromodichloromethane BQL 10.0 10 3/2/2005 Bromoform BQL 20.0 10 3/212005 Bromomethane BQL 10.0 10 31212005 Carbon tetrachloride BQL 10.0 10 31212005 Chlorobenzene BQL 10.0 10 3/2/2005 t Chloroethane BQL 10.0 10 312/2005 Chloroform BQL 10.0 10 3/212005 Chloromethane BQL 10.0 10 3/2/2005 Dibromochloromethane BQL . 10.0 10 3/2/2005 1,2-Dibromoethane (EDB) BQL 10.0 10 3/212005 1,2-Dichlorobenzene BQL 10.0 10 312/2005. 1,3-Dichlorobenzene BQL 10.0 10. 3/212005 1,4-Dichlorobenzene BQL . 10.0 10 31212005 1,1-Dichloroethane BQL 10.0 10 3/2/2005 1,2-Dichloroethane BQL 10.0 10 3/2/2005 1,1-Dichloroethene BQL 10.0 10 3/212005 cis-1,2-Dichloroethene BQL 10.0 _ 10 312/2005 trans-1,2-Dichloroethene BQL 10.0 10 312/2005 1,2-Dichloropropane BQL 10.0 10 3/212005 cis-1,3-Dichloropropene BQL 10.0 10 3/212005 trans-1,3-Dichloropropene BQL 10.0 10 312/2005 Methylene Chloride BQL 50.0 10 312/2005 1,1,2,2-Tetrachloroethane BQL 10.0 10 3/212005 Tetrachloroethene BQL 10.0 10 3/2/2005 ' 1,1,1-Trichloroethane BQL 10.0 10 3/212005 1,1,2-Trichloroethane BQL 10.0 10 312/2005 Trichloroethane' 217 10.0 10 3/212005 Trichlorofluoromethane BQL 10.0 10 312/200.5 Vinyl Chloride BQL 10.0 10 3l2/2005 Surrogate Spike Recoveries Spike Spike Percent Added Result Recovery 1,4-Dichlorobutane 40 41.3 103 Comments: All values corrected for dilution. BQL = Below quantitation limit. Reviewed By: A . 16 of 39 N.C. Certification #481 S.C. Certification #99029 PARADIGM ANALYTICAL LABURA1'URI S, INC. ' Results for Volatiles by GC 601 Client Sample ID: RW-3 Analyzed By: DCS ' Client Project ID: Toastmaster Laurinburg Date Collected: 2/22/2005 0:00 Lab Sample ID: G42046-16A Date Received: 2/25/2005 Lab Project ID: G420-46 Matrix: Water Analyte Result RL Dilution Date i ugn. ugn. Factor Analyzed Bromodichloromethane BQL 10.0 10 31212005 ? Bromoform BQL 20.0 10 3l2/2005 Bromomethane BQL 10A 10 312/2005 Carbon tetrachloride BQL 10.0 10 3/212005 Chlorobenzene BQL 10.0 10 31212005 j Chloroethane BQL 10.0 10 312/2005. Chloroform BQL 10.0 10 312/2005 Chloromethane BQL 10.0 10 3/212005 Dibromcchloromethane BQL 10.0 10 31212005 1,2-Dibromoethane (EDB) BQL 10.0 10 312/2005 1,2-Dichlorobenzene BQL 10.0 10 3/212005 1,3-Dichlorobenzene BQL . 10.0 10 3/2/2005 1,4-Dichlorobenzene BQL 10.0 10 3/212005 1,1-Dlchloroethane BQL 10.0 10.. 3/2/2005 1,2-Dichloroethane BQL 10.0 10 312/2005 M-Dichloroethene BQL 10.0 10 3/2/2005 cis-1,2-Dichloroethene 12.6 10.0 10 312/2005 trans-1,2-Dichloroethene BQL 10.0 10 31212005' i 1,2-Dichloropropane BQL 10.0 10 31212005 cis-1,3-Dichloropropene BQL 10.0 10 3/2/2005 trans-1,3-Dichloropropene BQL 10.0 10 312/2005 • Methylene Chloride BQL 50.0 10 3/212005 1,1,2,2-Tetrachloroeth3ne BQL 10.0 10 31212005 Tetrachloroethene BQL 10.0 10 31212005 1,1,1-Tdchloroethane BQL 10.0 .10 312/2005 1,1,2-Trichl6roethane BQL 10.0 10 3/2/2005 Trichloroethene 157 10.0 10 312/2005 Trichlorofluoromethane BQL 10.0 10 31212005 Vinyl Chloride BQL 10.0 10 3/212005 ' Surrogate Spike Recoveries Spike Spike Percent Added Result Recovery 1,4-Dichlorobutane 40 40.6 102. Comments: All values corrected for dilution. BQL = Below quantitation limit. Reviewed By:zLF 17 bf 39 N.C. Certification.4481 S.C. Certification #99029 PARADIGM ANALYTICAL LABURAI'URIES, INC. Results for Volatlles by GC 601 Client Sample ID: Influent Analyzed By: JTF Client Project ID: Toastmaster Laurinburg Date Collected: 2/22/2005 0:00 Lab Sample ID: G420-46-17A Date Received: 2/25/2005 ' Lab Project ID: G420-46 Matrix: Water Analyte B ro mod ichloromethan e Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chlomethane Chloroform Chloromethane Di bromo ch loromethane 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-D i chloroethen e trans-1,2-Dichloroethene 1,2-Dichloropropane ci s-1,3-Dichloropropene trans-1, 3-Dichloropropene Methylene Chloride 1,1,2,2-Tetrachloroelhane Tetrachloroethene 1,1,1-Trichloroethane 1,1,2-Tdchloroethane Trichloroethene Trichlorofluo rometha ne Vinyl Chloride Surrogate Spike Recoveries 1,4-Dichlorobutane Comments: All values corrected for dilution. BQL = Below quantitation limit. Result RL ugrL uglL Dilution Date Factor Analyzed BQL 25.0 25 3/212005 BQL 50.0 25 312/2005 BQL 25.0 25 312/2005 BQL 25.0 25 312/2005 BQL 25.0 25 312/2005 BQL 25.0 25 312/2005 BQL 25.0 25 3/2/2005 BQL 25.0 25 312/2005 BQL 25.0 25 3/2/2005 BQL 25.0 25 3/2/2005 BQL 25.0 25 3/2/2005 BQL 25.0 25 312/2005 BQL 25.0 25 312/2005 BQL 25.0 25 3/2/2005 BQL 25.0 25 3/212005 BQL 25.0 25 3/2/2005 BQL 25.0 25 3/2/2005 BQL 25.0 25 3/2/2005 BQL 25.0 25 3/2/2005 BQL 25.0 25 3/2/2005 BQL 25.0 25 3/2/2005 BQL 125 25 31212005 BQL 25.0 25 312/2005 BQL 25.0 25 3/212005 BQL 25.0 25 31212005 BQL 25.0 25 3/2/2005 374 25.0 25 312/2005 BQL 25.0 25 3/2/2005 BQL 25.0 25 312/2005 Spike Spike Percent Added Result Recovery 40 41.8 105 Reviewed By: 18 of 39 N.C. Certification #481 S.C. Certification #99029 YARA1111iM ANALY'11C:AL LA1fUKAIUKLL: i, 1NU. Results for Volatiles by GC 601 Client Sample ID: Effluent Analyzed By: DCS i Client Project ID:,Toastmaster Laurinburg Date Collected: 2122/2005 0:00 Lab Sample ID: G420=46-18A Date Received: 2/25/2005 Lab Project ID: G420-46 Matrix: Water I Analyte Result RL Dilution Data ug/L ug/L Factor Analyzed Bromodichloromethane BQL 1.00 1 3/112005 Bromoform BQL 2.00 1 3/112005 i Bromomethane BQL 1.00 1 811/2005 Carbon tetrachloride BQL 1.00 1 31112005 i Chlorobenzene BQL 1.00 1 3/1/2005 Chloroethane BQL 1.00 1. 3/1/2005 Chloroform BQL 1.00 1 311/2005 Chloromethane BQL 1.00 1' 311/2005 Dibromochloromethane BQL 1.00 1 311/2005 t 1,2-Dibromoethane (EDB) BQL 1.00 1 3/1/2005 1,2-Dichlorobenzene SQL. 1.00 1 3/1/2005 ' 1,3-Dichlorobenzene BQL 1.00 1 311/2005 { 1,4-Dichlorobenzene BQL 1.00 1 311/2005 1,1-Dichloroethane BQL 1.00 1 3/1/2005 ' 1,2-Dichloroethane BQL 1.00 1 3/1/2005 1,1-Dichloroethene BQL 1.00 1 3/1/2005 cis-1,2-Dichloroethene 2.54 1.00 1 3/1/2005. trans-1,2-Dichl6roethene BQL 1.00' 1 3/112005 1,2-Dichloropropane BQL 1.00 1 3/1/2005 cis-1,3-Dichloropropene BQL 1.00 1 3/1/2005 trans-1,3-Dichloropropene BQL 1.00 1 ' 3/1/2005 Methylene Chloride BQL 5.00 1 311/2005 1,1,2,2-Tetrachloroethane BQL 1.00 1 311/2005 Tetrachloroethene BQL 1.00 1 311/2005 1,1,1-Trichloroettiane BQL 1.00 1 _ 3/1/2005 1,1,2-Trichlorcethane BQL 1.00 1 3/1/2005 Trichloroethene 10.8 1.00 1 3/1/2005 Trichlorofluoromethane SQL, 1.00 1 311/2005 Vinyl Chloride BQL 1.00 1 3/1/2005 Surrogate Spike Recoveries Spike Spike" Percent Added' Result Recovery 1,4-Dichlorobutane 40 40.7 102 Comments: All values corrected for dilution. BQL = Below quantitation limit. Reviewed By:A 19 of 39 N.C. Certification #481 S.C. Certification #99029 PARADIGM ANALY'1'1GAL LABO.RAl'UH1LJ, 11V1;. Results for Inorganics Client Sample110: MN/-1 Analyzed By: RML . Client Project ID: Toastmaster Laurinburg- Date Collected: 02-22-2005 0:00 Lab Sample ID: G42046-1D Date Received: 02-25-2005 14:55 Lab Project ID: G42046 Matrix: Water Parameter Result Units Procedure Date Analyzed pH 5.77 S.U. 150.1 03-16-2005 12:24 Temperature 22.1 PC Comments: Samples analyzed out of 15 minute hold time. Reviewed By: PH_LIMS W.1 20 of 39 N.C. Certification #481 S.C. Certification #99029 PARADIGM ANALYTICAL LABORATORIES, INC. Results forinorganics i ' Client Sample ID: MW-2 Analyzed By: RML Client Project ID: Toastmaster Laurinburg Date Collected: 02-22-2005 0:00 Lab Sample ID: G420.46-2D Date Received: 02-25-2005 14:55 I Lab Project ID:' G42046 Matrix: Water I Parameter Result Units Procedure Date Analyzed f . pH 5.41 S.U. 150.1 03-1672005 12:26 Temperature 22.1 °C I l i i I I Comments: Samples analyzed out of 15 minute hold time. Reviewed By: 4e ' WLum w i Of 39 N.C. Certification #481 S.C. Certification #99029 YAHAll1G1V1 ALV ALY 111.AL LAIS V iCA1 V 1C11,' .7, u� a,: Results forinorganlcs Client Sample ID: MW-3 Analyzed By: RML Client Project ID: Toastmaster Laurinburg Date Collected: 02-22-2005 0:00 Lab Sample ID: G420-46-313 Date Received: 02-25-N05 14:55 . Lab Project ID: G420-46 Matrix: Water Parameter Result Units Procedure Date Analyzed pH 5.24 S.U. 150.1 03-16-2005 12:28 Temperature 22.1 °C Comments Samples analyzed out of 15 minute hold time. Reviewed By: pH_LIMS v L of 39 N.C. Certification #481 S.C. Certification #99029 FAKA11IUM AINALILIUAL JbAZVKa1V1c1rO, 1INt— Results for lnorganics Client Sample ID: MW-4 Analyzed By: RML Client Project ID: Toastmaster Laurinburg Date Collected: 02-22-2005 0:00 Lab Sample ID: G420-46-41) Date Received: 02-25-2005 14:55 Lab Project ID: G420-46 Matrix: Water Parameter Result Units Procedure . Date Analyzed pH 5.01 S.U. 150.1 03-16-2005.12:30 Temperature 22.1 °C Comments: Samples analyzed out of 15 minute hold time. Reviewed By: A off uMs w23 of 39 N.C. Certification #481 S.C. Certification #99029 YAKAlJ1G1V1 AIVALY 11l:AL LAIfVKA1VKIL'�h 11V 1.. Results for Inorganics; Client Sample ID: MW-5 Analyzed By: RML Client Project ID: Toastmaster Laurinburg Date Collected: 02-22-2005 0:00 Lab Sample ID: G420A6-5D Date Received: 02-25-2005 14:55 Lab Project ID: G420-46 Matrix: Water Parameter Result Units Procedure Date Analyzed pH 4.84 S.U. 150.1 ' 03-16-2005 12:32.' Temperature 22.1 °C Comments: Samples analyzed out of 15 minute hold time. Reviewed By:A—F nN uMs w.i 24'of.39 N.C. Certification #481 S.C. Certification #99029 YARA1111iM ANALILIUAL LAI5UKAIVKM3, llvl. Results for Inorganics Client Sample ID: MW-6 Analyzed By: RML - Client Project ID: Toastmaster Laurinburg Date Collected: 02-22-2005 0:00 Lab Sample ID: G420-46-61) Date Received: 02-25-2005 14:55 Lab Project ID: G42046 Matrix: Water Parameter Result Units Procedure Date Analyzed pH 5.02 S.U. 150A 03-16-2005 12:34 Temperature 22.2 °C Comments: Samples analyzed out of 15 minute hold time. Reviewed By: owums w25 of 39 N.C. Certification #481 S.C. Certification #99029 PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: MW-7 Client Project ID: Toastmaster Laurinburg Lab Sample ID: G420-46-7D Lab Project ID: G42046 Parameter Result Units pH 5.23 S.U. Temperature 22.1 °C Comments: Samples analyzed out of 15 minute hold time. Analyzed By: RML Date Collected: 02-22-2005 0:00 . Date Received: 02-25-2005 14:55 Matrix: Water Procedure Date Analyzed 150.1 03-16-2005 12:37 Reviewed By:/ off uMs w26 of 39 N.C. Certification #481 S.C. Certification #99029 PARADIGM ANALY'1'1CAL LAISUKAlUK1EN, 11VC. Results for Inorganics Client Sample ID: MW-9 Analyzed By: RML Client Project ID: Toastmaster Laurinburg Date Collected: 02-22-2005 0:00 Lab Sample ID: G420-46-BD Date Received: 02-25-2005 14:55 Lab Project ID: G420-46 Matrix: Water. Parameter Result Units Procedure Date . Analyzed I pH 4.88 S.U. 150.1 03-16-2005 12:39 Temperature 22.1 °C t . i Comments: Samples analyzed out of 15 minute hold time. Reviewed By:/ cN_uns w27 of 39 1. N.C. Certification #481 S.C. Certification #99029 PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: MW-10 Analyzed By: RML Client Project ID: Toastmaster Laurinburg Date Collected: 02-22-2005 0:00 Lab Sample ID: G420-46-9D. Date Received: 02-25-2005 14:55 Lab Project ID: G420-46 Matrix: Water Parameter Result Units Procedure Date Analyzed . pH 4.31 S.U. 150.1 03-16-200512:42 Temperature 22.1 °C Comments: Samples analyzed out of 15 minute hold time. 7 Reviewed By:� vH ums_w i 28 of 39 N.C. Certification 4481 S.C. Certification #99029 lAl\AL1Ul1l Aa�[aL.a aavaau uaarv�u� a.....� .. �• Results for Inorganics . Client Sample ID: MWA1 Analyzed By: RML Client. Project ID: Toastmaster Laurinburg Date Collected: 02-22-2005 0:00 Lab Sample ID: G420-46-100 Date Received: 02-25-2005 14:55 Lab Project ID: G42046 Matrix: Water Parameter Result' Units Procedure Date Analyzed pH 4.95 S.U. 150.1 03-16-200512:44 Temperature 22.1 °C Comments: Samples analyzed out of 15 minute hold time. Reviewed By: v taus w29 of 39 N.C. Certification #481 S.C. Certification #99029 . rAl�tlLl VlYl ALYAlJl 11\iAL uC\u VI\!>1Vl\luV� 11\a... Results for Inorganics Client Sample ID: MWA2 Analyzed By: RML Client Project ID: Toastmaster Laurinburg Date Collected: 02-22-2005 0:00 Lab Sample ID: G42046-11D Date Received: 02-25-2005 14:55 Lab Project ID: G420-46 Matrix: Water Parameter Result Units Procedure Date pH 5.08 S.U. Temperature 22.2 °C Comments: Samples analyzed out of 15 minute hold time. n Analyzed 150.1 03-16-2005 12:46 .Reviewed By: aH uW w.i 30 of 39 N.C. Certification #481. S.C. Certification #99029 YAKAL1lr1V1 AIVALI 11l.AL LADVl[A1V1C1L"Op 11V 1.. Results for Inorganics Client Sample ID: MWA3 Analyzed By: RML Client Project ID: Toastmaster Laurinburg Date Collecte& 02-22-2005 0:00 Lab Sample ID: G42046-12D Date Received: 02-25-2005 14:55 Lab Project ID: G420-46 Matrix: Water ' Parameter Result Units Procedure Date Analyzed pH 5.39 S.U. 150.1 03-16-200512:49 Temperature 22.1 °C Comments: Samples analyzed out of 15 minute hold time. Reviewed By: AF- PxLums w31 of 39 N.C. Certification #481 S.C. Certification #99029 Results for Inorganics Client Sample ID. MW-14. Client Project ID: Toastmaster Laudnburg Lab Sample ID: G42046-13D Lab Project ID:"G420-46 Parameter Result pH 5.56 Temperature 22.2 Analyzed By: RML Date Collected: 02-22-2005 0:00 Date Received: 02-25-2005 14:55 Matrix: Water Units Procedure Date Analyzed S.U. 150.1 03-16-2005 12:50 °C Comments: Samples analyzed out of 15 minute hold time. Reviewed By: O ums w32 of 39 IN.C. Certification #481 S.C. Certification #99029 'YAHAL1l31V1 A1VAL111l.AL 11V1.. Results for Inorganics Client Sample ID: RW-1 Analyzed By: RML Client Project ID: Toastmaster Laurinburg Date Collected: 02-22-2005 0:00 Lab Sample ID: G426-46-14D Date Received: 02-25-2005 14:55 Lab Project ID: G420-46 Matrix: Water Parameter Result Units Procedure Date ' Analyzed pH 5.35 S.U. 150.1 03-16-2005 12:52 Temperature 22.2 °C Comments: Samples analyzed out of 15 minute hold time. - Reviewed By: cH uMs w33 of 39 N.C. Certification #481 S.C. Certification #99029 PARADIGM ANALY 11CAL LA1fUKALUK1LJ, 11V — Results for Inorganics Client Sample ID: RW-2 Analyzed By: RML Client Project ID: Toastmaster Laurinburg Date Collected: 02-22-2005 0:00 Lab Sample ID: G420-46-15D Date Received: 02-25-2005 14:55 . Lab Project ID: G420-46 ° Matrix: Water Parameter Result Units Procedure Date Analyzed pH 5.53 S.U. ' 160.1 03-16-2005 12:54 Temperature 22.2 °C Comments: Samples analyzed out of 15 minute hold time. . Reviewed By: ox un+s 0 34 of 39 N.C. Certification #481 S.C. Certification #99029. rHi(L1L11z1Y1 Al`IL1La lal.[1L 1JALva\[1a va�aL' U� at. v. Results for Inorganics Client Sample'ID: Influent Analyzed By: RML Client Project ID: Toastmaster Laurinburg Date Collected:.02-22-2005 0:00 Lab Sample ID: G420-46-17D Date Received: 02-25-2005 14:55 Lab Project ID: G420-46 Matrix: Water Parameter Result Units Procedure Date Analyzed pH 5.22 S.U. 150.1. .03-16-2005 12:56 Temperature 22.2 °c Comments: Samples analyzed out of 15 minute hold time. Reviewed By: pH ❑MS 01 35 of 39 N.C. Certification #481 S.C. Certification #99029 YAKAD16M ANALY11l:AL LAIfVKA1VKIEn, 11V1.. Results for Inorganics Client Sample ID: Effluent Analyzed By: RML Client Project ID: Toastmaster Laurinburg Date Collected: 02-22-2005 0:00 Lab Sample ID: G420-46-16D Date Received: 02-25-2005 14:55 Lab Project ID: G420-46 Matrix: Water l Parameter Result Units Procedure Date pH 6.06 Temperature 22.3 Analyzed S.U. 150.1 03-16-2005 12:59 "C Comments: Samples analyzed out of 15 minute hold time. Reviewed By:,k pN UMS O 1 36 of 39 N.C. Certification #481 S.C. Certification #99029 YAHAUIUM ALIALIL111AL Ll' .. List of Reporting Abbreviations. and Data Qualifiers B = Compound also detected in batch blank BQL = Below Quantitalion Limit DF = Dilution Factor Dup = Duplicate E= Estimated concentration, exceeds calibration range. J = Estimated concentration; below calibration range and above MDL LCS(D) = Laboratory Control Spike (Duplicate) MDL = Method Detection Limit i MS(D) = Matrix Spike (Duplicate) PQL = Practical Quantitation Limit RL = Reporting Limit RPD = Relative Percent Difference mg/kg = milligram per kilogram, ppm, parts per million uglkg = micrograms per kilogram, ppb, parts per billion mglL = milligram per liter, ppm, parts per million ug/L = micrograms per liter, ppb, parts per billion % Rec = Percent Recovery solids = Percent Solids Special Notes: 1) Metals and mercury samples are digested with a hot block, see the standard operating procedure document for details. 2) Uncertainty for all reported data is less than or equal to 30 percent. M134:011404.1 37 of 39 N.C. Certification #481 S.C. Certification #99029 ANALYTICAL LABORATORIES, INC. 5500 Business Drive, Wilmington, NC 28405 Phone:(910)-350-1903 FAX:(910)-350-1557 Client: 164A" Ari0- (?4_Wk+ Address: It ( N SwJAZLn� Address: 6i1044A- TA 0 Quote #: Chain -of Custody Record & Analytical Request )Wject ID:1 W C AhM LA Contact: IL 5 44'17hu-sIr Phone�LsLL�_ Fax: cou 44115 Page —t of Report To: A Turnaround: 4mohdovf Job Number: P.O. Number: Invoice To: Lm— •e 1 • •.:- ru it 1 ' I: M I 1 I l l 1 1 ■■■�■ ■■■■ �i■��■■■■■■■ • 4 1 1 1 1 : m 111 • LYG 1 : � 11 11 1.. 11 .: 11 ✓. A 1 1 • 1 :. 1 10, I I ! Vnll PARADIGM ANALYTICAL LABORATORIES, INC. 5500 Business Drive, Wilmington, NC 28405 Chain -of Custody Record & Analytical Request Phone:(910)-350-1903 FAX:(910)-350-1557 Client: �,' cs i ;.Project ID: 1�41�r� Address:_I"(-�Wi(MM Or Contact: RS Li�� Address: Phon nnnte # Fan• cou 4411-4 . Page —2�— of i �Aate: z Ys Report To: ' � � IM► aft' Turnaround: L-Amy CJAt Job Number: P.O. Number.Invoice To: —� G 14 k .III 1 II I 1 II 1 nl . :I LII WII � 1 s - ■■■■ n■n■■■■■■■ .� 1■®1®■■■■ 11■11■■■■■■■ r wompl ■■■■ l l■l mom mom Nor -IF", 1 1 I :1 : III I Y' :1 :® 11 1 I 1' : I I 1 I. 11I ✓. 1 1 I 1 1 :� 1 /m 'IINI:.�I 00 0 U I i