WQ0004972_Monitoring - 03-2024_20240430 (3)

Monitoring Report Submittal
...................................................
Permit Number#* WQ0004972
Name of Facility:*
Month: * March
Forest Lake WWTP
Report Information
Type *
NDMR, NDAR-1, NDAR-2, NDMLR
Confirmation Email Address: *
Name of Submitter: *
Signature:
Date of submittal:
Initial Review
Year:* 2024
Upload Document*
2024_March_Forest_Lake_WQ0004972_Monthly 1.55MB
Report Complete.pdf
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59).
[e-mail]
Amanda Grenier
OAOW-� (It W;! 't
Reviewer: Wanda.Gerald
4/30/2024
This will be filled in automatically

Is the project number correct?* WQ0004972
Is the monitoring report accepted?* Yes No
Regional Office* Winston-Salem
Reviewer: _anonymous
Review Date: 5/20/2024

DocuSign Envelope ID: 99C20C46-ODOA-4BA3-A604-6EC8304FBFA1 NON -DISCHARGE APPLICATION REPORT (NDAR-1)
Page of
Permit No.: WQ0004972
Facility Name: Forest Lake
County: Davie
Month: March
Year: 2024
Did irrigation
Field Name:
Field Name:
Field Name:
Field Name:
occur
Area (acres):
6
Area (acres):
Area (acres):
Area (acres):
at this facility?
Cover Crop:Grass/Trees
Cover Crop:
p�
Cover Crop:
p�
Cover Crop:
p:
Hourly Rate (in):
0.11
Hourly Rate (in):
Hourly Rate (in):
Hourly Rate (in):
Annual Rate (in):
46.8
Annual Rate (in):
Annual Rate (in):
Annual Rate (in):
Weather
Freeboard
Field Irrigated?
Field Irrigated?
Field Irrigated?
Field Irrigated?
p
m
-o
o
°CL
4
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2
E 2
i
Ea
~ '
a
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Ev
L'
xt
OE
J
2
°F
in
ft
ft
gal
min
in
in
gal
min
in
in
gal
min
in
in
gal
min
in
in
1
CL
46
0
4'
2
CL
66
0
3
CL
66
0
4
CL
67
1"
3'
5
PC
69
0
2.8'
39,399
240
0.24
.06
6
R
59
.36"
3.4'
7
CL
68
0
3'
8
CL
61
0
2.8'
40,620
240
0.25
0.06
9
CL
53
0
10
CL
51
0
11
C
61
1"
2.7'
12
C
70
0
2.5'
40,916
300
0.25
0.05
13
C
75
0
3.3'
14
C
78
0
3.1'
36,233
240
0.22
0.06
15
CL
66
0
4.1'
16
C
69
0
17
CL
71
0
18
C
60
0
3'
19
C
54
0
2.8'
20
C
71
0
2.5'
21
C
64
0
2.3'
46,198
300
0.28
0.06
22
CL
60
0
3.3'
26,775
180
0.16
0.05
23
R
60
0
24
C
54
0.86
25
C
58
1"
3'
26
CL
54
0"
2.8'
53,008
300
0.33
0.07
27
R
52
0
4'
28
CL
65
.5"
3.8'
29
C
69
0
30
PC
74
0
311
PC
1 81
1 0
Monthly Loading:
283,149
1.74
0
0.00
0
0.00
0
0.00
onth Floating Total (in):
23.46
Sam Perry (Apr30, 202)r16:36 EDT)

DocuSign Envelope ID: 99C2OC46-ODOA-4BA3-A604-6EC8304FBFA1 NON -DISCHARGE APPLICATION REPORT (NDAR-1)
Did the application rates exceed the limits in Attachment B of your permit?
Page of
O Compliant ❑ Non -Compliant
Were adequate measures taken to prevent effluent ponding in or runoff from the sites? O Compliant ❑ Non -Compliant
Was a suitable vegetative cover maintained on all sites as specified in your permit? O Compliant ❑ Non -Compliant
Were all setbacks listed in your permit maintained for every application to each permitted site? O Compliant ❑ Non -Compliant
Were all freeboards maintained in accordance with the specified freeboard heights in your permit? O Compliant ❑ Non -Compliant
If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective
action(s) taken. Attach additional sheets if necessary.
Operator in Responsible Charge (ORC) Certification
Permittee Certification
ORC: Sam Perry
Permittee:
MHC TT, LP
Certification No.: 1014038
Signing Official: George Gudgeon
Grade: SI Phone Number: 919-548-2381
Signing Officials Title: Sr. Vice President
Has the ORC changed since the previous NDAR-1?
Phone Number: 312-279-1400 Permit Exp.: 10/31 /27
hl TeLr4 4/30/24
4/30/2024
Signature Date
Signature Date
By this signature, I certify that this report is accurrate and complete to the best of my knowledge.
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
Mail Original and Two Copies to:
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
M

p2np of
DocuSign Envelope ID: 99C20C46-ODOA-4BA3-A604-6EC8304FBFA1 NON -DISCHARGE MONITORING REPORT NDMR
Permit No.: WQ0004972
Facility Name: Forest Lake Preserve ELS
County: Davie
Month: March
Year: 2024
PPI: 001
Flow Measuring Point:
Parameter Monitoring Point:
Parameter Code
50050
00400
50060
70300
00530
00310
31616
00600
00610
00625
00630
00620
00615
00665
00940
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24-hr
hrs
GPD
su
mg/L
mg/L
mg/L
mg/L
#/100 mL
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
1
08:00
5
31,940
7.12
1.2
2
53,176
3
33,850
4
08:00
5
35,926
6.37
0.2
5
08:00
5
34,319
7.22
1.7
6
08:00
5
33,867
7.25
0.8
7
08:00
5
55,983
6.91
1.7
8
8:00
5
39,975
6.63
1.6
9
46,623
10
74,273
11
08:00
5
42,457
6.04
0.4
12
08:00
5
40,375
6.27
0.8
13
08:00
5
40,633
6.9
1.7
255
3.4
2
1
18.3
12.2
14.3
4
4
<0.02
5.8
62.5
14
08:00
5
40,429
7.15
2.1
15
08:00
5
22,235
7.04
1.4
16
34,459
17
27,012
18
08:00
5
29,972
7.13
0.04
19
08:00
5
23,703
7.05
0.08
20
08:00
5
22,781
7.07
0.06
21
08:00
5
25,746
6.29
0.8
22
08:00
5
25,549
6.43
1.2
23
42,634
24
29,939
25
08:00
5
32,620
6.33
0.2
26
08:00
5
26,632
6.14
0.6
27
08:00
5
27,778
6.35
0.8
28
08:00
5
52,854
6.48
0.8
29
38,500
30
29,855
311
1
32,419
Average:
36,404
0.91
255.00
3.40
2.00
1.00
18.30
12.20
14.30
4.00
4.00
0.00
5.80
62.50
Daily Maximum:
74,273
7.25
2.10
255.00
3.40
2.00
1.00
18.30
12.20
14.30
4.00
4.00
0.02
5.80
62.50
Daily Minimum:
22,235
6.04
0.04
255.00
3.40
2.00
1.00
18.30
12.20
14.30
4.00
4.00
0.02
5.80
62.50
Sampling Type:
Monthly Avg. Limit:
Daily Limit:
Sample Frequency:
Continuous
5x/Week
5)(/Week
Monthly
Monthly
Monthly
Monthly
Monthly
Monthly
Monthly
Monthly
Monthly
Monthly
Monthly
3X/year

DocuSign Envelope ID: 99C2OC46-ODOA-4BA3-A604-6EC8304FBFA1
Sampling Person(s)
Certified Laboratories
Name: Sam Perry
Name:
Name: Greener EHS Solutions, LLC
Name: Pace Analytical
Does all monitoring data and sampling frequencies meet the requirements in Attachment A of your permit? ❑ Compliant O Non -Compliant
If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective
action(s) taken. Attach additional sheets if necessary.
The Monthly average flow exceeded the permitted flow of 24,400 gpd. The permitted application rate was not exceeded. The flow meter was calibrated on June 27, 2023 and the meter was reading significantly
low before the calibration. This was noted on the June 2023 NDMR. The plant is in the process of an upgrade to increase the capacity as well as investigating extraneous flow for 1/1 and leaking fixtures. Lab
Qualifiers, 3/13/24 - Phosphorus, chloride and TKN, M1 - Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
Operator in Responsible Charge (ORC) Certification
Permittee Certification
ORC: Sam Perry
Permittee: MHC TT, LP
Certification No.: 1014038
Signing Official: George Gudgeon
Grade: SI Phone Number: 919-548-2381
Signing Officials Title: Sr. Vice President
Has the ORC changed since the previous NDMR? El Yes O No
Phone Number: 312-279-1400 Permit Expiration: 10/31/2027
Saw Tetlt�
4/30/2024 1 9
4/30/24
-
Sam Perry (Apr30, 202 16:36 EDT)
Signature Date
Signature Date
By this signature, I certify that this report is accurrate and complete to the best of my knowledge.
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information
submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
Mail Original and Two Copies to:
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
53 .

DocuSign Envelope ID: 99C2OC46-ODOA-4BA3-A604-6EC8304FBFA1
aceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
March 27, 2024
Amanda D. Grenier
Greener EHS Solutions
21 Selby Ct.
Holly Springs, NC 27540
RE: Project: Forest Lake -March
Pace Project No.: 92718818
Dear Amanda Grenier:
Enclosed are the analytical results for sample(s) received by the laboratory on March 13, 2024. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
704-977-0942
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 18

DocuSign Envelope ID: 99C2OC46-ODOA-4BA3-A604-6EC8304FBFA1
aceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Forest Lake -March
Pace Project No.: 92718818
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
VirginiaNELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 18

DocuSign Envelope ID: 99C2OC46-ODOA-4BA3-A604-6EC8304FBFA1 Pace Analytical Services, LLC
�aceo 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Forest Lake -March
Pace Project No.: 92718818
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92718818001 Greener EHS Effluent
SM 9222D-2015
KDF
1
PASI-C
SM 2540C-2015
JMH1
1
PASI-A
SM 2540D-2015
JAY
1
PASI-A
SM 521OB-2016
MDM
1
PASI-A
TKN+NO3+NO2 Calculation
MJP
1
PASI-A
EPA 350.1 Rev 2.0 1993
NCF
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 365.1 Rev 2.0 1993
Zip
1
PASI-A
SM 4500-CI-E-2011
MMA
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 18

DocuSign Envelope ID: 99C2OC46-ODOA-4BA3-A604-6EC8304FBFA1
aceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Forest Lake -March
Pace Project No.: 92718818
Sample: Greener EHS Effluent Lab ID: 92718818001 Collected: 03/13/24 12:00 Received: 03/13/24 13:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Charlotte
Fecal Coliforms
1.0 CFU/100 mL 1.0
1
03/13/24 17:13 03/14/24 15:20
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2015
Pace Analytical Services -Asheville
Total Dissolved Solids
255 mg/L 25.0
1
03/16/24 13:34
2540D Total Suspended Solids
Analytical Method: SM 2540D-2015
Pace Analytical Services -Asheville
Total Suspended Solids
3.4 mg/L 2.5
1
03/19/24 11:57
5210B BOD, 5 day
Analytical Method: SM 521OB-2016
Pace Analytical Services -Asheville
BOD, 5 day
2.0 mg/L 2.0
1
03/15/24 06:10 03/20/24 02:51
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Pace Analytical Services -Asheville
Total Nitrogen
18.3 mg/L 0.040
1
03/27/24 10:25
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
12.2 mg/L 0.30
3
03/22/24 18:00 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation
Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Kjeldahl, Total
14.3 mg/L 0.50
1
03/26/24 19:28 03/27/24 06:48 7727-37-9
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
4.0 mg/L 0.020
1
03/14/24 02:00 14797-55-8
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation
Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
5.8 mg/L 0.10
2
03/26/2414:31 03/27/2413:28 7723-14-0
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride
62.5 mg/L 2.0
2
03/22/24 21:25 16887-00-6
Date: 03/27/2024 04:14 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
M1
Page 4 of 18

DocuSign Envelope ID: 99C2OC46-ODOA-4BA3-A604-6EC8304FBFA1 Pace Analytical Services, LLC
�aceo 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Forest Lake -March
Pace Project No.: 92718818
QC Batch: 838808 Analysis Method: SM 9222D-2015
QC Batch Method: SM 9222D-2015 Analysis Description: 9222D Fecal Coliform(MF) - CHT
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92718818001
METHOD BLANK: 4332967 Matrix: Water
Associated Lab Samples: 92718818001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms CFU/100 mL ND 1.0 03/14/24 15:20
SAMPLE DUPLICATE: 4332968
Parameter
Fecal Coliforms
92718697001 Dup
Units Result Result RPD Qualifiers
CFU/100 mL ND ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2024 04:14 PM without the written consent of Pace Analytical Services, LLC.
Page 5 of 18

DocuSign Envelope ID: 99C2OC46-ODOA-4BA3-A604-6EC8304FBFA1 Pace Analytical Services, LLC
�aceo 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Forest Lake -March
Pace Project No.: 92718818
QC Batch: 839545 Analysis Method: SM 2540C-2015
QC Batch Method: SM 2540C-2015 Analysis Description: 2540C Total Dissolved Solids
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92718818001
METHOD BLANK: 4336953
Associated Lab Samples: 92718818001
Parameter
Units
Total Dissolved Solids
mg/L
LABORATORY CONTROL SAMPLE:
4336954
Parameter
Units
Total Dissolved Solids
mg/L
SAMPLE DUPLICATE: 4336955
Parameter
Units
Total Dissolved Solids
mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 25.0 03/16/2413:33
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 266 106 90-110
92719223001 Dup
Result Result RPD Qualifiers
139 139 0
SAMPLE DUPLICATE: 4336956
92718853002 Dup
Parameter Units Result Result
Total Dissolved Solids mg/L 1470 1440
RPD Qualifiers
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2024 04:14 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 18

DocuSign Envelope ID: 99C2OC46-ODOA-4BA3-A604-6EC8304FBFA1 Pace Analytical Services, LLC
�aceo 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Forest Lake -March
Pace Project No.: 92718818
QC Batch: 839967 Analysis Method: SM 2540D-2015
QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92718818001
METHOD BLANK: 4338420
Associated Lab Samples: 92718818001
Parameter
Units
Total Suspended Solids
mg/L
LABORATORY CONTROL SAMPLE:
4338421
Parameter
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 4338791
Parameter
Units
Total Suspended Solids
mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 03/19/2411:52
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 244 98 90-110
92718799001 Dup
Result Result RPD Qualifiers
3580 3520 1
SAMPLE DUPLICATE: 4338792
92718861001 Dup
Parameter Units Result Result
Total Suspended Solids mg/L 376 412
RPD Qualifiers
9
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2024 04:14 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 18

DocuSign Envelope ID: 99C2OC46-ODOA-4BA3-A604-6EC8304FBFA1 Pace Analytical Services, LLC
�aceo 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Forest Lake -March
Pace Project No.: 92718818
QC Batch: 839193 Analysis Method: SM 521 OB-2016
QC Batch Method: SM 521OB-2016 Analysis Description: 5210E BOD, 5 day
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92718818001
METHOD BLANK: 4335001
Associated Lab Samples: 92718818001
Parameter Units
BOD, 5 day mg/L
LABORATORY CONTROL SAMPLE: 4335003
Parameter Units
BOD, 5 day mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 03/20/24 04:11
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
198 199 101 84.6-115
SAMPLE DUPLICATE: 4335004
92719058002 Dup
Parameter Units Result Result
BOD, 5 day mg/L ND ND
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2024 04:14 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 18

DocuSign Envelope ID: 99C2OC46-ODOA-4BA3-A604-6EC8304FBFA1 Pace Analytical Services, LLC
�aceo 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Forest Lake -March
Pace Project No.: 92718818
QC Batch: 840810 Analysis Method: EPA 350.1 Rev 2.0 1993
QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92718818001
METHOD BLANK: 4342688
Associated Lab Samples: 92718818001
Parameter Units
Nitrogen, Ammonia mg/L
LABORATORY CONTROL SAMPLE: 4342689
Parameter Units
Nitrogen, Ammonia mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.10 03/22/24 15:57
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
5 5.1 103 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4342690 4342691
MS MSD
92718779003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/L 0.053J 5 5 5.2 5.2 103 103 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4342692 4342693
MS MSD
92718779004 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/L 4.0 5 5 8.9 8.8 97 97 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2024 04:14 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 18

DocuSign Envelope ID: 99C2OC46-ODOA-4BA3-A604-6EC8304FBFA1 Pace Analytical Services, LLC
�aceo 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Forest Lake -March
Pace Project No.: 92718818
QC Batch: 841567 Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92718818001
METHOD BLANK: 4346603
Associated Lab Samples: 92718818001
Parameter Units
Nitrogen, Kjeldahl, Total mg/L
LABORATORY CONTROL SAMPLE: 4346604
Parameter Units
Nitrogen, Kjeldahl, Total mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.50 03/27/24 06:23
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
10 10.2 102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4346605 4346606
MS MSD
92718723001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mg/L 39.0 10 10 50.6 51.9 116 129 90-110 3 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2024 04:14 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 18

DocuSign Envelope ID: 99C2OC46-ODOA-4BA3-A604-6EC8304FBFA1 Pace Analytical Services, LLC
�aceo 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Forest Lake -March
Pace Project No.: 92718818
QC Batch: 838846 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92718818001
METHOD BLANK: 4333247
Associated Lab Samples: 92718818001
Parameter Units
Nitrogen, Nitrate mg/L
LABORATORY CONTROL SAMPLE: 4333248
Parameter Units
Nitrogen, Nitrate mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.020 03/14/24 01:44
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
1.5 1.6 106 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4333249 4333250
MS MSD
92718645002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Nitrate mg/L 8.0 1.5 1.5 9.6 9.6 107 111 90-110 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2024 04:14 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 18

DocuSign Envelope ID: 99C2OC46-ODOA-4BA3-A604-6EC8304FBFA1 Pace Analytical Services, LLC
�aceo 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Forest Lake -March
Pace Project No.: 92718818
QC Batch: 841618 Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92718818001
METHOD BLANK: 4346933
Associated Lab Samples: 92718818001
Parameter Units
Phosphorus mg/L
LABORATORY CONTROL SAMPLE: 4346934
Parameter Units
Phosphorus mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.050 03/27/24 10:32
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
2.5 2.5 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4346935 4346936
MS MSD
92718818001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/L 5.8 2.5 2.5 8.1 8.0 90 88 90-110 1 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4346937 4346938
MS MSD
92718838001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/L ND 2.5 2.5 2.5 2.5 100 99 90-110 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2024 04:14 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 18

DocuSign Envelope ID: 99C2OC46-ODOA-4BA3-A604-6EC8304FBFA1 Pace Analytical Services, LLC
�aceo 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Forest Lake -March
Pace Project No.: 92718818
QC Batch: 841264 Analysis Method: SM 4500-CI-E-2011
QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92718818001
METHOD BLANK: 4345359
Associated Lab Samples: 92718818001
Parameter Units
Chloride mg/L
LABORATORY CONTROL SAMPLE: 4345360
Parameter Units
Chloride mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 1.0 03/22/24 21:06
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
20 20.7 104 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4345361 4345362
MS MSD
92719121001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chloride mg/L 18.9 10 10 30.2 30.2 113 113 90-110 0 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2024 04:14 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 18

DocuSign Envelope ID: 99C2OC46-ODOA-4BA3-A604-6EC8304FBFA1
aceo
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: Forest Lake -March
Pace Project No.: 92718818
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2024 04:14 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 18

DocuSign Envelope ID: 99C2OC46-ODOA-4BA3-A604-6EC8304FBFA1 Pace Analytical Services, LLC
�aceo 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Forest Lake -March
92718818
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92718818001
Greener EHS Effluent
SM 9222D-2015
838808
SM 9222D-2015
838809
92718818001
Greener EHS Effluent
SM 254OC-2015
839545
92718818001
Greener EHS Effluent
SM 2540D-2015
839967
92718818001
Greener EHS Effluent
SM 521OB-2016
839193
SM 521OB-2016
839225
92718818001
Greener EHS Effluent
TKN+NO3+NO2
842097
Calculation
92718818001
Greener EHS Effluent
EPA 350.1 Rev 2.0 1993
840810
92718818001
Greener EHS Effluent
EPA 351.2 Rev 2.0 1993
841567
EPA 351.2 Rev 2.0 1993
842023
92718818001
Greener EHS Effluent
EPA 353.2 Rev 2.0 1993
838846
92718818001
Greener EHS Effluent
EPA 365.1 Rev 2.0 1993
841618
EPA 365.1 Rev 2.0 1993
841919
92718818001
Greener EHS Effluent
SM 4500-CI-E-2011
841264
Date: 03/27/2024 04:14 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 18

--9 I r,r.a 'r;&I—. 17AI%1 CMRA ur 1A14 nn" ..n3 Sample Condition Upon Receipt
DocuSign Envelope ID: 99C2OC46-ODOA-4BA3-A604-6EC8304FBFA1 —
rdcc
Effective Date: 11/29/2023 4:16:30 PM
Laboratory receiving samples:
Asheville ❑ Eden] Greenwood ❑ Huntersville ED,' Raleigh[] Mechanicsville❑ Atlanta❑ KernPrcuill .71
Sample Condition Client Name:6" ywU-�'� ltsUpon Receipt S�'t� nD -1 Project #: ' WO • 92718818
Courier. Fe Ex ups USPS Client II I II' I II' I II I IIII I III
❑ Commercial ace El other: 92718818
I
Custody Seal Present? Elles ❑ No Seals Intact? ❑Yes ❑ No ❑ N/A
Date/Initials Person Examining Contents:
Packing Material: ❑Bubble Wrap ❑ Bubble Bags ❑ None ❑ Other Biological Tissue Frozen?
Thermom ter: CG� ���� ❑ Yes ❑ No ❑ N/A
IR Gun ID: L) Type of Ice: ddWet ❑Blue ❑None
Correction Factor:
Cooler Temp: I Add/Subtract (°C) Temp should be above freezing to 6°C
❑ Samples out of temp criteria. Samples on ice, cooling process
Cooler Temp Corrected (°C): 3 has begun
USDA Regulated Soil (❑ N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC Did samples originate from a foreign source (internationally,
frhar4 -.17 M V.. N., includine Hawaii and Puerto Ricol? ❑ Yes ❑ No
Comments/Discrepancy:
Chain of Custody Present?
Yes
❑ No
] N/A
1.
Samples Arrived within Hold Time?
© es
❑ No
❑ N/A
2.
Short Hold rime Analysis (<72 hr.)?
❑ Yes
No,
❑ N/A
3.
Rush Turn Around Time Requested?
❑ Yes
6No
❑ N/A
4.
Sufficient Volume?
Yes
❑ No
❑ N/A
S.
Correct Containers Used?
-Pace Containers Used?
8XeS
I]Yes
❑ No
❑ No
❑ N/A
❑ N/A
6.
Containers Intact?
LJ Yes
❑ No
❑ N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
❑No
N/A
8.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
}} Yes
(" 1
❑ No
❑ N/A
9.
Headspace in VOA Vials (>5-6mm)?
❑ Yes
❑ N/A
10.
Trip Blank Present?
TripBlank Custody Seals Present?
❑Yes
❑ Yes
,--,No
Wo
❑ N/A
❑ N/A
11.
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Lot ID of split containers:
Date/Time:
Date:
Date:
Field Data Required? U Yes LJ No
Qualtrax ID: 69614 Paae 1 of 2 Page 16 of 18

vvrr r ruc. L-11 V Fr vvoJ vvc_oa►nNtC a,vnUrtrUn VNUn rCeIL-etpt
DocuSign Envelope ID: 99C2OC46-ODOA-4BA3-A604-6EC8304FBFA1
I I -
Effective Date: 11/14/2022
"Check mark top half of box if PH and/or dechlorination is verified and
within the acceptance range for preservation samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC. LLHS
"Bottom half of box is to list number of bottles
***Check all unpreserved Nitrates for chlorine
Project 4
TWO.#_:92718818
PM: MWB Due Date: 03/27/24
CLIENT: 92—Greener
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot 4
Note: Whenever there rs a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DENR Certification Office. (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Qualtrax ID: 69614 Page 2 of 2
Page 17 of 18

Pace" Location Requested (City/State):
LAB USE ONLY- Affix WorkordorlLogin Label Here
Pace Analytical Charlotte CHAIN -OF -CUSTODY Analytical Request Document
(--P'ace 9800 Kincey Ave. Suite 100, Huntersville, NC 28078 Chain -of -Custody is a LEGAL DOCUMENT -Complete all relevant fields
O F"
N 4 `
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Company Name: Greener EHS Solutions
Contact/Report To: Amanda Grenier
Street Address: 192 Thousand Trail Dr., Advance, NC 27006
Phone N: [phone]:'.f'¢.
. r 1r
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E-Mail:
� Scan OR Code for instructions a
Cc E-Mail:
Customer Project A:
----- '-'--_ .- —- --— _.,._ —.
Specify Container Size "
site: (1) si(1) 1L. (z) 500mL, 1312somL, (4)
�. .- -- ---- Project Name: Forest Lake- March
Invoice To: _
TerraCore, (9) 90,1(1d101her
Invoice E-Mail:
Identify Container Preservative Type'^
••• Pre —al— Types: (1) None, Iz) HNO3, 131
Site Collection Info/Facility ID (as applicable):
Purchase Order H (if
H2SO4, (4) IICL (5) NaDH, (6) Zn Acetate, (7)
applicable):
NalIS04. (8) Sod. Thiosulfate, (9) Ascorblc Aod, 110)
Analysis Requested
r&CH, (11) other
Quote tt:
Pro. Mgr:
Matthew Brainard
Time Zone Collected: ( ) AK [ ] PT [ J MT [ J CT [ ) ET
iCounty / State origin of sample(s): North Carolina
Data Deliverables:
Regulatory Program (DW, RCRA, etc.) as applicable: Reportable [ I Yes [ ] No
AcctNum / Client ID:
Level II [ J Level III [ J level IV
LL
Rush (Pre -approval required):
DW PWSIO l or WW Permit n as applicable.
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Profile/Template:
6 E
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Requested:
Analysis:
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14849_8
' Matrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Waste Water (W W), Product (P), Soil/Solid (55), OilE
(OL), Wipe (WP), Tissue ITS), Bioassay
Prelog /Bottle Ord. ID:
B , Vapor IV), Surface Water SW ,Sediment SED , Sludge SL , Caulk CK , Leachate LL , Biosolid BS , Other OT
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a Coolers: Tl a momeler ID: Correction Factor VC): Obs, Temp. ('Cl Corrected Temp. ('Cl On Ice:
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