Loading...
HomeMy WebLinkAboutWQ0013263_Application_20240516Initial Review Reviewer nathaniel.thorn burg Is this submittal an application? (Excluding additional information.) * Yes No Permit Number (IR) * WQ0013263 Applicant/Permittee Town Of Boone Applicant/Permittee Address PO Box 192 Boone, NC 28607 Is the owner in BIMS? Yes ) No Is the facility in BIMS? Owner Type Facility Name County Fee Category Minor Is this a complete application?* Yes No Signature Authority Signature Authority Title Signature Authority Email Document Type (if non -application) Email Notifications Municipal Town of Boone Class A Residuals Program Watauga Does this need review by the hydrogeologist? * Yes No Regional Office CO Reviewer Admin Reviewer Fee Amount Complete App Date 05116/2024 Yes No $348 Below list any additional email address that need notification about a new project. Email Address Comments to be added to email notfication Comments for Admin Comments for RO Comments for Reviewer Comments for Applicant Submittal Form Project Contact Information Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence. Name* Kenneth Howell Email Address* kenneth.howell@townofboone.net Project Information ......................... Application/Document Type* New (Fee Required) Modification - Major (Fee Required) Renewal with Major Modification (Fee Required) Annual Report Additional Information Other Phone Number* 8282686270 Modification - Minor Renewal GW-59, NDMR, NDMLR, NDAR-1, N DAR-2 Residual Annual Report Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* Wastewater Irrigation High -Rate Infiltration Other Wastewater Reclaimed Water Closed -Loop Recycle Residuals Single -Family Residence Wastewater Other Irrigation Permit Number:* WQ0013263 Has Current Existing permit number Applicant/Permittee * Town Of Boone Applicant/Permittee Address* PO Box 192 Boone, NC 28607 Facility Name* Town of Boone Class A Residuals Program Please provide comments/notes on your current submittal below. Please find attached Land Application renewal permit for the Town of Boone, NC. This is a resubmittal. At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here. (Application Form, Engineering Plans, Specifications, Calculations, Etc.) Biosolids Permit renewal 2024.pdf 2.3MB Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger than upload limit. * By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature iYi-"C/ (1�lell Submission Date 5/16/2024 2/22/2024 Non -Discharge Permitting Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Dear Madam/Sir, Please find attached the renewal application for Town of Bonne Class A Residual program permit #WQ 0013263. The current permit will expire on December 315t, 2024. We are requesting that the signature authority for this permit be Changed from John Ward to Amy Davis, Town Manager for the Town of Boone. No changes to the Drying Process have been Made since the last renewal. In November of 2023, The town of Boone WWTP upgraded the Trojan UV system to a Wedeco UV system. The new system was placed in the existing channel with little modifications performed. it is marked on the site flow chart included with this application. We are also asking to have our Maximum Dry Tonnage per year increased from 1250 tons to 1500 tons. This is due to the growth of the Town of Boone and increase in enrollment of students at Appalachian State University. Sincererly Kenneth Howell Senior Operator Kenneth.howell@townofboone.net 828-268-6270 CC: Rudy Broschinski, WWTP Superintendent Todd Moody, Director of Public Works State of North Carolina Department of Environmental Quality Division of Water Resources 15ANCAC 02T .1100 -- DISTRIBUTION OF CLASS ARESIDUALS FORNE DCAR 06-16 I. APPLICANT INFORMATION: 1. Applicant's name: Town of Boone Applicant type: Individual Corporation General Partnership Privately -Owned Public Utility Federal State x Municipal County Signature authority's name per 1 SA NCAC 02T .0106: Amy Davis Title:. Town Manager Applicant's mailing address: P.O. Box 192 City: Boone State: NC Zip: - 28607 Telephone number 8f 28 ) 268 6200 Email Address: Amy, Davis@iownofboone.net 2. Consultant's name: License Number (for P.E.): Affiliation; On Staff Retained (Finn: ) Consultant's mailing address; City: State.• Zip: - Telephone number. () - Email Address: . 3. Fee submitted: (See Instruction B) II. PERMIT INFORMATION: 1, Application is for (check all that apply): new, modified, X renewed pen -nit 2. If this application is being submitted to renew ormodify an existing permit, provide the following: Permit number. 3YQ0013263 Date of most -recently issued permit: _ _ October 1.2019 Date of most -recently certified Attachment A (if different than the permit): M. FACILITY INFORMATION: L. Name of residuals processing facility: Jimmy S 'th City: Boone State: NC Zip: _ 28607 - Coordinates: Latitude: 360 12 ' 52 Longitude: _$j,,,,,o __R ' __�ff" Datum: Level of accuracy: Method of measurement: County where facility is located: Watauga 2. Facility contact (person familiar with residuals preparation): Name: &ujigth 11o=111 Title: SCUIQr pgMLQL Mailing address, P.O. hg2j 122 City: Boone State: NC Zip: 28607 - Telephone number. (828) 268 - 6270 E-mail address: kenneth.howell@trvwnofboone.net FORM: DCAR 06-16 Page 4 of 3 _ is the residual process facility also the generator? X Yes; No If No, please specify delivery frequency and quantity of residual to be processed: 1. Length of residuals storage at facility: 90 days (Note: the Division requires minimum 30 days storage in units that are separate from treatment system, i.e. not in clarifiers, aeration basins, etc.) IV. RESIDUALS QUALITY INFORMATION: 1. Specify how these residuals will be distributed: sold or given away in bags or other containers; X lawn (bulk); home garden (bulk), X other (explain); Most residuals are sold or given in bulk to farmers. Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a load capacity of one metric ton or less. 2. ( ;omplete the lollowing it residuals are to be mixed with other Type of Materials Amounts to be added per 1.0 dry ton of residuals (dry ton) 3. Approximate amounts of the residuals received and processed at the facility: 865 dry tons peryear: 4. Approximate amounts of the final product (processed residuals)to be distributed: 654 dry tons peryear: 5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and maximum storage times prior to distribution): Residuals are stored in a shed for90 to 120 days. Residuals are kept se ep rate and are not released to the public without lab results. L. Does the facility have a stormwater management plan? Yes; X No Explain whether the treatment and storage areas are under roof or how storrnwater runoff will be handled: Treatment and storage are under a roof. V. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source) Complete and submit the attached Residuals Source Certification and all associated documentation. FORM: DCAR 06-16 Page 5 of 3 Professional ):engineer's Certification: (Application Involving New or Changes to Treatment or Storage Units) attest that this application for has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal package may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have reviewed this material and have judged it to be consistent with the proposed design. North Carolina Professional Engineer's Seal, Signature, and Date: Applicant's Certification: The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105. Q Yes U., No, Explain; 1, ,yiC Ivy M Authority's Name — PLEASE PRINT) (Title) attest that this application for 1J t y'i j VLH � I R1 �1y S U .Y 1 �� ` m a rL� P t clj (Facility Name) has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action, which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water Resources should a condition of this permit be violated. I also understand that if all required pants of this application are not completed and that if all required supporting information and attachments are not included, this application package will be returned to me as incomplete. Note: In accordance with North Carolina General Statutes § 143-215.6A and §143-215.6B, any person who knowingly makes any false statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to exceed $10,000 as well as civil penalties up to $25,000 per violation. Signature: Date: ' 2 o 4- FORM: DCAR 06-16 Page 3 of 3 State of North Carolina Eir Department of Environmental Quality NEW AW Division of Water Resources Division of Water Resources RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted the Applicant shall submit one original and two copies of the application and supporting documentation For more in formation, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General -- This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or disposal in accordance with 15A NCAC 02T .I 100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Source Certification (FORM: RSC 11-15): ❑ Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ❑ For new or renewed permits, submit a separate certification for each source facility. ❑ For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification. ❑ Complete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Residuals Source -Generating Facility Information: ❑ For each source facility, attach the following: ❑ Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for Residuals Land Application Permits". ❑ Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. ❑ Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. ❑ Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling fi•equency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Residuals Quality Information: ❑ For each source facility, attach the following: ❑ Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. ❑ Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. ❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06-16 Page I of I � m � o P�4 G 0 H A A CC i.s Cal U F. 6) z s d G O U a� z 'u 0 x 6l Cd O Un U Dlvlslon of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 1. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): L Facility Name: Jimmy Smith WWTP 2. Facility permit holder is: Q Federal, El State, Ej Local Government, or Q Private. Facility permit issued by: xEj Div. of Water Resources, El Div. of Environmental Health, or E3, Other (explain ). 3. Facility contact person and title: Kenneth Howell, Senior Operator Complete mailing address: PO 192 City: Boone State: NC Zip: 28607 2- Telephone number: (82_8) 268-6270 E-wail address: Kenneth.HowelI@townofboone.net 4. Facility physical address: 201 Casey Lane City: Boone State: NC Zip: 28607 M Coordinates: Latitude: 36' 12' 52" Longitude: 8 1' 38' 41" Datum Level of accuracy EL Method of measurement.:..- _._:,: 5. Purpose of the facility: Q treatment of municipal wastewater, E] treatment of 100% domestic wastewater, E] treatment of potable water, E3 treatment of 100% industrial wastewater, treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: 336 % industrial and 96.4 % domestic) E] other (explain € ). 6. Does the facility have an approved pretreatment program: x[] Yes E] No 7. Facility permitted/design flow: 4.82 MGD and facility average daily flow: 226 MGD 8. Average amount of residuals being generated at this facility 865 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: Thermal Drier Class A , 2000 Ton Storage Shed Type and volume of residuals storage (i.e., outside of residuals treatment units) II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: 40 CFR Part 503 or [ 40 CFR Part 257. Note: Only residuals that are generated during dourestichnunicipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: t] Biological Non -Biological Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed Elm systems). FORM: RSC 06-16 Pagel of 5 4. Metals Determination; Complete one of the following tables (Le., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated tinder 15A NCAC 02T .1105. a. For Distribution/Laud Appileallo►t: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Pace Analytical and Date of analysis: 02/08/2024 Parameter Ceiling Concentration Limits (C1assA & ClassB) (ingAg) Monthly Average Concentration Limits (Class A Only) (mg4g) Result )ng/kg) Arsenic 75 41 2.7 Cadmium 85 39 1.2 Copper 4,300 1,500 4l0 Lead 840 300 13.6 Mercury 57 17 0.36 Molybdenum 75 n/a 5.1 Nickel 420 420 15.6 Selenium 100 100 3.7 Zinc 7,500 2,800 875 b. For Surface Disposal Unit (la►(lTll): Fill in the following table with the results of the latest analyses (i.e., on a dr-y weight basis) for the following metal parameters: Laboratory Em and Date of analysis: j Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (nig/kg) Chromium (mg4g) Nickel (H1949) > 0 but <25 30 200 210 > 25 but < 50 34 220 240 > 50 but < 75 39 260 270 > 75 but < 100 46 300 320 > 100 but < 125 53 360 390 > 125 62 450 420 Result (nig4g) FORM: RSC 06-16 Page 3 of 5 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: yes Q. no. If yes, list the number(s) LAM b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: Q yes x0 no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Pace Analytical and Date of analysis: 05/05/2022 Passed corrosivity test: xyes 13 no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: xyes 0 no. Flashpoint € M IF (> 1400F) Passed reactivity test: x[ yes One. HCN:, mg/kg (<250) & H2S mg/kg (<500) TCLP Parameter Limit Ong/1) Result (nrg/1) TCLP Parameter Limit (nrg/1) Result (1)19/1) Arsenic 5.0 ND Hexachlorobenzene 0.13 ND Barium 100.0 ND Hexachloro-1,3-Butadiene 0,5 ND Benzene 0.5 ND Hexachloroethane 3.0 ND Cadmium 1.0 ND Lead 5.0 ND Carbon Tetrachloride 0.5 ND Lindane 0.4 ND Chlordane 0.03 ND Mercury 0.2 ND Chlorobenzene 100.0 ND Methoxychlor 10.0 ND Chloroform 6.0 ND Methyl Ethyl Ketone 200.0 ND Chromium 5.0 ND Nitrobenzene 2.0 ND m-Cresol 200.0 ND Pentachloroplienol 100.0 ND o-Cresol 200.0 ND Pyridine 5.0 ND p-Cresol 200.0 ND Selenium 1.0 ND Cresol 200.0 ND Silver 5.0 ND 2,4-D 10.0 BRL Tetrachloroethylene 0.7 ND 1,4-Dichlorobenzene 7.5 ND Toxaphene 0.5 ND 1,2-Dichloroethane 0.5 ND Trichloroethylene 0.5 ND 1,1-Dichloroethylene 0.7 ND 2,4,5-Trichlorophenol 400.0 ND 2,4-Dinitrotoluene 0.13 ND 2,4,6-Trichlorophenol 2.0 ND Endrin 0.02 ND 2,4,5-TP (Silvex) 1.0 BRL Heptachlor and its Hydroxide 0.008 ND Vinyl Chloride 0.2 Ni) NORM: RSC 06-16 Page 2 of 5 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 91.8 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Pace Analytical and Date of analysis: 02/08/2024 Parameter Result (mg/kg) Aluminum 17400 Ammonia -Nitrogen 1220 Calcium 29200 Magnesium 2420 Nitrate -Nitrite Nitrogen ND pH (Standard Unit) 5.7 Phosphorus 15800 Potassium 3330 Sodium 940 Total Kjeldahl Nitrogen 53000 c. Using the results listed in Item I1. 5b. above, calculate the sodium adsorption ration (SAR): 1.5 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodiurn. application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 30 %. This rate is a (check one): XEJ default value, or 1B actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: j,I e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (1s°) Year PAN Five -Year Maximum Adjusted PAN (mg4g) (mg/kg) Surface 16144 20502 Injection/Incorporation 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: none FORM: RSC 06-16 Page 4 of 5 7. Pathogen Reduction_: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For DistriLuliar/Larrrl Apnlicatiorr_of Class A or Equivalent: C A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or 7 A sahnonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): Alternative 1 [I5A NCAC 02T.1106(b)(3)(A)] - Time/Temperature Compliance. Alternative 2 [15A NCAC. 02T.1106(b)(3)(B)] - Alkaline Treatment. Alternative 3 [ 15A NCAC 02T, t 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Hehninth Ova. Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Hehninth Ova. Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: composting, E] heat drying, Q heat treatment, thermophilie aerobic digestion, El beta ray irradiation, gamma ray irradiation, or pasteurization. K For Land A plicrrtion of Class B. Alternative 1 [15A NCAC 02T.1106(c)(t)] - Fecal Coliform Density Demonstration. Alternative 2 [15A NCAC 02T. 1 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP). Specify one. aerobic digestion, air drying, [ anaerobic digestion, composting, or Q line stabilization. c. Far Surface Disposal: Ej Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II.7a. above. El Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item 11. 7b. above. Q Exempt -If Daily Cover Alternative is chosen in Item I1.8, below [ 15A NCAC 02T.1106(a)(2)]. Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: Alternative 1 [I5A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). Alternative 2 [15A NCAC 02T.1107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). Alternative 3 [15A NCAC 02T.1107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes. Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization. xAlternative 7 [15A NCAC 02T.1107(a)(7)] - Drying of Stabilized Residuals. Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals. Alternative 9 [ 15A NCAC 02T.I 107(a)(9)] - Injection. Alternative 10 [15A NCAC 02T.I 107(a)(10)] - Incorporation. Alternative for Surface Disposal Units Only - Soil/Other Material Cover [I5A NCAC 02T.I 107(b)(2)]. 0 Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution, Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of 5 r NARRATIVE FOR CLASS A PERMIT RENEWAL Permit No. WCLOO13263 Town of Boone The residuals are treated and stored onsite. Solids are wasted to aerobic digesters then piped to the drier building to be processed. The solids are mixed with a polymer to make a cake to be run through a 2 meter Eimco belt press. The water from the solids is drained back to the headworks. The solids then go through a thermal heat drying process that produces an 85-92% residual. A storage shed is attached to the drier building and the dried residuals drop from a chute to a concrete floor. After each drier run residuals are stored in a designated area under the shed, until lab results confirm they can be released. The class A Biosolids are sold or given away in bulk. All recipients sign an information sheet with instructions for proper use and a copy is retained on file at the plant. We require that the biosolids be covered with a tarp when hauled. . n . Y �.. .. .._. ... _ _ _. J I 1 .M1 Nib 4 .}_ ..zE•.. �'.{:. - �..\.. .. '-h:,<�;��.I'- 'pia.: ,il,i.;�,:... ..E. •" _. _...�.._ �_. ' �'� 1�; ',; ..'. �a;,:•ile:i!! : �I� Ell:ria'.-,�iililiii. •i �`�,. ii:a,:,l, '\` • - . ,3 1' =:•l;:_.�.;.��:>•:I,;lys !I �+', �!rta ,;flu°r'silE;?�.It!j+ ic-,=!!!�� �il �F�- �,,...,_s.M., .. � ..:: .. t•.. ' �� • l i : y i ,' i�j �,�`� :; �:!� i.'' •$: Ley' :':,,.I'.''{: ' °_ ti� ON ❑� Eq °®i €9EV.E � ' ° 1 I F ! !f O: ^ oar •� •�J � ��. KEllp !r;l, !r"i.;l — _•`� 2._ E_ ._.'i'! ]'I•" IL.:i�.l •y n. !si:..' i'! l �c- ' 4.9 1 F y "il'li'i;-�ll`!I !ili�•!!s: I;a i,{. ...._° _ .._ _ , ,! ^� O� it •I��i!�I ay!-.}..1 .L} ! .�.!: .! n¢ �� �g : b6 oo �t!!E.�tlkknlli ��I (!i,J.i!,Ejai[-�f;'+I�ulrliik;<:iiisfY w , ! o _ I � % !' � .!E•_?;:.! :: ' '[: F:: �!' ,I;'<.lf:,r! i�':� I II;I?11•! Es _.-- r e � .j- �_°^« I 'g.; __�. _ I -" •-- — I'�_!.:II!i I! �E_ila Irreli!1 � .. N q 0 OMMIS OAR TOM OF 60011E WASTEWATER TREATMENT 1{obb; UpcAtrrdl#jlesacfele7 PJ 6 PLANT IAIPROYEAIENTS £NFS rinTFuzl�W °t', IIJIInISJAOf?u C +�V &P .,n IYnl7on-Se.MTIhC-S°W:.rnPhlh•AC 24 JryrF• RaaI.A $C E X SITE PLAN t7oe �09o-S4p�?{opa7t+r Wx-lon]'T ' �,i R If a wa, Lu _Ull NONE? I TR, V ;lilt AN. Om 10, OKMIC C, 0 c) fob" 0 0 0 1. OfA gl� v " '0. le; jq, ir U -.9 aw p -a] gp 011�E41 ��'r1S' lieu i 15I 1T,Jj.' Il' I I�i3 Gi',�o I'I'' r;•I �. {I I s�JIMF- VYA A �Rll - • M" Ujj�.; Nvn writ lkq�j let 77f!h 6 sm 11 "­ "I _', �j WAS YP 'r 4 too Nk' i LI) t wm"=� 4 4 @N!3 41 loll Emu ................ ................ X m UJ. Co. wx ............ Ll ai :ka fu i qj . ' L • 1, I i,`I O • i ` •• = • i i pf 41) cq ai .{r cd , JU d Ii ku • • h C' N y O /�l V L7 'i7 o R M0 T ` ,.'�• 43 ups •a 1 •rf C a�] � y i'• a lam{ . F.4 ' � �-t • ♦ 1 � � ! � j._r f-i may. � ' 1 �. `I � 1 `4• h � � j ' r• iLi •+l Q ' � ' ' • , k .I � � ' H . .'� C) � s' W_,�. �� i� o _, C� �C fGl � C'l1 '� Ii t :y •t C) � s' W_,�. �� i� o _, C� �C fGl � C'l1 '� Ii t :y •t ; .:�i •.. EXHAUST VAPOR OUT -LET SEALED ACCESS COVER MATERIAL INLET SCRAPER 'BAR {� 'VAPOR -DOME _ DISC.�1, 1 r STEAM % CONDENSATE PIPE •DAFFLE PLATE STATOR I SUPPORT SADDLE MATERIAL OUTLET' I ' FOUNDATION - la1;l�,:}.1�1,i �,1.'1:E�l:iln fi1!i,l. I • , END •VIEW ,SECTION EXHAUST VAPOR OUTLET* ' VAPOR DOME •--�• ,_ � . I t SCRAPER' BARS MATERIAL INLET i ROTOR ARIds Discs ? i SEAL ROTOR. BEARING `� �..-_.......� SIPHON TUBE } ROTOR AIR VENT��_ 7 CONDENSATE OUTLET CONNECTION IL ���� lr � ROTARY STEAM JOINT 'HOLLOW 5f IAFT• GEARBOX ! STEAM INLET . 1 ROTOR. SHAFT }t STEAM / CONDENSWE PIPES ' PADDLES . — MATERIAL OUTLET FdUNDATION SUPPORT SADDLE' S.IDE' VIEW SEQTION Alas -Stork ROTADISC® INDIRECT HEATED DISC DRIER Figure 1 �o Operators: Claps A Resictza1s Process Log Dig # Date Beg LVI End Lvl Gallons %solids Dry Tons Start up Shut Down Time, DatefTime Startup I B tfi 24 32 40 4B 56, Notes Hof Well Temp, 190-205 Steam Press, 80 psi r �atwell 1~Iring Rate 20% Feed Pres. 5o e d s ftn r H n' 0 Hardness Hotwell TDS < 8550 -r:< SO3 50 �= �T `-. �; Hardness SCR 0 = f ` SCR TDS < 8550 pH 10.5-12.5 803 50 - 100;;,'-r P-AIk > 300 ,._ =.sou N®R,; Iron < or = 5.0 Iron Cond, < 0.5 TDS' 5%of SCR P HMEOW TIME COMPLETE 6 12 is 24 30 36 42 49 54 Chem Nix Driptrap Air Com, . Air & H2O Lines Drive B elts Sludge Pump Rollers/Belts Fzt/Rr Grease E=t Oil. Levels Bolts/Nuts Corlveyerp Gas/FI20 Leaks Pumps Baghouse GasMO Lines Pumps/Drives Meter P=ps salt c F„S:L�_f 7 iY �'.i f� 1?_'i3 •- f+'ri ii �i�S.Ta. Gas - PSIGz Mn ��_. Y Drains DryBl.owdowa (refer to procedure) Drier Log DATA: _ Datelii Ii i e cu cn PA 4-1 p � U 4.) .. N rl � cq n w S. PA ,aa t, .L, r0 M -� H �n. 0 \ .as " 0 a� 4� `" c \ I I I I / � I 1 I 1 I I I - 1 I I I I I I . aYuLca. HC114 12/2lJ93 � - 0 Date ' Time Bag_House Ist Stage Scrubber pH Recirc. Pump 2nd Stage Scrubber pH ORP Re rc. Pump REMARKS: Hello 619199 Drier Building ®cloy Control Equipment Log For each check please write OK and Initials Notes: �. > �;�. �� 11 �� �- __-__. T �_ _ _ _ _ �� S _��_�.._ T _�.._--------------_-- i � �� - I L--- ... �--------�.`..__...-------' �� ���� ��-i�t _. �r 11 - ����� '-- i __ _ 3 � �: � �� I 3��. :.JL_.___ __. _ �, 1���_.. Operation and Maintenance A. Solids flow from a digester to the drier building and mixed with a polymer to form a cake. This cake is then run through a belt press, then through conveyors to a thermal drier heated by a steam generator. The residuals are then transported by another conveyor to a chute where it drops to a concreter floor under a storage shed that is attached to the drier building. A dust collection and air scrubbing system are part of this process. B. The drier is in operation 2 — 3 days each week (24hrs per day). Each shift is responsible for checking boiler chemicals and preventative maintenance inspections listed on the Class A residuals. Process Log (included). Small maintenance repairs can be completed by the operators, any large repairs and services are performed by our Maintenance Technician. C. All equipment is operated with manufacturers safety equipment. The town of Boone has a mandatory safety Training program for all operators. The boiler system is inspected by the DOI annually. Certificate is posted on the boiler. Orc checks weekly. D. In case of a spill it is determined if it can be contained and if any went to a water source. Spill is cleaned up, calling help as needed. Determine cause of spill to prevent reoccurrence. LA ORC Mike Everett 828-773-3709, WWTP ORC Rudy Broschinski 828-297-6242 and Ken Howell 828-263-8157. Notify DENR within 24 hrs. of spill. 336-776-9800 Outside business hours 800- 858-0368 or 919-773-3300. Sampling and Monoriting Mike Everett and Ken Howell are responsible for sampling and monoriting of the biosolids. Biosolids are stored in a covered shed behind the drier building. Biosolids with confirmed lab results are keep separated from those that have not been analyzed. Samples are taken quarterly and analyzed for nutrients, metals, and pathogens and vector reduction. An annual TCLP is performed each permit cycle. Biosolids are not released to the public without a confirmed lab report. Spill and Response Plan 1) if a spill occurs determine if you can contain it. If not get up with someone on the contact list start at top of the list. 2) When contained fill out spill notification form. If any of the spill has gotten into a water source estimate haw much. 3) Start cleaning up spill and take it back to the storage shed. Call for help if needed. 4) Determine cause of spill so we can prevent incident from happening again. 5) Notify DENR within 24 hr. of spill. 336-776-9800. Outside business hours 800-858- 0368 or 919-773-3300 Emergency contact list: - LA ORC: Mike Everett 828-2644503/828-773-3709 WWTP ORC: Rudy Broschlnski 828-297-6242/828-773-9520 Senior Operator: Ken Howell 828-263-8157/828-4f6-4*6-k-" LS 1- rI O'l Agency C0Oti.lCLLOU cm^IN/________ Only some (if the igcnu, IiNted bere Inay need to lie notified in any PikI-tiCLII;LI- incidenc the Response Coordi wi toes bestjmgmcn,okouk\L*/mecl. Those mxd'cd.,id`^nnuterisk should 6rno/ifio|pc,rveoc ' gencies Ap Phone No. ------ Contact Date/Time Regional Offiec in Aflanta, GA Emergency 800-321-C)SHA in Aflani a, GA 800-12-1-880-1 Division of Eniciv Chemical/Oil Spill Reporrino Linc City Hall - Town Ninnaper 268-6200 268-6254 ' ----' -- — ' ' 7,18 '-------'' —' ---- ' —' — Synagro mical mstc iisoomJ;nVO take -------� — '----- ^'Safety 1\"ICCJI kh*ni*J u;I`mWill 5-11 t I']pxny) — — � � | �--�---' —[-- ----- Pace Analytical Services, LLC � y�+p �ir1 r g @ 1377 South Park Drive VQV A alyti /►al Ke€nersvilte, NC 27284 www.pactl&bs.corn (704)977-0981 Page 1 of 2 Laboratory Report Karen Reece Report Date: 05/05/2022 Town of Boone VVVVTP Date Received: 04/21/2022 P4 Drawer 192 Boone, NC 28607 Project: Boone - TCLP Biosolids Pace Project No.: 92600489 Sample: Blosolids TCLP Lab ID: 92600489001 Collected. 04/21/22 07:30 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Method Parameters Results Units Report Limit Analyzed Qualifiers EPA8081B gamma-BHC (Lindane) ND ug/L 0.50 04/29/22 14:51 R1 EPA8081B Chlordane (Technical) ND ug/L 3.0 04/29/22 14:51 EPA8081B Endrin NO ug/L 0.50 04/2912214:51 EPA8081B Heptachlor NO ug/L 0.50 04/2912214:51 R1 EPA 8081 B Heptachlor epoxide ND ug/L 0.50 04/29/22 14:51 EPA8081B Methoxychlor ND ug/L 1000 0412912214:51 EPA 8081 B Toxaphene ND ug1L 3.0 04/29/22 14:51 EPA6010D Arsenic ND mg/L 0.050 04/2712211:29 EPA6010D Barium ND mg/L 0.25 04/2712211:29 EPA6010D Cadmium ND mg/L 0.0050 04/2712211:29 EPA6010D Chromium ND mg/L 0.050 04/27/2211:29 EPA6010D Lead NO mg/L 0.025 04/27/2211:29 EPA6010D Selenium NO mglL 0.10 0412712211:29 EPA6010D Silver NO mg/L 0.025 04127/2211:29 EPA7470A Mercury NO mg/L 0,00020 05/0212215A6 EPA 8270E 1,4-Dichlorobenzene NO ug/L 50.0 04/27/22 16:49 EPA 8270E 2,4-Dinitrotoluene ND ug/L 50.0 04/27/22 16:49 EPA 8270E Hexachloro-1,3-butadiene ND ug/L 50,0 04127/22 16:49 EPA 8270E Hexachlorobenzene ND ug1L 50.0 04127/22 16:49 EPA 8270E Hexachforoethane ND ug/L 50.0 04127/22 16:49 EPA 8270E 2-Methylphenol(o-Cresol) NO uglL 50.0 04/27/22 16:49 EPA 8270E 3&4-Meihylphenol(m&p Cresol) ND uglL 50.0 04127/22 16:49 EPA 8270E Nitrobenzene ND ug/L 50.0 04/27/22 16:49 EPA 8270E Pentachlorophenol NO ug/L 100 04/2712216:49 EPA 8270E Pyridine NO ug/L 50.0 04/27/22 16:49 EPA 8270E 2,4,5-Trichlorophenol NO ug/L 50.0 04/27/22 16:49 EPA 8270E 2,4,6-Trichlorophenol NO, ug/L 50.0 04/27/22 16:49 EPA 8260D Benzene ND ug/L 100 04/27/22 19:45 EPA 8260D 2-Butanone(MEK) ND ug/L 200 04127/22 19:45 EPA82600 Carbon tetrachloride NO uglL 100 04/27/22 19:45 EPA 8260D Chlorobenzene ND ug/L 100 04/27/22 19:45 EPA 8260D Chloroform NO ug/L 100 04/27/22 19:45 EPA8260O 1,4-Dichlorobenzene NO ug/L 100 04/27/22 19:45 EPA 8260D 1,2-Dichloroethane NO ug/L 100 04/27/22 19:45 } EPA 8260D 1,1-Dlchloroethene NO ug/L 100 04/27/22 19:45 EPA 8260D Tetrachloroethene ND ug/L 100 04/27/22 19:45 EPA 8260D Trichloroethene ND ug/L 100 04/27/22 19:45 EPA 8260D Vinyl chloride ND ug/L 100 04/2712219:45 EPA 9045D pH at 25 Degrees C 6.5 Std. Units 0.10 04/26/22 09:52 H3 EPA 1030 lgnitability NO mm/sec 2 04125122 12:00 Pagel of 28 41 aceAnalyllcal rtww.pasalahs,catn ANALYTE QUALIFIERS H3 Sample was received or analysis requested beyond the recognized method holding time. R1 RPD value was outside control limits. Reviewed by: Stephanie Knott 704-977-0981 stephanie.knott@pacelabs,com Pace Analytical Gulf Coast 7979 Innovation Park Drive, Baton Rouge, LA 70820 Arkansas Certification #: 88-0655 DoO FLAP Certification #: L18-597 Florida Certification #, E87854 Illinois Certification #: 004685 Kansas Certification #: E-10354 Louisianall-ELAP Certification M 01955 North Carolina Certification #: 618 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersvil le, NC 28078 North Carolina Drinking Water Certification M 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 North Dakota Certification #: R-195 Oklahoma Certification #: 2019-101 South Carolina Certification #: 73006001 Texas Certification #: T104704178-19-11 USDA Soil Permit # P330-19-00209 Virginia Certification #: 460215 Washington Certification M C929 South Carolina Certification #: 99006001 South Carolina Drinking Water Cart. #: 99006003 FloridalNELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: t A029 ViirginiaNEtAP Certification #: 460221 South Carolina Laboratory ID: 99030 South Carolina Certification #: 99030001 VieginiaNELAP Certification #: 460222 Pace Analytical Services, LLC 1377 South Park Drive Kernersville, NC 27284 (704)977-09Bl Page 2 of 2 Page 2 of 28 lum { (WAIoupoly3yenplsa8 1 (UNISldI-0 Z •auayd9x0l,'j0lyahx0yl2A •ouvpun x 'xilyaaldaH 'UVPu3'Cl+Z 'aueplolg3 �sap(,Iq�al�rsappgsad =d131 eP91�tS'NO-�1lnAneail �d101 0 E 0 •z 0 t7 J aLL Q m L z }{d•kwsonOa:dlol x 0 z � pua4daol43yl-9'4'7,'tauagd4>�014»rl rr..r_ r• -4'4'Z'aulpuAd'lnuaydaolyaesuaa 'auazuagoAIN'aucylaaolya 0H .�.. a 'aualp%ng0wl4]EK0H x 11 euazuagaolyoaxay Du o n jolo4luia *t'r ' Q uazuagoJOIW KI -Iosoaio q i 'josoaj3'losoajD-d � � � � Q -w'psoaio-o-sel¢EIOn-I�a5�d101 ,, (CD G E i a appowalAUA ` —O) g uallyt00j0Syouj-auajAipaa)0l3egal �w °C auolaxlAylalRylaW'aualAylaaoly�O O © O �@ x Il eueylaamtgaOt('uuojomly� ♦9 'Ouazuaq=lgo,OPPOlyoeilol �r uogieo'suazuae-sai9eMA -d101 C) Sy'ag x cr d 0 'Bi{'gd'�O'PO'eH'sysleiaW:dlOi Wa.L sasd(euV m jaylo CJ CL l4ueylaW iwI c in w £OZSZeN u o o � �a HOeiJ ~ [OR WL2i 0 K EONH O ` z y1 $ m 2 a WSZH Patiasa�du� N V u—E 4 [ Lj np, a a SIl3N1tlAN0�30t NOI.[03ri00 iV dYi�i.33dWYS ', 0 LL � r Z Q V r n w n U lam— o p u m y c$} O O J uj 8 p- r N O v� O ♦ N w Y wW y U W Y 6 IdWOD=a slVeD-0) 3dAL31dwvs m E 2 0 (ygolsapu�p4�+.asj a000xrtiivw a 42 r h Vq 9 9 g i &yy,, S 03�02 N C m CqC Cq .. } � � f c N p . r U c 0 I— 0. N a O ' m O] immills MENEM mommommommms `s m m (wAl Am salliweg wA rsp000 paleas. INlAI aol uo paelaaaa O w cjNn Page 3 of 28 } Laboratory receiving samples: Asheville ❑ Eden[—] Greenwood ❑ Huntersville r BC�r`�(;rilfl�lCBl'^ Document Name: Document Revised: November 15, 2g21 Sample Condition Upon Receipt (SCUR) I Page 1 of 2 Document No,: Issuing Authority, I F-CAR-CS-033-Rev.03 Pace Carolinas quality OT-fice Raleigh Mechanicsville AdantaE] Kernersville- Cile ame: 7UP Project R: Courier: [—]Fed Ex ❑UPS ❑LISPS ❑Client ❑ Commercial Qy ce ❑Other: Custody Seal Present? ❑Yes4o Seats Intact? ❑Yes ❑Pin Packing Material: ❑Bubble Wrap >�ble Bags ❑None ❑ Other Thermometer: et ❑81ue ❑ IR Gun 10: Type of ice: Correction Factor- Cooler Temp: Add/Subtract ('C) Q 10 Cooler Temp Corrected ('Q. USDA Regulated Sall (❑ N/A, water sample) Did samples wfgin in a quarantine zone within the United States: CA, NY, or SC (check maps)? ❑Yes o Biological Tissue Frozen? ❑Yes ❑NoW/A ❑None Temp should be above freezing to 6'C ❑Samples out of temp criteria. Samples on ice, coating process has begun Did samples originate from a foreign source (internatl naily, Inrludtne Hawaii and Auprsn Riml? € lYps I .' Comments%Discrepancy: Chain of Custody Present? es ❑No ❑N/A 1. Samples Arrived within Hold Time? es ❑No ❑N/A 2. Short Hold Tlme Analysis (<72 hr.)? []Yes., G; vo ❑N/A 3. Rush Turn Around Time Requested? ❑Yes o ❑N/A 4. Sufficient Volume? [es ❑Na ❑N/A S. Correct Containers Used? -Pace Containers Used? (fifes es []No [:]No ❑N/A ❑N/A 6. Containers Intact? Yes ❑Na ❑N/A 7. Dissolved analysis: Samples Field Filtered? []Yes ❑No /A B. Sample Labels Match �pC? -Includes Date�me/ID/Analys€s Matrix: Ves []No ❑N/A 9, Headspace in VOA Vials (>S-6mmj? []Yes [-]No [!/A 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes ❑Yes ❑Na ❑No /A A 11, COMMENTS/SAMPLE DISCREPANCY CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Date/Time: Lot ID of split containers: Date: field Data Required? ❑Yes []NO Project Manager SRF Review: Date: Page 4 of 28 I'-Cr:�•�3•� is -lit �, r c _ ` r. - hz;!1' cl- b i 1" an cr r i yl:,�� a� � 1':I:rr:r� i �? a=C�^:3':�� (u::j� �L•.' C't�33:'I�,:C� a m I125, ,, V:1"Cz.'_ . ,ice Ct, a,:: 11� `Sam ha!`.:c�!: 0 IvL:t i5 to jis: r!.':;,..er a.' ba!ti5 1 - C C C U 1 r'c- f 7. l" 0 C 1 C : C t a '_ F _ 1 - i 1 { ; { 1 I C 3 { [ [ C u l: ` C; I C I } I ] C 7 rr Ii i n C �•. v+ i i C ; 7 ! C 1 IN 1 I I\ I I I I \\ I 4jlI INI1 N n i i III!II ! IN I I NNNNI I III 11 1 1 I I I I I \ 4 IL\j j I j j\I.\I\I I III\I\EN I I I l i I I I I \I I i Ni I I i I I \1 I I1 \III 31 I NI I 1__ i\\\ III\ I \ I I j\IIIIIII�,j�k +°I 12I\ NI I \ I i I j, II-F-]- I �4 r E\\\! 1 pH Adjustment Loy for Preserved Samnles ply 10 Ti,a a'?rasarn:ive PH u;on receipt Da'e reservi'ion ad'3stad p 1' Tsmz,�reser'r3:iar, adjusted A—�aun: of Pre,zr•ra .vn added lot a 1 r t i � I I `rr ------------------ ----------- L i:c• _-r_ .. c_ r� u ...�u .ry c ,__,.r.p -,,,r.,. �3:�.,r.J c. .uc[c Sa'F.G'�i. a Cv;:'(N 1r�::.'C 'A'!: �@ i2^i :G Sf 2 �r7r:" C]"....!'3 Cc^fir? [9•.,(C,i: Cr• v'�,C•_ .6c,'ircarrec:pre sarrat,vs, Out Of temp, incolreC: cortainersy Page 5 of 28 (��a'c ie A na /y tic l LELAP CERTIFICATE NUMBER: 01955 DOD -FLAP ACCREDITATION NUMBER: 74960 ANALYTICAL RESULTS PERFORMED BY Pace Analytical Gulf Coast 7979 innovation Park Dr. Baton Rouge, LA 70820 (225) 769-4900 Report Date 04/26/2022 IIIIReIIpIIIortV ^p^Ip2W2Ip2pf1Y4yI2303 NY��I�I�IIIu II�MI RN���� Project 92600489 Boone-TCLP Biosolids Samples Collected 4/21/22 Deliver To Additional Recipients Stephanie Knott NONE Pace Analytical Kernersville 1377 south Park Drive Kernersville, NC 27824 704-977-0981 1*6nwok PJ LA T"Ung uoo cv►r Pace Gulf Coast Report#: 222042303 Page 1 of 9 Report#: 222042303 Project ID: 92600489 Boone-TCLP Biosotids Report Date: 04/26/2022 Laboratory Endorsement Sample analysis was performed in accordance with approved methodologies provided by the Environmental Protection Agency or other recognized agencies. The samples and their corresponding extracts will be maintained for a period of 30 days unless otherwise arranged. Following this retention period the samples will be disposed In accordance with Pace Gulf Coast's Standard Operating Procedures. Common Abbreviations that may be Utilized in this Report ND Indicates the result was Not Detected at the specified reporting limit NO Indicates the sample did not ignite when preliminary test performed for EPA Method 1030 DO Indicates the result was Diluted Out Mt indicates the result was subject to Matrix Interference TNTC Indicates the result was Too Numerous To Count SUBC Indicates the analysis was Sub -Contracted FLD Indicates the analysis was performed in the Field DL Detection Limit LOD Limit of Detection LOQ Limit of Quantitation RE Re -analysis CF HPLC or GC Confirmation 00:01 Reported as a time equivalent to 12:00 AM Reporting Flags that may be Utilized in this Report J or I Indicates the result is between the MDL and LOQ J DOD flag on analyte in the parent sample for MSlMSD outside acceptance criteria U Indicates the compound was analyzed for but not detected B or V Indicates the analyte was detected in the associated Method Blank Q Indicates a non -compliant QC Result (See Q Flag Application Report) * Indicates a non -compliant or not applicable QC recovery or RPD — see narrative E Organics - The result Is estimated because it exceeded the instrument calibration range E Metals - % diference for the serial dilution is > 10% L Reporting Limits adjusted to meet risk -based limit. P RPD between primary and confirmation result is greater than 40 DL Diluted analysis — when appended to Client Sample ID Sample receipt at Pace Gulf Coast is documented through the attached chain of custody. In accordance with NELAC, this report shall be reproduced only in full and with the written permission of Pace Gulf Coast, The results contained within this report relate only to the samples reported. The documented results are presented within this report. This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results contained within this report are intended for the use of the client. Any unauthorized use of the information contained in this report is prohibited. t certify that this data package is in compliance with The NELAC Institute (TNI) Standard 2009 and terms and conditions of the contract and Statement of Work both technically and for completeness, for other than the conditions In the case narrative. Release of the data contained In this hardcopy data package and in the computer readable data submitted has been authorized by the Quality Assurance Manager of hislher designee, as verified by the following signature. Estimated uncertainty of measurement is available upon request. This report is in compliance with the DOD QSM as specified in the contract if applicable. Authorized Signature Pace Gulf Coast Report 222042303 Pace Gulf Coast Report#: 222042303 Page 2 of 9 � .�aceA+,ayrka+' ReportH: 222042303 Project ID: 92600489 Boone-TCLP Biosolids Report Date; 04/26/2022 Certifications Certification Certification Number DOD FLAP 74960 Alabama 01955 Arkansas 88-0655 Colorado 01955 Delaware 01955 Florida E87854 Georgia 01955 Hawaii 01955 Idaho 01955 Illinois 200048 Indiana 01955 Kansas E-10354 Kentucky 95 Louisiana 01955 Maryland 01955 Massachusetts 01955 Michigan 01955 Mississippi 01955 Missouri 01955 Montana N/A Nebraska 01955 New Mexico 01955 North Carolina 618 North Dakota R-195 Okiahoma 9403 South Carolina 73006001 South Dakota 01955 Tennessee 01955 Texas T104704178 Vermont 01955 Virginia 460215 Washington. C929 USDA Soil Permit P330-16-00234 Pace Gulf Coast Report#: 222042303 Page 3 of 9 MiytxaV' Report#: 222042303 Project ID: 92600489 Boone-TCLP Biosol'€ds Report Date: 04/26/2022 Case Narrative Client: Pace Analytical Services Report: 222042303 Pace Analytical Gulf Coast received and analyzed the sample(s) listed on the Report Sample Summary page of this report. Receipt of the sample(s) is documented by the attached chain of custody. This applies only to the sample(s) listed in this report. No sample integrity or quality control exceptions were identified unless noted below. No anomalies were found for the analyzed sample(s). Pace Gulf Coast Report#: 222042303 Page 4 of 9 Report#: 222042303 Auly1xa!' Project ID: 92600489 Boone-TCLP Biosolids Report Rate: 04/26/2022 Sample Summary Lab 1D Client ID Matrix Collect Date Receive Date 22204230301 BIOSOLIDS TCLP Solid 4/21/22 07:30 4/22122 09:30 Pace Gulf Coast Report#: 222042303 Page 5 of 9 Report#: 222042303 f project 1D: 92600489 Boone-TCtP Biosolids Detect Summary No analytes were detected for analyses performed by Pace Gulf Coast. Report Date: 04/26/2022 in Pace Gulf Coast Report#: 222042303 Page 6 of 9 aiah6car' Report#: 222042303 Project ID: 92600489 Boone-TCLP Biosoticls Report Date: 04/26/2022 Sample Results BIOSOLIDS TCLP Collect Date 04/21/2022 07:30 Lab iD 22204230301 Receive Date 04/22/2022 09:30 Matrix Solid k1030 Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %aMolsture NA NA NA 1 0412512212:00 739338 JGI) 12.45 CAS# Parameter Result DL LOQ Reg Limit Units 000000-011-7 Ignitable NO 2 2 2 mmisec Pace Gulf Coast Report#: 222042303 Page 7 of 9 m J O y z m a. 5 0 o d � 1 c cr a z _ � O (asoLaa ON}N!j!ge571U 151 IS A3 JAJI�Q aj4 X d �y - O � a > CD m E.'°.� p01U0i01Gy� N z 1 O Nie CO m o O (p } 1 fL. 4M Cp 01 d/ w. c sJ .k N q C +r i Ck) � c Ri �IL,Zti F ? O C R' a 0' al m Dn C vc6.0 MEo O s (fJ CI. r Y U 0 co 0 0s m CL vi a m N O N CV 0 a a N O U 0 m 0 m (L MAN �I0000FIE ❑oo o Q Ln tO O ) U � a (D CL N a) 75 C z C �`' U N `0 U S CD � (iS U C > Q O Ln C N V 5 a) ET C ill N L LLI CL p U 1 ° @ p c� a Ea u� a � 3 fl3 -aE � N m a IFNc)L r-ry w IE R O ANA[YTICAE- ENVIRONMENTAL SERVICES, INC. AES April 29, 2022 Stephanie Knott Pace Analytical 1377 South Park Dr Kernsvilte NC 27294 RE: 92600489 Dear Stephanie Knott: Order No: 2204P 17 Analytical Environmental Services, Inc. received 1 samples on 4/22/2022 8:49:00 AM for the analyses presented in following report. "No problems were encountered during the analyses except as noted in the Case Narrative or by qualifiers in the report or QC Summary. Additionally, all results for the associated Quality Control samples were within EPA and/or AES established limits. AES' certifications are as follows: -NELAP/Florida State Laboratory ID E87582 for analysis of Non -Potable Water, Solid & Chemical Materials, Air & Emissions for Organics, and Drinking Water Microbiology & Metals, effective 07/01/21-06/30/22. North Carolina Certification number 562 for analysis of Surface Water, Groundwater, Effluent, effective until 12/31/22. -South Carolina Environmental Laboratory Certification number 99016003 effective until 6/30/22. These results relate only to the items tested as received. This report may only be reproduced in full and with written permission from the laboratory. If you have any questions regarding these test results, please feel free to call. Sincerely, 1, Paris Masoudi Project Manager ifk it �'�,•-i�lrttlial j3ri+',• Atlmtt,a.10440 �C,�l; �/�7lk.-i- �l.tit•['t Fax; 770.4<c:7.it188 " ,,JI I=rcu: 800,972.4889 • St'.,L•dtIt, nta.;7" Page 15 of 28 pang f of R 0 w N -% y m Z7 7C fA -' /'�O Im C7 zm eo m n �n„ �[ o V 0 Z .[0 y c :. M w a c ss �• � w ':i ` ro o p-Co o m _ m 4 e � N ^ Uveselved CA ,ti • t, : /�l Y /�I •Y All O m 1} �( TGLP HeMdd.. C 5 "gip' o 'r O :*��n N O a W 0 co 0 y r+ M Q l< Coil C71 NO N Analytical Environmental Services, Inc Date: 29-Apr-22 Client: Pace Analytical Client Sample ID: BIOSOLIDS TCLP Project Name .92600489 Collection Daft: 4/21/2022 7:30:00 AM Lab ID: 2204P17-001 Matrix: Solid Analyses Result Reporting Qual Units I3atchID "Hullo DatcAnalyzcd Analyst Limit 11 HERBICIDES,TCLP SW131118151A 2,4,5-TP (Silvex) BRL 0.20 2,4-D BRL 0.20 Surr: DCAA 77.8 50.1-120 !. Qualifiers: i Value exceeds maximum contaminant level BRL Belowreportinglimit H Holding limes for preparation or analysis exceeded N Analyte not NELAC certified B Analyle detected in the associated method blank > Greater than Result value (SW3510C) me/L 335157 1 04128/202213:43 KH mp/L 335157 1 04/28/202213:43 KH %REC 335157 1 04/28/20221143 KH E Estimated (value above quantilation ranee) S Spike Recovery outside limits due to n7atriK Narr See case narrative F Analyzed in the lab which is a deviation from the method Less titan Result value 7 Estimated value detected below Reporting Limit Page 17 of 28 Pans R of R .:r u u Q v w ce U, J Q D u a J IL a c a E E u V al I Y 0 01 � u m c Y a � ro a w w Y ❑'a = ho ro a to al V O z ' o C- *(D E) N C) N V U O O ✓1 C W a 0 CL v � � 0 a a u CL n F' F E a o0 h a t» uP u 0 a F- v pu u 'P p C 3 •V a b m G W al 3 73 w 2 a a a m CL E E F M N r C U U u u p p QL1 a n a f "m L a a E E F. F N lU L a a u c� 0 0 lO <T v d L y LO CL n ct to y a v E U a U N fi1 4 ui ui rr 00 OS 6 1-4rj chi a chi n i V O � v � � ro b C ro b � r H m or n• C E a � 3 a a u ,.. 3 O U N N G 0 Y C b n. U U c C C OF1 c •IL m E O ++' w+�+ 0 N Q N y Y Y ro b N 00 " -0 pCD 7 U 0 3 G U al u 0 u opp Q C) m G b '0 CLn A L d °1 C = „ � a '0' E rEo b a P n E 5 a •� P b a a O Q� Q C C it C a E 0 E ro ro E trii v U F u +: U u %A r r n' al N - A ro C A ro -v v a n• C G c ro Oa 'L H CL•� a N u U U a C 'C] E a`i u a O O a u croi m g c U c E r a ( P N Y V L } Q a u Y N C ! O .G Q a ro ro 0 °' n CL ro E n. E u .n E CL a n- c c c vroi °i a c 0 w •1,,n v c O 7 C C C O N CL u aci v a }o E .0 E u u w a n" N a fl 0 n c c a a a s m m m O u nl M } E '� w a '^ a E va °' CL y 0 v E p a ✓+ b 10 E ro r a 0> a 0 2 2 m a +' g V a a y N N a a a a ry p 3 n al a 3 s 3 u' u' N N ch N s-- N z O z io r 41 n c U CL a) 3 a2 d O Yb N U N a 4' ❑. N SG CL T E 0 0 G U) o � G E N to r, m Qt G .-I N c i d to 6 n ri rt H ri N N N N N N N N N fV N a r N L O to 00 N N C O 1+i N z-ru ao: d ? Y.. O m m u Q U r 7 N Cl 0 V fC � a Q Q C P ` � CL 2 O G .ty N C 'O 03 N om ja oy e y v m m � y m a m •3 i � u E 3 i u C C�V 7 0 C 5 m U O• N m ]. 41 r• o P a IV a w O a •=3 U N E A C � � N aai W kA c ro a C E C f=7 0 lg ` r m � � c o x C1 w r a u Q ro P m 0 H N 01 lAe 18 of 28 � a a O OO W N In 0T0 .N, ❑� `�00 'r r zz zz A zz A /& ul LOto A r ,N M CAN N N \ N N p \ N N SO p N 0 C O U QI-D 00 N 00 N N CD C'� y a a y in OL4 a.) c o N N C. o N x x x In n InDD �_ r In n in M E M 3 £ M a M a } , In jC) f� c> 00<D (q cz> t- o U N (q {U p: 00 000 OMO 00 r- n o 4 N In O t � �? d C3 0 0 � 0 0 0 7 C7 O .-+ O O O . . Vl } ,.� CD O d en � p M a. o o 6 o 0 0 rryy a w .a F l N N O F a Ci ( o 0 o o v, Ep�� CD � Q � � U �4 O u GC U p0 U N �_ O ON � N N 4¢�] 7 C7 ODD OHO V M M V '^� y Ski W OUT O F d � CN 00 o Qt o o R 03 N o x �+ O R ON N n M M M Vl py ..'L'ia p� M � V] � ••t � r +~ N 7 U ~ Q 6 R. U v ?� q m �[ A. n H G3 g. ix - G Q �n C1 n c to C� U r ¢ Q Q cn d ter" 4 cn Ps N N C,y C' N N 00 0 m a End of Report Page 20 of 28 Pans- R of R k ANALYTICAL. ENVIRONMENTAL SERVICES, INC. AES May 05, 2022 Stephanie Knott Pace Analytical 1377 South Park Dr Kernsville NC 27284 RE: 92600489 Dear Stephanie Knott: Order No: 2204T46 Analytical Environmental Services, Inc. received 1 samples on 4/27/2022 9:17:00 AM for the analyses presented in following report. "No problems were encountered during the analyses except as noted in the Case Narrative or by qualifiers in the report or QC Summary. Additionally, all results for the associated Quality Control samples were within EPA and/or AES established limits. AES' certifications are as follows: -NELAP/Florida State Laboratory ID E87582 for analysis of Non -Potable Water, Solid & Chemical Materials, Air & Emissions for Organics, and Drinking Water Microbiology & Metals, effective 07/01/21-06/30/22. -North Carolina Certification number 562 for analysis of Surface Water, Groundwater, Effluent, effective until 12/31 /22. -South Carolina Environmental Laboratory Certification number 98016003 effective until 6/30/22. These results relate only to the items tested as received. This report may only be reproduced in full and with written permission from the laboratory. If you have any questions regarding these test results, please feel free to call. Sincerely, pal,_4, IAczoa"C- Paris Masoudi Project Manager 3lji 11 l'r.••i.l •niinl I leivo • ;`lL�nE.�. C;,•.,r,:ia 31) 340 1 r�: l iEl. 1�'i.41 �"� Fax: 77t1.-��7.2�1 35 Toll I rcr: 8��{1.9! �. S$8<) w wkk, a.•.al l,.�,t.... „�„ Page 21 of 28 Pon. 1 of R o w N to A W N o O P 3 N m m N DCL �. N .M ID � o W v � N c a W w RT � �W 0 10 (o c's fp C %- r7 O m 0 O 3 ` � m o , n O 3 3 A I/ m C El) m 0-�m5 -v „ 0 n Z n- ...-- O "h m (D o 7c tb to ClO 00 J ,o �-'`mm � a O _ ? w Q C w y 0ro o O n 0) 0 � O x O Q Z N 00 O Cr 4 4 R W ow C. G 0 cn d 0 m 0 "L7 O 0 a •N N ed r� N a a n 0 � � �i s a Reactivity Analytical Environmental Services, Inc Date: 5-May-22 Client: face Analytical Client Sample Ill: BIOSOLIDS TCLP Project Name: 92600489 Collection Date: 4/21/2022 7:30:00 AM Lab ID: 2204T46-001 Matrix: Solid Analyses Reporting Result Limit Qua! uuu[mn Units Batc11ID iFaetor DateAnalyzcd Analyst Sulfide, Reactive SW846-7.3 (SW7.3.4.2) Sulfide, Reactive BRL 100 Mg/Kg 335376 1 04/28/2022 12:00 AD Cyanide, Reactive SW846-7.3 (SW7.3.3.2) Cyanide, Reactive 1.49 0.962 ❑1giK8 335102 1 05/04/2022 00:00 AD t�l�alifers: * Value exceeds maximum cuntaminant level -' BRL Hetowtepostinglimit H Holding times for preparation or analysis exceeded N Malyte not NELAC certified Anatyte detected in the associated method blank > Greater than Result value E Eslimated (value above quanfitalion mnec) 5 Spike Recovery outside limits due to matrix Narr See case narrative F Artalyzed in the lab which is a deviation from the method < Less than Result value 1 Estimaud value detected below Reporting Limit Page 23 of 28 (�nnc Z of R 42 C0 N O N n u u O O y ro C C E d E J � ri C al a C 0 m `° a a a y CLu E E w 66 y � 't co C E a m 2 o aL u u y CL ro m U a s 3 In m t3 a a y O v O a � � Y N � Y IU ro at a E E c � � 0 0 u u a z u u o p z ► r • r W y n, ro v a � O. ii ai aEr CD N `° y a a a O O c u u a c �; cu L _ Y v � n O a n• E u b � a c ro p_ fa m C N M1• CD m .GO>u a 0 a ai a T T G a d � 0 o a � -0 E a 7 f0 y f" y u u c— L Ln C a o a m E a `m E C c Q tE 3 r u u U u iLn bQ ai O V4 N ri rl r4 m ti M 2 u u c � 6 j 'o a L y O — o 0 ❑ U :3 0 Q � 0 r w a � N CL a a a`"i ayi E ° E E u c O C N V�3 ®c 0 rolmu u 0 0 0 aar Aq Y c c N N r• �i a3 N O T p m � C L N •O � a � � N v L " u c ro N M1. U W �+• L Y 6 Q 'n Q' °f Cl) u u u a s a d 'm c tJ t au c rc a c C y Y = a 2 CL o •� o..� n Gi u y c a O Y O at .� CL a m r Q. ." m E i4 a v m cx m a -"o L C N � � � C y C 41 0 v o c 2 a v u aci w L E CL L3 } Q Of y y 7 ro O A c a a E R ro a ro a 7a :5 E a'H ? y E 0 C. a c io ) a m 7 Qy an y a a ro :G a al a O 3UU' n° a 3 3a�:3 �: u ri r-1 � N N N N N N N N 10 20 R 00 co a- rn a r n � � N O O y N CV T co O N < O O a 0 0 0 0 0 ©fa (V GV � A a cov o N co fl! � 7 U — w U N co 'o Co d 7+ 7 x m O O rj) in O N (7 U �t V U m m a Q Q 0 O O a o 0 N FF- I�- m O O J C4 N 00 N w 0 LO N N Ql co O, 40 11 �IA H. ' C6 f��' d- CS .r t-: t-+ R N rt�R Trel R N �_ R 00 _ z z z z z C4 z G4 Z PC z CG C En ply/ �C4 ' o N N __ ell N _ Q N c U Q N N N N N N N N �y o o o © o o o o 00 N A q A q A A in q E o brp by bn oA M �+ M M b0 t M M 3 in M e tfl M Er!In 0 �D AQ � l � C4 1 P\oC V) v] cn v] cd 7 dd > C7 p Cd > o p cd > p O M M Rs M �4 ow M w K 7 00 04 v°i rn q m C4 riz CD Y 00 u y U E'er a] }•�I A dJ U H U Vim' 6CI U H � a' O v QCJ U R' f'-a d tR ,o z z 00 O n M O O W N tn M M M G O � D? U N N ai 7 r••� aL ? N ? fNV v cd Cd A >, V A 93. V) U3 fn r 7 C I'�+ in a a a 0 �n � �n o d' N e{ N00 .. N zz zz zz zz C d N 04 V) o ° d O \ U Q o o C> o c ch T o Q x x x in �m a �M ads E M a r M 3 M 3 cn rn 3 -� 3 N Q a N -+ U pq rJ W4 (.,� M Vcg vl 4-� O a w o a� o 7 7 r a r�ia � •r o icy 0 Q r O x x o �r O O R A v-e p O � � O C �n O O 06 U H � a O O 4 U`dN p. in �" In M M M co Se t] U N u 4 O a u : A 46 N a¢ a < U End of Report Page 28 of 28 Po -RrefR C w w .. cri a. w N i Y Vi m -0 7C j "O f� w $t 3co m m r a 7 m 1� = (D ,� 3 r p �. 4 Z w o : 'i !" b� to N N co ;kk o a: Cm 11 Q� G 7�F kv Q 1 •�„ � r � �.�Tpf859fY8d .�� G 1] kj "1 tit iC fCLP 1 ferbicldos Z y d N ,i Ct y z, !< � ; iU Of $tea y CL a W fD CL C`11 UI a y 3u k; dlttd 8Z to L 4 a0ed l wi l 8uiuoda nw�aq pa;aasap amen palewilsa ( anleA;[nsag uegl ialEDID an;eA vegl ssa-E > auo19 poglaw pale!aosse 041 us paloolop aldleuY g poglaw agl woij uopo!Aap e s! ya!gh%gel ogl u! pazdleuv d pou!l'oa 3v-lg d lou alA(euy ly aA!lujaeu asea aag DUN papaama s!s4leue so uo!leiedaid jod saw!l Su!plaH H x!tlew of onp sltwlj op!slno ljanooa21 ay!dS S i!w!l 8wuodax Mojag �{g (*Sue) uongl!Suanb oAogo on;eA) palEwgsg a janol lueu!weluoa wntu!xew spaaaxa oNeA ; :sAjljllunb I IIN £b:£I ZZOZ/SZ/ti0 1 LSIS££ DH21% OZl-1'09 SU V-Vo(l:ranS HN £b:£1 ZZOZ/SZIVO I L915££ `ow OZ'0 RiII Q-b`Z HN £b £I ZZOZ/SZ/P() 1 LSIS££ 'Otu OZ'O -mg (kaAIIS) di-S`b`Z OOIS£MS) VISIS/II£IMS drl3.L `S5(Q3If U9H )sdluuv u paz,(Ieuj+a),eQ ot�nur[ (IIIIa1m1I silufi Im!'I Inno �u1laodan 3lnsau luu sass I �' NOS 100-Lidtozz :(CI q�'I KV 00:0£'L ZZOZ/l Z/b :a1r.Q uolpalioD 68b009Z6 awuN laafoxd d'131 SQI'IOSOIH :([I aldmus )WID I1331),(Ietld30ud :lU3113 zz ady 6Z :31e(I Mll'saaIAaaS jVJUali[lIOJIAUj JUapnjLnV r n }a 96 ' z n x N O H O C a O Cl x N i a ffDD M fA cl 'i f1 N lD N 5 v CL 0 3 w fD _ v O O O J N < m a @ a 2 c CL :3n en c S �• 3 i CN � S ErEr f (D ro C �- � ro O. CL m m ro �s 7 �0 a o w N � a tf ro }� 2 ro o •� 3 .+ @ 0 i] M @ j fx CDED C 3 1'1 ro 2 R R to a' N W O 0. fU A ti d N � v 1 1 a ti D r N W N N N V N N N N N m in A W N N 1-+ F+ l' m N O ro Q. w fD N w fp @ N T @ w w O O @ El3 CL n a v n 3 troll+ d o ro m m cr w a 3 m '^ m a j I", b O �e• rD m � .� o fD r 3 a o fa+ A @ w. fD o cro, m ro o ^ ro' ro. 0. ,�-'p' cr (� (gi(pp 0fn M Ev 3 V ro ww CL O w N O a 61 3 0 Ts d. 0 0 3 0 �• O n v o 0 °r.' c m @ o s S a o vroi m o 3 o O m n ro n CL 3 @ u n n O J m ro ',1 •tl : v 67 d U w O 7 fD O: (OD U m P, G Q n CL au Q c 3 C-0rr U ro ti .0 o'®'�®' 0 1 o p�" .0 0�0 O�t a v S o• 3 o 7 m y @ G � � p C CL a o 0 c ❑ ❑ a ro � n. ro 3, IX K O CL @ ❑ ❑ 0 0 n Un A w N 0 0 0 g m O O R j U � ., fD F. ro w ro d CL � aa o t7 m w n 1f ro a @ a a � J i C z 0 0 fD m N ." L lu ro O w @ 0. A 0 N Lnn 0. fs1 ro O M 7 � w V n n O O fm m R V l .l m m (D v ro ro a nl � c fo m ri ri D O O O m m ro m 3 3 •o 10 ro fD Qj a M m ri fi vr a a b rrs! n 0 0 r- m m m m rl r- 101 N N C/I IJ N CA N N -_.... CD C/] � W ►%1 W � OU,J t C Oo '{yamry' 'Jd d O d Cd O O 4 }}j dj Enco ' 00 00 O O N-4� 0: .�-.• _cN C �7 N L, N _ p w O p t-y nO n n 0 0 d o o o o 0 0 CDr A "3 0 0 o Ll f�1 0 0 o m arA ro ro 0 0 o Ln v w o 0 111 0 (A ��74 �+ o 'FttyMM7 w C c`e LA o d 0 �4 C) oa CD 9 rn > a 9 CIO 10 CA e��-1 o 0 v J O ?i w O O A td C N .P .p C] b� C N C] o 0 0 d o co 0 0 o l7 Lh v M 0 0 o t J o 0 o t" C) C" Y b IZ � ��Vy is NtcN N� NN n a c o 0 0 o V} o N N o N N a N N W C7 C7 C "' CA � V1 1jf C/1 '/li V .o Xn A C r- da oo C F A Nm N N� b � O to I �Ilace, Laboratory Report Karen Reece Town of Boone WWTP PO Drawer 192 Boone, NC 28607 Project: Biosolids -Quarterly Pace Project No.: 92710176 Pace Analytical Services, LLC 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 Page i of 2 Report Date: 02/08/2024 Date Received: 01 /25/2024 Sample: Blosolids Lab ID: 927101176001 Collected: 01/25/24 09:45 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Method Parameters Results Units Report Limit Analyzed Qualifiers EPA6010D Aluminum 17400 mglkg 32.8 01130/2416:57 EPA 601 OD Arsenic 2.7 mglkg 1.6 01/30/24 15:13 EPA6010D Cadmium 1.2 mglkg 0.066 01/30/24 15:13 EPA6010D Calcium 29200 mglkg 82A 01/3012416:57 EPA 6010D Copper 410 mglkg 3.3 01/30/24 15:13 EPA6010D Lead 113.6 mglkg 0.66 01/3012415:13 EPA6010D Magnesium 2420 mglkg 6.6 01/30/24 15:113 EPA6010D Molybdenum 5.1 mglkg 3.3 01/30/2415:13 EPA 601 OD Nickel 15,6 mglkg 0.33 01/30124 15:13 EPA6010D Potassium 3330 mglkg 328 01130/24 15:13 EPA6010D Selenium 3.7 mglkg 3.3 01130/2416:57 EPA6010D Sodium 940 mglkg 328 01/3012415:13 EPA 601 OD Zinc 875 mglkg 3.3 01/30/24 16:57 EPA 601 Go Sodium Adsorption Ratio 1.5 megll. 02/08/24 10:59 N2 EPA7471B Mercury 0.36 mglkg 0.032 02/0112414:36 M1 SM 2540G-2011 Total Solids 91.8 % 0,10 01/26/24 17:04 SW-846 Percent Moisture 8.2 % 0.40 01/26/24 16:56 N2 EPA 9045D pH at 25 Degrees C 5.7 Std. Units 0,10 02/01/24 13:25 N3 None Plant Available Nitrogen 16100 mglkg 02/01/24 14:33 N2 TKN+NO3+NO2 Nitrogen 53000 mglkg 40.0 0210112414:36 Calculation EPA 350.1 Rev 2.0 1993 Nitrogen, Ammonia 1220 mglkg 31.4 01/31/24 05:39 Mod. EPA 351.2 Rev 2.0 1993 Nitrogen, Kjeldahl, Total 53000 mglkg 2590 01/31/24 04A4 EPA 353.2 Rev 2.0 1993 Nitrogen, NO2 plus M03 ND mglkg 4.3 01/27/24 00:26 EPA 353.2 Rev 2.0 1993 Nitrogen, Nitrate No mglkg 4.3 01/27124 00:26 EPA 353.2 Rev 2.0 1993 Nitrogen, Nitrite ND mglkg 4.3 01/27/24 00!26 R1 EPA 365.1 Rev 2.0 1993 Phosphorus 15800 mglkg 272 02/05/24 18:08 ANALYTE QUALIFIERS I13 Sample was received or analysis requested beyond the recognized method holding time. Mi Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. N2 The lab does not hold NELACfrNI accreditation for this parameter but other accreditations/certifications may apply. A complete list of accreditationslcertiflcations is available upon request. R1 RPD value was outside control limits. Page i of 5 �ace° Reviewed by: Stephanie Knott 704-977-0981 stephanie.knott@pace€abs.com Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 FloddalNELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 FloridalNELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: 1 A029 Virg€nlaNELAP Certification #: 460221 South Carolina Laboratory ID: 99030 South Carolina Certification #: 99030001 Virgin€aNELAP Certification #: 460222 Pace Analytical Services, LLC 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 Page 2 of 2 Page 2 of 5 C�' I r2' - t t Cl _; (ruUeuyo1401�nPKoN (ognoyd3)Hd 2 �Y�h ' lltl¢¢1R71=] (iiYS) alum uan&my wrepas . toologYd3);wjZ'wn!pGS'wnlualeg 'wrusselod'IeN?!N'WnuBpglloiY "�^"� r`= d 'tun!Seubely'pa07'mdda3wngle� _ 'wnwPeo *NOsM'wnvjwnN r (OOKZ WS) SHOR leltil tuayad � � � n EIS'S9£Yd3)srvo�dsa{dleloa Cl a c INY4).1--im-IO[1 AVWeld � � N t IL"£SCYd3) Z4N'L4N'{L"t5£ Yd3) H7S1'{L'OS£ Y43) N-THN 5 :3saj'sasdlaU s: faylq o- 0 = a IOueglerl U t £RiSipN (1p LU O C 4N4 q "CNN � d cc> F- ro E R r O £4NH C] o z o 4oszH Q $ m o a pwace,duR )— m G n o 8 A¢ c� $ a 8 3 a �° Sl1dN1Y1Noadoll • tsauoTMO it drr31 aedrn^s Vw w LL O q c a � L A L C 2 V) � G (dkYpa•7 9h1"�=aF Hdfl 31driYg V C� L $rz IYSf 41 tiP�RlN ax) 3QQ�XItllYW yyu a O E ce 2i MgMq z yz, qYr )g ,a a . a a y W cc 0 a 3 r a> N n [L a E a o O cmi c w )-EL d 2 o' VGAI (WA) ial000 PalaaS � 6 trl {N1Ai 67l ua panla�eb 0 uI dw31 Pago 3 of 5 DC# Title; ENV-FRM-HUN1-0083 v03—Sample Condition Upon Receipt ace yi,,�xr. tEnY�i Effective Date: 12/01/2023 Laboratory receiving samples: Asheville 0 Eden❑ Greenwood ❑ Huntersville ❑ Raleigh[-] Mechanicsville❑ Atlanta❑ Kernersvilleoj' k Client Name; Project a-, Courier: [—]Fed Ex ` ❑UPS ❑USPs 1710ient ❑ Commercial Ex-ce ❑t)ther; , „,,. - Custody Seal Present? ❑Yes Egho Seals intact? Des ❑No (3N/A ��� Date/initials Parson Examining [on;Qnts:���+�.s Packing Material: Bubble Wrap (ZI16ble Bags ❑None ❑ other Thermometer, ❑ iR Gun ID: TYPe oJ Ice: et ❑0'ue ❑None Gorractlan Factor: Biological Tissue Frozen? ❑Yes ❑No�J/A Cooler Tempt Add/Subtract (`Q Temp should be above freezing to VC; ❑Samples out of temp criteria. Samples on Ice, cooling process Cooler Temp [urreged {"Cj: _ _� �_ has begun Regulated Soil ( E) N/A, water samPlej Did samples originate In a quaFantlne zone with(n the United States: CA, NY, or SC bid samp:es originate from a foreign source (internatlonally, (check maps)? ❑Yes Including Nawall and Puerto Rico)? []Yes W [emmentsJDiscrepancy: Chain of Custody Present? j,'j ees []No❑NIA — 1, Samp°es Arrived within Hold Time? IRtet Nn 0 N/A 2, Short Hold time Analysis (<72 hr.)? UK, ❑Nu 3, 05, Rush Turn Around Time Requested? Dyes WKG, _❑N/A ON/A 4 Sufficient Volume? 9es No 0"/A 5. Correct Containers Used? -Pace Containers Used? Ufvs Ulles []No Elmo ❑N/A ❑N/A 6. Containers Intact? es ❑No ❑NIA 7, Dissolved analysis: Samples Field Filleted? ❑Yxs ❑No ll�/A 8. Sample Labels Match COC? -includes DateMme/lD/Analysis Matrix: Ves Oho ❑N/A 1 14eadspace In VOA Vials (>5.6mm)? ❑Yes ❑No U[jN/A 10, Trip Blank present? Trip Blank Custody Seals Present? ❑Yes ❑Yes ❑No ❑No A A 11. COMMENTS/SAMPLt DISCREPANCY Field Data Required? Dyes ❑No Lot 10 of split containers: CLIENiNOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Project Manager $RF Review: Date/Time: Daze: Date: Qualtrax ID: 69614 Page 1 of 2 Page 4 of 6 DC#JTRW ENV-FRM-HUN1.0083 03-Sample Condition Upon Receipt Effective Dat s: 12/01/2023 Check mark top half of box if pH and/or dechlorinatjon is verified and Project Ifi within the acceptance range for preservation samples. xeepl€onsYOd.Cntifcrm,iLZ Cll,tnSGrCaSti;€�seja7€ I"tljQf,tllE 'Bottom half of box is to list number of bottles R • "Check all unpreserved Nitrates for chlorine w N f n Q d v C Q ri M C: = { N ,� •� U K- 'L 4 x ri L Lt Z '.L V x i Z �• i E E �: L I_! � ri y � �_ ti N .ri .7 a m a a E E E ro E r•t b _ N > > 7 ur E tl M i i rE ? CD m m as E vti M w z m a E DES a E 6 4 6 yyan rr N 3 N (Q 7 x 7 4 Q t7 H M m M K N- - Sf .r W Z r_ i~ o Q ¢ V F- m 4 O1 l9 0 l7 t7 C? C y 7 m s i7 V m E %u IV a `_ A A ` n N Y r= d " �y { N f f C. O u E E b b : 7 0 A 1{ 1\\\ J 3 J N L _._._:_J _L 10 1 N-T, i.1 pH Adjustment Log for Preserved Samples _ µ sampte to Type of pfeservative pli Itpntt receipt Date preservat'san adjust,d Time preservation Amtu£kt of presorv.]iiV11 tot it atijitstrtd attdrd Pvntf:. IVlteneVV (rialpliano: , tmiks, a cop" vl thii t(ttr:t vril i; • s;, i! ur thr; .frr:h {'.arnlin,s 1):?It1 (.e.r:tfErat€on Offiu, ii F Ook of itcrld, in.;utr;'u pre;fpr,.i Ita-;, ou; of iirur% rr,tor:n_rl Page 5 of 5 FEB/12/2024/MON 12:50 PIS FAX No. P, 002/002 WATER QUALITY LAB $ OPERATIONS, INC. CLIENT: TOWN OF BOONE WWTP ADDRESS; P.O, BOX 192 CITY: 130ONE STATE: NC ZIP 28607 ID#: NCO020621 P.O. BOX 1167 BANNER ELK, NC 28604 ($28) 898-0277 RECEIVED DATE: REPORTED DATE; 26-Jan-24 12-Feb-24 ANALYSIS LSID # ANALYSIS MQI-'s UNIT$ SAMPLE ANALYSIS INT RESULTS LOCATION COMPLETED TOTAL SOLIDS 1 01.5 % SLUDGE FECAL COLIFORM 214 MPNIg SLUDGE 26-Jan-24 PI TOTAL $OI,IDS 2 90.8 % SLUDGE FECAL COLIFORM 277 MPN/g SLUDGE 26-Jan-24 Pi TOTAL SOLIDS 3 91.8 % SLUDGE FECAL COLIFORM 138 MPN/g SLUDGE 26-Jan-24 PI TOTAL SOLIDS 4 92.1 % SLUDGE FECAL COLIFORM 156 MPNI SLUDGE 20-Jan-24 P1 TOTAL SOLIDS' 6 913.0 % SLUDGE FECAL COLIFORM 176 MPNtg SLUDGE 26-Jan-24 PI TOTAL SOLIDS 6 91.6 % SLUDGE FECAL C00FORM 164 MPNIg SLUDGE 26-Jan-24 PI TOTAL SOLIDS 7 91.1 0/0 SLUDGE FECAL COLIFORM 190 MPNIg I $LUDGI~ 26-Jan-24 PI PAUL ISENHOUR, SUPERVISOR FEB/12/2024/MON 12:49 PM FAX No, P. 001/002 VVA'rER QUALITY SERVICES, INC. P.U, 130X 1102, BANNER I~LK, NC 28604 (a28) 89U-6277 fax (828) 898-6256 CHAIN OF CUSTgDY TpE SAMPLF— WASTEWATER DCATION: s 7~ r �CILITY ID #; . O WPLER NAME: 7- , DMPOS[TE SAMPLE, - AMPLE NAMEF ( PRI $ERVATION CODE - H2SO4, 2 - HNO3, 3 - HOL, 4 - NAOH, 5 - NONE, 0 � COOL ICE 7 - NA2S203, 8 - OTHER START TIME: 0 ; STOP TIME. ctintainem leaving the lab, unless ptherv,rl a ncted....�,,. CL.2-1)-CL2= Ohlorine check aflO dechlor"ation verification. -� :ESERVATION: COOL SIG: BOD, RESIDUE, CONDUCTIVITY, MBA$, COLOR, ALKALINITY, CR, VI, TURBIDITY COOL. 4C, PH<2 H2SO4: NH3, NO2-NO3, TKN, d xG, -fOC, COD, HARDNESS, PHENOLS, TOT PHOS, COOL 40, PH<2 HNO3 : METALS except OR, VI NONE: CHLORIDE, PH, FLUORIDE SAMPLE DEVIATION: `HER: COOL 4C, NA2S203 : COLIFORM BACTERIA Mgh' cduntu 6.1-9 B50SOHds Produced by the Town of Boone P.O. Drawer 192, Boone, NC 28607 High Country 6-1-0 (HC 610) Is a high organic content fertilizer manufactured by the Town of Boone Wastewater Treatment Facility. This product produces superior results on lawns, flower beds and shrubs providing nutrients at the rates indicated below: Guaranteed Analysis TotalNitrogen ......... ........................................... o Water Insoluble Nitrogen ......................................... 3.5% Avallable Phosphoric Acid ............................. /p n Soluble Potash .................. 1 Iron................................................................................. 1% Recommended Application Rates Lawn -Sod Establishment: Apply HC 610 at rate of 30 Ibs per 1000 sq feet. Turf Maintenance: 'Apply HC 610 at a rate of 10-15 lbs per 1000 sq feet. Plant Bed Establishment: Apply HC 610 at a rate of 2 lbs per 100 sq feet into soil. Planting Bed Maintenance: Apply HC 610 at a rate of 2 Ibs per 100 sq feet In Spring/Fall Warnings: HC 610- Is environmentally safe when used as directed, but can become a hazard If mismanaged. This product should not be used on soils intended for food crop production. ' Cover HC 610 with a tarp or plastic during transportation. Store HC 610 in a dry area away from wells or surface water where it could be washed into streams; keep product away from children's play areas. Limited Warranty and Disclaimer; The Town of Boone warrants that HC 610 meets the specifications stated above, and that the heavy metal content Is less than or equal to the limitations specified In the EPA and NC Dept of Environmental and Natural Resources sludge quality criteria for land application. If HC 610 fails to meet its specification, the buyer's sole remedy shall be the recovery of the purchase price. Under no circumstances shall the Town of Boone be liable for any other 'damages, including direct, indirect, consequential or special damages. The undersigned Buyer agrees to abide by the following Restrictions: HC 610 shall not be applied to land except In accordance with the instructions contained herein. HC 610 shall not be applied to any site that is flooded, frozen, or snow-covered. HC 610 shall not be applied within 100 feet: of any water supply, stream, river, or lake. Adequate measures shall be provided to prevent surface runoff from carrying this product into any surface waters. Buyer Signature Date Name (Print): Quantity: lbs/tons Street/Route: Intended Use:• City/State/Zip: Telephone: Amount Collected: Loaded By: Setback Rules for Land Applying Class A Biosolids Liquid Cake Private or public water supply source 100, 100, Surface waters such as intermittent and perennial streams, perennial Water bodies, and wetlands. 100' 25' Surface water diversions such as ephemeral streams, waterways, And ditches. 25' 0' Groundwater lowering ditches where the bottom of the ditch Intersects SHWA' 25' 0' Each well with exception of monitoring wells. 100, 100, Bedrock outcrops 25' 0 Bulk Class A residuals shall not be land applied under the following conditions; a. If the residuals are to adversely affect a threatened or endangered species listed under section 4 of the Endangered Species Act or its designated critical habitat; b. If the application causes nuisance conditions; c. If the land fails to assimilate the bulk residuals or the application causes the contravention of surface water or groundwater standards; d. if the land is flooded, frozen, or snow-covered, or is otherwise in a condition such that runoff of the residuals would occur; e. Within the 100-year flood elevation, Unless the residuals are injected or incorporated within a 24-hour period following a residuals land application event; f. During precipitation events, or within 24 hours following a rainfall event of 0.5 inches or greater in a 24-hour period; g. If the slope of the land is greater than 10% when liquid residuals are surfaced applied, or if the slope of the land is greater than 18% when liquid residuals are injected or incorporated; h. If the land does not have and established vegetative cover crop unless the land is a Division - approved no -till site, or the residuals are incorporated within a 24-hour period following the injection or application of residuals; L If the vertical separation of the seasonal high water table and the depth of residuals application is less than a foot; j. If the vertical separation of the depth to bedrock and the depth of residuals is less than one foot; k. If the application exceeds agronomic rates; or 1. If the land application sites are located within a WS-I watershed pursuant to 15A NCAC 02B.0212 or within the Critical Area of a WS-II pursuant to sub-item(4)(g) of rule 15A NCAC 028. 0212 or within Critical Area of WS-111 or WS-IV watershed pursuant to sub -item (4)(h) of rules 15A NCAC 02B .0215, and .0216. ©69113 STKOK05 06/16/202207'.53 -3910, 176158 DATE DESCRIPTION INV / PO AMOUNT 04/22/2024 APPLICATION PERMIT RENEWAL 04/22/24-N 348.00 TOTAL 348.00 11'176L5811" I:06?OLL7601: 4L«1400253911,