WQ0004972_Monitoring - 03-2024_20240430

Monitoring Report Submittal
Permit Number#* WQ0004972
Name of Facility:* Forest Lake RV WWTP
Month: * March Year: * 2024
Report Information
Type* Upload Document*
GW-59 2024_March_WQ0004972 GW-59 and 59a.pdf 1.83MB
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59).
Confirmation Email Address: * [e-mail]
Name of Submitter: * Amanda Grenier
Signature:
Date of submittal: 4/30/2024
This will be filled in automatically
Initial Review
Reviewer: Wanda.Gerald

Is the project number correct?* WQ0004972
Is the monitoring report accepted?* Yes No
Regional Office* Winston-Salem
Reviewer: _anonymous
Review Date: 5/20/2024

DocuSign Envelope ID: 66DE6EAF-E5EC-410E-BCF2-A2AC3BBF8424
SUBMIT FORM ON YELLOW PAPER ONLY
• •
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
• •
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 10/31/2027
Facility Name: Forest Lake RV WWTP
Non -Discharge WQ0004972 UIC
Permit Name (if different):
NPDES Other
Facility Address: 192 Thousand Trails Dr.
TYPE OF PERMITTED OPERATION BEING MONITORED
Advance NC
27006
County Davie
❑ Lagoon ❑ Remediation: Infiltration Gallery
❑■ Spray Field ❑ Remediation:
Contact Person: Amanda Grenier
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Forest Lake RV Spray Irrigation Field
No. of wells to be sampled: 4
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): 1
Date sample collected: 3/13/2024
FIELD ANALYSES:
WAS
Well Depth: 90.7 ft.
Well Diameter: 2 in.
pH 00400: 5.55 units Temp. 000lo: 14.9 °C
DRY at
Depth to Water Level 82546:65 ft. below measuring point
Screened Interval: ft.
to
ft. Spec. Cond. 00094: 70.7 µMhos
time of
sampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation:
ft.
Odor 00085: None
check
Volume of water pumped/bailed before sampling:
4.5
gallons
Appearance Clear
here:❑
Samples for metals were collected unfiltered: ❑ YES
❑■ NO and field acidified: ❑ YES ❑■ NO
LABORATORY INFORMATION
Date sample analyzed: 3/13/2024
Laboratory Name: Pace Analytical
Certification No. 12
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 2.0
/100mL
Nitrate (NO3) as N 00620 0.12
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL Phosphorus: Total as P 00665 <0.05
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300
mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 6.4
units
Ba - Barium 01007
ug/L
TOC 0068o 2.9
mg/L
Ca - Calcium 00916
mg/L
Chloride 0094o 2.6
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method #
Total Ammonia oo610 <0.10
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
George Gudgeon, Sr. Vice President
Permittee (or Authorized Aqent) Name and Title - Please print or type
nature of Permittee (or Authorized Aqent)
4/29/2024 1 8:49 AM PDT
(Date
GW-59 Rev.06-07-2018

DocuSign Envelope ID: 66DE6EAF-E5EC-410E-BCF2-A2AC3BBF8424
SUBMIT FORM ON YELLOW PAPER ONLY
• •
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
• •
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 10/31/2027
Facility Name: Forest Lake RV WWTP
Non -Discharge WQ0004972 UIC
Permit Name (if different):
NPDES Other
Facility Address: 192 Thousand Trails Dr.
TYPE OF PERMITTED OPERATION BEING MONITORED
Advance NC
27006
County Davie
❑ Lagoon ❑ Remediation: Infiltration Gallery
0 Spray Field ❑ Remediation:
Contact Person: Amanda Grenier
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Forest Lake RV Spray Irrigation Field
No. of wells to be sampled: 4
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): 2
Date sample collected: 3/13/2024
FIELD ANALYSES:
WAS
Well Depth: 46 ft.
Well Diameter: 2 in.
pH 00400: 5.58 units Temp. 000lo: 1 5.3 °C
DRY at
Depth to Water Level 82546:38.5 ft. below measuring point
Screened Interval: ft.
to
ft. Spec. Cond. 00094: 51.6 µMhos
time of
sampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation:
ft.
Odor 00085: None
check
Volume of water pumped/bailed before sampling:
2
gallons
Appearance Clear
here:❑
Samples for metals were collected unfiltered: ❑ YES
❑■ NO and field acidified: ❑ YES ❑■ NO
LABORATORY INFORMATION
Date sample analyzed: 3/13/2024
Laboratory Name: Pace Analytical
Certification No. 12
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 8.0
/100mL
Nitrate (NO3) as N 00620 0.45
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL Phosphorus: Total as P 00665 0.059
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300
mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 6.1
units
Ba - Barium 01007
ug/L
TOC 00680 <1
mg/L
Ca - Calcium 00916
mg/L
Chloride 0094o 3.0
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method #
Total Ammonia oo610 <0.1
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
George Gudgeon, Sr. Vice President
Permittee (or Authorized Aqent) Name and Title - Please print or type
4/29/2024 1 8:49 AM PDT
Siqnature of Permittee (or Authorized Aqent) (Date)
GW-59 Rev.06-07-2018

DocuSign Envelope ID: 66DE6EAF-E5EC-410E-BCF2-A2AC3BBF8424
SUBMIT FORM ON YELLOW PAPER ONLY
• •
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
• •
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 10/31/2027
Facility Name: Forest Lake RV WWTP
Non -Discharge WQ0004972 UIC
Permit Name (if different):
NPDES Other
Facility Address: 192 Thousand Trails Dr.
TYPE OF PERMITTED OPERATION BEING MONITORED
Advance NC
27006
County Davie
❑ Lagoon ❑ Remediation: Infiltration Gallery
0 Spray Field ❑ Remediation:
Contact Person: Amanda Grenier
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Forest Lake RV Spray Irrigation Field
No. of wells to be sampled: 4
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): 3
Date sample collected: 3/13/2024
FIELD ANALYSES:
WAS
Well Depth: 20.3 ft.
Well Diameter: 2 in.
pH 00400: 4.85 units Temp. 000lo: 1 2.4 °C
DRY at
Depth to Water Level 82546:7 ft. below measuring point
Screened Interval: ft.
to
ft. Spec. Cond. 00094: 207 µMhos
time of
sampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation:
ft.
Odor 00085: None
check
Volume of water pumped/bailed before sampling:
2.5
gallons
Appearance Clear
here:❑
Samples for metals were collected unfiltered: ❑ YES
❑■ NO and field acidified: ❑ YES ❑■ NO
LABORATORY INFORMATION
Date sample analyzed: 3/13/2024
Laboratory Name: Pace Analytical
Certification No. 12
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 39.0
/100mL
Nitrate (NO3) as N 00620 13.3
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL Phosphorus: Total as P 00665 0.19
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300
mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 5.3
units
Ba - Barium 01007
ug/L
TOC 00680 <1
mg/L
Ca - Calcium 00916
mg/L
Chloride 0094o 27.2
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method #
Total Ammonia oo610 <0.1
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
George Gudgeon, Sr. Vice President
Permittee (or Authorized Aqent) Name and Title - Please print or type
Siqnature of Permittee (or Authorized Aqent) (Date)
PDT
GW-59 Rev.06-07-2018

DocuSign Envelope ID: 66DE6EAF-E5EC-410E-BCF2-A2AC3BBF8424
SUBMIT FORM ON YELLOW PAPER ONLY
• •
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
• •
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 10/31/2027
Facility Name: Forest Lake RV WWTP
Non -Discharge WQ0004972 UIC
Permit Name (if different):
NPDES Other
Facility Address: 192 Thousand Trails Dr.
TYPE OF PERMITTED OPERATION BEING MONITORED
Advance NC
27006
County Davie
❑ Lagoon ❑ Remediation: Infiltration Gallery
❑■ Spray Field ❑ Remediation:
Contact Person: Amanda Grenier
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Forest Lake RV Spray Irrigation Field
No. of wells to be sampled: 4
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): 4
Date sample collected: 3/13/2024
FIELD ANALYSES:
WAS
Well Depth: 39 ft.
Well Diameter: 2 in.
pH 00400: 5.46 units Temp. 000lo: 1 3.7 °C
DRY at
Depth to Water Level 82546:29.6 ft. below measuring point
Screened Interval: ft.
to
ft. Spec. Cond. 00094: 87.9 µMhos
time of
sampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation:
ft.
Odor 00085: None
check
Volume of water pumped/bailed before sampling:
1.5
gallons
Appearance Clear
here:❑
Samples for metals were collected unfiltered: ❑ YES
❑■ NO and field acidified: ❑ YES ❑■ NO
LABORATORY INFORMATION
Date sample analyzed: 3/13/2024
Laboratory Name: Pace Analytical
Certification No. 12
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 2.8
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL Phosphorus: Total as P 00665 0.10
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300
mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 6.6
units
Ba - Barium 01007
ug/L
TOC 00680 <1
mg/L
Ca - Calcium 00916
mg/L
Chloride 0094o 6.9
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method #
Total Ammonia oo610 <0.1
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
George Gudgeon, Sr. Vice President
Permittee (or Authorized Aqent) Name and Title - Please print or type
4/29/2024 1 8:49 AM PDT
Siqnature of Permittee (or Authorized Aqent) (Date)
GW-59 Rev.06-07-2018

GW-59A COMPLIANCE POR Permit # WQ0004972
(Submit one each monitoring period with GW 59 forms,)
1
Enter date monitoring results were due. (4/3O/24 ) Will this monitoring report (GW-59 and GW-59A)
YES
NO
be submitted after the established due date?
X
2
Was any required information missing on the GW-59 report forms?
YES
NO
IF the answer to question I or 2 is "YES", list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
X
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Office for guidance.
X
4
Are any monitored constituents equal to or above the established standards?
YES
NO
If the answer to question 4 is "NO", skip to section 8.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the space provided below:
MW #1 field pH was 5.6, lab pH 6.4. MW #2 field pH was 5.6, lab pH 6.1. MW #3 field pH was 4.9,
lab pH 5.3 and nitrate was 13.3 mg/I. MW #4 field pH was 5.5, lab pH 6.6.
X
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
YES
NO
same constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is "NO", skip to section 8.
If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years).
Yes, DEQ is aware and have expressed concerns about the well.
X
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
If the answer is "YES", a groundwater quality problem maybe occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells maybe improperly
located, contact the Regional Office.
7
Is the permittee implementing previously approved actions required by the Division involving this
YES
NO
groundwater quality problem?
If the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 7 is "NO", contact the Regional Office within 90 days, an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation,
fines, and/or penalties.
8
The person completing this portion (GIN--59A) of the monitoring report should sign below and submit this
form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby acknowledge that the above information was evaluated and the information ''submitted in this
report (Compliance Report;GW-59A) is true and complete to the best of my knowledge.
-41t- ' 41\ 4/30/24
Signature of Permittee (or Authorized Agent) Date
Gib-59A 12/8/2003

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
March 27, 2024
Amanda D. Grenier
Greener EHS Solutions
21 Selby Ct.
Holly Springs, NC 27540
RE: Project: Forest Lake - MW's March
Pace Project No.: 92718838
Dear Amanda Grenier:
Enclosed are the analytical results for sample(s) received by the laboratory on March 13, 2024. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
704-977-0942
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 21

ace
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: Forest Lake - MW's March
Pace Project No.: 92718838
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 21

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Forest Lake - MW's March
92718838
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92718838001
MW # 1
SM 9222D-2015
KDF
1
PASI-C
EPA 9040C
YEG
1
PASI-A
EPA 350.1 Rev 2.0 1993
NCF
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 365.1 Rev 2.0 1993
Zip
1
PASI-A
SM 4500-CI-E-2011
MMA
1
PASI-A
SM 531OB-2014
MJP
1
PASI-A
92718838002
MW # 2
SM 9222D-2015
KDF
1
PASI-C
EPA 9040C
YEG
1
PASI-A
EPA 350.1 Rev 2.0 1993
NCF
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 365.1 Rev 2.0 1993
Zip
1
PASI-A
SM 4500-CI-E-2011
MMA
1
PASI-A
SM 531OB-2014
MJP
1
PASI-A
92718838003
MW # 3
SM 9222D-2015
KDF
1
PASI-C
EPA 9040C
YEG
1
PASI-A
EPA 350.1 Rev 2.0 1993
NCF
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 365.1 Rev 2.0 1993
Zip
1
PASI-A
SM 4500-CI-E-2011
MMA
1
PASI-A
SM 531OB-2014
MJP
1
PASI-A
92718838004
MW # 4
SM 9222D-2015
KDF
1
PASI-C
EPA 9040C
YEG
1
PASI-A
EPA 350.1 Rev 2.0 1993
NCF
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 365.1 Rev 2.0 1993
Zip
1
PASI-A
SM 4500-CI-E-2011
MMA
1
PASI-A
SM 531OB-2014
MJP
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 21

ANALYTICAL RESULTS
Project: Forest Lake - MW's March
Pace Project No.: 92718838
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW # 1 Lab ID: 92718838001 Collected: 03/13/24 09:20 Received: 03/13/24 12:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Charlotte
Fecal Coliforms
2.0 CFU/100 mL 1.0
1
03/13/24 16:08 03/14/24 14:09
9040 pH
Analytical Method: EPA 9040C
Pace Analytical Services -Asheville
pH at 25 Degrees C
6.4 Std. Units 0.10
1
03/25/24 13:29
H3
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg/L 0.10
1
03/22/24 16:35
7664-41-7
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
0.12 mg/L 0.020
1
03/14/24 01:26
14797-55-8
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
ND mg/L 0.050
1
03/26/2414:31 03/27/2410:54
7723-14-0
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride
2.6 mg/L 1.0
1
03/22/24 21:14
16887-00-6
5310B TOC
Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon
2.9 mg/L 1.0
1
03/19/24 04:15
7440-44-0
Date: 03/27/2024 04:15 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 21

ANALYTICAL RESULTS
Project: Forest Lake - MW's March
Pace Project No.: 92718838
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW # 2 Lab ID: 92718838002 Collected: 03/13/24 10:15 Received: 03/13/24 12:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Charlotte
Fecal Coliforms
8.0 CFU/100 mL 1.0
1
03/13/24 16:08 03/14/24 14:09
9040 pH
Analytical Method: EPA 9040C
Pace Analytical Services -Asheville
pH at 25 Degrees C
6.1 Std. Units 0.10
1
03/25/24 13:33
H3
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg/L 0.10
1
03/22/24 16:36
7664-41-7
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
0.45 mg/L 0.020
1
03/14/24 01:37
14797-55-8
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
0.059 mg/L 0.050
1
03/26/2414:31 03/27/2411:02
7723-14-0
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride
3.0 mg/L 1.0
1
03/22/24 21:15
16887-00-6
5310B TOC
Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon
ND mg/L 1.0
1
03/19/24 05:52
7440-44-0
Date: 03/27/2024 04:15 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 21

ANALYTICAL RESULTS
Project: Forest Lake - MW's March
Pace Project No.: 92718838
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW # 3 Lab ID: 92718838003 Collected: 03/13/24 10:35 Received: 03/13/24 12:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Charlotte
Fecal Coliforms
39.0 CFU/100 mL 1.0
1
03/13/24 17:13 03/14/24 15:20
9040 pH
Analytical Method: EPA 9040C
Pace Analytical Services -Asheville
pH at 25 Degrees C
5.3 Std. Units 0.10
1
03/25/24 13:38
H3
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg/L 0.10
1
03/22/24 16:38
7664-41-7
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
13.3 mg/L 0.10
5
03/14/24 02:07
14797-55-8
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
0.19 mg/L 0.050
1
03/26/2414:31 03/27/2411:03
7723-14-0
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride
27.2 mg/L 1.0
1
03/22/24 21:16
16887-00-6
5310B TOC
Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon
ND mg/L 1.0
1
03/19/24 06:48
7440-44-0
Date: 03/27/2024 04:15 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 21

ANALYTICAL RESULTS
Project: Forest Lake - MW's March
Pace Project No.: 92718838
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW # 4 Lab ID: 92718838004 Collected: 03/13/24 11:00 Received: 03/13/24 12:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Charlotte
Fecal Coliforms
ND CFU/100 mL 1.0
1
03/13/24 17:31 03/14/24 16:19
9040 pH
Analytical Method: EPA 9040C
Pace Analytical Services -Asheville
pH at 25 Degrees C
6.6 Std. Units 0.10
1
03/25/24 13:47
H3
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg/L 0.10
1
03/22/24 16:39
7664-41-7
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
2.8 mg/L 0.020
1
03/14/24 01:42
14797-55-8
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
0.10 mg/L 0.050
1
03/26/2414:31 03/27/2411:05
7723-14-0
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride
6.9 mg/L 1.0
1
03/22/24 21:19
16887-00-6
5310B TOC
Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon
ND mg/L 1.0
1
03/19/24 07:06
7440-44-0
Date: 03/27/2024 04:15 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 21

QUALITY CONTROL DATA
Project: Forest Lake - MW's March
Pace Project No.: 92718838
QC Batch: 838808 Analysis Method: SM 9222D-2015
QC Batch Method: SM 9222D-2015 Analysis Description: 9222D Fecal Coliform(MF) - CHT
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92718838003
METHOD BLANK: 4332967 Matrix: Water
Associated Lab Samples: 92718838003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms CFU/100 mL ND 1.0 03/14/24 15:20
SAMPLE DUPLICATE: 4332968
Parameter
Fecal Coliforms
92718697001 Dup
Units Result Result RPD Qualifiers
CFU/100 mL ND ND
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2024 04:15 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 21

QUALITY CONTROL DATA
Project: Forest Lake - MW's March
Pace Project No.: 92718838
QC Batch: 838810 Analysis Method: SM 9222D-2015
QC Batch Method: SM 9222D-2015 Analysis Description: 9222D Fecal Coliform(MF) - CHT
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92718838004
METHOD BLANK: 4332971 Matrix: Water
Associated Lab Samples: 92718838004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms CFU/100 mL ND 1.0 03/14/24 16:19
SAMPLE DUPLICATE: 4332972
Parameter
Fecal Coliforms
92718838004 Dup
Units Result Result RPD Qualifiers
CFU/100 mL ND ND
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2024 04:15 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 21

QUALITY CONTROL DATA
Project: Forest Lake - MW's March
Pace Project No.: 92718838
QC Batch: 839033 Analysis Method: SM 9222D-2015
QC Batch Method: SM 9222D-2015 Analysis Description: 9222D Fecal Coliform(MF) - CHT
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92718838001, 92718838002
METHOD BLANK: 4334023 Matrix: Water
Associated Lab Samples: 92718838001, 92718838002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms CFU/100 mL ND 1.0 03/14/24 14:09
SAMPLE DUPLICATE: 4334024
Parameter
Fecal Coliforms
92718787004 Dup
Units Result Result RPD Qualifiers
CFU/100 mL ND ND
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2024 04:15 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 21

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Forest Lake - MW's March
Pace Project No.: 92718838
QC Batch: 841527 Analysis Method: EPA 9040C
QC Batch Method: EPA 9040C Analysis Description: 9040 pH
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92718838001, 92718838002, 92718838003, 92718838004
SAMPLE DUPLICATE: 4346415
92719722001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 8.4 8.4 0 H3
SAMPLE DUPLICATE: 4346416
92719722002 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 3.9 3.9 0 H3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2024 04:15 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 21

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Forest Lake - MW's March
Pace Project No.: 92718838
QC Batch: 840810 Analysis Method: EPA 350.1 Rev 2.0 1993
QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92718838001, 92718838002, 92718838003, 92718838004
METHOD BLANK: 4342688
Matrix:
Water
Associated Lab Samples: 92718838001, 92718838002, 92718838003, 92718838004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Nitrogen, Ammonia
mg/L
ND
0.10
03/22/24 15:57
LABORATORY CONTROL SAMPLE:
4342689
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Nitrogen, Ammonia
mg/L
5
5.1
103 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4342690 4342691
MS MSD
92718779003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/L 0.053J 5 5 5.2 5.2 103 103 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4342692 4342693
MS MSD
92718779004 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/L 4.0 5 5 8.9 8.8 97 97 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2024 04:15 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 21

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Forest Lake - MW's March
Pace Project No.: 92718838
QC Batch: 838845 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92718838001, 92718838002, 92718838003, 92718838004
METHOD BLANK: 4333241
Matrix:
Water
Associated Lab Samples: 92718838001, 92718838002, 92718838003, 92718838004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Nitrogen, Nitrate
mg/L
ND
0.020
03/14/24 01:06
LABORATORY CONTROL SAMPLE:
4333242
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Nitrogen, Nitrate
mg/L
1.5
1.6
110 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4333245 4333246
MS MSD
92718838001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Nitrate mg/L 0.12 1.5 1.5 1.7 1.7 107 106 90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4333277 4333278
MS MSD
92718516001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Nitrate mg/L <0.020 1.5 1.5 1.6 1.6 105 105 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2024 04:15 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 21

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Forest Lake - MW's March
Pace Project No.: 92718838
QC Batch: 841618 Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92718838001, 92718838002, 92718838003, 92718838004
METHOD BLANK: 4346933
Matrix:
Water
Associated Lab Samples: 92718838001, 92718838002, 92718838003, 92718838004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Phosphorus
mg/L
ND
0.050
03/27/2410:32
LABORATORY CONTROL SAMPLE:
4346934
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Phosphorus
mg/L
2.5
2.5
99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4346935 4346936
MS MSD
92718818001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/L 5.8 2.5 2.5 8.1 8.0 90 88 90-110 1 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4346937 4346938
MS MSD
92718838001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/L ND 2.5 2.5 2.5 2.5 100 99 90-110 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2024 04:15 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 21

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Forest Lake - MW's March
Pace Project No.: 92718838
QC Batch: 841264 Analysis Method: SM 4500-CI-E-2011
QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92718838001, 92718838002, 92718838003, 92718838004
METHOD BLANK: 4345359
Matrix:
Water
Associated Lab Samples: 92718838001, 92718838002, 92718838003, 92718838004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Chloride
mg/L
ND
1.0
03/22/24 21:06
LABORATORY CONTROL SAMPLE:
4345360
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Chloride
mg/L
20
20.7
104 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4345361 4345362
MS MSD
92719121001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chloride mg/L 18.9 10 10 30.2 30.2 113 113 90-110 0 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2024 04:15 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 21

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Forest Lake - MW's March
Pace Project No.: 92718838
QC Batch: 839726 Analysis Method: SM 531 OB-2014
QC Batch Method: SM 531 OB-2014 Analysis Description: 5310E TOC
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92718838001, 92718838002, 92718838003, 92718838004
METHOD BLANK: 4337489
Matrix:
Water
Associated Lab Samples: 92718838001, 92718838002, 92718838003, 92718838004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Total Organic Carbon
mg/L
ND
1.0
03/19/24 01:52
LABORATORY CONTROL SAMPLE:
4337490
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Total Organic Carbon
mg/L
25
24.2
97 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4337491 4337492
MS MSD
92718838001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Total Organic Carbon mg/L 2.9 25 25 27.3 27.4 98 98 90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4337493 4337494
MS MSD
92718838002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Total Organic Carbon mg/L ND 25 25 24.7 24.7 99 99 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2024 04:15 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 21

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: Forest Lake - MW's March
Pace Project No.: 92718838
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2024 04:15 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 21

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Forest Lake - MW's March
92718838
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92718838001
MW #1
SM 9222D-2015
839033
SM 9222D-2015
839035
92718838002
MW # 2
SM 9222D-2015
839033
SM 9222D-2015
839035
92718838003
MW # 3
SM 9222D-2015
838808
SM 9222D-2015
838809
92718838004
MW # 4
SM 9222D-2015
838810
SM 9222D-2015
838811
92718838001
MW #1
EPA 9040C
841527
92718838002
MW # 2
EPA 9040C
841527
92718838003
MW # 3
EPA 9040C
841527
92718838004
MW # 4
EPA 9040C
841527
92718838001
MW # 1
EPA 350.1 Rev 2.0 1993
840810
92718838002
MW # 2
EPA 350.1 Rev 2.0 1993
840810
92718838003
MW # 3
EPA 350.1 Rev 2.0 1993
840810
92718838004
MW # 4
EPA 350.1 Rev 2.0 1993
840810
92718838001
MW # 1
EPA 353.2 Rev 2.0 1993
838845
92718838002
MW # 2
EPA 353.2 Rev 2.0 1993
838845
92718838003
MW # 3
EPA 353.2 Rev 2.0 1993
838845
92718838004
MW # 4
EPA 353.2 Rev 2.0 1993
838845
92718838001
MW # 1
EPA 365.1 Rev 2.0 1993
841618
EPA 365.1 Rev 2.0 1993
841919
92718838002
MW # 2
EPA 365.1 Rev 2.0 1993
841618
EPA 365.1 Rev 2.0 1993
841919
92718838003
MW # 3
EPA 365.1 Rev 2.0 1993
841618
EPA 365.1 Rev 2.0 1993
841919
92718838004
MW # 4
EPA 365.1 Rev 2.0 1993
841618
EPA 365.1 Rev 2.0 1993
841919
92718838001
MW #1
SM 4500-CI-E-2011
841264
92718838002
MW # 2
SM 4500-CI-E-2011
841264
92718838003
MW # 3
SM 4500-CI-E-2011
841264
92718838004
MW # 4
SM 4500-CI-E-2011
841264
92718838001
MW #1
SM 5310B-2014
839726
92718838002
MW # 2
SM 5310E-2014
839726
92718838003
MW # 3
SM 5310E-2014
839726
92718838004
MW # 4
SM 5310E-2014
839726
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/27/2024 04:15 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 21

Iace DC#_Title: ENV-FRM-HUN1-0083 v03_Samp1e Condition Upon Receipt
Effective Date: 11/29/202-3 4:16:30 PM
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersvill& Raleigh❑ Mechanicsville❑ Atlanta❑ Kernersville❑
ConditionSample Client Name: rWo# : 92718838
Upon Receipt �61 � Project #:
iC u 1 O v15
Courier. ed Ex UPS LISPS Ll Client 111111111111
II II
92
❑ Commercial Pace ❑ Other: 111111111
Custody Seal Present? ❑Yes 53No Seals Intact? El Yes No �N/A Date/Initials Person Examining Contents:L18ar,
Iy
Packing Material: ❑ Bubble Wrap Ll Bubble Bags ❑ None ❑ Other
Thermo m Eter:
�I IR Gun ID: quo�6 Type of Ice: tL.l Wet ❑ Blue
Q•3 Correction Factor:
Cooler Temp: Add/Subtract (°C)
Cooler Temp Corrected (° 3
USDA Regulated Soil ( L"J N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC
(check maosl? ❑ Yes ❑ No
Biological Tissue zen?
❑ Yes ❑ No N/A
❑ None
Temp should be above freezing to 6°C
❑ Samples out of temp criteria. Samples on ice, cooling process
has begun
Did samples originate from a foreign source (internationally,
including Hawaii and Puerto Rico)? ❑Yes ❑ No
Comments/Discrepancy:
Chain of Custody Present?
Yes
❑ No
:1 N/A
1.
Samples Arrived within Hold Time?
EfYes
❑ No
❑ N/A
2.
Short Hold Time Analysis (<72 hr.)?
Yes
❑ No
❑ N/A
3.
Rush Turn Around Time Requested?
0
No
❑N/A
4.
Sufficient Volume?
0Yes
fJ Yes
❑ No
❑ N/A
5.
Correct Containers Used?
-Pace Containers Used?
,.Yes
J Yes
Y
❑ No
❑ No
❑ N/A
❑ N/A
6.
Containers Intact?
Yes
❑ No
❑ N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
ffNo
❑ N/A
B.
Sample Labels Match COC7
-Includes Date Rme/ID/Analysis Matrix:
es
❑ No
❑ N/A
9.
Headspace in VOA Vials (>5-bmm)?
❑Yes
❑No
9 ltvA
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑ Yes
❑ Yes
❑ No
❑ No
N/A
EK/A
11.
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Lot ID of split containers:
Date/Time:
Date:
Date:
Field Data Required? U Yes U No
Qualtrax ID: 69614 Paae 1 of 2 Page 19 of 21

— Effective Date: 11/14/2022
`Check mark top half of box if pH and/or dechlorination is verified and
within the acceptance range far preservation samp es.
Exceptions: VOA, Coliform, TOC, Oil and Grease, ORO/8015 (water) DOC. LLHC
**Bottom half of box is to list number of bottles
""Check all unpreserved Nitrates for chlorine
- I
Project tf WOE: 92718838 _
PM: MWB Due Date: 03/27/24
CLIENT: 92-Greener
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pH Adjustment Log for Preserved Samples - T
Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservaAcn Amount of Preservative Lot q
adjusted J added
Note Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form %vill be sent to the Plorth Carolna DENR Cert
Out of hold, incorrect preservative, out el letup, incorrect containers.
Qualtrax ID. 6961.1
Pacle 2 of 2
uon Oihrr, (r
Page 20 of 21

Pace® Location Requested (City/State):
Pace Analytical Charlotte CHAIN -OF -CUSTODY Analytical Request Document
ace (Il9800 Kincey Ave. Suite 100, Huntersville, NC 28078 Chain-af-Custody is a LEGAL DOCUMENT - Complete all relevant fields
LAB USE ONLY- Affix Workorder/Login Label Here
"0 N
3, UN
O)
m
CL
Scan QR Code for instructions
Company Name: Greener EHS Solutions
Street Address: 192 Thousand Trail Dr., Advance, NC 27006
Customer Project R: 1
Project Name: _ Forest Lake- MW'sMarch 4
Site Collection Info/Facility ID (as applicable):
Contact/Report To: Amanda Grenief
Phone 11: [phone]
E-Mail:
Cc E-Mail:
Specify Container Size ••
"Container Size it) 3L, (2) 500mt, (3) 25Om1, (4)
Ternst,(5)9)90m(6{40trial,(7)Encore,(g{ -
TerraCore, (9) 90m1, 110) Other
InvoieeToa
Invoice E-Mail:
Purchase Order It (if
applicable):
Quote q:
Identify Container Preservative Type"•
" Preservative Types: (3) None, (2) HNO3, (3)
H2So4, (4) HCI, (5) NaOH, (6) Zn Acetate, 171
NaH504, (8) Sod. Thiosulfale, (9) Ascorbic Acid, (SO)
McOH, (11) Other
Analysis Requested
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Prat. Mgr:
Matthew Brainard
`
-
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Time Zone Collected: [ ] AK PT
[ J [ ] MT [ ] CT [ JET
County /State origin of sample(s): North Carolina
Data Deliverables:
[ J Level II [ J Level III [ ] Level IV
[ ] EQUIS
Other
Regulatory Program JDW, RCRA, etc.) as applicable: Reportable [ ] Yes [ ]No
AcctNum / Client to:
c
Rush ( pproval required):
Pre -a
I I Same Day [ ] 1 Day [ J 2 Day [ J 3 Day [ J Other
DW PWSID R or W W Permit q as applicable:
Ou Table q:
j
Date Results
Requested:
Field Filtered (if applicable): [ ] Yes [ J No
Analysis-.
q Profile / Template:
14849-9
= E
0 "
• Matrix Codes (Insert in Matrix box below): Drinking Water (OW), Ground Water (GW), Waste Water (WW), Product (P), Soil Solid (SS), Oil (OL), Wipe JWP), Tissue [TS), Bioassay
B , Vapor V , Surface Water SW ,Sediment SED Sludge 51., Caulk CK , Leachate LL , Biosolid BS , Other 07
Prelog /Bottle Ord. 10:
1114239
Customer Sample ID
Matrix •
Comp /
Grab
Composite Start
Collected or Composite End
q
Cont.
Res. Chlorine
r_1
Sample Comment
Date
Time
Date
Time
Results
Units
Z
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5
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Additional Instructions from Pace":
Collected By:
(Printed Name
Signature'
Customer Remarks / Special Conditions / Possible Hazards:
R Coolers: ThgDnometer ID: Correcuti jactc r I'Q: Obs. Temp, (-C) Ccin"dT, p. ('CI On Ice:
\//)
Rellequlshed by/Company) ISlgnalure)
Date/Time:
Received by/ �gnalure)
Date/Time: _
TracFing Number.
Relinquished by/Com nyj(Signature)
/1
C
Date/Time:
31131 �l � �
Received /C panY (Si nature)
E` _ ��
Date/T, '\
� l�
Delivered by: [ ] In -Person j Courier
Rebnquhh y/Company: (Signature)
Dale�me:
Received by/Company: (signature)
Date/Ti e.
[ J FedEX [ J UPS [ ]Other
Relinquished by/Companyl (Signature)
Date/Time:
Received by/Company: ISignature)
Date/Time:
Page: of
Submitting a sample via this chain of custody constitutes acknowledgment and acceptance of the Pace* Terms and Conditions found at https://www.pacelabs.com/resource-library/resource/pace-terms-and-conditions/ ENV+RM-G0RQ-0019_v02_110123 U