NC0026051_Pretreatment_Annual_Report_Revised_20240520

DocuSign Envelope ID: 2E712117-91C9-46C2-BFOC-FA96832036A1
Pretreatment Annual Report
POTW: Durham County Triangle WWTP
NPDES #: NCO026051
WWTP: Triangle Wastewater Treatment Plant
Reporting Period: January 1, 2023 to December 31, 2023
Person to contact
Regarding this report: Amy Moore
Phone #: [phone]
I certify that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel
properly gather and evaluate the information submitted. Based upon my inquiry of the
person or persons who manage the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and
belief, true, accurate and complete.
Docu((Signed by:
�TipU.AJMt, 2/26/2024
Step anie rixey_ I Date
Deputy Director of E&ES/POTW Director

Pretreatment Annual Report
POTW: Durham County Triangle WWTP
NPDES #: NC0026051
WWTP: Triangle Wastewater Treatment Plant
Reporting Period: January 1, 2023 to December 31, 2023
Person to contact
Regarding this report: Amy Moore
Phone #: [phone]
I certify that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel
properly gather and evaluate the information submitted. Based upon my inquiry of the
person or persons who manage the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and
belief, true, accurate and complete.
JnuxI 2
Amy M o e Date
Laboratory & Compliance Manager

DURHAM COUNTY
2023 PRETREATMENT ANNUAL REPORT
NARRATIVE
GENERAL PROGRAM INFORMATION:
Durham County submitted revisions to the Enforcement Response Plan (ERP) on
February 11, 2020, in response to the Dental Amalgam Rule, that was approved February
13, 2020. Durham County submitted a revision of the Long -Term Monitoring Plan
(LTMP) to the Division on September 5, 2013, that was approved by the Division on
October 8, 2013. Durham County submitted a revision of the Sewer Use Ordinance
(SUO) to the Division on December 18, 2012. A letter was received from the Division
on January 28, 2013, requesting additional information. The additional information was
submitted March 21, 2013, and approved by the Division on April 3, 2013. The
Industrial Waste Survey (IWS) was submitted to the Division on March 31, 2021. The
Division requested additional information that was submitted on May 3, 2021. The IWS
was approved by the Division on May 5, 2021. Durham County submitted a revision of
the Headwork's Analysis (HWA) on March 30, 2023, that has not been approved by the
Division. The current allocation table is a revision of the HWA that was submitted on
March 16, 2018, and approved on May 2, 2018.
A copy of the "Pretreatment Program Info Database" is included. Information on the
database sheet needs the following corrections:
- The current fiscal year PCI was conducted July 11, 2023.
- The % Design mgd is SIU permitted is 15.62.
- The Permitted SIUflow (mgd) /Pt_SIU) is 1.875.
- The Durham County Pretreatment Program has 17 SIU's and 16 CIU's.
- The HWA was received by DWR on March 30, 2023.
GENERAL PERMIT INFORMATION:
During the reporting period the following Industrial User Permits were issued, modified,
or renewed:
• AstraZeneca, IUP DC-078 was modified with an effective date of December 18,
2023. The permit was received by the Division of Environmental Quality for
streamline review on December 18, 2023, and approved on January 10, 2024. The
modification added Pipe 002 for manufacturing line 3.
• Biogen, IUP DC-080 was modified with an effective date of August 1, 2023. The
permit was received by the Division for streamline review on August 3, 2023. The
Division requested additional Categorical parameters and limits be established per
40 CFR 439 Part C. Durham County submitted a draft revision to the Division on
February 2, 2024. The Division reviewed the draft and sent comments back to
Durham County on February 22, 2024. Due to the request by the Division to

modify the Biogen permit to include Subpart C, the draft permit is currently under
review by Biogen and comments are due to Durham County by April 21, 2024.
• Cree LED, IUP DC-125 was issued a permit with an effective date of July 1,
2023. Cree LED manufactures LED components and is considered Categorical
under 40 CFR 469 Electrical and Electronic Components Subpart D Luminescent
Materials. The permit was submitted to the Division for review on June 1, 2023.
The Division has not issued an approval letter to date.
• Eli Lilly & Company, IUP DC-119 was issued a permit with an effective date of
March 25, 2023. Eli Lilly manufactures pharmaceutical products and is
considered Categorical under 40 CFR 439 Pharmaceutical Manufacturing Subpart
D Mixing/Compounding and Formulation. The permit was submitted to the
Division for review on February 22, 2023, and approved by the Division on
March 22, 2023.
• MP Pharma, IJP DC-114 was terminated on December 15, 2023, as
pharmaceutical production no longer occurs at the site. A close out inspection of
the facility was conducted on December 5, 2023. The Division received the
termination letter on December 18, 2023, and approved on January 10, 2024.
• Phononic, IUP DC-075, was renewed with an effective date of March 7, 2023.
The renewal was submitted to the Division for streamline review on March 6,
2023, and approved by the Division on March 22, 2023. The permit was modified
with an effective date of April 1, 2023, to increase the monthly average flow to
0.035 MGD from 0.020 MGD. The permit modification was submitted to the
Division for streamline review on April 8, 2023. The Division has not issued an
approval letter to date.
• Tergus Pharma, IUP DC-115 was renewed with an effective date of December 27,
2023. The permit was received by the Division for streamline review on
December 18, 2023, and was approved on January 10, 2024.
• TriPharm Services, Inc., IUP DC-106 was modified with an effective date of
March 1, 2023. The permit was modified to increase the monthly average now to
0.008 MGD from 0.005 MGD. The permit modification was received by the
Division on February 22, 2023, and approved on March 13, 2023. The permit was
renewed with an effective date of October 18, 2023. The permit was received by
the Division for streamline review on October 10, 2023, and approved on
November 7, 2023.
• Wolfspeed 40 Moore, IUP DC-126 was issued with an effective date of July 7,
2023. Wolfspeed 40 Moore conducts semiconductor manufacturing by shaping,
cutting, grinding, and polishing silicon carbide wafers and is considered
Categorical under 40 CFR 469 Electrical and Electronic Components Subpart A
Semiconductor. The permit was submitted to the Division for approval on June 6,

2023. Durham County has not received a Division approval letter for the initial
permit to date. The permit was modified effective November 11, 2023. The
modification included a monthly average flow increase to 0.2975 MGD from
0.0565 MGD with a new process line discharging to Pipe 002. The modification
was submitted to the Division for streamline review on December 4, 2023, and
was approved on December 19, 2023.
SIU INFORMATION:
1. AstraZeneca (IUP DC-078) — AstraZeneca was issued a Notice of Violation on
November 30, 2023, for exceeding the monthly flow average for October 2023
and failure to notify Durham County of the exceedance. AstraZeneca was issued a
Notice of Violation on February 26, 2024, for exceeding the monthly flow
average for November and December 2023 and failure to notify Durham County
of the exceedance.
2. Aurobindo USA (IUP DC-089) — Aurobindo was issued a Notice of Violation on
May 31, 2023, for failure to sample low-level mercury in accordance with the
permit. Aurobindo conducted low-level mercury sampling on February 21, 2023,
and submitted the results on June 1, 2023, in response to the NOV.
3. Binen (IUP DC-080) — No permit violations occurred at this facility.
4. Cintas (IUP DC-037) — Cintas was issued a Notice of Violation on February 16,
2023, for failure to sample chloride for the second semi-annual period of 2022,
and failure to sample monthly for zinc and fluoride. The NOV was revised on
February 28, 2023, for zinc and fluoride as those parameters no longer require
monthly monitoring. Cintas was issued a Notice of Violation on September 11,
2023, for late reporting and failure to monitor biochemical oxygen demand, total
suspended solids, total nitrogen and total phosphorus in July 2023. The June 2023
flow and monitoring report was received August 23, 2023. Cintas did not make up
the missed sampling for July 2023 and is in Significant Noncompliance.
5. Cree LED (IUP DC-125) — No permit violations occurred at this facility.
6. Eli Lilly (IUP DC-119) —No permit violations occurred at this facility.
7. Micross (IUP DC-085) — No permit violations occurred at this facility.
8. MP Pharma Services (IUP DC-114) — MP Pharma was issued a Notice of
Violation on April 27, 2023, for late reporting. Monitoring results for samples
collected on February 15, 2023, were received on April 5, 2023. A response to the
NOV was received on May 1, 2023. MP Pharma stopped production in November
2023 and the permit was terminated on December 15, 2023.
9. Phononic (IUP DC-075) — No permit violations occurred at this facility.

10. PowerSecure (IUP DC-095) — PowerSecure was issued a Notice of Violation on
April 28, 2023, for late reporting. February monitoring results and flow were
submitted April 1, 2023. PowerSecure was issued a Notice of Violation on
February 26, 2024, for exceeding the monthly average flow in November 2023.
IL SCM Metal (IUP DC-005) — No permit violations occurred at this facility.
12. Term Pharma, IUP (DC-115) — Tergus Pharma was issued a Notice of
Violation on March 22, 2023, for late reporting. The flow report for January 2023
was received on March 1, 2023. Tergus Pharma was issued a Notice of Violation
on April 28, 2023, for late reporting. The flow report for February 2023 was
received on April 17, 2023. A Notice of Violation was issued on February 26,
2024, for exceeding the monthly average flow limit for July, August, September,
and October 2023.
13. TriPharm Services (IUP DC-106) — TriPharm Services was issued a Notice of
Violation on March 22, 2023, for late reporting. The flow for January 2023 was
received March 1, 2023. TriPharm Services was issued a Notice of Violation on
June 2, 2023, for late permit renewal application. The permit renewal application
was due on April 20, 2023, and received on May 31, 2023. TriPharm Services
was issued a Notice of Violation for late reporting on August 25, 2023.
Monitoring results for February 21, 2023, were submitted July 19, 2023.
14. United Therapeutics (IUP DC-053) — No permit violations occurred at this
facility.
15. Wolfspeed 40 Moore (IUP DC-126) — No permit violations occurred at this
facility.
16. Wolfspeed Durham (IUP DC-076) — Wolfspeed Durham was issued a Notice of
Violation on June 2, 2023, for late reporting. February 16, 2023, monitoring
results were postmarked April 24, 2023. Wolfspeed Durham was issued a Notice
of Violation on August 4, 2023, for a fluoride excursion that occurred on June 25,
2023. The operator sent fluoride containing waste to the equalization basin due to
improper valve placement. The equalization basin containing high fluoride waste
was isolated, and waste was contained in the basin. A hauling company was
called to empty the contents of the equalization basin. The flow to the
equalization basin exceeded the capacity of the hauling company and Wolfspeed
Durham requested to discharge 10,000 gallons of the waste to the collection
system. Sampling of the waste was conducted during the discharge.
17. Wolfspeed RTP (IUP DC-040) — Wolfspeed RTP was issued a Notice of
Violation on June 2, 2023, for late reporting. February 16, 2023, monitoring
results were postmarked April 24, 2023.

Additional Information:
TriPharm was in SNC for late reporting in the first semi-annual period of 2023.
Cintas is in SNC for failure to self -monitor BOD, TSS, TN and TP monthly in the second
semi-annual period of 2023.
The Public Notice is included with this submittal and will be posted in the Durham -
Herald Sun. Proof of publication will be sent to the Division of Water Resources as soon
as it is available.

Pretreatment Program Info Database
printed on: 12/22/2023
for Program Name Durham County
WWTP Name Triangle
Program Approval Date 07/06/1995
Pretreatment Status Full
Region RRO
County Durham
Stream Information IWC % at 7Q10 100.00
7Q10 Flow cfs / mgd
0 / 0.00
1 Q10 Flow cfs / mgd
0.00 / 0.00
Stream Classification
ws-iv
Basin Number
CPF05
Receiving Stream Name
NORTHEAST CREEK
NPDES Number NC0026051
NPDES Effective Date
Last PAR Rec 02/28/2023
PAR Due Date03/01/2024
mercury
10/01/2022
1631
NPDES Expire Date
p� 04/30/2027
Current Fiscal 03/04/2020
required
Year PCI Done
POTW is Primary WWTP TRUE
Last Audit on 09/15/2021
Audit Year Nexl25/26
yes
Design Flow mgd 12.0000 % Design mgd is SIU permitted 14.40
Permitted SIU flow (mgd) [Pt_SIU)
1.72790
WWTP SIU's
15
Program SIUs 15
WWTP CIU's
13
Program CIUs 113
HWA LTMP
IWS SUo
ERP
date Inactive Date Next Due
04/01/2023
Date Received by DWR
03/16/2018 09/05/2013
03/31/2021 12/20/2012
02/11/2020
Date Approved
05/02/2018 10/08/2013
05/05/2021 04/03/2013
02/13/2020
Adopt Date Required
Date Adopted
03/11/2013
Info in this Box from Pt Contacts
Date Date Date
PT —Pro Attended Attended Attended
Formal Name g.Prime Phone1 ext Fax HWA Wksp IUP Wksp PAR Wksp
Ms. Stephanie Brixey
1 11919-560-9034
919-544-8590
11
1 6/22/2011 1/23/2007
L-1127713
[e-mail]
Deputy Director of E&ES/POTW
15926 NC Hwy 55 E
Ms. Amy Moore
Prim
919-560-9035
1
1919-544-8590
11 2/9/2012
1 4/18/2012 1/19/2012
[e-mail]
LABORATORY & COMPLIANCE
5926 NC Hwy 55 East
27713
Ms. Laura Melton
919-560-9042
919-544-8590
[e-mail]
Pretreatment Project Coordinator
15926 Highway 55 East
27713
I Pretreatment Related NOVs from D
DWR Central Office Contact JPretreatment Staff
DWR Regional Contact ICheng Zhang

Chapter 9, PAR Guidance
Pretreatment Performance Summary (PPS)
1.
Pretreatment Town Name: Durham County
2.
"Primary" NPDES Number NC00 26051
ThorColumn
office
or N on_D i scharge Permi t # i f appl i cabl e =>
Use only
EPA
WENDB
3.
PA R begi n D ate, pl ease enter 01 /01 /yy or 07/01 /yy 3. =>
1 / 1 /2023
PSSD
4.
PAR end Date, pl ease enter 06/30/yy or 12/31 /yy 4. =>
12/31 /2023
PSED
5.
Total number of SI Us, i ncl udes CI Us 5. =>
17
SUS
6.
Number of Cl Us 6. =>
16
CIUS
7.
Enter the Higher Number, either (7a) or (7b) here =>
0
NOIN
7a. Number of SIUs not sampled by POTW 7a. =>
0
7b. Number of SIUs not inspected by POTW 7b. =>
0
8.
Number of SlUswith no IUP, or with an expired IUP 8. =>
0
NOCM
9.
Total Number of SI Us in SNC due to either I U Reporti ng violations or
IUP Limit violations. To avoid double counting some SlUs
Enter ( 9a + 9b) - 9c here =>
2
PSNC
Enter the Number of SIUs in SNC for:
9a. I U Reporti ng vi of ati ons 9a. =>
2
M SNC
9b. IUP Limit violations 9b. =>
0
SNPS
9c. Both I U Reporti ng & L i mi t vi of ati ons 9c. =>
2
1o.
Number of SlUsin SNC due to I Reporting violations
that were not sampled or inspected by POTW 10. =>
0
SNIN
11.
Number of SIUs in SNC dueto violation of 11. =>
0
SSNC
Compl i ance Schedul e due dates
12.
Number NOVs, NNCs, AOs, or similar assesed to SIUs 12. =>
17
FENF
13.
Number Civil or Criminal Penal ti es assessed to SIUs 13. =>
0
JUDI
14.
Number of SIUs included in public notice 14. =>
2
SVPU
15.
Number of SlUsfrom which penal ti es col I ected 15. =>
0
IUPN
16.
Total A mount of Ci vi I Penal ti es Col I ected 16. => $
0.00
17.
Total N umber of SI Us on a compl i ance schedul e 17. =>
0
SOCS
Foot Notes: AO Administrative Order NOV Noticeof Violation
CIU Categorical Industrial User PAR Pretreatment Annual Report
CO Consent Order POTW Public Operated Treatment Works
IUP Industrial User Pretreatment Permit SIU Significant Industrial User
NNC Noticeof Non -Compliance SNC Significant Non -Compliance,
formerly RNC

Pretreatment Annual Report (PAR)
Significant Non -Compliance Report (SNCR)
WWTP = Wastewater Treatment PI ant, use separate form for each WWTP.
SIU = Significant Industrial User
SNC = Significant Non -Compliance
PAR covers this calendar year => 2023
Control Authority=Program=Town Name => Durham County
WWTP Name => Triangle WWTP
N PD ES # => N CO026051
A SNCR Form must be submitted with every PAR, please write" None" if you had No SIUs in SNC during calendar year
1 UP
#
Pipe
#
I ndustry Name
Parameter
or "Reporting"
SNC ? ( Yes/ No)
for each &-month period.
Jan. - June
July - Dec.
DC-106
001
TriPharm Services
reporting
Yes
No
DC-037
001
Ci Was
reporti ng
No
Yes
Form name: PAR,SNCR,2001
DateRevised: 1/4/2001

Public Notice
Durham County in accordance with Federal and State Regulations, is hereby giving public notice.
Listed below are users in significant noncompliance with national pretreatment regulations (40
CFR Part 403), state pretreatment regulations (15 NCAC 21-1.0900), or local pretreatment
regulations during January 2023 through December 2023.
TriPharm Services, Inc. dba Alcami Coporation, located at 627 Davis Drive, Suite 100, and
regulated by significant industrial user permit number DC-106 was in status of significant
noncompliance for late reporting in the first semiannual period of January through June 2023.
Monitoring results for February 2023 were received more than 30 days past the requirements as
stated in the permit. A written notification titled "Notice of Violation" was sent to the user's
authorized representative requiring them to notify the County of the cause of the violation.
TriPharm Services, Inc. dba Alcami Corporation reported a change in staff that lead to the
violations and took corrective action to return to compliance in the second semiannual period of
2023.
Cintas Corporation, located at 1003 Twin Creek Court, and regulated by local industrial user
permit number DC-037 was in status of significant noncompliance for failure to self -monitor
monthly parameters for biochemical oxygen demand, total suspended solids, total nitrogen and
total phosphorus in the second semiannual period of July through December 2023. A written
notification titled "Notice of Violation" was sent to the user's authorized representative requiring
them to notify the County of the cause of the violation.

TWWTP Allocation Table
POTW=>
NPDES#=>
]UP
Count
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Allocation Table
Headworks last approved: 05/02/18
Allocation Table updated: 02/26/24
Permits last modified: 12/18/23
Printed: 2/26/2024, 10:55 AM
Page 1 of 4
TriangleWWTP
NCO026051
Industry
INDUSTRY NAMES Permit
(Pl�u�f aphaba dy) number
Type Renewal Modification Date
Pipe of Effective Effective Permit
number I ndustry Date Date Expi res
FLOW
Permit Limits
BOD
Permit Limits
Ti
Permit
M GDgal/day
Conc. Load
mg/I I bstda
Conc.
m /I
AstraZeneca Pharmaceuticals
DC-078
001
439 D& E Pharmaceutical
01/01/22
12/18/23
12/31/26
0.0020
2,000
002
439 D& E Pharmaceutical
Aurobindo USA
DC-089
001
439 D& E Pharmaceutical
10/09/19
12/01/21
10/08/24
0.0390
39,000
monitor
Bi ogen
DC-080
001
439 C,D& E Pharmaceutical
08/24/20
08/01/23
08/23/25
0.1500
150,000
monitor
Cintas
DC-037
001
Ful I Servi ce L aundry Faci I i ty
11/02/22
11/01/27
0.1000
100,000
monitor
Cree LED Headquarters
DC-125
001
469 D Electrical Components LED
07/01/23
06/30/26
0.0030
3,000
Eli Lilly & Company
DC-119
001
Combined Discharge)
03/25/23
03/24/26
0.1215
121,481
monitor
002
439 D Pharmaceutical
0.0614
61,413
Wolfspeed Durham (008, 009)
DC-076
469 Semi Conductor Mfg.
08/01/19
08/23/23
07/31/24
0.5910
591,000
Wolfspeed Durham 008
008
Combined Dischar e)
monitor
Wolfspeed Durham 009
009
Combined Discharge)
monitor
Wolfspeed Durham 013
013
433 Metal Finisher
0.0300
monitor
Wolfspeed RTP
DC-040
012
469 Semi Conductor Mfg.
08/01/19
08/23/22
07/31/24
0.3290
329,000
M i cross A dvanced
DC-085
001
469 E R& D Semiconductor
10/21/19
10/20/24
0.0750
75,000
Phononic
DC-075
001
469 A Semi Conductor Mfg.
03/07/23
03/06/28
0.0200
20,000
PowerSecure
DC-095
001
433 Metal Finisher
11/13/19
06/01/22
11/12/24
0.0060
6,000
SCM Metals
DC-005
001
471.104A Powder Former
07/01/21
06/30/26
0.0500
50,000
TriPharm
DC-106
001
439 D&E Pharmaceutical
10/18/23
10/17/28
0.0080
8,000
monitor
Tergus Pharma
DC-115
001
439 D& E Pharmaceutical
12/27/23
12/26/28
0.0065
6,500
monitor
United Therapeutics
DC-053
001
Combined Discharge
05/25/20
09/01/21
05/24/25
0.0600
60,000
monitor
Wolfspeed 40 Moore
DC-126
001
469 A Semiconductor
07/07/23
11/21/23
07/06/26
0.2975
297,500
002
469A Semiconductor
monitor
Column Totals =>
1 1.94991
1,919,894
0
Basis=>
MAHL from HWA (lbs/day) =>
Uncontrollable Loading (lbs/day) =>
Total AIIowablefor Industry (MAIL) (Ibs/day) =>
Total Permitted to Industry (Ibstday) =>
MAIL left (lbs/day) =>
Percent Allow. Ind. (MAIL) still available (%) =>
Percent M A H L still available(%) =>
N PD ES Permitted FI ow=>
NPDES
Design
5 Percent M A H L (I bs(day) _>

TWWTP Allocation Table
POTW=-
NPDES#=-
IUP
Count
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Allocation Table
Headworks last approved: 05/02/18
Allocation Table updated: 02/26/24
Permits last modified: 12/18/23
Printed: 2/26/2024, 10:55 AM
Page 2 of 4
TriangleWWTP
NC0026051
Industry
INDUSTRY NAMES Permit
(Pl�u�f aphaba dy) number
3S
Limits
Pipe Load
number I bs/d
Ammonia
Permit Limits
Arsenic
Permit Limits
Cadmium
Permit Limits
Chromium
Permit Limits
Copper
Permit Limits
Cyanide
Permit Limits
Conc. Load
m /I I bs/da
Conc. Load
m /I I bs/d
Conc. Load
mg/I I bs/da
Conc. Load
mg/I I bs/d
Conc. Load
m /I I bs/da
Conc. Load
m /I I bs/day
AstraZeneca Pharmaceuticals
DC-078
001
002
Aurobindo USA
DC-089
001
monitor
monitor
monitor
monitor
monitor
Bi ogen
DC-080
001
monitor
monitor
monitor
0.0400
0.0500
Cintas
DC-037
001
monitor
monitor
monitor
monitor
monitor
Cree LED Headquarters
DC-125
001
monitor
0.0700
0.0018
monitor
monitor
monitor
Eli Lilly & Company
DC-119
001
monitor
monitor
monitor
monitor
monitor
monitor
monitor
002
Wolfspeed Durham (008, 009)
DC-076
Wolfspeed Durham 008
008
monitor
monitor
monitor
monitor
monitor
Wolfspeed Durham 009
009
monitor
Wolfspeed Durham 013
013
0.0700
0.0175
1.7100
0.4278
2.0700
0.5179
0.6500
0.1626
Wolfspeed RTP
DC-040
012
monitor
monitor
monitor
monitor
monitor
M i cross A dvanced
DC-085
001
monitor
monitor
monitor
monitor
Phononic
DC-075
001
PowerSecure
DC-095
001
0.0700
0.0035
1.7100
0.0856
2.0700
0.1036
0.5000
0.0250
SCM Metals
DC-005
001
monitor
monitor
0.5000
0.2085
0.0300
0.0125
TriPharm
DC-106
001
monitor
monitor
monitor
Tergus Pharma
DC-115
001
monitor
monitor
monitor
monitor
United Therapeutics
DC-053
001
monitor
monitor
monitor
monitor
Wolfspeed 40 Moore
DC-126
001
002
monitor
monitor
monitor
monitor
monitor
monitor
Column Totals =>
0
0
0.00001
1 0.5134
0.83001
1 0.2502
Bask=>
M A H L from H W A (I bs/day) _>
Uncontrollable Loading (lbs/day) _>
Total AIIowablefor Industry (MAIL) (Ibs/day) _>
Total Permitted to Industry (Ibs/day) _>
MAIL left (I bs/day) _>
Percent A I I ow. Ind. (MAIL) st i I I avai I abl e (%) _>
M A H L sti I I avai I abl e (%) _>
5 Percent M A H L (I bs(day) _>
Design
Design
Stream Std
Stream Std
Stream Std
AS/Nit/TF
inhibition
Stream Std
25020
2502.00
0.8962
0.2987
4.8465
23.6589
0.7950
9964
1306.42
0.1329
0.0133
0.1771
1.9308
0.0221
15056
1195.58
0.7633
0.2854
4.6694
21.7281
0.7728
0
0.00
0.0000
0.0228
0.5134
0.8300
0.2502
15056
1195.58
0.7633
0.2627
4.1560
20.8981
0.5226
100.0 %
100.0 %
100.0 %
89.0%
96.2 %
67.6Percent
60.2%
47.8 %
85.2%
M2.0
85.8 %
88.3 %
65.7%
1251
12510
0.0448
0.2423
1.1829
0.0397

TWWTP Allocation Table
POTW=-
NPDES#=-
IUP
Count
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Allocation Table
Headworks last approved: 05/02/18
Allocation Table updated: 02/26/24
Permits last modified: 12/18/23
Printed: 2/26/2024, 10:55 AM
Page 3 of 4
TriangleWWTP
NCO026051
Industry
INDUSTRY NAMES Permit
(pla hsl aphaba dy) number
Pipe
numb
Lead
Permit Limits
Mercury
Permit Limits
Molybdenum
Permit Limits
Nickel
Permit Limits
Selenium
Permit Limits
Silver
Permit Limits
Conc. Load
mg/I I bs/d
Conc. Load
mg/I I bs/da
Conc. Load
m /I I bs/da
Conc. Load
mg/I I bs/da
Conc. Load
m /I I bs/da
Conc. Load
mg/I I bs/da
AstraZeneca Pharmaceuticals
DC-078
001
0.000142
0.000002
002
monitor
Aurobindo USA
DC-089
001
0.000142
0.000046
monitor
Bi ogen
DC-080
001
0.000142
0.000178
monitor
Cintas
DC-037
001
monitor
0.000142
0.000118
monitor
monitor
monitor
Cree LED Headquarters
DC-125
001
monitor
0.000142
0.000004
monitor
monitor
monitor
Eli Lilly & Company
DC-119
001
monitor
0.000142
0.000144
monitor
monitor
monitor
monitor
002
Wolfspeed Durham (008, 009)
DC-076
0.000142
0.000700
Wolfspeed Durham 008
008
monitor
monitor
monitor
monitor
monitor
monitor
Wolfspeed Durham 009
009
monitor
monitor
Wolfspeed Durham 013
013
0.4300
0.1076
2.3800
0.5955
0.24001
0.0600
Wolfspeed RTP
DC-040
012
monitor
0.000142
0.000390
monitor
monitor
monitor
monitor
M i cross A dvanced
DC-085
001
monitor
0.000142
0.000089
monitor
monitor
monitor
Phononic
DC-075
001
0.000142
0.000024
monitor
0.0200
PowerSecure
DC-095
001
0.4300
0.0215
0.000142
0.000007
monitor
1.0000
0.0500
0.2400
0.0120
SCM Metals
DC-005
001
0.1000
0.0417
0.000142
0.000059
monitor
monitor
monitor
TriPharm
DC-106
001
0.000142
0.000009
monitor
Tergus Pharma
DC-115
001
monitor
0.000142
0.000008
monitor
United Therapeutics
DC-053
001
0.000142
0.000071
monitor
Wolfspeed 40 Moore
DC-126
001
0.000142
0.000352
002
monitor
monitor
monitor
monitor
monitor
monitor
Column Totals =>
0.17081
0.002201
1 0.0000
0.6655
0.0000
0.0721
Basis=>
MAHL from HWA (lbs/day) =>
Uncontrollable Loading (lbs/day) =>
Total AIIowablefor Industry (MAIL) (Ibs/day) =>
Total Permitted to Industry (Ibs/day) =>
MAIL left (lbs/day) =>
Percent Allow. Ind. (MAIL) still available(%) =>
Percent M A H L still available(%) =>
5 Percent M A H L (I bs(dav) =>
Stream Std
NPDES
Sludge
Ceiling HASL
Stream Std
Ceiling
HASL
AS/Nit/TF
inhibition
3.1596
0.025829
22.9553
2.4843
0.4219
12.3224
0.1949
0.003543
0.3366
0.3321
0.0930
0.0443
2.9647
0.022286
22.6188
2.1522
0.3289
12.2781
0.1708
0.002201
0.0000
0.6655
0.0000
0.0721
2.7939
0.020085
22.6188
1.4867
0.3289
12.2060
94.2 %
90.1 %
100.0 %
69.1 %
100.0 %
99.4
88.4 %
77.8 %
98.5 %
59.8 %
78.0 %
99.1 %
0.1580
0.001291
1.1478
0.1242
0.0211
0.6161

TWWTP Allocation Table
POTW=-
NPDES#=-
IUP
Count
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Allocation Table
Headworks last approved: 05/02/18
Allocation Table updated: 02/26/24
Permits last modified: 12/18/23
Printed: 2/26/2024, 10:55 AM
Page 4 of 4
TriangleWWTP
NC0026051
Industry
INDUSTRY NAMES Permit
(Pl�usl aphaba dy) number
Pipe
numb
Zinc
Permit Limits
Total Nitrogen
Permit Limits
Total Phos.
Permit Limits
Chloride
Permit Limits
Fluoride
Permit Limits
Conc. Load
mg/I I bs/d
Conc. Load
mg/I I bs/da
Conc. Load
m /I I bs/d
Conc. Load
m /I I bs/d
Conc. Load
mg/I I bs/day
AstraZeneca Pharmaceuticals
DC-078
001
002
Aurobindo USA
DC-089
001
monitor
monitor
monitor
monitor
monitor
Bi ogen
DC-080
001
monitor
monitor
monitor
monitor
monitor
Cintas
DC-037
001
monitor
monitor
monitor
monitor
monitor
Cree LED Headquarters
DC-125
001
0.6700
0.0168
monitor
monitor
7.0000
0.1751
Eli Lilly & Company
DC-119
001
monitor
monitor
monitor
monitor
monitor
002
Wolfspeed Durham (008, 009)
DC-076
7.0000
34.5026
Wolfspeed Durham 008
008
monitor
monitor
monitor
monitor
monitor
Wolfspeed Durham 009
009
monitor
monitor
Wolfspeed Durham 013
013
1.4800
0.3703
Wolfspeed RTP
DC-040
012
monitor
monitor
monitor
monitor
7.0000
19.2070
M i cross A dvanced
DC-085
001
monitor
monitor
monitor
monitor
6.0000
3.7530
Phononic
DC-075
001
PowerSecure
DC-095
001
1.4800
0.0741
SCM Metals
DC-005
001
monitor
monitor
monitor
monitor
monitor
TriPharm
DC-106
001
monitor
monitor
monitor
monitor
monitor
Tergus Pharma
DC-115
001
monitor
monitor
monitor
monitor
monitor
United Therapeutics
DC-053
001
monitor
monitor
monitor
monitor
monitor
Wolfspeed 40 Moore
DC-126
001
002
monitor
monitor
monitor
monitor
monitor
Column Totals =>
0.4611
0.00
0.00
0.0000
57.6377
Bass=>
M A H L from H W A (I bs/day) _>
Uncontrollable Loading (lbs/day) _>
Total AIIowablefor Industry (MAIL) (Ibs/day) _>
Total Permitted to Industry (Ibs/day) _>
MAIL left (I bs/day) _>
Percent Allow. Ind. (MAIL) still available (%) _>
Percent M A H L sti I I avai I abl e (%) _>
5 Percent M A R L (I bs(dav) =>
AS/Nit/TF
inhibition
Design
Design
Stream Std
NPDES
49.2894
4003.2000
650.00
16179.5562
100.329(
18.1304
1988.6492
238.92
3844.2251
31.7881
31.1590
2014.55
411.08
12335.3311
68.540�
0.4611
0.00
0.00
0.0000
57.637i
30.6978
2014.55
411.08
12335.3311
10.903�
98.5 %
100.0 %
100.0 %
100.0 %
15.9 0
62.3 %
50.3 %
63.2 %
76.2 %
10.9 o
2 464.5
inn 1 F
RnR 977R
5 n 16z
32 Sono

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
02/22/2023 S
AstraZeneca022223Sel <
0.025
/ 20.7
mg/L
<
/
f
05/30/2023 P
AstraZeneca053023PO
0.505
/ 20.7
mg/L
/
TW
Feb 2023
Week 4 <
0.025
/
mg/L
<
/
May 2023
Week 4
0.505
/
mg/L
/
Feb 2023
Average <
0.025
/ 8.2
mg/L
<
/
May 2023
Average
0.505
/ 8.2
mg/L
/
2023
Quarter 1 <
0.025
/
mg/L
<
/
2023
Quarter 2
0.505
/
mg/L
/
2023
1st 6 Months (Avg) <
0.265
/
mg/L
<
/
2023
1st 6 ...(Max)
0.505
/
mg/L
/
2023
Ist6... (Min) <
0.025
/
mg/L
<
/
2023
1st 6 ...(Count)
2
/
/
Sample Count : 2 Months Sampled:
2
Weeks Sampled
:
2
Quarters Sampled :
2
# Over Daily C:
0 0.00 # Over Mo Avg C:
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC
:
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Muss/Limit
Average Flow for Month
01/31/2023
S
AstraZeneca0123F1ow
02/28/2023
S
AstraZeneca0223F1ow
03/31/2023
S
AstraZeneca0323F1ow
04/30/2023
S
AstrraZeneca0423F1ow
05/31/2023
S
AstraZeneca0523F1ow
06/30/2023
S
AstraZeneca0623F1ow
Jan 2023
Week 4
Feb 2023
Week 4
Mar 2023
Week 4
Apr 2023
Week 4
May 2023
Week 4
Jun 2023
Week 4
Jan 2023
Average
Feb 2023
Average
Mar 2023
Average
Apr 2023
Average
May 2023
Average
Jun 2023
Average
0.00016
/
MGD /
0.000333
/
MGD /
0.000025
/
MGD /
0.000002
/
MGD /
0.000005
/
MGD /
0.000008
/
MGD /
0.00016
/
MGD /
0.000333
/
MGD /
0.000025
/
MGD /
0.000002
/
MGD /
0.000005
/
MGD /
0.000008
/
MGD /
0.00016
/ 0.002
MGD /
0.000333
/ 0.002
MGD /
0.000025
/ 0.002
MGD /
0.000002
/ 0.002
MGD /
0.000005
/ 0.002
MGD /
0.000008
/ 0.002
MGD /
Tuesday, February 13, 2024 1:23:17PM * Indicates Violation ** Indicates TRC Violation Page 1 of 6

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
2023
Quarter 1
0.000173
/
MGD
/
2023
Quarter 2
0.000005
/
MGD
/
2023
1 st 6 Months (Avg)
0.000089
/
MGD
/
2023
1st 6 ...(Max)
0.000333
/
MGD
/
2023
1st 6 ...(Min)
0.000002
/
MGD
/
2023
Ist6... (Count)
6
Sample Count: 6 Months Sampled
:
6
Weeks Sampled:
6
Quarters Sampled :
2
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
COD
02/22/2023 S
AstraZeneca022223Sel <
7.5
/
mg/L
<
/
f
05/30/2023 P
AstraZeneca053023P0
180
/
mg/L
/
TW
Feb 2023
Week 4 <
7.5
/
mg/L
<
/
May 2023
Week 4
180
/
mg/L
/
Feb 2023
Average <
7.5
/
mg/L
<
/
May 2023
Average
180
/
mg/L
/
2023
Quarter 1 <
7.5
/
mg/L
<
/
2023
Quarter 2
180
/
mg/L
/
2023
1st 6 Months (Avg) <
93.8
/
mg/L
<
/
2023
1st 6 ...(Max)
180
/
mg/L
/
2023
1st 6 ...(Min) <
7.5
/
mg/L
<
/
2023
1st 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
02/22/2023
S AstraZeneca022223Sel
<
0.003
/ 20.7
mg/L
< /
f
05/30/2023
P AstraZeneca053023PO
<
0.01
/ 20.7
mg/L
< /
TW
Feb 2023
Week 4
<
0.003
/
mg/L
< /
May 2023
Week 4
<
0.01
/
mg/L
< /
Feb 2023
Average
<
0.003
/ 8.2
mg/L
< /
May 2023
Average
<
0.01
/ 8.2
mg/L
< /
2023
Quarter 1
<
0.003
/
mg/L
< /
Tuesday, February 13, 2024 1:23:17PM * Indicates Violation ** Indicates TRC Violation Page 2 of 6

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
2023
Quarter 2
<
0.01
J
mg/L <
/
2023
1st 6 Months (Avg) <
0.006
/
mg/L <
/
2023
lst6... (Max)
<
0.01
/
mg/L <
/
2023
1st 6 ...(Min)
<
0.003
/
mg/L <
/
2023
1st 6 ...(Count)
2
Sample Count: 2
Months Sampled:
2
Weeks Sampled :
2
Quarters Sampled :
2
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
02/22/2023 S
AstraZeneca022223Sel <
0.003
/ 20.7
mg/L
<
/
f
05/30/2023 P
AstraZeneca053023PO <
0.01
/ 20.7
mg/L
<
/
TW
Feb 2023
Week 4 <
0.003
/
mg/L
<
/
May 2023
Week 4 <
0.01
/
mg/L
<
/
Feb 2023
Average <
0.003
/ 8.2
mg/L
<
/
May 2023
Average <
0.01
/ 8.2
mg/L
<
/
2023
Quarter I <
0.003
/
mg/L
<
/
2023
Quarter 2 <
0.01
/
mg/L
<
/
2023
1st 6 Months (Avg) <
0.006
/
mg/L
<
/
2023
1st 6 ...(Max) <
0.01
/
mg/L
<
/
2023
1st 6 ...(Min) <
0.003
/
mg/L
<
/
2023
1st 6 ...(Count)
2
Sample Count: 2 Months Sampled
:
2
Weeks Sampled :
2
Quarters Sampled :
2
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury - LL
02/22/2023 S AstraZeneca022223Sel < 0.000001 / 0.000142 mg/L < /
f
Tuesday, February 13, 2024 1:23:17PM * Indicates Violation ** Indicates TRC Violation Page 3 of 6

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Mercury - LL
05/30/2023 P
AstIaZeneca053023PO 0.000001
/ 0.000142
mg/L
/
TWHg
Feb 2023
Week 4
< 0.000001
/
mg/L <
/
May 2023
Week 4
0.000001
/
mg/L
/
Feb 2023
Average
< 0.000001
/
mg/L <
/
May 2023
Average
0.000001
/
mg/L
/
2023
Quarter 1
< 0.000001
/
mg/L <
/
2023
Quarter 2
0.000001
/
mg/L
/
2023
1st 6 Months (Avg) < 0.000001
/
mg/L <
/
2023
1st 6 ...(Max)
0.000001
/
mg/L
/
2023
1st 6 ...(Min)
< 0.000001
/
mg/L <
/
2023
1st 6 ...(Count)
2
Sample Count: 2
Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
2
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
Methylene Chloride
02/22/2023
S AstraZeneca022223Sel
<
0.003
/ 3.0
mg/L
< /
f
05/30/2023
P AstraZeneca053023PO
<
0.01
/ 3.0
mg/L
< /
TW
Feb 2023
Week 4
<
0.003
/
mg/L
< /
May 2023
Week 4
<
0.01
/
mg/L
< /
Feb 2023
Average
<
0.003
/ 0.7
mg/L
< /
May 2023
Average
<
0.01
/ 0.7
mg/L
< /
2023
Quarter 1
<
0.003
/
mg/L
< /
2023
Quarter 2
<
0.01
/
mg/L
< /
2023
1st 6 Months (Avg)
<
0.006
/
mg/L
< /
2023
1st 6 ...(Max)
<
0.01
/
mg/L
< /
2023
1st 6 ...(Min)
<
0.003
/
mg/L
< /
2023
1st 6 ...(Count)
2
Tuesday, February 13, 2024 1:23:17PM * Indicates Violation ** Indicates TRC Violation Page 4 of 6

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
2
Months Sampled :
2
Weeks Sampled:
2
Quarters Sampled :
2
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
02/22/2023 S
AstraZeneca022223Sel <
0.003
/ 20.7
mg/L
<
/
f
05/30/2023 P
AstraZeneca053023PO <
0.01
/ 20.7
mg/L
<
/
TW
Feb 2023
Week 4 <
0.003
/ 8.2
mg/L
<
/
May 2023
Week 4 <
0.01
/ 8.2
mg/L
<
/
Feb 2023
Average <
0.003
/
mg/L
<
/
May 2023
Average <
0.01
/
mg/L
<
/
2023
Quarter 1 <
0.003
/
mg/L
<
/
2023
Quarter 2 <
0.01
/
mg/L
<
/
2023
1st 6 Months (Avg) <
0.006
/
mg/L
<
/
2023
lst6... (Max) <
0.01
/
mg/L
<
/
2023
1st 6 ...(Min) <
0.003
/
mg/L
<
/
2023
1st 6... (Count)
2
Sample Count: 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
2
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
02/22/2023
S AstraZeneca022223Sel
7.7
/ 6.0 - 10.0
SU /
f
05/30/2023
P AstraZeneca053023PO
6.3
/ 6.0 - 10.0
SU /
TW
Feb 2023
Week 4
7.7
/
SU /
May 2023
Week 4
6.3
/
Su /
Feb 2023
Average
7.7
/
SU /
May 2023
Average
6.3
/
SU /
2023
Quarter 1
7.7
/
SU /
2023
Quarter 2
6.3
/
Su /
Tuesday, February 13, 2024 1:23:17PM * Indicates Violation ** Indicates TRC Violation Page 5 of 6

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outttall: 001
Sample Date SamplelD Result/Limit Mass/Limit
pH
2023
1st 6 Months (Avg)
7 /
SU
/
2023
1st 6 ...(Max)
7.7 /
SU
/
2023
lst6...
(Min)
6.3 /
SU
/
2023
1st 6 ...(Count)
2
Sample Count:
2
Months Sampled:
2
Weeks Sampled :
2
Quarters Sampled :
2
# Over Daily C:
0
0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M:
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0
0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Tuesday, February 13, 2024 1:23:17PM * Indicates Violation ** Indicates TRC Violation Page 6 of 6

Aurobindo USA
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
02/21/2023 S
Aurobindo022123Self <
0.025
/ 5.59
mg/L
<
/
05/31/2023 P
Aurobindo053123POT
0.113
/ 5.59
mg/L
/
W
Feb 2023
Week 3 <
0.025
/
mg/L
<
/
May 2023
Week 4
0.113
/
mg/L
/
Feb 2023
Average <
0.025
/ 2.21
mg/L
<
/
May 2023
Average
0.113
/ 2.21
mg/L
/
2023
Quarter 1 <
0.025
/
mg/L
<
/
2023
Quarter 2
0.113
/
mg/L
/
2023
1st 6 Months (Avg) <
0.069
/
mg/L
<
/
2023
1st 6 ...(Max)
0.113
/
mg/L
/
2023
1st 6 ...(Min) <
0.025
/
mg/L
<
/
2023
Ist 6 ...(Count)
2
/
/
Sample Count: 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
2
# Over Daily C :
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit IYlass/Limit
Ammonia
02/21/2023
S Aurobindo022123Self
3
/ mg/L
/
05/31/2023
P Aurobindo053123POT
19.3
/ mg/L
/
W
Feb 2023
Week 3
3
/ mg/L
/
May 2023
Week 4
19.3
/ mg/L
/
Feb 2023
Average
3
/ mg/L
/
May 2023
Average
19.3
/ mg/L
/
2023
Quarter 1
3
/ mg/L
/
2023
Quarter 2
19.3
/ mg/L
/
2023
1st 6 Months (Avg)
11.15
/ mg/L
/
2023
1st 6 ...(Max)
19.3
/ mg/L
/
2023
1st 6 ...(Min)
3
/ mg/L
/
2023
1st 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass/Lindt
Average Flow for Month
01/19/2023 S Aurobindo0123F1ow 0.00531 / MGD /
02/28/2023 S Aurobindo0223FIow 0.007103 / MGD /
Tuesday, February 13, 2024 2:16:21PM * Indicates Violation ** Indicates TRC Violation Page 1 of 12

Aurobindo USA
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
03/16/2023
S
Aurobindo0323F1ow
0.004809
/
MGD /
04/19/2023
S
Aurobindo0423Flow
0.003442
/
MGD /
05/18/2023
S
Aurobindo0523F1ow
0.004253
/
MGD /
06/22/2023
S
Aurobindo0623F1ow
0.003057
/
MGD /
Jan 2023
Week 3
0.00531
/
MGD /
Feb 2023
Week 4
0.007103
/
MGD /
Mar 2023
Week 3
0.004809
/
MGD /
Apr 2023
Week 3
0.003442
/
MGD /
May 2023
Week 3
0.004253
/
MGD /
Jun 2023
Week 4
0.003057
/
MGD /
Jan 2023
Average
0.00531
/ 0.039
MGD /
Feb 2023
Average
0.007103
/ 0.039
MGD /
Mar 2023
Average
0.004809
/ 0.039
MGD /
Apr 2023
Average
0.003442
/ 0.039
MGD /
May 2023
Average
0.004253
/ 0.039
MGD /
Jun 2023
Average
0.003057
/ 0.039
MGD /
2023
Quarter 1
0.005741
/
MGD /
2023
Quarter 2
0.003584
/
MGD /
2023
1 st 6 Months (Avg)
0.004662
/
MGD /
2023
1st 6 ...(Max)
0.007103
/
MGD /
2023
1st 6 ...(Min)
0.003057
/
MGD /
2023
lst 6 ... (Count)
6
Sample Count:
6 Months Sampled:
6
Weeks Sampled:
6
Quarters Sampled :
2
# Over Daily C:
0
0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C :
0
0.00
# Over Daily C TRC:
0
0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC :
0
0.00
# Over Daily M :
0
0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M :
0
0.00
# Over Daily M TRC:
0
0.00 # Over Mo Avg M TRC:
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC :
0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
BOD
02/21/2023 S
Aurobindo022123Self
86
/
mg/L
/
05/31/2023 P
Aurobindo053123POT
170
/
mg/L
/
W
Feb 2023
Week 3
86
/
mg/L
/
May 2023
Week 4
170
/
mg/L
/
Feb 2023
Average
86
/
mg/L
/
May 2023
Average
170
/
mg/L
/
2023
Quarter 1
86
/
mg/L
/
2023
Quarter 2
170
/
mg/L
/
Tuesday, February 13, 2024
2:16:21PM
* Indicates Violation
** Indicates TRC Violation
Page
2 of 12

Aurobindo USA
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
BOD
2023
2023
2023
2023
1st 6 Months (Avg)
1st 6 ...(Max)
lst6... (Min)
1st 6 ...(Count)
128
170
86
2
/
/
/
/
mg/L
mg/L
mg/L
/
/
/
/
Sample Date
SampleLD
Result/Limit
Mass/Limit
Cadmium
02/21/2023
S Aurobindo022123Self
<
0.00008
/
mg/L
<
/
05/31/2023
P Aurobindo053123POT
<
0.00008
/
mg/L
<
/
W
Feb 2023
Week 3
<
0.00008
/
mg/L
<
/
May 2023
Week 4
<
0.00008
/
mg/L
<
/
Feb 2023
Average
<
0.00008
/
mg/L
<
/
May 2023
Average
<
0.00008
/
mg/L
<
/
2023
Quarter 1
<
0.00008
/
mg/L
<
/
2023
Quarter 2
<
0.00008
/
mg/L
<
/
2023
1st 6 Months (Avg)
<
0.00008
/
mg/L
<
/
2023
lst 6 ...(Max)
<
0.00008
/
mg/L
<
/
2023
1st 6 ...(Min)
<
0.00008
/
mg/L
<
/
2023
lst6... (Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
02/21/2023
S Aurobindo022123Self
35
/ mg/L
/
05/31/2023
P Aurobindo053123POT
603
/ mg/L
/
W
Feb 2023
Week 3
35
/ mg/L
/
May 2023
Week 4
603
/ mg/L
/
Feb 2023
Average
35
/ mg/L
/
May 2023
Average
603
/ mg/L
/
2023
Quarter 1
35
/ mg/L
/
2023
Quarter 2
603
/ mg/L
/
2023
1 st 6 Months (Avg)
319
/ mg/L
/
2023
1st 6 ...(Max)
603
/ mg/L
/
2023
1st 6 ...(Min)
35
/ mg/L
/
2023
1st 6... (Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
COD
02/21/2023 S Aurobindo022123Self
05/31/2023 P Aurobindo053123POT
W
Tuesday, February 13, 2024 2:16:21PM
47 / mg/L /
389 / mg/L /
* Indicates Violation ** Indicates TRC Violation
Page 3 of 12

Aurobindo USA
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
COD
Feb 2023
Week 3
47 /
mg/L
/
May 2023
Week 4
389 /
mg/L
/
Feb 2023
Average
47 /
mg/L
/
May 2023
Average
389 /
mg/L
/
2023
Quarter 1
47 /
mg/L
/
2023
Quarter 2
389 /
mg/L
/
2023
1st 6 Months (Avg)
218 /
mg/L
/
2023
1st 6 ...(Max)
389 /
mg/L
/
2023
1st 6 ...(Min)
47 /
mg/L
/
2023
1st 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
Copper
02/21/2023
S Aurobindo022123Self
0.013
/ mg/L
/
05/31/2023
P Aurobindo053123POT
83.6
/ mg/L
/
W
Feb 2023
Week 3
0.013
/ mg/L
/
May 2023
Week 4
83.6
/ mg/L
/
Feb 2023
Average
0.013
/ mg/L
/
May 2023
Average
83.6
/ mg/L
/
2023
Quarter 1
0.013
/ mg/L
/
2023
Quarter 2
83.6
/ mg/L
/
2023
1st 6 Months (Avg)
41.806
/ mg/L
/
2023
Ist 6 ...(Max)
83.6
/ mg/L
/
2023
1st 6 ...(Min)
0.013
/ mg/L
/
2023
1st 6... (Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
02/21/2023
S Aurobindo022123Self
<
0.003
/ mg/L
< /
05/31/2023
P Aurobindo053123POT
<
0.003
/ mg/L
< /
W
Feb 2023
Week 3
<
0.003
/ mg/L
< /
May 2023
Week 4
<
0.003
/ mg/L
< /
Feb 2023
Average
<
0.003
/ mg/L
< /
May 2023
Average
<
0.003
/ mg/L
< /
2023
Quarter 1
<
0.003
/ mg/L
< /
2023
Quarter 2
<
0.003
/ mg/L
< /
2023
1st 6 Months (Avg)
<
0.003
/ mg/L
< /
2023
1st 6 ...(Max)
<
0.003
/ mg/L
< /
2023
lst6... (Min)
<
0.003
/ mg/L
< /
2023
1st 6 ...(Count)
2
Tuesday, February 13, 2024 2:16:21 PM * Indicates Violation ** Indicates TRC Violation Page 4 of 12

Aurobindo USA
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
02/21/2023 S
Aurobindo022123Self <
0.003
/ 5.59
mg/L
<
/
05/31/2023 P
Aurobindo053123POT <
0.005
/ 5.59
mg/L
<
/
W
Feb 2023
Week 3 <
0.003
/
mg/L
<
/
May 2023
Week 4 <
0.005
/
mg/L
<
/
Feb 2023
Average <
0.003
/ 2.21
mg/L
<
/
May 2023
Average <
0.005
/ 2.21
mg/L
<
/
2023
Quarter 1 <
0.003
/
mg/L
<
/
2023
Quarter 2 <
0.005
/
mg/L
<
/
2023
1st 6 Months (Avg) <
0.004
/
mg/L
<
/
2023
1st 6 ...(Max) <
0.005
/
mg/L
<
/
2023
1st 6 ...(Min) <
0.003
/
mg/L
<
/
2023
Ist 6 ...(Count)
2
/
/
Sample Count: 2 Months Sampled
:
2
Weeks Sampled:
2
Quarters Sampled :
2
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass /Limit
Fluoride
02/21/2023
S Aurobindo022123Self
0.65
/ mg/L
/
05/31/2023
P Aurobindo053123POT
0.61
/ mg/L
/
W
Feb 2023
Week 3
0.65
/ mg/L
/
May 2023
Week 4
0.61
/ mg/L
/
Feb 2023
Average
0.65
/ mg/L
/
May 2023
Average
0.61
/ mg/L
/
2023
Quarter 1
0.65
/ mg/L
/
2023
Quarter 2
0.61
/ mg/L
/
2023
1st 6 Months (Avg)
0.63
/ mg/L
/
2023
1st 6 ...(Max)
0.65
/ mg/L
/
2023
1st 6 ...(Min)
0.61
/ mg/L
/
2023
1st 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass/Lindt
Isopropyl acetate
02/21/2023 S Aurobindo022123Self < 0.003 / 5.59 mg/L < /
05/31/2023 P Aurobindo053123POT < 0.005 / 5.59 mg/L < /
W
Tuesday, February 13, 2024 2:16:21PM * Indicates Violation ** Indicates TRC Violation Page 5 of 12

Aurobindo USA
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
Feb 2023
Week 3
<
0.003
/
mg/L
<
/
May 2023
Week 4
<
0.005
/
mg/L
<
/
Feb 2023
Average
<
0.003
/ 2.21
mg/L
<
/
May 2023
Average
<
0.005
/ 2.21
mg/L
<
/
2023
Quarter 1
<
0.003
/
mg/L
<
/
2023
Quarter 2
<
0.005
/
mg/L
<
/
2023
1st 6 Months (Avg) <
0.004
/
mg/L
<
/
2023
1st 6 ...(Max)
<
0.005
/
mg/L
<
/
2023
1st 6 ...(Min)
<
0.003
/
mg/L
<
/
2023
1st 6 ...(Count)
2
/
/
Sample Count: 2
Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
2
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit
Mercury - LL
Mass /Limit
02/21/2023 S
Aurobindo022123Self
0.000088
/ 0,000142
mg/L
/
Hg
05/30/2023 P
Aurobindo053023POT
0.00001
/ 0.000142
mg/L
/
WHg
Feb 2023
Week 3
0.000088
/
mg/L
/
May 2023
Week 4
0.00001
/
mg/L
/
Feb 2023
Average
0.000088
/
mg/L
/
May 2023
Average
0.00001
/
mg/L
/
2023
Quarter 1
0.000088
/
mg/L
/
2023
Quarter 2
0.00001
/
mg/L
/
2023
1st 6 Months (Avg)
0.000049
/
mg/L
/
2023
1st 6 ...(Max)
0.000088
/
mg/L
/
2023
1st 6 ...(Min)
0.00001
/
mg/L
/
2023
1st 6 ...(Count)
2
/
/
Sample Count : 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
2
# Over Daily C:
0 0.00 # Over Mo Avg C:
0 0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C :
0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0 0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC :
0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0 0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M :
0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0 0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC :
0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Tuesday, February 13, 2024 2:16:21PM
* Indicates Violation
** Indicates TRC Violation
Page
6 of 12

Aurobindo USA
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
02/21/2023 S
Aurobindo022123Self <
0.003
/ 0.81
mg/L
<
/
05/31/2023 P
Aurobindo053123POT <
0.005
/ 0.81
mg/L
<
/
W
Feb 2023
Week 3 <
0.003
/
mg/L
<
/
May 2023
Week 4 <
0.005
/
mg/L
<
/
Feb 2023
Average <
0.003
/ 0.18
mg/L
<
/
May 2023
Average <
0.005
/ 0.18
mg/L
<
/
2023
Quarter 1 <
0.003
/
mg/L
<
/
2023
Quarter 2 <
0.005
/
mg/L
<
/
2023
1st 6 Months (Avg) <
0.004
/
mg/L
<
/
2023
1st 6 ...(Max) <
0.005
/
mg/L
<
/
2023
1st 6 ...(Min) <
0.003
/
mg/L
<
/
2023
Ist 6 ...(Count)
2
/
/
Sample Count: 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
2
# Over Daily C :
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit IYlass/Limit
Molybdenum
02/21/2023 S
Aurobindo022123Self
<
0.001
/ mg/L
<
/
05/31/2023 P
Aurobindo053123POT
<
0.001
/ mg/L
<
/
W
Feb 2023
Week 3
<
0.001
/ mg/L
<
/
May 2023
Week 4
<
0.001
/ mg/L
<
/
Feb 2023
Average
<
0.001
/ mg/L
<
/
May 2023
Average
<
0.001
/ mg/L
<
/
2023
Quarter I
<
0.001
/ mg/L
<
/
2023
Quarter 2
<
0.001
/ mg/L
<
/
2023
1st 6 Months (Avg)
<
0.001
/ mg/L
<
/
2023
1st 6 ...(Max)
<
0.001
/ mg/L
<
/
2023
1st 6 ...(Min)
<
0.001
/ mg/L
<
/
2023
1st 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass/Lindt
n-Amyl acetate
02/21/2023 S Aurobindo022123Self < 0.003 / 5.59 mg/L < /
05/31/2023 P Aurobindo053123POT < 0.005 / 5.59 mg/L < /
W
Tuesday, February 13, 2024 2:16:21PM * Indicates Violation ** Indicates TRC Violation Page 7 of 12

Aurobindo USA
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
Feb 2023
Week 3 <
0.003
/
mg/L
<
/
May 2023
Week 4 <
0.005
/
mg/L
<
/
Feb 2023
Average <
0.003
/ 2.21
mg/L
<
/
May 2023
Average <
0.005
/ 2.21
mg/L
<
/
2023
Quarter 1 <
0.003
/
mg/L
<
/
2023
Quarter 2 <
0.005
/
mg/L
<
/
2023
1st 6 Months (Avg) <
0.004
/
mg/L
<
/
2023
Ist 6 ...(Max) <
0.005
/
mg/L
<
/
2023
Ist 6 ...(Min) <
0.003
/
mg/L
<
/
2023
1st 6 ...(Count)
2
/
/
Sample Count: 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
2
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
Nitrate -Nitrite
02/21/2023 S
Aurobindo022123Self
0.6
/
mg/L
/
05/31/2023 P
Aurobindo053123POT
0.6
/
mg/L
/
W
Feb 2023
Week 3
0.6
/
mg/L
/
May 2023
Week 4
0.6
/
mg/L
/
Feb 2023
Average
0.6
/
mg/L
/
May 2023
Average
0.6
/
mg/L
/
2023
Quarter 1
0.6
/
mg/L
/
2023
Quarter 2
0.6
/
mg/L
/
2023
1st 6 Months (Avg)
0.6
/
mg/L
/
2023
Ist 6 ...(Max)
0.6
/
mg/L
/
2023
1st 6 ...(Min)
0.6
/
mg/L
/
2023
Ist 6 ...(Count)
2
/
/
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen, Total
02/21/2023 S Aurobindo022123Self
05/31/2023 P Aurobindo053123POT
W
Feb 2023 Week 3
May 2023 Week 4
14 / mg/L /
48.7 / mg/L /
14 / mg/L /
48.7 / mg/L /
Tuesday, February 13, 2024 2:16:21PM * Indicates Violation ** Indicates TRC Violation Page 8 of 12

Aurobindo USA
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen, Total
Feb 2023
Average
14
/
mg/L
/
May 2023
Average
48.7
/
mg/L
/
2023
Quarter 1
14
/
mg/L
/
2023
Quarter 2
48.7
/
mg/L
/
2023
1st 6 Months (Avg)
31.35
/
mg/L
/
2023
Ist 6... (Max)
48.7
/
mg/L
/
2023
Ist 6 ...(Min)
14
/
mg/L
/
2023
Ist 6 ...(Count)
2
/
/
Sample Date
SamplelD
Result/Limit
Mass /Limit
Oil & Grease, Total
02/21/2023 S
Aurobindo022123Self <
2.5
/ 200
mg/L
<
/
05/31/2023 P
Aurobindo053123POT <
2.5
/ 200
mg/L
<
/
W
Feb 2023
Week 3 <
2.5
/
mg/L
<
/
May 2023
Week 4 <
2.5
/
mg/L
<
/
Feb 2023
Average <
2.5
/
mg/L
<
/
May 2023
Average <
2.5
/
mg/L
<
/
2023
Quarter 1 <
2.5
/
mg/L
<
/
2023
Quarter 2 <
2.5
/
mg/L
<
/
2023
1st 6 Months (Avg) <
2.5
/
mg/L
<
/
2023
Ist 6 ...(Max) <
2.5
/
mg/L
<
/
2023
1st 6 ...(Min) <
2.5
/
mg/L
<
/
2023
Ist 6 ...(Count)
2
Sample Count : 2 Months Sampled
:
2
Weeks Sampled:
2
Quarters Sampled :
2
# Over Daily C:
0 0.00 # Over Mo Avg C:
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC
:
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
PH
02/21/2023
S Aurobindo022123Self
8 / 6.0 - 10.0
su /
05/31/2023
P Aurobindo053123POT
9 / 6.0 - 10.0
SU /
W
Feb 2023
Week 3
8 /
Su /
May 2023
Week 4
9 /
SU /
Feb 2023
Average
8 /
SU /
May 2023
Average
9 /
SU /
Tuesday, February 13, 2024 2:16:21PM * Indicates Violation ** Indicates TRC Violation Page 9 of 12

Aurobindo USA
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
PH
2023
Quarter 1
8
/
SU
/
2023
Quarter 2
9
/
SU
/
2023
1 st 6 Months (Avg)
8.5
/
SU
/
2023
1st 6 ...(Max)
9
/
SU
/
2023
1st 6 ...(Min)
8
/
SU
/
2023
1st 6 ...(Count)
2
Sample Count: 2
Months Sampled
:
2
Weeks Sampled:
2
Quarters Sampled :
2
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC:
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
Temperature
02/21/2023
S Aurobindo022123Self
18
/ 66
°C /
05/31/2023
P Aurobindo053123POT
21
/ 66
G /
W
Feb 2023
Week 3
18
/
°C /
May 2023
Week 4
21
/
°C /
Feb 2023
Average
18
/
°C /
May 2023
Average
21
/
°C /
2023
Quarter 1
18
/
°C /
2023
Quarter 2
21
/
°C /
2023
1st 6 Months (Avg)
19.5
/
°C /
2023
lst 6 ...(Max)
21
/
°C /
2023
1st 6 ...(Min)
18
/
°C /
2023
1st 6 ...(Count)
2
Sample Count:
2
Months Sampled :
2
Weeks Sampled :
2
Quarters Sampled :
2
# Over Daily C:
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC: 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily:
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass I Limit
TKN
02/21/2023 S Aurobindo022123Self
Tuesday, February 13,2024 2:16:21PM
13.4 / mg/L
* Indicates Violation ** Indicates TRC Violation
Page 10 of 12

Aurobindo USA
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
TKN
05/31/2023
P Aurobindo053123POT
48.1
/ mg/L
/
W
Feb 2023
Week 3
13.4
/ mg/L
/
May 2023
Week 4
48.1
/ mg/L
/
Feb 2023
Average
13A
/ mg/L
/
May 2023
Average
48.1
/ mg/L
/
2023
Quarter 1
13.4
/ mg/L
/
2023
Quarter 2
48.1
/ mg/L
/
2023
1st 6 Months (Avg)
30.75
/ mg/L
/
2023
1st 6 ...(Max)
48.1
/ mg/L
/
2023
1st 6 ...(Min)
13.4
/ mg/L
/
2023
1st 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass /Limit
Total Phosphorus
02/21/2023 S
Aurobindo022123Self
1.34
/
mg/L
/
05/31/2023 P
Aurobindo053123POT
4.22
/
mg/L
/
W
Feb 2023
Week 3
1.34
/
mg/L
/
May 2023
Week 4
4.22
/
mg/L
/
Feb 2023
Average
1.34
/
mg/L
/
May 2023
Average
4.22
/
mg/L
/
2023
Quarter 1
1.34
/
mg/L
/
2023
Quarter 2
4.22
/
mg/L
/
2023
1st 6 Months (Avg)
2.78
/
mg/L
/
2023
1st 6 ...(Max)
4.22
/
mg/L
/
2023
1st 6 ...(Min)
1.34
/
mg/L
/
2023
1st 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
TSS
02/21/2023
S Aurobindo022123Self
05/31/2023
P Aurobindo053123POT
W
Feb 2023
Week 3
May 2023
Week 4
Feb 2023
Average
May 2023
Average
2023
Quarter 1
2023
Quarter
2023
1st 6 Months (Avg)
2023
1st 6 ...(Max)
2023
1st 6 ...(Min)
28 /
mg/L /
56 /
mg/L /
28 /
1-9/1-
56 /
mg/L /
28 /
mg/L /
56 /
mg/L /
28 /
mg/L /
56 /
mg/L /
42 /
mg/L /
56 /
mg/L /
28 /
mg/L /
Tuesday, February 13, 2024 2:16:21PM * Indicates Violation ** Indicates TRC Violation Page 11 of 12

Aurobindo USA
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
TSS
2023
1st 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
VOC
02/21/2023
S
Aurobindo022123Self
<
0.025 /
mg/L
<
/
05/31/2023
P
Aurobindo053123POT
0.113 /
mg/L
/
W
Feb 2023
Week 3
<
0.025 /
mg/L
<
/
May 2023
Week 4
0.113 /
mg/L
/
Feb 2023
Average
<
0.025 /
mg/L
<
/
May 2023
Average
0.113 /
mg/L
/
2023
Quarter t
<
0.025 /
mg/L
<
/
2023
Quarter 2
0.113 /
mg/L
/
2023
1st 6 Months (Avg)
<
0.069 /
mg/L
<
/
2023
lst 6 ...(Max)
0.113 /
mg/L
/
2023
Ist 6 ...(Min)
<
0.025 /
mg/L
<
/
2023
Ist 6 ...(Count)
2 /
/
Sample Date
SamplelD
Result/Limit
Mass /Limit
Zinc
02/21/2023
S
Aurobindo022123Self
0.062 /
mg/L
/
05/31/2023
P
Aurobindo053123POT
0.557 /
mg/L
/
W
Feb 2023
Week 3
0.062 /
mg/L
/
May 2023
Week 4
0.557 /
mg/L
/
Feb 2023
Average
0.062 /
mg/L
/
May 2023
Average
0.557 /
mg/L
/
2023
Quarter 1
0.062 /
mg/L
/
2023
Quarter 2
0.557 /
mg/L
/
2023
1st 6 Months (Avg)
0.310 /
mg/L
/
2023
Ist 6 ...(Max)
0.557 /
mg/L
/
2023
Ist 6 ...(Min)
0.062 /
mg/L
/
2023
Ist 6... (Count)
2
Tuesday, February 13, 2024 2:16:21PM * Indicates Violation ** Indicates TRC Violation Page 12 of 12

Biogen
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
03/31/2023 P
Biogen033123POTW
0.404
/ 12.19
mg/L
0.2391 /
lbs/day
Mar 2023
Week 4
0.404
/
mg/L
0.2391 /
lbs/day
Mar 2023
Average
0.404
/ 4.83
mg/L
0.2391 /
lbs/day
2023
Quarter 1
0.404
/
mg/L
0.2391 /
Ibs/day
2023
1st 6 Months (Avg)
0.404
/
mg/L
0.2391 /
Ibs/day
2023
lst6... (Max)
0.404
/
mg/L
0.2391 /
Ibs/day
2023
1st 6 ...(Min)
0.404
/
mg/L
0.2391 /
Ibs/day
2023
1st 6 ...(Count)
1
/
1 /
Sample Count: 1 Months Sampled:
1
Weeks Sampled:
1 Quarters Sampled :
1
# Over Daily C :
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00 # Over Qt Avg C :
0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC: 0
0.00 # Over Qt Avg C TRC
: 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00 # Over Qtr Avg M :
0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass /Limit
Ammonia
02/07/2023
S Biogen02O723Self
3.94
/ mg/L
/
03/31/2023
P Biogen033123POTW
3.2
/ mg/L
1.8941
/ Ibs/day
Feb 2023
Week 1
3.94
/ mg/L
/
Mar 2023
Week 4
3.2
/ mg/L
1.8941
/ lbs/day
Feb 2023
Average
3.94
/ mg/L
/
Mar 2023
Average
3.2
/ mg/L
1.8941
/ lbs/day
2023
Quarter 1
3.57
/ mg/L
1.8941
/ lbs/day
2023
1st 6 Months (Avg)
3.57
/ mg/L
1.8941
/ Ibs/day
2023
1st 6 ...(Max)
3.94
/ mg/L
1.8941
/ Ibs/day
2023
1st 6 ...(Min)
3.2
/ mg/L
/
2023
1st 6 ...(Count)
2
/
1
/
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2023
S
Biogen0123F1ow
02/28/2023
S
Biogen0223F1ow
03/31/2023
S
Biogen0323F1ow
04/30/2023
S
Biogen0423FIow
05/31/2023
S
Biogen0523F1ow
06/30/2023
S
Biogen0623F1ow
Jan 2023
Week 4
Feb 2023
Week 4
0.061501
/ MGD /
0.059464
/ MGD /
0.066957
/ MGD /
0.100021
/ MGD /
0.111299
/ MGD /
0.099426
/ MGD /
0.061501
/ MGD /
0.059464
/ MGD /
Tuesday, February 13, 2024 2:27:30PM * Indicates Violation ** Indicates TRC Violation Page 1 of 10

Biogen
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
Mar 2023
Week 4
0.066957
/
MGD
/
Apr 2023
Week 4
0.100021
/
MGD
/
May 2023
Week 4
0.111299
/
MGD
/
Jun 2023
Week 4
0.099426
/
MGD
/
Jan 2023
Average
0.061501
/
MGD
/
Feb 2023
Average
0.059464
/
MGD
/
Mar 2023
Average
0.066957
/
MGD
/
Apr 2023
Average
0.100021
/
MGD
/
May 2023
Average
0.111299
/
MGD
/
Jun 2023
Average
0.099426
/
MGD
/
2023
Quarter 1
0.062641
/
MGD
/
2023
Quarter 2
0.103582
/
MGD
/
2023
1st 6 Months (Avg)
0.083111
/
MGD
/
2023
lst6... (Max)
0.111299
/
MGD
/
2023
lst6... (Min)
0.059464
/
MGD
/
2023
1st 6 ...(Count)
6
Sample Date
SamplelD
Result/Limit
Mass /Limit
BOD
02/07/2023
S Biogen02O723Self
219
/
mg/L
/
03/31/2023
P Biogen033123POTW
82.5
/
mg/L
48.832 /
lbs/day
Feb 2023
Week 1
219
/
mg/L
/
Mar 2023
Week 4
82.5
/
mg/L
48.832 /
lbs/day
Feb 2023
Average
219
/
mg/L
/
Mar 2023
Average
82.5
/
mg/L
48.832 /
Ibs/day
2023
Quarter 1
150.8
/
mg/L
48.832 /
Ibs/day
2023
1st 6 Months (Avg)
150.8
/
mg/L
48.832 /
Ibs/day
2023
1st 6 ...(Max)
219
/
mg/L
48.832 /
Ibs/day
2023
1st 6 ...(Min)
82.5
/
mg/L
/
2023
1st 6 ...(Count)
2
/
1 /
Sample Date
SamplelD
Result/Limit
Mass/Limit
Cadmium
03/31/2023
P Biogen033123POTW
<
0.00008
/ mg/L
<
0.000044 /
lbs/day
Mar 2023
Week 4
<
0.00008
/ mg/L
<
0.000044 /
lbs/day
Mar 2023
Average
<
0.00008
/ mg/L
<
0.000044 /
Ibs/day
2023
Quarter 1
<
0.00008
/ mg/L
<
0.000044 /
Ibs/day
2023
1st 6 Months (Avg)
<
0.00008
/ mg/L
<
0.000044 /
Ibs/day
2023
1st 6 ...(Max)
<
0.00008
/ mg/L
<
0.000044 /
Ibs/day
2023
1st 6 ...(Min)
<
0.00008
/ mg/L
<
0.000044 /
Ibs/day
2023
1st 6 ...(Count)
1
/
1 /
Tuesday, February 13, 2024 2:27:30PM * Indicates Violation ** Indicates TRC Violation Page 2 of 10

Biogen
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
02/07/2023
S Biogen02O723Self
53.7
/ mg/L
/
03/31/2023
P Biogen033123POTW
55
/ mg/L
32.5544 /
lbs/day
Feb 2023
Week 1
53.7
/ mg/L
/
Mar 2023
Week 4
55
/ mg/L
32.5544 /
Ibs/day
Feb 2023
Average
53.7
/ mg/L
/
Mar 2023
Average
55
/ mg/L
32.5544 /
Ibs/day
2023
Quarter 1
54.35
/ mg/L
32.5544 /
Ibs/day
2023
1st 6 Months (Avg)
54.35
/ mg/L
32.5544 /
Ibs/day
2023
1st 6 ...(Max)
55
/ mg/L
32.5544 /
Ibs/day
2023
1st 6 ...(Min)
53.7
/ mg/L
/
2023
lst6... (Count)
2
/
1 /
Sample Date SamplelD Result/Limit Mass/Limit
COD
02/07/2023
S Biogen02O723Self
445
/ mg/L
/
03/31/2023
P Biogen033123POTW
180
/ mg/L
106.54 /
lbs/day
Feb 2023
Week 1
445
/ mg/L
/
Mar 2023
Week 4
180
/ mg/L
106.54 /
Ibs/day
Feb 2023
Average
445
/ mg/L
/
Mar 2023
Average
180
/ mg/L
106.54 /
lbs/day
2023
Quarter 1
312.5
/ mg/L
106.54 /
lbs/day
2023
1st 6 Months (Avg)
312.5
/ mg/L
106.54 /
lbs/day
2023
1st 6 ...(Max)
445
/ mg/L
106.54 /
lbs/day
2023
1st 6 ...(Min)
180
/ mg/L
/
2023
1st 6 ...(Count)
2
/
1 /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
02/07/2023
S Biogen02O723Self
<
0.003
10.05
mg/L
<
/
03/31/2023
P Biogen033123POTW
<
0.003
10.05
mg/L
<
0.00148 /
Ibs/day
Feb 2023
Week 1
<
0.003
/
mg/L
<
/
Mar 2023
Week 4
<
0.003
/
mg/L
<
0.00148 /
lbs/day
Feb 2023
Average
<
0.003
/ 0.04
mg/L
<
/
Mar 2023
Average
<
0.003
/ 0.04
mg/L
<
0.00148 /
lbs/day
2023
Quarter 1
<
0.003
/
mg/L
<
0.00148 /
lbs/day
2023
1st 6 Months (Avg)
<
0.003
/
mg/L
<
0.001480 /
Ibs/day
2023
lst6... (Max)
<
0.003
/
mg/L
<
0.001480 /
Ibs/day
2023
lst6... (Min)
<
0.003
/
mg/L
<
/
2023
1st 6 ...(Count)
2
/
1 /
Tuesday, February 13, 2024 2:27:30PM * Indicates Violation ** Indicates TRC Violation Page 3 of 10

Biogen
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 2 Months Sampled : 2
Weeks Sampled:
2 Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C:
0 0.00
# Over Wk Avg C :
0
0.00 # Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0 0.00
# Over Wk Avg C TRC :
0
0.00 # Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0 0.00
# Over Wk Avg M :
0
0.00 # Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0 0.00
# Over Wk Avg M TRC :
0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
Diroximel fumarate
02/07/2023 S
Biogen02O723SelfDRF
0.048
/
mg/L
0.02 / Ibs/day
Feb 2023
Week 1
0.048
/
mg/L
0.02 /
Feb 2023
Average
0.048
/
mg/L
0.02 /
2023
Quarter 1
0.048
/
mg/L
0.02 /
2023
1 st 6 Months (Avg)
0.048
/
mg/L
0.02 /
2023
1st 6 ...(Max)
0.048
/
mg/L
0.02 /
2023
1st 6 ...(Min)
0.048
/
mg/L
0.02 /
2023
lst 6 ... (Count)
1
/
I /
Sample Date
SamplelD
Result/Limit
Mass /Limit
Ethyl acetate
03/31/2023 P
Biogen033123POTW <
0.005
/ 12.19
mg/L
<
0.003 / Ibs/day
Mar 2023
Week 4 <
0.005
/
mg/L
<
0.003 / Ibs/day
Mar 2023
Average <
0.005
/ 4.83
mg/L
<
0.003 / Ibs/day
2023
Quarter 1 <
0.005
/
mg/L
<
0.003 / lbs/day
2023
1st 6 Months (Avg) <
0.005
/
mg/L
<
0.0030 / lbs/day
2023
1st 6 ...(Max) <
0.005
/
mg/L
<
0.0030 / lbs/day
2023
lst 6 ...(Min) <
0.005
/
mg/L
<
0.0030 / lbs/day
2023
1st 6 ...(Count)
1
/
1 /
Sample Count: 1 Months Sampled:
1
Weeks Sampled:
1 Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0 0.00
# Over Wk Avg C :
0
0.00 # Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0 0.00
# Over Wk Avg C TRC :
0
0.00 # Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0 0.00 # Over Mo Avg M :
0 0.00
# Over Wk Avg M :
0
0.00 # Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0 0.00
# Over Wk Avg M TRC :
0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
Fluoride
02/07/2023 S
Biogen02O723Self <
0.5
/
mg/L
<
/
03/31/2023 P
Biogen033123POTW
1.06
/
mg/L
0.6274 / lbs/day
Feb 2023
Week 1 <
0.5
/
mg/L
<
/
Tuesday, February 13, 2024 2:27:30PM * Indicates Violation ** Indicates TRC Violation Page 4 of 10

Biogen
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
Mar 2023
Week 4
1.06
/
mg/L
0.6274 /
Ibs/day
Feb 2023
Average
<
0.5
/
mg/L
<
/
Mar 2023
Average
1.06
/
mg/L
0.6274 /
lbs/day
2023
Quarter 1
<
0.78
/
mg/L
<
0.6274 /
Ibs/day
2023
1st 6 Months (Avg) <
0.78
/
mg/L
<
0.6274 /
Ibs/day
2023
lst6... (Max)
1.06
/
mg/L
0.6274 /
Ibs/day
2023
1st 6 ...(Min)
<
0.5
/
mg/L
<
/
2023
1st 6 ...(Count)
2
/
1 /
Sample Date
Sample./D
Result/Limit
Mass /Limit
Isopropyl acetate
03/31/2023 P
Biogen033123POTW <
0.005
/ 12.19
mg/L
<
0.003 /
Ibs/day
Mar 2023
Week 4
<
0.005
/
mg/L
<
0.003 /
lbs/day
Mar 2023
Average
<
0.005
/ 4.83
mg/L
<
0.003 /
lbs/day
2023
Quarter 1
<
0.005
/
mg/L
<
0.003 /
lbs/day
2023
1st 6 Months (Avg) <
0.005
/
mg/L
<
0.0030 /
lbs/day
2023
1st 6 ...(Max)
<
0.005
/
mg/L
<
0.0030 /
Ibs/day
2023
1st 6 ...(Min)
<
0.005
/
mg/L
<
0.0030 /
Ibs/day
2023
1st 6 ...(Count)
1
/
1 /
Sample Count: 1
Months Sampled:
1
Weeks Sampled
:
1 Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C :
0 0.00
# Over Wk Avg C :
0
0.00 # Over Qt Avg C :
0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0 0.00
# Over Wk Avg C TRC :
0
0.00 # Over Qt Avg C TRC
: 0
0.00
# Over Daily M:
0 0.00
# Over Mo Avg M :
0 0.00
# Over Wk Avg M :
0
0.00 # Over Qtr Avg M :
0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC :
0 0.00
# Over Wk Avg M TRC :
0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SarnplclD Result/Limit Mass/Limit
Mercury - LL
02/07/2023 S
Biogen02O723Self
0.000006
/ 0.000142
mg/L /
03/31/2023 P
Biogen033123POTWH
0.000003
/ 0.000142
mg/L /
g
Feb 2023
Week 1
0.000006
/
mg/L /
Mar 2023
Week 4
0.000003
/
mg/L /
Feb 2023
Average
0.000006
/
mg/L /
Mar 2023
Average
0.000003
/
mg/L /
2023
Quarter 1
0.000004
/
mg/L /
2023
1st 6 Months (Avg)
0.000004
/
mg/L /
2023
1st 6 ...(Max)
0.000006
/
mg/L /
2023
lst6... (Min)
0.000003
/
mg/L /
2023
lst6... .(Count)
2
Tuesday, February 13, 2024 2:27:30PM * Indicates Violation ** Indicates TRC Violation Page 5 of 10

Biogen
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
2
Months Sampled :
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
03/31/2023 P
Biogen033123POTW <
0.003
/ 1.77
mg/L
<
0.00148 / lbs/day
Mar 2023
Week 4
<
0.003
/
mg/L
<
0.00148 / Ibs/day
Mar 2023
Average
<
0.003
/ 0.41
mg/L
<
0.00148 / Ibs/day
2023
Quarter 1
<
0.003
/
mg/L
<
0.00148 / lbs/day
2023
1 st 6 Months (Avg) <
0.003
/
mg/L
<
0.001480 / lbs/day
2023
ist 6 ...(Max)
<
0.003
/
mg/L
<
0.001480 / Ibs/day
2023
1st 6 ...(Min)
<
0.003
/
mg/L
<
0.001480 / Ibs/day
2023
lst 6 ... (Count)
1
/
I /
Sample Count:
1
Months Sampled:
1
Weeks Sampled:
1 Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00 # Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00 # Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00 # Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC:
0
0.00
# Over Wk Avg M TRC :
0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
03/31/2023
P Biogen033123POTW
<
0.001
/ mg/L
<
0.0006 /
lbs/day
Mar 2023
Week 4
<
0.001
/ mg/L
<
0.0006 /
Ibs/day
Mar 2023
Average
<
0.001
/ mg/L
<
0.0006 /
Ibs/day
2023
Quarter 1
<
0.001
/ mg/L
<
0.0006 /
Ibs/day
2023
1st 6 Months (Avg)
<
0.001
/ mg/L
<
0.0006 /
lbs/day
2023
1st 6 ...(Max)
<
0.001
/ mg/L
<
0.0006 /
lbs/day
2023
1st 6 ...(Min)
<
0.001
/ mg/L
<
0.0006 /
lbs/day
2023
1st 6 ...(Count)
1
/
I /
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
03/31/2023 P Biogen033123POTW <
Mar 2023 Week 4 <
Mar 2023 Average <
0.005 / 12.19 mg/L < 0.003 / Ibs/day
0.005 / mg/L < 0.003 / Ibs/day
0.005 / 4.83 mg/L < 0.003 / Ibs/day
Tuesday, February 13, 2024 2:27:30PM * Indicates Violation ** Indicates TRC Violation Page 6 of 10

Biogen
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
2023
Quarter 1
<
0.005
/
mg/L <
0.003 / lbs/day
2023
1st 6 Months (Avg) <
0.005
/
mg/L <
0.0030 / lbs/day
2023
lst6... (Max)
<
0.005
/
mg/L <
0.0030 / lbs/day
2023
1st 6 ...(Min)
<
0.005
/
mg/L <
0.0030 / lbs/day
2023
1st 6 ...(Count)
1
/
I /
Sample Count: l
Months Sampled:
I
Weeks Sampled :
I Quarters Sampled :
I
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00 # Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00 # Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00 # Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate -Nitrite
02/07/2023 S
Biogen02O723Self
0.7
/ mg/L
/
03/31/2023 P
Biogen033123POTW
0.4
/ mg/L
0.243 /
lbs/day
Feb 2023
Week 1
0.7
/ mg/L
/
Mar 2023
Week 4
0.4
/ mg/L
0.243 /
Ibs/day
Feb 2023
Average
0.7
/ mg/L
/
Mar 2023
Average
0.4
/ mg/L
0.243 /
Ibs/day
2023
Quarter 1
0.6
/ mg/L
0.243 /
lbs/day
2023
1st 6 Months (Avg)
0.6
/ mg/L
0.243 /
lbs/day
2023
1st 6 ...(Max)
0.7
/ mg/L
0.243 /
lbs/day
2023
lst 6 ...(Min)
0.4
/ mg/L
/
2023
1st 6 ...(Count)
2
/
I /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen, Total
02/07/2023 S
Biogen02O723Self
31.3
/ mg/L
/
03/31/2023 P
Biogen033123POTW
14.2
/ mg/L
8.405 /
Ibs/day
Feb 2023
Week 1
31.3
/ mg/L
/
Mar 2023
Week 4
14.2
/ mg/L
8.405 /
Ibs/day
Feb 2023
Average
31.3
/ mg/L
/
Mar 2023
Average
14.2
/ mg/L
8.405 /
lbs/day
2023
Quarter 1
22.75
/ mg/L
8.405 /
lbs/day
2023
1st 6 Months (Avg)
22.75
/ mg/L
8.405 /
Ibs/day
2023
1st 6 ...(Max)
31.3
/ mg/L
8.405 /
Ibs/day
2023
lst6... (Min)
14.2
/ mg/L
/
2023
1st 6 ...(Count)
2
/
1 /
Tuesday, February 13, 2024 2:27:30PM * Indicates Violation ** Indicates TRC Violation Page 7 of 10

Biogen
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Oil & Grease, Total
02/07/2023 S
Biogen02O723Self
9.9
/ 200
mg/L
/
03/31/2023 P
Biogen033123POTW <
2.5
/ 200
mg/L <
/
Feb 2023
Week 1
9.9
/
mg/L
/
Mar 2023
Week 4 <
2.5
/
mg/L <
/
Feb 2023
Average
9.9
/
mg/L
/
Mar 2023
Average <
2.5
/
mg/L <
/
2023
Quarter 1 <
6.2
/
mg/L <
/
2023
1st 6 Months (Avg) <
6.2
/
mg/L <
/
2023
1st 6 ...(Max)
9.9
/
mg/L
/
2023
1st 6 ...(Min) <
2.5
/
mg/L <
/
2023
1st 6... (Count)
2
Sample Count: 2 Months Sampled
:
2
Weeks Sampled :
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
02/07/2023 S
Biogen020723Se1f
9.4
/ 5.5 - 10.5
SU
/
03/31/2023 P
Biogen033123POTW
6.8
/ 5.5 - 10.5
SU
/
Feb 2023
Week 1
9.4
/
SU
/
Mar 2023
Week 4
6.8
/
SU
/
Feb 2023
Average
9.4
/
SU
/
Mar 2023
Average
6.8
/
SU
/
2023
Quarter 1
8.1
/
SU
/
2023
1st 6 Months (Avg)
8.1
/
SU
/
2023
1st 6 ...(Max)
9.4
/
SU
/
2023
1st 6 ...(Min)
6.8
/
SU
/
2023
1st 6 ...(Count)
2
Sample Count : 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Tuesday, February 13, 2024 2:27:30PM * Indicates Violation ** Indicates TRC Violation Page 8 of 10

Biogen
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
02/07/2023 S
Biogen02O723Self
22.4
/ 66
°C
/
03/31/2023 P
Biogen033123POTW
29
/ 66
°C
/
Feb 2023
Week 1
22.4
/
°C
/
Mar 2023
Week 4
29
/
°C
/
Feb 2023
Average
22.4
/
°C
/
Mar 2023
Average
29
/
°C
/
2023
Quarter 1
25.7
/
°C
/
2023
1st 6 Months (Avg)
25.7
/
°C
/
2023
1st 6 ...(Max)
29
/
°C
/
2023
1st 6 ...(Min)
22.4
/
°C
/
2023
lst 6 ... (Count)
2
Sample Count: 2 Months Sampled
:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
02/07/2023
S Biogen02O723Self
30.6
/ mg/L
/
03/31/2023
P Biogen033123POTW
13.8
/ mg/L
8.168 /
lbs/day
Feb 2023
Week 1
30.6
/ mg/L
/
Mar 2023
Week 4
13.8
/ mg/L
8.168 /
lbs/day
Feb 2023
Average
30.6
/ mg/L
/
Mar 2023
Average
13.8
/ mg/L
8.168 /
Ibs/day
2023
Quarter 1
22.2
/ mg/L
8.168 /
Ibs/day
2023
1st 6 Months (Avg)
22.2
/ mg/L
8.168 /
Ibs/day
2023
1st 6 ...(Max)
30.6
/ mg/L
8.168 /
lbs/day
2023
1st 6 ...(Min)
13.8
/ mg/L
/
2023
1st 6 ...(Count)
2
/
I /
Sample Date
SamplelD
Result/Limit
Mass/Limit
Total Phosphorus
02/07/2023 S
Biogen02O723Self
12.2 /
mg/L
/
03/31/2023 P
Biogen033123POTW
2.21 /
mg/L
1.3081 / Ibs/day
Feb 2023
Week 1
12.2 /
mg/L
/
Mar 2023
Week 4
2.21 /
mg/L
1.3081 / Ibs/day
Feb 2023
Average
12.2 /
mg/L
/
Tuesday, February 13, 2024 2:27:30PM * Indicates Violation ** Indicates TRC Violation Page 9 of 10

Biogen
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
Total Phosphorus
Mar 2023
Average
2.21 /
mg/L
1.3081 /
lbs/day
2023
Quarter 1
7.205 /
mg/L
1.3081 /
lbs/day
2023
1 st 6 Months (Avg)
7.205 /
mg/L
1.3081 /
lbs/day
2023
ist 6 ...(Max)
12.2 /
mg/L
1.3081 /
lbs/day
2023
1st 6 ...(Min)
2.21 /
mg/L
/
2023
lst6... (Count)
2 /
I /
Sample Date
SamplelD
Result/Limit
Mass /Limit
TSS
02/07/2023 S
Biogen02O723Self
420 /
mg/L
/
03/31/2023 P
Biogen033123POTW
174 /
mg/L
102.990276 /
lbs/day
Feb 2023
Week 1
420 /
mg/L
/
Mar 2023
Week 4
174 /
mg/L
102.990276 /
lbs/day
Feb 2023
Average
420 /
mg/L
/
Mar 2023
Average
174 /
mg/L
102.990276 /
lbs/day
2023
Quarter 1
297 /
mg/L
102.990276 /
lbs/day
2023
1st 6 Months (Avg)
297 /
mg/L
102.99 /
Ibs/day
2023
1st 6 ...(Max)
420 /
mg/L
102.990276 /
Ibs/day
2023
lst6... (Min)
174 /
mg/L
/
2023
1st 6 ...(Count)
2 /
1 /
Sample Date
SamplelD
Result/Limit
Mass/Limit
Zinc
02/07/2023
S Biogen02O723Self
0.641
/ mg/L
03/31/2023
P Biogen033123POTW
0.267
/ mg/L
Feb 2023
Week 1
0.641
/ mg/L
Mar 2023
Week 4
0.267
/ mg/L
Feb 2023
Average
0.641
/ mg/L
Mar 2023
Average
0.267
/ mg/L
2023
Quarter 1
0.454
/ mg/L
2023
1st 6 Months (Avg)
0.454
/ mg/L
2023
1st 6 ...(Max)
0.641
/ mg/L
2023
1st 6 ...(Min)
0.267
/ mg/L
2023
lst 6 ... (Count)
2
/
0.158037
/ lbs/day
0.158037
/ lbs/day
0.158037
/ Ibs/day
0.158037
/ Ibs/day
0.158037
/ Ibs/day
0.158037
/ Ibs/day
1
/
Tuesday, February 13, 2024 2:27:30PM * Indicates Violation ** Indicates TRC Violation Page 10 of 10

Cintas Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result/Limit Mass/Limit
Aluminum
01/17/2023
S CintasO11723Self
0.83
/
mg/L
0.504047 /
lbs/day
Jan 2023
Week 3
0.83
/
mg/L
0.504047 /
lbs/day
Jan 2023
Average
0.83
/
mg/L
0.504047 /
lbs/day
2023
Quarter 1
0.83
/
mg/L
0.504047 /
Ibs/day
2023
1st 6 Months (Avg)
0.83
/
mg/L
0.504047 /
Ibs/day
2023
lst6... (Max)
0.83
/
mg/L
0.504047 /
Ibs/day
2023
1st 6 ...(Min)
0.83
/
mg/L
0.504047 /
Ibs/day
2023
1st 6 ...(Count)
1
/
1 /
Sample Date
SampleID
Result/Limit
Mass/Limit
Ammonia
01/17/2023
S Cintas011723Self
9.9
/
mg/L
6.0121 /
Ibs/day
02/14/2023
S Cintas021423Self
2.8
/
mg/L
1.4527 /
lbs/day
04/14/2023
P Cintas041423POTW
4.9
/
mg/L
/
Jan 2023
Week 3
9.9
/
mg/L
6.0121 /
lbs/day
Feb 2023
Week 2
2.8
/
mg/L
1.4527 /
lbs/day
Apr 2023
Week 2
4.9
/
mg/L
/
Jan 2023
Average
9.9
/
mg/L
6.0121 /
Ibs/day
Feb 2023
Average
2.8
/
mg/L
1.4527 /
Ibs/day
Apr 2023
Average
4.9
/
mg/L
/
2023
Quarter 1
6.35
/
mg/L
3.7324 /
lbs/day
2023
Quarter 2
4.9
/
mg/L
/
2023
1st 6 Months (Avg)
5.87
/
mg/L
3.7324 /
lbs/day
2023
lst 6 ...(Max)
9.9
/
mg/L
6.0121 /
lbs/day
2023
1st 6 ...(Min)
2.8
/
mg/L
/
2023
1st 6 ...(Count)
3
/
2 /
Sample Date SampleID Result/Limit Mass /Limit
Average Flow for Month
01/31/2023
S
Cintas0123Flow
02/28/2023
S
Cintas0223Flow
03/31/2023
S
Cintas0323FIow
04/30/2023
S
Cintas0423Flow
05/31/2023
S
Cintas0523F1ow
06/30/2023
S
Cintas0623Flow
Jan 2023
Week 4
Feb 2023
Week 4
Mar 2023
Week 4
Apr 2023
Week 4
May 2023
Week 4
Jun 2023
Week 4
Jan 2023
Average
Saturday, February 24, 2024 11:38:55AM
0.056996 /
MGD /
0.052314 /
MGD /
0.052803 /
MGD /
0.047155 /
MGD /
0.038012 /
MGD /
0.040116 /
MGD /
0.056996 /
MGD /
0.052314 /
MGD /
0.052803 /
MGD /
0.047155 /
MGD /
0.038012 /
MGD /
0.040116 /
MGD /
0.056996 / 0.100
MGD /
* Indicates Violation
** Indicates TRC Violation
Page 1 of 13

Cintas Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
Feb 2023
Average
0.052314
/ 0.100
MGD
/
Mar 2023
Average
0.052803
/ 0.100
MGD
/
Apr 2023
Average
0.047155
/ 0.100
MGD
/
May 2023
Average
0.038012
/ 0.100
MGD
/
Jun 2023
Average
0.040116
/ 0.100
MGD
/
2023
Quarter 1
0.054038
/
MGD
/
2023
Quarter 2
0.041761
/
MGD
/
2023
1st 6 Months (Avg) 0.047899
/
MGD
/
2023
1st 6 ...(Max)
0.056996
/
MGD
/
2023
1st 6 ...(Min)
0.038012
/
MGD
/
2023
lst 6 ... (Count)
6
Sample Count: 6
Months Sampled:
6
Weeks Sampled:
6
Quarters Sampled :
2
# Over Daily C:
0 0.00
# Over Mo Avg C :
0 0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0 0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0 0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC :
0 0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
BOD
01/17/2023
S
Cintas011723Self
521
/ mg/L
316.396 /
lbs/day
01/19/2023
P
Cintas011923POTW
291
/ mg/L
/
02/14/2023
P
Cintas021423POTW
242
/ mg/L
/
02/14/2023
S
Cintas021423Self
283
/ mg/L
146.825 /
lbs/day
03/07/2023
S
Cintas03 0723 Self
326
/ mg/L
187.208 /
Ibs/day
03/14/2023
P
Cintas031423POTW
384
/ mg/L
/
04/04/2023
S
Cintas04O423Self
197
/ mg/L
71.963 /
Ibs/day
04/14/2023
P
Cintas041423POTW
490
/ mg/L
/
05/04/2023
S
Cintas05 0423 Self
897
/ mg/L
241.306 /
lbs/day
05/12/2023
P
Cintas051223POTW
902
/ mg/L
/
06/08/2023
S
Cintas06O823Self
588
/ mg/L
290.704 /
lbs/day
06/22/2023
P
Cintas062223POTW
567
/ mg/L
/
Jan 2023
Week 3
406
/ mg/L
316.396 /
Ibs/day
Feb 2023
Week 2
262.5
/ mg/L
146.825 /
Ibs/day
Mar 2023
Week 1
326
/ mg/L
187.208 /
Ibs/day
Mar 2023
Week 2
384
/ mg/L
/
Apr 2023
Week 1
197
/ mg/L
71.963 /
lbs/day
Apr 2023
Week 2
490
/ mg/L
/
May 2023
Week 1
897
/ mg/L
241.306 /
lbs/day
May 2023
Week 2
902
/ mg/L
/
Saturday, February 24, 2024 11:38:55AM * Indicates Violation ** Indicates TRC Violation Page 2 of 13

Cintas Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
BOD
Jun 2023
Week 2
588
/ mg/L
290.704 /
Ibs/day
Jun 2023
Week 4
567
/ mg/L
/
Jan 2023
Average
406
/ mg/L
316.396 /
lbs/day
Feb 2023
Average
262.5
/ mg/L
146.825 /
Ibs/day
Mar 2023
Average
355
/ mg/L
187.208 /
Ibs/day
Apr 2023
Average
343.5
/ mg/L
71.963 /
Ibs/day
May 2023
Average
899.5
/ mg/L
241.306 /
Ibs/day
Jun 2023
Average
577.5
/ mg/L
290.704 /
Ibs/day
2023
Quarter 1
341.2
/ mg/L
216.81 /
Ibs/day
2023
Quarter 2
606.8
/ mg/L
201.324 /
lbs/day
2023
1 st 6 Months (Avg)
474
/ mg/L
209.067 /
lbs/day
2023
ist 6 ...(Max)
902
/ mg/L
316.396 /
Ibs/day
2023
1st 6 ...(Min)
197
/ mg/L
/
2023
lst6... (Count)
12
/
6 /
Sample Date SamplelD Result/Limit Mass /Limit
Chloride
01/17/2023
S Cintas011723Self
104
/ mg/L
63.1577 /
Ibs/day
04/14/2023
P Cintas041423POTW
68.2
/ mg/L
/
Jan 2023
Week 3
104
/ mg/L
63.1577 /
Ibs/day
Apr 2023
Week 2
68.2
/ mg/L
/
Jan 2023
Average
104
/ mg/L
63.1577 /
lbs/day
Apr 2023
Average
68.2
/ mg/L
/
2023
Quarter 1
104
/ mg/L
63.1577 /
lbs/day
2023
Quarter 2
68.2
/ mg/L
/
2023
1st 6 Months (Avg)
86.1
/ mg/L
63.1577 /
Ibs/day
2023
1st 6 ...(Max)
104
/ mg/L
63.1577 /
Ibs/day
2023
1st 6 ...(Min)
68.2
/ mg/L
/
2023
1st 6 ...(Count)
2
/
I /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
01/17/2023
S CintasO11723Self
Jan 2023
Week 3
Jan 2023
Average
2023
Quarter
2023
1st 6 Months (Avg)
2023
1st 6 ...(Max)
2023
1st 6 ...(Min)
2023
1st 6 ...(Count)
0.068 /
mg/L
0.041295 /
lbs/day
0.068 /
mg/L
0.041295 /
lbs/day
0.068 /
mg/L
0.041295 /
lbs/day
0.068 /
mg/L
0.041295 /
Ibs/day
0.068 /
mg/L
0.041295 /
Ibs/day
0.068 /
mg/L
0.041295 /
Ibs/day
0.068 /
mg/L
0.041295 /
Ibs/day
1 /
I /
Saturday, February 24, 2024 11:38:55AM * Indicates Violation ** Indicates TRC Violation Page 3 of 13

Cintas Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
01/17/2023 S
CintasO11723Self <
0.05
/
mg/L
<
0.0304 /
Ibs/day
04/14/2023 P
Cintas041423POTW
0.58
/
mg/L
/
Jan 2023
Week 3 <
0.05
/
mg/L
<
0.0304 /
lbs/day
Apr 2023
Week 2
0.58
/
mg/L
/
Jan 2023
Average <
0.05
/
mg/L
<
0.0304 /
Ibs/day
Apr 2023
Average
0.58
/
mg/L
/
2023
Quarter 1 <
0.05
/
mg/L
<
0.0304 /
Ibs/day
2023
Quarter 2
0.58
/
mg/L
/
2023
1st 6 Months (Avg) <
0.32
/
mg/L
<
0.0304 /
Ibs/day
2023
1st 6 ...(Max)
0.58
/
mg/L
0.0304 /
lbs/day
2023
1st 6... (Min) <
0.05
/
mg/L
<
/
2023
1st 6 ...(Count)
2
/
1 /
SanrpleDate
SaamplelD
Result/Limit
Mass/Limit
Mercury - LL
01/17/2023 S
Cintas011723Self lg <
0.000001
/ 0.000142
mg/L
<
/
04/14/2023 P
Cintas041423POTWH
0.000048
/ 0.000142
mg/L
/
g
Jan 2023
Week 3 <
0.000001
/
mg/L
<
/
Apr 2023
Week 2
0.000048
/
mg/L
/
Jan 2023
Average <
0.000001
/
mg/L
<
/
Apr 2023
Average
0.000048
/
mg/L
/
2023
Quarter 1 <
0.000001
/
mg/L
<
/
2023
Quarter 2
0.000048
/
mg/L
/
2023
1st 6 Months (Avg) <
0.000024
/
mg/L
<
/
2023
lst 6 ...(Max)
0.000048
/
mg/L
/
2023
1st 6 ...(Min) <
0.000001
/
mg/L
<
/
2023
lst6... (Count)
2
Sample Count: 2 Months Sampled
: 2
Weeks Sampled:
2 Quarters Sampled :
2
# Over Daily C :
0 0.00 # Over Mo Avg C :
0 0.00
# Over Wk Avg C :
0
0.00 # Over Qt Avg C :
0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC
:
0 0.00
# Over Wk Avg C TRC:
0
0.00 # Over Qt Avg C TRC
: 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0 0.00
# Over Wk Avg M :
0
0.00 # Over Qtr Avg M :
0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC
:
0 0.00
# Over Wk Avg M TRC :
0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD
Result/Limit
Mass/Limit
Nickel
01/17/2023 S Cintas011723Self
0.016 /
mg/L
0.009717 /
Ibs/day
Jan 2023 Week 3
0.016 /
mg/L
0.009717 /
Ibs/day
Jan 2023 Average
0.016 /
mg/L
0.009717 /
Ibs/day
Saturday, February 24, 2024 11:38:55AM
* Indicates Violation
** Indicates TRC Violation
Page 4 of 13

Cintas Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SampleID
Result/Limit
Mass/Limit
Nickel
2023
Quarter 1
0.016 /
mg/L
0.009717 /
lbs/day
2023
1st 6 Months (Avg)
0.016 /
mg/L
0.009717 /
lbs/day
2023
lst6... (Max)
0.016 /
mg/L
0.009717 /
lbs/day
2023
1st 6 ...(Min)
0.016 /
mg/L
0.009717 /
lbs/day
2023
1st 6 ...(Count)
1 /
1 /
Sample Date
SampleID
Result/Limit
Mass/Limit
Nitrate -Nitrite
01/17/2023
S Cintas011723Self
0.1
/ mg/L
0.045 /
lbs/day
02/14/2023
S Cintas021423Self
0.1
/ mg/L
0.026 /
Ibs/day
03/07/2023
S Cintas03 0723 Self
0.1
/ mg/L
0.063 /
lbs/day
04/04/2023
S Cintas04O423Self
0.1
/ mg/L
0.019 /
lbs/day
04/14/2023
P Cintas041423POTW <
0.1
/ mg/L
< /
05/04/2023
S Cintas050423Self
0.4
/ mg/L
0.102 /
lbs/day
06/08/2023
S Cintas06O823Self
0.1
/ mg/L
0.069 /
ibs/day
Jan 2023
Week 3
0.1
/ mg/L
0.045 /
lbs/day
Feb 2023
Week 2
0.1
/ mg/L
0.026 /
lbs/day
Mar 2023
Week 1
0.1
/ mg/L
0.063 /
ibs/day
Apr 2023
Week 1
0.1
/ mg/L
0.019 /
lbs/day
Apr 2023
Week 2 <
0.1
/ mg/L
< /
May 2023
Week 1
0.4
/ mg/L
0.102 /
lbs/day
Jun 2023
Week 2
0.1
/ mg/L
0.069 /
lbs/day
Jan 2023
Average
0.1
/ mg/L
0.045 /
ibs/day
Feb 2023
Average
0.1
/ mg/L
0.026 /
lbs/day
Mar 2023
Average
0.1
/ mg/L
0.063 /
lbs/day
Apr 2023
Average <
0.1
/ mg/L
< 0.019 /
ibs/day
May 2023
Average
0.4
/ mg/L
0.102 /
lbs/day
Jun 2023
Average
0.1
/ mg/L
0.069 /
lbs/day
2023
Quarter 1
0.1
/ mg/L
0.045 /
lbs/day
2023
Quarter 2 <
0.2
/ mg/L
< 0.063 /
lbs/day
2023
1st 6 Months (Avg) <
0.1
/ mg/L
< 0.054 /
ibs/day
2023
lst 6 ...(Max)
0.4
/ mg/L
0.102 /
lbs/day
2023
1st 6 ...(Min)
0.1
/ mg/L
/
2023
1st 6 ...(Count)
7
/
6 /
Sample Date SampleID Result/Limit Mass /Limit
Nitrogen, Total
01/17/2023
S Cintas011723Self
02/14/2023
S Cintas021423Self
03/07/2023
S Cintas03 0723 Self
04/04/2023
S Cintas04O423Self
04/14/2023
P Cintas041423POTW
Saturday, February 24, 2024 11:38:55AM
42.7 /
mg/L
14.1 /
mg/L
38.8 /
mg/L
16.3 /
mg/L
30.9 /
mg/L
* Indicates Violation ** Indicates TRC Violation
25.931 / Ibs/day
7.315 / Ibs/day
22.281 / Ibs/day
5.954 / lbs/day
Page 5 of 13

Cintas Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen, Total
05/04/2023 S
Cintas05O423Self
30.9
/ mg/L
8.313 /
lbs/day
06/08/2023 S
Cintas06O823Self
61.5
/ mg/L
30.405 /
lbs/day
Jan 2023
Week 3
42.7
/ mg/L
25.931 /
lbs/day
Feb 2023
Week 2
14.1
/ mg/L
7.315 /
Ibs/day
Mar 2023
Week 1
38.8
/ mg/L
22.281 /
Ibs/day
Apr 2023
Week 1
16.3
/ mg/L
5.954 /
Ibs/day
Apr 2023
Week 2
30.9
/ mg/L
/
May 2023
Week 1
30.9
/ mg/L
8.313 /
Ibs/day
Jun 2023
Week 2
61.5
/ mg/L
30.405 /
Ibs/day
Jan 2023
Average
42.7
/ mg/L
25.931 /
lbs/day
Feb 2023
Average
14.1
/ mg/L
7.315 /
lbs/day
Mar 2023
Average
38.8
/ mg/L
22.281 /
Ibs/day
Apr 2023
Average
23.6
/ mg/L
5.954 /
Ibs/day
May 2023
Average
30.9
/ mg/L
8.313 /
Ibs/day
Jun 2023
Average
61.5
/ mg/L
30.405 /
Ibs/day
2023
Quarter 1
31.87
/ mg/L
18.509 /
Ibs/day
2023
Quarter 2
34.9
/ mg/L
14.891 /
Ibs/day
2023
1st 6 Months (Avg)
33.6
/ mg/L
16.7 /
lbs/day
2023
lst6... (Max)
61.5
/ mg/L
30.405 /
lbs/day
2023
1st 6 ...(Min)
14.1
/ mg/L
/
2023
1st 6 ...(Count)
7
/
6 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil & Grease, HEM (Polar)
01/17/2023
S
Cintas011723Self
02/14/2023
S
Cintas021423Self
03/07/2023
S
Cintas03 0723 Self <
04/04/2023
S
Cintas04O423Self <
04/14/2023
P
Cintas041423POTW <
05/04/2023
S
Cintas05O423Self
06/08/2023
S
Cintas06O823Self <
Jan 2023
Week 3
Feb 2023
Week 2
Mar 2023
Week 1 <
Apr 2023
Week 1 <
Apr 2023
Week 2 <
May 2023
Week 1
Jun 2023
Week 2 <
Jan 2023
Average
Feb 2023
Average
Mar 2023
Average <
Apr 2023
Average <
10.4
/ 100
mg/L
6.315769 /
Ibs/day
13.5
/ 100
mg/L
7.003999 /
Ibs/day
2.5
/ 100
mg/L
<
1.435648 /
Ibs/day
2.5
/ 100
mg/L
<
0.91323 /
Ibs/day
2.5
/ 100
mg/L
<
/
61.7
/ 100
mg/L
16.598228 /
lbs/day
2.5
/ 100
mg/L
<
1.235988 /
lbs/day
10.4
/
mg/L
6.315769 /
lbs/day
13.5
/
mg/L
7.003999 /
Ibs/day
2.5
/
mg/L
<
1.435648 /
Ibs/day
2.5
/
mg/L
<
0.91323 /
Ibs/day
2.5
/
mg/L
<
/
61.7
/
mg/L
16.598228 /
lbs/day
2.5
/
mg/L
<
1.235988 /
lbs/day
10.4
/
mg/L
6.315769 /
lbs/day
13.5
/
mg/L
7.003999 /
lbs/day
2.5
/
mg/L
<
1.435648 /
Ibs/day
2.5
/
mg/L
<
0.91323 /
Ibs/day
Saturday, February 24, 2024 11:38:55AM * Indicates Violation ** Indicates TRC Violation Page 6 of 13

Cintas Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Oil & Grease, HEM (Polar)
May 2023
Average
61.7
/
mg/L
16.598228 / lbs/day
Jun 2023
Average
<
2.5
/
mg/L <
1.235988 / lbs/day
2023
Quarter 1
<
8.8
/
mg/L <
4.918472 / lbs/day
2023
Quarter 2
<
17.3
/
mg/L <
6.249149 / Ibs/day
2023
1st 6 Months (Avg) <
13.7
/
mg/L <
5.58381 / Ibs/day
2023
lst6... (Max)
61.7
/
mg/L
16.598228 / Ibs/day
2023
1st 6 ...(Min)
<
2.5
/
mg/L <
/
2023
1st 6 ...(Count)
7
/
6 /
Sample Count: 7
Months Sampled:
6
Weeks Sampled:
7 Quarters Sampled :
2
# Over Daily C:
0 0.00
# Over Mo Avg C:
0
0.00
# Over Wk Avg C : 0
0.00 # Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00 # Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00 # Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass /Limit
Oil & Grease, SGT-HEM (Non -Polar)
01/17/2023
S
Cintas011723Self
02/14/2023
S
Cintas021423Self
03/07/2023
S
Cintas03 0723 Self
04/04/2023
S
Cintas04O423Self
04/14/2023
P
Cintas041423POTW
05/04/2023
S
Cintas05O423Self
06/08/2023
S
Cintas060823Self
Jan 2023
Week 3
Feb 2023
Week 2
Mar 2023
Week 1
Apr 2023
Week 1
Apr 2023
Week 2
May 2023
Week 1
Jun 2023
Week 2
Jan 2023
Average
Feb 2023
Average
Mar 2023
Average
Apr 2023
Average
May 2023
Average
Jun 2023
Average
2023
Quarter 1
2023
Quarter
2023
1st 6 Months (Avg)
< 2.5
/ 100
mg/L
<
1.5182 /
Ibs/day
< 2.5
/ 100
mg/L
<
1.297 /
Ibs/day
< 2.5
/ 100
mg/L
<
1.4356 /
Ibs/day
< 2.5
/ 100
mg/L
<
0.9132 /
lbs/day
< 2.5
/ 100
mg/L
<
/
16.6
/ 100
mg/L
4.4656 /
lbs/day
< 2.5
/ 100
mg/L
<
1.236 /
lbs/day
< 2.5
/
mg/L
<
1.5182 /
Ibs/day
< 2.5
/
mg/L
<
1.297 /
Ibs/day
< 2.5
/
mg/L
<
1.4356 /
Ibs/day
< 2.5
/
mg/L
<
0.9132 /
Ibs/day
< 2.5
/
mg/L
<
/
16.6
/
mg/L
4.4656 /
lbs/day
< 2.5
/
mg/L
<
1.236 /
lbs/day
< 2.5
/
mg/L
<
1.5182 /
lbs/day
< 2.5
/
mg/L
<
1.297 /
Ibs/day
< 2.5
/
mg/L
<
1.4356 /
Ibs/day
< 2.5
/
mg/L
<
0.9132 /
Ibs/day
16.6
/
mg/L
4.4656 /
Ibs/day
< 2.5
/
mg/L
<
1.236 /
lbs/day
< 2.5
/
mg/L
<
1.417 /
lbs/day
< 6
/
mg/L
<
2.205 /
lbs/day
< 4.5
/
mg/L
<
1.8110 /
lbs/day
Saturday, February 24, 2024 11:38:55AM * Indicates Violation ** Indicates TRC Violation Page 7 of 13

Cintas Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Oil & Grease, SGT-HEM (Non -Polar)
2023
1st 6 ...(Max)
16.6 /
mg/L
4.4656
/ Ibs/day
2023
1st 6 ...(Min)
< 2.5 /
mg/L <
/
2023
1st 6 ...(Count)
7 /
6 /
Sample Count:
7
Months Sampled :
6
Weeks Sampled:
7
Quarters Sampled :
2
# Over Daily C:
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
01/17/2023
S
Cintas0I1723Self
7.6
/ 6.0 - 10.5
SU /
02/14/2023
S
Cintas021423Self
7.2
/ 6.0 - 10.5
SU /
03/07/2023
S
Cintas03 0723 Self
7.1
/ 6.0 - 10.5
SU /
04/04/2023
S
Cintas04O423Self
7.3
/ 6.0 - 10.5
SU /
04/14/2023
P
Cintas041423POTW
7.3
/ 6.0 - 10.5
SU /
05/04/2023
S
Cintas05 0423 Self
7.3
/ 6.0 - 10.5
SU /
06/08/2023
S
Cintas06O823Self
7.3
/ 6.0 - 10.5
SU /
Jan 2023
Week 3
7.6
/
SU /
Feb 2023
Week 2
7.2
/
SU /
Mar 2023
Week 1
7.1
/
SU /
Apr 2023
Week 1
7.3
/
SU /
Apr 2023
Week 2
7.3
/
SU /
May 2023
Week 1
7.3
/
SU /
Jun 2023
Week 2
7.3
/
SU /
Jan 2023
Average
7.6
/
SU /
Feb 2023
Average
7.2
/
SU /
Mar 2023
Average
7.1
/
SU /
Apr 2023
Average
7.3
/
SU /
May 2023
Average
7.3
/
SU /
Jun 2023
Average
7.3
/
SU /
2023
Quarter 1
7.3
/
SU /
2023
Quarter 2
7.3
/
SU /
2023
1st 6 Months (Avg)
7.3
/
SU /
2023
1st 6 ...(Max)
7.6
/
SU /
2023
1st 6 ...(Min)
7.1
/
SU /
2023
1st 6 ...(Count)
7
Saturday, February 24, 2024 11:38:55AM * Indicates Violation ** Indicates TRC Violation Page 8 of 13

Cintas Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
7
Months Sampled :
6
Weeks Sampled:
7
Quarters Sampled :
2
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
01/17/2023 S
Cintas011723Self
27.1
/ 66
°C
/
02/14/2023 S
Cintas021423Self
29.7
/ 66
°C
/
03/07/2023 S
Cintas03 0723 Self
31.3
/ 66
°C
/
04/04/2023 S
Cintas04O423Self
32.3
/ 66
°C
/
04/14/2023 P
Cintas041423POTW
24
/ 66
°C
/
05/04/2023 S
Cintas050423Self
30.8
/ 66
°C
/
06/08/2023 S
Cintas06O823Self
32.3
/ 66
°C
/
Jan 2023
Week 3
27.1
/
°C
/
Feb 2023
Week 2
29.7
/
°C
/
Mar 2023
Week 1
31.3
/
°C
/
Apr 2023
Week 1
32.3
/
°C
/
Apr 2023
Week 2
24
/
°C
/
May 2023
Week 1
30.8
/
°C
/
Jun 2023
Week 2
32.3
/
°C
/
Jan 2023
Average
27.1
/
°C
/
Feb 2023
Average
29.7
/
°C
/
Mar 2023
Average
31.3
/
°C
/
Apr 2023
Average
28.2
/
°C
/
May 2023
Average
30.8
/
°C
/
Jun 2023
Average
32.3
/
°C
/
2023
Quarter 1
29.4
/
°C
/
2023
Quarter 2
29.9
/
°C
/
2023
1st 6 Months (Avg)
29.6
/
°C
/
2023
lst6... (Max)
32.3
/
°C
/
2023
lst6... (Min)
24
/
°G
/
2023
1st 6 ...(Count)
7
Sample Count: 7 Months Sampled:
6
Weeks Sampled:
7
Quarters Sampled :
2
# Over Daily C:
0 0.00 # Over Mo Avg C:
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Saturday, February 24, 2024 11:38:55AM * Indicates Violation ** Indicates TRC Violation Page 9 of 13

Cintas Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
TKN
01/17/2023
S
Cinta6011723Self
42.6
/ mg/L
25.87 /
lbs/day
01/19/2023
P
Cintas011923POTW
48.4
/ mg/L
/
02/14/2023
P
Cintas021423POTW
31.3
/ mg/L
/
02/14/2023
S
Cintas021423Self
14
/ mg/L
7.263 /
Ibs/day
03/07/2023
S
Cintas03 0723 Self
38.7
/ mg/L
22.224 /
Ibs/day
03/14/2023
P
Cintas031423POTW
25.6
/ mg/L
/
04/04/2023
S
Cintas04O423Self
16.3
/ mg/L
5.954 /
Ibs/day
04/14/2023
P
Cintas041423POTW
30.9
/ mg/L
/
05/04/2023
S
Cintas05O423Self
30.5
/ mg/L
8.205 /
lbs/day
05/12/2023
P
CintasO51223POTW
68.6
/ mg/L
/
06/08/2023
S
Cintas06O823Self
61.4
/ mg/L
30.356 /
lbs/day
06/22/2023
P
Cintas062223POTW
18.5
/ mg/L
/
Jan 2023
Week 3
45.5
/ mg/L
25.87 /
Ibs/day
Feb 2023
Week 2
22.65
/ mg/L
7.263 /
Ibs/day
Mar 2023
Week 1
38.7
/ mg/L
22.224 /
Ibs/day
Mar 2023
Week 2
25.6
/ mg/L
/
Apr 2023
Week 1
16.3
/ mg/L
5.954 /
Ibs/day
Apr 2023
Week 2
30.9
/ mg/L
/
May 2023
Week 1
30.5
/ mg/L
8.205 /
lbs/day
May 2023
Week 2
68.6
/ mg/L
/
Jun 2023
Week 2
61.4
/ mg/L
30356 /
Ibs/day
Jun 2023
Week 4
18.5
/ mg/L
/
Jan 2023
Average
45.5
/ mg/L
25.87 /
Ibs/day
Feb 2023
Average
22.65
/ mg/L
7.263 /
Ibs/day
Mar 2023
Average
32.15
/ mg/L
22.224 /
Ibs/day
Apr 2023
Average
23.6
/ mg/L
5.954 /
lbs/day
May 2023
Average
49.55
/ mg/L
8.205 /
lbs/day
Jun 2023
Average
39.95
/ mg/L
30.356 /
Ibs/day
2023
Quarter 1
33.43
/ mg/L
18.453 /
Ibs/day
2023
Quarter 2
37.7
/ mg/L
14.838 /
Ibs/day
2023
1st 6 Months (Avg)
35.57
/ mg/L
16.645 /
Ibs/day
2023
1st 6 ...(Max)
68.6
/ mg/L
30.356 /
Ibs/day
2023
1st 6 ...(Min)
14
/ mg/L
/
2023
1st 6 ...(Count)
12
/
6 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
01/17/2023
S
Cintas011723Self
01/19/2023
P
Cintas011923POTW
02/14/2023
P
Cintas021423POTW
02/14/2023
S
Cintas021423Self
03/07/2023
S
Cintas03 0723 Self
4.3
/ mg/L
2.6113 /
3.85
/ mg/L
/
2.81
/ mg/L
/
1.6
/ mg/L
0.8301 /
4
/ mg/L
2.297 /
lbs/day
Ibs/day
Ibs/day
Saturday, February 24, 2024 11:38:55AM * Indicates Violation ** Indicates TRC Violation Page 10 of 13

Cintas Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
03/14/2023
P
Cintas031423POTW
1.05
/ mg/L
/
04/04/2023
S
Cintas04O423Self
1.2
/ mg/L
0.4384 /
lbs/day
04/14/2023
P
Cintas041423POTW
2.85
/ mg/L
/
05/04/2023
S
CintasO50423Self
3.4
/ mg/L
0.9147 /
Ibs/day
05/12/2023
P
Cintas051223POTW
5.34
/ mg/L
/
06/08/2023
S
Cintas060823Self
6.2
/ mg/L
3.0653 /
Ibs/day
06/22/2023
P
Cintas062223POTW
1.56
/ mg/L
/
Jan 2023
Week 3
4.075
/ mg/L
2.6113 /
Ibs/day
Feb 2023
Week 2
2.205
/ mg/L
0.8301 /
Ibs/day
Mar 2023
Week 1
4
/ mg/L
2.297 /
lbs/day
Mar 2023
Week 2
1.05
/ mg/L
/
Apr 2023
Week 1
1.2
/ mg/L
0.4384 /
Ibs/day
Apr 2023
Week 2
2.85
/ mg/L
/
May 2023
Week 1
3.4
/ mg/L
0.9147 /
Ibs/day
May 2023
Week 2
5.34
/ mg/L
/
Jun 2023
Week 2
6.2
/ mg/L
3.0653 /
Ibs/day
Jun 2023
Week 4
1.56
/ mg/L
/
Jan 2023
Average
4.075
/ mg/L
2.6113 /
lbs/day
Feb 2023
Average
2.205
/ mg/L
0.8301 /
lbs/day
Mar 2023
Average
2.525
/ mg/L
2.297 /
Ibs/day
Apr 2023
Average
2.025
/ mg/L
0.4384 /
Ibs/day
May 2023
Average
4.37
/ mg/L
0.9147 /
Ibs/day
Jun 2023
Average
3.88
/ mg/L
3.0653 /
Ibs/day
2023
Quarter 1
2.935
/ mg/L
1.9128 /
Ibs/day
2023
Quarter 2
3.425
/ mg/L
1.4728 /
Ibs/day
2023
1st 6 Months (Avg)
3.18
/ mg/L
1.6928 /
lbs/day
2023
lst6... (Max)
6.2
/ mg/L
3.0653 /
lbs/day
2023
1st 6 ...(Min)
1.05
/ mg/L
/
2023
1st 6 ...(Count)
12
/
6 /
Sample Date SampleID Result/Limit Mass /Limit
TSS
01/17/2023
S
Cintas011723Self
374
/ mg/L
227.124755
/ Ibs/day
01/19/2023
P
Cintas011923POTW
188
/ mg/L
/
02/14/2023
P
Cintas021423POTW
160
/ mg/L
/
02/14/2023
S
Cintas021423Self
85.7
/ mg/L
44.462422
/ Ibs/day
03/07/2023
S
Cintas03 0723 Self
126
/ mg/L
72.356639
/ lbs/day
03/14/2023
P
Cintas031423POTW
182
/ mg/L
/
04/04/2023
S
Cintas040423Self
91.2
/ mg/L
33.31463
/ Ibs/day
04/14/2023
P
Cintas041423POTW
332
/ mg/L
/
05/04/2023
S
Cintas050423Self
244
/ mg/L
65.63967
/ Ibs/day
05/12/2023
P
Cintas051223POTW
420
/ mg/L
/
Saturday, February 24, 2024 11:38:55AM * Indicates Violation ** Indicates TRC Violation Page 11 of 13

Cintas Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
TSS
06/08/2023
S Cintas06O823Self
278
/
mg/L
137.441866
/
Ibs/day
06/22/2023
P CintasO62223POTW
240
/
mg/L
/
Jan 2023
Week 3
281
/
mg/L
227.124755
/
lbs/day
Feb 2023
Week 2
122.9
/
mg/L
44.462422
/
Ibs/day
Mar 2023
Week 1
126
/
mg/L
72.356639
/
Ibs/day
Mar 2023
Week 2
182
/
mg/L
/
Apr 2023
Week 1
91.2
/
mg/L
33.31463
/
Ibs/day
Apr 2023
Week 2
332
/
mg/L
/
May 2023
Week 1
244
/
mg/L
65.63967
/
lbs/day
May 2023
Week 2
420
/
mg/L
/
Jun 2023
Week 2
278
/
mg/L
137.441866
/
lbs/day
Jun 2023
Week 4
240
/
mg/L
/
Jan 2023
Average
281
/
mg/L
227.124755
/
Ibs/day
Feb 2023
Average
122.9
/
mg/L
44.462422
/
Ibs/day
Mar 2023
Average
154
/
mg/L
72.356639
/
Ibs/day
Apr 2023
Average
211.6
/
mg/L
33.31463
/
Ibs/day
May 2023
Average
332
/
mg/L
65.63967
/
Ibs/day
Jun 2023
Average
259
/
mg/L
137.441866
/
lbs/day
2023
Quarter 1
186
/
mg/L
114.647938
/
lbs/day
2023
Quarter 2
267.5
/
mg/L
78.798722
/
Ibs/day
2023
1st 6 Months (Avg)
226.7
/
mg/L
96.7233
/
Ibs/day
2023
lst6... (Max)
420
/
mg/L
227.124755
/
Ibs/day
2023
1st 6 ...(Min)
85.7
/
mg/L
/
2023
1st 6 ...(Count)
12
/
6
/
Sample Date
SamplelD
Result/Limit
Mass /Limit
VOC
01/17/2023
S Cintas011723Self
0.681
/
mg/L
/
Jan 2023
Week 3
0.681
/
mg/L
/
Jan 2023
Average
0.681
/
mg/L
/
2023
Quarter 1
0.681
/
mg/L
/
2023
1st 6 Months (Avg)
0.681
/
mg/L
/
2023
1st 6 ...(Max)
0.681
/
mg/L
/
2023
1st 6 ...(Min)
0.681
/
mg/L
/
2023
1st 6 ...(Count)
1
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
01/17/2023
S CintaS011723Self
Jan 2023
Week 3
Jan 2023
Average
2023
Quarter
0.74 / mg/L 0.449391 / Ibs/day
0.74 / mg/L 0.449391 / Ibs/day
0.74 / mg/L 0.449391 / lbs/day
0.74 / mg/L 0.449391 / lbs/day
Saturday, February 24, 2024 11:38:55AM * Indicates Violation ** Indicates TRC Violation Page 12 of 13

Cintas Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
2023
1st 6 Months (Avg)
0.74 / mg/L
0.449391 /
2023
1st 6 ...(Max)
0.74 / mg/L
0.449391 /
2023
lst6... (Min)
0.74 / mg/L
0.449391 /
2023
1st 6 ...(Count)
1 /
1 /
lbs/day
lbs/day
lbs/day
Saturday, February 24, 2024 11:38:55AM * Indicates Violation ** Indicates TRC Violation Page 13 of 13

Eli Lilly & Company
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Arsenic
06/13/2023
S EhLilly061323Self
<
0.001
/ mg/L
<
/
06/15/2023
P E1iLi1ly061523P0TW
<
0.001
/ mg/L
<
/
Jun 2023
Week 2
<
0.001
/ mg/L
<
/
Jun 2023
Week 3
<
0.001
/ mg/L
<
/
Jun 2023
Average
<
0.001
/ mg/L
<
/
2023
Quarter 2
<
0.001
/ mg/L
<
/
2023
1st 6 Months (Avg)
<
0.001
/ mg/L
<
/
2023
1st 6 ...(Max)
<
0.001
/ mg/L
<
/
2023
1st 6 ...(Min)
<
0.001
/ mg/L
<
/
2023
1st 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
03/31/2023 S
EliLilly0323FIow
0.035333
/
MGD
/
04/30/2023 S
EliLilly0423F1ow
0.036037
/
MGD
/
05/31/2023 S
EliLilly0523F1ow
0.032531
/
MGD
/
06/30/2023 S
EliLilly0623FIow
0.040374
/
MGD
/
Mar 2023
Week 4
0.035333
/
MGD
/
Apr 2023
Week 4
0.036037
/
MGD
/
May 2023
Week 4
0.032531
/
MGD
/
Jun 2023
Week 4
0.040374
/
MGD
/
Mar 2023
Average
0.035333
/ 0.121481
MGD
/
Apr 2023
Average
0.036037
/ 0.121481
MGD
/
May 2023
Average
0.032531
/ 0.121481
MGD
/
Jun 2023
Average
0.040374
/ 0.121481
MGD
/
2023
Quarter 1
0.035333
/
MGD
/
2023
Quarter 2
0.036314
/
MGD
/
2023
1st 6 Months (Avg)
0.036069
/
MGD
/
2023
1st 6 ...(Max)
0.040374
/
MGD
/
2023
1st 6 ...(Min)
0.032531
/
MGD
/
2023
1st 6 ...(Count)
4
/
/
Sample Count : 4 Months Sampled
: 4
Weeks Sampled:
4
Quarters Sampled :
2
# Over Daily C:
0 0.00 # Over Mo Avg C :
0 0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0 0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0 0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC :
0 0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Saturday, February 24, 2024 1:54:03PM * Indicates Violation ** Indicates TRC Violation Page 1 of 9

Eli Lilly & Company
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
BOD
06/13/2023
S Elil illy061323Self
129
/ mg/L
/
06/15/2023
P EliLilly06l523POTW
>
3200
/ mg/L
>
/
Jun 2023
Week 2
129
/ mg/L
/
Jun 2023
Week 3
>
3200
/ mg/L
>
/
Jun 2023
Average
>
1664.5
/ mg/L
>
/
2023
Quarter 2
>
1664.5
/ mg/L
>
/
2023
1st 6 Months (Avg)
>
1664.5
/ mg/L
>
/
2023
1st 6 ...(Max)
>
3200
/ mg/L
>
/
2023
1st 6 ...(Min)
129
/ mg/L
/
2023
1st 6 ...(Count)
2
/
/
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
06/13/2023
S EliLilly061323Self
<
0.00008
/
mg/L
<
/
06/15/2023
P EliLi1ly06l523POTW
<
0.00008
/
mg/L
<
/
Jun 2023
Week 2
<
0.00008
/
mg/L
<
/
Jun 2023
Week 3
<
0.00008
/
mg/L
<
/
Jun 2023
Average
<
0.00008
/
mg/L
<
/
2023
Quarter 2
<
0.00008
/
mg/L
<
/
2023
1st 6 Months (Avg)
<
0.00008
/
mg/L
<
/
2023
1st 6 ...(Max)
<
0.00008
/
mg/L
<
/
2023
1st 6 ...(Min)
<
0.00008
/
mg/L
<
/
2023
1st 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
Chloride
06/13/2023
S EhLIl1y061323Self
70
/ mg/L
/
06/15/2023
P EhLilly061523POTW
110
/ mg/L
/
Jun 2023
Week 2
70
/ mg/L
/
Jun 2023
Week 3
110
/ mg/L
/
Jun 2023
Average
90
/ mg/L
/
2023
Quarter 2
90
/ mg/L
/
2023
1st 6 Months (Avg)
90
/ mg/L
/
2023
1st 6... (Max)
110
/ mg/L
/
2023
1st 6 ...(Min)
70
/ mg/L
/
2023
1st 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass /Limit
Chromium
06/13/2023 S EliLilly061323Self < 0.001 / mg/L < /
06/15/2023 P EliLilly061523POTW 0.004 / mg/L /
Saturday, February 24, 2024 1:54:03PM * Indicates Violation ** Indicates TRC Violation
Page 2 of 9

Eli Lilly & Company
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
Jun 2023
Week 2 <
0.001
/
mg/L <
/
Jun 2023
Week 3
0.004
/
mg/L
/
Jun 2023
Average <
0.002
/
mg/L <
/
2023
Quarter 2 <
0.002
/
mg/L <
/
2023
1st 6 Months (Avg) <
0.002
/
mg/L <
/
2023
lst6... (Max)
0.004
/
mg/L
/
2023
1st 6 ...(Min) <
0.001
/
mg/L <
/
2023
1st 6 ...(Count)
2
Sample Date
SampleID
Result/Limit
Mass/Limit
Copper
06/13/2023
S EliLilly061323Self
0.047
/
mg/L
/
06/15/2023
P EliLilly061523POTW
0.089
/
mg/L
/
Jun 2023
Week 2
0.047
/
mg/L
/
Jun 2023
Week 3
0.089
/
mg/L
/
Jun 2023
Average
0.068
/
mg/L
/
2023
Quarter 2
0.068
/
mg/L
/
2023
1st 6 Months (Avg)
0.068
/
mg/L
/
2023
1st 6 ...(Max)
0.089
/
mg/L
/
2023
1st 6 ...(Min)
0.047
/
mg/L
/
2023
1st 6 ...(Count)
2
Sample Date SampleID Result/Limit Mass/Limit
Cyanide
06/13/2023
S EliLilly061323Self
<
0.003
/ mg/L
<
/
06/15/2023
P EhLilly061523POTW
<
0.003
/ mg/L
<
/
Jun 2023
Week 2
<
0.003
/ mg/L
<
/
Jun 2023
Week 3
<
0.003
/ mg/L
<
/
Jun 2023
Average
<
0.003
/ mg/L
<
/
2023
Quarter 2
<
0.003
/ mg/L
<
/
2023
1st 6 Months (Avg)
<
0.003
/ mg/L
<
/
2023
1st 6 ...(Max)
<
0.003
/ mg/L
<
/
2023
1st 6 ...(Min)
<
0.003
/ mg/L
<
/
2023
1st 6... (Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
06/13/2023
S EliLi1ly06l323Self <
0.05
/ mg/L < /
06/15/2023
P EliLi1ly06l523POTW
1.51
/ mg/L /
Jun 2023
Week 2 <
0.05
/ mg/L < /
Jun 2023
Week 3
1.51
/ mg/L /
Saturday, February 24, 2024 1:54:03PM * Indicates Violation ** Indicates TRC Violation Page 3 of 9

Eli Lilly & Company
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
Fluoride
Jun 2023
Average
<
0.78 /
mg/L
<
/
2023
Quarter 2
<
0.78 /
mg/L
<
/
2023
1st 6 Months (Avg)
<
0.78 /
mg/L
<
/
2023
1st 6 ...(Max)
1.51 /
mg/L
/
2023
1st 6 ...(Min)
<
0.05 /
mg/L
<
/
2023
lst6... (Count)
2
Sample Date
SamplelD
Result/Limit
Mass /Limit
Lead
06/13/2023
S EhLilly061323Self
<
0.0003 /
mg/L
<
/
06/15/2023
P E1iLi11y061523P0TW
0.001 /
mg/L
/
Jun 2023
Week 2
<
0.0003 /
mg/L
<
/
Jun 2023
Week 3
0.001 /
mg/L
/
Jun 2023
Average
<
0.0006 /
mg/L
<
/
2023
Quarter 2
<
0.0006 /
mg/L
<
/
2023
1st 6 Months (Avg)
<
0.0006 /
mg/L
<
/
2023
1st 6 ...(Max)
0.0010 /
mg/L
/
2023
1st 6 ...(Min)
<
0.0003 /
mg/L
<
/
2023
1st 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
Mercury - LL
06/13/2023 S
EhLi11y061323Se1tHg 0.000003
/ 0.000142
mg/L
/
06/14/2023 P
E1iLilly061423P0TW 0.000121
/ 0.000142
mg/L
/
Hg
Jun 2023
Week 2 0.000062
/
mg/L
/
Jun 2023
Average 0.000062
/
mg/L
/
2023
Quarter 2 0.000062
/
mg/L
/
2023
1st 6 Months (Avg) 0.000062
/
mg/L
/
2023
1st 6 ...(Max) 0.000121
/
mg/L
/
2023
lst6... (Min) 0.000003
/
mg/L
/
2023
lst6... (Count) 2
Sample Count: 2 Months Sampled
:
1
Weeks Sampled:
1
Quarters Sampled :
1
# Over Daily C :
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Saturday, February 24, 2024 1:54:03PM * Indicates Violation ** Indicates TRC Violation Page 4 of 9

Eli Lilly & Company
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
06/13/2023 S
EhLilly061323Self
<
0.001
/ mg/L
<
/
06/15/2023 P
E1iLi1ly06l523POTW
<
0.001
/ mg/L
<
/
Jun 2023
Week 2
<
0.001
/ mg/L
<
/
Jun 2023
Week 3
<
0.001
/ mg/L
<
/
Jun 2023
Average
<
0.001
/ mg/L
<
/
2023
Quarter 2
<
0.001
/ mg/L
<
/
2023
1st 6 Months (Avg)
<
0.001
/ mg/L
<
/
2023
1st 6 ...(Max)
<
0.001
/ mg/L
<
/
2023
1st 6 ...(Min)
<
0.001
/ mg/L
<
/
2023
1st 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
06/13/2023
S ERLi11y061323Self
0.0036
/ mg/L
/
06/15/2023
P E1iLi11y061523POTW
0.0082
/ mg/L
/
Jun 2023
Week 2
0.0036
/ mg/L
/
Jun 2023
Week 3
0.0082
/ mg/L
/
Jun 2023
Average
0.0059
/ mg/L
/
2023
Quarter 2
0.0059
/ mg/L
/
2023
1st 6 Months (Avg)
0.0059
/ mg/L
/
2023
1st 6 ...(Max)
0.0082
/ mg/L
/
2023
1st 6 ...(Min)
0.0036
/ mg/L
/
2023
1st 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate -Nitrite
06/13/2023 S
EhLIl1y061323Self
0.6
/ mg/L
/
06/15/2023 P
EhLilly061523POTW
0.7
/ mg/L
/
Jun 2023
Week 2
0.6
/ mg/L
/
Jun 2023
Week 3
0.7
/ mg/L
/
Jun 2023
Average
0.6
/ mg/L
/
2023
Quarter 2
0.6
/ mg/L
/
2023
1st 6 Months (Avg)
0.6
/ mg/L
/
2023
1st 6... (Max)
0.7
/ mg/L
/
2023
1st 6 ...(Min)
0.6
/ mg/L
/
2023
1st 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass /Limit
Nitrogen, Total
06/13/2023 S E1iLi11y061323Self
06/15/2023 P E1iLi11y061523POTW
Saturday, February 24, 2024 1:54:03PM
51.5 / mg/L /
143 / mg/L /
* Indicates Violation ** Indicates TRC Violation
Page 5 of 9

Eli Lilly & Company
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen, Total
Jun 2023
Week 2
51.5
/
mg/L
/
Jun 2023
Week 3
143
/
mg/L
/
Jun 2023
Average
97.25
/
mg/L
/
2023
Quarter 2
97.25
/
mg/L
/
2023
1st 6 Months (Avg)
97.25
/
mg/L
/
2023
lst6... (Max)
143
/
mg/L
/
2023
1st 6 ...(Min)
51.5
/
mg/L
/
2023
1st 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass /Limit
Oil & Grease, Total
06/13/2023 S
EliLilly061323Self <
2.5
/ 200
mg/L
<
/
06/15/2023 P
EliLilly06l523POTW <
2.5
/ 200
mg/L
<
/
Jun 2023
Week 2 <
2.5
/
mg/L
<
/
Jun 2023
Week 3 <
2.5
/
mg/L
<
/
Jun 2023
Average <
2.5
/
mg/L
<
/
2023
Quarter 2 <
2.5
/
mg/L
<
/
2023
1st 6 Months (Avg) <
2.5
/
mg/L
<
/
2023
1st 6 ...(Max) <
2.5
/
mg/L
<
/
2023
1st 6 ...(Min) <
2.5
/
mg/L
<
/
2023
1st 6 ...(Count)
2
Sample Count: 2 Months Sampled:
1
Weeks Sampled
:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C:
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC
:
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
PH
06/13/2023
S EhLilly061323Self
6.4
/ 6.0 - 10.0
SU /
06/15/2023
P EliLiHy06l523POTW
8.2
/ 6.0 - 10.0
SU /
Jun 2023
Week 2
6.4
/
SU /
Jun 2023
Week 3
8.2
/
SU /
Jun 2023
Average
7.3
/
SU /
2023
Quarter 2
7.3
/
SU /
2023
1st 6 Months (Avg)
7.3
/
SU /
2023
lst6... (Max)
8.2
/
SU /
2023
1st 6 ...(Min)
6.4
/
SU /
Saturday, February 24, 2024 1:54:03PM * Indicates Violation ** Indicates TRC Violation Page 6 of 9

Eli Lilly & Company
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
PH
2023
1st 6 ...(Count)
2
Sample Count: 2
Months Sampled: I
Weeks Sampled:
2
Quarters Sampled :
I
# Over Daily C :
0 0.00 # Over Mo Avg C :
0 0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC
: 0 0.00
# Over Wk Avg C TRC:
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0 0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC
: 0 0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass /Limit
Selenium
06/13/2023 S
E1iLi11y061323Self
<
0.0005 /
mg/L
<
/
06/15/2023 P
E1iLi11y061523P0TW
0.0024 /
mg/L
/
Jun 2023
Week 2
<
0.0005 /
mg/L
<
/
Jun 2023
Week 3
0.0024 /
mg/L
/
Jun 2023
Average
<
0.0015 /
mg/L
<
/
2023
Quarter 2
<
0.0015 /
mg/L
<
/
2023
1st 6 Months (Avg)
<
0.0015 /
mg/L
<
/
2023
1st 6 ...(Max)
0.0024 /
mg/L
/
2023
1st 6 ...(Min)
<
0.0005 /
mg/L
<
/
2023
1st 6 ...(Count)
2 /
/
Sample Date
SamplelD
Result/Limit
Mass/Limit
Silver
06/13/2023 S
EhLi11y061323Self
<
0.0003 /
mg/L
<
/
06/15/2023 P
EhLi11y061523P0TW
<
0.0003 /
mg/L
<
/
Jun 2023
Week 2
<
0.0003 /
mg/L
<
/
Jun 2023
Week 3
<
0.0003 /
mg/L
<
/
Jun 2023
Average
<
0.0003 /
mg/L
<
/
2023
Quarter 2
<
0.0003 /
mg/L
<
/
2023
1st 6 Months (Avg)
<
0.0003 /
mg/L
<
/
2023
1st 6 ...(Max)
<
0.0003 /
mg/L
<
/
2023
1st 6 ...(Min)
<
0.0003 /
mg/L
<
/
2023
1st 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
Temperature
06/13/2023 S
EliLi11y061323Self
22.3 / 66
°C
/
06/15/2023 P
E1iLi11y061523P0TW
17 / 66
°C
/
Jun 2023
Week 2
22.3 /
°C
/
Saturday, February 24, 2024 1:54:03PM * Indicates Violation ** Indicates TRC Violation Page 7 of 9

Eli Lilly & Company
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
Jun 2023
Week 3
17
/
°C
/
Jun 2023
Average
19.7
/
°C
/
2023
Quarter 2
19.7
/
°C
/
2023
1st 6 Months (Avg)
19.7
/
°C
/
2023
1st 6 ...(Max)
22.3
/
°C
/
2023
lst6... (Min)
17
/
°C
/
2023
1st 6 ...(Count)
2
Sample
Count: 2
Months Sampled:
1
Weeks Sampled:
2
Quarters Sampled :
1
# I%
#
%
#
%
#
%
# Over Daily C :
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass /Limit
TKN
06/13/2023
S EliLilly061323Self
50.9
/ mg/L
/
06/15/2023
P EliLilly061523POTW
142
/ mg/L
/
Jun 2023
Week 2
50.9
/ mg/L
/
Jun 2023
Week 3
142
/ mg/L
/
Jun 2023
Average
96.45
/ mg/L
/
2023
Quarter 2
96.45
/ mg/L
/
2023
1st 6 Months (Avg)
96.45
/ mg/L
/
2023
lst 6 ...(Max)
142
/ mg/L
/
2023
1st 6 ...(Min)
50.9
/ mg/L
/
2023
1st 6 ...(Count)
2
/
/
Sample Date SamplelD Result/Limit Mass / Limit
Total Phosphorus
06/13/2023 S
EliLilly061323Self
06/15/2023 P
EhLi11y061523P0TW
Jun 2023
Week 2
Jun 2023
Week 3
Jun 2023
Average
2023
Quarter 2
2023
1st 6 Months (Avg)
2023
1st 6 ...(Max)
2023
1st 6 ...(Min)
2023
1st 6 ...(Count)
4.95
/ mg/L /
11.2
/ mg/L /
4.95
/ mg/L /
11.2
/ mg/L /
8.075
/ mg/L /
8.075
/ mg/L /
8.075
/ mg/L /
11.2
/ mg/L /
4.95
/ mg/L /
2
Saturday, February 24, 2024 1:54:03PM * Indicates Violation ** Indicates TRC Violation Page 8 of 9

Eli Lilly & Company
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
TSS
06/13/2023
S Elil illy061323Self
31
/ mg/L
/
06/15/2023
P EliLilly06l523POTW
158
/ mg/L
/
Jun 2023
Week 2
31
/ mg/L
/
Jun 2023
Week 3
158
/ mg/L
/
Jun 2023
Average
94.5
/ mg/L
/
2023
Quarter 2
94.5
/ mg/L
/
2023
1st 6 Months (Avg)
94.5
/ mg/L
/
2023
1st 6 ...(Max)
158
/ mg/L
/
2023
1st 6 ...(Min)
31
/ mg/L
/
2023
1st 6 ...(Count)
2
/
/
Sample Date SamplelD Result/Limit Mass/Limit
VOC
06/13/2023
S EliLilly061323Self
0.0081
/ mg/L
/
06/15/2023
P EliLi1ly06l523POTW
0.0973
/ mg/L
/
Jun 2023
Week 2
0.0081
/ mg/L
/
Jun 2023
Week 3
0.0973
/ mg/L
/
Jun 2023
Average
0.0527
/ mg/L
/
2023
Quarter 2
0.0527
/ mg/L
/
2023
1st 6 Months (Avg)
0.0527
/ mg/L
/
2023
1st 6 ...(Max)
0.0973
/ mg/L
/
2023
1st 6 ...(Min)
0.0081
/ mg/L
/
2023
1st 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
06/13/2023
S EhLIl1y061323Self
0.214
/ mg/L
/
06/15/2023
P EhLilly061523POTW
0.464
/ mg/L
/
Jun 2023
Week 2
0.214
/ mg/L
/
Jun 2023
Week 3
0.464
/ mg/L
/
Jun 2023
Average
0.339
/ mg/L
/
2023
Quarter 2
0.339
/ mg/L
/
2023
1st 6 Months (Avg)
0.339
/ mg/L
/
2023
1st 6... (Max)
0.464
/ mg/L
/
2023
1st 6 ...(Min)
0.214
/ mg/L
/
2023
1st 6 ...(Count)
2
111/2023 To 613012023 Sample Type: Effluent Wastewater Oufall: 002
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
Saturday, February 24,2024 1:54:03PM
* Indicates Violation ** Indicates TRC Violation
Page 9 of 9

Eli Lilly & Company
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 002
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
03/31/2023
S
EliLiRyP20323F1ow
0.01905
/
MGD /
04/30/2023
S
EliLillyP20423F1ow
0.01719
/
MGD /
05/31/2023
S
EliLillyP20523F1ow
0.017709
/
MGD /
06/30/2023
S
EliLIl1yP20623F1ow
0.011187
/
MGD /
Mar 2023
Week 4
0.01905
/
MGD /
Apr 2023
Week 4
0.01719
/
MGD /
May 2023
Week 4
0.017709
/
MGD /
Jun 2023
Week 4
0.011187
/
MGD /
Mar 2023
Average
0.01905
/ 0.061413
MGD /
Apr 2023
Average
0.01719
/ 0.061413
MGD /
May 2023
Average
0.017709
/ 0.061413
MGD /
Jun 2023
Average
0.011187
/ 0.061413
MGD /
2023
Quarter 1
0.01905
/
MGD /
2023
Quarter 2
0.015362
/
MGD /
2023
1st 6 Months (Avg)
0.016284
/
MGD /
2023
1st 6 ...(Max)
0.01905
/
MGD /
2023
1st 6 ...(Min)
0.011187
1
MGD /
2023
1st 6 ...(Count)
4
Sample Count:
4
Months Sampled:
4
Weeks Sampled:
4
Quarters Sampled :
2
# Over Daily C:
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Saturday, February 24, 2024 1:54:03PM * Indicates Violation ** Indicates TRC Violation Page 1 of 1

Micross Advanced Interconnect Technolou, LLC
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
Aluminum
01/18/2023
S MicrossO 11823 Self
0.022
/
mg/L
0.00554 /
lbs/day
04/27/2023
P Micross042723POTW
0.017
/
mg/L
0.00493 /
lbs/day
Jan 2023
Week 3
0.022
/
mg/L
0.00554 /
lbs/day
Apr 2023
Week 4
0.017
/
mg/L
0.00493 /
Ibs/day
Jan 2023
Average
0.022
/
mg/L
0.00554 /
Ibs/day
Apr 2023
Average
0.017
/
mg/L
0.00493 /
Ibs/day
2023
Quarter 1
0.022
/
mg/L
0.00554 /
Ibs/day
2023
Quarter 2
0.017
/
mg/L
0.00493 /
Ibs/day
2023
1st 6 Months (Avg)
0.020
/
mg/L
0.005235 /
Ibs/day
2023
1st 6 ...(Max)
0.022
/
mg/L
0.005540 /
lbs/day
2023
1st 6... (Min)
0.017
/
mg/L
0.004930 /
lbs/day
2023
1st 6 ...(Count)
2
/
2 /
Sample Date
SamplelD
Result/Limit
Mass/Limit
Ammonia
01/18/2023
S Micross011823Self
2
/
mg/L
0.5037 /
lbs/day
04/27/2023
P Micross042723POTW
3.7
/
mg/L
1.0544 /
Ibs/day
Jan 2023
Week 3
2
/
mg/L
0.5037 /
Ibs/day
Apr 2023
Week 4
3.7
/
mg/L
1.0544 /
Ibs/day
Jan 2023
Average
2
/
mg/L
0.5037 /
Ibs/day
Apr 2023
Average
3.7
/
mg/L
1.0544 /
lbs/day
2023
Quarter 1
2
/
mg/L
0.5037 /
lbs/day
2023
Quarter 2
3.7
/
mg/L
1.0544 /
lbs/day
2023
1st 6 Months (Avg)
2.85
/
mg/L
0.7790 /
lbs/day
2023
1st 6 ...(Max)
3.7
/
mg/L
1.0544 /
Ibs/day
2023
1st 6 ...(Min)
2
/
mg/L
0.5037 /
Ibs/day
2023
1st 6 ...(Count)
2
/
2 /
Sample Date
SamplelD
Result/Limit
Mass/Limit
Average Flow for Month
01/31/2023
S
Micross0123F1ow
02/28/2023
S
Micross0223FIow
03/31/2023
S
Mieross0323FIow
04/30/2023
S
Micross0423FIow
05/31/2023
S
Mieross0523F1ow
06/30/2023
S
Micross0623FIow
Jan 2023
Week 4
Feb 2023
Week 4
Mar 2023
Week 4
Apr 2023
Week 4
May 2023
Week 4
Jun 2023
Week 4
0.025528
/ 0.100
MGD /
0.025451
/ 0.100
MGD /
0.02673
/ 0.100
MGD /
0.038967
/ 0.100
MGD /
0.038538
/ 0.100
MGD /
0.048493
/ 0.100
MGD /
0.025528
/
MGD /
0.025451
/
MGD /
0.02673
/
MGD /
0.038967
/
MGD /
0.038538
/
MGD /
0.048493
/
MGD /
Tuesday, February 13, 2024 10:36:17AM * Indicates Violation ** Indicates TRC Violation Page 1 of 10

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
Jan 2023
Average
0.025528
/ 0.075
MGD
/
Feb 2023
Average
0.025451
/ 0.075
MGD
/
Mar 2023
Average
0.02673
/ 0.075
MGD
/
Apr 2023
Average
0.038967
/ 0.075
MGD
/
May 2023
Average
0.038538
/ 0.075
MGD
/
Jun 2023
Average
0.048493
/ 0.075
MGD
/
2023
Quarter 1
0.025903
/
MGD
/
2023
Quarter 2
0.041999
/
MGD
/
2023
1st 6 Months (Avg) 0.033951
/
MGD
/
2023
1st 6 ...(Max)
0.048493
/
MGD
/
2023
lst6... (Min)
0.025451
/
MGD
/
2023
1st 6 ...(Count)
6
Sample Count: 6
Months Sampled
: 6
Weeks Sampled :
6
Quarters Sampled :
2
# Over Daily C:
0 0.00
# Over Mo Avg C :
0 0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0 0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0 0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC :
0 0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
01/18/2023
S Micross011823Self
<
0.0025
/ mg/L
<
0.00063
/ lbs/day
04/27/2023
P Micross042723POTW
<
0.00008
/ mg/L
<
0.000021
/ lbs/day
Jan 2023
Week 3
<
0.0025
/ mg/L
<
0.00063
/ lbs/day
Apr 2023
Week 4
<
0.00008
/ mg/L
<
0.000021
/ Ibs/day
Jan 2023
Average
<
0.0025
/ mg/L
<
0.00063
/ Ibs/day
Apr 2023
Average
<
0.00008
/ mg/L
<
0.000021
/ Ibs/day
2023
Quarter 1
<
0.0025
/ mg/L
<
0.00063
/ Ibs/day
2023
Quarter 2
<
0.00008
/ mg/L
<
0.000021
/ lbs/day
2023
1st 6 Months (Avg)
<
0.00129
/ mg/L
<
0.000325
/ lbs/day
2023
1st 6 ...(Max)
<
0.0025
/ mg/L
<
0.000630
/ lbs/day
2023
lst 6 ...(Min)
<
0.00008
/ mg/L
<
0.000021
/ lbs/day
2023
1st 6 ...(Count)
2
/
2
/
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
01/18/2023 S MicrossO11823Self 22 / mg/L 5.5402 / Ibs/day
04/27/2023 P Micross042723POTW 60 / mg/L 17.0987 / Ibs/day
Jan 2023 Week 3 22 / mg/L 5.5402 / Ibs/day
Tuesday, February 13, 2024 10:36:17AM * Indicates Violation ** Indicates TRC Violation Page 2 of 10

Micross Advanced Interconnect Technolou, LLC
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: '001
Sample Date
SamplelD
Result/Limit
Mass/Limit
Chloride
Apr 2023
Week 4
60
/
mg/L
17.0987 /
lbs/day
Jan 2023
Average
22
/
mg/L
5.5402 /
lbs/day
Apr 2023
Average
60
/
mg/L
17.0987 /
lbs/day
2023
Quarter 1
22
/
mg/L
5.5402 /
Ibs/day
2023
Quarter 2
60
/
mg/L
17.0987 /
Ibs/day
2023
1st 6 Months (Avg)
41
/
mg/L
11.3194 /
Ibs/day
2023
1st 6 ...(Max)
60
/
mg/L
17.0987 /
Ibs/day
2023
1st 6 ...(Min)
22
/
mg/L
5.5402 /
Ibs/day
2023
1st 6 ...(Count)
2
/
2 /
Sample Date
SamplelD
Result/Limit
Mass/Limit
Chromium
01/18/2023
S Micross011823Self
0.004
/
mg/L
0.001007 /
lbs/day
04/27/2023
P Micross042723POTW
0.003
/
mg/L
0.000772 /
lbs/day
Jan 2023
Week 3
0.004
/
mg/L
0.001007 /
lbs/day
Apr 2023
Week 4
0.003
/
mg/L
0.000772 /
lbs/day
Jan 2023
Average
0.004
/
mg/L
0.001007 /
Ibs/day
Apr 2023
Average
0.003
/
mg/L
0.000772 /
Ibs/day
2023
Quarter 1
0.004
/
mg/L
0.001007 /
Ibs/day
2023
Quarter 2
0.003
/
mg/L
0.000772 /
Ibs/day
2023
1st 6 Months (Avg)
0.003
/
mg/L
0.000890 /
lbs/day
2023
1st 6 ...(Max)
0.004
/
mg/L
0.001007 /
lbs/day
2023
1st 6 ...(Min)
0.003
/
mg/L
0.000772 /
lbs/day
2023
lst 6 ...(Count)
2
/
2 /
Sample Date
SamplelD
Result/Limit
Mass/Limit
Copper
01/18/2023
S Micross011823Self
0.037
/
mg/L
0.009318 /
Ibs/day
04/27/2023
P Micross042723POTW
0.024
/
mg/L
0.006811 /
Ibs/day
Jan 2023
Week 3
0.037
/
mg/L
0.009318 /
Ibs/day
Apr 2023
Week 4
0.024
/
mg/L
0.006811 /
Ibs/day
Jan 2023
Average
0.037
/
mg/L
0.009318 /
Ibs/day
Apr 2023
Average
0.024
/
mg/L
0.006811 /
lbs/day
2023
Quarter 1
0.037
/
mg/L
0.009318 /
lbs/day
2023
Quarter 2
0.024
/
mg/L
0.006811 /
lbs/day
2023
1st 6 Months (Avg)
0.030
/
mg/L
0.008064 /
Ibs/day
2023
lst6... (Max)
0.037
/
mg/L
0.009318 /
Ibs/day
2023
lst6... (Min)
0.024
/
mg/L
0.006811 /
Ibs/day
2023
1st 6 ...(Count)
2
/
2 /
Tuesday, February 13, 2024 10:36:17AM * Indicates Violation ** Indicates TRC Violation Page 3 of 10

Micross Advanced Interconnect Technolou, LLC
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
01/18/2023
S Micross011823Self
<
0.001
/
mg/L
<
0.000315 /
lbs/day
04/27/2023
P Micross042723POTW
<
0.003
/
mg/L
<
0.000712 /
lbs/day
Jan 2023
Week 3
<
0.001
/
mg/L
<
0.000315 /
lbs/day
Apr 2023
Week 4
<
0.003
/
mg/L
<
0.000712 /
Ibs/day
Jan 2023
Average
<
0.001
/
mg/L
<
0.000315 /
Ibs/day
Apr 2023
Average
<
0.003
/
mg/L
<
0.000712 /
Ibs/day
2023
Quarter 1
<
0.001
/
mg/L
<
0.000315 /
Ibs/day
2023
Quarter 2
<
0.003
/
mg/L
<
0.000712 /
Ibs/day
2023
1st 6 Months (Avg)
<
0.002
/
mg/L
<
0.000514 /
Ibs/day
2023
1st 6 ...(Max)
<
0.003
/
mg/L
<
0.000712 /
lbs/day
2023
1st 6... (Min)
<
0.001
/
mg/L
<
0.000315 /
kbs/day
2023
1st 6 ...(Count)
2
/
2 /
Sample Date
SamplelD
Result/Limit
Mass/Limit
Fluoride
01/18/2023
S Micross011823Self
2
/
mg/L
0.5037 /
lbs/day
04/27/2023
P Micross042723POTW
1.7
/
mg/L
0.4845 /
Ibs/day
Jan 2023
Week 3
2
/
mg/L
0.5037 /
Ibs/day
Apr 2023
Week 4
1.7
/
mg/L
0.4845 /
Ibs/day
Jan 2023
Average
2
/
mg/L
0.5037 /
Ibs/day
Apr 2023
Average
1.7
/
mg/L
0.4845 /
lbs/day
2023
Quarter 1
2
/
mg/L
0.5037 /
lbs/day
2023
Quarter 2
1.7
/
mg/L
0.4845 /
lbs/day
2023
1st 6 Months (Avg)
1.85
/
mg/L
0.4941 /
lbs/day
2023
1st 6 ...(Max)
2
/
mg/L
0.5037 /
Ibs/day
2023
1st 6 ...(Min)
1.7
/
mg/L
0.4845 /
Ibs/day
2023
1st 6 ...(Count)
2
/
2 /
Sample Date
SamplelD
Result/Limit
Mass/Limit
Lead
01/18/2023
S MicrossO11823Self
<
0.005
/ mg/L
<
0.001259 /
Ibs/day
04/27/2023
P Micross042723POTW
0.0016
/ mg/L
0.000445 /
Ibs/day
Jan 2023
Week 3
<
0.005
/ mg/L
<
0.001259 /
lbs/day
Apr 2023
Week 4
0.0016
/ mg/L
0.000445 /
kbs/day
Jan 2023
Average
<
0.005
/ mg/L
<
0.001259 /
lbs/day
Apr 2023
Average
0.0016
/ mg/L
0.000445 /
Ibs/day
2023
Quarter 1
<
0.005
/ mg/L
<
0.001259 /
Ibs/day
2023
Quarter 2
0.0016
/ mg/L
0.000445 /
Ibs/day
2023
1st 6 Months (Avg)
<
0.0033
/ mg/L
<
0.000852 /
Ibs/day
2023
1st 6 ...(Max)
<
0.005
/ mg/L
<
0.001259 /
Ibs/day
2023
1st 6 ...(Min)
0.0016
/ mg/L
0.000445 /
lbs/day
2023
1st 6... (Count)
2
/
2 /
Tuesday, February 13, 2024 10:36:17AM * Indicates Violation ** Indicates TRC Violation Page 4 of 10

Micross Advanced Interconnect Technolou, LLC
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: '001
SarnpleDate SamplelD Result/Limit Mass/Lunit
Mercury - LL
01/18/2023 S
MicrossO 11823 Self 0.000012
/ 0.000142
mg/L
/
04/27/2023 P
Micross042723POTW 0.000007
/ 0.000142
mg/L
/
Hg
Jan 2023
Week 3
0.000012
/
mg/L
/
Apr 2023
Week 4
0.000007
/
mg/L
/
Jan 2023
Average
0.000012
/
mg/L
/
Apr 2023
Average
0.000007
/
mg/L
/
2023
Quarter 1
0.000012
/
mg/L
/
2023
Quarter 2
0.000007
/
mg/L
/
2023
1st 6 Months (Avg) 0.000010
/
mg/L
/
2023
Ist 6 ...(Max)
0.000012
/
mg/L
/
2023
1st 6 ...(Min)
0.000007
/
mg/L
/
2023
Ist 6 ...(Count)
2
Sample Count: 2
Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
2
# Over Daily C :
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Illass/Limit
Molybdenum
01/18/2023 S
Micross011823Self
0.03
/
mg/L
0.0076 /
lbs/day
04/27/2023 P
Micross042723POTW
0.167
/
mg/L
0.0476 /
lbs/day
Jan 2023
Week 3
0.03
/
mg/L
0.0076 /
Ibs/day
Apr 2023
Week 4
0.167
/
mg/L
0.0476 /
lbs/day
Jan 2023
Average
0.03
/
mg/L
0.0076 /
lbs/day
Apr 2023
Average
0.167
/
mg/L
0.0476 /
Ibs/day
2023
Quarter 1
0.03
/
mg/L
0.0076 /
lbs/day
2023
Quarter 2
0.167
/
mg/L
0.0476 /
Ibs/day
2023
1st 6 Months (Avg)
0.0985
/
mg/L
0.0276 /
lbs/day
2023
Ist 6 ...(Max)
0.167
/
mg/L
0.0476 /
lbs/day
2023
1st 6 ...(Min)
0.03
/
mg/L
0.0076 /
lbs/day
2023
Ist 6 ...(Count)
2
/
2 /
Sample Date
SamplelD
Result/Limit
Mass /Limit
Nickel
01/18/2023 S
Micross011823Self
0.005
/
mg/L
0.001259 /
Ibs/day
04/27/2023 P
Micross042723POTW
0.0058
/
mg/L
0.001656 /
Ibs/day
Jan 2023
Week 3
0.005
/
mg/L
0.001259 /
lbs/day
Tuesday, February 13, 2024 10:36:17AM * Indicates Violation ** Indicates TRC Violation Page 5 of 10

Micross Advanced Interconnect Technolou, LLC
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: '001
Sample Date
SamplelD
Result/Limit
Mass/Limit
Nickel
Apr 2023
Week 4
0.0058
/
mg/L
0.001656 /
lbs/day
Jan 2023
Average
0.005
/
mg/L
0.001259 /
lbs/day
Apr 2023
Average
0.0058
/
mg/L
0.001656 /
lbs/day
2023
Quarter 1
0.005
/
mg/L
0.001259 /
Ibs/day
2023
Quarter 2
0.0058
/
mg/L
0.001656 /
Ibs/day
2023
1st 6 Months (Avg)
0.0054
/
mg/L
0.001457 /
Ibs/day
2023
1st 6 ...(Max)
0.0058
/
mg/L
0.001656 /
Ibs/day
2023
1st 6 ...(Min)
0.005
/
mg/L
0.001259 /
Ibs/day
2023
1st 6 ...(Count)
2
/
2 /
Sample Date
SamplelD
Result/Limit
Mass/Limit
Nitrate -Nitrite
01/18/2023 S
Micross011823Self
1.1
/
mg/L
0.277 /
lbs/day
04/27/2023 P
Micross042723POTW
1.1
/
mg/L
0.308 /
lbs/day
Jan 2023
Week 3
1.1
/
mg/L
0.277 /
lbs/day
Apr 2023
Week 4
1.1
/
mg/L
0.308 /
lbs/day
Jan 2023
Average
1.1
/
mg/L
0.277 /
Ibs/day
Apr 2023
Average
1.1
/
mg/L
0.308 /
Ibs/day
2023
Quarter 1
1.1
/
mg/L
0.277 /
Ibs/day
2023
Quarter 2
1.1
/
mg/L
0.308 /
Ibs/day
2023
1st 6 Months (Avg)
1.1
/
mg/L
0.292 /
lbs/day
2023
1st 6 ...(Max)
1.1
/
mg/L
0.308 /
lbs/day
2023
1st 6 ...(Min)
1.1
/
mg/L
0.277 /
lbs/day
2023
lst 6 ...(Count)
2
/
2 /
Sample Date
SamplelD
Result/Limit
Mass/Limit
Nitrogen, Total
01/18/2023 S
Micross011823Self
5.9
/
mg/L
1.486 /
Ibs/day
04/27/2023 P
Micross042723POTW
11.8
/
mg/L
3.363 /
Ibs/day
Jan 2023
Week 3
5.9
/
mg/L
1.486 /
Ibs/day
Apr 2023
Week 4
11.8
/
mg/L
3.363 /
Ibs/day
Jan 2023
Average
5.9
/
mg/L
1.486 /
Ibs/day
Apr 2023
Average
11.8
/
mg/L
3.363 /
lbs/day
2023
Quarter 1
5.9
/
mg/L
1.486 /
lbs/day
2023
Quarter 2
11.8
/
mg/L
3.363 /
lbs/day
2023
1st 6 Months (Avg)
8.85
/
mg/L
2.424 /
Ibs/day
2023
lst6... (Max)
11.8
/
mg/L
3.363 /
Ibs/day
2023
lst6... (Min)
5.9
/
mg/L
1.486 /
Ibs/day
2023
1st 6 ...(Count)
2
/
2 /
Tuesday, February 13, 2024 10:36:17AM * Indicates Violation ** Indicates TRC Violation Page 6 of 10

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: '001
Sainple Date SamplelD Result/Limit Mass/Lunit
Oil & Grease, Total
01/18/2023 S
MicrossO 11823 Self
21.3
/ 200
mg/L
/
04/27/2023 P
Micross042723POTW
8.2
/ 200
mg/L
/
Jan 2023
Week 3
21.3
/
mg/L
/
Apr 2023
Week 4
8.2
/
mg/L
/
Jan 2023
Average
21.3
/
mg/L
/
Apr 2023
Average
8.2
/
mg/L
/
2023
Quarter 1
21.3
/
mg/L
/
2023
Quarter 2
8.2
/
mg/L
/
2023
1st 6 Months (Avg)
14.75
/
mg/L
/
2023
1st 6 ...(Max)
21.3
/
mg/L
/
2023
1st 6... (Min)
8.2
/
mg/L
/
2023
1st 6 ...(Count)
2
Sample Count: 2 Months Sampled
:
2
Weeks Sampled :
2
Quarters Sampled :
2
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
01/18/2023
S Micross011823Self
7.31
/ 5.5 - 10.5
SU /
04/27/2023
P Micross042723POTW
7.3
/ 5.5 - 10.5
SU /
Jan 2023
Week 3
7.31
/
SU /
Apr 2023
Week 4
7.3
/
SU /
Jan 2023
Average
7.31
/
SU /
Apr 2023
Average
7.3
/
SU /
2023
Quarter 1
7.31
/
Su /
2023
Quarter 2
7.3
/
SU /
2023
1st 6 Months (Avg)
7.31
/
SU /
2023
1st 6 ...(Max)
7.31
/
SU /
2023
lst 6 ...(Min)
7.3
/
SU /
2023
1st 6 ...(Count)
2
Tuesday, February 13, 2024 10:36:17AM * Indicates Violation ** Indicates TRC Violation Page 7 of 10

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: '001
Sample Count:
2
Months Sampled :
2
Weeks Sampled:
2
Quarters Sampled :
2
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
Silver
01/18/2023
S Micross011823Self
0.0002
/ mg/L
0.000055 /
lbs/day
04/27/2023
P Micross042723POTW
<
0.0003
/ mg/L
<
0.000071 /
Ibs/day
Jan 2023
Week 3
0.0002
/ mg/L
0.000055 /
Ibs/day
Apr 2023
Week 4
<
0.0003
/ mg/L
<
0.000071 /
lbs/day
Jan 2023
Average
0.0002
/ mg/L
0.000055 /
lbs/day
Apr 2023
Average
<
0.0003
/ mg/L
<
0.000071 /
Ibs/day
2023
Quarter 1
0.0002
/ mg/L
0.000055 /
Ibs/day
2023
Quarter 2
<
0.0003
/ mg/L
<
0.000071 /
Ibs/day
2023
1st 6 Months (Avg)
<
0.0002
/ mg/L
<
0.000063 /
Ibs/day
2023
1st 6 ...(Max)
<
0.0003
/ mg/L
<
0.000071 /
Ibs/day
2023
1st 6 ...(Min)
0.0002
/ mg/L
0.000055 /
Ibs/day
2023
1st 6 ...(Count)
2
/
2 /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
01/18/2023
S Micross011823Self
17.3
/ 66
°C /
04/27/2023
P Micross042723POTW
18
/ 66
°C /
Jan 2023
Week 3
17.3
/
°C /
Apr 2023
Week 4
18
/
G /
Jan 2023
Average
17.3
/
°C /
Apr 2023
Average
18
/
°C /
2023
Quarter 1
17.3
/
°C /
2023
Quarter 2
18
/
°C /
2023
1st 6 Months (Avg)
17.7
/
°C /
2023
1st 6 ...(Max)
18
/
°C /
2023
lst 6 ...(Min)
17.3
/
°C /
2023
1st 6 ...(Count)
2
Tuesday, February 13, 2024 10:36:17AM * Indicates Violation ** Indicates TRC Violation Page 8 of 10

Micross Advanced Interconnect Technolou, LLC
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: '001
Sample Count:
2
Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
2
# Over Daily C :
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0,00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
Tin
01/18/2023
S Micross011823Self
<
0.025000000 /
mg/L
<
0.006295658 /
lbs/day
04/27/2023
P Micross042723POTW
<
0.012500000 /
mg/L
<
0.003562223 /
Ibs/day
Jan 2023
Week 3
<
0 /
mg/L
<
0 /
Ibs/day
Apr 2023
Week 4
<
0 /
mg/L
<
0 /
lbs/day
Jan 2023
Average
<
0 /
mg/L
<
0 /
lbs/day
Apr 2023
Average
<
0 /
mg/L
<
0 /
Ibs/day
2023
Quarter 1
<
0 /
mg/L
<
0 /
Ibs/day
2023
Quarter 2
<
0 /
mg/L
<
0 /
Ibs/day
2023
1st 6 Months (Avg)
<
0 /
mg/L
<
0 /
Ibs/day
2023
1st 6 ...(Max)
<
0 /
mg/L
<
0 /
Ibs/day
2023
1st 6 ...(Min)
<
0 /
mg/L
<
0 /
Ibs/day
2023
1st 6 ...(Count)
2 /
2 /
Sample Date SamplelD Result/Limit Mass/Limit
TKN
01/18/2023
S Micross011823Self
4.8
/ mg/L
1.209 /
lbs/day
04/27/2023
P Micross042723POTW
10.7
/ mg/L
3.049 /
lbs/day
Jan 2023
Week 3
4.8
/ mg/L
1.209 /
lbs/day
Apr 2023
Week 4
10.7
/ mg/L
3.049 /
Ibs/day
Jan 2023
Average
4.8
/ mg/L
1.209 /
Ibs/day
Apr 2023
Average
10.7
/ mg/L
3.049 /
Ibs/day
2023
Quarter 1
4.8
/ mg/L
1.209 /
Ibs/day
2023
Quarter 2
10.7
/ mg/L
3.049 /
lbs/day
2023
1st 6 Months (Avg)
7.75
/ mg/L
2.129 /
lbs/day
2023
1st 6 ...(Max)
10.7
/ mg/L
3.049 /
lbs/day
2023
lst 6 ...(Min)
4.8
/ mg/L
1.209 /
lbs/day
2023
1st 6 ...(Count)
2
/
2 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
01/18/2023 S MicrossO11823Self
04/27/2023 P Micross042723POTW
Jan 2023 Week 3
Tuesday, February 13,2024 10:36:17AM
5.3 / mg/L 1.3347 / Ibs/day
1.37 / mg/L 0.3904 / Ibs/day
5.3 / mg/L 1.3347 / Ibs/day
* Indicates Violation ** Indicates TRC Violation Page 9 of 10

Micross Advanced Interconnect Technolou, LLC
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: '001
Sample Date
SamplelD
Result/Limit
Mass/Limit
Total Phosphorus
Apr 2023
Week 4
1.37 /
mg/L
0.3904 /
lbs/day
Jan 2023
Average
5.3 /
mg/L
1.3347 /
lbs/day
Apr 2023
Average
1.37 /
mg/L
0.3904 /
lbs/day
2023
Quarter 1
5.3 /
mg/L
1.3347 /
Ibs/day
2023
Quarter 2
1.37 /
mg/L
0.3904 /
Ibs/day
2023
1st 6 Months (Avg)
3.335 /
mg/L
0.8625 /
Ibs/day
2023
1st 6 ...(Max)
5.3 /
mg/L
1.3347 /
Ibs/day
2023
1st 6 ...(Min)
1.37 /
mg/L
0.3904 /
Ibs/day
2023
1st 6 ...(Count)
2 /
2 /
Sample Date
SamplelD
Result/Limit
Mass/Limit
VOC
01/18/2023 S
Micross011823Self
0.062 /
mg/L
/
Jan 2023
Week 3
0.062 /
mg/L
/
Jan 2023
Average
0.062 /
mg/L
/
2023
Quarter 1
0.062 /
mg/L
/
2023
1st 6 Months (Avg)
0.062 /
mg/L
/
2023
1st 6 ...(Max)
0.062 /
mg/L
/
2023
1st 6... (Min)
0.062 /
mg/L
/
2023
1st 6 ...(Count)
1
Sample Date
SamplelD
Result/Limit
Mass/Limit
Zinc
01/18/2023
S Micross011823Self
04/27/2023
P Micross042723POTW
Jan 2023
Week 3
Apr 2023
Week 4
Jan 2023
Average
Apr 2023
Average
2023
Quarter 1
2023
Quarter 2
2023
1st 6 Months (Avg)
2023
1st 6 ...(Max)
2023
1st 6 ...(Min)
2023
1st 6 ...(Count)
0.43
/ mg/L
0.349
/ mg/L
0.43
/ mg/L
0.349
/ mg/L
0.43
/ mg/L
0.349
/ mg/L
0.43
/ mg/L
0.349
/ mg/L
0.390
/ mg/L
0.43
/ mg/L
0.349
/ mg/L
2
/
0.108285 /
Ibs/day
0.099457 /
lbs/day
0.108285 /
lbs/day
0.099457 /
Ibs/day
0.108285 /
Ibs/day
0.099457 /
Ibs/day
0.108285 /
Ibs/day
0.099457 /
Ibs/day
0.103871 /
Ibs/day
0.108285 /
lbs/day
0.099457 /
lbs/day
2 /
Tuesday, February 13, 2024 10:36:17AM * Indicates Violation ** Indicates TRC Violation Page 10 of 10

MP Pharma Services, Inc.
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
02/15/2023 S
MPPhanna021523Self <
0.013
/ 20.7
mg/L
<
/
03/30/2023 P
MPPhanna033023POT <
0.025
/ 20.7
mg/L
<
/
W
Feb 2023
Week 3
<
0.013
/
mg/L
<
/
Mar 2023
Week 4
<
0.025
/
mg/L
<
/
Feb 2023
Average
<
0.013
/ 8.2
mg/L
<
/
Mar 2023
Average
<
0.025
/ 8.2
mg/L
<
/
2023
Quarter 1
<
0.019
/
mg/L
<
/
2023
1st 6 Months (Avg) <
0.0188
/
mg/L
<
/
2023
1st 6 ...(Max)
<
0.025
/
mg/L
<
/
2023
1st 6 ...(Min)
<
0.0125
/
mg/L
<
/
2023
1st 6 ...(Count)
2
Sample Count: 2
Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC
:
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
Average Flow for Month
01/31/2023
S
MPPhanna0123F1ow
02/28/2023
S
MPPharma0223F1ow
03/31/2023
S
MPPhanna0323F1ow
04/30/2023
S
MPPhanna0423F1ow
05/31/2023
S
MPPhanna0523F1ow
06/30/2023
S
MPPhanna0623F1ow
Jan 2023
Week 4
Feb 2023
Week 4
Mar 2023
Week 4
Apr 2023
Week 4
May 2023
Week 4
Jun 2023
Week 4
Jan 2023
Average
Feb 2023
Average
Mar 2023
Average
Apr 2023
Average
May 2023
Average
Jun 2023
Average
2023
Quarter 1
0.001415
/
MGD /
0.001865
/
MGD /
0.001448
/
MGD /
0.001678
/
MGD /
0.001815
/
MGD /
0.002269
/
MGD /
0.001415
/
MGD /
0.001865
/
MGD /
0.001448
/
MGD /
0.001678
/
MGD /
0.001815
/
MGD /
0.002269
/
MGD /
0.001415
/ 0.002
MGD /
0.001865
/ 0.002
MGD /
0.001448
/ 0.002
MGD /
0.001678
/ 0.002
MGD /
0.001815
/ 0.002
MGD /
0.002269
/ 0.002
MGD * /
0.001576
/
MGD /
Tuesday, February 13, 2024 10:37:35AM * Indicates Violation ** Indicates TRC Violation Page 1 of 6

MP Pharma Services, Inc.
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
Average Flow for Month
2023
Quarter 2
0.001921 J
MGD
/
2023
1st 6 Months (Avg) 0.001748 /
MGD
/
2023
lst6... (Max)
0.002269 /
MGD
/
2023
1st 6 ...(Min)
0.001415 /
MGD
/
2023
1st 6 ...(Count)
6
Sample Count: 6
Months Sampled: 6
Weeks Sampled :
6
Quarters Sampled :
2
# Over Daily C:
0 0.00
# Over Mo Avg C : 1 16.67
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC : 0 0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M : 0 0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC : 0 0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
Ethyl acetate
02/15/2023 S
MPPharma02l523Self <
0.005
/ 20.7
mg/L
<
/
03/30/2023 P
MPPharma033023POT <
0.005
/ 20.7
mg/L
<
/
W
Feb 2023
Week 3
<
0.005
/
mg/L
<
/
Mar 2023
Week 4
<
0.005
/
mg/L
<
/
Feb 2023
Average
<
0.005
/ 8.2
mg/L
<
/
Mar 2023
Average
<
0.005
/ 8.2
mg/L
<
/
2023
Quarter 1
<
0.005
/
mg/L
<
/
2023
1st 6 Months (Avg) <
0.005
/
mg/L
<
/
2023
Ist 6 ...(Max)
<
0.005
/
mg/L
<
/
2023
1st 6 ...(Min)
<
0.005
/
mg/L
<
/
2023
1st 6 ...(Count)
2
/
/
Sample Count: 2
Months Sampled:
2
Weeks Sampled
:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C:
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC
:
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
Isopropyl acetate
02/15/2023 S MPPharma021523Self < 0.005 / 20.7 mg/L < /
03/30/2023 P MPPhanna033023POT < 0.005 / 20.7 mg/L < /
W
Tuesday, February 13, 2024 10:37:35AM * Indicates Violation ** Indicates TRC Violation Page 2 of 6

MP Pharma Services, Inc.
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
Feb 2023
Week 3
<
0.005
/
mg/L
< /
Mar 2023
Week 4
<
0.005
/
mg/L
< /
Feb 2023
Average
<
0.005
/ 8.2
mg/L
< /
Mar 2023
Average
<
0.005
/ 8.2
mg/L
< /
2023
Quarter 1
<
0.005
/
mg/L
< /
2023
1st 6 Months (Avg)
<
0.005
/
mg/L
< /
2023
1st 6 ...(Max)
<
0.005
/
mg/L
< /
2023
1st 6 ...(Min)
<
0.005
/
mg/L
< /
2023
1st 6 ...(Count)
2
/
/
Sample Count:
2
Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SampleID Result/Limit Mass /Limit
Mercury - LL
02/15/2023 S
MPPharma021523Self
<
0.000001
/ 0.000142
mg/L
< /
03/30/2023 P
MPPharma033023POT
<
0.000001
/ 0.000142
mg/L
< /
WHg
Feb 2023
Week 3
<
0.000001
/
mg/L
< /
Mar 2023
Week 4
<
0.000001
/
mg/L
< /
Feb 2023
Average
<
0.000001
/
mg/L
< /
Mar 2023
Average
<
0.000001
/
mg/L
< /
2023
Quarter 1
<
0.000001
/
mg/L
< /
2023
1st 6 Months (Avg)
<
0.000001
/
mg/L
< /
2023
1st 6 ...(Max)
<
0.000001
/
mg/L
< /
2023
1st 6 ...(Min)
<
0.000001
/
mg/L
< /
2023
1st 6 ...(Count)
2
Sample Count :
2
Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Tuesday, February 13, 2024 10:37:35AM * Indicates Violation ** Indicates TRC Violation Page 3 of 6

MP Pharma Services, Inc.
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
02/15/2023 S
MPPhanna021523Self <
0.003
/ 3.0
mg/L
<
/
03/30/2023 P
MPPhartna033023POT <
0.005
/ 3.0
mg/L
<
/
W
Feb 2023
Week 3
<
0.003
/
mg/L
<
/
Mar 2023
Week 4
<
0.005
/
mg/L
<
/
Feb 2023
Average
<
0.003
/ 0.7
mg/L
<
/
Mar 2023
Average
<
0.005
/ 0.7
mg/L
<
/
2023
Quarter 1
<
0.004
/
mg/L
<
/
2023
1st 6 Months (Avg) <
0.004
/
mg/L
<
/
2023
1st 6 ...(Max)
<
0.005
/
mg/L
<
/
2023
1st 6 ...(Min)
<
0.003
/
mg/L
<
/
2023
1st 6 ...(Count)
2
/
/
Sample Count:
2
Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
n-Amyl acetate
02/15/2023 S MPPharma021523Self < 0.025 / 20.7 mg/L
03/30/2023 P MPPharma033023POT < 0.005 / 20.7 mg/L
W
Feb 2023
Week 3
<
0.025
/
mg/L
<
Mar 2023
Week 4
<
0.005
/
mg/L
<
Feb 2023
Average
<
0.025
/ 8.2
mg/L
<
Mar 2023
Average
<
0.005
/ 8.2
mg/L
<
2023
Quarter 1
<
0.015
/
mg/L
<
2023
1st 6 Months (Avg) <
0.015
/
mg/L
<
2023
1st 6 ...(Max)
<
0.025
/
mg/L
<
2023
1st 6 ...(Min)
<
0.005
/
mg/L
<
2023
1st 6 ...(Count)
2
/
Sample
Count : 2
Months Sampled:
2
Weeks Sampled:
# Over Daily C:
0 0.00
# Over Mo Avg C:
0
0.00
# Over Wk Avg C :
0
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Tuesday, February 13, 2024 10:37:35AM
* Indicates
Violation
** Indicates TRC
Violation
2
Quarters Sampled :
1
#
0.00
# Over Qt Avg C : 0
0.00
0.00
# Over Qt Avg C TRC : 0
0.00
0.00
# Over Qtr Avg M : 0
0.00
0.00
# Over Qtr Avg M TRC : 0
0.00
Page 4 of 6

MP Pharma Services, Inc.
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
PH
02/15/2023 S
MPPhanna021523Self
7.1
/ 6.0 - 10.0
SU
/
03/30/2023 P
MPPhartna033023POT
7.1
/ 6.0 - 10.0
SU
/
W
Feb 2023
Week 3
7.1
/
SU
/
Mar 2023
Week 4
7.1
/
SU
/
Feb 2023
Average
7.1
/
SU
/
Mar 2023
Average
7.1
/
SU
/
2023
Quarter 1
7.1
/
SU
/
2023
1st 6 Months (Avg)
7.1
/
SU
/
2023
1st 6 ...(Max)
7.1
/
SU
/
2023
1st 6 ...(Min)
7.1
/
SU
/
2023
1st 6 ...(Count)
2
Sample Count: 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0 0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0 0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0 0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC :
0 0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
Temperature
02/15/2023 S
MPPharma021523Self
19.9
/ 66
°C
/
03/30/2023 P
MPPharma033023POT
17
/ 66
°C
/
W
Feb 2023
Week 3
19.9
/
°C
/
Mar 2023
Week 4
17
/
°C
/
Feb 2023
Average
19.9
/
°C
/
Mar 2023
Average
17
/
°C
/
2023
Quarter 1
18.5
/
°C
/
2023
1st 6 Months (Avg)
18.5
/
°C
/
2023
1st 6 ...(Max)
19.9
/
°C
/
2023
1st 6 ...(Min)
17
/
°C
/
2023
1st 6 ...(Count)
2
Sample Count : 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C:
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Tuesday, February 13, 2024 10:37:35AM
* Indicates
Violation
** Indicates TRC Violation
Page 5 of 6

MP Pharma Services, Inc.
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
VOC
02/15/2023
S MPPhanna02I523Self
0.0093
/ mg/L /
Feb 2023
Week 3
0.0093
/ mg/L /
Feb 2023
Average
0.0093
/ mg/L /
2023
Quarter 1
0.0093
/ mg/L /
2023
1st 6 Months (Avg)
0.0093
/ mg/L /
2023
Ist6... (Max)
0.0093
/ mg/L /
2023
1st 6 ...(Min)
0.0093
/ mg/L /
2023
1st 6 ...(Count)
1
Tuesday, February 13, 2024 10:37:35AM * Indicates Violation ** Indicates TRC Violation Page 6 of 6

Phononic
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outttall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2023
S
Phononic0123Flow
0.013783
/
MGD /
02/28/2023
S
Phononic0223Flow
0.010655
/
MGD /
03/31/2023
S
Phononie0323Fiow
0.005836
/
MGD /
04/30/2023
S
Phononic0423Flow
0.004611
/
MGD /
05/31/2023
S
Phononic0523F1ow
0.005851
/
MGD /
06/30/2023
S
Phononic0623Flow
0.006137
/
MGD /
Jan 2023
Week 4
0.013783
/
MGD /
Feb 2023
Week 4
0.010655
/
MGD /
Mar 2023
Week 4
0.005836
/
MGD /
Apr 2023
Week 4
0.004611
/
MGD /
May 2023
Week 4
0.005851
/
MGD /
Jun 2023
Week 4
0.006137
/
MGD /
Jan 2023
Average
0.013783
/ 0.020
MGD /
Feb 2023
Average
0.010655
/ 0.020
MGD /
Mar 2023
Average
0.005836
/
MGD /
Apr 2023
Average
0.004611
/ 0.035
MGD /
May 2023
Average
0.005851
/ 0.035
MGD /
Jun 2023
Average
0.006137
/ 0.035
MGD /
2023
Quarter 1
0.005836
/
MGD /
2023
Quarter 1
0.012219
/
MGD /
2023
Quarter 1
0.005836
/
MGD /
2023
Quarter 1
0.012219
/
MGD /
2023
Quarter 2
0.005533
/
MGD /
2023
1st 6 Months (Avg)
0.007812
/
MGD /
2023
1st 6 ...(Max)
0.013783
/
MGD /
2023
1st 6 ...(Min)
0.004611
/
MGD /
2023
lst6... (Count)
6
Sample Count:
6
Months Sampled :
6
Weeks Sampled:
6
Quarters Sampled :
5
# Over Daily C:
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
Bismuth
01/17/2023
S
Phononic011723Self
0.005
/ mg/L /
02/14/2023
S
Phononic021423Self <
0.003
/ mg/L < /
03/22/2023
S
Phononic032223F]ow
0.037
/ mg/L /
04/27/2023
S
Phononic042723Self
0.012
/ mg/L /
Tuesday, February 13, 2024 10:38:54AM * Indicates Violation ** Indicates TRC Violation Page I of 6

Phononic
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Bismuth
04/27/2023
P Phononic042723POT
1.51 /
mg/L
/
W
05/18/2023
S Phononic051823Self
0.237 /
mg/L
/
06/13/2023
S Phononic061323Self
0.02 /
mg/L
/
Jan 2023
Week 3
0.005 /
mg/L
/
Feb 2023
Week 2
<
0.003 /
mg/L
<
/
Mar 2023
Week 4
0.037 /
mg/L
/
Apr 2023
Week 4
0.761 /
mg/L
/
May 2023
Week 3
0.237 /
mg/L
/
Jun 2023
Week 2
0.02 /
mg/L
/
Jan 2023
Average
0.005 /
mg/L
/
Feb 2023
Average
<
0.003 /
mg/L
<
/
Mar 2023
Average
0.037 /
mg/L
/
Apr 2023
Average
0.761 /
mg/L
/
May 2023
Average
0.237 /
mg/L
/
Jun 2023
Average
0.02 /
mg/L
/
2023
Quarter 1
<
0.004 /
mg/L
<
/
2023
Quarter 1
0.037 /
mg/L
/
2023
Quarter 1
<
0.004 /
mg/L
<
/
2023
Quarter 1
0.037 /
mg/L
/
2023
Quarter 2
0.445 /
mg/L
/
2023
1st 6 Months (Avg)
<
0.261 /
mg/L
<
/
2023
1st 6 ...(Max)
1.51 /
mg/L
/
2023
lst6... (Min)
<
0.003 /
mg/L
<
/
2023
lst6... (Count)
7
Sample Date SamplelD Result/Limit Mass/Limit
Mercury - LL
04/27/2023 P
Phononic042723POT
<
0.000001
/ 0.000142
mg/L
< /
WHg
05/18/2023 S
Phononic051823Self
<
0.0001
/ 0.000142
mg/L
< /
Apr 2023
Week 4
<
0.000001
/
mg/L
< /
May 2023
Week 3
<
0.0001
/
mg/L
< /
Apr 2023
Average
<
0.000001
/
mg/L
< /
May 2023
Average
<
0.0001
/
mg/L
< /
2023
Quarter 2
<
0.0001
/
mg/L
< /
2023
Quarter 2
<
0.000001
/
mg/L
< /
2023
Quarter 2
<
0.0001
/
mg/L
< /
2023
Quarter 2
<
0.000001
/
mg/L
< /
2023
1st 6 Months (Avg)
<
0.000050
/
mg/L
< /
2023
1st 6 ...(Max)
<
0.0001
/
mg/L
< /
2023
1st 6 ...(Min)
<
0.000001
/
mg/L
< /
2023
1st 6 ...(Count)
2
/
/
Tuesday, February 13, 2024 10:38:54AM * Indicates Violation ** Indicates TRC Violation Page 2 of 6

Phononic
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
2
Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
4
# Over Daily C :
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0,00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Samplc Date SamplelD Result/Limit Mass/Limit
Molybdenum
04/27/2023
P
Phononic042723POT
<
0.001
/
mg/L
<
0.0001
/
Ibs/day
W
05/18/2023
S
Phononic051823Self
<
0.0025
/
mg/L
<
0.0002
/
Ibs/day
Apr 2023
Week 4
<
0.001
/
mg/L
<
0.0001
/
Ibs/day
May 2023
Week 3
<
0.0025
/
mg/L
<
0.0002
/
Ibs/day
Apr 2023
Average
<
0.001
/
mg/L
<
0.0001
/
lbs/day
May 2023
Average
<
0.0025
/
mg/L
<
0.0002
/
lbs/day
2023
Quarter 2
<
0.0018
/
mg/L
<
0.0001
/
Ibs/day
2023
1st 6 Months (Avg)
<
0.0018
/
mg/L
<
0.0001
/
Ibs/day
2023
lst6... (Max)
<
0.0025
/
mg/L
<
0.0002
/
Ibs/day
2023
lst6... (Min)
<
0.001
/
mg/L
<
0.0001
/
Ibs/day
2023
1st 6 ...(Count)
2
/
2
/
Sample Date
SamplelD
Result/Limit
Mass /Limit
Nickel
01/03/2023
S
Phononic010323Self
0.013
/
mg/L
0.00066
/ 0.02
Ibs/day
01/17/2023
S
Phononic011723Self
0.026
/
mg/L
0.004253
/ 0.02
lbs/day
02/07/2023
S
Phononic02O723Self
0.026
/
mg/L
0.00471
/ 0.02
lbs/day
02/14/2023
S
Phononic021423Self
0.014
/
mg/L
0.002556
/ 0.02
Ibs/day
03/22/2023
S
Phononic032223FIow
<
0.0025
/
mg/L
<
0.000288
/ 0.02
lbs/day
04/27/2023
S
Phononic042723Self
0.005
/
mg/L
0.000537
/ 0.02
Ibs/day
04/27/2023
P
Phononic042723POT
0.0335
/
mg/L
0.004049
/ 0.02
Ibs/day
W
05/18/2023
S
Phononic051823Self
0.01
/
mg/L
0.000711
/ 0.02
Ibs/day
06/13/2023
S
Phononic061323Self
0.01
/
mg/L
0.001228
/ 0.02
Ibs/day
Jan 2023
Week 1
0.013
/
mg/L
0.00066
/
Ibs/day
Jan 2023
Week 3
0.026
/
mg/L
0.004253
/
lbs/day
Feb 2023
Week 1
0.026
/
mg/L
0.00471
/
lbs/day
Feb 2023
Week 2
0.014
/
mg/L
0.002556
/
lbs/day
Mar 2023
Week 4
<
0.0025
/
mg/L
<
0.000288
/
lbs/day
Apr 2023
Week 4
0.0193
/
mg/L
0.002293
/
Ibs/day
May 2023
Week 3
0.01
/
mg/L
0.000711
/
Ibs/day
Jun 2023
Week 2
0.01
/
mg/L
0.001228
/
Ibs/day
Jan 2023
Average
0.0195
/
mg/L
0.002456
/
Ibs/day
Feb 2023
Average
0.02
/
mg/L
0.003633
/
lbs/day
Tuesday, February 13, 2024 10:38:54AM * Indicates Violation ** Indicates TRC Violation Page 3 of 6

Phononic
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
Mar 2023
Average
<
0.0025
/
mg/L <
0.000288 /
lbs/day
Apr 2023
Average
0.0193
/
mg/L
0.002293 /
lbs/day
May 2023
Average
0.01
/
mg/L
0.000711 /
lbs/day
Jun 2023
Average
0.01
/
mg/L
0.001228 /
Ibs/day
2023
Quarter 1
0.0198
/
mg/L
0.003045 /
Ibs/day
2023
Quarter 1
<
0.0025
/
mg/L <
0.000288 /
Ibs/day
2023
Quarter 1
0.0198
/
mg/L
0.003045 /
Ibs/day
2023
Quarter 1
<
0.0025
/
mg/L <
0.000288 /
Ibs/day
2023
Quarter 2
0.0146
/
mg/L
0.001631 /
Ibs/day
2023
1st 6 Months (Avg) <
0.0156
/
mg/L <
0.002110 /
lbs/day
2023
1st 6... (Max)
0.0335
/
mg/L
0.004710 /
lbs/day
2023
1st 6 ...(Min)
<
0.0025
/
mg/L <
0.000288 /
Ibs/day
2023
1st 6 ...(Count)
9
/
9 /
Sample Count: 9
Months Sampled:
6
Weeks Sampled:
8 Quarters Sampled :
5
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00 # Over Qt Avg C :
0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC
:
0
0.00
# Over Wk Avg C TRC : 0
0.00 # Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00 # Over Qtr Avg M :
0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC : 0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
04/27/2023
P Phononic042723POT
6.9
/ 5.0 - 10.0
SU /
W
05/18/2023
S Phononic051823Self
7.92
/ 5.0 - 10.0
SU /
05/24/2023
S Phononic052423Self
6.65
/ 5.0 - 10.0
SU /
Apr 2023
Week 4
6.9
/
SU /
May 2023
Week 3
7.92
/
Su /
May 2023
Week 4
6.65
/
SU /
Apr 2023
Average
6.9
/
SU /
May 2023
Average
7.29
/
SU /
2023
Quarter 2
7.16
/
SU /
2023
1st 6 Months (Avg)
7.16
/
SU /
2023
lst 6 ...(Max)
7.92
/
SU /
2023
1st 6 ...(Min)
6.65
/
SU /
2023
1st 6 ...(Count)
3
Tuesday, February 13, 2024 10:39:54AM * Indicates Violation ** Indicates TRC Violation Page 4 of 6

Phononic
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
3
Months Sampled:
2
Weeks Sampled:
3
Quarters Sampled :
1
# Over Daily C :
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0,00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Samplc Date SamplelD Result/Limit Mass/Limit
Tellurium
01/17/2023
S
Phononic011723Self
0.04 /
mg/L
/
02/14/2023
S
Phononic021423Self
0.017 /
mg/L
/
03/22/2023
S
Phononic032223FIow
0.048 /
mg/L
/
04/27/2023
S
Phononic042723Self
0.044 /
mg/L
/
04/27/2023
P
Phononic042723POT
0.169 /
mg/L
/
W
05/18/2023
S
Phononic051823Self
0.281 /
mg/L
/
06/13/2023
S
Phononic061323Self
0.036 /
mg/L
/
Jan 2023
Week 3
0.04 /
mg/L
/
Feb 2023
Week 2
0.017 /
mg/L
/
Mar 2023
Week 4
0.048 /
mg/L
/
Apr 2023
Week 4
0.107 /
mg/L
/
May 2023
Week 3
0.281 /
mg/L
/
Jun 2023
Week 2
0.036 /
mg/L
/
Jan 2023
Average
0.04 /
mg/L
/
Feb 2023
Average
0.017 /
mg/L
/
Mar 2023
Average
0.048 /
mg/L
/
Apr 2023
Average
0.107 /
mg/L
/
May 2023
Average
0.281 /
mg/L
/
Jun 2023
Average
0.036 /
mg/L
/
2023
Quarter 1
0.029 /
mg/L
/
2023
Quarter 1
0.048 /
mg/L
/
2023
Quarter 1
0.029 /
mg/L
/
2023
Quarter 1
0.048 /
mg/L
/
2023
Quarter 2
0.133 /
mg/L
/
2023
1 st 6 Months (Avg)
0.091 /
mg/L
/
2023
lst6... (Max)
0.281 /
mg/L
/
2023
1st 6 ...(Min)
0.017 /
mg/L
/
2023
1st 6 ...(Count)
7 /
/
Sample Date SamplelD Result/Limit Muss/Limit
Temperature
04/27/2023 P Phononic042723POT 18 / °C /
W
05/24/2023 S Phononic052423Self 21.7 / °C /
Tuesday, February 13, 2024 10:39:54AM * Indicates Violation ** Indicates TRC Violation Page 5 of 6

Phononic
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
Apr 2023
Week 4
18
/ °C /
May 2023
Week 4
21.7
/ °C /
Apr 2023
Average
18
/ °C /
May 2023
Average
21.7
/ °C /
2023
Quarter 2
19.9
/ °C /
2023
1st 6 Months (Avg)
19.9
/ °C /
2023
1st 6 ...(Max)
21.7
/ °C /
2023
1st 6 ...(Min)
18
/ °C /
2023
1st 6 ...(Count)
2
Tuesday, February 13, 2024 10:38:54AM * Indicates Violation ** Indicates TRC Violation Page 6 of 6

PowerSecure
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Aluminum
02/07/2023
02/08/2023
Feb 2023
Feb 2023
Feb 2023
2023
2023
2023
2023
2023
P
S
PowerSecure02O723P
OTW
PowerSecure02O823Se
if
Week 1
Week 2
Average
Quarter 1
1st 6 Months (Avg)
lst6... (Max)
1st 6 ...(Min)
1st 6 ...(Count)
0.869
2.72
0.869
2.72
1.795
1.795
1.795
2.72
0.869
2
/
/
/
/
/
/
/
/
/
/
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
/
/
/
/
/
/
/
/
/
/
Sample Date
SamplelD
Result/Limit
Muss/Limit
Average Flow for Month
01/19/2023
S
PowerSecure0123FIow
0.001074
/
MGD
/
02/28/2023
S
PowerSecure0223F1ow
0.000154
/
MGD
/
03/31/2023
S
PowerSecure0323F1ow
0.000171
/
MGD
/
04/30/2023
S
PowerSecure0423FIow
0.001541
/
MGD
/
05/31/2023
S
PowerSecure0523FIow
0.001908
/
MGD
/
06/30/2023
S
PowerSecure0623F1ow
0.004989
/
MGD
/
Jan 2023
Week 3
0.001074
/
MGD
/
Feb 2023
Week 4
0.000154
/
MGD
/
Mar 2023
Week 4
0.000171
/
MGD
/
Apr 2023
Week 4
0.001541
/
MGD
/
May 2023
Week 4
0.001908
/
MGD
/
Jun 2023
Week 4
0.004989
/
MGD
/
Jan 2023
Average
0.001074
/ 0.006
MGD
/
Feb 2023
Average
0.000154
/ 0.006
MGD
/
Mar 2023
Average
0.000171
/ 0.006
MGD
/
Apr 2023
Average
0.001541
/ 0.006
MGD
/
May 2023
Average
0.001908
/ 0.006
MGD
/
Jun 2023
Average
0.004989
/ 0.006
MGD
/
2023
Quarter 1
0.000466
/
MGD
/
2023
Quarter 2
0.002813
/
MGD
/
2023
1st 6 Months (Avg)
0.001640
/
MGD
/
2023
1st 6 ...(Max)
0.004989
/
MGD
/
2023
1st 6 ...(Min)
0.000154
/
MGD
/
2023
1st 6 ...(Count)
6
Tuesday, February 13, 2024 11:04:34AM * Indicates Violation ** Indicates TRC Violation Page 1 of 8

PowerSecure
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
6
Months Sampled :
6
Weeks Sampled:
6
Quarters Sampled :
2
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
02/07/2023 P
PowerSecure02O723P <
0.00008
/ 0.11
mg/L
<
/
OTW
02/08/2023 S
PowerSecure02O823Se <
0.0005
/ 0.11
mg/L
<
/
if
Feb 2023
Week 1
<
0.00008
/
mg/L
<
/
Feb 2023
Week 2
<
0.0005
/
mg/L
<
/
Feb 2023
Average
<
0.00029
/ 0.07
mg/L
<
/
2023
Quarter 1
<
0.00029
/
mg/L
<
/
2023
1st 6 Months (Avg) <
0.00029
/
mg/L
<
/
2023
1st 6 ...(Max)
<
0.0005
/
mg/L
<
/
2023
1st 6 ...(Min)
<
0.00008
/
mg/L
<
/
2023
Ist 6 ... (Count)
2
Sample Count: 2
Months
Sampled:
1
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SampleID
Result/Limit
Mass/Limit
Chloride
02/07/2023
P PowerSecure02O723P
1430
/
mg/L /
OTW
02/08/2023
S PowerSecure020823Se
1550
/
mg/L /
if
Feb 2023
Week 1
1430
/
mg/L /
Feb 2023
Week 2
1550
/
mg/L /
Feb 2023
Average
1490
/
mg/L /
2023
Quarter 1
1490
/
mg/L /
2023
1st 6 Months (Avg)
1490
/
mg/L /
2023
Ist 6 ...(Max)
1550
/
mg/L /
2023
1st 6 ...(Min)
1430
/
mg/L /
2023
1st 6 ...(Count)
2
Tuesday, February 13, 2024 11:04:34AM
* Indicates Violation
** Indicates TRC Violation
Page 2 of 8

PowerSecure
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
02/07/2023 P
PowerSecure02O723P <
0.001
/ 2.77
mg/L
<
/
OTW
02/08/2023 S
PowerSecure02O823Se <
0.003
/ 2.77
mg/L
<
/
if
Feb 2023
Week 1 <
0.001
/
mg/L
<
/
Feb 2023
Week 2 <
0.003
/
mg/L
<
/
Feb 2023
Average <
0.002
/ 1.71
mg/L
<
/
2023
Quarter 1 <
0.002
/
mg/L
<
/
2023
1st 6 Months (Avg) <
0.002
/
mg/L
<
/
2023
Ist6... (Max) <
0.003
/
mg/L
<
/
2023
1st 6 ...(Min) <
0.001
/
mg/L
<
/
2023
1st 6 ...(Count)
2
/
/
Sample Count: 2 Months Sampled:
1
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass /Limit
Copper
02/07/2023 P
PowerSecure02O723P
0.074
/ 3.38
mg/L
/
OTW
02/08/2023 S
PowerSecure02O823Se
0.091
/ 3.38
mg/L
/
if
Feb 2023
Week 1
0.074
/
mg/L
/
Feb 2023
Week 2
0.091
/
mg/L
/
Feb 2023
Average
0.082
/ 2.07
mg/L
/
2023
Quarter 1
0.082
/
mg/L
/
2023
1st 6 Months (Avg)
0.082
/
mg/L
/
2023
1st 6 ...(Max)
0.091
/
mg/L
/
2023
1st 6 ...(Min)
0.074
/
mg/L
/
2023
1st 6 ...(Count)
2
Sample Count: 2 Months Sampled
:
1
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Tuesday, February 13, 2024 11:04:34AM * Indicates Violation ** Indicates TRC Violation Page 3 of 8

PowerSecure
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
02/07/2023 P
PowerSecure02O723P <
0.003
/ 0.60
mg/L
<
/
OTW
02/08/2023 S
PowerSecure02O823Se <
0.004
/ 0.60
mg/L
<
/
if
Feb 2023
Week 1 <
0.003
/
mg/L
<
/
Feb 2023
Week 2 <
0.004
/
mg/L
<
/
Feb 2023
Average <
0.003
/ 0.50
mg/L
<
/
2023
Quarter 1 <
0.003
/
mg/L
<
/
2023
1st 6 Months (Avg) <
0.003
/
mg/L
<
/
2023
Ist6... (Max) <
0.004
/
mg/L
<
/
2023
1st 6 ...(Min) <
0.003
/
mg/L
<
/
2023
1st 6 ...(Count)
2
/
/
Sample Count: 2 Months Sampled:
1
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass /Limit
Lead
02/07/2023 P
PowerSecure02O723P <
0.0003
/ 0.69
mg/L
<
/
OTW
02/08/2023 S
PowerSecure020823Se <
0.005
/ 0.69
mg/L
<
/
if
Feb 2023
Week 1 <
0.0003
/
mg/L
<
/
Feb 2023
Week 2 <
0.005
/
mg/L
<
/
Feb 2023
Average <
0.0026
/ 0.43
mg/L
<
/
2023
Quarter 1 <
0.0026
/
mg/L
<
/
2023
1st 6 Months (Avg) <
0.0026
/
mg/L
<
/
2023
1st 6 ...(Max) <
0.005
/
mg/L
<
/
2023
1st 6 ...(Min) <
0.0003
/
mg/L
<
/
2023
1st 6 ...(Count)
2
Sample Count: 2 Months Sampled
:
1
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC
:
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Tuesday, February 13, 2024 11:04:34AM * Indicates Violation ** Indicates TRC Violation Page 4 of 8

PowerSecure
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Mercury - LL
02/07/2023 P
PowerSecure02O723P
<
0.000001
/
mg/L
<
/
OTWHg
02/08/2023 S
PowerSecure020823Se
<
0.000001
/
mg/L
<
/
if
Feb 2023
Week 1
<
0.000001
/
mg/L
<
/
Feb 2023
Week 2
<
0.000001
/
mg/L
<
/
Feb 2023
Average
<
0.000001
/
mg/L
<
/
2023
Quarter 1
<
0.000001
/
mg/L
<
/
2023
1st 6 Months (Avg)
<
0.000001
/
mg/L
<
/
2023
Ist 6... (Max)
<
0.000001
/
mg/L
<
/
2023
Ist 6 ...(Min)
<
0.000001
/
mg/L
<
/
2023
Ist 6 ...(Count)
2
/
/
Sample Date
SamplelD
Result/Limit
Muss/Limit
Molybdenum
02/08/2023 S
PowerSecure02O823Se
0.01
/
mg/L
/
if
Feb 2023
Week 2
0.01
/
mg/L
/
Feb 2023
Average
0.01
/
mg/L
/
2023
Quarter 1
0.01
/
mg/L
/
2023
1st 6 Months (Avg)
0.01
/
mg/L
/
2023
Ist 6 ...(Max)
0.01
/
mg/L
/
2023
Ist 6 ...(Min)
0.01
/
mg/L
/
2023
Ist 6 ...(Count)
1
Sample Date SarnpleID Result/Limit Mass /Limit
Nickel
02/07/2023
P PowerSecure02O723P
OTW
02/08/2023
S PowerSecure020823Se
if
Feb 2023
Week 1
Feb 2023
Week 2
Feb 2023
Average
2023
Quarter 1
2023
1st 6 Months (Avg)
2023
1st 6 ...(Max)
2023
Ist 6 ...(Min)
2023
Ist 6 ...(Count)
0.0109
/ 1.30
mg/L /
0.012
/ 1.30
mg/L /
0.0109
/
mg/L /
0.012
/
mg/L /
0.0115
/ 1.00
mg/L /
0.0115
/
mg/L /
0.0115
/
mg/L /
0.012
/
mg/L /
0.0109
/
mg/L /
2
/
/
Tuesday, February 13, 2024 11:04:34AM * Indicates Violation ** Indicates TRC Violation Page 5 of 8

PowerSecure
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
2
Months Sampled :
1
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
PH
02/07/2023 P
PowerSecure02O723P
8.1
/ 6.0 - 10.0
SU
/
OTW
02/08/2023 S
PowerSecure02O823Se
8.8
/ 6.0 - 10.0
SU
/
if
Feb 2023
Week 1
8.1
/
SU
/
Feb 2023
Week 2
8.8
/
SU
/
Feb 2023
Average
8.45
/
SU
/
2023
Quarter 1
8.45
/
Su
/
2023
1st 6 Months (Avg)
8.45
/
SU
/
2023
1st 6 ...(Max)
8.8
/
SU
/
2023
1st 6 ...(Min)
8.1
/
SU
/
2023
Ist 6 ... (Count)
2
Sample Count: 2 Months Sampled:
1
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0 0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0 0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0 0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0 0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SampleID
Result/Limit
Mass/Limit
Silver
02/07/2023
P PowerSecure02O723P
<
0.0003
/ 0.43
mg/L
< /
OTW
02/08/2023
S PowerSecure020823Se
<
0.0025
/ 0.43
mg/L
< /
if
Feb 2023
Week 1
<
0.0003
/
mg/L
< /
Feb 2023
Week 2
<
0.0025
/
mg/L
< /
Feb 2023
Average
<
0.0014
/ 0.24
mg/L
< /
2023
Quarter l
<
0.0014
/
mg/L
< /
2023
1st 6 Months (Avg)
<
0.0014
/
mg/L
< /
2023
Ist 6 ...(Max)
<
0.0025
/
mg/L
< /
2023
1st 6 ...(Min)
<
0.0003
/
mg/L
< /
2023
1st 6 ...(Count)
2
Tuesday, February 13, 2024 11:04:34AM
* Indicates Violation
** Indicates TRC Violation
Page 6 of 8

PowerSecure
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
2
Months Sampled :
1
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
02/07/2023 P
PowerSecure02O723P
18
/ 66
°C
/
OTW
02/08/2023 S
PowerSecure02O823Se
21.4
/ 66
°C
/
if
Feb 2023
Week 1
18
/
°C
/
Feb 2023
Week 2
21A
/
°C
/
Feb 2023
Average
19.7
/
°C
/
2023
Quarter 1
19.7
/
°C
/
2023
1st 6 Months (Avg)
19.7
/
°C
/
2023
1st 6 ...(Max)
21.4
/
°C
/
2023
1st 6 ...(Min)
18
/
°C
/
2023
Ist 6 ... (Count)
2
Sample Count: 2 Months Sampled:
1
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SampleID
Result/Limit
Mass/Limit
TTO
02/08/2023 S
PowerSecure020823Se <
0.025
/ 2,13
mg/L
<
/
if
Feb 2023
Week 2 <
0.025
/
mg/L
<
/
Feb 2023
Average <
0.025
/
mg/L
<
/
2023
Quarter 1 <
0.025
/
mg/L
<
/
2023
1st 6 Months (Avg) <
0.025
/
mg/L
<
/
2023
1st 6 ...(Max) <
0.025
/
mg/L
<
/
2023
1st 6 ...(Min) <
0.025
/
mg/L
<
/
2023
1st 6 ...(Count)
1
Tuesday, February 13, 2024 11:04:34AM * Indicates Violation ** Indicates TRC Violation Page 7 of 8

PowerSecure
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
1
Months Sampled :
1
Weeks Sampled:
1
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
02/07/2023 P
PowerSecure02O723P
0.007
/ 2.61
mg/L
/
OTW
02/08/2023 S
PowerSecure02O823Se <
0.01
/ 2.61
mg/L
<
/
if
Feb 2023
Week 1
0.007
/
mg/L
/
Feb 2023
Week 2 <
0.01
/
mg/L
<
/
Feb 2023
Average <
0.009
/ 1.48
mg/L
<
/
2023
Quarter 1 <
0.009
/
mg/L
<
/
2023
1st 6 Months (Avg) <
0.009
/
mg/L
<
/
2023
1st 6 ...(Max) <
0.01
/
mg/L
<
/
2023
1st 6 ...(Min)
0.007
/
mg/L
/
2023
Ist 6 ... (Count)
2
Sample Count: 2 Months Sampled:
1
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Tuesday, February 13, 2024 11:04:34AM * Indicates Violation ** Indicates TRC Violation Page 8 of 8

SCM Metal Products, Inc.
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
03/01/2023
Mar 2023
Mar 2023
2023
2023
2023
2023
2023
S
SCM030123Self
Week 1
Average
Quarter 1
1st 6 Months (Avg)
lst6... (Max)
1st 6 ...(Min)
1st 6 ...(Count)
3.6
3.6
3.6
3.6
3.6
3.6
3.6
1
/
/
/
/
/
/
/
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
/
/
/
/
/
/
/
Sample Date
Sample/D
Result/Limit
Mass /Limit
Average Flow for Month
01/31/2023
S
SCM0123F1ow
0.016667
/ 0.080
MGD
/
02/28/2023
S
SCM0223F1ow
0.014916
/ 0.080
MGD
/
03/31/2023
S
SCM0323F1ow
0.014154
/ 0.080
MGD
/
04/30/2023
S
SCM0423F1ow
0.0147
/ 0.080
MGD
/
05/31/2023
S
SCM0523F1ow
0.01661
/ 0.080
MGD
/
06/30/2023
S
SCM0623FIow
0.02055
/ 0.080
MGD
/
Jan 2023
Week 4
0.016667
/
MGD
/
Feb 2023
Week 4
0.014916
/
MGD
/
Mar 2023
Week 4
0.014154
/
MGD
/
Apr 2023
Week 4
0.0147
/
MGD
/
May 2023
Week 4
0.01661
/
MGD
/
Jun 2023
Week 4
0.02055
/
MGD
/
Jan 2023
Average
0.016667
10.050
MGD
/
Feb 2023
Average
0.014916
10.050
MGD
/
Mar 2023
Average
0.014154
10.050
MGD
/
Apr 2023
Average
0.0147
10.050
MGD
/
May 2023
Average
0.01661
/ 0.050
MGD
/
Jun 2023
Average
0.02055
/ 0.050
MGD
/
2023
Quarter 1
0.015246
/
MGD
/
2023
Quarter 2
0.017287
/
MGD
/
2023
1st 6 Months (Avg)
0.016266
/
MGD
/
2023
1st 6 ...(Max)
0.02055
/
MGD
/
2023
1st 6 ...(Min)
0.014154
/
MGD
/
2023
1st 6 ...(Count)
6
Tuesday, February 13, 2024 11:05:31AM * Indicates Violation ** Indicates TRC Violation Page 1 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
6
Months Sampled:
6
Weeks Sampled:
6
Quarters Sampled :
2
# Over Daily C :
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0,00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Samplc Date SamplelD Result/Limit Mass/Limit
Cadmium
02/21/2023
P SCM022123POTW
<
0.00008
/ mg/L
<
0.000009 /
Ibs/day
03/01/2023
S SCM030123Self
<
0.0005
/ mg/L
<
/
Feb 2023
Week 3
<
0.00008
/ mg/L
<
0.000009 /
Ibs/day
Mar 2023
Week 1
<
0.0005
/ mg/L
<
/
Feb 2023
Average
<
0.00008
/ mg/L
<
0.000009 /
lbs/day
Mar 2023
Average
<
0.0005
/ mg/L
<
/
2023
Quarter 1
<
0.00029
/ mg/L
<
0.000009 /
Ibs/day
2023
1st 6 Months (Avg)
<
0.00029
/ mg/L
<
0.000009 /
Ibs/day
2023
lst6... (Max)
<
0.0005
/ mg/L
<
0.000009 /
Ibs/day
2023
1st 6 ...(Min)
<
0.00008
/ mg/L
<
/
2023
1st 6 ...(Count)
2
/
1 /
Sample Date SamplelD Result/Limit Mass /Limit
Chloride
02/21/2023
P SCM022123POTW
30
/ mg/L
3.487 /
lbs/day
03/01/2023
S SCM030123Self
15.8
/ mg/L
/
Feb 2023
Week 3
30
/ mg/L
3.487 /
lbs/day
Mar 2023
Week 1
15.8
/ mg/L
/
Feb 2023
Average
30
/ mg/L
3.487 /
Ibs/day
Mar 2023
Average
15.8
/ mg/L
/
2023
Quarter 1
22.9
/ mg/L
3.487 /
Ibs/day
2023
1st 6 Months (Avg)
22.9
/ mg/L
3.4870 /
Ibs/day
2023
1st 6 ...(Max)
30
/ mg/L
3.4870 /
lbs/day
2023
Ist 6 ...(Min)
15.8
/ mg/L
/
2023
1st 6 ...(Count)
2
/
I /
Sample Date
SamplelD
Result/Limit
Mass/Limit
Copper
02/21/2023
P SCM022123POTW
0.085 / 0.75
mg/L
0.009903 /
lbs/day
03/01/2023
S SCM030123Self
0.021 / 0.75
mg/L
/
05/17/2023
S SCM051723Self
0.095 / 0.75
mg/L
0.015939 /
Ibs/day
Feb 2023
Week 3
0.085 /
mg/L
0.009903 /
Ibs/day
Mar 2023
Week 1
0.021 /
mg/L
/
Tuesday, February 13, 2024 11:05:31AM * Indicates Violation ** Indicates TRC Violation Page 2 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Copper
May 2023
Week 3
0.095
/
mg/L
0.015939 / lbs/day
Feb 2023
Average
0.085
10.50
mg/L
0.009903 / lbs/day
Mar 2023
Average
0.021
10.50
mg/L
/
May 2023
Average
0.095
10.50
mg/L
0.015939 / Ibs/day
2023
Quarter 1
0.053
/
mg/L
0.009903 / Ibs/day
2023
Quarter 2
0.095
/
mg/L
0.015939 / Ibs/day
2023
1st 6 Months (Avg)
0.067
/
mg/L
0.012921 / Ibs/day
2023
1st 6 ...(Max)
0.095
/
mg/L
0.015939 / Ibs/day
2023
1st 6 ...(Min)
0.021
/
mg/L
/
2023
1st 6 ...(Count)
3
/
2 /
Sample Count: 3
Months Sampled:
3
Weeks Sampled:
3 Quarters Sampled :
2
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00 # Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00 # Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00 # Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit
Cyanide
Mass /Limit
02/21/2023 P
SCM022123POTW <
0.003
/ 0.04
mg/L
<
0.000291 /
Ibs/day
03/01/2023 S
SCM030123Self
0.02
/ 0.04
mg/L
/
Feb 2023
Week 3 <
0.003
/
mg/L
<
0.000291 /
lbs/day
Mar 2023
Week 1
0.02
/
mg/L
/
Feb 2023
Average <
0.003
/ 0.03
mg/L
<
0.000291 /
lbs/day
Mar 2023
Average
0.02
/ 0.03
mg/L
/
2023
Quarter 1 <
0.011
/
mg/L
<
0.000291 /
Ibs/day
2023
1st 6 Months (Avg) <
0.011
/
mg/L
<
0.000291 /
Ibs/day
2023
1st 6 ...(Max)
0.02
/
mg/L
0.000291 /
Ibs/day
2023
1st 6 ...(Min) <
0.003
/
mg/L
<
/
2023
1st 6 ...(Count)
2
/
I /
Sample Count: 2 Months Sampled
:
2
Weeks Sampled:
2 Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00 # Over Qt Avg C :
0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00 # Over Qt Avg C TRC
: 0
0.00
# Over Daily M:
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00 # Over Qtr Avg M :
0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Tuesday, February 13, 2024 11:05:31AM * Indicates Violation ** Indicates TRC Violation Page 3 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
02/21/2023
P SCM022123POTW
0.62
/ mg/L
0.0721
/ Ibs/day
03/01/2023
S SCM030123Self
0.76
/ mg/L
/
Feb 2023
Week 3
0.62
/ mg/L
0.0721
/ lbs/day
Mar 2023
Week 1
0.76
/ mg/L
/
Feb 2023
Average
0.62
/ mg/L
0.0721
/ Ibs/day
Mar 2023
Average
0.76
/ mg/L
/
2023
Quarter 1
0.69
/ mg/L
0.0721
/ Ibs/day
2023
1st 6 Months (Avg)
0.69
/ mg/L
0.0721
/ Ibs/day
2023
1st 6 ...(Max)
0.76
/ mg/L
0.0721
/ Ibs/day
2023
1st 6 ...(Min)
0.62
/ mg/L
/
2023
lst6... (Count)
2
/
1
/
Sample Date SamplelD Result/Limit Mass/Limit
Lead
02/21/2023 P
SCM022123POTW <
0.0003
/ 0.20
mg/L
<
0.000029 /
lbs/day
03/01/2023 S
SCM030123Self
<
0.005
/ 0.20
mg/L
<
/
05/17/2023 S
SCM051723Self
<
0.0005
/ 0.20
mg/L
<
0.000084 /
Ibs/day
Feb 2023
Week 3
<
0.0003
/
mg/L
<
0.000029 /
Ibs/day
Mar 2023
Week 1
<
0.005
/
mg/L
<
/
May 2023
Week 3
<
0.0005
/
mg/L
<
0.000084 /
Ibs/day
Feb 2023
Average
<
0.0003
/ 0.10
mg/L
<
0.000029 /
lbs/day
Mar 2023
Average
<
0.005
/ 0.10
mg/L
<
/
May 2023
Average
<
0.0005
/ 0.10
mg/L
<
0.000084 /
lbs/day
2023
Quarter 1
<
0.0026
/
mg/L
<
0.000029 /
lbs/day
2023
Quarter 2
<
0.0005
/
mg/L
<
0.000084 /
Ibs/day
2023
1st 6 Months (Avg) <
0.0019
/
mg/L
<
0.000056 /
Ibs/day
2023
1st 6 ...(Max)
<
0.005
/
mg/L
<
0.000084 /
Ibs/day
2023
1st 6 ...(Min)
<
0.0003
/
mg/L
<
/
2023
Ist 6 ... (Count)
3
/
2 /
Sample Count: 3
Months Sampled:
3
Weeks Sampled
:
3 Quarters Sampled :
2
# Over Daily C:
0 0.00
# Over Mo Avg C:
0
0.00
# Over Wk Avg C :
0
0.00 # Over Qt Avg C :
0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC
:
0
0.00
# Over Wk Avg C TRC :
0
0.00 # Over Qt Avg C TRC
: 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00 # Over Qtr Avg M :
0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury - LL
02/21/2023 P SCM022123POTWHg
0.000016 / 0.000142 mg/L
Tuesday, February 13, 2024 11:05:31AM * Indicates Violation ** Indicates TRC Violation Page 4 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Mercury - LL
Feb 2023
Week 3
0.000016
/
mg/L
/
Feb 2023
Average
0.000016
/
mg/L
/
2023
Quarter 1
0.000016
/
mg/L
/
2023
1st 6 Months (Avg) 0.000016
/
mg/L
/
2023
1st 6 ...(Max)
0.000016
/
mg/L
/
2023
lst6... (Min)
0.000016
/
mg/L
/
2023
1st 6 ...(Count)
1
Sample
Count: 1
Months Sampled
:
1
Weeks Sampled:
1
Quarters Sampled :
1
# I%
#
%
#
%
#
%
# Over Daily C :
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
02/21/2023 P
SCM022123POTW
<
0.001
/ mg/L
<
0.0001
/ Ibs/day
03/01/2023 S
SCM030123Self
<
0.005
/ mg/L
<
/
Feb 2023
Week 3
<
0.001
/ mg/L
<
0.0001
/ Ibs/day
Mar 2023
Week 1
<
0.005
/ mg/L
<
/
Feb 2023
Average
<
0.001
/ mg/L
<
0.0001
/ lbs/day
Mar 2023
Average
<
0.005
/ mg/L
<
/
2023
Quarter 1
<
0.003
/ mg/L
<
0.0001
/ lbs/day
2023
1st 6 Months (Avg)
<
0.003
/ mg/L
<
0.0001
/ lbs/day
2023
1st 6 ...(Max)
<
0.005
/ mg/L
<
0.0001
/ Ibs/day
2023
1st 6 ...(Min)
<
0.001
/ mg/L
<
/
2023
1st 6 ...(Count)
2
/
1
/
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
02/21/2023
P SCM022123POTW
0.0009
/
mg/L
0.000105 /
Ibs/day
03/01/2023
S SCM030123Self
<
0.0025
/
mg/L
<
/
Feb 2023
Week 3
0.0009
/
mg/L
0.000105 /
lbs/day
Mar 2023
Week 1
<
0.0025
/
mg/L
<
/
Feb 2023
Average
0.0009
/
mg/L
0.000105 /
lbs/day
Mar 2023
Average
<
0.0025
/
mg/L
<
/
2023
Quarter 1
<
0.0017
/
mg/L
<
0.000105 /
Ibs/day
2023
1st 6 Months (Avg)
<
0.0017
/
mg/L
<
0.000105 /
Ibs/day
2023
1st 6 ...(Max)
<
0.0025
/
mg/L
<
0.000105 /
Ibs/day
Tuesday, February 13, 2024 11:05:31AM
* Indicates Violation
** Indicates TRC Violation
Page 5 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
Nickel
2023
1st 6 ...(Min)
0.0009 /
mg/L
/
2023
1st 6 ...(Count)
2 /
1 /
Sample Date
SamplelD
Result/Limit
Mass /Limit
Nitrate -Nitrite
02/21/2023
P
SCM022123POTW
0.4 /
mg/L
0.042 /
lbs/day
03/01/2023
S
SCM030123Self
0.3 /
mg/L
/
Feb 2023
Week 3
0.4 /
mg/L
0.042 /
lbs/day
Mar 2023
Week 1
0.3 /
mg/L
/
Feb 2023
Average
0.4 /
mg/L
0.042 /
Ibs/day
Mar 2023
Average
0.3 /
mg/L
/
2023
Quarter 1
0.3 /
mg/L
0.042 /
Ibs/day
2023
1st 6 Months (Avg)
0.3 /
mg/L
0.042 /
lbs/day
2023
1st 6 ...(Max)
0.4 /
mg/L
0.042 /
lbs/day
2023
1st 6 ...(Min)
0.3 /
mg/L
/
2023
lst 6 ...(Count)
2 /
1 /
Sample Date
SamplelD
Result/Limit
Mass/Limit
Nitrogen, Total
02/21/2023
P
SCM022123POTW
14.3 /
mg/L
1.662 /
Ibs/day
03/01/2023
S
SCM030123Self
10.3 /
mg/L
/
Feb 2023
Week 3
14.3 /
mg/L
1.662 /
Ibs/day
Mar 2023
Week 1
10.3 /
mg/L
/
Feb 2023
Average
14.3 /
mg/L
1.662 /
Ibs/day
Mar 2023
Average
10.3 /
mg/L
/
2023
Quarter 1
12.3 /
mg/L
1.662 /
lbs/day
2023
1st 6 Months (Avg)
12.3 /
mg/L
1.662 /
Ibs/day
2023
1st 6 ...(Max)
14.3 /
mg/L
1.662 /
Ibs/day
2023
lst6... (Min)
10.3 /
mg/L
/
2023
lst6... (Count)
2 /
1 /
Sample Date
SamplelD
Result/Limit
Mass /Limit
Oil & Grease, Total
02/21/2023
P
SCM022123POTW <
2.5 / 200
mg/L
< /
03/01/2023
S
SCM030123Self
15.9 / 200
mg/L
/
Feb 2023
Week 3 <
2.5 /
mg/L
< /
Mar 2023
Week 1
15.9 /
mg/L
/
Feb 2023
Average <
2.5 /
mg/L
< /
Mar 2023
Average
15.9 /
mg/L
/
2023
Quarter 1 <
9.2 /
mg/L
< /
2023
1st 6 Months (Avg) <
9.2 /
mg/L
< /
Tuesday, February 13, 2024 11:05:31AM * Indicates Violation ** Indicates TRC Violation Page 6 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Oil & Grease, Total
2023
1st 6 ...(Max)
15.9 /
mg/L
/
2023
1st 6 ...(Min)
< 2.5 /
mg/L <
/
2023
lst6...
(Count)
2
Sample Count:
2
Months Sampled :
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
02/21/2023 P
SCM022123POTW
7.5
/ 6.0 - 10.5
SU
/
03/01/2023 S
SCM030123Self
7.4
/ 6.0 - 10.5
SU
/
05/17/2023 S
SCM051723Self
7.4
/ 6.0 - 10.5
SU
/
Feb 2023
Week 3
7.5
/
SU
/
Mar 2023
Week 1
7.4
/
SU
/
May 2023
Week 3
7.4
/
SU
/
Feb 2023
Average
7.5
/
SU
/
Mar 2023
Average
7.4
/
SU
/
May 2023
Average
7.4
/
SU
/
2023
Quarter 1
7.45
/
SU
/
2023
Quarter 2
7.4
/
SU
/
2023
1st 6 Months (Avg)
7.43
/
SU
/
2023
1st 6 ...(Max)
7.5
/
SU
/
2023
1st 6 ...(Min)
7.4
/
SU
/
2023
1st 6 ...(Count)
3
Sample Count: 3 Months Sampled:
3
Weeks Sampled:
3
Quarters Sampled :
2
# Over Daily C:
0 0.00 # Over Mo Avg C:
0 0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0 0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0 0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0 0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Selenium
02/21/2023 P SCM022123POTW <
Tuesday, February 13, 2024 11:05:31AM
0.0005 / mg/L < 0.000058 / Ibs/day
* Indicates Violation ** Indicates TRC Violation
Page 7 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Selenium
03/01/2023
S SCM030123Self
<
0.0075
/ mg/L
<
/
Feb 2023
Week 3
<
0.0005
/ mg/L
<
0.000058 /
lbs/day
Mar 2023
Week 1
<
0.0075
/ mg/L
<
/
Feb 2023
Average
<
0.0005
/ mg/L
<
0.000058 /
Ibs/day
Mar 2023
Average
<
0.0075
/ mg/L
<
/
2023
Quarter 1
<
0.004
/ mg/L
<
0.000058 /
Ibs/day
2023
1st 6 Months (Avg)
<
0.004
/ mg/L
<
0.000058 /
Ibs/day
2023
1st 6 ...(Max)
<
0.0075
/ mg/L
<
0.000058 /
Ibs/day
2023
1st 6 ...(Min)
<
0.0005
/ mg/L
<
/
2023
1st 6 ...(Count)
2
/
1 /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
02/21/2023 P
SCM022123POTW
18
/ 66
°C
/
03/01/2023 S
SCM030123Self
17.1
/ 66
°C
/
05/17/2023 S
SCM051723Self
22.4
/ 66
°C
/
Feb 2023
Week 3
18
/
c
/
Mar 2023
Week 1
17.1
/
°C
/
May 2023
Week 3
22.4
/
°C
/
Feb 2023
Average
18
/
°C
/
Mar 2023
Average
17.1
/
°C
/
May 2023
Average
22.4
/
°C
/
2023
Quarter 1
17.6
/
°C
/
2023
Quarter 2
22.4
/
°C
/
2023
1st 6 Months (Avg)
19.2
/
c
/
2023
1st 6 ...(Max)
22.4
/
°C
/
2023
1st 6 ...(Min)
17.1
/
°C
/
2023
1st 6 ...(Count)
3
Sample Count: 3 Months Sampled
:
3
Weeks Sampled:
3
Quarters Sampled :
2
# Over Daily C:
0 0.00 # Over Mo Avg C:
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass /Limit
TKN
02/21/2023 P SCM022123POTW
03/01/2023 S SCM030123Self
Tuesday, February 13, 2024 11:05:31AM
13.9 / mg/L 1.616 /
10.1 / mg/L /
* Indicates Violation ** Indicates TRC Violation
Ibs/day
Page 8 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
TKN
Feb 2023
Week 3
13.9 /
mg/L
1.616 /
Ibs/day
Mar 2023
Week 1
10.1 /
mg/L
/
Feb 2023
Average
13.9 /
mg/L
1.616 /
lbs/day
Mar 2023
Average
10.1 /
mg/L
/
2023
Quarter 1
12 /
mg/L
1.616 /
Ibs/day
2023
1st 6 Months (Avg)
12 /
mg/L
1.616 /
Ibs/day
2023
1st 6 ...(Max)
13.9 /
mg/L
1.616 /
Ibs/day
2023
1st 6 ...(Min)
10.1 /
mg/L
/
2023
1st 6 ...(Count)
2 /
I /
Sample Date
SamplelD
Result/Limit
Mass/Limit
Total Phosphorus
02/21/2023
P
SCM022123POTW
1.55 /
mg/L
0.1802 /
lbs/day
03/01/2023
S
SCM030123Self
1.2 /
mg/L
/
Feb 2023
Week 3
1.55 /
mg/L
0.1802 /
lbs/day
Mar 2023
Week 1
1.2 /
mg/L
/
Feb 2023
Average
1.55 /
mg/L
0.1802 /
Ibs/day
Mar 2023
Average
1.2 /
mg/L
/
2023
Quarter 1
1.375 /
mg/L
0.1802 /
Ibs/day
2023
1st 6 Months (Avg)
1.375 /
mg/L
0.1802 /
Ibs/day
2023
1st 6 ...(Max)
1.55 /
mg/L
0.1802 /
lbs/day
2023
1st 6 ...(Min)
1.2 /
mg/L
/
2023
1st 6 ...(Count)
2 /
1 /
Sample Date
SamplelD
Result/Limit
Mass/Limit
VOC
03/01/2023
S
SCM030123Self
0.0258 /
mg/L
/
Mar 2023
Week 1
0.0258 /
mg/L
/
Mar 2023
Average
0.0258 /
mg/L
/
2023
Quarter 1
0.0258 /
mg/L
/
2023
1st 6 Months (Avg)
0.0258 /
mg/L
/
2023
1st 6 ...(Max)
0.0258 /
mg/L
/
2023
1st 6 ...(Min)
0.0258 /
mg/L
/
2023
1st 6... (Count)
1
Sample Date
SamplelD
Result/Limit
Mass/Limit
Zinc
02/21/2023
P
SCM022123POTW
0.278 /
mg/L
0.032313 /
lbs/day
03/01/2023
S
SCM030123Self
0.304 /
mg/L
/
Feb 2023
Week 3
0.278 /
mg/L
0.032313 /
Ibs/day
Mar 2023
Week 1
0.304 /
mg/L
/
Tuesday, February 13, 2024 11:05:31AM * Indicates Violation ** Indicates TRC Violation Page 9 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
Feb 2023
Average
0.278 /
mg/L
0.032313 /
Mar 2023
Average
0.304 /
mg/L
/
2023
Quarter 1
0.291 /
mg/L
0.032313 /
2023
1st 6 Months (Avg)
0.291 /
mg/L
0.032313 /
2023
1st 6 ...(Max)
0.304 /
mg/L
0.032313 /
2023
lst6... (Min)
0.278 /
mg/L
/
2023
1st 6 ...(Count)
2 /
1 /
Ibs/day
lbs/day
Ibs/day
Ibs/day
Tuesday, February 13, 2024 11:05:31AM * Indicates Violation ** Indicates TRC Violation Page 10 of 10

Tergus Pharma
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
02/21/2023 P
Tergus022123POTW
0.066
/ 20.7
mg/L
/
03/24/2023 S
Tergus032423Self
0.019
/ 20.7
mg/L
/
Feb 2023
Week 3
0.066
/
mg/L
/
Mar 2023
Week 4
0.019
/
mg/L
/
Feb 2023
Average
0.066
/ 8.2
mg/L
/
Mar 2023
Average
0.019
/ 8.2
mg/L
/
2023
Quarter 1
0.043
/
mg/L
/
2023
1st 6 Months (Avg)
0.043
/
mg/L
/
2023
1st 6 ...(Max)
0.066
/
mg/L
/
2023
1st 6 ...(Min)
0.019
/
mg/L
/
2023
lst 6 ... (Count)
2
Sample Count: 2 Months Sampled
:
2
Weeks Sampled :
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Arsenic
02/21/2023
P Tergus022123POTW
<
0.001
/ mg/L
<
/
03/24/2023
S Tergus032423Self
<
0.0015
/ mg/L
<
/
Feb 2023
Week 3
<
0.001
/ mg/L
<
/
Mar 2023
Week 4
<
0.0015
/ mg/L
<
/
Feb 2023
Average
<
0.001
/ mg/L
<
/
Mar 2023
Average
<
0.0015
/ mg/L
<
/
2023
Quarter 1
<
0.0013
/ mg/L
<
/
2023
1st 6 Months (Avg)
<
0.0013
/ mg/L
<
/
2023
1st 6 ...(Max)
<
0.0015
/ mg/L
<
/
2023
1st 6 ...(Min)
<
0.001
/ mg/L
<
/
2023
1st 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
Average Flow for Month
01/31/2023
S
Tergus0123FIow
0.00629
/
MGD
/
02/28/2023
S
Tergus0223F1ow
0.005436
/
MGD
/
03/31/2023
S
Tergus0323F1ow
0.005957
/
MGD
/
04/30/2023
S
Tergus0423F1ow
0.004523
/
MGD
/
05/31/2023
S
Tergus0523F1ow
0.004415
/
MGD
/
Saturday, February 24, 2024 7:42:19PM * Indicates Violation ** Indicates TRC Violation Page 1 of 13

Tergus Pharma
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
06/30/2023
Tergus0623FIow
0.004859
/
MGD /
Jan 2023
Week 4
0.00629
/
MGD /
Feb 2023
Week 4
0.005436
/
MGD /
Mar 2023
Week 4
0.005957
/
MGD /
Apr 2023
Week 4
0.004523
/
MGD /
May 2023
Week 4
0.004415
/
MGD /
Jun 2023
Week 4
0.004859
/
MGD /
Jan 2023
Average
0.00629
/ 0.006512
MGD /
Feb 2023
Average
0.005436
/ 0.006512
MGD /
Mar 2023
Average
0.005957
/ 0.006512
MGD /
Apr 2023
Average
0.004523
/ 0.006512
MGD /
May 2023
Average
0.004415
/ 0.006512
MGD /
Jun 2023
Average
0.004859
/ 0.006512
MGD /
2023
Quarter 1
0.005894
/
MGD /
2023
Quarter 2
0.004599
/
MGD /
2023
1st 6 Months (Avg)
0.005247
/
MGD /
2023
1st 6 ...(Max)
0.00629
/
MGD /
2023
1st 6 ...(Min)
0.004415
/
MGD /
2023
1st 6 ...(Count)
6
Sample Count:
6
Months Sampled :
6
Weeks Sampled :
6
Quarters Sampled :
2
# Over Daily C:
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
BOD
02/21/2023
P Tergus022123POTW
77
/ mg/L /
03/24/2023
S Tergus032423Self
19.8
/ mg/L /
Feb 2023
Week 3
77
/ mg/L /
Mar 2023
Week 4
19.8
/ mg/L /
Feb 2023
Average
77
/ mg/L /
Mar 2023
Average
19.8
/ mg/L /
2023
Quarter 1
48.4
/ mg/L /
2023
1st 6 Months (Avg)
48.4
/ mg/L /
2023
1st 6 ...(Max)
77
/ mg/L /
2023
1st 6 ...(Min)
19.8
/ mg/L /
2023
1st 6 ...(Count)
2
Saturday, February 24, 2024 7:42:19PM * Indicates Violation ** Indicates TRC Violation Page 2 of 13

Tergus Pharma
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
02/21/2023
P Tergus022123POTW
<
0.00008
/ mg/L
<
/
03/24/2023
S Tergus032423Self
<
0.00025
/ mg/L
<
/
Feb 2023
Week 3
<
0.00008
/ mg/L
<
/
Mar 2023
Week 4
<
0.00025
/ mg/L
<
/
Feb 2023
Average
<
0.00008
/ mg/L
<
/
Mar 2023
Average
<
0.00025
/ mg/L
<
/
2023
Quarter 1
<
0.00016
/ mg/L
<
/
2023
1st 6 Months (Avg)
<
0.00016
/ mg/L
<
/
2023
1st 6 ...(Max)
<
0.00025
/ mg/L
<
/
2023
1st 6 ...(Min)
<
0.00008
/ mg/L
<
/
2023
lst6 ... (Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
02/21/2023
P Tergus022123POTW
35
/ mg/L
/
03/24/2023
S Tergus032423Self
8.93
/ mg/L
/
Feb 2023
Week 3
35
/ mg/L
/
Mar 2023
Week 4
8.93
/ mg/L
/
Feb 2023
Average
35
/ mg/L
/
Mar 2023
Average
8.93
/ mg/L
/
2023
Quarter 1
21.97
/ mg/L
/
2023
1st 6 Months (Avg)
21.97
/ mg/L
/
2023
1st 6 ...(Max)
35
/ mg/L
/
2023
lst 6 ...(Min)
8.93
/ mg/L
/
2023
1st 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
02/21/2023
P Tergus022123POTW
<
0.001
/ mg/L
< /
03/24/2023
S Tergus032423Self
<
0.003
/ mg/L
< /
Feb 2023
Week 3
<
0.001
/ mg/L
< /
Mar 2023
Week 4
<
0.003
/ mg/L
< /
Feb 2023
Average
<
0.001
/ mg/L
< /
Mar 2023
Average
<
0.003
/ mg/L
< /
2023
Quarter 1
<
0.002
/ mg/L
< /
2023
1st 6 Months (Avg)
<
0.002
/ mg/L
< /
2023
lst6... (Max)
<
0.003
/ mg/L
< /
2023
lst6... (Min)
<
0.001
/ mg/L
< /
2023
1st 6 ...(Count)
2
Saturday, February 24, 2024 7:42:19PM * Indicates Violation ** Indicates TRC Violation Page 3 of 13

Tergus Pharma
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Copper
02/21/2023
P Tergus022123POTW
0.044
/ mg/L
/
03/24/2023
S Tergus032423Self
0.031
/ mg/L
/
Feb 2023
Week 3
0.044
/ mg/L
/
Mar 2023
Week 4
0.031
/ mg/L
/
Feb 2023
Average
0.044
/ mg/L
/
Mar 2023
Average
0.031
/ mg/L
/
2023
Quarter 1
0.038
/ mg/L
/
2023
1st 6 Months (Avg)
0.038
/ mg/L
/
2023
1st 6 ...(Max)
0.044
/ mg/L
/
2023
1st 6 ...(Min)
0.031
/ mg/L
/
2023
lst6 ... (Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
02/21/2023
P Tergus022123POTW
<
0.003
/ mg/L
<
/
03/24/2023
S Tergus032423Self
<
0.003
/ mg/L
<
/
Feb 2023
Week 3
<
0.003
/ mg/L
<
/
Mar 2023
Week 4
<
0.003
/ mg/L
<
/
Feb 2023
Average
<
0.003
/ mg/L
<
/
Mar 2023
Average
<
0.003
/ mg/L
<
/
2023
Quarter 1
<
0.003
/ mg/L
<
/
2023
1st 6 Months (Avg)
<
0.003
/ mg/L
<
/
2023
1st 6 ...(Max)
<
0.003
/ mg/L
<
/
2023
lst 6 ...(Min)
<
0.003
/ mg/L
<
/
2023
1st 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
02/21/2023
P Tergus022123POTW
<
0.003
/ 20.7
mg/L
< /
03/24/2023
S Tergus032423Self
<
0.005
/ 20.7
mg/L
< /
Feb 2023
Week 3
<
0.003
/
mg/L
< /
Mar 2023
Week 4
<
0.005
/
mg/L
< /
Feb 2023
Average
<
0.003
/ 8.2
mg/L
< /
Mar 2023
Average
<
0.005
/ 8.2
mg/L
< /
2023
Quarter 1
<
0.004
/
mg/L
< /
2023
1st 6 Months (Avg)
<
0.004
/
mg/L
< /
2023
lst6... (Max)
<
0.005
/
mg/L
< /
2023
lst6... (Min)
<
0.003
/
mg/L
< /
2023
1st 6 ...(Count)
2
Saturday, February 24, 2024 7:42:19PM * Indicates Violation ** Indicates TRC Violation Page 4 of 13

Tergus Pharma
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
2
Months Sampled :
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
02/21/2023
P Tergus022123POTW
1.4
/ mg/L
/
03/24/2023
S Tergus032423Self
0.64
/ mg/L
/
Feb 2023
Week 3
1.4
/ mg/L
/
Mar 2023
Week 4
0.64
/ mg/L
/
Feb 2023
Average
1.4
/ mg/L
/
Mar 2023
Average
0.64
/ mg/L
/
2023
Quarter 1
1.02
/ mg/L
/
2023
1st 6 Months (Avg)
1.02
/ mg/L
/
2023
lst6... (Max)
1.4
/ mg/L
/
2023
1st 6 ...(Min)
0.64
/ mg/L
/
2023
1st 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
02/21/2023 P
Tergus022123POTW <
0.003
/ 20.7
mg/L
<
/
03/24/2023 S
Tergus032423Self <
0.003
/ 20.7
mg/L
<
/
Feb 2023
Week 3 <
0.003
/
mg/L
<
/
Mar 2023
Week 4 <
0.003
/
mg/L
<
/
Feb 2023
Average <
0.003
/ 8.2
mg/L
<
/
Mar 2023
Average <
0.003
/ 8.2
mg/L
<
/
2023
Quarter 1 <
0.003
/
mg/L
<
/
2023
1st 6 Months (Avg) <
0.003
/
mg/L
<
/
2023
1st 6 ...(Max) <
0.003
/
mg/L
<
/
2023
1st 6 ...(Min) <
0.003
/
mg/L
<
/
2023
1st 6 ...(Count)
2
Sample Count : 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Saturday, February 24, 2024 7:42:19PM * Indicates Violation ** Indicates TRC Violation Page 5 of 13

Tergus Pharma
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Lead
02/21/2023
P Tergus022123POTW
<
0.0003
/ mg/L
<
/
03/24/2023
S Tergus032423Self
<
0.0013
/ mg/L
<
/
Feb 2023
Week 3
<
0.0003
/ mg/L
<
/
Mar 2023
Week 4
<
0.0013
/ mg/L
<
/
Feb 2023
Average
<
0.0003
/ mg/L
<
/
Mar 2023
Average
<
0.0013
/ mg/L
<
/
2023
Quarter 1
<
0.0008
/ mg/L
<
/
2023
1st 6 Months (Avg)
<
0.0008
/ mg/L
<
/
2023
1st 6 ...(Max)
<
0.0013
/ mg/L
<
/
2023
1st 6 ...(Min)
<
0.0003
/ mg/L
<
/
2023
lst6 ... (Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
Mercury - LL
02/21/2023 P
Tergus022123POTWH < 0.000001
/ 0.000142
mg/L
<
/
g
03/24/2023 S
Tergus032423Self < 0.000001
/ 0.000142
mg/L
<
/
Feb 2023
Week 3 < 0.000001
/
mg/L
<
/
Mar 2023
Week 4 < 0.000001
/
mg/L
<
/
Feb 2023
Average < 0.000001
/
mg/L
<
/
Mar 2023
Average < 0.000001
/
mg/L
<
/
2023
Quarter 1 < 0.000001
/
mg/L
<
/
2023
1st 6 Months (Avg) < 0.000001
/
mg/L
<
/
2023
Ist 6 ...(Max) < 0.000001
/
mg/L
<
/
2023
1st 6 ...(Min) < 0.000001
/
mg/L
<
/
2023
1st 6 ...(Count) 2
Sample Count: 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C:
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
02/21/2023 P
Tergus022123POTW <
03/24/2023 S
Tergus032423Self <
Feb 2023
Week 3 <
Mar 2023
Week 4 <
Feb 2023
Average <
0.003
/ 3.0
mg/L < /
0.003
/ 3.0
mg/L < /
0.003
/
mg/L < /
0.003
/
mg/L < /
0.003
/ 0.7
mg/L < /
Saturday, February 24, 2024 7:42:19PM * Indicates Violation ** Indicates TRC Violation Page 6 of 13

Tergus Pharma
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
Mar 2023
Average <
0.003
/ 0.7
mg/L
<
/
2023
Quarter 1 <
0.003
/
mg/L
<
/
2023
1 st 6 Months (Avg) <
0.003
/
mg/L
<
/
2023
1st 6 ...(Max) <
0.003
/
mg/L
<
/
2023
1st 6 ...(Min) <
0.003
/
mg/L
<
/
2023
1st 6 ...(Count)
2
Sample Count:
2 Months Sampled
:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass /Limit
Molybdenum
02/21/2023 P
Tergus022123POTW <
0.001
/
mg/L
<
/
03/24/2023 S
Tergus032423Self <
0.003
/
mg/L
<
/
Feb 2023
Week 3 <
0.001
/
mg/L
<
/
Mar 2023
Week 4 <
0.003
/
mg/L
<
/
Feb 2023
Average <
0.001
/
mg/L
<
/
Mar 2023
Average <
0.003
/
mg/L
<
/
2023
Quarter 1 <
0.002
/
mg/L
<
/
2023
1st 6 Months (Avg) <
0.002
/
mg/L
<
/
2023
lst 6 ...(Max) <
0.003
/
mg/L
<
/
2023
1st 6 ...(Min) <
0.001
/
mg/L
<
/
2023
1st 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass / Limit
n-Amyl acetate
02/21/2023 P
Tergus022123POTW
03/24/2023 S
Tergas032423Self
Feb 2023
Week 3
Mar 2023
Week 4
Feb 2023
Average
Mar 2023
Average
2023
Quarter 1
2023
1st 6 Months (Avg)
2023
1st 6 ...(Max)
2023
1st 6 ...(Min)
< 0.003
/ 20.7
mg/L
< /
< 0.003
/ 20.7
mg/L
< /
< 0.003
/
mg/L
< /
< 0.003
/
mg/L
< /
< 0.003
/ 8.2
mg/L
< /
< 0.003
/ 8.2
mg/L
< /
< 0.003
/
mg/L
< /
< 0.003
/
mg/L
< /
< 0.003
/
mg/L
< /
< 0.003
/
mg/L
< /
Saturday, February 24, 2024 7:42:19PM * Indicates Violation ** Indicates TRC Violation Page 7 of 13

Tergus Pharma
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
n-Amyl acetate
2023
1st 6 ...(Count)
2
Sample Count: 2 Months Sampled: 2
Weeks Sampled: 2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C:
0 0.00
# Over Wk Avg C :
0 0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC
: 0 0.00
# Over Wk Avg C TRC :
0 0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0 0.00
# Over Wk Avg M :
0 0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC
: 0 0.00
# Over Wk Avg M TRC :
0 0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SampleID
Result/Limit
Mass /Limit
Nickel
02/21/2023 P
Tergus022123POTW
0.0006 /
mg/L
/
03/24/2023 S
Tergus032423Self <
0.0005 /
mg/L
<
/
Feb 2023
Week 3
0.0006 /
mg/L
/
Mar 2023
Week 4 <
0.0005 /
mg/L
<
/
Feb 2023
Average
0.0006 /
mg/L
/
Mar 2023
Average <
0.0005 /
mg/L
<
/
2023
Quarter 1 <
0.0006 /
mg/L
<
/
2023
1st 6 Months (Avg) <
0.0006 /
mg/L
<
/
2023
1st 6 ...(Max)
0.0006 /
mg/L
/
2023
1st 6 ...(Min) <
0.0005 /
mg/L
<
/
2023
1st 6 ...(Count)
2 /
/
Sample Date
SamplelD
Result/Limit
Mass/Limit
Nitrate -Nitrite
02/21/2023 P
Tergus022123POTW
0.3 /
mg/L
/
Feb 2023
Week 3
0.3 /
mg/L
/
Feb 2023
Average
0.3 /
mg/L
/
2023
Quarter 1
0.3 /
mg/L
/
2023
1st 6 Months (Avg)
0.3 /
mg/L
/
2023
lst6... (Max)
0.3 /
mg/L
/
2023
1st 6 ...(Min)
0.3 /
mg/L
/
2023
1st 6 ...(Count)
1
Sample Date
SampleID
Result/Limit
Mass/Limit
Nitrogen, Total
02/21/2023 P
Tergus022123POTW
2.31 /
mg/L
/
03/24/2023 S
Tergus032423Self
0.43 /
mg/L
/
Feb 2023
Week 3
2.31 /
mg/L
/
Mar 2023
Week 4
0.43 /
mg/L
/
Saturday, February 24, 2024 7:42:19PM * Indicates Violation ** Indicates TRC Violation Page 8 of 13

Tergus Pharma
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
Nitrogen, Total
Feb 2023
Average
2.31
/
mg/L
/
Mar 2023
Average
0.43
/
mg/L
/
2023
Quarter 1
1.37
/
mg/L
/
2023
1st 6 Months (Avg)
1.37
/
mg/L
/
2023
1st 6 ...(Max)
2.31
/
mg/L
/
2023
lst6... (Min)
0.43
/
mg/L
/
2023
1st 6 ...(Count)
2
Sample Date
SamplelD
Result /Limit
Mass /Limit
Oil & Grease, Total
02/21/2023 P
Tergus022123POTW <
2.5
/ 200
mg/L
<
/
03/24/2023 S
Tergus032423Self <
2.5
/ 200
mg/L
<
/
Feb 2023
Week 3 <
2.5
/
mg/L
<
/
Mar 2023
Week 4 <
2.5
/
mg/L
<
/
Feb 2023
Average <
2.5
/
mg/L
<
/
Mar 2023
Average <
2.5
/
mg/L
<
/
2023
Quarter 1 <
2.5
/
mg/L
<
/
2023
1st 6 Months (Avg) <
2.5
/
mg/L
<
/
2023
1st 6 ...(Max) <
2.5
/
mg/L
<
/
2023
1st 6 ...(Min) <
2.5
/
mg/L
<
/
2023
1st 6 ...(Count)
2
Sample Count: 2 Months Sampled:
2
Weeks Sampled
:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C:
0 0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC
:
0 0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0 0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC
:
0 0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
PH
02/21/2023 P
Tergus022123POTW
7.6
/ 6.0 - 10.0
SU
/
03/24/2023 S
Tergus032423Self
7.52
/ 6.0 - 10.0
SU
/
Feb 2023
Week 3
7.6
/
SU
/
Mar 2023
Week 4
7.52
/
SU
/
Feb 2023
Average
7.6
/
SU
/
Mar 2023
Average
7.52
/
SU
/
2023
Quarter 1
7.56
/
SU
/
2023
1st 6 Months (Avg)
7.56
/
SU
/
2023
1st 6 ...(Max)
7.6
/
SU
/
Saturday, February 24, 2024 7:42:19PM * Indicates Violation ** Indicates TRC Violation Page 9 of 13

Tergus Pharma
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
pH
2023
1st 6 ...(Min)
7.52
/
SU
/
2023
1st 6 ...(Count)
2
/
/
Sample Count : 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC
:
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
Selenium
02/21/2023 P
Tergus022123POTW <
0.0005
/
mg/L
<
/
03/24/2023 S
Tergus032423Self <
0.0013
/
mg/L
<
/
Feb 2023
Week 3 <
0.0005
/
mg/L
<
/
Mar 2023
Week 4 <
0.0013
/
mg/L
<
/
Feb 2023
Average <
0.0005
/
mg/L
<
/
Mar 2023
Average <
0.0013
/
mg/L
<
/
2023
Quarter 1 <
0.0009
/
mg/L
<
/
2023
1st 6 Months (Avg) <
0.0009
/
mg/L
<
/
2023
1st 6 ...(Max) <
0.0013
/
mg/L
<
/
2023
1st 6 ...(Min) <
0.0005
/
mg/L
<
/
2023
1st 6 ...(Count)
2
/
/
Sample Date SamplelD Result/Limit Mass/Limit
Silver
02/21/2023
P Tergus022123POTW
<
0.0003
/ mg/L
<
/
03/24/2023
S Tergus032423Self
<
0.0005
/ mg/L
<
/
Feb 2023
Week 3
<
0.0003
/ mg/L
<
/
Mar 2023
Week 4
<
0.0005
/ mg/L
<
/
Feb 2023
Average
<
0.0003
/ mg/L
<
/
Mar 2023
Average
<
0.0005
/ mg/L
<
/
2023
Quarter 1
<
0.0004
J mg/L
<
/
2023
1st 6 Months (Avg)
<
0.0004
/ mg/L
<
/
2023
1st 6... (Max)
<
0.0005
/ mg/L
<
/
2023
1st 6 ...(Min)
<
0.0003
/ mg/L
<
/
2023
1st 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass /Limit
Temperature
Saturday, February 24, 2024 7:42:19PM * Indicates Violation ** Indicates TRC Violation Page 10 of 13

Tergus Pharma
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
Temperature
02/21/2023 P
Tergus022123POTW
27 / 66
°C
/
03/24/2023 S
Tergus032423Self
10.6 / 66
°C
/
Feb 2023
Week 3
27 /
°C
/
Mar 2023
Week 4
10.6 /
°C
/
Feb 2023
Average
27 /
°C
/
Mar 2023
Average
10.6 /
°C
/
2023
Quarter 1
18.8 /
°C
/
2023
1st 6 Months (Avg)
18.8 /
°C
/
2023
1st 6 ...(Max)
27 /
°C
/
2023
1st 6 ...(Min)
10.6 /
°C
/
2023
lst 6 ... (Count)
2
Sample Count: 2 Months Sampled : 2
Weeks Sampled :
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0 0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0 0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0 0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC :
0 0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
TKN
02/21/2023 P
Tergus022123POTW
2.01 /
mg/L
/
Feb 2023
Week 3
2.01 /
mg/L
/
Feb 2023
Average
2.01 /
mg/L
/
2023
Quarter 1
2.01 /
mg/L
/
2023
1st 6 Months (Avg)
2.01 /
mg/L
/
2023
1st 6 ...(Max)
2.01 /
mg/L
/
2023
1st 6 ...(Min)
2.01 /
mg/L
/
2023
Ist 6 ... (Count)
1
Sample Date
SamplelD
Result/Limit
Mass/Limit
Total Phosphorus
02/21/2023 P
Tergus022123POTW
0.725 /
mg/L
/
03/24/2023 S
Tergus032423Self
0.486 /
mg/L
/
Feb 2023
Week 3
0.725 /
mg/L
/
Mar 2023
Week 4
0.486 /
mg/L
/
Feb 2023
Average
0.725 /
mg/L
/
Mar 2023
Average
0.486 /
mg/L
/
2023
Quarter 1
0.606 /
mg/L
/
2023
1st 6 Months (Avg)
0.606 /
mg/L
/
Saturday, February 24, 2024 7:42:19PM * Indicates Violation ** Indicates TRC Violation Page 11 of 13

Tergus Pharma
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
Total Phosphorus
2023
1st 6 ...(Max)
0.725 /
mg/L
/
2023
1st 6 ...(Min)
0.486 /
mg/L
/
2023
1st 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
TSS
02/21/2023
P
Tergus022123POTW
6 /
mg/L
/
03/24/2023
S
Tergus032423Self
<
1.3 /
mg/L
<
/
Feb 2023
Week 3
6 /
mg/L
/
Mar 2023
Week 4
<
1.3 /
mg/L
<
/
Feb 2023
Average
6 /
mg/L
/
Mar 2023
Average
<
1.3 /
mg/L
<
/
2023
Quarter 1
<
3.6 /
mg/L
<
/
2023
1st 6 Months (Avg)
<
3.6 /
mg/L
<
/
2023
1st 6 ...(Max)
6 /
mg/L
/
2023
lst 6 ...(Min)
<
1.3 /
mg/L
<
/
2023
lst6... (Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
VOC
02/21/2023
P
Tergus022123POTW
0.0657 /
mg/L
/
03/24/2023
S
Tergus032423Self
0.0489 /
mg/L
/
Feb 2023
Week 3
0.0657 /
mg/L
/
Mar 2023
Week 4
0.0489 /
mg/L
/
Feb 2023
Average
0.0657 /
mg/L
/
Mar 2023
Average
0.0489 /
mg/L
/
2023
Quarter 1
0.0573 /
mg/L
/
2023
1st 6 Months (Avg)
0.0573 /
mg/L
/
2023
lst6... (Max)
0.0657 /
mg/L
/
2023
lst6... (Min)
0.0489 /
mg/L
/
2023
1st 6 ...(Count)
2 /
/
Sample Date
SamplelD
Result/Limit
Mass /Limit
Zinc
02/21/2023
P
Tergus022123POTW
0.238 /
mg/L
/
03/24/2023
S
Tergus032423Self
0.388 /
mg/L
/
Feb 2023
Week 3
0.238 /
mg/L
/
Mar 2023
Week 4
0.388 /
mg/L
/
Feb 2023
Average
0.238 /
mg/L
/
Mar 2023
Average
0.388 /
mg/L
/
2023
Quarter 1
0.313 /
mg/L
/
Saturday, February 24, 2024 7:42:19PM * Indicates Violation ** Indicates TRC Violation Page 12 of 13

Tergus Pharma
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
2023
1st 6 Months (Avg)
0.313 /
mg/L /
2023
1st 6 ...(Max)
0.388 /
mg/L /
2023
lst6... (Min)
0.238 /
mg/L /
2023
1st 6 ...(Count)
2 /
/
Saturday, February 24, 2024 7:42:19PM * Indicates Violation ** Indicates TRC Violation Page 13 of 13

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result/Limit Mass/Limit
Acetone
01/31/2023 P
TriPharm013123POT
0.327
/ 5.44
mg/L
0.0101 / lbs/day
W
02/21/2023 S
TriPhartn022123Self <
0.003
/ 5.44
mg/L
<
/
Jan 2023
Week 4
0.327
/
mg/L
0.0101 / lbs/day
Feb 2023
Week 3 <
0.003
/
mg/L
<
/
Jan 2023
Average
0.327
/ 2.15
mg/L
0.0101 / Ibs/day
Feb 2023
Average <
0.003
/ 2,15
mg/L
<
/
2023
Quarter 1 <
0.165
/
mg/L
<
0.0101 / Ibs/day
2023
1st 6 Months (Avg) <
0.165
/
mg/L
<
0.0101 / Ibs/day
2023
1st 6 ...(Max)
0.327
/
mg/L
0.0101 / Ibs/day
2023
1st 6 ...(Min) <
0.003
/
mg/L
<
/
2023
1st 6 ...(Count)
2
/
1 /
Sample Count: 2 Months Sampled:
2
Weeks Sampled:
2 Quarters Sampled :
I
# Over Daily C :
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00 # Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC
:
0
0.00
# Over Wk Avg C TRC :
0
0.00 # Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00 # Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SampleID
Result/Limit
Mass /Limit
Ammonia
01/31/2023
P TriPharm013123POT
0.2
/ mg/L
0.0062 /
Ibs/day
W
02/21/2023
S TriPharm022123Self
0.4
/ mg/L
/
Jan 2023
Week 4
0.2
/ mg/L
0.0062 /
lbs/day
Feb 2023
Week 3
0.4
/ mg/L
/
Jan 2023
Average
0.2
/ mg/L
0.0062 /
Ibs/day
Feb 2023
Average
0.4
/ mg/L
/
2023
Quarter 1
0.3
/ mg/L
0.0062 /
Ibs/day
2023
1st 6 Months (Avg)
0.3
/ mg/L
0.0062 /
Ibs/day
2023
1st 6 ...(Max)
0.4
/ mg/L
0.0062 /
Ibs/day
2023
1st 6 ...(Min)
0.2
/ mg/L
/
2023
1st 6 ...(Count)
2
/
1 /
Sample Date SampleID Result/Limit Mass I Limit
Average Flow for Month
01/31/2023
S
TriPharm0123171ow
02/28/2023
S
TriPharm0223F1ow
03/31/2023
S
TriPharm0323Flow
04/30/2023
S
TriPharm0423F1ow
0.005578 /
MGD /
0.002601 /
MGD /
0.003273 /
MGD /
0.003725 /
MGD /
Saturday, February 24, 2024 9:18:36PM * Indicates Violation ** Indicates TRC Violation Page 1 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater 0111M11: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
05/31/2023 S
TriPharm0523F1ow
0.005347
/
MGD
/
06/30/2023 S
TriPharm0623Flow
0.005112
/
MGD
/
Jan 2023
Week 4
0.005578
/
MGD
/
Feb 2023
Week 4
0.002601
/
MGD
/
Mar 2023
Week 4
0.003273
/
MGD
/
Apr 2023
Week 4
0.003725
/
MGD
/
May 2023
Week 4
0.005347
/
MGD
/
Jun 2023
Week 4
0.005112
/
MGD
/
Jan 2023
Average
0.005578
/
MGD
/
Feb 2023
Average
0.002601
/
MGD
/
Mar 2023
Average
0.003273
/ 0.008
MGD
/
Apr 2023
Average
0.003725
/ 0.008
MGD
/
May 2023
Average
0.005347
/ 0.008
MGD
/
Jun 2023
Average
0.005112
/ 0.008
MGD
/
2023
Quarter 1
0.00409
/
MGD
/
2023
Quarter 1
0.003273
/
MGD
/
2023
Quarter 1
0.00409
/
MGD
/
2023
Quarter 1
0.003273
/
MGD
/
2023
Quarter 2
0.004728
/
MGD
/
2023
1st 6 Months (Avg) 0.004273
/
MGD
/
2023
1st 6 ...(Max)
0.005578
/
MGD
/
2023
lst6... (Min)
0.002601
/
MGD
/
2023
1st 6 ...(Count)
6
Sample Count: 6
Months Sampled
: 6
Weeks Sampled:
6
Quarters Sampled :
5
# Over Daily C :
0 0.00
# Over Mo Avg C:
0 0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0 0.00
# Over Wk Avg C TRC: 0
0.00
# Over Qt Avg C TRC: 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0 0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC :
0 0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass /Limit
BOD
01/31/2023
P TriPharm013123POT
69.5
/ mg/L
2.143 /
Ibs/day
W
02/21/2023
S TriPhann022123Self
36
/ mg/L
/
Jan 2023
Week 4
69.5
/ mg/L
2.143 /
Ibs/day
Feb 2023
Week 3
36
/ mg/L
/
Jan 2023
Average
69.5
/ mg/L
1143 /
lbs/day
Feb 2023
Average
36
/ mg/L
/
2023
Quarter 1
52.8
/ mg/L
2.143 /
lbs/day
Saturday, February 24, 2024 9:18:36PM * Indicates Violation ** Indicates TRC Violation Page 2 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
BOD
2023
2023
2023
2023
1st 6 Months (Avg)
1st 6 ...(Max)
lst6... (Min)
1st 6 ...(Count)
52.8
69.5
36
2
/
/
/
/
mg/L
mg/L
mg/L
2.143 /
2.143 /
/
1 /
lbs/day
lbs/day
Sample Date
SamplelD
Result/Limit
Mass/Limit
Cadmium
01/31/2023
P TriPhann013123POT
<
0.00008
/
mg/L
<
0.000002 /
lbs/day
W
02/21/2023
S TriPharm022123Self
<
0.00008
/
mg/L
<
/
Jan 2023
Week 4
<
0.00008
/
mg/L
<
0.000002 /
lbs/day
Feb 2023
Week 3
<
0.00008
/
mg/L
<
/
Jan 2023
Average
<
0.00008
/
mg/L
<
0.000002 /
lbs/day
Feb 2023
Average
<
0.00008
/
mg/L
<
/
2023
Quarter 1
<
0.00008
/
mg/L
<
0.000002 /
lbs/day
2023
1st 6 Months (Avg)
<
0.00008
/
mg/L
<
0.000002 /
lbs/day
2023
1st 6 ...(Max)
<
0.00008
/
mg/L
<
0.000002 /
Ibs/day
2023
Ist 6 ...(Min)
<
0.00008
/
mg/L
<
/
2023
1st 6 ...(Count)
2
/
1 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
01/31/2023
P TriPharm013123POT
20.4
/ mg/L
0.6292 /
Ibs/day
W
02/21/2023
S TriPhann022123Self
1600
/ mg/L
/
Jan 2023
Week 4
20.4
/ mg/L
0.6292 /
lbs/day
Feb 2023
Week 3
1600
/ mg/L
/
Jan 2023
Average
20.4
/ mg/L
0.6292 /
Ibs/day
Feb 2023
Average
1600
/ mg/L
/
2023
Quarter 1
810.2
/ mg/L
0.6292 /
lbs/day
2023
1st 6 Months (Avg)
810.2
/ mg/L
0.6292 /
lbs/day
2023
1st 6 ...(Max)
1600
/ mg/L
0.6292 /
lbs/day
2023
lst6... (Min)
20.4
/ mg/L
/
2023
1st 6 ...(Count)
2
/
1 /
Sample Date SamplelD Result/Limit Mass/Limit
COD
01/31/2023 P TriPharm013123POT <
7.5
/
mg/L <
0.23 / Ibs/day
W
02/21/2023 S TriPharm022123Self
41
/
mg/L
/
Jan 2023 Week 4 <
7.5
/
mg/L <
0.23 / lbs/day
Feb 2023 Week 3
41
/
mg/L
/
Saturday, February 24, 2024 9:18:36PM
* Indicates Violation
** Indicates TRC Violation
Page 3 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
COD
Jan 2023
Average
<
7.5
/
mg/L
<
0.23 /
Ibs/day
Feb 2023
Average
41
/
mg/L
/
2023
Quarter 1
<
24.3
/
mg/L
<
0.23 /
lbs/day
2023
1st 6 Months (Avg)
<
24.3
/
mg/L
<
0.23 /
Ibs/day
2023
lst 6 ...(Max)
41
/
mg/L
0.23 /
Ibs/day
2023
lst6... (Min)
<
7.5
/
mg/L
<
/
2023
1st 6 ...(Count)
2
/
1 /
Sample Date
SamplelD
Result /Limit
Mass /Limit
Ethyl acetate
01/31/2023 P
TriPharm013123POT
<
0.003
/ 5.44
mg/L
<
0.0001 /
lbs/day
W
02/21/2023 S
TriPharm022123Self
<
0.05
/ 5.44
mg/L
<
/
Jan 2023
Week 4
<
0.003
/
mg/L
<
0.0001 /
Ibs/day
Feb 2023
Week 3
<
0.05
/
mg/L
<
/
Jan 2023
Average
<
0.003
/ 2,15
mg/L
<
0.0001 /
lbs/day
Feb 2023
Average
<
0.05
/ 2.15
mg/L
<
/
2023
Quarter 1
<
0.026
/
mg/L
<
0.0001 /
lbs/day
2023
1st 6 Months (Avg)
<
0.026
/
mg/L
<
0.0001 /
Ibs/day
2023
1st 6 ...(Max)
<
0.05
/
mg/L
<
0.0001 /
Ibs/day
2023
1st 6 ...(Min)
<
0.003
/
mg/L
<
/
2023
1st 6 ...(Count)
2
/
1 /
Sample Count : 2
Months Sampled:
2
Weeks Sampled:
2 Quarters Sampled :
1
# Over Daily C :
0 0.00 # Over Mo Avg C :
0 0.00
# Over Wk Avg C :
0
0.00 # Over Qt Avg C :
0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC
:
0 0.00
# Over Wk Avg C TRC :
0
0.00 # Over Qt Avg C TRC
: 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0 0.00
# Over Wk Avg M :
0
0.00 # Over Qtr Avg M :
0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC
:
0 0.00
# Over Wk Avg M TRC:
0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
Fluoride
01/31/2023 P
TriPharm013123POT
0.96
/
mg/L
0.0296 /
lbs/day
W
02/21/2023 S
TriPharrn022123Self
0.51
/
mg/L
/
Jan 2023
Week 4
0.96
/
mg/L
0.0296 /
Ibs/day
Feb 2023
Week 3
0.51
/
mg/L
/
Jan 2023
Average
0.96
/
mg/L
0.0296 /
lbs/day
Feb 2023
Average
0.51
/
mg/L
/
2023
Quarter 1
0.74
/
mg/L
0.0296 /
Ibs/day
2023
1st 6 Months (Avg)
0.74
/
mg/L
0.0296 /
lbs/day
Saturday, February 24, 2024 9:18:36PM * Indicates Violation ** Indicates TRC Violation Page 4 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
Fluoride
2023
Ist 6 ...(Max)
0.96
/
mg/L
0.0296 /
lbs/day
2023
1st 6 ...(Min)
0.51
/
mg/L
/
2023
Ist 6 ...(Count)
2
/
1 /
Sample Date
SamplelD
Result/Limit
Mass/Limit
Isopropyl acetate
01/31/2023 P
TriPharm013123POT
<
0.003
/ 5.44
mg/L
<
0.0001 /
lbs/day
W
02/21/2023 S
TriPhann022123Self
<
0.003
/ 5.44
mg/L
<
/
Jan 2023
Week 4
<
0.003
/
mg/L
<
0.0001 /
lbs/day
Feb 2023
Week 3
<
0.003
/
mg/L
<
/
Jan 2023
Average
<
0.003
/ 2.15
mg/L
<
0.0001 /
Ibs/day
Feb 2023
Average
<
0.003
/ 2.15
mg/L
<
/
2023
Quarter 1
<
0.003
/
mg/L
<
0.0001 /
lbs/day
2023
1st 6 Months (Avg)
<
0.003
/
mg/L
<
0.0001 /
lbs/day
2023
Ist 6 ...(Max)
<
0.003
/
mg/L
<
0.0001 /
lbs/day
2023
1st 6 ...(Min)
<
0.003
/
mg/L
<
/
2023
Ist 6 ...(Count)
2
/
1 /
Sample Count: 2
Months Sampled:
2
Weeks Sampled:
2 Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C:
0 0.00
# Over Wk Avg C :
0
0.00 # Over Qt Avg C :
0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0 0.00
# Over Wk Avg C TRC :
0
0.00 # Over Qt Avg C TRC
: 0
0.00
# Over Daily M:
0 0.00 # Over Mo Avg M :
0 0.00
# Over Wk Avg M :
0
0.00 # Over Qtr Avg M :
0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC :
0 0.00
# Over Wk Avg M TRC :
0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
Mercury - LL
01/30/2023 P
TriPharm013023POT
<
0.000001
/ 0.000142
mg/L
<
/
WHg
02/21/2023 S
TriPharm022123SelfH
<
0.000001
/ 0.000142
mg/L
<
/
g
Jan 2023
Week 4
<
0.000001
/
mg/L
<
/
Feb 2023
Week 3
<
0.000001
/
mg/L
<
/
Jan 2023
Average
<
0.000001
/
mg/L
<
/
Feb 2023
Average
<
0.000001
/
mg/L
<
/
2023
Quarter 1
<
0.000001
/
mg/L
<
/
2023
1st 6 Months (Avg)
<
0.000001
/
mg/L
<
/
2023
Ist 6 ...(Max)
<
0.000001
/
mg/L
<
/
2023
Ist 6 ...(Min)
<
0.000001
/
mg/L
<
/
2023
Ist 6 ...(Count)
2
Saturday, February 24, 2024 9:18:36PM * Indicates Violation ** Indicates TRC Violation Page 5 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
2
Months Sampled :
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
01/31/2023 P
TriPharm013123POT <
0.003
/ 0.78
mg/L
<
0.000077 /
lbs/day
W
02/21/2023 S
TriPhann022123Self <
0.025
/ 0.78
mg/L
<
/
Jan 2023
Week 4
<
0.003
/
mg/L
<
0.000077 /
Ibs/day
Feb 2023
Week 3
<
0.025
/
mg/L
<
/
Jan 2023
Average
<
0.003
/ 0.18
mg/L
<
0.000077 /
lbs/day
Feb 2023
Average
<
0.025
/ 0.18
mg/L
<
/
2023
Quarter 1
<
0.014
/
mg/L
<
0.000077 /
lbs/day
2023
1st 6 Months (Avg) <
0.014
/
mg/L
<
0.000077 /
Ibs/day
2023
lst6... (Max)
<
0.025
/
mg/L
<
0.000077 /
Ibs/day
2023
lst6... (Min)
<
0.003
/
mg/L
<
/
2023
1st 6 ...(Count)
2
/
1 /
Sample Count
: 2
Months Sampled
:
2
Weeks Sampled:
2 Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C:
0
0.00
# Over Wk Avg C :
0
0.00 # Over Qt Avg C :
0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00 # Over Qt Avg C TRC
: 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00 # Over Qtr Avg M :
0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass /Limit
Molybdenum
01/31/2023 P
TriPharm013123POT
<
0.001
/ mg/L
<
0 /
Ibs/day
W
02/21/2023 S
TriPharm022123Self
<
0.001
/ mg/L
<
/
Jan 2023
Week 4
<
0.001
/ mg/L
<
0 /
Ibs/day
Feb 2023
Week 3
<
0.001
/ mg/L
<
/
Jan 2023
Average
<
0.001
/ mg/L
<
0 /
lbs/day
Feb 2023
Average
<
0.001
/ mg/L
<
/
2023
Quarter 1
<
0.001
/ mg/L
<
0 /
lbs/day
2023
1st 6 Months (Avg)
<
0.001
/ mg/L
<
0.0000 /
lbs/day
2023
1st 6 ...(Max)
<
0.001
/ mg/L
<
0.0000 /
Ibs/day
2023
1st 6 ...(Min)
<
0.001
/ mg/L
<
/
2023
1st 6 ...(Count)
2
/
1 /
Saturday, February 24, 2024 9:18:36PM * Indicates Violation ** Indicates TRC Violation Page 6 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result/Limit Mass/Limit
n-Amyl acetate
01/31/2023 P
TriPharm013123POT <
0.003
/ 5.44
mg/L
<
0.0001 / lbs/day
W
02/21/2023 S
TriPhartn022123Self <
0.05
/ 5.44
mg/L
<
/
Jan 2023
Week 4
<
0.003
/
mg/L
<
0.0001 / lbs/day
Feb 2023
Week 3
<
0.05
/
mg/L
<
/
Jan 2023
Average
<
0.003
/ 2.15
mg/L
<
0.0001 / Ibs/day
Feb 2023
Average
<
0.05
/ 2,15
mg/L
<
/
2023
Quarter 1
<
0.026
/
mg/L
<
0.0001 / Ibs/day
2023
1st 6 Months (Avg) <
0.026
/
mg/L
<
0.0001 / Ibs/day
2023
1st 6 ...(Max)
<
0.05
/
mg/L
<
0.0001 / Ibs/day
2023
1st 6 ...(Min)
<
0.003
/
mg/L
<
/
2023
1st 6 ...(Count)
2
/
1 /
Sample Count: 2
Months Sampled:
2
Weeks Sampled:
2 Quarters Sampled :
1
# Over Daily C :
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00 # Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC
:
0
0.00
# Over Wk Avg C TRC :
0
0.00 # Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00 # Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SampleID
Result/Limit
Mass /Limit
Nitrate -Nitrite
01/31/2023 P
TriPharm013123POT
4.4
/ mg/L
0.135 /
Ibs/day
W
02/21/2023 S
TriPharm022123Self
3.6
/ mg/L
/
Jan 2023
Week 4
4.4
/ mg/L
0.135 /
lbs/day
Feb 2023
Week 3
3.6
/ mg/L
/
Jan 2023
Average
4.4
/ mg/L
0.135 /
Ibs/day
Feb 2023
Average
3.6
/ mg/L
/
2023
Quarter 1
4
/ mg/L
0.135 /
Ibs/day
2023
1st 6 Months (Avg)
4.0
/ mg/L
0.135 /
Ibs/day
2023
1st 6 ...(Max)
4.4
/ mg/L
0.135 /
Ibs/day
2023
1st 6 ...(Min)
3.6
/ mg/L
/
2023
1st 6 ...(Count)
2
/
1 /
Sample Date SampleID Result/Limit Mass/Limit
Nitrogen, Total
01/31/2023 P TriPharm013123POT
W
02/21/2023 S TriPhann022123Self
Jan 2023 Week 4
Feb 2023 Week 3
5.07 / mg/L 0.156 / lbs/day
4.77 / mg/L /
5.07 / mg/L 0.156 / Ibs/day
4.77 / mg/L /
Saturday, February 24, 2024 9:18:36PM * Indicates Violation ** Indicates TRC Violation Page 7 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
Nitrogen, Total
Jan 2023
Average
5.07
/
mg/L
0.156 / Ibs/day
Feb 2023
Average
4.77
/
mg/L
/
2023
Quarter 1
4.92
/
mg/L
0.156 / lbs/day
2023
1st 6 Months (Avg)
4.92
/
mg/L
0.156 / Ibs/day
2023
1st 6 ...(Max)
5.07
/
mg/L
0.156 / Ibs/day
2023
lst6... (Min)
4.77
/
mg/L
/
2023
Ist 6 ...(Count)
2
/
1 /
Sample Date
SamplelD
Result /Limit
Mass /Limit
pH
01/31/2023 P
TriPharm013123POT
7.9
/ 5.5 - 10.5
SU
/
W
02/21/2023 S
TriPharm022123Self
8
/ 5.5 - 10.5
SU
/
Jan 2023
Week 4
7.9
/
SU
/
Feb 2023
Week 3
8
/
SU
/
Jan 2023
Average
7.9
/
SU
/
Feb 2023
Average
8
/
SU
/
2023
Quarter 1
7.95
/
SU
/
2023
1st 6 Months (Avg)
7.95
/
SU
/
2023
1st 6 ...(Max)
8
/
SU
/
2023
1st 6 ...(Min)
7.9
/
SU
/
2023
1st 6 ...(Count)
2
Sample Count : 2 Months Sampled:
2
Weeks Sampled:
2 Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C:
0 0.00
# Over Wk Avg C : 0
0.00 # Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0 0.00
# Over Wk Avg C TRC : 0
0.00 # Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0 0.00
# Over Wk Avg M : 0
0.00 # Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0 0.00
# Over Wk Avg M TRC : 0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
Temperature
01/31/2023 P
TriPharm013123POT
18
/ 66
°C
/
W
02/21/2023 S
TriPhartn022123Self
28
/ 66
oc
/
Jan 2023
Week 4
18
/
°C
/
Feb 2023
Week 3
28
/
°C
/
Jan 2023
Average
18
/
°C
/
Feb 2023
Average
28
/
°C
/
2023
Quarter 1
23
/
°C
/
2023
1st 6 Months (Avg)
23
/
°C
/
Saturday, February 24, 2024 9:18:36PM * Indicates Violation ** Indicates TRC Violation Page 8 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
2023
1st 6 ...(Max)
28 /
°C
/
2023
1st 6 ...(Min)
18 /
°C
/
2023
lst6...
(Count)
2
Sample Count:
2
Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled:
1
# Over Daily C :
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
01/31/2023
P TriPharm013123POT
0.7
/ mg/L
0.022 /
lbs/day
W
02/21/2023
S TriPharm022123Self
1.22
/ mg/L
/
Jan 2023
Week 4
0.7
/ mg/L
0.022 /
lbs/day
Feb 2023
Week 3
1.22
/ mg/L
/
Jan 2023
Average
0.7
/ mg/L
0.022 /
lbs/day
Feb 2023
Average
1.22
/ mg/L
/
2023
Quarter 1
0.96
/ mg/L
0.022 /
Ibs/day
2023
1st 6 Months (Avg)
0.96
/ mg/L
0.022 /
lbs/day
2023
1st 6 ...(Max)
1.22
/ mg/L
0.022 /
Ibs/day
2023
1st 6 ...(Min)
0.7
/ mg/L
/
2023
1st 6 ...(Count)
2
/
1 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
01/31/2023 P
TriPharm013123POT
0.429
/ mg/L
0.0132 /
lbs/day
W
02/21/2023 S
TriPharm022123Self
0.304
/ mg/L
/
Jan 2023
Week 4
0.429
/ mg/L
0.0132 /
lbs/day
Feb 2023
Week 3
0.304
/ mg/L
/
Jan 2023
Average
0.429
/ mg/L
0.0132 /
Ibs/day
Feb 2023
Average
0.304
/ mg/L
/
2023
Quarter 1
0.367
/ mg/L
0.0132 /
Ibs/day
2023
1st 6 Months (Avg)
0.367
/ mg/L
0.0132 /
Ibs/day
2023
1st 6 ...(Max)
0.429
/ mg/L
0.0132 /
lbs/day
2023
lst6... (Min)
0.304
/ mg/L
/
2023
1st 6 ...(Count)
2
/
1 /
Saturday, February 24, 2024 9:18:36PM * Indicates Violation ** Indicates TRC Violation Page 9 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
TSS
01/31/2023
P TriPham1013123POT
<
1.3
/ mg/L
<
0.038552 /
Ibs/day
W
02/21/2023
S TriPhartn022123Self
<
1.3
/ mg/L
<
/
Jan 2023
Week 4
<
1.3
/ mg/L
<
0.038552 /
lbs/day
Feb 2023
Week 3
<
1.3
/ mg/L
<
/
Jan 2023
Average
<
1.3
/ mg/L
<
0.038552 /
Ibs/day
Feb 2023
Average
<
1.3
/ mg/L
<
/
2023
Quarter 1
<
1.3
/ mg/L
<
0.038552 /
Ibs/day
2023
1st 6 Months (Avg)
<
1.3
/ mg/L
<
0.038552 /
Ibs/day
2023
1st 6 ...(Max)
<
1.3
/ mg/L
<
0.038552 /
Ibs/day
2023
1st 6 ...(Min)
<
1.3
/ mg/L
<
/
2023
1st 6 ...(Count)
2
/
1 /
Sample Date SamplelD Result/Limit Mass /Limit
VOC
01/31/2023
P TriPharm013123POT
0.341
/ mg/L
/
W
02/21/2023
S TriPharm022123Self
0.317
/ mg/L
/
Jan 2023
Week 4
0.341
/ mg/L
/
Feb 2023
Week 3
0.317
/ mg/L
/
Jan 2023
Average
0.341
/ mg/L
/
Feb 2023
Average
0.317
/ mg/L
/
2023
Quarter 1
0.329
/ mg/L
/
2023
1st 6 Months (Avg)
0.329
/ mg/L
/
2023
1st 6 ...(Max)
0.341
/ mg/L
/
2023
1st 6 ...(Min)
0.317
/ mg/L
/
2023
1st 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
Zinc
01/31/2023
P TriPharm013123POT
0.084
/
mg/L
0.002591
/
Ibs/day
W
02/21/2023
S TriPharm022123Self
0.314
/
mg/L
/
Jan 2023
Week 4
0.084
/
mg/L
0.002591
/
Ibs/day
Feb 2023
Week 3
0.314
/
mg/L
/
Jan 2023
Average
0.084
/
mg/L
0.002591
/
Ibs/day
Feb 2023
Average
0.314
/
mg/L
/
2023
Quarter 1
0.199
/
mg/L
0.002591
/
lbs/day
2023
1st 6 Months (Avg)
0.199
/
mg/L
0.002591
/
lbs/day
2023
1st 6 ...(Max)
0.314
/
mg/L
0.002591
/
lbs/day
2023
1st 6 ...(Min)
0.084
/
mg/L
/
2023
1st 6 ...(Count)
2
/
1
/
Saturday, February 24, 2024 9:18:36PM * Indicates Violation ** Indicates TRC Violation Page 10 of 10

United Therapeutics Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
01/24/2023
P UTP1012423POTW
3.3
/ mg/L
/
02/07/2023
S UTP1020723Self
3.7
/ mg/L
1.1968 /
lbs/day
Jan 2023
Week 4
3.3
/ mg/L
/
Feb 2023
Week 1
3.7
/ mg/L
1.1968 /
Ibs/day
Jan 2023
Average
3.3
/ mg/L
/
Feb 2023
Average
3.7
/ mg/L
1.1968 /
Ibs/day
2023
Quarter 1
3.5
/ mg/L
1.1968 /
Ibs/day
2023
1st 6 Months (Avg)
3.5
/ mg/L
1.1968 /
Ibs/day
2023
1st 6 ...(Max)
3.7
/ mg/L
1.1968 /
Ibs/day
2023
1st 6 ...(Min)
3.3
/ mg/L
/
2023
lst6... (Count)
2
/
1 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2023
S
UT0123F1ow
0.025
/
MGD /
02/28/2023
S
UT0223F1ow
0.026
/
MGD /
03/31/2023
S
UT0323F1ow
0.043
/
MGD /
04/30/2023
S
UT0423F1ow
0.034
/
MGD /
05/31/2023
S
UT0523F1ow
0.025
/
MGD /
06/30/2023
S
UT0623F1oiw
0.03
/
MGD /
Jan 2023
Week 4
0.025
/
MGD /
Feb 2023
Week 4
0.026
/
MGD /
Mar 2023
Week 4
0.043
/
MGD /
Apr 2023
Week 4
0.034
/
MGD /
May 2023
Week 4
0.025
/
MGD /
Jun 2023
Week 4
0.03
/
MGD /
Jan 2023
Average
0.025
/ 0.060
MGD /
Feb 2023
Average
0.026
/ 0.060
MGD /
Mar 2023
Average
0.043
/ 0.060
MGD /
Apr 2023
Average
0.034
/ 0.060
MGD /
May 2023
Average
0.025
/ 0.060
MGD /
Jun 2023
Average
0.03
/ 0.060
MGD /
2023
Quarter 1
0.031333
/
MGD /
2023
Quarter 2
0.029667
/
MGD /
2023
1st 6 Months (Avg)
0.0305
/
MGD /
2023
1st 6 ...(Max)
0.043
/
MGD /
2023
1st 6 ...(Min)
0.025
/
MGD /
2023
1st 6 ...(Count)
6
Sunday, February 25, 2024 5:55:38PM * Indicates Violation ** Indicates TRC Violation Page 1 of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
6
Months Sampled:
6
Weeks Sampled:
6
Quarters Sampled :
2
# Over Daily C :
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0,00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Samplc Date
SamplelD
Result/Limit
Mass/Limit
BOD
01/24/2023
P
UTP1012423POTW
216
/
mg/L
/
02/07/2023
S
UTP 1020723 Self
119
/
mg/L
38.493 /
Ibs/day
Jan 2023
Week 4
216
/
mg/L
/
Feb 2023
Week 1
119
/
mg/L
38.493 /
lbs/day
Jan 2023
Average
216
/
mg/L
/
Feb 2023
Average
119
/
mg/L
38.493 /
Ibs/day
2023
Quarter 1
167.5
/
mg/L
38.493 /
Ibs/day
2023
1st 6 Months (Avg)
167.5
/
mg/L
38.493 /
Ibs/day
2023
1st6... (Max)
216
/
mg/L
38.493 /
Ibs/day
2023
1st 6 ...(Min)
119
/
mg/L
/
2023
1st 6 ...(Count)
2
/
1 /
Sample Date
SamplelD
Result/Limit
Mass/Limit
Cadmium
02/07/2023
S
UTP1020723Sclf
<
0.00008
/
mg/L
<
0.000024 /
lbs/day
Feb 2023
Week 1
<
0.00008
/
mg/L
<
0.000024 /
lbs/day
Feb 2023
Average
<
0.00008
/
mg/L
<
0.000024 /
lbs/day
2023
Quarter I
<
0.00008
/
mg/L
<
0.000024 /
lbs/day
2023
1st 6 Months (Avg)
<
0.00008
/
mg/L
<
0.000024 /
Ibs/day
2023
1st 6 ...(Max)
<
0.00008
/
mg/L
<
0.000024 /
Ibs/day
2023
1st 6 ...(Min)
<
0.00008
/
mg/L
<
0.000024 /
Ibs/day
2023
1st 6 ...(Count)
1
/
I /
Sample Date
SamplelD
Result/Limit
Mass/Limit
Chloride
01/24/2023
P
UTP1012423POTW
65
/
mg/L
1
02/07/2023
S
UTP1020723Self
132
/
mg/L
42.6976 /
lbs/day
Jan 2023
Week 4
65
/
mg/L
/
Feb 2023
Week 1
132
/
mg/L
42.6976 /
lbs/day
Jan 2023
Average
65
/
mg/L
/
Feb 2023
Average
132
/
mg/L
42.6976 /
Ibs/day
2023
Quarter 1
98.5
/
mg/L
42.6976 /
Ibs/day
2023
1st 6 Months (Avg)
98.5
/
mg/L
42.6976 /
Ibs/day
Sunday, February 25, 2024 5:55:38PM * Indicates Violation ** Indicates TRC Violation Page 2 of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
Chloride
2023
1st 6 ...(Max)
132 /
mg/L
42.6976 /
Ibs/day
2023
1st 6 ...(Min)
65 /
mg/L
/
2023
1st 6 ...(Count)
2 /
1 /
Sample Date
SamplelD
Result/Limit
Mass/Limit
COD
01/24/2023
P UTP1012423POTW
333 /
mg/L
/
02/07/2023
S UTP1020723Self
317 /
mg/L
102.54 /
lbs/day
Jan 2023
Week 4
333 /
mg/L
/
Feb 2023
Week 1
317 /
mg/L
102.54 /
Ibs/day
Jan 2023
Average
333 /
mg/L
/
Feb 2023
Average
317 /
mg/L
102.54 /
Ibs/day
2023
Quarter 1
325 /
mg/L
102.54 /
lbs/day
2023
1st 6 Months (Avg)
325 /
mg/L
102.54 /
lbs/day
2023
1st 6 ...(Max)
333 /
mg/L
102.54 /
lbs/day
2023
lst 6 ...(Min)
317 /
mg/L
/
2023
lst6... (Count)
2 /
1 /
Sample Date
SamplelD
Result/Limit
Mass/Limit
Cyanide
01/24/2023
P UTP1012423POTW
<
0.003
/
mg/L
<
/
02/07/2023
S UTP1020723Self
<
0.003
/
mg/L
<
0.000809 /
Ibs/day
Jan 2023
Week 4
<
0.003
/
mg/L
<
/
Feb 2023
Week 1
<
0.003
/
mg/L
<
0.000809 /
Ibs/day
Jan 2023
Average
<
0.003
/
mg/L
<
/
Feb 2023
Average
<
0.003
/
mg/L
<
0.000809 /
lbs/day
2023
Quarter 1
<
0.003
/
mg/L
<
0.000809 /
Ibs/day
2023
1st 6 Months (Avg)
<
0.003
/
mg/L
<
0.000809 /
Ibs/day
2023
lst6... (Max)
<
0.003
/
mg/L
<
0.000809 /
Ibs/day
2023
lst6... (Min)
<
0.003
/
mg/L
<
/
2023
1st 6 ...(Count)
2
/
1 /
Sample Date
SamplelD
Result/Limit
Mass /Limit
Fluoride
02/07/2023
S UTP1020723Self
0.57
/
mg/L
0.1844 /
Ibs/day
Feb 2023
Week 1
0.57
/
mg/L
0.1844 /
lbs/day
Feb 2023
Average
0.57
/
mg/L
0.1844 /
lbs/day
2023
Quarter 1
0.57
/
mg/L
0.1844 /
lbs/day
2023
1st 6 Months (Avg)
0.57
/
mg/L
0.1844 /
lbs/day
2023
1st 6 ...(Max)
0.57
/
mg/L
0.1844 /
Ibs/day
2023
1st 6 ...(Min)
0.57
/
mg/L
0.1844 /
Ibs/day
Sunday, February 25, 2024 5:55:38PM * Indicates Violation ** Indicates TRC Violation Page 3 of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
Fluoride
2023
1st 6 ...(Count)
Sample Date
SamplelD
Result/Limit
Mass/Limit
Mercury - LL
01/24/2023 P
UTP1012423POTWHg
0.000003
/ 0.000142
mg/L
/
02/07/2023 S
UTP1020723Self
0.00002
/ 0.000142
mg/L
/
Jan 2023
Week 4
0.000003
/
mg/L
/
Feb 2023
Week 1
0.00002
/
mg/L
/
Jan 2023
Average
0.000003
/
mg/L
/
Feb 2023
Average
0.00002
/
mg/L
/
2023
Quarter 1
0.000011
/
mg/L
/
2023
1st 6 Months (Avg)
0.000011
/
mg/L
/
2023
1st 6 ...(Max)
0.000020
/
mg/L
/
2023
1st 6 ...(Min)
0.000003
/
mg/L
/
2023
1st 6 ...(Count)
2
/
/
Sample Count : 2 Months Sampled
: 2
Weeks Sampled:
2 Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0 0.00
# Over Wk Avg C :
0
0.00 # Over Qt Avg C :
0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0 0.00
# Over Wk Avg C TRC :
0
0.00 # Over Qt Avg C TRC
: 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0 0.00
# Over Wk Avg M :
0
0.00 # Over Qtr Avg M :
0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC :
0 0.00
# Over Wk Avg M TRC :
0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Lhnit
Molybdenum
02/07/2023 S
UTP1020723Self <
0.001
/
mg/L
<
0.0003 /
lbs/day
Feb 2023
Week 1 <
0.001
/
mg/L
<
0.0003 /
lbs/day
Feb 2023
Average <
0.001
/
mg/L
<
0.0003 /
lbs/day
2023
Quarter 1 <
0.001
/
mg/L
<
0.0003 /
Ibs/day
2023
1st 6 Months (Avg) <
0.001
/
mg/L
<
0.0003 /
Ibs/day
2023
lst6... (Max) <
0.001
/
mg/L
<
0.0003 /
Ibs/day
2023
1st 6 ...(Min) <
0.001
/
mg/L
<
0.0003 /
Ibs/day
2023
1st 6 ...(Count)
1
/
1 /
Sample Date
SampleID
Result/Limit
Mass/Limit
Nickel
02/07/2023 S
UTP1020723Sclf
0.0047
/
mg/L
0.00152 /
lbs/day
Feb 2023
Week 1
0.0047
/
mg/L
0.00152 /
lbs/day
Feb 2023
Average
0.0047
/
mg/L
0.00152 /
lbs/day
2023
Quarter 1
0.0047
/
mg/L
0.00152 /
lbs/day
Sunday, February 25, 2024 5:55:38PM * Indicates Violation ** Indicates TRC Violation Page 4 of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleLD Result/Limit Mass/Limit
Nickel
2023
2023
2023
2023
1st 6 Months (Avg)
1st 6 ...(Max)
lst6... (Min)
1st 6 ...(Count)
0.0047
0.0047
0.0047
1
/
/
/
/
mg/L
mg/L
mg/L
0.001520 /
0.001520 /
0.001520 /
1 /
lbs/day
lbs/day
lbs/day
Sample Date
SampleLD
Result/Limit
Mass/Limit
Nitrate -Nitrite
01/24/2023 P
UTP1012423POTW
0.7
/
mg/L
/
02/07/2023 S
UTP1020723Self
0.7
/
mg/L
0.239 /
Ibs/day
Jan 2023
Week 4
0.7
/
mg/L
/
Feb 2023
Week 1
0.7
/
mg/L
0.239 /
Ibs/day
Jan 2023
Average
0.7
/
mg/L
/
Feb 2023
Average
0.7
/
mg/L
0.239 /
lbs/day
2023
Quarter 1
0.7
/
mg/L
0.239 /
lbs/day
2023
1st 6 Months (Avg)
0.7
/
mg/L
0.239 /
lbs/day
2023
lst 6 ...(Max)
0.7
/
mg/L
0.239 /
lbs/day
2023
1st 6 ...(Min)
0.7
/
mg/L
/
2023
1st 6 ...(Count)
2
/
1 /
Sample Date SampleLD Result/Limit Mass / Limit
Nitrogen, Total
01/24/2023 P
UTP1012423POTW
30.9
/ mg/L
/
02/07/2023 S
UTP1020723Self
25.5
/ mg/L
8.248 /
Ibs/day
Feb 2023
Week 1
25.5
/ mg/L
8.248 /
Ibs/day
Jan 2023
Week 4
30.9
/ mg/L
/
Jan 2023
Average
30.9
/ mg/L
/
Feb 2023
Average
25.5
/ mg/L
8.248 /
Ibs/day
2023
Quarter 1
28.2
/ mg/L
8.248 /
Ibs/day
2023
1st 6 Months (Avg)
28.2
/ mg/L
8.248 /
Ibs/day
2023
lst6... (Max)
30.9
/ mg/L
8.248 /
Ibs/day
2023
1st 6 ...(Min)
25.5
/ mg/L
/
2023
1st 6 ...(Count)
2
/
1 /
Sample Date SampleLD Result/Limit Mass/Limit
Oil & Grease, Total
01/24/2023 P
UTP1012423POTW
14
/ 200
mg/L /
02/07/2023 S
UTP1020723Self <
2.5
/ 200
mg/L < /
Jan 2023
Week 4
14
/
mg/L /
Feb 2023
Week 1 <
2.5
/
mg/L < /
Jan 2023
Average
14
/
mg/L /
Feb 2023
Average <
2.5
/
mg/L < /
Sunday, February 25, 2024 5:55:38PM * Indicates Violation ** Indicates TRC Violation Page 5 of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Oil & Grease, Total
2023
Quarter 1
<
8.25 /
mg/L <
/
2023
1st 6 Months (Avg) <
8.25 /
mg/L <
/
2023
lst6... (Max)
14 /
mg/L
/
2023
1st 6 ...(Min)
<
2.5 /
mg/L <
/
2023
1st 6 ...(Count)
2
Sample Count: 2
Months Sampled:
2
Weeks Sampled :
2
Quarters Sampled :
I
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
01/24/2023 P
UTP1012423POTW
9.3
/ 5.5 - 10.0
SU
/
02/07/2023 S
UTP1020723Se1f
7.6
/ 5.5 - 10.0
SU
/
Jan 2023
Week 4
9.3
/
SU
/
Feb 2023
Week 1
7.6
/
SU
/
Jan 2023
Average
9.3
/
SU
/
Feb 2023
Average
7.6
/
SU
/
2023
Quarter 1
8.45
/
SU
/
2023
1st 6 Months (Avg)
8.45
/
SU
/
2023
1st 6 ...(Max)
9.3
/
SU
/
2023
lst 6 ...(Min)
7.6
/
SU
/
2023
1st 6 ...(Count)
2
Sample Count: 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
01/24/2023 P UTP1012423POTW
02/07/2023 S UTP 1020723 Self
Jan 2023 Week 4
15 / 66 °C /
17 / 66 °C /
15 / °C /
Sunday, February 25, 2024 5:55:38PM * Indicates Violation ** Indicates TRC Violation Page 6 of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
Feb 2023
Week 1
17
/
°C
/
Jan 2023
Average
15
/
°C
/
Feb 2023
Average
17
/
°C
/
2023
Quarter 1
16
/
°C
/
2023
1st 6 Months (Avg)
16
/
°C
/
2023
lst6... (Max)
17
/
°C
/
2023
1st 6 ...(Min)
15
/
°C
/
2023
1st 6 ...(Count)
2
Sample Count: 2
Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C:
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass /Limit
TKN
01/24/2023
P UTP1012423POTW
30.2
/ mg/L
/
02/07/2023
S UTP1020723Self
24.8
/ mg/L
8.022 /
Ibs/day
Jan 2023
Week 4
30.2
/ mg/L
/
Feb 2023
Week 1
24.8
/ mg/L
8.022 /
lbs/day
Jan 2023
Average
30.2
/ mg/L
/
Feb 2023
Average
24.8
/ mg/L
8.022 /
lbs/day
2023
Quarter 1
27.5
/ mg/L
8.022 /
lbs/day
2023
1st 6 Months (Avg)
27.5
/ mg/L
8.022 /
Ibs/day
2023
1st 6 ...(Max)
30.2
/ mg/L
8.022 /
Ibs/day
2023
1st 6 ...(Min)
24.8
/ mg/L
/
2023
Ist 6 ... (Count)
2
/
1 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
01/24/2023 P
UTP1012423POTW
02/07/2023 S
UTP1020723Self
Jan 2023
Week 4
Feb 2023
Week 1
Jan 2023
Average
Feb 2023
Average
2023
Quarter 1
2023
1st 6 Months (Avg)
Sunday, February 25, 2024 5:55:38PM
2.82 /
mg/L
/
0.955 /
mg/L
0.3089 /
lbs/day
2.82 /
mg/L
/
0.955 /
mg/L
0.3089 /
Ibs/day
2.82 /
mg/L
/
0.955 /
mg/L
0.3089 /
Ibs/day
1.888 /
mg/L
0.3089 /
Ibs/day
1.888 /
mg/L
0.3089 /
Ibs/day
* Indicates Violation
** Indicates TRC Violation
Page 7 of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
Total Phosphorus
2023
1st 6 ...(Max)
2.82 /
mg/L
0.3089 /
Ibs/day
2023
1st 6 ...(Min)
0.955 /
mg/L
/
2023
1st 6 ...(Count)
2 /
1 /
Sample Date
SamplelD
Result/Limit
Mass/Limit
TSS
01/24/2023 P
UTP1012423POTW
III /
mg/L
/
02/07/2023 S
UTP1020723Self
57 /
mg/L
18.437613 /
lbs/day
Jan 2023
Week 4
1 I 1 /
mg/L
/
Feb 2023
Week 1
57 /
mg/L
18.437613 /
Ibs/day
Jan 2023
Average
III /
mg/L
/
Feb 2023
Average
57 /
mg/L
18.437613 /
Ibs/day
2023
Quarter 1
84 /
mg/L
18.437613 /
lbs/day
2023
1st 6 Months (Avg)
84 /
mg/L
18.4376 /
lbs/day
2023
1st 6 ...(Max)
1I1 /
mg/L
18.437613 /
lbs/day
2023
lst 6 ...(Min)
57 /
mg/L
/
2023
lst6... (Count)
2 /
1 /
Sample Date
SamplelD
Result/Limit
Mass/Limit
VOC
02/07/2023 S
UTP1020723Self
0.233 /
mg/L
/
Feb 2023
Week 1
0.233 /
mg/L
/
Feb 2023
Average
0.233 /
mg/L
/
2023
Quarter 1
0.233 /
mg/L
/
2023
1st 6 Months (Avg)
0.233 /
mg/L
/
2023
1st 6... (Max)
0.233 /
mg/L
/
2023
1st 6 ...(Min)
0.233 /
mg/L
/
2023
1st 6 ...(Count)
1
Sample Date
SamplelD
Result/Limit
Mass /Limit
Zinc
02/07/2023 S
UTP1020723Self
0.779 /
mg/L
0.251981 /
Ibs/day
Feb 2023
Week 1
0.779 /
mg/L
0.251981 /
Ibs/day
Feb 2023
Average
0.779 /
mg/L
0.251981 /
Ibs/day
2023
Quarter 1
0.779 /
mg/L
0.251981 /
Ibs/day
2023
1st 6 Months (Avg)
0.779 /
mg/L
0.251981 /
lbs/day
2023
Ist 6 ...(Max)
0.779 /
mg/L
0.251981 /
Ibs/day
2023
1st 6 ...(Min)
0.779 /
mg/L
0.251981 /
lbs/day
2023
lst 6 ...(Count)
1 /
1 /
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 002
Sunday, February 25, 2024 5:55:38PM * Indicates Violation ** Indicates TRC Violation Page 8 of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 002
SarnpleDate SamplelD Result/Limit Mass/Limit
Acetone
01/27/2023
P UTP2012723POTW
0.051
/ 20.7
mg/L /
02/07/2023
S UTP2020723Self
0.474
/ 20.7
mg/L /
Jan 2023
Week 4
0.051
/
mg/L /
Feb 2023
Week 1
0.474
/
mg/L /
Jan 2023
Average
0.051
/ 8.2
mg/L /
Feb 2023
Average
0.474
/ 8.2
mg/L /
2023
Quarter 1
0.263
/
mg/L /
2023
1st 6 Months (Avg)
0.263
/
mg/L /
2023
1st 6 ...(Max)
0.474
/
mg/L /
2023
1st 6 ...(Min)
0.051
/
mg/L /
2023
1st 6... (Count)
2
Sample Count:
2
Months Sampled :
2
Weeks Sampled :
2
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
01/27/2023
P UTP2012723POTW
<
0.005
/ 20.7
mg/L
< /
02/07/2023
S UTP2020723Sclf
<
0.001
/ 20.7
mg/L
< /
Jan 2023
Week 4
<
0.005
/
mg/L
< /
Feb 2023
Week 1
<
0.001
/
mg/L
< /
Jan 2023
Average
<
0.005
/ 8.2
mg/L
< /
Feb 2023
Average
<
0.001
/ 8.2
mg/L
< /
2023
Quarter 1
<
0.003
/
mg/L
< /
2023
1st 6 Months (Avg)
<
0.003
/
mg/L
< /
2023
1st 6 ...(Max)
<
0.005
/
mg/L
< /
2023
1st 6 ...(Min)
<
0.001
/
mg/L
< /
2023
1st 6 ...(Count)
2
Sample Count :
2
Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sunday, February 25, 2024 5:55:38PM * Indicates Violation ** Indicates TRC Violation Page 1 of 3

United Therapeutics Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 002
SarnpleDate SamplelD Result/Limit Mass/Limit
Isopropyl acetate
01/27/2023 P
UTP2012723POTW <
0.005
/ 20.7
mg/L
<
/
02/07/2023 S
UTP2020723Self <
0.001
/ 20.7
mg/L
<
/
Jan 2023
Week 4 <
0.005
/
mg/L
<
/
Feb 2023
Week 1 <
0.001
/
mg/L
<
/
Jan 2023
Average <
0.005
/ 8.2
mg/L
<
/
Feb 2023
Average <
0.001
/ 8.2
mg/L
<
/
2023
Quarter 1 <
0.003
/
mg/L
<
/
2023
1st 6 Months (Avg) <
0.003
/
mg/L
<
/
2023
1st 6 ...(Max) <
0.005
/
mg/L
<
/
2023
1st 6 ...(Min) <
0.001
/
mg/L
<
/
2023
1st 6... (Count)
2
Sample Count: 2 Months Sampled
:
2
Weeks Sampled :
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
01/27/2023 P
UTP2012723POTW <
0.005
/ 3.0
mg/L
<
/
02/07/2023 S
UTP2020723Sclf
0.005
/ 3.0
mg/L
/
Jan 2023
Week 4 <
0.005
/
mg/L
<
/
Feb 2023
Week 1
0.005
/
mg/L
/
Jan 2023
Average <
0.005
/ 0.7
mg/L
<
/
Feb 2023
Average
0.005
/ 0.7
mg/L
/
2023
Quarter 1 <
0.005
/
mg/L
<
/
2023
1st 6 Months (Avg) <
0.005
/
mg/L
<
/
2023
1st 6 ...(Max) <
0.005
/
mg/L
<
/
2023
1st 6 ...(Min)
0.005
/
mg/L
/
2023
1st 6 ...(Count)
2
Sample Count
: 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sunday, February 25, 2024 5:55:38PM * Indicates Violation ** Indicates TRC Violation Page 2 of 3

United Therapeutics Corporation
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 002
SarnpleDate SamplelD Result/Limit Mass/Lunit
n-Amyl acetate
01/27/2023 P
UTP2012723POTW <
0.005
/ 20.7
mg/L
<
/
02/07/2023 S
UTP2020723Self <
0.001
/ 20.7
mg/L
<
/
Jan 2023
Week 4 <
0.005
/
mg/L
<
/
Feb 2023
Week 1 <
0.001
/
mg/L
<
/
Jan 2023
Average <
0.005
/ 8.2
mg/L
<
/
Feb 2023
Average <
0.001
/ 8.2
mg/L
<
/
2023
Quarter 1 <
0.003
/
mg/L
<
/
2023
1st 6 Months (Avg) <
0.003
/
mg/L
<
/
2023
1st 6 ...(Max) <
0.005
/
mg/L
<
/
2023
1st 6 ...(Min) <
0.001
/
mg/L
<
/
2023
1st 6... (Count)
2
Sample Count: 2 Months Sampled
:
2
Weeks Sampled :
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sunday, February 25, 2024 5:55:38PM * Indicates Violation ** Indicates TRC Violation Page 3 of 3

Wolfspeed Durham
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 007
Sample Date
SamplelD
Result/Limit
Mass/Limit
PH
02/16/2023 S
WolfspeedP7021623Se
7.7 /
SU
/
if
Feb 2023
Week 3
7.7 /
SU
/
Feb 2023
Average
7.7 /
SU
/
2023
Quarter 1
7.7 /
SU
/
2023
1st 6 Months (Avg)
7.7 /
SU
/
2023
1st 6 ...(Max)
7.7 /
SU
/
2023
lst6... (Min)
7.7 /
SU
/
2023
lst6... (Count)
1
Sample Date
SampleID
Result/Limit
Mass /Limit
Temperature
02/16/2023 S
WolfspeedP7021623Se
21 /
°C
/
if
Feb 2023
Week 3
21 /
°C
/
Feb 2023
Average
21 /
°C
/
2023
Quarter 1
21 /
°C
/
2023
1st 6 Months (Avg)
21 /
°C
/
2023
1st 6 ...(Max)
21 /
°C
/
2023
1st 6 ...(Min)
21 /
°C
/
2023
1st 6 ...(Count)
1
Sample Date
SamplelD
Result/Limit
Mass/Limit
VOC
02/16/2023 S
WolfspeedP7021623Se
0.464 /
mg/L
/
if
Feb 2023
Week 3
0.464 /
mg/L
/
Feb 2023
Average
0.464 /
mg/L
/
2023
Quarter 1
0.464 /
mg/L
/
2023
1st 6 Months (Avg)
0.464 /
mg/L
/
2023
Ist 6 ...(Marc)
0.464 /
mg/L
/
2023
lst6... (Min)
0.464 /
mg/L
/
2023
1st 6 ...(Count)
1 /
/
11112023
To 613012023
Sample Type: Effluent Wastewater
Outfall: 008
Sample Date
SampleID
Result/Limit
Mass/Limit
Aluminum
03/16/2023 S
WolfspeedP8021623Se
0.423 /
mg/L
/
if
Mar 2023
Week 3
0.423 /
mg/L
/
Mar 2023
Average
0.423 /
mg/L
/
Tuesday, February 13, 2024 11:09:47AM * Indicates Violation ** Indicates TRC Violation Page 1 of 1

Wolfspeed Durham
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 008
Sample Date
SamplelD
Result/Limit
Mass/Limit
Aluminum
2023
Quarter 1
0.423
/
mg/L
/
2023
1st 6 Months (Avg)
0.423
/
mg/L
/
2023
lst6... (Max)
0.423
/
mg/L
/
2023
1st 6 ...(Min)
0.423
/
mg/L
/
2023
1st 6 ...(Count)
1
Sample Date
SampleID
Result/Limit
Mass/Limit
Ammonia
03/16/2023
P
WolfspeedP8031623P
15.3
/
mg/L
/
OTW
03/16/2023
S
WolfspeedP8021623Se
19.8
/
mg/L
/
If
Mar 2023
Week 3
17.55
/
mg/L
/
Mar 2023
Average
17.55
/
mg/L
/
2023
Quarter 1
17.55
/
mg/L
/
2023
1st 6 Months (Avg)
17.55
/
mg/L
/
2023
1st 6 ...(Max)
19.8
/
mg/L
/
2023
1st 6 ...(Min)
15.3
/
mg/L
/
2023
1st 6 ...(Count)
2
/
/
Sample Date
SamplelD
Result/Limit
Mass/Limit
Average Flow for Month
01/31/2023
S
WolfspeedP80123F1ow
0.485612
/
MGD
/
02/28/2023
S
WolfspeedP80223F1ow
0.461068
/
MGD
/
03/31/2023
S
WolfspeedP80323F1ow
0.494258
/
MGD
/
04/30/2023
S
WolfspeedP80423F1ow
0.492223
/
MGD
/
05/31/2023
S
WolfspeedP80523F1ow
0.503774
/
MGD
/
06/30/2023
S
WolfspeedP80623F1ow
0.5219
/
MGD
/
Jan 2023
Week 4
0.485612
/
MGD
/
Feb 2023
Week 4
0.461068
/
MGD
/
Mar 2023
Week 4
0.494258
/
MGD
/
Apr 2023
Week 4
0.492223
/
MGD
/
May 2023
Week 4
0.503774
/
MGD
/
Jun 2023
Week 4
0.5219
/
MGD
/
Jan 2023
Average
0.485612
/
MGD
/
Feb 2023
Average
0.461068
/
MGD
/
Mar 2023
Average
0.494258
/
MGD
/
Apr 2023
Average
0.492223
/
MGD
/
May 2023
Average
0.503774
/
MGD
/
Jun 2023
Average
0.5219
/
MGD
/
2023
Quarter 1
0.480313
/
MGD
/
2023
Quarter 2
0.505966
/
MGD
/
Tuesday, February 13, 2024 11:09:47AM * Indicates Violation ** Indicates TRC Violation Page 1 of 9

Wolfspeed Durham
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 008
Sample Date
SamplelD
Result/Limit
Mass/Limit
Average Flow for Month
2023
1st 6 Months (Avg)
0.493139 /
MGD
/
2023
1st 6 ...(Max)
0.5219 /
MGD
/
2023
Ist 6... (Min)
0.461068 /
MGD
/
2023
Ist 6 ...(Count)
6
Sample Date
SampleID
Result/Limit
Mass/Limit
Barium
03/16/2023
S
WolfspeedP8021623Se
0.029 /
mg/L
/
if
Mar 2023
Week 3
0.029 /
mg/L
/
Mar 2023
Average
0.029 /
mg/L
/
2023
Quarter 1
0.029 /
mg/L
/
2023
1st 6 Months (Avg)
0.029 /
mg/L
/
2023
Ist 6 ...(Max)
0.029 /
mg/L
/
2023
1st 6 ...(Min)
0.029 /
mg/L
/
2023
Ist 6 ...(Count)
1
Sample Date
SampleID
Result/Limit
Mass/Limit
Cadmium
03/16/2023
S
WolfspeedP8021623Se
<
0.0005 /
mg/L
<
/
if
Mar 2023
Week 3
<
0.0005 /
mg/L
<
/
Mar 2023
Average
<
0.0005 /
mg/L
<
/
2023
Quarter 1
<
0.0005 /
mg/L
<
/
2023
1st 6 Months (Avg)
<
0.0005 /
mg/L
<
/
2023
Ist 6 ...(Max)
<
0.0005 /
mg/L
<
/
2023
Ist 6 ...(Min)
<
0.0005 /
mg/L
<
/
2023
Ist 6 ...(Count)
1
Sample Date
SamplelD
Result/Limit
Mass/Limit
Chloride
03/16/2023
P
WolfspeedP8031623P
200 /
mg/L
/
OTW
03/16/2023
S
WolfspeedP8021623Se
168 /
mg/L
/
if
Mar 2023
Week 3
184 /
mg/L
/
Mar 2023
Average
184 /
mg/L
/
2023
Quarter 1
184 /
mg/L
/
2023
1st 6 Months (Avg)
184 /
mg/L
/
2023
1st 6 ...(Max)
200 /
mg/L
/
2023
Ist 6 ...(Min)
168 /
mg/L
/
2023
Ist 6 ...(Count)
2
Tuesday, February 13, 2024 11:09:47AM * Indicates Violation ** Indicates TRC Violation Page 2 of 9

Wolfspeed Durham
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 008
Sample Date
SamplelD
Result/Limit
Mass/Limit
Chromium
03/16/2023
S
WolfspeedP8021623Se
0.006 /
mg/L
/
if
Mar 2023
Week 3
0.006 /
mg/L
/
Mar 2023
Average
0.006 /
mg/L
/
2023
Quarter 1
0.006 /
mg/L
/
2023
1st 6 Months (Avg)
0.006 /
mg/L
/
2023
1st 6 ...(Max)
0.006 /
mg/L
/
2023
lst6... (Min)
0.006 /
mg/L
/
2023
lst6... (Count)
1
Sample Date
SamplelD
Result/Limit
Mass/Limit
Copper
03/16/2023
S
WolfspeedP8021623Se
0.022 /
mg/L
/
if
Mar 2023
Week 3
0.022 /
mg/L
/
Mar 2023
Average
0.022 /
mg/L
/
2023
Quarter 1
0.022 /
mg/L
/
2023
1st 6 Months (Avg)
0.022 /
mg/L
/
2023
1st 6 ...(Max)
0.022 /
mg/L
/
2023
1st 6 ...(Min)
0.022 /
mg/L
/
2023
1st 6 ...(Count)
1
Sample Date
SamplelD
Result/Limit
Mass/Limit
Cyanide
03/16/2023
P
WolfspeedP8031623P
<
0.003 /
mg/L
<
/
OTW
03/16/2023
S
WolfspeedP8021623Se
<
0.003 /
mg/L
<
/
if
Mar 2023
Week 3
<
0.003 /
mg/L
<
/
Mar 2023
Average
<
0.003 /
mg/L
<
/
2023
Quarter 1
<
0.003 /
mg/L
<
/
2023
1st 6 Months (Avg)
<
0.003 /
mg/L
<
/
2023
1st 6 ...(Max)
<
0.003 /
mg/L
<
/
2023
1st 6 ...(Min)
<
0.003 /
mg/L
<
/
2023
1st 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
Fluoride
03/16/2023
P
WolfspeedP8031623P
1.9 /
mg/L
/
OTW
03/16/2023
S
WolfspeedP8021623Se
2.3 /
mg/L
/
if
03/16/2023
S
WolfspeedP8031623Se
2 /
mg/L
/
if
Tuesday, February
13, 2024 11:09:47AM
* Indicates Violation
** Indicates TRC Violation
Page 3 of 9

Wolfspeed Durham
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 008
Sample Date
SamplelD
Result/Limit
Mass/Limit
Fluoride
Mar 2023
Week 3
2.07 /
mg/L
/
Mar 2023
Average
2.07 /
mg/L
/
2023
Quarter 1
2.07 /
mg/L
/
2023
1st 6 Months (Avg)
2.07 /
mg/L
/
2023
1st 6 ...(Max)
2.3 /
mg/L
/
2023
lst6... (Min)
1.9 /
mg/L
/
2023
1st 6 ...(Count)
3
Sample Date
SamplelD
Result /Limit
Mass /Limit
Iodine
03/16/2023 S
WolfspeedP8021623Se
<
0.005 /
mg/L
<
/
if
05/11/2023 S
WolfspeedP8051123Se
0.01 /
mg/L
/
if
Mar 2023
Week 3
<
0.005 /
<
/
May 2023
Week 2
0.01
Mar 2023
Average
<
0.005 /
<
/
May 2023
Average
0.01
2023
Quarter 1
<
0.005 /
<
/
2023
Quarter 2
0.01
2023
1st 6 Months (Avg)
<
0.0075 /
mg/L
<
/
2023
1st 6 ...(Max)
0.01 /
mg/L
/
2023
1st 6 ...(Min)
<
0.005 /
mg/L
<
/
2023
1st 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
Lead
03/16/2023 S
WolfspeedP8021623Se
<
0.0025 /
mg/L
<
/
if
Mar 2023
Week 3
<
0.0025 /
mg/L
<
/
Mar 2023
Average
<
0.0025 /
mg/L
<
/
2023
Quarter 1
<
0.0025 /
mg/L
<
/
2023
1st 6 Months (Avg)
<
0.0025 /
mg/L
<
/
2023
1st 6 ...(Max)
<
0.0025 /
mg/L
<
/
2023
lst6... (Min)
<
0.0025 /
mg/L
<
/
2023
1st 6 ...(Count)
1
Sample Date
SamplelD
Result/Limit
Mass/Limit
Mercury - LL
02/16/2023 S
WolfspeedP8021623Se
<
0.000001 /
mg/L
<
/
1fHg
Feb 2023
Week 3
<
0.000001 /
mg/L
<
J
Feb 2023
Average
<
0.000001 /
mg/L
<
/
Tuesday, February 13, 2024 11:09:47AM * Indicates Violation ** Indicates TRC Violation Page 4 of 9

Wolfspeed Durham
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 008
Sample Date
SamplelD
Result/Limit
Mass/Limit
Mercury - LL
2023
Quarter 1 <
0.000001 /
mg/L <
/
2023
1st 6 Months (Avg) <
0.000001 /
mg/L <
/
2023
lst6... (Max) <
0.000001 /
mg/L <
/
2023
1st 6 ...(Min) <
0.000001 /
mg/L <
/
2023
1st 6 ...(Count)
1
Sample Date
SampleID
Result/Limit
Mass/Limit
Molybdenum
03/16/2023 S
WolfspeedP8021623Se
0.061 /
mg/L
/
if
Mar 2023
Week 3
0.061 /
mg/L
/
Mar 2023
Average
0.061 /
mg/L
/
2023
Quarter 1
0.061 /
mg/L
/
2023
1st 6 Months (Avg)
0.061 /
mg/L
/
2023
1st 6 ...(Max)
0.061 /
mg/L
/
2023
Ist 6 ...(Min)
0.061 /
mg/L
/
2023
1st 6 ...(Count)
I /
/
Sample Date
SamplelD
Result/Limit
Mass/Limit
Nickel
03/16/2023 S
WolfspeedP8021623Se
0.01 /
mg/L
/
if
Mar 2023
Week 3
0.01 /
mg/L
/
Mar 2023
Average
0.01 /
mg/L
/
2023
Quarter 1
0.01 /
mg/L
/
2023
1st 6 Months (Avg)
0.01 /
mg/L
/
2023
1st 6 ...(Max)
0.01 /
mg/L
/
2023
1st 6 ...(Min)
0.01 /
mg/L
/
2023
lst 6 ... (Count)
1
SampleDate
SamplelD
Result/Limit
Mass/Limit
Nitrate -Nitrite
03/16/2023 P
WolfspeedP8031623P
5 /
mg/L
/
OTW
03/16/2023 S
WolfspeedP8021623Se
7.4 /
mg/L
/
if
Mar 2023
Week 3
6.2 /
mg/L
/
Mar 2023
Average
6.2 /
mg/L
/
2023
Quarter 1
6.2 /
mg/L
/
2023
1 st 6 Months (Avg)
6.2 /
mg/L
/
2023
1st 6 ...(Max)
7.4 /
mg/L
/
2023
1st 6 ...(Min)
5.0 /
mg/L
/
2023
1st 6 ...(Count)
2
Tuesday, February 13, 2024 11:09:47AM * Indicates Violation ** Indicates TRC Violation Page 5 of 9

Wolfspeed Durham
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen, Total
03/16/2023 P
WolfspeedP8031623P
22.7
/ mg/L
/
OTW
03/16/2023 S
WolfspeedP8021623Se
36.43
/ mg/L
/
if
Mar 2023
Week 3
29.57
/ mg/L
/
Mar 2023
Average
29.57
/ mg/L
/
2023
Quarter 1
29.57
/ mg/L
/
2023
1st 6 Months (Avg)
29.57
/ mg/L
/
2023
1st 6 ...(Max)
36.43
/ mg/L
/
2023
lst6... (Min)
22.7
/ mg/L
/
2023
1st 6 ...(Count)
2
/
/
Sample Date SamplelD Result/Limit Mass /Limit
Oil & Grease, Total
03/16/2023 P
WolfspeedP8031623P
<
2.5
/ mg/L
<
/
OTW
03/16/2023 S
WolfspeedP8021623Se
5.7
/ mg/L
/
if
05/11/2023 S
WolfspeedP8051123Se
<
2.5
/ mg/L
<
/
if
Mar 2023
Week 3
<
4.1
/ mg/L
<
/
May 2023
Week 2
<
2.5
/ mg/L
<
/
Mar 2023
Average
<
4.1
/ mg/L
<
/
May 2023
Average
<
2.5
/ mg/L
<
/
2023
Quarter 1
<
4.1
/ mg/L
<
/
2023
Quarter 2
<
2.5
/ mg/L
<
/
2023
1 st 6 Months (Avg)
<
3.57
/ mg/L
<
/
2023
1st 6 ...(Max)
5.7
/ mg/L
/
2023
1st 6 ...(Min)
<
2.5
/ mg/L
<
/
2023
1st 6 ...(Count)
3
/
/
Sample Date SamplelD Result/Limit Mass/Limit
pH
03/16/2023
P WolfspeedP8031623P
OTW
03/16/2023
S WolfspeedP8021623Se
if
03/16/2023
S WolfspeedP8031623Se
If
Mar 2023
Week 3
Mar 2023
Average
2023
Quarter 1
2023
1st 6 Months (Avg)
2023
1st 6 ...(Max)
2023
1st 6 ...(Min)
Tuesday, February 13, 2024 11:09:47AM
7.9
/5.0-10.5
SU /
8.5
/5.0-10.5
SU /
7.8
/ 5.0 - 10.5
SU /
8.07
/
SU /
8.07
/
SU /
8.07
/
SU /
8.07
/
SU /
8.5
/
SU /
7.8
/
SU /
* Indicates Violation ** Indicates TRC Violation
Page 6 of 9

Wolfspeed Durham
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 008
Sample Date
SamplelD
Result/Limit
Mass/Limit
PH
2023
1st 6 ...(Count)
3
Sample Count: 3
Months Sampled: I
Weeks Sampled:
I
Quarters Sampled :
I
# Over Daily C :
0 0.00 # Over Mo Avg C :
0 0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Me Avg C TRC
: 0 0.00
# Over Wk Avg C TRC:
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0 0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC
: 0 0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
Selenium
03/16/2023 S
WolfspeedP8021623Se
<
0.005 /
mg/L
<
/
if
Mar 2023
Week 3
<
0.005 /
mg/L
<
/
Mar 2023
Average
<
0.005 /
mg/L
<
/
2023
Quarter 1
<
0.005 /
mg/L
<
/
2023
1st 6 Months (Avg)
<
0.005 /
mg/L
<
/
2023
1st 6 ...(Max)
<
0.005 /
mg/L
<
/
2023
lst 6 ...(Min)
<
0.005 /
mg/L
<
/
2023
lst6... (Count)
1
Sample Date
SamplelD
Result/Limit
Mass/Limit
Silver
03/16/2023 S
WolfspeedP8021623Se
<
0.0025 /
mg/L
<
/
if
Mar 2023
Week 3
<
0.0025 /
mg/L
<
/
Mar 2023
Average
<
0.0025 /
mg/L
<
/
2023
Quarter 1
<
0.0025 /
mg/L
<
/
2023
1st 6 Months (Avg)
<
0.0025 /
mg/L
<
/
2023
1st 6 ...(Max)
<
0.0025 /
mg/L
<
/
2023
lst6... (Min)
<
0.0025 /
mg/L
<
/
2023
1st 6 ...(Count)
1 /
/
Sample Date
SamplelD
Result/Limit
Mass/Limit
Temperature
03/16/2023 P
WolfspeedP8031623P
16 / 66
°C
/
OTW
03/16/2023 S
WolfspeedP8031623Se
17 / 66
°C
/
if
Mar 2023
Week 3
16.5 /
°C
/
Mar 2023
Average
16.5 /
°C
/
2023
Quarter 1
16.5 /
°C
/
Tuesday, February 13, 2024 11:09:47AM * Indicates Violation ** Indicates TRC Violation Page 7 of 9

Wolfspeed Durham
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
2023
1st 6 Months (Avg)
16.5 /
°C
/
2023
1st 6 ...(Max)
17 /
°C
/
2023
lst6... (Min)
16 /
°C
/
2023
1st 6 ...(Count)
2 /
/
Sample Count: 2
Months Sampled :
1
Weeks Sampled :
1
Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M:
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass /Limit
TKN
03/16/2023
P WolfspeedP8031623P
17.7
/ mg/L
/
OTW
03/16/2023
S WolfspeedP8021623Se
29
/ mg/L
/
if
Mar 2023
Week 3
23.35
/ mg/L
/
Mar 2023
Average
23.35
/ mg/L
/
2023
Quarter 1
23.35
/ mg/L
/
2023
1st 6 Months (Avg)
23.35
/ mg/L
/
2023
1st 6 ...(Max)
29
/ mg/L
/
2023
1st 6 ...(Min)
17.7
/ mg/L
/
2023
1st 6 ...(Count)
2
/
/
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
03/16/2023 P
WolfspeedP8031623P
1.05
/ mg/L
/
OTW
03/16/2023 S
WolfspeedP8021623Se
1.42
/ mg/L
/
if
Mar 2023
Week 3
1.235
/ mg/L
/
Mar 2023
Average
1.235
/ mg/L
/
2023
Quarter 1
1.235
/ mg/L
/
2023
1st 6 Months (Avg)
1.235
/ mg/L
/
2023
1st 6 ...(Max)
1.42
/ mg/L
/
2023
1st 6 ...(Min)
1.05
/ mg/L
/
2023
lst6... (Count)
2
Sample Date SamplelD Result/Limit Mass /Limit
Zinc
Tuesday, February 13, 2024 11:09:47AM * Indicates Violation ** Indicates TRC Violation Page 8 of 9

Wolfspeed Durham
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 008
Sample Date
SamplelD
Result/Limit
Mass/Limit
Zinc
03/16/2023
S WolfspeedP8021623Se
0.506 /
mg/L
/
if
Mar 2023
Week 3
0.506 /
mg/L
/
Mar 2023
Average
0.506 /
mg/L
/
2023
Quarter 1
0.506 /
mg/L
/
2023
1st 6 Months (Avg)
0.506 /
mg/L
/
2023
1st 6 ...(Max)
0.506 /
mg/L
/
2023
lst6... (Min)
0.506 /
mg/L
/
2023
lst6... (Count)
1
Sample Date
SamplelD
Result/Limit
Mass /Limit
Zirconium
03/16/2023
S WolfspeedP8021623Se
0.006 /
mg/L
/
if
05/11/2023
S WolfspeedP8051123Se
0.005 /
mg/L
/
if
Mar 2023
Week 3
0.006
May 2023
Week 2
0.005
Mar 2023
Average
0.006
May 2023
Average
0.005
2023
Quarter 1
0.006
2023
Quarter 2
0.005
2023
1st 6 Months (Avg)
0.0055 /
mg/L
/
2023
1st 6 ...(Max)
0.006 /
mg/L
/
2023
1st 6 ...(Min)
0.005 /
mg/L
/
2023
1st 6 ...(Count)
2
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 009
Sample Date SamplelD Result/Limit Mass /Limit
Average Flow for Month
01/31/2023
S
WolfspeedP90123F1ow
0.051081 /
MGD
/
02/28/2023
S
WolfspeedP90223F1ow
0.051063 /
MGD
/
03/31/2023
S
WolfspeedP90323171ow
0.046776 /
MGD
/
04/30/2023
S
WolfspeedP90423F1ow
0.044033 /
MGD
/
05/31/2023
S
WolfspeedP90523171ow
0.031266 /
MGD
/
06/30/2023
S
WolfspeedP90623171ow
0.032272 /
MGD
/
Jan 2023
Week 4
0.051081 /
MGD
/
Feb 2023
Week 4
0.051063 /
MGD
/
Mar 2023
Week 4
0.046776 /
MGD
/
Apr 2023
Week 4
0.044033 /
MGD
/
May 2023
Week 4
0.031266 /
MGD
/
Jun 2023
Week 4
0.032272 /
MGD
/
Tuesday, February 13, 2024 11:09:47AM * Indicates Violation ** Indicates TRC Violation Page 9 of 9

Wolfspeed Durham
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 009
Sample Date
SamplelD
Result/Limit
Mass/Limit
Average Flow for Mouth
Jan 2023
Average
0.051081 /
MGD
/
Feb 2023
Average
0.051063 /
MGD
/
Mar 2023
Average
0.046776 /
MGD
/
Apr 2023
Average
0.044033 /
MGD
/
May 2023
Average
0.031266 /
MGD
/
Jun 2023
Average
0.032272 /
MGD
/
2023
Quarter 1
0.04964 /
MGD
/
2023
Quarter 2
0.035857 /
MGD
/
2023
1st 6 Months (Avg)
0.042749 /
MGD
/
2023
1st 6 ...(Max)
0.051081 /
MGD
/
2023
1st 6... (Min)
0.031266 /
MGD
/
2023
1st 6 ...(Count)
6
Sample Date
SamplelD
Result/Limit
Mass/Limit
Chloride
03/16/2023
S
WolfspeedP9031623Se
15 /
mg/L
/
if
Mar 2023
Week 3
15 /
mg/L
/
Mar 2023
Average
15 /
mg/L
/
2023
Quarter 1
15 /
mg/L
/
2023
1st 6 Months (Avg)
15 /
mg/L
/
2023
1st 6 ...(Max)
15 /
mg/L
/
2023
1st 6 ...(Min)
15 /
mg/L
/
2023
1st 6 ...(Count)
1 /
/
Sample Date
SamplelD
Result/Limit
Mass/Limit
Copper
03/16/2023
S
WolfspeedP9031623Se
0.012 /
mg/L
/
if
Mar 2023
Week 3
0.012 /
mg/L
/
Mar 2023
Average
0.012 /
mg/L
/
2023
Quarter 1
0.012 /
mg/L
/
2023
1 st 6 Months (Avg)
0.012 /
mg/L
/
2023
1st 6 ...(Max)
0.012 /
mg/L
/
2023
1st 6 ...(Min)
0.012 /
mg/L
/
2023
1st 6 ...(Count)
1
Sample Date
SamplelD
Result/Limit
Mass/Limit
Fluoride
03/16/2023
P
WolfspeedP3031623P
0.46 /
mg/L
/
OTW
03/16/2023
S
WolfspeedP9031623Se
1.1 /
mg/L
/
1f
Tuesday, February 13, 2024 11:09:47AM * Indicates Violation ** Indicates TRC Violation Page 1 of 4

Wolfspeed Durham
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 009
Sample Date
SamplelD
Result/Limit
Mass/Limit
Fluoride
Mar 2023
Week 3
0.78 /
mg/L
/
Mar 2023
Average
0.78 /
mg/L
/
2023
Quarter 1
0.78 /
mg/L
/
2023
1st 6 Months (Avg)
0.78 /
mg/L
/
2023
1st 6 ...(Max)
1.1 /
mg/L
/
2023
lst6... (Min)
0.46 /
mg/L
/
2023
1st 6 ...(Count)
2
Sample Date
SamplelD
Result /Limit
Mass /Limit
Mercury - LL
02/16/2023
S
WolfspeedP9021623Se
0.000022 /
mg/L
/
lfHg
Feb 2023
Week 3
0.000022 /
mg/L
/
Feb 2023
Average
0.000022 /
mg/L
/
2023
Quarter 1
0.000022 /
mg/L
/
2023
1st 6 Months (Avg)
0.000022 /
mg/L
/
2023
1st 6 ...(Max)
0.000022 /
1119/1.
/
2023
lst 6 ...(Min)
0.000022 /
mg/L
/
2023
1st 6 ...(Count)
1 /
/
Sample Date
SamplelD
Result/Limit
Mass/Limit
Molybdenum
03/16/2023
P
WolfspeedP3031623P
0.105 /
mg/L
/
OTW
03/16/2023
S
WolfspeedP9031623Se
0.388 /
mg/L
/
if
Mar 2023
Week 3
0.247 /
mg/L
/
Mar 2023
Average
0.247 /
mg/L
/
2023
Quarter 1
0.247 /
mg/L
/
2023
1st 6 Months (Avg)
0.247 /
mg/L
/
2023
Ist 6 ...(Max)
0.388 /
mg/L
/
2023
Ist6... (Min)
0.105 /
mg/L
/
2023
1st 6 ...(Count)
2 /
/
Sample Date
SamplelD
Resalt/Lintit
Muss/Limit
Oil & Grease, Total
02/16/2023
S
WolfspeedP9021623Se
9.1 /
mg/L
/
if
03/16/2023
P
WolfspeedP3031623P <
2.5 /
mg/L <
/
OTW
03/16/2023
S
WolfspeedP9031623Se
7.1 /
mg/L
/
if
05/11/2023
S
WolfspeedP9051123Se
25.2 /
mg/L
/
if
Tuesday, February 13,
2024 11:09:47AM
* Indicates Violation
** Indicates TRC Violation
Page 2 of 4

Wolfspeed Durham
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 009
Sample Date SamplelD Result/Limit Mass/Limit
Oil & Grease, Total
Feb 2023
Week 3
9.1
/
mg/L
/
Mar 2023
Week 3 <
4.8
/
mg/L <
/
May 2023
Week 2
25.2
/
mg/L
/
Feb 2023
Average
9.1
/
mg/L
/
Mar 2023
Average <
4.8
/
mg/L <
/
May 2023
Average
25.2
/
mg/L
/
2023
Quarter 1 <
6.23
/
mg/L <
/
2023
Quarter 2
25.2
/
mg/L
/
2023
1st 6 Months (Avg) <
10.98
/
mg/L <
/
2023
1st 6 ...(Max)
25.2
/
mg/L
/
2023
1st 6... (Min) <
2.5
/
mg/L <
/
2023
1st 6 ...(Count)
4
Sample Date
SamplelD
Result/Limit
Mass/Limit
pH
02/16/2023 S
WolfspeedP9021623Se
5.9
/ 5.0 - 10.5
Su
/
if
03/16/2023 P
WolfspeedP3031623P
6.7
/ 5.0 - 10.5
SU
/
OTW
03/16/2023 S
WolfspeedP9031623Se
7.5
/ 5.0 - 10.5
SU
/
if
Feb 2023
Week 3
5.9
/
SU
/
Mar 2023
Week 3
7.1
/
SU
/
Feb 2023
Average
5.9
/
SU
/
Mar 2023
Average
7.1
/
SU
/
2023
Quarter 1
6.7
/
SU
/
2023
1st 6 Months (Avg)
6.7
/
SU
/
2023
1st 6 ...(Max)
7.5
/
SU
/
2023
1st 6 ...(Min)
5.9
/
SU
/
2023
1st 6 ...(Count)
3
Sample Count: 3 Months Sampled:
2
Weeks Sampled :
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C:
0 0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC
:
0 0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0 0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC
:
0 0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
03/16/2023 S WolfspeedP9031623Se 15 / °C /
if
Tuesday, February 13, 2024 11:09:47AM * Indicates Violation ** Indicates TRC Violation Page 3 of 4

Wolfspeed Durham
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 009
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
Mar 2023
Week 3
15
/ °C
/
Mar 2023
Average
15
/ °C
/
2023
Quarter 1
15
/ °C
/
2023
1st 6 Months (Avg)
15
/ °C
/
2023
1st 6 ...(Max)
15
/ °C
/
2023
lst6... (Min)
15
/ °C
/
2023
1st 6 ...(Count)
1
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 010
Sample Date SamplelD Result/Limit Mass/Limit
VOC
02/16/2023
S WolfspeedP10021623S
0.0543
/ mg/L
/
elf
Feb 2023
Week 3
0.0543
/ mg/L
/
Feb 2023
Average
0.0543
/ mg/L
/
2023
Quarter 1
0.0543
/ mg/L
/
2023
1st 6 Months (Avg)
0.0543
/ mg/L
/
2023
1st 6 ...(Max)
0.0543
/ mg/L
/
2023
1st 6 ...(Min)
0.0543
/ mg/L
/
2023
1st 6 ...(Count)
1
/
/
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: All
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2023
S
Wolfspeed0123F1ow
0.536693
/
MGD /
02/28/2023
S
Wolfspeed0223FIow
0.512131
/
MGD /
03/31/2023
S
Wolfspeed0323FIow
0.541034
/
MGD /
04/30/2023
S
Wolfspeed0423F1ow
0.536256
/
MGD /
05/31/2023
S
Wolfspeed0523F1ow
0.53504
/
MGD /
06/30/2023
S
Wolfspeed0623F1ow
0.554172
/
MGD /
Jan 2023
Week 4
0.536693
/
MGD /
Feb 2023
Week 4
0.512131
/
MGD /
Mar 2023
Week 4
0.541034
/
MGD /
Apr 2023
Week 4
0.536256
/
MGD /
May 2023
Week 4
0.53504
/
MGD /
Jun 2023
Week 4
0.554172
/
MGD /
Jan 2023
Average
0.536693
/ 0.591
MGD /
Feb 2023
Average
0.512131
/ 0.591
MGD /
Mar 2023
Average
0.541034
/ 0.591
MGD /
Tuesday, February 13, 2024 11:09:47AM * Indicates Violation ** Indicates TRC Violation Page 4 of 4

Wolfspeed Durham
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: All
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
Apr 2023 Average
0.536256
/ 0.591
MGD /
May 2023 Average
0.53504
/ 0.591
MGD /
Jun 2023 Average
0.554172
/ 0.591
MGD /
2023 Quarter 1
0.529953
/
MGD /
2023 Quarter 2
0.541823
/
MGD /
2023 1st 6 Months (Avg)
0.535888
/
MGD /
2023 1st 6 ...(Max)
0.554172
/
MGD /
2023 1st 6 ...(Min)
0.512131
/
MGD /
2023 1st 6 ...(Count)
6
Sample Count:
6
Months Sampled:
6
Weeks Sampled:
6
Quarters Sampled :
2
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
11112023 To 613012023 Sample Type: Effluent Wastewater OuVWL- 013
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2023
S
WolfspeedP130123F10
w
02/28/2023
S
WolfspeedP130223F10
w
03/31/2023
S
WolfspeedP130323F10
w
04/30/2023
S
Wolfspec:0130423F10
w
05/31/2023
S
WolfspeedP130523F10
w
06/30/2023
S
Wolfspec:01306231710
W
Jan 2023
Week 4
Feb 2023
Week 4
Mar 2023
Week 4
Apr 2023
Week 4
May 2023
Week 4
Jun 2023
Week 4
Jan 2023
Average
Feb 2023
Average
Mar 2023
Average
Apr 2023
Average
0.000377
/
MGD /
0.000449
/
MGD /
0.000606
/
MGD /
0.000696
/
MGD /
0.000711
/
MGD /
0.000747
/
MGD /
0.000377
/
MGD /
0.000449
/
MGD /
0.000606
/
MGD /
0.000696
/
MGD /
0.000711
/
MGD /
0.000747
/
MGD /
0.000377
/ 0.030
MGD /
0.000449
/ 0.030
MGD /
0.000606
/ 0.030
MGD /
0.000696
/ 0.030
MGD /
Tuesday, February 13, 2024 11:09:47AM * Indicates Violation ** Indicates TRC Violation Page 1 of 1

Wolfspeed Durham
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 013
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Mouth
May 2023 Average
0.000711
/ 0.030
MGD /
Jun 2023 Average
0.000747
/ 0.030
MGD /
2023 Quarter 1
0.000477
/
MGD /
2023 Quarter 2
0.000718
/
MGD /
2023 1st 6 Months (Avg)
0.000598
/
MGD /
2023 lst6... (Max)
0.000747
/
MGD /
2023 1st 6 ...(Min)
0.000377
/
MGD /
2023 1st 6 ...(Count)
6
Sample Count:
6
Months Sampled:
6
Weeks Sampled:
6
Quarters Sampled :
2
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass /Limit
Cadmium
03/13/2023 P
WolfspeedP13031323P
< 0.00008
/ 0.11
mg/L
<
/
OTW
Mar 2023
Week 2
< 0.00008
/
mg/L
<
/
Mar 2023
Average
< 0.00008
/ 0.07
mg/L
<
/
2023
Quarter 1
< 0.00008
/
mg/L
<
/
2023
1st 6 Months (Avg) < 0.00008
/
mg/L
<
/
2023
Ist 6 ...(Max)
< 0.00008
/
mg/L
<
/
2023
1st 6 ...(Min)
< 0.00008
/
mg/L
<
/
2023
1st 6 ...(Count)
1
/
/
Sample Count: 1
Months Sampled:
1
Weeks Sampled:
1
Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C:
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
Chromium
03/13/2023 P WolfspeedP13031323P < 0.001 / 2.77 mg/L < /
OTW
Mar 2023 Week 2 < 0.001 / mg/L < /
Tuesday, February 13, 2024 11:09:47AM * Indicates Violation ** Indicates TRC Violation Page 1 of 5

Wolfspeed Durham
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 013
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
Mar 2023
Average
<
0.001
/ 1.71
mg/L
<
/
2023
Quarter 1
<
0.001
/
mg/L
<
/
2023
1 st 6 Months (Avg) <
0.001
/
mg/L
<
/
2023
Ist 6 ...(Max)
<
0.001
/
mg/L
<
/
2023
1st 6 ...(Min)
<
0.001
/
mg/L
<
/
2023
1st 6 ...(Count)
1
Sample Count: 1
Months Sampled
:
1
Weeks Sampled:
1
Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C :
0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC :
0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M :
0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC :
0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
Copper
03/13/2023 P
WolfspeedP1303'1323P
<
0.001
/ 3.38
mg/L
<
/
OTW
Mar 2023
Week 2
<
0.001
/
mg/L
<
/
Mar 2023
Average
<
0.001
/ 2.07
mg/L
<
/
2023
Quarter 1
<
0.001
/
mg/L
<
/
2023
1st 6 Months (Avg) <
0.001
/
mg/L
<
/
2023
Ist 6 ...(Max)
<
0.001
/
mg/L
<
/
2023
1st 6 ...(Min)
<
0.001
/
mg/L
<
/
2023
Ist 6 ...(Count)
1
/
/
Sample Count: 1
Months Sampled
:
1
Weeks Sampled:
1
Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C:
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C :
0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC:
0
0.00
# Over Qt Avg C TRC :
0
0.00
# Over Daily M:
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M :
0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC :
0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
03/13/2023
P WolfspeedP13031323P <
0.003
/ 1.20
mg/L < /
OTW
Mar 2023
Week 2 <
0.003
/
mg/L < /
Mar 2023
Average <
0.003
/ 0.65
mg/L < /
2023
Quarter 1 <
0.003
/
mg/L < /
Tuesday, February 13, 2024 11:09:47AM * Indicates Violation ** Indicates TRC Violation Page 2 of 5

Wolfspeed Durham
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 013
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
2023
1st 6 Months (Avg) < 0.003
/
mg/L <
/
2023
1st 6 ...(Max)
< 0.003
/
mg/L <
/
2023
lst6... (Min)
< 0.003
/
mg/L <
/
2023
1st 6 ...(Count)
1
/
/
Sample Count: 1
Months Sampled
:
1
Weeks Sampled:
1
Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M:
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass /Limit
Lead
03/13/2023 P
WolfspeedP13031323P
<
0.0003
/ 0.69
mg/L
<
/
OTW
Mar 2023
Week 2
<
0.0003
/
mg/L
<
/
Mar 2023
Average
<
0.0003
/ 0.43
mg/L
<
/
2023
Quarter 1
<
0.0003
/
mg/L
<
/
2023
1st 6 Months (Avg) <
0.0003
/
mg/L
<
/
2023
1st 6 ...(Max)
<
0.0003
/
mg/L
<
/
2023
1st 6 ...(Min)
<
0.0003
/
mg/L
<
/
2023
1st 6 ...(Count)
1
Sample Count : 1
Months Sampled:
1
Weeks Sampled:
1
Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C:
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC
:
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
03/13/2023
P WolfspeedP13031323P
0.114
/ 3.98
mg/L /
OTW
Mar 2023
Week 2
0.114
/
mg/L /
Mar 2023
Average
0.114
/ 2.38
mg/L /
2023
Quarter 1
0.114
/
mg/L /
2023
1st 6 Months (Avg)
0.114
/
mg/L /
2023
1st 6 ...(Max)
0.114
/
mg/L /
Tuesday, February 13, 2024 11:09:47AM * Indicates Violation ** Indicates TRC Violation Page 3 of 5

Wolfspeed Durham
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 013
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
2023
1st 6 ...(Min)
0.114
/
mg/L
/
2023
1st 6 ...(Count)
1
/
/
Sample Count :
1
Months Sampled:
1
Weeks Sampled:
1
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit
Silver
Mass/Limit
03/13/2023 P
WolfspeedP13031323P <
0.0003
/ 0.43
mg/L
<
/
OTW
Mar 2023
Week 2
<
0.0003
/
mg/L
<
/
Mar 2023
Average
<
0.0003
/ 0.24
mg/L
<
/
2023
Quarter 1
<
0.0003
/
mg/L
<
/
2023
1st 6 Months (Avg) <
0.0003
/
mg/L
<
/
2023
lst 6 ...(Max)
<
0.0003
/
mg/L
<
/
2023
1st 6 ...(Min)
<
0.0003
/
mg/L
<
/
2023
lst6... (Count)
1
Sample Count: 1
Months Sampled:
1
Weeks Sampled
:
1
Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC
:
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily:
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
03/13/2023
P WolfspeedP13031323P
<
0.003
/ 2,61
mg/L
< /
OTW
Mar 2023
Week 2
<
0.003
/
mg/L
< /
Mar 2023
Average
<
0.003
/ 1.48
mg/L
< /
2023
Quarter 1
<
0.003
/
mg/L
< /
2023
1st 6 Months (Avg)
<
0.003
/
mg/L
< /
2023
1st 6 ...(Max)
<
0.003
/
mg/L
< /
2023
1st 6 ...(Min)
<
0.003
/
mg/L
< /
2023
1st 6 ...(Count)
1
/
/
Tuesday, February 13, 2024 11:09:47AM * Indicates Violation ** Indicates TRC Violation Page 4 of 5

Wolfspeed Durham
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outttall: 013
Sample Count:
1
Months Sampled :
1
Weeks Sampled:
1
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Tuesday, February 13, 2024 11:09:47AM * Indicates Violation ** Indicates TRC Violation Page 5 of 5

Wolfspeed RTP
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 012
Sample Date
SamplelD
Result/Limit
Mass/Limit
Aluminum
02/16/2023
S
WolfspeedRTPP12021
0.031 /
mg/L
/
623Self
Feb 2023
Week 3
0.031 /
mg/L
/
Feb 2023
Average
0.031 /
mg/L
/
2023
Quarter 1
0.031 /
mg/L
/
2023
1st 6 Months (Avg)
0.031 /
mg/L
/
2023
Ist 6 ...(Max)
0.031 /
mg/L
/
2023
Ist 6... (Min)
0.031 /
mg/L
/
2023
Ist 6 ... (Count)
1
Sample Date
SamplelD
Result/Limit
Mass /Limit
Ammonia
01/06/2023
P
WolfspeedRTPP12010
6.3 /
mg/L
/
623POTW
02/16/2023
S
WolfspeedRTPP12021
5.55 /
mg/L
/
623Self
Jan 2023
Week 1
6.3 /
mg/L
/
Feb 2023
Week 3
5.55 /
mg/L
/
Jan 2023
Average
6.3 /
mg/L
/
Feb 2023
Average
5.55 /
mg/L
/
2023
Quarter 1
5.93 /
mg/L
/
2023
1st 6 Months (Avg)
5.93 /
mg/L
/
2023
Ist 6 ...(Max)
6.3 /
mg/L
/
2023
Ist 6 ...(Min)
5.55 /
mg/L
/
2023
Ist 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
Arsenic
02/16/2023
S
WolfspeedRTPP12021
<
0.0025 /
mg/L
<
/
623Self
Feb 2023
Week 3
<
0.0025 /
mg/L
<
/
Feb 2023
Average
<
0.0025 /
mg/L
<
/
2023
Quarter 1
<
0.0025 /
mg/L
<
/
2023
1st 6 Months (Avg)
<
0.0025 /
mg/L
<
/
2023
Ist 6 ...(Max)
<
0.0025 /
mg/L
<
/
2023
Ist 6 ...(Min)
<
0.0025 /
mg/L
<
/
2023
Ist 6 ...(Count)
1 /
/
Sample Date
SamplelD
Result/Limit
Mass/Limit
Average Flow for Month
01 31/2023
S
WolfspeedRTPP12012
0.064627 / 0.469
MGD
/
3Flow
02/28/2023
S
WolfspeedRTPP12022
0.061576 / 0.469
MGD
/
3Flow
Tuesday, February 13, 2024 11:10:41AM * Indicates Violation ** Indicates TRC Violation Page 1 of 10

Wolfspeed RTP
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
03/31/2023
S
WolfspeedRTPP12032
0.060248
/ 0.469
MGD /
3Flow
04/30/2023
S
WolfspeedRTPP12042
0.061938
/ 0.469
MGD /
3Flow
05/31/2023
S
WolfspeedRTPP12052
0.06246
/ 0.469
MGD /
3Flow
06/30/2023
S
WolfspeedRTPP12062
0.058295
/ 0.469
MGD /
3Flow
Jan 2023
Week 4
0.064627
/
MGD /
Feb 2023
Week 4
0.061576
/
MGD /
Mar 2023
Week 4
0.060248
/
MGD /
Apr 2023
Week 4
0.061938
/
MGD /
May 2023
Week 4
0.06246
/
MGD /
Jun 2023
Week 4
0.058295
/
MGD /
Jan 2023
Average
0.064627
/ 0.329
MGD /
Feb 2023
Average
0.061576
/ 0.329
MGD /
Mar 2023
Average
0.060248
/ 0.329
MGD /
Apr2023
Average
0.061938
/ 0.329
MGD /
May 2023
Average
0.06246
/ 0.329
MGD /
Jun 2023
Average
0.058295
/ 0.329
MGD /
2023
Quarter 1
0.06215
/
MGD /
2023
Quarter 2
0.060898
/
MGD /
2023
1st 6 Months (Avg)
0.061524
/
MGD /
2023
1st 6 ...(Max)
0.064627
/
MGD /
2023
1st 6 ...(Min)
0.058295
/
MGD /
2023
1st 6 ...(Count)
6
Sample Count:
6
Months Sampled :
6
Weeks Sampled:
6
Quarters Sampled :
2
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
Barium
02/16/2023
S WolfspeedRTPP12021
0.025 /
mg/L
/
623Self
Feb 2023
Week 3
0.025 /
mg/L
/
Feb 2023
Average
0.025 /
mg/L
/
2023
Quarter 1
0.025 /
mg/L
/
2023
1st 6 Months (Avg)
0.025 /
mg/L
/
2023
1st 6 ...(Max)
0.025 /
mg/L
/
Tuesday, February 13, 2024 11:10:41AM * Indicates Violation ** Indicates TRC Violation Page 2 of 10

Wolfspeed RTP
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 012
Sample Date
SamplelD
Result/Limit
Mass/Limit
Barium
2023
1st 6 ...(Min)
0.025 /
mg/L
/
2023
1st 6 ...(Count)
1
Sample Date
SamplelD
Result/Limit
Mass/Limit
Cadmium
02/16/2023
S WolfspeedRTPP12021
<
0.0005 /
mg/L
<
/
623Self
Feb 2023
Week 3
<
0.0005 /
mg/L
<
/
Feb 2023
Average
<
0.0005 /
mg/L
<
/
2023
Quarter 1
<
0.0005 /
mg/L
<
/
2023
1st 6 Months (Avg)
<
0.0005 /
mg/L
<
/
2023
1st 6 ...(Max)
<
0.0005 /
mg/L
<
/
2023
1st 6 ...(Min)
<
0.0005 /
mg/L
<
/
2023
1st 6 ...(Count)
1 /
/
Sample Date
SamplelD
Result/Limit
Mass/Limit
Chloride
01/06/2023
P WolfspeedRTPP12010
152 /
mg/L
/
623POTW
02/16/2023
S WolfspeedRTPP12021
127 /
mg/L
/
623Self
Jan 2023
Week 1
152 /
mg/L
/
Feb 2023
Week 3
127 /
mg/L
/
Jan 2023
Average
152 /
mg/L
/
Feb 2023
Average
127 /
mg/L
/
2023
Quarter 1
139.5 /
mg/L
/
2023
1st 6 Months (Avg)
139.5 /
mg/L
/
2023
1st 6 ...(Max)
152 /
mg/L
/
2023
1st 6 ...(Min)
127 /
mg/L
/
2023
1st 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
Chromium
02/16/2023
S WolfspeedRTPP12021
0.005
/ mg/L
/
623Self
Feb 2023
Week 3
0.005
/ mg/L
/
Feb 2023
Average
0.005
/ mg/L
/
2023
Quarter 1
0.005
/ mg/L
/
2023
1st 6 Months (Avg)
0.005
/ mg/L
/
2023
1st 6 ...(Max)
0.005
/ mg/L
/
2023
1st 6 ...(Min)
0.005
/ mg/L
/
2023
1st 6 ...(Count)
1
Tuesday, February 13, 2024 11:10:41AM * Indicates Violation ** Indicates TRC Violation Page 3 of 10

Wolfspeed RTP
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 012
Sample Date
SamplelD
Result/Limit
Mass/Limit
Copper
02/16/2023
S
WolfspeedRTPP12021
0.012
/
mg/L
/
623Self
Feb 2023
Week 3
0.012
/
mg/L
/
Feb 2023
Average
0.012
/
mg/L
/
2023
Quarter 1
0.012
/
mg/L
/
2023
1st 6 Months (Avg)
0.012
/
mg/L
/
2023
Ist 6 ...(Max)
0.012
/
mg/L
/
2023
Ist 6... (Min)
0.012
/
mg/L
/
2023
Ist 6 ... (Count)
1
Sample Date
SamplelD
Result/Limit
Mass /Limit
Cyanide
01/06/2023
P
WolfspeedRTPP12010
0.006
/
mg/L
/
623POTW
02/16/2023
S
WolfspeedRTPP12021
<
0.003
/
mg/L
<
/
623Self
Jan 2023
Week 1
0.006
/
mg/L
/
Feb 2023
Week 3
<
0.003
/
mg/L
<
/
Jan 2023
Average
0.006
/
mg/L
/
Feb 2023
Average
<
0.003
/
mg/L
<
/
2023
Quarter I
<
0.004
/
mg/L
<
/
2023
1st 6 Months (Avg)
<
0.004
/
mg/L
<
/
2023
Ist 6 ...(Max)
0.006
/
mg/L
/
2023
Ist 6 ...(Min)
<
0.003
/
mg/L
<
/
2023
Ist 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
Fluoride
01/06/2023
P
WolfspeedRTPP12010
1.89
/ 8.0
mg/L
/
623POTW
02/16/2023
S
WolfspeedRTPP12021
2.6
/ 8.0
mg/L
/
623Self
Jan 2023
Week 1
1.89
/
mg/L
/
Feb 2023
Week 3
2.6
/
mg/L
/
Jan 2023
Average
1.89
/ 7.0
mg/L
/
Feb 2023
Average
2.6
/ 7.0
mg/L
/
2023
Quarter 1
2.25
/
mg/L
/
2023
1st 6 Months (Avg)
2.25
/
mg/L
/
2023
Ist 6 ...(Max)
2.6
/
mg/L
/
2023
Ist 6 ...(Min)
1.89
/
mg/L
/
2023
Ist 6 ...(Count)
2
Tuesday, February 13, 2024 11:10:41AM * Indicates Violation ** Indicates TRC Violation Page 4 of 10

Wolfspeed RTP
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 012
Sample Count: 2
Months Sampled :
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C:
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C :
0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC :
0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M :
0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC :
0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
Lead
02/16/2023 S
WolfspeedRTPP12021 < 0.0025
/
mg/L
<
/
623Self
Feb 2023
Week 3
< 0.0025
/
mg/L
<
/
Feb 2023
Average
< 0.0025
/
mg/L
<
/
2023
Quarter 1
< 0.0025
/
mg/L
<
/
2023
1st 6 Months (Avg) < 0.0025
/
mg/L
<
/
2023
Ist 6 ...(Max)
< 0.0025
/
mg/L
<
/
2023
Ist 6 ...(Min)
< 0.0025
/
mg/L
<
/
2023
Ist 6 ...(Count)
1
Sample Date
SamplelD
Result/Limit
Mass /Limit
Mercury - LL
02/16/2023 S
WolfspeedRTPP12021 < 0.000001
/
mg/L
<
/
623Self
05/01/2023 P
WolfspeedRTPP12050 0.000008
/
mg/L
/
123POTWHg
Feb 2023
Week 3
< 0.000001
/
mg/L
<
/
May 2023
Week 1
0.000008
/
mg/L
/
Feb 2023
Average
< 0.000001
/ 0.000142
mg/L
<
/
May 2023
Average
0.000008
/ 0.000142
mg/L
/
2023
Quarter 1
< 0.000001
/
mg/L
<
/
2023
Quarter 2
0.000008
/
mg/L
/
2023
1st 6 Months (Avg) < 0.000004
/
mg/L
<
/
2023
Ist 6 ...(Max)
0.000008
/
mg/L
/
2023
Ist 6 ...(Min)
< 0.000001
/
mg/L
<
/
2023
Ist 6 ...(Count)
2
Sample Count: 2
Months Sampled
:
2
Weeks Sampled:
2
Quarters Sampled :
2
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C :
0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC :
0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M :
0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC :
0
0.00
# Under Daily:
0 0.00
# Under Daily TRC:
0 0.00
Tuesday, February 13, 2024 11:10:41AM * Indicates Violation ** Indicates TRC Violation Page 5 of 10

Wolfspeed RTP
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
01/06/2023 P
WolfspeedRTPP12010
0.02
/ mg/L
/
623POTW
02/16/2023 S
WolfspeedRTPP12021
0.018
/ mg/L
/
623Self
Jan 2023
Week 1
0.02
/ mg/L
/
Feb 2023
Week 3
0.018
/ mg/L
/
Jan 2023
Average
0.02
/ mg/L
/
Feb 2023
Average
0.018
/ mg/L
/
2023
Quarter 1
0.019
/ mg/L
/
2023
1 st 6 Months (Avg)
0.019
/ mg/L
/
2023
Ist 6 ...(Max)
0.020
/ mg/L
/
2023
Ist 6 ...(Min)
0.018
/ mg/L
/
2023
Ist 6 ...(Count)
2
/
/
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
02/16/2023 S
WolfspeedRTPP12021
0.012
/
mg/L
/
623Self
Feb 2023
Week 3
0.012
/
mg/L
/
Feb 2023
Average
0.012
/
mg/L
/
2023
Quarter 1
0.012
/
mg/L
/
2023
1st 6 Months (Avg)
0.012
/
mg/L
/
2023
Ist 6 ...(Max)
0.012
/
mg/L
/
2023
Ist 6 ...(Min)
0.012
/
mg/L
/
2023
Ist 6 ...(Count)
1
Sample Date
SamplelD
Result/Limit
Mass/Limit
Nitrate -Nitrite
01/06/2023 P
WolfspeedRTPP12010
3.4
/
mg/L
/
623POTW
02/16/2023 S
WolfspeedRTPP12021
2.3
/
mg/L
/
623Self
Jan 2023
Week 1
3.4
/
mg/L
/
Feb 2023
Week 3
2.3
/
mg/L
/
Jan 2023
Average
3.4
/
mg/L
/
Feb 2023
Average
2.3
/
mg/L
/
2023
Quarter 1
2.9
/
mg/L
/
2023
1st 6 Months (Avg)
2.9
/
mg/L
/
2023
Ist 6 ...(Max)
3.4
/
mg/L
/
2023
Ist 6 ...(Min)
2.3
/
mg/L
/
2023
Ist 6 ...(Count)
2
Tuesday, February 13, 2024 11:10:41AM * Indicates Violation ** Indicates TRC Violation Page 6 of 10

Wolfspeed RTP
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen, Total
01/06/2023 P
WolfspeedRTPP12010
16.6
/ mg/L
/
623POTW
02/16/2023 S
WolfspeedRTPP12021
14.29
/ mg/L
/
623Self
Jan 2023
Week 1
16.6
/ mg/L
/
Feb 2023
Week 3
14.29
/ mg/L
/
Jan 2023
Average
16.6
/ mg/L
/
Feb 2023
Average
14.29
/ mg/L
/
2023
Quarter 1
15.45
/ mg/L
/
2023
1 st 6 Months (Avg)
15.45
/ mg/L
/
2023
1st 6 ...(Max)
16.6
/ mg/L
/
2023
1st 6 ...(Min)
14.29
/ mg/L
/
2023
1st 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass /Limit
Oil & Grease, Total
01/06/2023 P
WolfspeedRTPP12010 <
2.5
/ 200
mg/L
<
/
623POTW
02/16/2023 S
WolfspeedRTPP12021
7.1
/ 200
mg/L
/
623Self
05/11/2023 S
WolfspeedRTPP12051 <
2.5
/ 200
mg/L
<
/
123Self
Jan 2023
Week 1 <
2.5
/
mg/L
<
/
Feb 2023
Week 3
7.1
/
mg/L
/
May 2023
Week 2 <
2.5
/
mg/L
<
/
Jan 2023
Average <
2.5
/
mg/L
<
/
Feb 2023
Average
7.1
/
mg/L
/
May 2023
Average <
2.5
/
mg/L
<
/
2023
Quarter 1 <
4.8
/
mg/L
<
/
2023
Quarter 2 <
2.5
/
mg/L
<
/
2023
1st 6 Months (Avg) <
4.03
/
mg/L
<
/
2023
1st 6 ...(Max)
7.1
/
mg/L
/
2023
1st 6 ...(Min) <
2.5
/
mg/L
<
/
2023
1st 6 ...(Count)
3
Sample Count: 3 Months Sampled:
3
Weeks Sampled:
3
Quarters Sampled :
2
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Tuesday, February 13, 2024 11:10:41AM * Indicates Violation ** Indicates TRC Violation Page 7 of 10

Wolfspeed RTP
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 012
Sample Date
SamplelD
Result/Limit
Mass/Limit
PH
01/06/2023 P
WolfspeedRTPP12010
7 / 5.0 - 10.5
SU
/
623POTW
02/16/2023 S
WolfspeedRTPP12021
6.8 / 5.0 - 10.5
SU
/
623Self
Jan 2023
Week 1
7 /
SU
/
Feb 2023
Week 3
6.8 /
SU
/
Jan 2023
Average
7 /
SU
/
Feb 2023
Average
6.8 /
SU
/
2023
Quarter 1
6.9 /
SU
/
2023
1 st 6 Months (Avg)
6.9 /
SU
/
2023
Ist 6 ...(Max)
7 /
SU
/
2023
Ist 6 ...(Min)
6.8 /
SU
/
2023
Ist 6 ...(Count)
2
Sample Count: 2 Months Sampled: 2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C:
0 0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0 0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0 0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0 0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
Selenium
02/16/2023 S
WolfspeedRTPP12021 <
0.005 /
mg/L
<
/
623Self
Feb 2023
Week 3 <
0.005 /
mg/L
<
/
Feb 2023
Average <
0.005 /
mg/L
<
/
2023
Quarter 1 <
0.005 /
mg/L
<
/
2023
1 st 6 Months (Avg) <
0.005 /
mg/L
<
/
2023
1st 6 ...(Max) <
0.005 /
mg/L
<
/
2023
Ist 6 ...(Min) <
0.005 /
mg/L
<
/
2023
Ist 6 ...(Count)
I
Sample Date
SamplelD
Result/Limit
Mass/Limit
Silver
02/16/2023
S WolfspeedRTPP12021 <
623Self
Feb 2023
Week 3 <
Feb 2023
Average <
2023
Quarter 1 <
2023
1st 6 Months (Avg) <
2023
Ist 6 ...(Max) <
0.0025
/ mg/L
<
0.0025
/ mg/L
<
0.0025
/ mg/L
<
0.0025
/ mg/L
<
0.0025
/ mg/L
<
0.0025
/ mg/L
<
Tuesday, February 13, 2024 11:10:41AM * Indicates Violation ** Indicates TRC Violation Page 8 of 10

Wolfspeed RTP
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 012
Sample Date
SamplelD
Result/Limit
Mass/Limit
Over
2023
1st 6 ...(Min) <
0.0025 /
mg/L <
/
2023
1st 6 ...(Count)
1
Sample Date
SamplelD
Result/Limit
Mass/Limit
Temperature
01/06/2023 P
WolfspeedRTPP12010
13 / 66
°C
/
623POTW
02/16/2023 S
WolfspeedRTPP12021
8 / 66
°C
/
623Self
Jan 2023
Week 1
13 /
°C
/
Feb 2023
Week 3
8 /
°G
/
Jan 2023
Average
13 /
°C
/
Feb 2023
Average
8 /
°C
/
2023
Quarter 1
10.5 /
°C
/
2023
1st 6 Months (Avg)
10.5 /
°C
/
2023
1st 6 ...(Max)
13 /
°C
/
2023
1st 6 ...(Min)
8 /
°C
/
2023
1st 6 ...(Count)
2
Sample Count : 2 Months Sampled: 2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0 0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC
: 0 0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M:
0 0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC
: 0 0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
TKN
01/06/2023 P
WolfspeedRTPP12010
13.2 /
mg/L
/
623POTW
02/16/2023 S
WolfspeedRTPP12021
11.98 /
mg/L
/
623Self
Jan 2023
Week 1
13.2 /
mg/L
/
Feb 2023
Week 3
11.98 /
mg/L
/
Jan 2023
Average
13.2 /
mg/L
/
Feb 2023
Average
11.98 /
mg/L
/
2023
Quarter 1
12.59 /
mg/L
/
2023
1st 6 Months (Avg)
12.59 /
mg/L
/
2023
1st 6 ...(Max)
13.2 /
mg/L
/
2023
1st 6 ...(Min)
11.98 /
mg/L
/
2023
1st 6 ...(Count)
2
Tuesday, February 13, 2024 11:10:41AM * Indicates Violation ** Indicates TRC Violation Page 9 of 10

Wolfspeed RTP
SAMPLE OVERVIEW
11112023 To 613012023 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
01/06/2023 P
WolfspeedRTPP12010
3.55
/ mg/L
/
623POTW
02/16/2023 S
WolfspeedRTPP12021
1.34
/ mg/L
/
623Self
Jan 2023
Week 1
3.55
/ mg/L
/
Feb 2023
Week 3
1.34
/ mg/L
/
Jan 2023
Average
3.55
/ mg/L
/
Feb 2023
Average
1.34
/ mg/L
/
2023
Quarter 1
2.445
/ mg/L
/
2023
1 st 6 Months (Avg)
2.445
/ mg/L
/
2023
Ist 6 ...(Max)
3.55
/ mg/L
/
2023
Ist 6 ...(Min)
1.34
/ mg/L
/
2023
Ist 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
VOC
02/16/2023
S WolfspeedRTPP12021
0.829
/
mg/L
/
623Self
Feb 2023
Week 3
0.829
/
mg/L
/
Feb 2023
Average
0.829
/
mg/L
/
2023
Quarter 1
0.829
/
mg/L
/
2023
1st 6 Months (Avg)
0.829
/
mg/L
/
2023
Ist 6 ...(Max)
0.829
/
mg/L
/
2023
Ist 6 ...(Min)
0.829
/
mg/L
/
2023
Ist 6 ...(Count)
1
Sample Date
SamplelD
Result/Limit
Mass/Limit
Zinc
02/16/2023
S WolfspeedRTPP12021
0.412
/
mg/L
/
623Self
Feb 2023
Week 3
0.412
/
mg/L
/
Feb 2023
Average
0.412
/
mg/L
/
2023
Quarter 1
0.412
/
mg/L
/
2023
1st 6 Months (Avg)
0.412
/
mg/L
/
2023
Ist 6 ...(Max)
0.412
/
mg/L
/
2023
Ist 6 ...(Min)
0.412
/
mg/L
/
2023
Ist 6 ...(Count)
1
/
/
Tuesday, February 13, 2024 11:10:41AM * Indicates Violation ** Indicates TRC Violation Page 10 of 10

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
08/29/2023
S AStIaZeneca082923Sel
<
0.025
/ 20.7
mg/L
< /
f
Aug 2023
Week 4
<
0.025
/
mg/L
< /
Aug 2023
Average
<
0.025
/ 8.2
mg/L
< /
2023
Quarter 3
<
0.025
/
mg/L
< /
2023
2nd 6 Months (Avg)
<
0.025
/
mg/L
< /
2023
2nd 6 ...(Max)
<
0.025
/
mg/L
< /
2023
2nd 6 ...(Min)
<
0.025
/
mg/L
< /
2023
2nd 6 ...(Count)
1
Sample Count:
l
Months Sampled :
1
Weeks Sampled:
1
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass /Limit
Average Flow for Month
07/31/2023
S
AstraZeneca0723FIow
08/31/2023
S
AstraZeneca0823F1ow
09/30/2023
S
AstraZeneca0923F1ow
10/31/2023
S
AstraZenecal023F1ow
11/30/2023
S
AstraZeneca1123F1ow
12/31/2023
S
AstraZenecal223F1ow
Jul 2023
Week 4
Aug 2023
Week 4
Sep 2023
Week 4
Oct 2023
Week 4
Nov 2023
Week 4
Dec 2023
Week 4
Ju12023
Average
Aug 2023
Average
Sep 2023
Average
Oct 2023
Average
Nov 2023
Average
Dec 2023
Average
2023
Quarter 3
2023
Quarter 4
2023
2nd 6 Months (Avg)
2023
2nd 6 ...(Max)
0.000104
/
MGD /
0.000545
/
MGD /
0.000806
/
MGD /
0.003033
/
MGD /
0.002213
/
MGD /
0.002174
/
MGD /
0.000104
/
MGD /
0.000545
/
MGD /
0.000806
/
MGD /
0.003033
/
MGD /
0.002213
/
MGD /
0.002174
/
MGD /
0.000104
/ 0.002
MGD /
0.000545
/ 0.002
MGD /
0.000806
/ 0.002
MGD /
0.003033
/ 0.002
MGD * /
0.002213
/ 0.002
MGD * /
0.002174
/ 0.002
MGD * /
0.000485
/
MGD /
0.002473
/
MGD /
0.001479
/
MGD /
0.003033
/
MGD /
Tuesday, February 13, 2024 1:26:02PM * Indicates Violation ** Indicates TRC Violation Page 1 of 5

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
2023
2nd 6 ...(Min)
0.000104
/
MGD
/
2023
2nd 6 ...(Count)
6
/
/
Sample Count : 6
Months Sampled:
6
Weeks Sampled:
6
Quarters Sampled :
2
# Over Daily C:
0 0.00
# Over Mo Avg C :
3
50.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
COD
08/29/2023 S
AstraZeneca082923Se1
<
7.5
/
mg/L
<
/
f
09/15/2023 P
AstraZeneca091523P0
<
7.5
/
mg/L
<
/
TW
Aug 2023
Week 4
<
7.5
/
mg/L
<
/
Sep 2023
Week 3
<
7.5
/
mg/L
<
/
Aug 2023
Average
<
7.5
/
mg/L
<
/
Sep 2023
Average
<
7.5
/
mg/L
<
/
2023
Quarter 3
<
7.5
/
mg/L
<
/
2023
2nd 6 Months (Avg) <
7.5
/
mg/L
<
/
2023
2nd 6 ...(Max)
<
7.5
/
mg/L
<
/
2023
2nd 6 ...(Min)
<
7.5
/
mg/L
<
/
2023
2nd 6 ...(Count)
2
/
/
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
08/29/2023
S AStraZeneca082923Sel
<
0.005
/ 20.7
mg/L
< /
f
Aug 2023
Week 4
<
0.005
/
mg/L
< /
Aug 2023
Average
<
0.005
/ 8.2
mg/L
< /
2023
Quarter 3
<
0.005
/
mg/L
< /
2023
2nd 6 Months (Avg)
<
0.005
/
mg/L
< /
2023
2nd 6 ...(Max)
<
0.005
/
mg/L
< /
2023
2nd 6 ...(Min)
<
0.005
/
mg/L
< /
2023
2nd 6 ...(Count)
1
/
/
Tuesday, February 13, 2024 1:26:02PM * Indicates Violation ** Indicates TRC Violation Page 2 of 5

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
1
Months Sampled :
1
Weeks Sampled:
1
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
08/29/2023 S
AstraZeneca082923Sel
<
0.005
/ 20.7
mg/L
<
/
f
Aug 2023
Week 4
<
0.005
/
mg/L
<
/
Aug 2023
Average
<
0.005
/ 8.2
mg/L
<
/
2023
Quarter 3
<
0.005
/
mg/L
<
/
2023
2nd 6 Months (Avg) <
0.005
/
mg/L
<
/
2023
2nd 6 ...(Max)
<
0.005
/
mg/L
<
/
2023
2nd 6 ...(Min)
<
0.005
/
mg/L
<
/
2023
2nd 6 ...(Count)
1
Sample Count: 1
Months Sampled:
l
Weeks Sampled :
1
Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C:
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury - LL
09/29/2023 S
AstraZeneca082923Sel
<
0.000001
/ 0.000142
mg/L < /
fHg
09/15/2023 P
AstraZeneca091523PO
0.000001
/ 0.000142
mg/L /
TWHg
Aug 2023
Week 4
<
0.000001
/
mg/L < /
Sep 2023
Week 3
0.000001
/
mg/L /
Aug 2023
Average
<
0.000001
/
mg/L < /
Sep 2023
Average
0.000001
/
mg/L /
2023
Quarter 3
<
0.000001
/
mg/L < /
2023
2nd 6 Months (Avg)
<
0.000001
/
mg/L < /
2023
2nd 6 ...(Max)
0.000001
/
mg/L /
2023
2nd 6 ...(Min)
<
0.000001
/
mg/L < /
2023
2nd 6 ...(Count)
2
Tuesday, February 13, 2024 1:26:02PM * Indicates Violation ** Indicates TRC Violation Page 3 of 5

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
2
Months Sampled :
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
08/29/2023 S
AstraZeneca082923Sel
<
0.005
/ 3.0
mg/L
<
/
f
Aug 2023
Week 4
<
0.005
/
mg/L
<
/
Aug 2023
Average
<
0.005
/ 0.7
mg/L
<
/
2023
Quarter 3
<
0.005
/
mg/L
<
/
2023
2nd 6 Months (Avg) <
0.005
/
mg/L
<
/
2023
2nd 6 ...(Max)
<
0.005
/
mg/L
<
/
2023
2nd 6 ...(Min)
<
0.005
/
mg/L
<
/
2023
2nd 6 ...(Count)
1
Sample Count:
1
Months Sampled:
l
Weeks Sampled :
1
Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C:
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
09/29/2023 S
AstraZeneca082923Sel
<
0.005
/ 20.7
mg/L
< /
f
Aug 2023
Week 4
<
0.005
/ 8.2
mg/L
< /
Aug 2023
Average
<
0.005
/
mg/L
< /
2023
Quarter 3
<
0.005
/
mg/L
< /
2023
2nd 6 Months (Avg)
<
0.005
/
mg/L
< /
2023
2nd 6 ...(Max)
<
0.005
/
mg/L
< /
2023
2nd 6 ...(Min)
<
0.005
/
mg/L
< /
2023
2nd 6 ...(Count)
1
Tuesday, February 13, 2024 1:26:02PM * Indicates Violation ** Indicates TRC Violation Page 4 of 5

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
1
Months Sampled :
1
Weeks Sampled:
1
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
PH
08/29/2023 S
AstraZeneca082923Sel
6.9
/ 6.0 - 10.0
SU
/
f
09/15/2023 P
AstraZeneca091523PO
7.2
/ 6.0 - 10.0
SU
/
TW
Aug 2023
Week 4
6.9
/
SU
/
Sep 2023
Week 3
7.2
/
SU
/
Aug 2023
Average
6.9
/
SU
/
Sep 2023
Average
7.2
/
Su
/
2023
Quarter 3
7.05
/
SU
/
2023
2nd 6 Months (Avg)
7.05
/
SU
/
2023
2nd 6 ...(Max)
7.2
/
SU
/
2023
2nd 6 ...(Min)
6.9
/
SU
/
2023
2nd 6 ...(Count)
2
Sample Count: 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C:
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Tuesday, February 13, 2024 1:26:02PM * Indicates Violation ** Indicates TRC Violation Page 5 of 5

Aurobindo USA
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
09/29/2023 S
Aurobindo092923Self
0.139
/ 5.59
mg/L
/
Sep 2023
Week 4
0.139
/
mg/L
/
Sep 2023
Average
0.139
/ 2.21
mg/L
/
2023
Quarter 3
0.139
/
mg/L
/
2023
2nd 6 Months (Avg)
0.139
/
mg/L
/
2023
2nd 6 ...(Max)
0.139
/
mg/L
/
2023
2nd 6 ...(Min)
0.139
/
mg/L
/
2023
2nd 6 •..(Count)
I
Sample Count: 1 Months Sampled:
1
Weeks Sampled:
1
Quarters Sampled :
1
# Over Daily C :
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC: 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass /Limit
Ammonia
09/29/2023
S Aurobindo092923Self
1.3
/ mg/L
/
10/24/2023
P Aurobindol02423POT
14.3
/ mg/L
/
W
Sep 2023
Week 4
1.3
/ mg/L
/
Oct 2023
Week 4
14.3
/ mg/L
/
Sep 2023
Average
1.3
/ mg/L
/
Oct 2023
Average
14.3
/ mg/L
/
2023
Quarter 3
1.3
/ mg/L
/
2023
Quarter 4
14.3
/ mg/L
/
2023
2nd 6 Months (Avg)
7.8
/ mg/L
/
2023
2nd 6 ...(Max)
14.3
/ mg/L
/
2023
2nd 6 ...(Min)
1.3
/ mg/L
/
2023
2nd 6 ...(Count)
2
/
/
Sample Date SamplelD Result/Limit Mass /Croat
Average Flow for Month
07/24/2023
S
Aurobindo0723FIow
08/17/2023
S
Aurobindo0823F1ow
09/21/2023
S
Aurobindo0923FIow
10/31/2023
S
Aurobindo1023F1ow
11/16/2023
S
Aurobindoll23F1ow
12/20/2023
S
Aurobindol223F1ow
Aug 2023
Week 3
0.002594 /
MGD /
0.002658 /
MGD /
0.002586 /
MGD /
0.005458 /
MGD /
0.003298 /
MGD /
0.008311 /
MGD /
0.002658 /
MGD /
Saturday, February 24, 2024 10:58:57AM * Indicates Violation ** Indicates TRC Violation Page 1 of 11

Aurobindo USA
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
Jul 2023
Week 4
0.002594
/
MGD /
Sep 2023
Week 3
0.002586
/
MGD /
Oct 2023
Week 4
0.005458
/
MGD /
Nov 2023
Week 3
0.003298
/
MGD /
Dec 2023
Week 3
0.008311
/
MGD /
Jul 2023
Average
0.002594
/ 0.039
MGD /
Aug 2023
Average
0.002658
/ 0.039
MGD /
Sep 2023
Average
0.002586
/ 0.039
MGD /
Oct 2023
Average
0.005458
/ 0.039
MGD /
Nov 2023
Average
0.003298
/ 0.039
MGD /
Dec 2023
Average
0.008311
/ 0.039
MGD /
2023
Quarter 3
0.002613
/
MGD /
2023
Quarter 4
0.005689
/
MGD /
2023
2nd 6 Months (Avg)
0.004151
/
MGD /
2023
2nd 6 ...(Max)
0.008311
/
MGD /
2023
2nd 6 ...(Min)
0.002586
/
MGD /
2023
2nd 6 ...(Count)
6
Sample Count:
6
Months Sampled:
6
Weeks Sampled:
6
Quarters Sampled :
2
# Over Daily C:
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass /Limit
BOD
09/29/2023
S Aurobindo092923Self
42
/ mg/L /
10/24/2023
P Aurobindo102423POT
86.8
/ mg/L /
W
Sep 2023
Week 4
42
/ mg/L /
Oct 2023
Week 4
86.8
/ mg/L /
Sep 2023
Average
42
/ mg/L /
Oct 2023
Average
86.8
/ mg/L /
2023
Quarter 3
42
/ mg/L /
2023
Quarter 4
86.8
/ mg/L /
2023
2nd 6 Months (Avg)
64.4
/ mg/L /
2023
2nd 6 ...(Max)
86.8
/ mg/L /
2023
2nd 6 ...(Min)
42
/ mg/L /
2023
2nd 6 ...(Count)
2
Saturday, February 24, 2024 10:58:57AM * Indicates Violation ** Indicates TRC Violation Page 2 of 11

Aurobindo USA
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
09/29/2023
S Aurobindo092923Self
<
0.00008 /
mg/L
<
/
10/24/2023
P Aurobindo102423POT
<
0.00008 /
mg/L
<
/
W
Sep 2023
Week 4
<
0.00008 /
mg/L
<
/
Oct 2023
Week 4
<
0.00008 /
mg/L
<
/
Sep 2023
Average
<
0.00008 /
mg/L
<
/
Oct 2023
Average
<
0.00008 /
mg/L
<
/
2023
Quarter 3
<
0.00008 /
mg/L
<
/
2023
Quarter 4
<
0.00008 /
mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.00008 /
mg/L
<
/
2023
2nd 6 ...(Max)
<
0.00008 /
mg/L
<
/
2023
2nd 6 ...(Min)
<
0.00008 /
mg/L
<
/
2023
2nd 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
09/29/2023
S Aurobindo092923Self
47.6
/ mg/L
/
10/24/2023
P Aurobindo102423POT
1210
/ mg/L
/
W
Sep 2023
Week 4
47.6
/ mg/L
/
Oct 2023
Week 4
1210
/ mg/L
/
Sep 2023
Average
47.6
/ mg/L
/
Oct 2023
Average
1210
/ mg/L
/
2023
Quarter 3
47.6
/ mg/L
/
2023
Quarter 4
1210
/ mg/L
/
2023
2nd 6 Months (Avg)
628.8
/ mg/L
/
2023
2nd 6 ...(Max)
1210
/ mg/L
/
2023
2nd 6 ...(Min)
47.6
/ mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
COD
09/29/2023
S Aurobindo092923Self
10/24/2023
P Aurobindo102423POT
W
Sep 2023
Week 4
Oct 2023
Week 4
Sep 2023
Average
Oct 2023
Average
2023
Quarter 3
2023
Quarter 4
2023
2nd 6 Months (Avg)
2023
2nd 6 ...(Max)
Saturday, February 24, 2024 10:58:57AM
81 /
mg/L /
1100 /
mg/L /
81 /
mg/L /
1100 /
mg/L /
81 /
mg/L /
1100 /
mg/L /
81 /
mg/L /
1100 /
mg/L /
590.5 /
mg/L /
1100 /
mg/L /
* Indicates Violation
** Indicates TRC Violation
Page 3 of 11

Aurobindo USA
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
COD
2023
2nd 6 ...(Min)
81 /
mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
Copper
09/29/2023
S
Aurobindo092923Self
0.027 /
mg/L
/
10/24/2023
P
Aurobindol02423POT
0.206 /
mg/L
/
W
Sep 2023
Week 4
0.027 /
mg/L
/
Oct 2023
Week 4
0.206 /
mg/L
/
Sep 2023
Average
0.027 /
mg/L
/
Oct 2023
Average
0.206 /
mg/L
/
2023
Quarter 3
0.027 /
mg/L
/
2023
Quarter 4
0.206 /
mg/L
/
2023
2nd 6 Months (Avg)
0.117 /
mg/L
/
2023
2nd 6 ...(Max)
0.206 /
mg/L
/
2023
2nd 6 ...(Min)
0.027 /
mg/L
/
2023
2nd 6 ...(Count)
2 /
/
Sample Date
SamplelD
Result/Limit
Mass/Limit
Cyanide
09/29/2023
S
Aurobindo092923Self
<
0.003 /
mg/L
<
/
10/24/2023
P
Aurobindo102423POT
<
0.003 /
mg/L
<
/
W
Sep 2023
Week 4
<
0.003 /
mg/L
<
/
Oct 2023
Week 4
<
0.003 /
mg/L
<
/
Sep 2023
Average
<
0.003 /
mg/L
<
/
Oct 2023
Average
<
0.003 /
mg/L
<
/
2023
Quarter 3
<
0.003 /
mg/L
<
/
2023
Quarter 4
<
0.003 /
mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.003 /
mg/L
<
/
2023
2nd 6 ...(Max)
<
0.003 /
mg/L
<
/
2023
2nd 6 ...(Min)
<
0.003 /
mg/L
<
/
2023
2nd 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
Ethyl acetate
09/29/2023
S
Aurobindo092923Self
<
0.005 / 5.59
mg/L
<
/
Sep 2023
Week 4
<
0.005 /
mg/L
<
/
Sep 2023
Average
<
0.005 / 2.21
mg/L
<
/
2023
Quarter 3
<
0.005 /
mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.005 /
mg/L
<
/
Saturday, February 24, 2024 10:58:57AM * Indicates Violation ** Indicates TRC Violation Page 4 of 11

Aurobindo USA
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
2023
2nd 6
...(Max)
< 0.005 /
mg/L <
/
2023
2nd 6
...(Min)
< 0.005 /
mg/L <
/
2023
2nd 6
...(Count)
1
Sample Count:
1
Months Sampled:
1
Weeks Sampled:
1
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
09/29/2023
S Aurobindo092923Self
0.76
/ mg/L
/
10/24/2023
P Aurobindo102423POT
0.65
/ mg/L
/
W
Sep 2023
Week 4
0.76
/ mg/L
/
Oct 2023
Week 4
0.65
/ mg/L
/
Sep 2023
Average
0.76
/ mg/L
/
Oct 2023
Average
0.65
/ mg/L
/
2023
Quarter 3
0.76
/ mg/L
/
2023
Quarter 4
0.65
/ mg/L
/
2023
2nd 6 Months (Avg)
0.71
/ mg/L
/
2023
2nd 6 ...(Max)
0.76
/ mg/L
/
2023
2nd 6 ...(Min)
0.65
/ mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
09/29/2023 S
Aurobindo092923Self
<
0.005
/ 5.59
mg/L
< /
Sep 2023
Week 4
<
0.005
/
mg/L
< /
Sep 2023
Average
<
0.005
/ 2.21
mg/L
< /
2023
Quarter 3
<
0.005
/
mg/L
< /
2023
2nd 6 Months (Avg)
<
0.005
/
mg/L
< /
2023
2nd 6 ...(Max)
<
0.005
/
mg/L
< /
2023
2nd 6 ...(Min)
<
0.005
/
mg/L
< /
2023
2nd 6 ...(Count)
1
/
/
Saturday, February 24, 2024 10:58:57AM * Indicates Violation ** Indicates TRC Violation Page 5 of 11

Aurobindo USA
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
1
Months Sampled :
1
Weeks Sampled:
1
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury - LL
09/29/2023 S
Aurobindo092923Self 0.000031
/ 0.000142
mg/L
/
10/24/2023 P
Aurobindo102423POT 0.000004
/ 0.000142
mg/L
/
WHg
Sep 2023
Week 4
0.000031
/
mg/L
/
Oct 2023
Week 4
0.000004
/
mg/L
/
Sep 2023
Average
0.000031
/
mg/L
/
Oct 2023
Average
0.000004
/
mg/L
/
2023
Quarter 3
0.000031
/
mg/L
/
2023
Quarter 4
0.000004
/
mg/L
/
2023
2nd 6 Months (Avg) 0.000018
/
mg/L
/
2023
2nd 6 ...(Max)
0.000031
/
mg/L
/
2023
2nd 6 ...(Min)
0.000004
/
mg/L
/
2023
2nd 6 ...(Count)
2
/
/
Sample Count: 2
Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
2
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass /Limit
Methylene Chloride
09/29/2023 S
Aurobindo092923Self <
Sep 2023
Week 4 <
Sep 2023
Average <
2023
Quarter 3 <
2023
2nd 6 Months (Avg) <
2023
2nd 6 ...(Max) <
2023
2nd 6 ...(Min) <
2023
2nd 6 ...(Count)
0.005
/ 0.81
mg/L
< /
0.005
/
mg/L
< /
0.005
/ 0.18
mg/L
< /
0.005
/
mg/L
< /
0.005
/
mg/L
< /
0.005
/
mg/L
< /
0.005
/
mg/L
< /
1
Saturday, February 24, 2024 10:58:57AM * Indicates Violation ** Indicates TRC Violation Page 6 of 11

Aurobindo USA
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
1
Months Sampled :
1
Weeks Sampled:
1
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
09/29/2023 S
Aurobindo092923Self
<
0.001
/ mg/L
<
/
10/24/2023 P
Aurobindo102423POT
<
0.001
/ mg/L
<
/
W
Sep 2023
Week 4
<
0.001
/ mg/L
<
/
Oct 2023
Week 4
<
0.001
/ mg/L
<
/
Sep 2023
Average
<
0.001
/ mg/L
<
/
Oct 2023
Average
<
0.001
/ mg/L
<
/
2023
Quarter 3
<
0.001
/ mg/L
<
/
2023
Quarter 4
<
0.001
/ mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.001
/ mg/L
<
/
2023
2nd 6 ...(Max)
<
0.001
/ mg/L
<
/
2023
2nd 6 ...(Min)
<
0.001
/ mg/L
<
/
2023
2nd 6 ...(Count)
2
/
/
Sample Date SamplelD Result/Limit Mass /Limit
n-Amyl acetate
09/29/2023 S
Aurobindo092923Self <
0.005
/ 5.59
mg/L
<
/
Sep 2023
Week 4
<
0.005
/
mg/L
<
/
Sep 2023
Average
<
0.005
/ 2.21
mg/L
<
/
2023
Quarter 3
<
0.005
/
mg/L
<
/
2023
2nd 6 Months (Avg) <
0.005
/
mg/L
<
/
2023
2nd 6 ...(Max)
<
0.005
/
mg/L
<
/
2023
2nd 6 ...(Min)
<
0.005
/
mg/L
<
/
2023
2nd 6 ...(Count)
1
Sample Count: 1
Months Sampled:
1
Weeks Sampled:
1
Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C:
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Saturday, February 24, 2024 10:58:57AM * Indicates Violation ** Indicates TRC Violation Page 7 of 11

Aurobindo USA
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
Nitrate -Nitrite
09/29/2023
S
Aurobindo092923Self
0.2
/
mg/L
/
10/24/2023
P
Aurobindo102423POT
0.5
/
mg/L
/
W
Sep 2023
Week 4
0.2
/
mg/L
/
Oct 2023
Week 4
0.5
/
mg/L
/
Sep 2023
Average
0.2
/
mg/L
/
Oct 2023
Average
0.5
/
mg/L
/
2023
Quarter 3
0.2
/
mg/L
/
2023
Quarter 4
0.5
/
mg/L
/
2023
2nd 6 Months (Avg)
0.3
/
mg/L
/
2023
2nd 6 ...(Max)
0.5
/
mg/L
/
2023
2nd 6 ...(Min)
0.2
/
mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
Nitrogen, Total
09/29/2023
S
Aurobindo092923Self
5.7
/
mg/L
/
Sep 2023
Week 4
5.7
/
mg/L
/
Sep 2023
Average
5.7
/
mg/L
/
2023
Quarter 3
5.7
/
mg/L
/
2023
2nd 6 Months (Avg)
5.7
/
mg/L
/
2023
2nd 6 ...(Max)
5.7
/
mg/L
/
2023
2nd 6 ...(Min)
5.7
/
mg/L
/
2023
2nd 6 ...(Count)
1
Sample Date
SamplelD
Result/Limit
Mass/Limit
Oil & Grease, Total
09/29/2023
S
Aurobindo092923Self
<
2.5
/ 200
mg/L
<
/
10/24/2023
P
Aurobindo102423POT
<
2.5
/ 200
mg/L
<
/
W
Sep 2023
Week 4
<
2.5
/
mg/L
<
/
Oct 2023
Week 4
<
2.5
/
mg/L
<
/
Sep 2023
Average
<
2.5
/
mg/L
<
/
Oct 2023
Average
<
2.5
/
mg/L
<
/
2023
Quarter 3
<
2.5
/
mg/L
<
/
2023
Quarter 4
<
2.5
/
mg/L
<
/
2023
2nd 6 Months (Avg)
<
2.5
/
mg/L
<
/
2023
2nd 6 ...(Max)
<
2.5
/
mg/L
<
/
2023
2nd 6 ...(Min)
<
2.5
/
mg/L
<
/
2023
2nd 6 ...(Count)
2
Saturday, February 24, 2024 10:58:57AM * Indicates Violation ** Indicates TRC Violation Page 8 of l l

Aurobindo USA
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
2
Months Sampled :
2
Weeks Sampled:
2
Quarters Sampled :
2
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
PH
09/29/2023 S
Aurobindo092923Self
7.3
/ 6.0 - 10.0
SU
/
10/24/2023 P
Aurobindo102423POT
7.4
/ 6.0 - 10.0
SU
/
W
Sep 2023
Week 4
7.3
/
SU
/
Oct 2023
Week 4
7.4
/
SU
/
Sep 2023
Average
7.3
/
Su
/
Oct 2023
Average
7.4
/
SU
/
2023
Quarter 3
7.3
/
SU
/
2023
Quarter 4
7.4
/
SU
/
2023
2nd 6 Months (Avg)
7.35
/
SU
/
2023
2nd 6 ...(Max)
7.4
/
SU
/
2023
2nd 6 ...(Min)
7.3
/
SU
/
2023
2nd 6 ...(Count)
2
Sample Count: 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
2
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass /Limit
Temperature
09/29/2023
S Aurobindo092923Self
21
/ 66
°C /
10/24/2023
P Aurobindo102423POT
18
/ 66
°C /
W
Sep 2023
Week 4
21
/
°C /
Oct 2023
Week 4
18
/
°C /
Sep 2023
Average
21
/
°C /
Oct 2023
Average
18
/
°C /
2023
Quarter
21
/
°C /
2023
Quarter 4
18
/
°C /
2023
2nd 6 Months (Avg)
19.5
/
°C /
2023
2nd 6 ...(Max)
21
/
°C /
Saturday, February 24, 2024 10:58:57AM * Indicates Violation ** Indicates TRC Violation Page 9 of 11

Aurobindo USA
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
2023
2nd 6 ...(Min)
18
/
°C
/
2023
2nd 6 ...(Count)
2
/
/
Sample Count : 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
2
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
TKN
09/29/2023 S
Aurobindo092923Self
5.5
/
mg/L
/
10/24/2023 P
Aurobindol02423POT
26.2
/
mg/L
/
W
Sep 2023
Week 4
5.5
/
mg/L
/
Oct 2023
Week 4
26.2
/
mg/L
/
Sep 2023
Average
5.5
/
mg/L
/
Oct 2023
Average
26.2
/
mg/L
/
2023
Quarter 3
5.5
/
mg/L
/
2023
Quarter 4
26.2
/
mg/L
/
2023
2nd 6 Months (Avg)
15.85
/
mg/L
/
2023
2nd 6 ...(Max)
26.2
/
mg/L
/
2023
2nd 6 ...(Min)
5.5
/
mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
09/29/2023 S
Aurobindo092923Self
1.48 /
mg/L /
10/24/2023 P
Aurobindo102423POT
7.39 /
mg/L /
W
Sep 2023
Week 4
1.48 /
mg/L /
Oct 2023
Week 4
7.39 /
mg/L /
Sep 2023
Average
1.48 /
mg/L /
Oct 2023
Average
7.39 /
mg/L /
2023
Quarter 3
1.48 /
mg/L /
2023
Quarter 4
7.39 /
mg/L /
2023
2nd 6 Months (Avg)
4.435 /
mg/L /
2023
2nd 6 ...(Max)
7.39 /
mg/L /
2023
2nd 6 ...(Min)
1.48 /
mg/L /
2023
2nd 6 ...(Count)
2
Saturday, February 24, 2024 10:58:57AM * Indicates Violation ** Indicates TRC Violation Page 10 of 11

Aurobindo USA
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
TSS
09/29/2023
S
Aurobindo092923Self
15 /
mg/L
/
10/24/2023
P
Aurobindo102423POT
70 /
mg/L
/
W
Sep 2023
Week 4
15 /
mg/L
/
Oct 2023
Week 4
70 /
mg/L
/
Sep 2023
Average
15 /
mg/L
/
Oct 2023
Average
70 /
mg/L
/
2023
Quarter 3
15 /
mg/L
/
2023
Quarter 4
70 /
mg/L
/
2023
2nd 6 Months (Avg)
42.5 /
mg/L
/
2023
2nd 6 ...(Max)
70 /
mg/L
/
2023
2nd 6 ...(Min)
15 /
mg/L
/
2023
2nd 6 ...(Count)
2 /
/
Sample Date
SamplelD
Result/Limit
Mass/Limit
VOC
09/29/2023
S
Aurobindo092923Self
0.153 /
mg/L
/
Sep 2023
Week 4
0.153 /
mg/L
/
Sep 2023
Average
0.153 /
mg/L
/
2023
Quarter 3
0.153 /
mg/L
/
2023
2nd 6 Months (Avg)
0.153 /
mg/L
/
2023
2nd 6 ...(Max)
0.153 /
mg/L
/
2023
2nd 6 ...(Min)
0.153 /
mg/L
/
2023
2nd 6 ...(Count)
1 /
/
Sample Date
SamplelD
Result/Limit
Mass/Limit
Zinc
09/29/2023
S
Aurobindo092923Self
0.223 /
mg/L
/
10/24/2023
P
Aurobindo102423POT
1.06 /
mg/L
/
W
Sep 2023
Week 4
0.223 /
mg/L
/
Oct 2023
Week 4
1.06 /
mg/L
/
Sep 2023
Average
0.223 /
mg/L
/
Oct 2023
Average
1.06 /
mg/L
/
2023
Quarter 3
0.223 /
mg/L
/
2023
Quarter 4
1.06 /
mg/L
/
2023
2nd 6 Months (Avg)
0.642 /
mg/L
/
2023
2nd 6 ...(Max)
1.06 /
mg/L
/
2023
2nd 6 ...(Min)
0.223 /
mg/L
/
2023
2nd 6 ...(Count)
2
Saturday, February 24, 2024 10:58:57AM * Indicates Violation ** Indicates TRC Violation Page 11 of 11

Biogen
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
07/25/2023 P
Biogen072523POTW <
0.025
/ 12.19
mg/L
<
0.0254 /
lbs/day
Jul 2023
Week 4
<
0.025
/
mg/L
<
0.0254 /
lbs/day
Jul 2023
Average
<
0.025
/ 4.83
mg/L
<
0.0254 /
lbs/day
2023
Quarter 3
<
0.025
/
mg/L
<
0.0254 /
Ibs/day
2023
2nd 6 Months (Avg) <
0.025
/
mg/L
<
0.0254 /
Ibs/day
2023
2nd 6 ...(Max)
<
0.025
/
mg/L
<
0.0254 /
Ibs/day
2023
2nd 6 ...(Min)
<
0.025
/
mg/L
<
0.0254 /
Ibs/day
2023
2nd 6 •..(Count)
I
/
I /
Sample Count: 1
Months Sampled:
1
Weeks Sampled:
1 Quarters Sampled :
1
# Over Daily C :
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00 # Over Qt Avg C :
0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC:
0
0.00 # Over Qt Avg C TRC
: 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00 # Over Qtr Avg M :
0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass /Limit
Ammonia
07/25/2023
P Biogen072523POTW
1.5
/ mg/L
1.5221
/ Ibs/day
08/30/2023
S Biogen083023Self
1.02
/ mg/L
1.0421
/ Ibs/day
Jul 2023
Week 4
1.5
/ mg/L
1.5221
/ Ibs/day
Aug 2023
Week 4
1.02
/ mg/L
1.0421
/ lbs/day
Jul 2023
Average
1.5
/ mg/L
1.5221
/ lbs/day
Aug 2023
Average
1.02
/ mg/L
1.0421
/ lbs/day
2023
Quarter 3
1.26
/ mg/L
1.2821
/ lbs/day
2023
2nd 6 Months (Avg)
1.26
/ mg/L
1.2821
/ Ibs/day
2023
2nd 6 ...(Max)
1.5
/ mg/L
1.5221
/ Ibs/day
2023
2nd 6 ...(Min)
1.02
/ mg/L
1.0421
/ Ibs/day
2023
2nd 6 ...(Count)
2
/
2
/
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2023
S
Biogen0723F1ow
08/31/2023
S
Biogen0823F1ow
09/30/2023
S
Biogen0923F1ow
10/31/2023
S
Biogen1023F1ow
11/30/2023
S
Biogen1123FIow
12/31/2023
S
Biogenl223Flow
Jul 2023
Week 4
Aug 2023
Week 4
0.121188
/ MGD /
0.124079
/ MGD /
0.08442
/ MGD /
0.107209
/ MGD /
0.09239
/ MGD /
0.050747
/ MGD /
0.121188
/ MGD /
0.124079
/ MGD /
Tuesday, February 13, 2024 2:31:58PM * Indicates Violation ** Indicates TRC Violation Page 1 of 11

Biogen
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
Sep 2023
Week 4
0.08442
/
MGD /
Oct 2023
Week 4
0.107209
/
MGD /
Nov 2023
Week 4
0.09239
/
MGD /
Dec 2023
Week 4
0.050747
/
MGD /
Jul 2023
Average
0.121188
/
MGD /
Aug 2023
Average
0.124079
10.150
MGD /
Sep 2023
Average
0.08442
10.150
MGD /
Oct 2023
Average
0.107209
10.150
MGD /
Nov 2023
Average
0.09239
10.150
MGD /
Dec 2023
Average
0.050747
10.150
MGD /
2023
Quarter 3
0.121188
/
MGD /
2023
Quarter 3
0.10425
/
MGD /
2023
Quarter 3
0.121188
/
MGD /
2023
Quarter 3
0.10425
/
MGD /
2023
Quarter 4
0.083449
/
MGD /
2023
2nd 6 Months (Avg)
0.096672
/
MGD /
2023
2nd 6 ...(Max)
0.124079
/
MGD /
2023
2nd 6 ...(Min)
0.050747
/
MGD /
2023
2nd 6 ...(Count)
6
Sample Count :
6
Months Sampled :
6
Weeks Sampled :
6
Quarters Sampled :
5
# Over Daily C :
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
BOD
07/25/2023
P Biogen072523POTW
53.5
/ mg/L
54.288 /
lbs/day
08/30/2023
S Biogen083023Self
43.6
/ mg/L
44.544 /
lbs/day
Jul 2023
Week 4
53.5
/ mg/L
54.288 /
lbs/day
Aug 2023
Week 4
43.6
/ mg/L
44.544 /
lbs/day
Jul 2023
Average
53.5
/ mg/L
54.288 /
Ibs/day
Aug 2023
Average
43.6
/ mg/L
44.544 /
Ibs/day
2023
Quarter 3
48.6
/ mg/L
49.416 /
Ibs/day
2023
2nd 6 Months (Avg)
48.6
/ mg/L
49.416 /
Ibs/day
2023
2nd 6 ...(Max)
53.5
/ mg/L
54.288 /
lbs/day
2023
2nd 6 ...(Min)
43.6
/ mg/L
44.544 /
lbs/day
2023
2nd 6 ...(Count)
2
/
2 /
Tuesday, February 13, 2024 2:31:58PM * Indicates Violation ** Indicates TRC Violation Page 2 of 11

Biogen
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
07/25/2023
P Biogen072523POTW
<
0.00008
/
mg/L
<
0.000076 /
lbs/day
Jul 2023
Week 4
<
0.00008
/
mg/L
<
0.000076 /
lbs/day
Jul 2023
Average
<
0.00008
/
mg/L
<
0.000076 /
lbs/day
2023
Quarter 3
<
0.00008
/
mg/L
<
0.000076 /
Ibs/day
2023
2nd 6 Months (Avg)
<
0.00008
/
mg/L
<
0.000076 /
Ibs/day
2023
2nd 6 ...(Max)
<
0.00008
/
mg/L
<
0.000076 /
Ibs/day
2023
2nd 6 ...(Min)
<
0.00008
/
mg/L
<
0.000076 /
Ibs/day
2023
2nd 6 ...(Count)
1
/
1 /
Sample Date
SamplelD
Result/Limit
Mass/Limit
Chloride
07/25/2023
P Biogen072523POTW
75
/
mg/L
76.1052 /
Ibs/day
08/30/2023
S Biogen083023Self
128
/
mg/L
130.7712 /
lbs/day
Jul 2023
Week 4
75
/
mg/L
76.1052 /
lbs/day
Aug 2023
Week 4
128
/
mg/L
130.7712 /
lbs/day
Jul 2023
Average
75
/
mg/L
76.1052 /
lbs/day
Aug 2023
Average
128
/
mg/L
130.7712 /
Ibs/day
2023
Quarter 3
101.5
/
mg/L
103.4382 /
Ibs/day
2023
2nd 6 Months (Avg)
101.5
/
mg/L
103.438 /
Ibs/day
2023
2nd 6 ...(Max)
128
/
mg/L
130.7712 /
Ibs/day
2023
2nd 6 ...(Min)
75
/
mg/L
76.1052 /
lbs/day
2023
2nd 6 ...(Count)
2
/
2 /
Sample Date SamplelD Result/Limit Mass/Limit
COD
07/25/2023
P Biogen072523POTW
190
/ mg/L
192.8 /
lbs/day
08/30/2023
S Biogen083023Self
92.9
/ mg/L
94.91 /
Ibs/day
Jul 2023
Week 4
190
/ mg/L
192.8 /
Ibs/day
Aug 2023
Week 4
92.9
/ mg/L
94.91 /
Ibs/day
Jul 2023
Average
190
/ mg/L
192.8 /
Ibs/day
Aug 2023
Average
92.9
/ mg/L
94.91 /
Ibs/day
2023
Quarter 3
141.5
/ mg/L
143.86 /
Ibs/day
2023
2nd 6 Months (Avg)
141.5
/ mg/L
143.86 /
lbs/day
2023
2nd 6 ...(Max)
190
/ mg/L
192.80 /
lbs/day
2023
2nd 6 ...(Min)
92.9
/ mg/L
94.91 /
lbs/day
2023
2nd 6 ...(Count)
2
/
2 /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
07/25/2023 P Biogen072523POTW <
08/30/2023 S Biogen083023Self <
Tuesday, February 13, 2024 2:31:58PM
0.003 10.05 mg/L < 0.002537 /
0.005 / 0.05 mg/L < 0.005108 /
* Indicates Violation ** Indicates TRC Violation
Ibs/day
Ibs/day
Page 3 of 11

Biogen
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
Jul 2023
Week 4
<
0.003
/
mg/L
<
0.002537 /
lbs/day
Aug 2023
Week 4
<
0.005
/
mg/L
<
0.005108 /
lbs/day
Jul 2023
Average
<
0.003
/ 0.04
mg/L
<
0.002537 /
lbs/day
Aug 2023
Average
<
0.005
/ 0.04
mg/L
<
0.005108 /
Ibs/day
2023
Quarter 3
<
0.004
/
mg/L
<
0.003823 /
Ibs/day
2023
2nd 6 Months (Avg) <
0.004
/
mg/L
<
0.003823 /
Ibs/day
2023
2nd 6 ...(Max)
<
0.005
/
mg/L
<
0.005108 /
Ibs/day
2023
2nd 6 ...(Min)
<
0.003
/
mg/L
<
0.002537 /
Ibs/day
2023
2nd 6 ...(Count)
2
/
2 /
Sample
Count : 2
Months Sampled:
2
Weeks Sampled:
2 Quarters
Sampled :
I
# Over Daily C :
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00 # Over Qt Avg C :
0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC:
0
0.00 # Over Qt Avg C TRC
: 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M:
0
0.00
# Over Wk Avg M :
0
0.00 # Over Qtr Avg M :
0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Diroximel fumarate
08/10/2023 S
Biogen081023SelfDRF
<
0.024
/ mg/L
<
0.03 / Ibs/day
10/20/2023 S
Biogen102023SelfDRF
0.035
/ mg/L
0.03 / Ibs/day
Aug 2023
Week 2
<
0.024
/ mg/L
<
0.03 /
Oct 2023
Week 3
0.035
/ mg/L
0.03 /
Aug 2023
Average
<
0.024
/ mg/L
<
0.03 /
Oct 2023
Average
0.035
/ mg/L
0.03 /
2023
Quarter 3
<
0.024
/ mg/L
<
0.03 /
2023
Quarter 4
0.035
/ mg/L
0.03 /
2023
2nd 6 Months (Avg)
<
0.030
/ mg/L
<
0.03 /
2023
2nd 6 ...(Max)
0.035
/ mg/L
0.03 /
2023
2nd 6 ...(Min)
<
0.024
/ mg/L
<
0.03 /
2023
2nd 6 ...(Count)
2
/
2 /
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
07/25/2023
P Biogen072523POTW <
Jul 2023
Week 4 <
Jul 2023
Average <
2023
Quarter <
2023
2nd 6 Months (Avg) <
2023
2nd 6 ...(Max) <
0.005
/ 12.19
mg/L
<
0.0051
/ lbs/day
0.005
/
mg/L
<
0.0051
/ lbs/day
0.005
/ 4.83
mg/L
<
0.0051
/ Ibs/day
0.005
/
mg/L
<
0.0051
/ Ibs/day
0.005
/
mg/L
<
0.0051
/ Ibs/day
0.005
/
mg/L
<
0.0051
/ Ibs/day
Tuesday, February 13, 2024 2:31:58PM * Indicates Violation ** Indicates TRC Violation Page 4 of 11

Biogen
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
2023
2nd 6 ...(Min) <
0.005
/
mg/L <
0.0051 /
Ibs/day
2023
2nd 6 ...(Count)
1
/
1 /
Sample Count : 1 Months Sampled:
1
Weeks Sampled:
1 Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00 # Over Qt Avg C :
0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00 # Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00 # Over Qtr Avg M :
0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
Fluoride
07/25/2023 P
Biogen072523POTW
1.04
/
mg/L
1.0553 /
Ibs/day
08/30/2023 S
Biogen083023Self
0.81
/
mg/L
0.8275 /
lbs/day
Jul 2023
Week 4
1.04
/
mg/L
1.0553 /
lbs/day
Aug 2023
Week 4
0.81
/
mg/L
0.8275 /
lbs/day
Jul 2023
Average
1.04
/
mg/L
1.0553 /
lbs/day
Aug 2023
Average
0.81
/
mg/L
0.8275 /
Ibs/day
2023
Quarter 3
0.93
/
mg/L
0.9414 /
Ibs/day
2023
2nd 6 Months (Avg)
0.93
/
mg/L
0.9414 /
Ibs/day
2023
2nd 6 ...(Max)
1.04
/
mg/L
1.0553 /
Ibs/day
2023
2nd 6 ...(Min)
0.81
/
mg/L
0.8275 /
lbs/day
2023
2nd 6 ...(Count)
2
/
2 /
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
07/25/2023 P
Biogen072523POTW
<
0.005
/ 12.19
mg/L
<
0.0051
/ lbs/day
Jul 2023
Week 4
<
0.005
/
mg/L
<
0.0051
/ lbs/day
Jul 2023
Average
<
0.005
/ 4.83
mg/L
<
0.0051
/ Ibs/day
2023
Quarter 3
<
0.005
/
mg/L
<
0.0051
/ Ibs/day
2023
2nd 6 Months (Avg)
<
0.005
/
mg/L
<
0.0051
/ Ibs/day
2023
2nd 6 ...(Max)
<
0.005
/
mg/L
<
0.0051
/ Ibs/day
2023
2nd 6 ...(Min)
<
0.005
/
mg/L
<
0.0051
/ Ibs/day
2023
2nd 6 ...(Count)
1
/
1
/
Tuesday, February 13, 2024 2:31:58PM * Indicates Violation ** Indicates TRC Violation Page 5 of 11

Biogen
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
1
Months Sampled :
1
Weeks Sampled:
1
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury - LL
07/25/2023 P
Biogen072523POTVM 0.000005
/ 0.000142
mg/L
/
g
08/30/2023 S
Biogen083023Self 0.000001
/ 0.000142
mg/L
/
Jul 2023
Week 4 0.000005
/
mg/L
/
Aug 2023
Week 4 0.000001
/
mg/L
/
Jul 2023
Average 0.000005
/
mg/L
/
Aug 2023
Average 0.000001
/
mg/L
/
2023
Quarter 3 0.000003
/
mg/L
/
2023
2nd 6 Months (Avg) 0.000003
/
mg/L
/
2023
2nd 6 ...(Max) 0.000005
/
mg/L
/
2023
2nd 6 ...(Min) 0.000001
/
mg/L
/
2023
2nd 6 ...(Count) 2
Sample Count : 2 Months Sampled
:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C:
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass /Limit
Methylene Chloride
07/25/2023 P
Biogen072523POTW
<
0.005
/ 1.77
mg/L
<
0.005074 /
Ibs/day
Jul 2023
Week 4
<
0.005
/
mg/L
<
0.005074 /
lbs/day
Jul 2023
Average
<
0.005
/ 0.41
mg/L
<
0.005074 /
Ibs/day
2023
Quarter 3
<
0.005
/
mg/L
<
0.005074 /
lbs/day
2023
2nd 6 Months (Avg)
<
0.005
/
mg/L
<
0.005074 /
lbs/day
2023
2nd 6 ...(Max)
<
0.005
/
mg/L
<
0.005074 /
Ibs/day
2023
2nd 6 ...(Min)
<
0.005
/
mg/L
<
0.005074 /
lbs/day
2023
2nd 6 ...(Count)
1
/
I /
Tuesday, February 13, 2024 2:31:58PM * Indicates Violation ** Indicates TRC Violation Page 6 of 11

Biogen
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
1
Months Sampled :
1
Weeks Sampled:
1
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
07/25/2023 P
Biogen072523POTW <
0.005
/ 12.19
mg/L
<
0.0051 / lbs/day
Jul 2023
Week 4
<
0.005
/
mg/L
<
0.0051 / Ibs/day
Jul 2023
Average
<
0.005
/ 4.83
mg/L
<
0.0051 / Ibs/day
2023
Quarter 3
<
0.005
/
mg/L
<
0.0051 / lbs/day
2023
2nd 6 Months (Avg) <
0.005
/
mg/L
<
0.0051 / lbs/day
2023
2nd 6 ...(Max)
<
0.005
/
mg/L
<
0.0051 / Ibs/day
2023
2nd 6 ...(Min)
<
0.005
/
mg/L
<
0.0051 / Ibs/day
2023
2nd 6 ...(Count)
1
/
I /
Sample Count: 1
Months Sampled:
1
Weeks Sampled:
1 Quarters Sampled :
I
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00 # Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00 # Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00 # Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC:
0
0.00
# Over Wk Avg M TRC :
0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate -Nitrite
07/25/2023 P
Biogen072523POTW
0.2
/ mg/L
0.223 /
lbs/day
08/30/2023 S
Biogen083023Self
0.4
/ mg/L
0.388 /
Ibs/day
Jul 2023
Week 4
0.2
/ mg/L
0.223 /
Ibs/day
Aug 2023
Week 4
0.4
/ mg/L
0.388 /
Ibs/day
Jul 2023
Average
0.2
/ mg/L
0.223 /
Ibs/day
Aug 2023
Average
0.4
/ mg/L
0.388 /
lbs/day
2023
Quarter 3
0.3
/ mg/L
0.306 /
lbs/day
2023
2nd 6 Months (Avg)
0.3
/ mg/L
0.306 /
lbs/day
2023
2nd 6 ...(Max)
0.4
/ mg/L
0.388 /
lbs/day
2023
2nd 6 ...(Min)
0.2
/ mg/L
0.223 /
Ibs/day
2023
2nd 6 ...(Count)
2
/
2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen, Total
Tuesday, February 13, 2024 2:31:58PM * Indicates Violation ** Indicates TRC Violation Page 7 of 11

Biogen
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen, Total
07/25/2023 P
Biogen072523POTW
10.6
/ mg/L
10.756 /
lbs/day
08/30/2023 S
Biogen083023Self
5
/ mg/L
5.108 /
lbs/day
Jul 2023
Week 4
10.6
/ mg/L
10.756 /
lbs/day
Aug 2023
Week 4
5
/ mg/L
5.108 /
Ibs/day
Jul 2023
Average
10.6
/ mg/L
10.756 /
Ibs/day
Aug 2023
Average
5
/ mg/L
5.108 /
Ibs/day
2023
Quarter 3
7.8
/ mg/L
7.932 /
Ibs/day
2023
2nd 6 Months (Avg)
7.8
/ mg/L
7.932 /
Ibs/day
2023
2nd 6 ...(Max)
10.6
/ mg/L
10.756 /
Ibs/day
2023
2nd 6 ...(Min)
5
/ mg/L
5.108 /
lbs/day
2023
2nd 6 ...(Count)
2
/
2 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil & Grease, Total
07/25/2023 P
Biogen072523POTW
9.5
/ 200
mg/L
/
Jul 2023
Week 4
9.5
/
mg/L
/
Jul 2023
Average
9.5
/
mg/L
/
2023
Quarter 3
9.5
/
mg/L
/
2023
2nd 6 Months (Avg)
9.5
/
mg/L
/
2023
2nd 6 ...(Max)
9.5
/
mg/L
/
2023
2nd 6 ...(Min)
9.5
/
mg/L
/
2023
2nd 6 ...(Count)
1
Sample Count : 1 Months Sampled:
1
Weeks Sampled:
1
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
PH
07/25/2023
P Biogen072523POTW
08/30/2023
S Biogen083023Self
Jul 2023
Week 4
Aug 2023
Week 4
Jul 2023
Average
Aug 2023
Average
2023
Quarter 3
2023
2nd 6 Months (Avg)
8.8
1 5.5 - 10.5
SU /
9.05
1 5.5 - 10.5
SU /
8.8
/
SU /
9.05
/
SU /
8.8
/
SU /
9.05
/
SU /
8.93
/
SU /
8.93
/
SU /
Tuesday, February 13, 2024 2:31:58PM * Indicates Violation ** Indicates TRC Violation Page 8 of l l

Biogen
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
PH
2023
2nd 6
...(Max)
9.05 /
SU
/
2023
2nd 6
...(Min)
8.8 /
Su
/
2023
2nd 6
...(Count)
2
Sample Count:
2
Months Sampled :
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
07/25/2023 P
Biogen072523POTW
29
/ 66
°C
/
08/30/2023 S
Biogen083023Self
24.1
/ 66
°C
/
Jul 2023
Week 4
29
/
°C
/
Aug 2023
Week 4
24.1
/
°C
/
Jul 2023
Average
29
/
G
/
Aug 2023
Average
24.1
/
°C
/
2023
Quarter 3
26.6
/
°C
/
2023
2nd 6 Months (Avg)
26.6
/
°C
/
2023
2nd 6 ...(Max)
29
/
°C
/
2023
2nd 6 ...(Min)
24.1
/
°C
/
2023
2nd 6 ...(Count)
2
Sample Count : 2 Months Sampled
:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Muss /Lhnit
TKN
07/25/2023
P Biogen072523POTW
10.4
/ mg/L
10.553 /
lbs/day
08/30/2023
S Biogen083023Self
4.52
/ mg/L
4.618 /
lbs/day
Jul 2023
Week 4
10.4
/ mg/L
10.553 /
Ibs/day
Aug 2023
Week 4
4.52
/ mg/L
4.618 /
Ibs/day
Jul 2023
Average
10.4
/ mg/L
10.553 /
Ibs/day
Tuesday, February 13, 2024 2:31:58PM * Indicates Violation ** Indicates TRC Violation Page 9 of 11

Biogen
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
TKN
Aug 2023
Average
4.52
/
mg/L
4.618 /
lbs/day
2023
Quarter 3
7.46
/
mg/L
7.586 /
lbs/day
2023
2nd 6 Months (Avg)
7.46
/
mg/L
7.586 /
lbs/day
2023
2nd 6 ...(Max)
10.4
/
mg/L
10.553 /
Ibs/day
2023
2nd 6 ...(Min)
4.52
/
mg/L
4.618 /
Ibs/day
2023
2nd 6 ...(Count)
2
/
2 /
Sample Date
SamplelD
Result/Limit
Mass /Limit
Total Phosphorus
07/25/2023
P
Biogen072523POTW
1.29
/
mg/L
1.309 /
Ibs/day
08/30/2023
S
Biogen083023Self
0.28
/
mg/L
0.2861 /
Ibs/day
Jul 2023
Week 4
1.29
/
mg/L
1.309 /
Ibs/day
Aug 2023
Week 4
0.28
/
mg/L
0.2861 /
lbs/day
Jul 2023
Average
1.29
/
mg/L
1.309 /
lbs/day
Aug 2023
Average
0.28
/
mg/L
0.2861 /
lbs/day
2023
Quarter 3
0.785
/
mg/L
0.7975 /
lbs/day
2023
2nd 6 Months (Avg)
0.785
/
mg/L
0.7975 /
Ibs/day
2023
2nd 6 ...(Max)
1.29
/
mg/L
1.3090 /
Ibs/day
2023
2nd 6 ...(Min)
0.28
/
mg/L
0.2861 /
Ibs/day
2023
2nd 6 ...(Count)
2
/
2 /
Sample Date
SamplelD
Result/Limit
Mass/Limit
TSS
07/25/2023
P
Biogen072523POTW
153
/
mg/L
155.254629 /
Ibs/day
08/30/2023
S
Biogen083023Self
18
/
mg/L
18.3897 /
lbs/day
Jul 2023
Week 4
153
/
mg/L
155.254629 /
lbs/day
Aug 2023
Week 4
18
/
mg/L
18.3897 /
Ibs/day
Jut 2023
Average
153
/
mg/L
155.254629 /
Ibs/day
Aug 2023
Average
18
/
mg/L
18.3897 /
Ibs/day
2023
Quarter 3
85.5
/
mg/L
86.822165 /
Ibs/day
2023
2nd 6 Months (Avg)
85.5
/
mg/L
86.8222 /
Ibs/day
2023
2nd 6 ...(Max)
153
/
mg/L
155.254629 /
Ibs/day
2023
2nd 6 ...(Min)
18
/
mg/L
18.3897 /
lbs/day
2023
2nd 6 ...(Count)
2
/
2 /
Sample Date
SamplelD
Result/Limit
Mass/Limit
Zinc
07/25/2023
P
Biogen072523POTW
1.01
/
mg/L
1.024884 /
lbs/day
08/30/2023
S
Biogen083023Self
0.566
/
mg/L
0.578254 /
lbs/day
Jul 2023
Week 4
1.01
/
mg/L
1.024884 /
Ibs/day
Aug 2023
Week 4
0.566
/
mg/L
0.578254 /
Ibs/day
Tuesday, February 13, 2024 2:31:58PM * Indicates Violation ** Indicates TRC Violation Page 10 of 11

Biogen
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
Jul 2023
Average
1.01
/ mg/L
1.024884 /
Aug 2023
Average
0.566
/ mg/L
0.578254 /
2023
Quarter 3
0.788
/ mg/L
0.801569 /
2023
2nd 6 Months (Avg)
0.788
/ mg/L
0.801569 /
2023
2nd 6 ...(Max)
1.01
/ mg/L
1.024884 /
2023
2nd 6 ...(Min)
0.566
/ mg/L
0.578254 /
2023
2nd 6 ...(Count)
2
/
2 /
lbs/day
lbs/day
lbs/day
Ibs/day
Ibs/day
Ibs/day
Tuesday, February 13, 2024 2:31:58PM * Indicates Violation ** Indicates TRC Violation Page 11 of l l

Cintas Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
08/15/2023
Aug 2023
Aug 2023
2023
2023
2023
2023
2023
P
Cintas081523POTW
Week 3
Average
Quarter 3
2nd 6 Months (Avg)
2nd 6 ...(Max)
2nd 6 ...(Min)
2nd 6 ...(Count)
16.3
16.3
16.3
16.3
16.3
16.3
16.3
1
/
/
/
/
/
/
/
/
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
1.6019 /
1.6019 /
1.6019 /
1.6019 /
1.6019 /
1.6019 /
1.6019 /
1 /
lbs/day
lbs/day
lbs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Sample Date
Sample./D
Result/Limit
Mass/Limit
Average Flow for Month
07/31/2023
S
Cintas0723F1ow
0.036467
/
MGD
/
08/31/2023
S
Cintas08223F1ow
0.039818
/
MGD
/
09/30/2023
S
Cintas0923F1ow
0.065685
/
MGD
/
10/31/2023
S
Cintasl023Flow
0.085712
/
MGD
/
11/30/2023
S
Cintas1123171ow
0.078176
/
MGD
/
12/31/2023
S
Cintas1223171ow
0.076004
/
MGD
/
Jul 2023
Week 4
0.036467
/
MGD
/
Aug 2023
Week 4
0.039818
/
MGD
/
Sep 2023
Week 4
0.065685
/
MGD
/
Oct 2023
Week 4
0.085712
/
MGD
/
Nov 2023
Week 4
0.078176
/
MGD
/
Dec 2023
Week 4
0.076004
/
MGD
/
Jul 2023
Average
0.036467
/ 0.100
MGD
/
Aug 2023
Average
0.039818
/ 0.100
MGD
/
Sep 2023
Average
0.065685
/ 0.100
MGD
/
Oct 2023
Average
0.085712
/ 0.100
MGD
/
Nov 2023
Average
0.078176
/ 0.100
MGD
/
Dec 2023
Average
0.076004
/ 0.100
MGD
/
2023
Quarter 3
0.047323
/
MGD
/
2023
Quarter 4
0.079964
/
MGD
/
2023
2nd 6 Months (Avg)
0.063644
/
MGD
/
2023
2nd 6 ...(Max)
0.085712
/
MGD
/
2023
2nd 6 ...(Min)
0.036467
/
MGD
/
2023
2nd 6 ...(Count)
6
Saturday, February 24, 2024 11:42:58AM * Indicates Violation ** Indicates TRC Violation Page 1 of 11

Cintas Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
6
Months Sampled:
6
Weeks Sampled:
6
Quarters Sampled :
2
# Over Daily C :
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0,00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SampleID Result/Limit Mass/Limit
BOD
07/20/2023
P
Cintas072023POTW
582
/ mg/L
/
08/02/2023
S
Cintas08O223Self
888
/ mg/L
153.273 /
Ibs/day
08/15/2023
P
Cintas081523POTW
1640
/ mg/L
161.177 /
Ibs/day
09/06/2023
S
Cintas09O623Self
383
/ mg/L
235.785 /
lbs/day
09/12/2023
P
Cintas091223POTW
426
/ mg/L
/
10/03/2023
S
Cintas 100323 Self
621
/ mg/L
440.434 /
lbs/day
10/17/2023
P
Cintasl01723POTW
485
/ mg/L
/
11/08/2023
S
Cintas110823Self
493
/ mg/L
343.501 /
Ibs/day
11/14/2023
P
Cintaslll423POTW
795
/ mg/L
/
12/05/2023
S
Cintas 120523 Self
369
/ mg/L
244.966 /
Ibs/day
12/12/2023
P
Cintas121223POTW
256
/ mg/L
/
Jul 2023
Week 3
582
/ mg/L
/
Aug 2023
Week 1
888
/ mg/L
153.273 /
lbs/day
Aug 2023
Week 3
1640
/ mg/L
161.177 /
lbs/day
Sep 2023
Week 1
383
/ mg/L
235.785 /
Ibs/day
Sep 2023
Week 2
426
/ mg/L
/
Oct 2023
Week 1
621
/ mg/L
440.434 /
Ibs/day
Oct 2023
Week 3
485
/ mg/L
/
Nov 2023
Week 2
644
/ mg/L
343.501 /
Ibs/day
Dec 2023
Week 1
369
/ mg/L
244.966 /
lbs/day
Dec 2023
Week 2
256
/ mg/L
/
Jul 2023
Average
582
/ mg/L
/
Aug 2023
Average
1264
/ mg/L
157.225 /
Ibs/day
Sep 2023
Average
404.5
/ mg/L
235.785 /
Ibs/day
Oct 2023
Average
553
/ mg/L
440.434 /
Ibs/day
Nov 2023
Average
644
/ mg/L
343.501 /
Ibs/day
Dec 2023
Average
312.5
/ mg/L
244.966 /
Ibs/day
2023
Quarter 3
783.8
/ mg/L
183.411 /
lbs/day
2023
Quarter 4
503.2
/ mg/L
342.967 /
lbs/day
2023
2nd 6 Months (Avg)
630.7
/ mg/L
263.189 /
Ibs/day
2023
2nd 6 ...(Max)
1640
/ mg/L
440.434 /
Ibs/day
2023
2nd 6 ...(Min)
256
/ mg/L
/
2023
2nd 6 ...(Count)
I
/
6 /
Saturday, February 24, 2024 11:42:58AM * Indicates Violation ** Indicates TRC Violation Page 2 of 11

Cintas Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
08/15/2023
P Cintas081523POTW
110
/
mg/L
10.8106 /
lbs/day
Aug 2023
Week 3
110
/
mg/L
10.8106 /
lbs/day
Aug 2023
Average
110
/
mg/L
10.8106 /
lbs/day
2023
Quarter 3
110
/
mg/L
10.8106 /
Ibs/day
2023
2nd 6 Months (Avg)
110
/
mg/L
10.8106 /
Ibs/day
2023
2nd 6 ...(Max)
110
/
mg/L
10.8106 /
Ibs/day
2023
2nd 6 ...(Min)
110
/
mg/L
10.8106 /
Ibs/day
2023
2nd 6 ...(Count)
1
/
1 /
Sample Date
SamplelD
Result/Limit
Mass/Limit
Fluoride
08/15/2023
P Cintas081523POTW
0.79
/
mg/L
0.0776 /
Ibs/day
Aug 2023
Week 3
0.79
/
mg/L
0.0776 /
lbs/day
Aug 2023
Average
0.79
/
mg/L
0.0776 /
lbs/day
2023
Quarter 3
0.79
/
mg/L
0.0776 /
lbs/day
2023
2nd 6 Months (Avg)
0.79
/
mg/L
0.0776 /
lbs/day
2023
2nd 6 ...(Max)
0.79
/
mg/L
0.0776 /
Ibs/day
2023
2nd 6 ...(Min)
0.79
/
mg/L
0.0776 /
Ibs/day
2023
2nd 6 ...(Count)
1
/
1 /
Sample Date
SamplelD
Result/Limit
Mass/Limit
Mercury - LL
07/05/2023 S
Cimas070523Self
0.000003
/ 0.000142
mg/L /
08/14/2023 P
Cintas08l423POTVvH
0.000002
/ 0.000142
mg/L /
g
Jul 2023
Week 1
0.000003
/
mg/L /
Aug 2023
Week 2
0.000002
/
mg/L /
Jul 2023
Average
0.000003
/
mg/L /
Aug 2023
Average
0.000002
/
mg/L /
2023
Quarter 3
0.000003
/
mg/L /
2023
2nd 6 Months (Avg)
0.000003
/
mg/L /
2023
2nd 6 ...(Max)
0.000003
/
mg/L /
2023
2nd 6 ...(Min)
0.000002
/
mg/L /
2023
2nd 6 ...(Count)
2
Sample Count :
2
Months Sampled :
2
Weeks Sampled :
2
Quarters Sampled :
1
# Over Daily C :
0
0.00
# Over Mo Avg C:
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C :
0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC: 0
0.00
# Over Qt Avg C TRC :
0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M :
0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC :
0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Saturday, February 24, 2024
11:42:58AM
* Indicates Violation
** Indicates TRC Violation
Page
3 of 11

Cintas Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate -Nitrite
08/02/2023
S Cintas08O223Self
0.7
/ mg/L
0.124 /
lbs/day
08/15/2023
P Cintas081523POTW
0.2
/ mg/L
0.017 /
lbs/day
09/06/2023
S Cintas09O623Self
0.1
/ mg/L
0.062 /
lbs/day
10/03/2023
S Cintas 100323 Self
0
/ mg/L
0.03 /
Ibs/day
11/08/2023
S Cintas110823Self
0.1
/ mg/L
0.035 /
Ibs/day
12/05/2023
S Cintas 120523 Self
0.1
/ mg/L
0.066 /
Ibs/day
Aug 2023
Week 1
0.7
/ mg/L
0.124 /
Ibs/day
Aug 2023
Week 3
0.2
/ mg/L
0.017 /
Ibs/day
Sep 2023
Week 1
0.1
/ mg/L
0.062 /
Ibs/day
Oct 2023
Week 1
0
/ mg/L
0.03 /
lbs/day
Nov 2023
Week 2
0.1
/ mg/L
0.035 /
lbs/day
Dec 2023
Week 1
0.1
/ mg/L
0.066 /
Ibs/day
Aug 2023
Average
0.4
/ mg/L
0.07 /
Ibs/day
Sep 2023
Average
0.1
/ mg/L
0.062 /
Ibs/day
Oct 2023
Average
0
/ mg/L
0.03 /
Ibs/day
Nov 2023
Average
0.1
/ mg/L
0.035 /
Ibs/day
Dec 2023
Average
0.1
/ mg/L
0.066 /
Ibs/day
2023
Quarter 3
0.3
/ mg/L
0.068 /
lbs/day
2023
Quarter 4
0.1
/ mg/L
0.044 /
lbs/day
2023
2nd 6 Months (Avg)
0.2
/ mg/L
0.056 /
Ibs/day
2023
2nd 6 ...(Max)
0.7
/ mg/L
0.124 /
Ibs/day
2023
2nd 6 ...(Min)
0.0
/ mg/L
0.017 /
Ibs/day
2023
2nd 6 ...(Count)
6
/
6 /
Sample Date SamplelD Result/Limit Mass /Limit
Nitrogen, Total
08/02/2023
S Cintas080223Self
08/15/2023
P Cintas081523POTW
09/06/2023
S Cintas09O623Self
10/03/2023
S Cintas100323Self
11/08/2023
S Cintas110823Self
12/05/2023
S Cintas120523Self
Aug 2023
Week 1
Aug 2023
Week 3
Sep 2023
Week 1
Oct 2023
Week 1
Nov 2023
Week 2
Dec 2023
Week 1
Aug 2023
Average
Sep 2023
Average
Oct 2023
Average
Nov 2023
Average
53.1
/ mg/L
9.165 /
Ibs/day
49.8
/ mg/L
4.894 /
Ibs/day
19.7
/ mg/L
12.128 /
lbs/day
44.6
/ mg/L
31.632 /
lbs/day
36.6
/ mg/L
25.501 /
lbs/day
45
/ mg/L
29.874 /
lbs/day
53.1
/ mg/L
9.165 /
Ibs/day
49.8
/ mg/L
4.894 /
Ibs/day
19.7
/ mg/L
12.128 /
Ibs/day
44.6
/ mg/L
31.632 /
Ibs/day
36.6
/ mg/L
25.501 /
lbs/day
45
/ mg/L
29.874 /
lbs/day
51.45
/ mg/L
7.03 /
lbs/day
19.7
/ mg/L
12.128 /
lbs/day
44.6
/ mg/L
31.632 /
Ibs/day
36.6
/ mg/L
25.501 /
Ibs/day
Saturday, February 24, 2024 11:42:58AM * Indicates Violation ** Indicates TRC Violation Page 4 of 11

Cintas Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
Nitrogen, Total
Dec 2023
Average
45
/
mg/L
29.874 /
lbs/day
2023
Quarter 3
40.87
/
mg/L
8.729 /
lbs/day
2023
Quarter 4
42.07
/
mg/L
29.002 /
lbs/day
2023
2nd 6 Months (Avg)
41.47
/
mg/L
18.866 /
Ibs/day
2023
2nd 6 ...(Max)
53.1
/
mg/L
31.632 /
Ibs/day
2023
2nd 6 ...(Min)
19.7
/
mg/L
4.894 /
Ibs/day
2023
2nd 6 ...(Count)
6
/
6 /
Sample Date
SamplelD
Result /Limit
Mass /Limit
Oil & Grease, HEM (Polar)
07/05/2023
S Cintas07O523Self
22.7
/ 100
mg/L
/
08/02/2023
S Cintas080223Self
5
/ 100
mg/L
0.863023 /
Ibs/day
08/15/2023
P Cintas081523POTW
<
2.5
/ 100
mg/L
<
0.245696 /
lbs/day
09/06/2023
S Cintas09O623Self
4.9
/ 100
mg/L
3.016565 /
lbs/day
10/03/2023
S Cintas 100323 Self
16
/ 100
mg/L
11.347738 /
lbs/day
11/08/2023
S Cintas110823Self
17.4
/ 100
mg/L
12.123571 /
lbs/day
12/05/2023
S Cintas120523Self
<
2.5
/ 100
mg/L
<
1.65966 /
Ibs/day
Jul 2023
Week 1
22.7
/
mg/L
/
Aug 2023
Week 1
5
/
mg/L
0.863023 /
Ibs/day
Aug 2023
Week 3
<
2.5
/
mg/L
<
0.245696 /
Ibs/day
Sep 2023
Week 1
4.9
/
mg/L
3.016565 /
lbs/day
Oct 2023
Week 1
16
/
mg/L
11.347738 /
lbs/day
Nov 2023
Week 2
17.4
/
mg/L
12.123571 /
lbs/day
Dec 2023
Week 1
<
2.5
/
mg/L
<
1.65966 /
lbs/day
Jul 2023
Average
22.7
/
mg/L
/
Aug 2023
Average
<
3.8
/
mg/L
<
0.55436 /
Ibs/day
Sep 2023
Average
4.9
/
mg/L
3.016565 /
Ibs/day
Oct 2023
Average
16
/
mg/L
11.347738 /
Ibs/day
Nov 2023
Average
17.4
/
mg/L
12.123571 /
lbs/day
Dec 2023
Average
<
2.5
/
mg/L
<
1.65966 /
lbs/day
2023
Quarter 3
<
8.8
/
mg/L
<
1.375095 /
lbs/day
2023
Quarter 4
<
12
/
mg/L
<
8.37699 /
lbs/day
2023
2nd 6 Months (Avg)
<
10.1
/
mg/L
<
4.87604 /
Ibs/day
2023
2nd 6 ...(Max)
22.7
/
mg/L
12.123571 /
Ibs/day
2023
2nd 6 ...(Min)
<
2.5
/
mg/L
<
/
2023
2nd 6 ...(Count)
7
/
6 /
Saturday, February 24, 2024 11:42:58AM * Indicates Violation ** Indicates TRC Violation Page 5 of 11

Cintas Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
7
Months Sampled :
6
Weeks Sampled:
7
Quarters Sampled :
2
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
Oil & Grease, SGT-HEM (Non -Polar)
07/05/2023
S
Cintas07O523Self
<
2.5
/ 100
mg/L
<
/
08/02/2023
S
Cintas080223Self
<
2.5
/ 100
mg/L
<
0.4315 /
Ibs/day
08/15/2023
P
Cintas081523POTW
<
2.5
/ 100
mg/L
<
0.2457 /
Ibs/day
09/06/2023
S
Cintas090623Self
<
2.5
/ 100
mg/L
<
1.5391 /
lbs/day
10/03/2023
S
Cintas 100323 Self
<
2.5
/ 100
mg/L
<
1.7731 /
lbs/day
11/08/2023
S
Cintas 110823 Self
6.7
/ 100
mg/L
4.6683 /
Ibs/day
12/05/2023
S
Cintas 120523 Self
<
2.5
/ 100
mg/L
<
1.6597 /
Ibs/day
Jul 2023
Week 1
<
2.5
/
mg/L
<
/
Aug 2023
Week 1
<
2.5
/
mg/L
<
0.4315 /
Ibs/day
Aug 2023
Week 3
<
2.5
/
mg/L
<
0.2457 /
Ibs/day
Sep 2023
Week 1
<
2.5
/
mg/L
<
1.5391 /
Ibs/day
Oct 2023
Week 1
<
2.5
/
mg/L
<
1.7731 /
lbs/day
Nov 2023
Week 2
6.7
/
mg/L
4.6683 /
lbs/day
Dec 2023
Week 1
<
2.5
/
mg/L
<
1.6597 /
lbs/day
Ju12023
Average
<
2.5
/
mg/L
<
/
Aug 2023
Average
<
2.5
/
mg/L
<
0.3386 /
Ibs/day
Sep 2023
Average
<
2.5
/
mg/L
<
1.5391 /
Ibs/day
Oct 2023
Average
<
2.5
/
mg/L
<
1.7731 /
Ibs/day
Nov 2023
Average
6.7
/
mg/L
4.6683 /
Ibs/day
Dec 2023
Average
<
2.5
/
mg/L
<
1.6597 /
lbs/day
2023
Quarter 3
<
2.5
/
mg/L
<
0.7388 /
lbs/day
2023
Quarter 4
<
3.9
/
mg/L
<
2.7003 /
lbs/day
2023
2nd 6 Months (Avg)
<
3.1
/
mg/L
<
1.7196 /
Ibs/day
2023
2nd 6 ...(Max)
6.7
/
mg/L
4.6683 /
Ibs/day
2023
2nd 6 ...(Min)
<
2.5
/
mg/L
<
/
2023
2nd 6 ...(Count)
7
/
6 /
Sample Count:
7
Months Sampled:
6
Weeks Sampled:
7
Quarters Sampled :
2
# Over Daily C:
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Saturday, February 24, 2024 11:42:58AM * Indicates Violation ** Indicates TRC Violation Page 6 of 11

Cintas Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
PH
07/05/2023 S
Cintas07O523Self
7.8
/ 6.0 - 10.5
SU
/
08/02/2023 S
Cintas08O223Self
7.7
/ 6.0 - 10.5
SU
/
08/15/2023 P
Cintas081523POTW
7.3
/ 6.0 - 10.5
SU
/
09/06/2023 S
Cintas09O623Self
7.3
/ 6.0 - 10.5
SU
/
10/03/2023 S
CintasI00323Self
7
/ 6.0 - 10.5
Su
/
11/08/2023 S
Cintas110823Self
7
/ 6.0 - 10.5
Su
/
12/05/2023 S
Cintas 120523 Self
8
/ 6.0 - 10.5
SU
/
Jul 2023
Week 1
7.8
/
SU
/
Aug 2023
Week 1
7.7
/
Su
/
Aug 2023
Week 3
7.3
/
SU
/
Sep 2023
Week 1
7.3
/
SU
/
Oct 2023
Week 1
7
/
SU
/
Nov 2023
Week 2
7
/
Su
/
Dec 2023
Week 1
8
/
Su
/
Jul 2023
Average
7.8
/
SU
/
Aug 2023
Average
7.5
/
SU
/
Sep 2023
Average
7.3
/
SU
/
Oct 2023
Average
7
/
SU
/
Nov 2023
Average
7
/
SU
/
Dec 2023
Average
8
/
SU
/
2023
Quarter 3
7.53
/
Su
/
2023
Quarter 4
7.33
/
Su
/
2023
2nd 6 Months (Avg)
7.44
/
SU
/
2023
2nd 6 ...(Max)
8
/
SU
/
2023
2nd 6 ...(Min)
7
/
SU
/
2023
2nd 6 ...(Count)
7
/
/
Sample Count : 7 Months Sampled:
6
Weeks Sampled :
7
Quarters Sampled :
2
# Over Daily C:
0 0.00 # Over Mo Avg C :
0 0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0 0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0 0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0 0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
07/05/2023 S Cintas07O523Self
31.8
/ 66
°C
/
08/02/2023 S CintaS080223Self
35
/ 66
°C
/
08/15/2023 P Cintas081523POTW
28
/ 66
°C
/
09/06/2023 S Cintas09O623Self
38.1
/ 66
°C
/
10/03/2023 S Cintas100323Self
34.7
/ 66
°C
/
Saturday, February 24, 2024 11:42:58AM
* Indicates Violation
** Indicates TRC Violation
Page 7 of 11

Cintas Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
11/08/2023 S
Cintas110823Self
33.9
/ 66
°C
/
12/05/2023 S
Cintas120523Self
20.2
/ 66
°C
/
7u12023
Week 1
31.8
/
°C
/
Aug 2023
Week 1
35
/
°C
/
Aug 2023
Week 3
28
/
°C
/
Sep 2023
Week 1
38.1
/
°C
/
Oct 2023
Week 1
34.7
/
°C
/
Nov 2023
Week 2
33.9
/
°C
/
Dec 2023
Week 1
20.2
/
°C
/
7u12023
Average
31.8
/
°C
/
Aug 2023
Average
31.5
/
°C
/
Sep 2023
Average
38.1
/
°C
/
Oct 2023
Average
34.7
/
°C
/
Nov 2023
Average
33.9
/
°C
/
Dec 2023
Average
20.2
/
°C
/
2023
Quarter 3
33.2
/
°C
/
2023
Quarter 4
29.6
/
°C
/
2023
2nd 6 Months (Avg)
31.7
/
°C
/
2023
2nd 6 ...(Max)
38.1
/
°C
/
2023
2nd 6 ...(Min)
20.2
/
°C
/
2023
2nd 6 ...(Count)
7
Sample Count: 7 Months Sampled:
6
Weeks Sampled:
7
Quarters Sampled:
2
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
07/20/2023
P
Cintas072023POTW
35.4
/ mg/L
/
08/02/2023
S
Cintas080223Self
52.4
/ mg/L
9.044 /
lbs/day
08/15/2023
P
Cintas081523POTW
49.6
/ mg/L
4.875 /
Ibs/day
09/06/2023
S
Cintas09O623Self
19.6
/ mg/L
12.066 /
Ibs/day
09/12/2023
P
Cintas091223POTW
10.7
/ mg/L
/
10/03/2023
S
Cintas 100323 Self
44.6
/ mg/L
31.632 /
Ibs/day
10/17/2023
P
CintasI01723POTW
19.5
/ mg/L
/
11/08/2023
S
Cintas110823Self
36.5
/ mg/L
25.432 /
lbs/day
11/14/2023
P
Cintas1I1423POTW
20.8
/ mg/L
/
12/05/2023
S
Cintas120523Self
44.9
/ mg/L
29.807 /
lbs/day
Saturday, February 24, 2024 11:42:58AM * Indicates Violation ** Indicates TRC Violation Page 8 of 11

Cintas Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
TKN
12/12/2023
P Cintas121223POTW
54.5
/ mg/L
/
Jul 2023
Week 3
35.4
/ mg/L
/
Aug 2023
Week 1
52.4
/ mg/L
9.044 /
lbs/day
Aug 2023
Week 3
49.6
/ mg/L
4.875 /
Ibs/day
Sep 2023
Week 1
19.6
/ mg/L
12.066 /
Ibs/day
Sep 2023
Week 2
10.7
/ mg/L
/
Oct 2023
Week 1
44.6
/ mg/L
31.632 /
Ibs/day
Oct 2023
Week 3
19.5
/ mg/L
/
Nov 2023
Week 2
28.65
/ mg/L
25.432 /
Ibs/day
Dec 2023
Week 1
44.9
/ mg/L
29.807 /
lbs/day
Dec 2023
Week 2
54.5
/ mg/L
/
Jul 2023
Average
35.4
/ mg/L
/
Aug 2023
Average
51
/ mg/L
6.96 /
Ibs/day
Sep 2023
Average
15.15
/ mg/L
12.066 /
Ibs/day
Oct 2023
Average
32.05
/ mg/L
31.632 /
Ibs/day
Nov 2023
Average
28.65
/ mg/L
25.432 /
Ibs/day
Dec 2023
Average
49.7
/ mg/L
29.807 /
Ibs/day
2023
Quarter 3
33.54
/ mg/L
8.662 /
lbs/day
2023
Quarter 4
36.8
/ mg/L
28.957 /
lbs/day
2023
2nd 6 Months (Avg)
35.32
/ mg/L
18.809 /
Ibs/day
2023
2nd 6 ...(Max)
54.5
/ mg/L
31.632 /
Ibs/day
2023
2nd 6 ...(Min)
10.7
/ mg/L
/
2023
2nd 6 ...(Count)
I
/
6 /
Sample Date SamplelD Result/Limit Mass /Limit
Total Phosphorus
07/20/2023
P
Cintas072023POTW
08/02/2023
S
Cintas08O223Self
08/15/2023
P
Cintas081523POTW
09/06/2023
S
Cintas09O623Self
09/12/2023
P
Cintas091223POTW
10/03/2023
S
Cintas100323Self
10/17/2023
P
CintasI01723POTW
11/08/2023
S
Cintas110823Self
11/14/2023
P
Cintasll1423POTW
12/05/2023
S
Cintas 120523 Self
12/12/2023
P
Cintasl2l223POTW
Jul 2023
Week 3
Aug 2023
Week 1
Aug 2023
Week 3
Sep 2023
Week 1
Sep 2023
Week 2
3.3
/ mg/L
/
5.4
/ mg/L
0.9321 /
Ibs/day
5.03
/ mg/L
0.4943 /
lbs/day
3.4
/ mg/L
2.0931 /
lbs/day
2.27
/ mg/L
/
4.1
/ mg/L
2.9079 /
lbs/day
1.19
/ mg/L
/
4.1
/ mg/L
2.8567 /
Ibs/day
2.32
/ mg/L
/
3.5
/ mg/L
2.3235 /
Ibs/day
3.88
/ mg/L
/
3.3
/ mg/L
/
5.4
/ mg/L
0.9321 /
lbs/day
5.03
/ mg/L
0.4943 /
lbs/day
3.4
/ mg/L
2.0931 /
Ibs/day
2.27
/ mg/L
/
Saturday, February 24, 2024 11:42:58AM * Indicates Violation ** Indicates TRC Violation Page 9 of 11

Cintas Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
Oct 2023
Week 1
4.1
/ mg/L
2.9079 /
Ibs/day
Oct 2023
Week 3
1.19
/ mg/L
/
Nov 2023
Week 2
3.21
/ mg/L
2.8567 /
lbs/day
Dec 2023
Week 1
3.5
/ mg/L
2.3235 /
lbs/day
Dec 2023
Week 2
3.88
/ mg/L
/
Ju12023
Average
3.3
/ mg/L
/
Aug 2023
Average
5.215
/ mg/L
0.7132 /
Ibs/day
Sep 2023
Average
2.835
/ mg/L
2.0931 /
Ibs/day
Oct 2023
Average
2.645
/ mg/L
2.9079 /
Ibs/day
Nov 2023
Average
3.21
/ mg/L
2.8567 /
lbs/day
Dec 2023
Average
3.69
/ mg/L
2.3235 /
lbs/day
2023
Quarter 3
3.88
/ mg/L
1.1732 /
Ibs/day
2023
Quarter 4
3.182
/ mg/L
2.696 /
Ibs/day
2023
2nd 6 Months (Avg)
3.499
/ mg/L
1.9346 /
Ibs/day
2023
2nd 6 ...(Max)
5.4
/ mg/L
2.9079 /
Ibs/day
2023
2nd 6 ...(Min)
1.19
/ mg/L
/
2023
2nd 6 ...(Count)
11
/
6 /
Sample Date SamplelD Result/Limit Mass/Limit
TSS
07/20/2023
P
Cintas072023POTW
588
/ mg/L
/
08/02/2023
S
Cintas080223Self
664
/ mg/L
114.609481
/ lbs/day
08/15/2023
P
Cintas081523POTW
412
/ mg/L
40.490767
/ lbs/day
09/06/2023
S
Cintas09O623Self
308
/ mg/L
189.612636
/ lbs/day
09/12/2023
P
Cintas091223POTW
184
/ mg/L
/
10/03/2023
S
Cintas100323Self
317
/ mg/L
224.827051
/ Ibs/day
10/17/2023
P
Cintas101723POTW
143
/ mg/L
/
11/08/2023
S
Cintas110823Self
528
/ mg/L
367.887675
/ Ibs/day
11/14/2023
P
Cintas111423POTW
414
/ mg/L
/
12/05/2023
S
Cintas120523Self
130
/ mg/L
86.30232
/ lbs/day
12/12/2023
P
Cintasl21223POTW
148
/ mg/L
/
Jul 2023
Week 3
588
/ mg/L
/
Aug 2023
Week 1
664
/ mg/L
114.609481
/ Ibs/day
Aug 2023
Week 3
412
/ mg/L
40.490767
/ Ibs/day
Sep 2023
Week 1
308
/ mg/L
189.612636
/ Ibs/day
Sep 2023
Week 2
184
/ mg/L
/
Oct 2023
Week 1
317
/ mg/L
224.827051
/ lbs/day
Oct 2023
Week 3
143
/ mg/L
/
Nov 2023
Week 2
471
/ mg/L
367.887675
/ lbs/day
Dec 2023
Week 1
130
/ mg/L
86.30232
/ lbs/day
Dec 2023
Week 2
148
/ mg/L
/
Jul 2023
Average
588
/ mg/L
/
Saturday, February 24, 2024 11:42:58AM * Indicates Violation ** Indicates TRC Violation Page 10 of 11

Cintas Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
TSS
Aug 2023
Average
538
/ mg/L
77.550124 /
lbs/day
Sep 2023
Average
246
/ mg/L
189.612636 /
lbs/day
Oct 2023
Average
230
/ mg/L
224.827051 /
lbs/day
Nov 2023
Average
471
/ mg/L
367.887675 /
Ibs/day
Dec 2023
Average
139
/ mg/L
86.30232 /
Ibs/day
2023
Quarter 3
431.2
/ mg/L
114.904294 /
Ibs/day
2023
Quarter 4
280
/ mg/L
226.339015 /
Ibs/day
2023
2nd 6 Months (Avg)
348.7
/ mg/L
170.622 /
Ibs/day
2023
2nd 6 ...(Max)
664
/ mg/L
367.887675 /
Ibs/day
2023
2nd 6 ...(Min)
130
/ mg/L
/
2023
2nd 6 ...(Count)
I
/
6 /
Sample Date SamplelD Result/Limit Mass/Limit
VOC
07/05/2023
S Cintas07O523Self
0.0088
/ mg/L /
Jul 2023
Week 1
0.0088
/ mg/L /
Jul 2023
Average
0.0088
/ mg/L /
2023
Quarter 3
0.0088
/ mg/L /
2023
2nd 6 Months (Avg)
0.0088
/ mg/L /
2023
2nd 6 ...(Max)
0.0088
/ mg/L /
2023
2nd 6 ...(Min)
0.0088
/ mg/L /
2023
2nd 6 ...(Count)
1
Saturday, February 24, 2024 11:42:58AM * Indicates Violation ** Indicates TRC Violation Page 11 of l l

Cree LED Headquarters
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result /Limit Mass /Limit
Aluminum
08/08/2023
S
CreeLED080823Self
1.29 /
mg/L
/
09/19/2023
S
CreeLED091923Self
2.36 /
mg/L
/
10/12/2023
S
CreeLED101223Sclf
2.61 /
mg/L
/
11/14/2023
S
CreeLED111423Self
5.07 /
mg/I.
/
11/28/2023
P
CreeLED112823PO
0.272 /
mg/L
/
TW
Aug 2023
Week 2
1.29 /
mg/L
/
Sep 2023
Week 3
2.36 /
mg/L
/
Oct 2023
Week 2
2.61 /
mg/L
/
Nov 2023
Week 2
5.07 /
mg/L
/
Nov 2023
Week 4
0.272 /
mg/L
/
Aug 2023
Average
1.29 /
mg/L
/
Sep 2023
Average
2.36 /
mg/L
/
Oct 2023
Average
2.61 /
mg/L
/
Nov 2023
Average
2.671 /
mg/L
/
2023
Quarter 3
1.825 /
mg/L
/
2023
Quarter 4
2.651 /
mg/L
/
2023
2nd 6 Months (Avg)
2.320 /
mg/L
/
2023
2nd 6 ...(Max)
5.07 /
mg/L
/
2023
2nd 6 ...(Min)
0.272 /
mg/L
/
2023
2nd 6 ...(Count)
5
Sample Date SamplelD Result/Limit Mass /Limit
Antimony
08/08/2023
S
CreeLED080823Self <
09/19/2023
S
CreeLED091923Self <
10/12/2023
S
CreeLED101223Self <
11/14/2023
S
CreeLED111423Self <
11/28/2023
P
CreeLED112823PO <
TW
Aug 2023
Week 2 <
Sep 2023
Week 3 <
Oct 2023
Week 2 <
Nov 2023
Week 2 <
Nov 2023
Week 4 <
Aug 2023
Average <
Sep 2023
Average <
Oct2023
Average <
0.02 /
0.10
mg/L
< /
0.02 /
0.10
mg/L
< /
0.02 /
0.10
mg/L
< /
0.02 /
0.10
mg/L
< /
0.0003 /
0.10
mg/L
< /
0.02 /
mg/L
< /
0.02 /
mg/L
< /
0.02 /
mg/L
< /
0.02 /
mg/L
< /
0.0003 /
mg/L
< /
0.02 /
0.04
mg/L
< /
0.02 /
0.04
mg/L
< /
0.02 /
0.04
mg/L
< /
Saturday, February 24, 2024 10:47:41PM * Indicates Violation ** Indicates TRC Violation Page I of 16

Cree LED Headquarters
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SampleID
Result /Limit
Mass /Limit
Antimony
Nov 2023
Average
<
0.0101 /
0.04
mg/L
<
/
2023
Quarter 3
<
0.02 /
mg/L
<
/
2023
Quarter 4
<
0.0134 /
mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.0161 /
mg/L
<
/
2023
2nd 6 ...(Max)
<
0.02 /
m911-
<
/
2023
2nd 6 ...(Min)
<
0.0003 /
mg/L
<
/
2023
2nd 6 ...(Count)
5
Sample Date
SampleID
Result/Limit
Mass/Limit
Average Flow
for
Month
07/31/2023
S
CreeLED0723F1ow
0.000003 /
MOD
/
08/31/2023
S
CreeLED0823F1ow
0.000323 /
MOD
/
09/30/2023
S
CreeLED0923F1ow
0.000517 /
MOD
/
10/31/2023
S
CreeLED1023FIow
0.000284 /
MOD
/
11/30/2023
S
CreeLED1123FIow
0.00047 /
MOD
/
12/31/2023
S
CreeLED1223F1ow
0.000761 /
MOD
/
Jul 2023
Week 4
0.000003 /
MOD
/
Aug 2023
Week 4
0.000323 /
MOD
/
Sep 2023
Week 4
0.000517 /
MOD
/
Oct2023
Week
0.000284 /
MOD
/
Nov 2023
Week 4
0.00047 /
MOD
/
Dec 2023
Week 4
0.000761 /
MOD
/
Ju12023
Average
0.000003 /
0.003
MOD
/
Aug 2023
Average
0.000323 /
0.003
MOD
/
Sep 2023
Average
0.000517 /
0.003
MOD
/
Oct 2023
Average
0.000284 /
0.003
MOD
/
Nov 2023
Average
0.00047 /
0.003
MOD
/
Dec 2023
Average
0.000761 /
0.003
MOD
/
2023
Quarter 3
0.000281 /
MOD
/
2023
Quarter 4
0.000505 /
MOD
/
2023
2nd 6 Months (Avg)
0.000393 /
MOD
/
2023
2nd 6 ...(Max)
0.000761 /
MOD
/
2023
2nd 6 ...(Min)
0.000003 /
MOD
/
2023
2nd 6 ...(Count)
6 /
/
Sample Date
SampleID
Result/Limit
Mass / Limit
Barium
Saturday, February 24, 2024 10:47:41PM * Indicates Violation ** Indicates TRC Violation Page 2 of 16

Cree LED Headquarters
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result /Limit Mass /Limit
Barium
08/08/2023
S
CreeLED080823Self
0.027 /
mg/L
/
09/19/2023
S
CreeLED091923Self
0.118 /
mg/L
/
10/12/2023
S
CreeLED101223Sclf
0.117 /
mg/L
/
11/14/2023
S
CreeLED111423Self
0.108 /
mg/I.
/
11/28/2023
P
CreeLED112823PO
0.024 /
mg/L
/
TW
Aug 2023
Week 2
0.027 /
mg/L
/
Sep 2023
Week 3
0.118 /
mg/L
/
Oct 2023
Week 2
0.117 /
mg/L
/
Nov 2023
Week 2
0.108 /
mg/L
/
Nov 2023
Week 4
0.024 /
mg/L
/
Aug 2023
Average
0.027 /
mg/L
/
Sep 2023
Average
0.118 /
mg/L
/
Oct 2023
Average
0.117 /
mg/L
/
Nov 2023
Average
0.066 /
mg/L
/
2023
Quarter 3
0.072 /
mg/L
/
2023
Quarter 4
0.083 /
mg/L
/
2023
2nd 6 Months (Avg)
0.079 /
mg/L
/
2023
2nd 6 ...(Max)
0.118 /
mg/L
/
2023
2nd 6 ...(Min)
0.024 /
mg/L
/
2023
2nd 6 ...(Count)
5
Sample Date SamplelD Result /Limit Mass /Limit
BOD
08/08/2023
S
CreeLED080823Self
09/19/2023
S
CreeLED091923Self
10/12/2023
S
CreeLED101223Self
11/14/2023
S
CreeLED111423Self
Aug 2023
Week 2
Sep 2023
Week 3
Oct 2023
Week 2
Nov 2023
Week 2
Aug 2023
Average
Sep 2023
Average
Oct2023
Average
Nov 2023
Average
2023
Quarter 3
2023
Quarter 4
121 /
mg/L /
85.6 /
mg/L /
284 /
mg/L /
476 /
mg/L /
121 /
mg/L /
85.6 /
mg/L, /
284 /
mg/L /
476 /
mg/L /
121 /
mgfL /
85.6 /
mg/L /
284 /
mg/L /
476 /
mg/L /
103.3 /
mg/L /
380 /
ing/L /
Saturday, February 24, 2024 10:47:41PM * Indicates Violation ** Indicates TRC Violation Page 3 of 16

Cree LED Headquarters
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result /Limit
Mass /Limit
BOD
2023
2nd 6 Months (Avg)
241.7 /
mg/L
/
2023
2nd 6 ...(Max)
476 /
mg/L
/
2023
2nd 6 ...(Min)
85.6 /
mg/L
/
2023
2nd 6 ...(Count)
4 /
/
Sample Date
SamplelD
Result/Limit
Mass /Limit
Cadmium
08/08/2023
S
CreeLED080823Self
<
0.0004 / 0.14
mg/L
<
/
09/19/2023
S
CreeLED091923Self
<
0.0004 / 0.14
mg/L
<
/
10/12/2023
S
CreeLED101223Self
<
0.0004 / 0.14
mg/L
<
/
11/14/2023
S
CreeLED111423Self
<
0.004 / 0.14
mg/L
<
/
11/28/2023
P
CreeLED112823PO
<
0.00025 / 0.14
mg/L
<
/
TW
Aug 2023
Week 2
<
0.0004 /
mg/L
<
/
Sep 2023
Week 3
<
0.0004 /
mg/L
<
/
Oct 2023
Week 2
<
0.0004 /
mg/L
<
/
Nov 2023
Week 2
<
0.004 /
mg/L
<
/
Nov 2023
Week 4
<
0.00025 /
mg/L
<
/
Aug 2023
Average
<
0.0004 / 0.07
mg/L
<
/
Sep 2023
Average
<
0.0004 / 0.07
mg/L
<
/
Oct 2023
Average
<
0.0004 / 0.07
mg/L
<
/
Nov 2023
Average
<
0.00213 / 0.07
mg/L
<
/
2023
Quarter 3
<
0.0004 /
mg/L
<
/
2023
Quarter 4
<
0.00155 /
mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.00109 /
mg/L
<
/
2023
2nd 6 ...(Max)
<
0.004 /
mg/L
<
/
2023
2nd 6 ...(Min)
<
0.00025 /
mg/L
<
/
2023
2nd 6 ...(Count)
5
Sample Date
SamplelD
Result/Limit
Mass/Limit
Chloride
08/08/2023
S
CreeLED080823Self
43.2 /
mg/L
/
09/19/2023
S
CreeLED091923Self
56.3 /
mg/L
/
10/12/2023
S
CreeLED 10 1223 Self
71.2 /
mg/L
/
11/14/2023
S
CreeLED111423Self
48.9 /
mg/L
/
11/28/2023
P
CreeLED112823PO
140 /
mg/L
/
TW
Aug 2023
Week 2
43.2 /
mg/L
/
Saturday, February 24, 2024 10:47:41PM * Indicates Violation ** Indicates TRC Violation Page 4 of 16

Cree LED Headquarters
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result /Limit Mass /Limit
Chloride
Sep 2023
Week 3
56.3 /
mg/L
/
Oct 2023
Week 2
71.2 /
mg/L
/
Nov 2023
Week 2
48.9 /
mg/L
/
Nov 2023
Week 4
140 /
mg/L
/
Aug 2023
Average
43.2 /
mg/L
/
Sep 2023
Average
56.3 /
mg/L
/
Oct 2023
Average
71.2 /
mg/L
/
Nov 2023
Average
94.45 /
mg/L
/
2023
Quarter 3
49.75 /
mg/L
/
2023
Quarter 4
86.7 /
mg/L
/
2023
2nd 6 Months (Avg)
71.92 /
mg/L
/
2023
2nd 6 ...(Max)
140 /
mg/L
/
2023
2nd 6 ...(Min)
43.2 /
mg/L
/
2023
2nd 6 ...(Count)
5
Sample Date SamplelD Result /Limit Mass/Limit
Chromium
08/08/2023 S CreeLED080823Self
09/19/2023 S CreeLED091923Self <
10/12/2023 S CreeLED 10 1223 Self <
11/14/2023 S CreeLED111423Self <
11/28/2023 P CreeLED112823PO
TW
Aug 2023 Week 2
Sep 2023 Week 3 <
Oct 2023 Week 2 <
Nov 2023 Week 2 <
Nov 2023 Week 4
Aug 2023 Average
Sep 2023 Average <
Oct 2023 Average <
Nov 2023 Average <
2023 Quarter 3 <
2023 Quarter 4 <
2023 2nd 6 Months (Avg) <
2023 2nd 6 ...(Max)
2023 2nd 6 ...(Min) <
2023 2nd 6 ...(Count)
0.002 /
mg/L
/
0.001 /
mg/L
< /
0.001 /
mg/L
< /
0.001 /
mg/L
< /
0.007 /
mg/L
/
0.002 /
mg/L
/
0.001 /
mg/L
< /
0.001 /
mg/L
< /
0.001 /
mg/L
< /
0.007 /
mg/L
/
0.002 /
mg/L
/
0.001 /
mg/L
< /
0.001 /
mg/L
< /
0.004 /
mg/L
< /
0.002 /
mg/L
< /
0.003 /
mg/L
< /
0.002 /
mg/L
< /
0.007 /
mg/L
/
0.001 /
mg/L
< /
5/
/
Saturday, February 24, 2024 10:47:41PM * Indicates Violation ** Indicates TRC Violation Page 5 of 16

Cree LED Headquarters
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result /Limit Mass /Limit
Copper
08/08/2023
S
CreeLED080823Self
0.034 /
mg/L
/
09/19/2023
S
CreeLED091923Self
0.064 /
mg/L
/
10/12/2023
S
CreeLED101223Sclf
0.036 /
mg/L
/
11/14/2023
S
CreeLED111423Self
0.07 /
mg/I.
/
11/28/2023
P
CreeLED112823PO
0.122 /
mg/L
/
TW
Aug 2023
Week 2
0.034 /
mg/L
/
Sep 2023
Week 3
0.064 /
mg/L
/
Oct 2023
Week 2
0.036 /
mg/L
/
Nov 2023
Week 2
0.07 /
mg/L
/
Nov 2023
Week 4
0.122 /
mg/L
/
Aug 2023
Average
0.034 /
mg/L
/
Sep 2023
Average
0.064 /
mg/L
/
Oct 2023
Average
0.036 /
mg/L
/
Nov 2023
Average
0.096 /
mg/L
/
2023
Quarter 3
0.049 /
mg/L
/
2023
Quarter 4
0.076 /
mg/L
/
2023
2nd 6 Months (Avg)
0.065 /
mg/L
/
2023
2nd 6 ...(Max)
0.122 /
mg/L
/
2023
2nd 6 ...(Min)
0.034 /
mg/L
/
2023
2nd 6 ...(Count)
5
Sample Date SamplelD Result/Limit Mass /Limit
Cyanide
08/08/2023
S
CreeLED080823Self <
09/19/2023
S
CreeLED091923Self <
10/12/2023
S
CreeLED101223Self <
11/14/2023
S
CreeLED111423Self <
11/28/2023
P
CreeLED112823PO <
TW
Aug 2023
Week 2 <
Sep 2023
Week 3 <
Oct 2023
Week 2 <
Nov 2023
Week 2 <
Nov 2023
Week 4 <
Aug 2023
Average <
Sep 2023
Average <
Oct2023
Average <
0.003 /
mg/L
< /
0.025 /
mg/L
< /
0.063 /
mg/L
< /
0.05 /
mg/L
< /
0.003 /
mg/L
< /
0.003 /
mg/L
< /
0.025 /
mgJL
< /
0.063 /
mg/L
< /
0.05 /
mg/L
< /
0.003 /
mg/L
< /
0.003 /
mg/L
< /
0.025 /
mg/L
< /
0.063 /
mg/L
< /
Saturday, February 24, 2024 10:47:41PM * Indicates Violation ** Indicates TRC Violation Page 6 of 16

Cree LED Headquarters
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result /Limit
Mass /Limit
Cyanide
Nov 2023
Average
<
0.026 /
mg/L
<
/
2023
Quarter 3
<
0.014 /
mg/L
<
/
2023
Quarter 4
<
0.038 /
mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.029 /
mg/L
<
/
2023
2nd 6 ...(Max)
<
0.063 /
m911-
<
/
2023
2nd 6 ...(Min)
<
0.003 /
mg/L
<
/
2023
2nd 6 ...(Count)
5
Sample Date
SamplelD
Result/Limit
Mass/Limit
Fluoride
08/08/2023
S
CreeLED080823Self
0.26 / 14.0
mg/L
/
09/19/2023
S
CreeLED091923Self
0.39 / 14.0
mg/L
/
10/12/2023
S
CreeLED 10 1223 Self
0.46 / 14.0
mg/L
/
11/14/2023
S
CreeLED 111423 Self
0.22 / 14.0
mg/L
/
11/28/2023
P
CreeLED112823PO
0.13 / 14.0
mg/L
/
TW
Aug 2023
Week 2
0.26 /
mg/L
/
Sep 2023
Week 3
0.39 /
mg/L
/
Oct 2023
Week 2
0.46 /
mg/L
/
Nov 2023
Week 2
0.22 /
mg/L
/
Nov 2023
Week 4
0.13 /
mg/L
/
Aug 2023
Average
0.26 / 7.0
mg/L
/
Sep 2023
Average
0.39 / 7.0
mg/L
/
Oct 2023
Average
0.46 / 7.0
mg/L
/
Nov 2023
Average
0.18 / 7.0
mg/L
/
2023
Quarter 3
0.33 /
mg/L
/
2023
Quarter 4
0.27 /
mg/L
/
2023
2nd 6 Months (Avg)
0.29 /
mg/L
/
2023
2nd 6 ...(Max)
0.46 /
mg/L
/
2023
2nd 6 ...(Min)
0.13 /
mg/L,
/
2023
2nd 6 ...(Count)
5 /
/
Sample Date
SamplelD
Result/Limit
Mass/Limit
Lead
08/08/2023
S
CreeLED080823 Self
0.002 /
mg/L
/
09/19/2023
S
CreeLED091923Self
0,0016 /
mg/L
/
10/12/2023
S
CreeLED101223Self
<
0.0003 /
mg/L
<
/
Saturday, February 24, 2024 10:47:41PM * Indicates Violation ** Indicates TRC Violation Page 7 of 16

Cree LED Headquarters
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result /Limit Mass /Limit
Lead
11/14/2023
S CreeLED111423Self
0.0014 /
mg/L
/
11/28/2023
P CreeLED112823PO
0.0027 /
mg/L
/
TW
Aug 2023
Week 2
0.002 /
mg/L
/
Sep 2023
Week 3
0.0016 /
mg/L
/
Oct 2023
Week 2 <
0.0003 /
mg/L <
/
Nov 2023
Week 2
0.0014 /
mg/L
/
Nov 2023
Week 4
0.0027 /
mg/L
/
Aug 2023
Average
0.002 /
mg/L
/
Sep 2023
Average
0.0016 /
mg/L
/
Oct 2023
Average <
0.0003 /
mg/L <
/
Nov 2023
Average
0.002 /
mg/L
/
2023
Quarter 3
0.0018 /
mg/L
/
2023
Quarter 4 <
0.0014 /
mg/L <
/
2023
2nd 6 Months (Avg) <
0.0016 /
mg/L <
/
2023
2nd 6 ...(Max)
0.0027 /
mg/L
/
2023
2nd 6 ...(Min) <
0.0003 /
mg/L <
/
2023
2nd 6 ...(Count)
5
Sample Date SampleID Result/Limit Mass / Limit
Mercury - LL
08/08/2023
S CreeLED080823Self
0.000004 /
0.000142
mg/L
/
09/19/2023
S CreeLED091923Self
<
0.000001 /
0.000142
mg/L
< /
10/12/2023
S CreeLED101223Self
<
0.000001 /
0.000142
mg/L
< /
11/14/2023
S CreeLED111423Self
0.000001 /
0.000142
mg/L
/
11/27/2023
P CreeLED112723PO
0.000021 /
0.000142
mg/L
/
TWHg
Aug 2023
Week 2
0.000004 /
mg/L
/
Sep 2023
Week 3
<
0.000001 /
mg/L
< /
Oct 2023
Week 2
<
0.000001 /
ing/L
< /
Nov 2023
Week 2
0.000001 /
mg/L
/
Nov 2023
Week 4
0.000021 /
mgJL
/
Aug 2023
Average
0.000004 /
mg/L
/
Sep 2023
Average
<
0.000001 /
mg/L
< /
Oct 2023
Average
<
0.000001 /
mg/L
< /
Nov 2023
Average
0.000011 /
mg/L
/
2023
Quarter 3
<
0.000002 /
mg/L
< /
2023
Quarter 4
<
0.000008 /
mg/L
< /
Saturday, February 24, 2024 10:47:41PM * Indicates Violation ** Indicates TRC Violation Page 8 of 16

Cree LED Headquarters
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result /Limit
Mass /Limit
Mercury - LL
2023
2nd 6 Months (Avg)
<
0.000005 /
mg/L
<
/
2023
2nd 6 ...(Max)
0.000021 /
mg/L
/
2023
2nd 6 ...(Min)
<
0.000001 /
mg/L
<
/
2023
2nd 6 ...(Count)
5 /
/
Sample Date
SamplelD
Result /Limit
Mass /Limit
Molybdenum
08/08/2023
S CreeLED080823Self
<
0.004 /
mg/L
<
/
09/19/2023
S CreeLED091923Self
0.109 /
mg/L
/
10/12/2023
S CreeLED101223Self
<
0.004 /
mg/L
<
/
11/14/2023
S CreeLED111423Self
0.0113 /
mg/L
/
11/28/2023
P CreeLED112823PO
0.043 /
mg/L
/
TW
Aug 2023
Week 2
<
0.004 /
mg/L
<
/
Sep 2023
Week 3
0.109 /
mg/L
/
Oct 2023
Week 2
<
0.004 /
mg/L
<
/
Nov 2023
Week 2
0.0113 /
mg/L
/
Nov 2023
Week 4
0.043 /
mg/L
/
Aug 2023
Average
<
0.004 /
mg/L
<
/
Sep 2023
Average
0.109 /
mg/L
/
Oct 2023
Average
<
0.004 /
mg/L
<
/
Nov 2023
Average
0.0272 /
mg/L
/
2023
Quarter 3
<
0.0565 /
mg/L
<
/
2023
Quarter 4
<
0.0194 /
mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.0343 /
mg/L
<
/
2023
2nd 6 ...(Max)
0.109 /
mg/L
/
2023
2nd 6 ...(Min)
<
0.004 /
mg/L
<
/
2023
2nd 6 ...(Count)
5 /
/
Sample Date
SamplelD
Result/Limit
Mass/Limit
Nickel
08/08/2023
S
CreeLED080823Self <
0.004 /
mg/L <
/
09/19/2023
S
CreeLED091923Self <
0.004 /
mg/L <
/
10/12/2023
S
CreeLED 10 1223 Self <
0.004 /
mg/L <
/
11/14/2023
S
CreeLED111423Self <
0.004 /
mg/L <
/
11/28/2023
P
CreeLED112823PO
0.0095 /
mg/L
/
TW
Aug 2023
Week 2 <
0.004 /
mg/L <
/
Saturday, February 24, 2024 10:47:41PM * Indicates Violation ** Indicates TRC Violation Page 9 of 16

Cree LED Headquarters
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result /Limit Mass /Limit
Nickel
Sep 2023
Week 3
<
0.004 /
mg/L
<
/
Oct 2023
Week 2
<
0.004 /
mg/L
<
/
Nov 2023
Week 2
<
0.004 /
mg/L
<
/
Nov 2023
Week 4
0.0095 /
mg/L
/
Aug 2023
Average
<
0.004 /
mg/L
<
/
Sep 2023
Average
<
0.004 /
mg/L
<
/
Oct 2023
Average
<
0.004 /
mg/L
<
/
Nov 2023
Average
<
0.0068 /
mg/L
<
/
2023
Quarter 3
<
0.004 /
mg/L
<
/
2023
Quarter 4
<
0.0058 /
mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.0051 /
mg/L
<
/
2023
2nd 6 ...(Max)
0.0095 /
mg/L
/
2023
2nd 6 ...(Min)
<
0.004 /
mg/L
<
/
2023
2nd 6 ...(Count)
5
Sample Date SamplelD Result /Limit Mass I Limit
Nitrate -Nitrite
08/08/2023 S
CreeLED080823Self
0.2 /
mg/L
/
10/12/2023 S
CreeLED101223Self
0.1 /
mg/L
/
11/14/2023 S
CreeLED111423Self
<
0 /
mg/L
< /
11/28/2023 P
CreeLED112823PO
0.7 /
mg/L
/
TW
Aug 2023
Week 2
0.2 /
mg/L
/
Oct 2023
Week 2
0.1 /
mg/L
/
Nov 2023
Week 2
<
0 /
mg/L
< /
Nov 2023
Week 4
0.7 /
mg/L
/
Aug 2023
Average
0.2 /
mg/L
/
Oct 2023
Average
0.1 /
mg/L
/
Nov 2023
Average
<
0.4 /
mg/L
< /
2023
Quarter 3
0.2 /
mg/L
/
2023
Quarter 4
<
0.3 /
mg/L
< /
2023
2nd 6 Months (Avg)
<
0.3 /
mg/L
< /
2023
2nd 6 ...(Max)
0.7 /
mg/L
/
2023
2nd 6 ...(Min)
<
0.0 /
mg/L
< /
2023
2nd 6 ...(Count)
4
Saturday, February 24, 2024 10:47:41PM * Indicates Violation ** Indicates TRC Violation Page 10 of 16

Cree LED Headquarters
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result /Limit Mass /Limit
Nitrogen, Total
08/08/2023
S
CreeLED080823Self
2.73 /
mg/L
/
09/19/2023
S
CreeLED091923Self
5.62 /
mg/L
/
10/12/2023
S
CreeLED101223Sclf
3.75 /
mg/L
/
11/14/2023
S
CreeLED111423Self
15.8 /
mg/I.
/
11/28/2023
P
CreeLED112823PO
53.9 /
mg/L
/
TW
Aug 2023
Week 2
2.73 /
mg/L
/
Sep 2023
Week 3
5.62 /
mg/L
/
Oct 2023
Week 2
3.75 /
mg/L
/
Nov 2023
Week 2
15.8 /
mg/L
/
Nov 2023
Week 4
53.9 /
mg/L
/
Aug 2023
Average
2.73 /
mg/L
/
Sep 2023
Average
5.62 /
mg/L
/
Oct 2023
Average
3.75 /
mg/L
/
Nov 2023
Average
34.85 /
mg/L
/
2023
Quarter 3
4.18 /
mg/L
/
2023
Quarter 4
24.48 /
mg/L
/
2023
2nd 6 Months (Avg)
16.36 /
mg/L
/
2023
2nd 6 ...(Max)
53.9 /
mg/L
/
2023
2nd 6 ...(Min)
2.73 /
mg/L
/
2023
2nd 6 ...(Count)
5
Sample Date SamplelD Result/Limit Mass /Limit
pH
08/08/2023
S
CreeLED080823Self
09/19/2023
S
CreeLED091923Self
10/12/2023
S
CreeLED101223Self
11/14/2023
S
CreeLED111423Self
11/28/2023
P
CreeLED112823PO
TW
Aug 2023
Week 2
Sep 2023
Week 3
Oct 2023
Week 2
Nov 2023
Week 2
Nov 2023
Week 4
Aug 2023
Average
Sep 2023
Average
Oct2023
Average
8.3 /
6.0 - 10.0
su /
8.2 /
6.0 - 10.0
SU /
8.1 /
6.0 - 10.0
SU /
7.8 /
6.0 - 10.0
su /
7.9 /
6.0 - 10.0
su /
8.3 /
su /
8.2 /
Su /
8.1 /
su /
7.8 /
Su /
7.9 /
su /
8.3 /
su /
8.2 /
Su /
8.1 /
SU /
Saturday, February 24, 2024 10:47:41PM * Indicates Violation ** Indicates TRC Violation Page 11 of 16

Cree LED Headquarters
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result /Limit
Mass /Limit
pH
Nov 2023
Average
7.85 /
su
/
2023
Quarter 3
8.25 /
su
/
2023
Quarter 4
7.93 /
su
/
2023
2nd 6 Months (Avg)
8.06 /
su
/
2023
2nd 6 ...(Max)
8.3 /
su
/
2023
2nd 6 ...(Min)
7.8 /
su
/
2023
2nd 6 ...(Count)
5 /
/
Sample Date
SamplelD
Result/Limit
Mass/Limit
Silver
08/08/2023
S CreeLED080823Self
<
0.002 /
mg/L
<
/
09/19/2023
S CreeLED091923Self
<
0.002 /
mg/L
<
/
10/12/2023
S CrecLED 10 1223 Self
<
0.002 /
mg/L
<
/
11/14/2023
S CreeLED111423Self
<
0.002 /
mg/L
<
/
11/28/2023
P CreeLED112823PO
<
0.0003 /
mg/L
<
/
TW
Aug 2023
Week 2
<
0.002 /
mg/L
<
/
Sep 2023
Week 3
<
0.002 /
mg/L
<
/
Oct 2023
Week 2
<
0.002 /
mg/L
<
/
Nov 2023
Week 2
<
0.002 /
mg/L
<
/
Nov 2023
Week 4
<
0.0003 /
mg/L
<
/
Aug 2023
Average
<
0.002 /
mg/L
<
/
Sep 2023
Average
<
0.002 /
mg/L
<
/
Oct 2023
Average
<
0.002 /
mg/L
<
/
Nov 2023
Average
<
0.0011 /
mg/L
<
/
2023
Quarter 3
<
0.002 /
mg/L
<
/
2023
Quarter 4
<
0.0014 /
mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.0017 /
mg/L
<,
/
2023
2nd 6 ...(Max)
<
0.002 /
mg/L
<
/
2023
2nd 6 ...(Min)
<
0.0003 /
mg/L,
<
/
2023
2nd 6 ...(Count)
5 /
/
Sample Date
SamplelD
Result/Limit
Mass/Limit
Temperature
08/08/2023
S CreeLED080823Self
23 / 66
°C
/
09/19/2023
S CreeLED091923Self
19 / 66
°C
/
10/12/2023
S CreeLED101223Self
17 / 66
°c
/
Saturday, February 24, 2024 10:47:41PM * Indicates Violation ** Indicates TRC Violation Page 12 of 16

Cree LED Headquarters
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result /Limit Mass /Limit
Temperature
11/14/2023 S
CreeLED111423Self
18 / 66
°c
/
11/28/2023 P
CreeLED112823PO
17 / 66
°c
/
TW
Aug 2023
Week 2
23 /
°c
/
Sep 2023
Week 3
19 /
°c
/
Oct 2023
Week 2
17 /
°C
/
Nov 2023
Week 2
18 /
°c
/
Nov 2023
Week 4
17 /
T
/
Aug 2023
Average
23 /
°c
/
Sep 2023
Average
19 /
°c
/
Oct 2023
Average
17 /
°c
/
Nov 2023
Average
17.5 /
°c
/
2023
Quarter 3
21 /
°c
/
2023
Quarter 4
17.3 /
°c
/
2023
2nd 6 Months (Avg)
18.8 /
°c
/
2023
2nd 6 ...(Max)
23 /
°c
/
2023
2nd 6 ...(Min)
17 /
°C
/
2023
2nd 6 ...(Count)
5
Sample Date SampleID Result/Limit Mass / Lintit
TKN
08/08/2023
S
CreeLED080823Self
10/12/2023
S
CreeLED101223Self
11/14/2023
S
CreeLED111423Self
11/28/2023
P
CreeLED112823PO
TW
Aug 2023
Week 2
Oct 2023
Week 2
Nov 2023
Week 2
Nov 2023
Week 4
Aug 2023
Average
Oct2023
Average
Nov 2023
Average
2023
Quarter 3
2023
Quarter 4
2023
2nd 6 Months (Avg)
2023
2nd 6 ...(Max)
2023
2nd 6 ...(Min)
2.51 /
mg/L /
3.6 /
mg(L /
15.8 /
mg/L /
53.2 /
mg/L /
2.51 /
mg/L /
3.6 /
mg/L /
15.8 /
mg/L /
53.2 /
ing/L /
2.51 /
mg/L /
3.6 /
mgJL /
34.5 /
mg/L /
2.51 /
mg/L /
24.2 /
mg/L /
18.78 /
mg/L /
53.2 /
mg/L /
2.51 /
mg/L /
Saturday, February 24, 2024 10:47:41PM * Indicates Violation ** Indicates TRC Violation Page 13 of 16

Cree LED Headquarters
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result /Limit
Mass /Limit
TKN
2023
2nd 6 ...(Count)
4
Sample Date
SamplelD
Result/Limit
Mass /Limit
Total Phosphorus
08/08/2023
S
CreeLED080823Self
<
0.1 /
mg/L
<
/
09/19/2023
S
CreeLED091923Self
0.25 /
mg/L
/
10/12/2023
S
CreeLED101223Self
<
0.1 /
mg/L
<
/
11/14/2023
S
CreeLED111423Self
<
0.1 /
mg/L
<
/
11/28/2023
P
CreeLED112823PO
5.08 /
mg/I,
/
TW
Aug 2023
Week 2
<
0.1 /
mg/L
<
/
Sep 2023
Week 3
0.25 /
mg/L
/
Oct 2023
Week 2
<
0.1 /
mg/L
<
/
Nov 2023
Week 2
<
0.1 /
mg/L
<
/
Nov 2023
Week 4
5.08 /
mg/L
/
Aug 2023
Average
<
0.1 /
mg/L
<
/
Sep 2023
Average
0.25 /
mg/L
/
Oct 2023
Average
<
0.1 /
mg/L
<
/
Nov 2023
Average
<
2.59 /
mg/L
<
/
2023
Quarter 3
<
0.175 /
mg/L
<
/
2023
Quarter 4
<
1.76 /
mg/L
<
/
2023
2nd 6 Months (Avg)
<
1,126 /
mg/L
<
/
2023
2nd 6 ...(Max)
5.08 /
mg/L
/
2023
2nd 6 ...(Min)
<
0.1 /
mg/L
<
/
2023
2nd 6 ...(Count)
5 /
/
Sample Date
SampleID
Result/Limit
Mass/Limit
TSS
08/08/2023
S
CreeLED080823Self
6.8 /
mg/L
/
09/19/2023
S
CreeLED091923Self
19.8 /
mg/L
/
10/12/2023
S
CreeLED101223Self
5.5 /
mg/L
/
11/14/2023
S
CreeLED111423Self
14.8 /
mg/L
/
11/28/2023
P
CreeLED112823PO
128 /
mg/L
/
TW
Aug 2023
Week 2
6.8 /
mg/L
/
Sep 2023
Week 3
19.8 /
mg/L
/
Oct 2023
Week 2
5.5 /
mg/L
/
Nov 2023
Week 2
14.8 /
mg/L
/
Saturday, February 24, 2024 10:47:41PM * Indicates Violation ** Indicates TRC Violation Page 14 of 16

Cree LED Headquarters
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result /Limit Mass /Limit
TSS
Nov 2023
Week 4
128 /
mg/L
/
Aug 2023
Average
6.8 /
mg/L
/
Sep 2023
Average
19.8 /
mg/L
/
Oct 2023
Average
5.5 /
mglL
/
Nov 2023
Average
71.4 /
mg/L
/
2023
Quarter 3
13.3 /
mg/L
/
2023
Quarter 4
49.4 /
mg/L
/
2023
2nd 6 Months (Avg)
35.0 /
mg/L
/
2023
2nd 6 ...(Max)
128 /
mg/L
/
2023
2nd 6 ...(Min)
5.5 /
mg/L
/
2023
2nd 6 ...(Count)
5
Sample Date
Sample/D
Result/Limit
Mass / Limit
VOC
08/08/2023
S
CreeLED080823Self
5.927 /
mg/L
/
09/19/2023
S
CreeLED091923Self
11.22 /
mg/L
/
10/12/2023
S
CreeLED 10 1223 Self
12.012 /
mg/L
/
11/14/2023
S
CreeLED111423Self
7.886 /
mg/L
/
11/28/2023
P
CreeLED112823PO
0.235 /
mg/L
/
TW
Aug 2023
Week 2
5.927 /
mg/L
/
Sep 2023
Week 3
11.22 /
mg/L
/
Oct 2023
Week 2
12.012 /
mg/L
/
Nov 2023
Week 2
7.886 /
mg/L
/
Nov 2023
Week 4
0.235 /
mg/L
/
Aug 2023
Average
5.927 /
mg/L
/
Sep 2023
Average
11.22 /
mg/L
/
Oct 2023
Average
12.012 /
mg/L
/
Nov 2023
Average
4.0605 /
mg/L
/
2023
Quarter 3
8.5735 /
mg/L,
/
2023
Quarter 4
6.711 /
mg/L
/
2023
2nd 6 Months (Avg)
7.456 /
mg/L
/
2023
2nd 6 ...(Max)
12.012 /
mg/L
/
2023
2nd 6 ...(Min)
0.235 /
mg/L
/
2023
2nd 6 ...(Count)
5
Saturday, February 24, 2024 10:47:41PM * Indicates Violation ** Indicates TRC Violation Page 15 of 16

Cree LED Headquarters
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result /Limit Mass /Limit
Zinc
08/08/2023
S
CreeLED080823Self
0.073 /
1.64
mg/L /
09/19/2023
S
CreeLED091923Self
0.133 /
1.64
mg/L /
10/12/2023
S
CreeLED101223Sclf
0.012 /
1.64
mg/L /
11/14/2023
S
CreeLED111423Self
0.04 /
1.64
mg/L /
11/28/2023
P
CreeLED112823PO
0.218 /
1.64
mg/L /
TW
Aug 2023
Week 2
0.073 /
mg/L /
Sep 2023
Week 3
0.133 /
mg/L /
Oct 2023
Week 2
0.012 /
mg/L /
Nov 2023
Week 2
0.04 /
mg/L /
Nov 2023
Week 4
0.218 /
mg/L /
Aug 2023
Average
0.073 /
0.67
mg/L /
Sep 2023
Average
0.133 /
0.67
mg/L /
Oct 2023
Average
0.012 /
0.67
mg/L /
Nov 2023
Average
0.129 /
0.67
mg/L /
2023
Quarter 3
0.103 /
mg/L /
2023
Quarter 4
0.09 /
mg/L /
2023
2nd 6 Months (Avg)
0.095 /
mg/L /
2023
2nd 6 ...(Max)
0.218 /
mg/L /
2023
2nd 6 ...(Min)
0.012 /
mg/L /
2023
2nd 6 ...(Count)
5 /
/
Saturday, February 24, 2024 10:47:41PM * Indicates Violation ** Indicates TRC Violation Page 16 of 16

Eli Lilly & Company
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Arsenic
10/25/2023
P EliLilly102523POTW
<
0.001
/ mg/L
<
/
12/12/2023
S EhLilly121223Self
<
0.005
/ mg/L
<
/
Oct 2023
Week 4
<
0.001
/ mg/L
<
/
Dec 2023
Week 2
<
0.005
/ mg/L
<
/
Oct 2023
Average
<
0.001
/ mg/L
<
/
Dec 2023
Average
<
0.005
/ mg/L
<
/
2023
Quarter 4
<
0.003
/ mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.003
/ mg/L
<
/
2023
2nd 6 ...(Max)
<
0.005
/ mg/L
<
/
2023
2nd 6 ...(Min)
<
0.001
/ mg/L
<
/
2023
2nd 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2023
S
EliLilly0723FIow
08/31/2023
S
EliLilly0823F1ow
09/30/2023
S
EliLilly0923FIow
10/31/2023
S
EliLillyl023F1ow
11/30/2023
S
EliLillyll23F1ow
12/31/2023
S
EliLillyl223F1ow
Jul 2023
Week 4
Aug 2023
Week 4
Sep 2023
Week 4
Oct 2023
Week 4
Nov 2023
Week 4
Dec 2023
Week 4
Jul 2023
Average
Aug 2023
Average
Sep 2023
Average
Oct 2023
Average
Nov 2023
Average
Dec 2023
Average
2023
Quarter
2023
Quarter 4
2023
2nd 6 Months (Avg)
2023
2nd 6 ...(Max)
2023
2nd 6 ...(Min)
2023
2nd 6 ...(Count)
0.037585
/
MGD /
0.038799
/
MGD /
0.0461
/
MGD /
0.039052
/
MGD /
0.042173
/
MGD /
0.046437
/
MGD /
0.037585
/
MGD /
0.038799
/
MGD /
0.0461
/
MGD /
0.039052
/
MGD /
0.042173
/
MGD /
0.046437
/
MGD /
0.037585
/ 0.121481
MGD /
0.038799
/ 0.121481
MGD /
0.0461
/ 0.121481
MGD /
0.039052
/ 0.121481
MGD /
0.042173
/ 0.121481
MGD /
0.046437
/ 0.121481
MGD /
0.040828
/
MGD /
0.042554
/
MGD /
0.041691
/
MGD /
0.046437
/
MGD /
0.037585
/
MGD /
6
Saturday, February 24, 2024 1:57:50PM * Indicates Violation ** Indicates TRC Violation Page 1 of 10

Eli Lilly & Company
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
6
Months Sampled:
6
Weeks Sampled:
6
Quarters Sampled :
2
# Over Daily C :
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0,00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Samplc Date SamplelD Result/Limit Mass/Limit
BOD
10/25/2023
P E1iLi11y102523POTW
733
/ mg/L
/
12/12/2023
S EhLilly121223Self
132
/ mg/L
/
Oct 2023
Week 4
733
/ mg/L
/
Dec 2023
Week 2
132
/ mg/L
/
Oct 2023
Average
733
/ mg/L
/
Dec 2023
Average
132
/ mg/L
/
2023
Quarter 4
432.5
/ mg/L
/
2023
2nd 6 Months (Avg)
432.5
/ mg/L
/
2023
2nd 6 ...(Max)
733
/ mg/L
/
2023
2nd 6 ...(Min)
132
/ mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
10/25/2023
P EhLilly102523POTW
<
0.00008
/ mg/L
<
/
12/12/2023
S EliLilly121223Self
<
0.001
/ mg/L
<
/
Oct 2023
Week 4
<
0.00008
/ mg/L
<
/
Dec 2023
Week 2
<
0.001
/ mg/L
<
/
Oct 2023
Average
<
0.00008
/ mg/L
<
/
Dec 2023
Average
<
0.001
/ mg/L
<
/
2023
Quarter 4
<
0.00054
/ mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.00054
/ mg/L
<
/
2023
2nd 6 ...(Max)
<
0.001
/ mg/L
<
/
2023
2nd 6 ...(Min)
<
0.00008
/ mg/L
<
/
2023
2nd 6 ...(Count)
2
/
/
Sample Date
SamplelD
Result/Limit
Mass/Limit
Chloride
10/25/2023
P EhLi11y102523POTW
126 /
mg/L
/
12/12/2023
S EhLilly121223Se1f
60 /
mg/L
/
Oct 2023
Week 4
126 /
mg/L
/
Dec 2023
Week 2
60 /
mg/L
/
Oct 2023
Average
126 /
mg/L
/
Saturday, February 24, 2024 1:57:50PM * Indicates Violation ** Indicates TRC Violation Page 2 of 10

Eli Lilly & Company
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
Chloride
Dec 2023
Average
60 /
mg/L
/
2023
Quarter 4
93 /
mg/L
/
2023
2nd 6 Months (Avg)
93 /
mg/L
/
2023
2nd 6 ...(Max)
126 /
mg/L
/
2023
2nd 6 ...(Min)
60 /
mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass /Limit
Chromium
10/25/2023
P EliLillyl02523POTW
0.004 /
mg/L
/
12/12/2023
S EliLillyl21223Self
<
0.003 /
mg/L
<
/
Oct 2023
Week 4
0.004 /
mg/L
/
Dec 2023
Week 2
<
0.003 /
mg/L
<
/
Oct 2023
Average
0.004 /
mg/L
/
Dec 2023
Average
<
0.003 /
mg/L
<
/
2023
Quarter 4
<
0.003 /
mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.003 /
mg/L
<
/
2023
2nd 6 ...(Max)
0.004 /
mg/L
/
2023
2nd 6 ...(Min)
<
0.003 /
mg/L
<
/
2023
2nd 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
Copper
10/25/2023
P EliLi11yl02523POTW
0.084 /
mg/L
/
12/12/2023
S EhLilly121223Self
0.029 /
mg/L
/
Oct 2023
Week 4
0.084 /
mg/L
/
Dec 2023
Week 2
0.029 /
mg/L
/
Oct 2023
Average
0.084 /
mg/L
/
Dec 2023
Average
0.029 /
mg/L
/
2023
Quarter 4
0.057 /
mg/L
/
2023
2nd 6 Months (Avg)
0.057 /
mg/L
/
2023
2nd 6 ...(Max)
0.084 J
mg/L
/
2023
2nd 6 ...(Min)
0.029 /
mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
10/25/2023 P EliLillyl02523POTW <
0.003 /
mg/L <
/
12/12/2023 S EliLillyl21223Sclf <
0.003 /
mg/L <
/
Oct 2023 Week 4 <
0.003 /
mg/L <
/
Dec 2023 Week 2 <
0.003 /
mg/L <
/
Saturday, February 24, 2024 1:57:50PM
* Indicates Violation
** Indicates TRC Violation
Page 3 of 10

Eli Lilly & Company
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
Cyanide
Oct 2023
Average
<
0.003 /
mg/L
<
/
Dec 2023
Average
<
0.003 /
mg/L
<
/
2023
Quarter 4
<
0.003 /
mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.003 /
mg/L
<
/
2023
2nd 6 ...(Max)
<
0.003 /
mg/L
<
/
2023
2nd 6 ...(Min)
<
0.003 /
mg/L
<
/
2023
2nd 6 ...(Count)
2
Sample Date
SamplelD
Result /Limit
Mass /Limit
Fluoride
10/25/2023
P
EliLilly102523POTW
1.12 /
mg/L
/
12/12/2023
S
EhLilly121223Self
0.2 /
mg/L
/
Oct 2023
Week 4
1.12 /
mg/L
/
Dee 2023
Week 2
0.2 /
mg/L
/
Oct 2023
Average
1.12 /
mg/L
/
Dec 2023
Average
0.2 /
mg/L
/
2023
Quarter 4
0.66 /
mg/L
/
2023
2nd 6 Months (Avg)
0.66 /
mg/L
/
2023
2nd 6 ...(Max)
1.12 /
mg/L
/
2023
2nd 6 ...(Min)
0.2 /
mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
Lead
10/25/2023
P
EliLillyl02523POTW
0.0018 /
mg/L
/
12/12/2023
S
EliLilly 121223 Self
<
0.005 /
mg/L
<
/
Oct 2023
Week 4
0.0018 /
mg/L
/
Dec 2023
Week 2
<
0.005 /
mg/L
<
/
Oct 2023
Average
0.0018 /
mg/L
/
Dec 2023
Average
<
0.005 /
mg/L
<
/
2023
Quarter 4
<
0.0034 /
mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.0034 /
mg/L
<
/
2023
2nd 6 ...(Max)
<
0.005 /
mg/L
<
/
2023
2nd 6 ...(Min)
0.0018 /
mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
Mercury - LL
10/24/2023
P
EliLi11yl02423POTW
0.000039 / 0.000142
mg/L
/
Hg
12/12/2023
S
EliLilly121223Self
0.000027 / 0.000142
mg/L
/
Oct 2023
Week 4
0.000039 /
mg/L
/
Saturday, February 24, 2024 1:57:50PM * Indicates Violation ** Indicates TRC Violation Page 4 of 10

Eli Lilly & Company
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Mercury - LL
Dec 2023
Week 2
0.000027
/
mg/L
/
Oct 2023
Average
0.000039
/
mg/L
/
Dec 2023
Average
0.000027
/
mg/L
/
2023
Quarter 4
0.000033
/
mg/L
/
2023
2nd 6 Months (Avg) 0.000033
/
mg/L
/
2023
2nd 6 ...(Max)
0.000039
/
mg/L
/
2023
2nd 6 ...(Min)
0.000027
/
mg/L
/
2023
2nd 6 •..(Count)
2
Sample Count: 2
Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C :
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC: 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass /Limit
Molybdenum
10/25/2023 P
EliLilly102523POTW
0.0024
/ mg/L
/
12/12/2023 S
EliLillyl21223Self
<
0.0025
/ mg/L
<
/
Oct 2023
Week 4
0.0024
/ mg/L
/
Dec 2023
Week 2
<
0.0025
/ mg/L
<
/
Oct 2023
Average
0.0024
/ mg/L
/
Dec 2023
Average
<
0.0025
/ mg/L
<
/
2023
Quarter 4
<
0.0025
/ mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.0025
/ mg/L
<
/
2023
2nd 6 ...(Max)
<
0.0025
/ mg/L
<
/
2023
2nd 6 ...(Min)
0.0024
/ mg/L
/
2023
2nd 6 ...(Count)
2
SarnpleDate SamplelD Result/Limit Mass/Lunit
Nickel
10/25/2023
P EliLiHy102523POTW
12/12/2023
S EhLilly121223Self
Oct 2023
Week 4
Dec 2023
Week 2
Oct 2023
Average
Dec 2023
Average
2023
Quarter 4
2023
2nd 6 Months (Avg)
0.0056
/ mg/L /
0.012
/ mg/L /
0.0056
/ mg/L /
0.012
/ mg/L /
0.0056
/ mg/L /
0.012
/ mg/L /
0.0088
/ mg/L /
0.0088
/ mg/L /
Saturday, February 24, 2024 1:57:50PM * Indicates Violation ** Indicates TRC Violation Page 5 of 10

Eli Lilly & Company
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
Nickel
2023
2nd 6 ...(Max)
0.012 /
mg/L
/
2023
2nd 6 ...(Min)
0.0056 /
mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
Nitrate -Nitrite
10/25/2023
P
EliLilly102523POTW
<
0.1 /
mg/L
<
/
12/12/2023
S
EliLilly121223Sclf
0.4 /
mg/L
/
Oct 2023
Week 4
<
0.1 /
mg/L
<
/
Dec 2023
Week 2
0.4 /
mg/L
/
Oct 2023
Average
<
0.1 /
mg/L
<
/
Dec 2023
Average
0.4 /
mg/L
/
2023
Quarter 4
<
0.2 /
mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.2 /
mg/L
<
/
2023
2nd 6 ...(Max)
0.4 /
mg/L
/
2023
2nd 6 ...(Min)
<
0.1 /
mg/L
<
/
2023
2nd 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
Nitrogen, Total
10/25/2023
P
E1iLi11yl02523P0TW
177 /
mg/L
/
12/12/2023
S
Elil illy121223Self
52.5 /
mg/L
/
Oct 2023
Week 4
177 /
mg/L
/
Dec 2023
Week 2
52.5 /
mg/L
/
Oct 2023
Average
177 /
mg/L
/
Dec 2023
Average
52.5 /
mg/L
/
2023
Quarter 4
114.75 /
mg/L
/
2023
2nd 6 Months (Avg)
114.75 /
mg/L
/
2023
2nd 6 ...(Max)
177 /
mg/L
/
2023
2nd 6 ...(Min)
52.5 /
mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass /Limit
Oil & Grease, Total
10/25/2023
P
EliLilly102523POTW
10 1200
mg/L
/
12/12/2023
S
EliLil1yl21223Se1f
<
2.5 / 200
mg/L
<
/
Oct 2023
Week 4
10 /
mg/L
/
Dec 2023
Week 2
<
2.5 /
mg/L
<
/
Oct 2023
Average
10 /
mg/L
/
Dec 2023
Average
<
2.5 /
mg/L
<
/
2023
Quarter 4
<
6.25 /
mg/L
<
/
Saturday, February 24, 2024 1:57:50PM * Indicates Violation ** Indicates TRC Violation Page 6 of 10

Eli Lilly & Company
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Oil & Grease, Total
2023
2nd 6 Months (Avg) <
6.25 /
mg/L <
/
2023
2nd 6 ...(Max)
10 /
mg/L
/
2023
2nd 6 ...(Min)
<
2.5 /
mg/L <
/
2023
2nd 6 ...(Count)
2 /
/
Sample Count: 2
Months Sampled
:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M:
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass /Limit
pH
10/25/2023 P
EliLilly102523POTW
7.8
/ 6.0 - 10.0
SU
/
12/12/2023 S
EliLilly121223Self
6.8
/ 6.0 - 10.0
SU
/
Oct 2023
Week 4
7.8
/
SU
/
Dec 2023
Week 2
6.8
/
SU
/
Oct 2023
Average
7.8
/
SU
/
Dec 2023
Average
6.8
/
SU
/
2023
Quarter 4
7.3
/
SU
/
2023
2nd 6 Months (Avg)
7.3
/
SU
/
2023
2nd 6 ...(Max)
7.8
/
SU
/
2023
2nd 6 ...(Min)
6.8
/
SU
/
2023
2nd 6 ...(Count)
2
Sample Count: 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Selenium
10/25/2023
P EliLillyl02523POTW
0.0026 /
mg/L
/
12/12/2023
S EliLilly 121223 Self <
0.005 /
mg/L <
/
Oct 2023
Week 4
0.0026 /
mg/L
/
Dec 2023
Week 2 <
0.005 /
mg/L <
/
Saturday, February 24, 2024 1:57:50PM * Indicates Violation ** Indicates TRC Violation Page 7 of 10

Eli Lilly & Company
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
Selenium
Oct 2023
Average
0.0026 /
mg/L
/
Dec 2023
Average
<
0.005 /
mg/L
<
/
2023
Quarter
<
0.0038 /
mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.0038 /
mg/L
<
/
2023
2nd 6 ...(Max)
<
0.005 /
mg/L
<
/
2023
2nd 6 ...(Min)
0.0026 /
mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date
SamplelD
Result /Limit
Mass /Limit
Silver
10/25/2023
P
EliLilly102523POTW
<
0.0003 /
mg/L
<
/
12/12/2023
S
EliLillyl21223Self
<
0.0025 /
mg/L
<
/
Oct 2023
Week 4
<
0.0003 /
mg/L
<
/
Dee 2023
Week 2
<
0.0025 /
mg/L
<
/
Oct 2023
Average
<
0.0003 /
mg/L
<
/
Dec 2023
Average
<
0.0025 /
mg/L
<
/
2023
Quarter 4
<
0.0014 /
mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.0014 /
mg/L
<
/
2023
2nd 6 ...(Max)
<
0.0025 /
mg/L
<
/
2023
2nd 6 ...(Min)
<
0.0003 /
mg/L
<
/
2023
2nd 6 ...(Count)
2 /
/
Sample Date
SamplelD
Result/Limit
Mass/Limit
Temperature
10/25/2023
P
EliLillyl02523POTW
24 / 66
°C
/
12/12/2023
S
EhLilly 121223 Self
16 / 66
°C
/
Oct 2023
Week 4
24 /
°C
/
Dec 2023
Week 2
16 /
°C
/
Oct 2023
Average
24 /
°C
/
Dec 2023
Average
16 /
°C
/
2023
Quarter 4
20 /
°C
/
2023
2nd 6 Months (Avg)
20 /
°C
/
2023
2nd 6 ...(Max)
24 /
°C
/
2023
2nd 6 ...(Min)
16 /
°C
/
2023
2nd 6 ...(Count)
2
Saturday, February 24, 2024 1:57:50PM * Indicates Violation ** Indicates TRC Violation Page 8 of 10

Eli Lilly & Company
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
2
Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C :
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0,00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Samplc Date SamplelD Result/Limit Mass/Limit
TKN
10/25/2023
P E1iLi11y102523POTW
177
/ mg/L
/
12/12/2023
S EhLilly121223Self
52.1
/ mg/L
/
Oct 2023
Week 4
177
/ mg/L
/
Dec 2023
Week 2
52.1
/ mg/L
/
Oct 2023
Average
177
/ mg/L
/
Dec 2023
Average
52.1
/ mg/L
/
2023
Quarter 4
114.55
/ mg/L
/
2023
2nd 6 Months (Avg)
114.55
/ mg/L
/
2023
2nd 6 ...(Max)
177
/ mg/L
/
2023
2nd 6 ...(Min)
52.1
/ mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass /Limit
Total Phosphorus
10/25/2023 P
EhLilly102523POTW
20.9
/ mg/L
/
12/12/2023 S
EliLilly121223Self
3.73
/ mg/L
/
Oct 2023
Week 4
20.9
/ mg/L
/
Dec 2023
Week 2
3.73
/ mg/L
/
Oct 2023
Average
20.9
/ mg/L
/
Dec 2023
Average
3.73
/ mg/L
/
2023
Quarter 4
12.315
/ mg/L
/
2023
2nd 6 Months (Avg)
12.315
/ mg/L
/
2023
2nd 6 ...(Max)
20.9
/ mg/L
/
2023
2nd 6 ...(Min)
3.73
/ mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
TSS
10/25/2023
P EhLi11y102523POTW
331 /
mg/L
/
12/12/2023
S EhLilly121223Self
55 /
mg/L
/
Oct 2023
Week 4
331 /
mg/L
/
Dec 2023
Week 2
55 /
mg/L
/
Oct 2023
Average
331 /
mg/L
/
Saturday, February 24, 2024 1:57:50PM * Indicates Violation ** Indicates TRC Violation Page 9 of 10

Eli Lilly & Company
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
TSS
Dec 2023
Average
55 /
mg/L
/
2023
Quarter 4
193 /
mg/L
/
2023
2nd 6 Months (Avg)
193 /
mg/L
/
2023
2nd 6 ...(Max)
331 /
mg/L
/
2023
2nd 6 ...(Min)
55 /
mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass /Limit
voc
10/25/2023
P EliLillyl02523POTW
0.174 /
mg/L
/
12/12/2023
S EliLillyl21223Self
0.126 /
mg/L
/
Oct 2023
Week 4
0.174 /
mg/L
/
Dec 2023
Week 2
0.126 /
mg/L
/
Oct 2023
Average
0.174 /
mg/L
/
Dec 2023
Average
0.126 /
mg/L
/
2023
Quarter 4
0.15 /
mg/L
/
2023
2nd 6 Months (Avg)
0.15 /
mg/L
/
2023
2nd 6 ...(Max)
0.174 /
mg/L
/
2023
2nd 6 ...(Min)
0.126 /
mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
Zinc
10/25/2023
P EliLi11yl02523POTW
0.591
/ mg/L
/
12/12/2023
S EhLilly121223Self
0.253
/ mg/L
/
Oct 2023
Week 4
0.591
/ mg/L
/
Dec 2023
Week 2
0.253
/ mg/L
/
Oct 2023
Average
0.591
/ mg/L
/
Dec 2023
Average
0.253
/ mg/L
/
2023
Quarter 4
0.422
/ mg/L
/
2023
2nd 6 Months (Avg)
0.422
/ mg/L
/
2023
2nd 6 ...(Max)
0.591
/ mg/L
/
2023
2nd 6 ...(Min)
0.253
/ mg/L
/
2023
2nd 6 ...(Count)
2
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 002
Sample Date SamplelD Result/Limit Mass /Limit
Average Flow for Month
07/31/2023 S EliLillyP20723F1ow 0.008008 / MGD /
08/31/2023 S EliLillyP20823F1ow 0.007453 / MGD /
Saturday, February 24, 2024 1:57:50PM * Indicates Violation ** Indicates TRC Violation Page 10 of 10

Eli Lilly & Company
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 002
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
09/30/2023
S
EliLiiyP20923F1ow
0.010656
/
MGD /
10/31/2023
S
EliLillyP21023F1ow
0.016758
/
MGD /
11/30/2023
S
EliLillyP21123F1ow
0.020418
/
MGD /
12/31/2023
S
EliLillyP21223F1ow
0.021715
/
MGD /
Jul 2023
Week 4
0.008008
/
MGD /
Aug 2023
Week 4
0.007453
/
MGD /
Sep 2023
Week 4
0.010656
/
MGD /
Oct 2023
Week 4
0.016758
/
MGD /
Nov 2023
Week 4
0.020418
/
MGD /
Dee 2023
Week 4
0.021715
/
MGD /
Jul 2023
Average
0.008008
/ 0.061413
MGD /
Aug 2023
Average
0.007453
/ 0.061413
MGD /
Sep 2023
Average
0.010656
/ 0.061413
MGD /
Oct 2023
Average
0.016758
/ 0.061413
MGD /
Nov 2023
Average
0.020418
/ 0.061413
MGD /
Dec 2023
Average
0.021715
/ 0.061413
MGD /
2023
Quarter 3
0.008706
/
MGD /
2023
Quarter 4
0.01963
/
MGD /
2023
2nd 6 Months (Avg)
0.014168
/
MGD /
2023
2nd 6 ...(Max)
0.021715
/
MGD /
2023
2nd 6 ...(Min)
0.007453
/
MGD /
2023
2nd 6 ...(Count)
6
Sample Count:
6
Months Sampled:
6
Weeks Sampled:
6
Quarters Sampled :
2
# Over Daily C:
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0
0.00
# Over Mo Avg M TRC: 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Saturday, February 24, 2024 1:57:50PM * Indicates Violation ** Indicates TRC Violation Page 1 of 1

Micross Advanced Interconnect Technolo2y, LLC
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
Aluminum
07/14/2023
S Micross071423Self
0.034
/
mg/L
/
10/19/2023
P Micross101923POTW
0.363
/
mg/L
0.09619 /
lbs/day
Jul 2023
Week 2
0.034
/
mg/L
/
Oct 2023
Week 3
0.363
/
mg/L
0.09619 /
Ibs/day
Jul 2023
Average
0.034
/
mg/L
/
Oct 2023
Average
0.363
/
mg/L
0.09619 /
Ibs/day
2023
Quarter 3
0.034
/
mg/L
/
2023
Quarter 4
0.363
/
mg/L
0.09619 /
Ibs/day
2023
2nd 6 Months (Avg)
0.199
/
mg/L
0.096190 /
Ibs/day
2023
2nd 6 ...(Max)
0.363
/
mg/L
0.096190 /
lbs/day
2023
2nd 6 ...(Min)
0.034
/
mg/L
/
2023
2nd 6 ...(Count)
2
/
1 /
Sample Date
SamplelD
Result/Limit
Mass/Limit
Ammonia
07/14/2023
S Micross071423Self
0.71
/
mg/L
/
10/19/2023
P Micross101923POTW
3.8
/
mg/L
1.0069 /
Ibs/day
Jul 2023
Week 2
0.71
/
mg/L
/
Oct 2023
Week 3
3.8
/
mg/L
1.0069 /
Ibs/day
Jul 2023
Average
0.71
/
mg/L
/
Oct 2023
Average
3.8
/
mg/L
1.0069 /
lbs/day
2023
Quarter 3
0.71
/
mg/L
/
2023
Quarter 4
3.8
/
mg/L
1.0069 /
lbs/day
2023
2nd 6 Months (Avg)
2.26
/
mg/L
1.0070 /
lbs/day
2023
2nd 6 ...(Max)
3.8
/
mg/L
1.0069 /
Ibs/day
2023
2nd 6 ...(Min)
0.71
/
mg/L
/
2023
2nd 6 ...(Count)
2
/
1 /
Sample Date
SamplelD
Result/Limit
Mass /Limit
Average Flow for Month
07/31/2023
S
Micross0723F1ow
08/31/2023
S
Micross0823F1ow
08/31/2023
S
Micross0923F1ow
10/31/2023
S
Micross1023FIow
11/30/2023
S
Micross1123FIow
12/31/2023
S
Micross1223FIow
Jul 2023
Week 4
Aug 2023
Week 4
Oct 2023
Week 4
Nov 2023
Week 4
Dee 2023
Week 4
Jul 2023
Average
0.04916
/ 0.100
MGD /
0.052827
/ 0.100
MGD /
0.044861
/ 0.100
MGD /
0.038339
/ 0.100
MGD /
0.027912
/ 0.100
MGD /
0.030078
/ 0.100
MGD /
0.04916
/
MGD /
0.048844
/
MGD /
0.038339
/
MGD /
0.027912
/
MGD /
0.030078
/
MGD /
0.04916
/ 0.075
MGD /
Saturday, February 24, 2024 6:04:27PM * Indicates Violation ** Indicates TRC Violation Page 1 of 7

Micross Advanced Interconnect Technolo2y, LLC
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater 0111M11: '001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Mouth
Aug 2023
Average
0.048844
/ 0.075
MGD
/
Oct 2023
Average
0.038339
/ 0.075
MGD
/
Nov 2023
Average
0.027912
/ 0.075
MGD
/
Dec 2023
Average
0.030078
/ 0.075
MGD
/
2023
Quarter 3
0.048949
/
MGD
/
2023
Quarter 4
0.03211
/
MGD
/
2023
2nd 6 Months (Avg)
0.040530
/
MGD
/
2023
2nd 6 ...(Max)
0.052827
/
MGD
/
2023
2nd 6 ...(Min)
0.027912
/
MGD
/
2023
2nd 6 ...(Count)
6
Sample Count: 6 Months Sampled:
5
Weeks Sampled:
5 Quarters Sampled :
2
# Over Daily C:
0 0.00 # Over Mo Avg C :
0 0.00
# Over Wk Avg C :
0
0.00 # Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC
:
0 0.00
# Over Wk Avg C TRC :
0
0.00 # Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0 0.00
# Over Wk Avg M :
0
0.00 # Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC
:
0 0.00
# Over Wk Avg M TRC :
0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Resalt/Limit
Mass/Limit
Chloride
07/14/2023 S
Micross071423Self
140
/
mg/L
/
10/19/2023 P
Micross101923POTW
33.3
/
mg/L
8.8241 / lbs/day
Jul 2023
Week 2
140
/
mg/L
/
Oct 2023
Week 3
33.3
/
mg/L
8.8241 / lbs/day
Jul 2023
Average
140
/
mg/L
/
Oct 2023
Average
33.3
/
mg/L
8.8241 / Ibs/day
2023
Quarter 3
140
/
mg/L
/
2023
Quarter 4
33.3
/
mg/L
8.8241 / Ibs/day
2023
2nd 6 Months (Avg)
86.65
/
mg/L
8.8241 / Ibs/day
2023
2nd 6 ...(Max)
140
/
mg/L
8.8241 / lbs/day
2023
2nd 6 ...(Min)
33.3
/
mg/L
/
2023
2nd 6 ...(Count)
2
/
1 /
Sample Date
SQmpleID
Result/Limit
Mass/Limit
Chromium
07/14/2023
S Micross071423Self
0.004 /
mg/L
/
10/19/2023
P MicrossI01923POTW <
0.001 /
mg/L
< 0.000265 / Ibs/day
Jul 2023
Week 2
0.004 /
mg/L
/
Oct 2023
Week 3 <
0.001 /
mg/L
< 0.000265 / Ibs/day
Jul 2023
Average
0.004 /
mg/L
/
Saturday, February 24, 2024 6:04:27PM * Indicates Violation ** Indicates TRC Violation Page 2 of 7

Micross Advanced Interconnect Technolo2y, LLC
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: '001
Sample Date
SamplelD
Result/Limit
Mass/Limit
Chromium
Oct 2023
Average <
0.001
/
mg/L
< 0.000265 /
Ibs/day
2023
Quarter 3
0.004
/
mg/L
/
2023
Quarter 4 <
0.001
/
mg/L
< 0.000265 /
lbs/day
2023
2nd 6 Months (Avg) <
0.002
/
mg/L
< 0.000265 /
Ibs/day
2023
2nd 6 ...(Max)
0.004
/
mg/L
0.000265 /
Ibs/day
2023
2nd 6 ...(Min) <
0.001
/
mg/L
< /
2023
2nd 6 ...(Count)
2
/
1 /
Sample Date
SamplelD
Result /Limit
Mass /Limit
Copper
07/14/2023
S
Micross071423Self
0.054
/
mg/L
/
10/19/2023
P
MicrossI01923POTW
0.028
/
mg/L
0.007526 /
Ibs/day
Ju12023
Week 2
0.054
/
mg/L
/
Oct 2023
Week 3
0.028
/
mg/L
0.007526 /
lbs/day
Ju12023
Average
0.054
/
mg/L
/
Oct 2023
Average
0.028
/
mg/L
0.007526 /
lbs/day
2023
Quarter 3
0.054
/
mg/L
/
2023
Quarter 4
0.028
/
mg/L
0.007526 /
Ibs/day
2023
2nd 6 Months (Avg)
0.041
/
mg/L
0.007526 /
Ibs/day
2023
2nd 6 ...(Max)
0.054
/
mg/L
0.007526 /
Ibs/day
2023
2nd 6 ...(Min)
0.028
/
mg/L
/
2023
2nd 6 ...(Count)
2
/
1 /
Sample Date
SamplelD
Result/Limit
Mass/Limit
Fluoride
07/14/2023
S
Mieross071423Self
1.4
/
mg/L
/
10/19/2023
P
MicrossI01923POTW
1.68
/
mg/L
0.4452 /
lbs/day
Jul 2023
Week 2
1.4
/
mg/L
/
Oct 2023
Week 3
1.68
/
mg/L
0.4452 /
Ibs/day
Jul 2023
Average
1.4
/
mg/L
/
Oct 2023
Average
1.68
/
mg/L
0.4452 /
Ibs/day
2023
Quarter 3
1.4
J
mg/L
/
2023
Quarter 4
1.68
/
mg/L
0.4452 /
lbs/day
2023
2nd 6 Months (Avg)
1.54
/
mg/L
0.4452 /
lbs/day
2023
2nd 6 ...(Max)
1.68
/
mg/L
0.4452 /
lbs/day
2023
2nd 6 ...(Min)
1.4
/
mg/L
/
2023
2nd 6 ...(Count)
2
/
1 /
Sample Date
SamplelD
Result/Limit
Mass /Limit
Mercury - LL
07/14/2023
S
Micross071423Self
0.000011
/ 0.000142
mg/L
/
Saturday, February 24, 2024 6:04:27PM * Indicates Violation ** Indicates TRC Violation Page 3 of 7

Micross Advanced Interconnect Technolo2y, LLC
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: '001
SarnpleDate SamplelD Result/Limit Mass/Limit
Mercury - LL
07/26/2023 S
Micross072623Selfl4g
0.000006
/ 0.000142
mg/L
/
10/19/2023 P
M1crossI01923POTW
0.00001
/ 0.000142
mg/L
/
Hg
Jul 2023
Week 2
0.000011
/
mg/L
/
Jul 2023
Week 4
0.000006
/
mg/L
/
Oct 2023
Week 3
0.00001
/
mg/L
/
Jul 2023
Average
0.000009
/
mg/L
/
Oct 2023
Average
0.00001
/
mg/L
/
2023
Quarter 3
0.000009
/
mg/L
/
2023
Quarter 4
0.00001
/
mg/L
/
2023
2nd 6 Months (Avg)
0.000009
/
mg/L
/
2023
2nd 6 ...(Max)
0.000011
/
mg/L
/
2023
2nd 6 ...(Min)
0.000006
/
mg/L
/
2023
2nd 6 ...(Count)
3
Sample Count: 3 Months Sampled:
2
Weeks Sampled:
3
Quarters Sampled :
2
# Over Daily C :
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC
:
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC: 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass /Limit
Nickel
07/14/2023
S Micross071423Self
0.011
/ mg/L
/
10/19/2023
P Micross101923POTW
0.0142
/ mg/L
0.003763 /
Ibs/day
Jul 2023
Week 2
0.011
/ mg/L
/
Oct 2023
Week 3
0.0142
/ mg/L
0.003763 /
Ibs/day
Jul 2023
Average
0.011
/ mg/L
/
Oct 2023
Average
0.0142
/ mg/L
0.003763 /
lbs/day
2023
Quarter 3
0.011
/ mg/L
/
2023
Quarter 4
0.0142
/ mg/L
0.003763 /
lbs/day
2023
2nd 6 Months (Avg)
0.0126
/ mg/L
0.003763 /
lbs/day
2023
2nd 6 ...(Max)
0.0142
/ mg/L
0.003763 /
lbs/day
2023
2nd 6 ...(Min)
0.011
/ mg/L
/
2023
2nd 6 ...(Count)
2
/
1 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate -Nitrite
07/14/2023 S Micross071423Self 0.5 / mg/L /
10/19/2023 P MicrossI01923POTW 1.9 / mg/L 0.514 / Ibs/day
Saturday, February 24, 2024 6:04:27PM * Indicates Violation ** Indicates TRC Violation Page 4 of 7

Micross Advanced Interconnect Technolou, LLC
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate -Nitrite
Jul 2023
Week 2
0.5
/ mg/L
/
Oct 2023
Week 3
1.9
/ mg/L
0.514 /
lbs/day
Jul 2023
Average
0.5
/ mg/L
/
Oct 2023
Average
1.9
/ mg/L
0.514 /
Ibs/day
2023
Quarter 3
0.5
/ mg/L
/
2023
Quarter 4
1.9
/ mg/L
0.514 /
Ibs/day
2023
2nd 6 Months (Avg)
1.2
/ mg/L
0.514 /
Ibs/day
2023
2nd 6 ...(Max)
1.9
/ mg/L
0.514 /
Ibs/day
2023
2nd 6 ...(Min)
0.5
/ mg/L
/
2023
2nd 6 ...(Count)
2
/
1 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen, Total
07/14/2023 S
Micross071423Self
8.5
/ mg/L
/
10/19/2023 P
MicrossI01923POTW
14.4
/ mg/L
3.816 /
lbs/day
Jul 2023
Week 2
8.5
/ mg/L
/
Oct 2023
Week 3
14.4
/ mg/L
3.816 /
Ibs/day
Jul 2023
Average
8.5
/ mg/L
/
Oct 2023
Average
14.4
/ mg/L
3.816 /
Ibs/day
2023
Quarter 3
8.5
/ mg/L
/
2023
Quarter 4
14.4
/ mg/L
3.816 /
lbs/day
2023
2nd 6 Months (Avg)
11.45
/ mg/L
3.816 /
lbs/day
2023
2nd 6 ...(Max)
14.4
/ mg/L
3.816 /
lbs/day
2023
2nd 6 ...(Min)
8.5
/ mg/L
/
2023
2nd 6 ...(Count)
2
/
1 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil & Grease, Total
10/19/2023 P
MicrossI01923POTW
<
2.5
/ 200
mg/L
< /
Oct 2023
Week 3
<
2.5
/
mg/L
< /
Oct 2023
Average
<
2.5
/
mg/L
< /
2023
Quarter 4
<
2.5
/
mg/L
< /
2023
2nd 6 Months (Avg)
<
2.5
/
mg/L
< /
2023
2nd 6 ...(Max)
<
2.5
/
mg/L
< /
2023
2nd 6 ...(Min)
<
2.5
/
mg/L
< /
2023
2nd 6 ...(Count)
I
Saturday, February 24, 2024 6:04:27PM * Indicates Violation ** Indicates TRC Violation Page 5 of 7

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: '001
Sample Count:
1
Months Sampled :
1
Weeks Sampled:
1
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
PH
07/14/2023 S
Micross071423Self
7.4
/ 5.5 - 10.5
SU
/
07/26/2023 S
Micross072623SelfHg
9.1
/ 5.5 - 10.5
SU
/
10/19/2023 P
MicrossI01923POTW
7.1
/ 5.5 - 10.5
SU
/
Jul 2023
Week 2
7.4
/
SU
/
Jul 2023
Week 4
9.1
/
SU
/
Oct 2023
Week 3
7.1
/
SU
/
Ju12023
Average
8.25
/
Su
/
Oct 2023
Average
7.1
/
Su
/
2023
Quarter 3
8.25
/
SU
/
2023
Quarter 4
7.1
/
SU
/
2023
2nd 6 Months (Avg)
7.87
/
SU
/
2023
2nd 6 ...(Max)
9.1
/
SU
/
2023
2nd 6 ...(Min)
7.1
/
SU
/
2023
2nd 6 ...(Count)
3
Sample Count: 3 Months Sampled:
2
Weeks Sampled :
3
Quarters Sampled :
2
# Over Daily C:
0 0.00 # Over Mo Avg C :
0 0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0 0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0 0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC :
0 0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
07/14/2023
S Micross071423Self
24.2
/ 66
°C /
07/26/2023
S Micross072623SelfHg
25.7
/ 66
°C /
10/19/2023
P Micross101923POTW
22
/ 66
°C /
Jul 2023
Week 2
24.2
/
G /
Jul 2023
Week 4
25.7
/
°C /
Oct 2023
Week 3
22
/
°C /
Jul 2023
Average
25
/
°C /
Oct 2023
Average
22
/
°C /
2023
Quarter 3
25
/
°C /
Saturday, February 24, 2024 6:04:27PM * Indicates Violation ** Indicates TRC Violation Page 6 of 7

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Lunit
Temperature
2023
Quarter 4
22
J
°C
/
2023
2nd 6 Months (Avg)
24.0
/
°C
/
2023
2nd 6 ...(Max)
25.7
/
°C
/
2023
2nd 6 ...(Min)
22
/
°C
/
2023
2nd 6 ...(Count)
3
Sample Count: 3
Months Sampled:
2
Weeks Sampled :
3
Quarters Sampled :
2
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
07/14/2023
S Micross071423Self
8
/ mg/L
/
10/19/2023
P Micross101923POTW
12.5
/ mg/L
3.312 /
lbs/day
Jul 2023
Week 2
8
/ mg/L
/
Oct 2023
Week 3
12.5
/ mg/L
3.312 /
Ibs/day
Jul 2023
Average
8
/ mg/L
/
Oct 2023
Average
12.5
/ mg/L
3.312 /
Ibs/day
2023
Quarter 3
8
/ mg/L
/
2023
Quarter 4
12.5
/ mg/L
3.312 /
lbs/day
2023
2nd 6 Months (Avg)
10.25
/ mg/L
3.312 /
lbs/day
2023
2nd 6 ...(Max)
12.5
/ mg/L
3.312 /
lbs/day
2023
2nd 6 ...(Min)
8
/ mg/L
/
2023
2nd 6 ...(Count)
2
/
I /
Saturday, February 24, 2024 6:04:27PM * Indicates Violation ** Indicates TRC Violation Page 7 of 7

MP Pharma Services, Inc.
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
07/27/2023 P
MPPharma072723POT
<
0.025
/ 20.7
mg/L
<
/
W
08/23/2023 S
MPPharma082323Self
<
0.013
/ 20.7
mg/L
<
/
Jul 2023
Week 4
<
0.025
/
mg/L
<
/
Aug 2023
Week 4
<
0.013
/
mg/L
<
/
Jul 2023
Average
<
0.025
/ 8.2
mg/L
<
/
Aug 2023
Average
<
0.013
/ 8.2
mg/L
<
/
2023
Quarter 3
<
0.019
/
mg/L
<
/
2023
2nd 6 Months (Avg) <
0.019
/
mg/L
<
/
2023
2nd 6 ...(Max)
<
0.025
/
mg/L
<
/
2023
2nd 6 ...(Min)
<
0.013
/
mg/L
<
/
2023
2nd 6 ...(Count)
2
Sample Count: 2
Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C :
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC
:
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
Average Flow for Month
07/31/2023
S
MPPharma0723F1ow
08/31/2023
S
MPPharma0823F1ow
09/30/2023
S
MPPharma0923F1ow
10/31/2023
S
MPPharma1023F1ow
11/30/2023
S
MPPharma1123171ow
Jul 2023
Week 4
Aug 2023
Week 4
Sep 2023
Week 4
Oct 2023
Week 4
Nov 2023
Week 4
Ju12023
Average
Aug 2023
Average
Sep 2023
Average
Oct 2023
Average
Nov 2023
Average
2023
Quarter 3
2023
Quarter 4
2023
2nd 6 Months (Avg)
2023
2nd 6 ...(Max)
0.002431
/
MGD /
0.00163
/
MGD /
0.001127
/
MGD /
0.000694
/
MGD /
0.000562
/
MGD /
0.002431
/
MGD /
0.00163
/
MGD /
0.001127
/
MGD /
0.000694
/
MGD /
0.000562
/
MGD /
0.002431
/ 0.002
MGD * /
0.00163
/ 0.002
MGD /
0.001127
/ 0.002
MGD /
0.000694
/ 0.002
MGD /
0.000562
/ 0.002
MGD /
0.001729
/
MGD /
0.000628
/
MGD /
0.001289
/
MGD /
0.002431
/
MGD /
Saturday, February 24, 2024 6:18:42PM * Indicates Violation ** Indicates TRC Violation Page 1 of 5

MP Pharma Services, Inc.
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
2023 2nd 6
...(Min)
0.000562
/
MGD
/
2023 2nd 6
...(Count)
5
/
/
Sample Count :
5
Months Sampled:
5
Weeks Sampled:
5
Quarters Sampled :
2
# Over Daily C: 0
0.00
# Over Mo Avg C :
1
20.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC: 0
0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M : 0
0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC : 0
0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily : 0
0.00
# Under Daily TRC: 0
0.00
Sample Date SamplelD Result/Limit
Ethyl acetate
Mass/Limit
07/27/2023 P
MPPharma072723POT <
0.005
/ 20.7
mg/L
<
/
W
08/23/2023 S
MPPharma082323Self <
0.05
/ 20.7
mg/L
<
/
Jul 2023
Week 4 <
0.005
/
mg/L
<
/
Aug 2023
Week 4 <
0.05
/
mg/L
<
/
Jul 2023
Average <
0.005
/ 8.2
mg/L
<
/
Aug 2023
Average <
0.05
/ 8.2
mg/L
<
/
2023
Quarter 3 <
0.028
/
mg/L
<
/
2023
2nd 6 Months (Avg) <
0.028
/
mg/L
<
/
2023
2nd 6 ...(Max) <
0.05
/
mg/L
<
/
2023
2nd 6 ...(Min) <
0.005
/
mg/L
<
/
2023
2nd 6 ...(Count)
2
Sample Count : 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
I
# Over Daily C:
0 0.00 # Over Mo Avg C:
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
07/27/2023 P
MPPhartna072723POT <
W
08/23/2023 S
MPPharma082323Self <
Jul 2023
Week 4 <
Aug 2023
Week 4 <
Jul 2023
Average <
0.005 / 20.7 mg/L < /
0.05 / 20.7 mg/L < /
0.005 / mg/L < /
0.05 / mg/L < /
0.005 / 8.2 mg/L < /
Saturday, February 24, 2024 6:18:42PM * Indicates Violation ** Indicates TRC Violation Page 2 of 5

MP Pharma Services, Inc.
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
Aug 2023
Average
< 0.05
/ 8.2
mg/L
<
/
2023
Quarter 3
< 0.028
/
mg/L
<
/
2023
2nd 6 Months (Avg) < 0.028
/
mg/L
<
/
2023
2nd 6 ...(Max)
< 0.05
/
mg/L
<
/
2023
2nd 6 ...(Min)
< 0.005
/
mg/L
<
/
2023
2nd 6 ...(Count)
2
Sample Count: 2
Months Sampled
:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C :
0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC :
0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M :
0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC :
0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
Mercury - LL
07/27/2023 P
MPPharm072723POT
0.000006
/ 0.000142
mg/L
/
WHg
08/23/2023 S
MPPharma082323Self
< 0.000001
/ 0.000142
mg/L
<
/
Jul 2023
Week 4
0.000006
/
mg/L
/
Aug 2023
Week 4
< 0.000001
/
mg/L
<
/
Jul 2023
Average
0.000006
/
mg/L
/
Aug 2023
Average
< 0.000001
/
mg/L
<
/
2023
Quarter 3
< 0.000003
/
mg/L
<
/
2023
2nd 6 Months (Avg) < 0.000003
/
mg/L
<
/
2023
2nd 6 ...(Max)
0.000006
/
mg/L
/
2023
2nd 6 ...(Min)
< 0.000001
/
mg/L
<
/
2023
2nd 6 ...(Count)
2
Sample Count: 2
Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C :
0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC :
0
0.00
# Over Daily M:
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M :
0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC :
0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
07/27/2023 P MPPharma072723POT < 0.005 / 3.0 mg/L < /
W
Saturday, February 24, 2024 6:18:42PM * Indicates Violation ** Indicates TRC Violation Page 3 of 5

MP Pharma Services, Inc.
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
08/23/2023 S
MPPharma082323Self
<
0.003
/ 3.0
mg/L
< /
Jul 2023
Week 4
<
0.005
/
mg/L
< /
Aug 2023
Week 4
<
0.003
/
mg/L
< /
Jul 2023
Average
<
0.005
/ 0.7
mg/L
< /
Aug 2023
Average
<
0.003
/ 0.7
mg/L
< /
2023
Quarter 3
<
0.004
/
mg/L
< /
2023
2nd 6 Months (Avg)
<
0.004
/
mg/L
< /
2023
2nd 6 ...(Max)
<
0.005
/
mg/L
< /
2023
2nd 6 ...(Min)
<
0.003
/
mg/L
< /
2023
2nd 6 ...(Count)
2
/
/
Sample Count:
2
Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
07/27/2023 P
MPPharma072723POT <
0.005
/ 20.7
mg/L
<
/
W
08/23/2023 S
MPPhanna082323Self <
0.025
/ 20.7
mg/L
<
/
Jul 2023
Week 4 <
0.005
/
mg/L
<
/
Aug 2023
Week 4 <
0.025
/
mg/L
<
/
Jul 2023
Average <
0.005
/ 8.2
mg/L
<
/
Aug 2023
Average <
0.025
/ 8.2
mg/L
<
/
2023
Quarter 3 <
0.015
/
mg/L
<
/
2023
2nd 6 Months (Avg) <
0.015
/
mg/L
<
/
2023
2nd 6 ...(Max) <
0.025
/
mg/L
<
/
2023
2nd 6 ...(Min) <
0.005
/
mg/L
<
/
2023
2nd 6 ...(Count)
2
Sample Count : 2 Months Sampled:
2
Weeks Sampled
:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C:
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Saturday, February 24, 2024 6:18:42PM * Indicates Violation ** Indicates TRC Violation Page 4 of 5

MP Pharma Services, Inc.
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
PH
08/23/2023 S
MPPharma082323Self
7.2
/ 6.0 - 10.0
SU
/
Aug 2023
Week 4
7.2
/
SU
/
Aug 2023
Average
7.2
/
SU
/
2023
Quarter 3
7.2
/
SU
/
2023
2nd 6 Months (Avg)
7.2
/
SU
/
2023
2nd 6 ...(Max)
7.2
/
SU
/
2023
2nd 6 ...(Min)
7.2
/
SU
/
2023
2nd 6 •..(Count)
1
Sample Count: 1
Months Sampled:
1
Weeks Sampled:
1
Quarters Sampled :
I
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass /Limit
Temperature
07/27/2023 P
MPPharma072723POT
30
/ 66
°C
/
W
08/23/2023 S
MPPharma082323Self
30.2
/ 66
°C
/
Ju12023
Week 4
30
/
°C
/
Aug 2023
Week 4
30.2
/
°C
/
Ju12023
Average
30
/
°C
/
Aug 2023
Average
30.2
/
°C
/
2023
Quarter 3
30.1
/
°C
/
2023
2nd 6 Months (Avg)
30.1
/
°C
/
2023
2nd 6 ...(Max)
30.2
/
°C
/
2023
2nd 6 ...(Min)
30
/
°C
/
2023
2nd 6 ...(Count)
2
Sample Count: 2 Months Sampled
:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C:
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Saturday, February 24, 2024 6:18:42PM * Indicates Violation ** Indicates TRC Violation Page 5 of 5

Phononic
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2023
S
Phononic0723F1ow
0.00598
/
MGD /
08/31/2023
S
Phononic0823FIow
0.010661
/
MGD /
09/30/2023
S
Phononic0923FIow
0.008506
/
MGD /
10/31/2023
S
Phononic1023F1ow
0.008185
/
MGD /
11/30/2023
S
Phononicl123Flow
0.008909
/
MGD /
12/31/2023
S
Phononicl223F1ow
0.006122
/
MGD /
Jul 2023
Week 4
0.00598
/
MGD /
Aug 2023
Week 4
0.010661
/
MGD /
Sep 2023
Week 4
0.008506
/
MGD /
Oct 2023
Week 4
0.008185
/
MGD /
Nov 2023
Week 4
0.008909
/
MGD /
Dec 2023
Week 4
0.006122
/
MGD /
Jul 2023
Average
0.00598
/ 0.035
MGD /
Aug 2023
Average
0.010661
/ 0.035
MGD /
Sep 2023
Average
0.008506
/ 0.035
MGD /
Oct 2023
Average
0.008185
/ 0.035
MGD /
Nov 2023
Average
0.008909
/ 0.035
MGD /
Dec 2023
Average
0.006122
/ 0.035
MGD /
2023
Quarter 3
0.008382
/
MGD /
2023
Quarter 4
0.007739
/
MGD /
2023
2nd 6 Months (Avg)
0.008061
/
MGD /
2023
2nd 6 ...(Max)
0.010661
/
MGD /
2023
2nd 6 ...(Min)
0.00598
/
MGD /
2023
2nd 6 •..(Count)
6
Sample Count:
6
Months Sampled:
6
Weeks Sampled:
6
Quarters Sampled :
2
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass /Limit
Bismuth
07/18/2023
S
Phononic071823Self
0.048
/ mg/L /
08/15/2023
S
Phononic081523Self
0.015
/ mg/L /
08/29/2023
P
Phononic082923POT
0.404
/ mg/L /
W
09/14/2023
S
Phononic091423Self
0.021
/ mg/L /
10/12/2023
S
Phononic 10 1223 Self <
0.003
/ mg/L < /
11/14/2023
S
Phononic111423Self
0.046
/ mg/L /
Saturday, February 24, 2024 6:28:47PM * Indicates Violation ** Indicates TRC Violation Page 1 of 6

Phononic
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Bismuth
12/19/2023 S
Phononic 121923 Self
0.016
/
mg/L
/
Jul 2023
Week 3
0.048
/
mg/L
/
Aug 2023
Week 3
0.015
/
mg/L
/
Aug 2023
Week 4
0.404
/
mg/L
/
Sep 2023
Week 2
0.021
/
mg/L
/
Oct 2023
Week 2
<
0.003
/
mg/L
<
/
Nov 2023
Week 2
0.046
/
mg/L
/
Dec 2023
Week 3
0.016
/
mg/L
/
Jul 2023
Average
0.048
/
mg/L
/
Aug 2023
Average
0.21
/
mg/L
/
Sep 2023
Average
0.021
/
mg/L
/
Oct 2023
Average
<
0.003
/
mg/L
<
/
Nov 2023
Average
0.046
/
mg/L
/
Dec 2023
Average
0.016
/
mg/L
/
2023
Quarter 3
0.122
/
mg/L
/
2023
Quarter 4
<
0.022
/
mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.079
/
mg/L
<
/
2023
2nd 6 ...(Max)
0.404
/
mg/L
/
2023
2nd 6 ...(Min)
<
0.003
/
mg/L
<
/
2023
2nd 6 ...(Count)
7
Sample Date
SamplelD
Result/Limit
Mass/Limit
Mercury - LL
08/29/2023 P
Phononic082923POT
0.000002
/ 0.000142
mg/L
/
WHg
09/21/2023 S
Phononic092123Self
<
0.0001
/ 0.000142
mg/L
<
/
Aug 2023
Week 4
0.000002
/
mg/L
/
Sep 2023
Week 3
<
0.0001
/
mg/L
<
/
Aug 2023
Average
0.000002
/
mg/L
/
Sep 2023
Average
<
0.0001
/
mg/L
<
/
2023
Quarter 3
<
0.0001
/
mg/L
<
/
2023
Quarter 3
0.000002
/
mg/L
/
2023
Quarter 3
0.000002
/
mg/L
/
2023
Quarter 3
<
0.0001
/
mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.000051
/
mg/L
<
/
2023
2nd 6 ...(Max)
<
0.0001
/
mg/L
<
/
2023
2nd 6 ...(Min)
0.000002
/
mg/L
/
2023
2nd 6 ...(Count)
2
Saturday, February 24, 2024 6:28:47PM * Indicates Violation ** Indicates TRC Violation Page 2 of 6

Phononic
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
2
Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
4
# Over Daily C :
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0,00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Samplc Date SamplelD Result/Limit Mass/Limit
Molybdenum
08/29/2023
P
Phononic082923POT
<
0.001
/
mg/L
<
0.0002 /
lbs/day
W
09/21/2023
S
Phononic092123Self
<
0.0025
/
mg/L
<
/
Aug 2023
Week 4
<
0.001
/
mg/L
<
0.0002 /
Ibs/day
Sep 2023
Week 3
<
0.0025
/
mg/L
<
/
Aug 2023
Average
<
0.001
/
mg/L
<
0.0002 /
lbs/day
Sep 2023
Average
<
0.0025
/
mg/L
<
/
2023
Quarter 3
<
0.0018
/
mg/L
<
0.0002 /
lbs/day
2023
2nd 6 Months (Avg)
<
0.0018
/
mg/L
<
0.0002 /
Ibs/day
2023
2nd 6 ...(Max)
<
0.0025
/
mg/L
<
0.0002 /
Ibs/day
2023
2nd 6 ...(Min)
<
0.001
/
mg/L
<
/
2023
2nd 6 ...(Count)
2
/
1 /
Sample Date
SamplelD
Result/Limit
Mass /Limit
Nickel
07/18/2023
S
Phononic071823Self
0.054
/
mg/L
0.009392 / 0.02
Ibs/day
08/15/2023
S
Phononic081523Self
0.017
/
mg/L
0.00316 / 0.02
lbs/day
08/29/2023
P
Phononic082923POT
0.0139
/
mg/L
0.002986 / 0.02
Ibs/day
W
09/14/2023
S
Phononic091423Self
<
0.0025
/
mg/L
<
0.000465 / 0.02
Ibs/day
10/12/2023
S
Phononic 10 1223 Self
<
0.0025
/
mg/L
<
0.00032 / 0.02
lbs/day
11/14/2023
S
Phononic111423Self
0.009
/
mg/L
0.001401 / 0.02
lbs/day
12/19/2023
S
Phononic 121923 Self
0.008
/
mg/L
0.001527 / 0.02
Ibs/day
Jul 2023
Week 3
0.054
/
mg/L
0.009392 /
Ibs/day
Aug 2023
Week 3
0.017
/
mg/L
0.00316 /
Ibs/day
Aug 2023
Week 4
0.0139
/
mg/L
0.002986 /
Ibs/day
Sep 2023
Week 2
<
0.0025
/
mg/L
<
0.000465 /
lbs/day
Oct 2023
Week 2
<
0.0025
/
mg/L
<
0.00032 /
lbs/day
Nov 2023
Week 2
0.009
/
mg/L
0.001401 /
lbs/day
Dec 2023
Week 3
0.008
/
mg/L
0.001527 /
lbs/day
Jul 2023
Average
0.054
/
mg/L
0.009392 /
Ibs/day
Aug 2023
Average
0.0155
/
mg/L
0.003073 /
Ibs/day
Sep 2023
Average
<
0.0025
/
mg/L
<
0.000465 /
Ibs/day
Oct 2023
Average
<
0.0025
/
mg/L
<
0.00032 /
Ibs/day
Nov 2023
Average
0.009
/
mg/L
0.001401 /
lbs/day
Saturday, February 24, 2024 6:28:47PM * Indicates Violation ** Indicates TRC Violation Page 3 of 6

Phononic
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
Dec 2023
Average
0.008
/
mg/L
0.001527 / lbs/day
2023
Quarter 3
<
0.0219
/
mg/L <
0.004 / lbs/day
2023
Quarter 4
<
0.0065
/
mg/L <
0.001083 / lbs/day
2023
2nd 6 Months (Avg) <
0.0153
/
mg/L <
0.002750 / Ibs/day
2023
2nd 6 ...(Max)
0.054
/
mg/L
0.009392 / Ibs/day
2023
2nd 6 ...(Min)
<
0.0025
/
mg/L <
0.000320 / Ibs/day
2023
2nd 6 ...(Count)
7
/
7 /
Sample Count: 7
Months Sampled:
6
Weeks Sampled:
7 Quarters Sampled :
2
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00 # Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC
:
0
0.00
# Over Wk Avg C TRC : 0
0.00 # Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00 # Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC : 0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass /Limit
pH
08/29/2023
P
Phononic082923POT
6.9
/ 5.0 - 10.0
SU /
W
09/14/2023
S
Phononic091423Self
5.73
/ 5.0 - 10.0
SU /
09/21/2023
S
Phononic092123Self
6.86
/ 5.0 - 10.0
SU /
10/12/2023
S
Phononic101223Self
7.48
/ 5.0 - 10.0
SU /
12/19/2023
S
Phononic 121923 Self
6.4
/ 5.0 - 10.0
SU /
Aug 2023
Week 4
6.9
/
SU /
Sep 2023
Week 2
5.73
/
SU /
Sep 2023
Week 3
6.86
/
SU /
Oct 2023
Week 2
7.48
/
SU /
Dec 2023
Week 3
6.4
/
SU /
Aug 2023
Average
6.9
/
SU /
Sep 2023
Average
6.3
/
SU /
Oct 2023
Average
7.48
/
SU /
Dec 2023
Average
6.4
/
SU /
2023
Quarter 3
6.5
/
SU /
2023
Quarter 4
6.94
/
SU /
2023
2nd 6 Months (Avg)
6.67
/
SU /
2023
2nd 6 ...(Max)
7.48
/
SU /
2023
2nd 6 ...(Min)
5.73
/
SU /
2023
2nd 6 ...(Count)
5
/
/
Saturday, February 24, 2024 6:28:47PM * Indicates Violation ** Indicates TRC Violation Page 4 of 6

Phononic
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
5
Months Sampled:
4
Weeks Sampled:
5
Quarters Sampled :
2
# Over Daily C :
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0,00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Samplc Date SamplelD Result/Limit Mass/Limit
Tellurium
07/18/2023
S
Phononic071823Self
0.109 /
mg/L
/
08/15/2023
S
Phononic081523Self
0.067 /
mg/L
/
08/29/2023
P
Phononic082923POT
0.29 /
mg/L
/
W
09/14/2023
S
Phononic091423Self
0.022 /
mg/L
/
10/12/2023
S
Phononic 10 1223 Self
<
0.003 /
mg/L
<
/
11/14/2023
S
Phononic111423Self
0.141 /
mg/L
/
12/19/2023
S
Phononic 121923 Self
0.052 /
mg/L
/
Jul 2023
Week 3
0.109 /
mg/L
/
Aug 2023
Week 3
0.067 /
mg/L
/
Aug 2023
Week 4
0.29 /
mg/L
/
Sep 2023
Week 2
0.022 /
mg/L
/
Oct 2023
Week 2
<
0.003 /
mg/L
<
/
Nov 2023
Week 2
0.141 /
mg/L
/
Dec 2023
Week 3
0.052 /
mg/L
/
Ju12023
Average
0.109 /
mg/L
/
Aug 2023
Average
0.179 /
mg/L
/
Sep 2023
Average
0.022 /
mg/L
/
Oct 2023
Average
<
0.003 /
mg/L
<
/
Nov 2023
Average
0.141 /
mg/L
/
Dec 2023
Average
0.052 /
mg/L
/
2023
Quarter 3
0.122 /
mg/L
/
2023
Quarter 4
<
0.065 /
mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.098 /
mg/L
<
/
2023
2nd 6 ...(Max)
0.29 /
mg/L
/
2023
2nd 6 ...(Min)
<
0.003 /
mg/L
<
/
2023
2nd 6 ...(Count)
7
Sample Date SamplelD Result/Limit Mass /Limit
Temperature
08/29/2023
P Phononic082923POT
W
Aug 2023
Week 4
Aug 2023
Average
2023
Quarter 3
23 /
°C /
23 /
°C /
23 /
°C /
23 /
°C /
Saturday, February 24, 2024 6:28:47PM * Indicates Violation ** Indicates TRC Violation Page 5 of 6

Phononic
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
2023
2nd 6 Months (Avg)
23
/
°C
/
2023
2nd 6 ...(Max)
23
/
°C
/
2023
2nd 6 ...(Min)
23
/
°C
/
2023
2nd 6 ...(Count)
1
/
/
Sample Date
SamplelD
Result/Limit
Mass/Limit
TTO
09/12/2023 S
Phononic091223Self <
0.005
/ 1.096
mg/L
<
/
Sep 2023
Week 2 <
0.005
/
mg/L
<
/
Sep 2023
Average <
0.005
/
mg/L
<
/
2023
Quarter 3 <
0.005
/
mg/L
<
/
2023
2nd 6 Months (Avg) <
0.005
/
mg/L
<
/
2023
2nd 6 ...(Max) <
0.005
/
mg/L
<
/
2023
2nd 6 ...(Min) <
0.005
/
mg/L
<
/
2023
2nd 6 ...(Count)
1
Sample Count : 1 Months Sampled
: 1
Weeks Sampled:
1
Quarters Sampled :
1
# %
# %
#
°/,
#
°/,
# Over Daily C :
0 0.00 # Over Mo Avg C :
0 0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC
:
0 0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0 0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC
:
0 0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Saturday, February 24, 2024 6:28:47PM * Indicates Violation ** Indicates TRC Violation Page 6 of 6

PowerSecure
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Aluminum
08/15/2023
P PowerSecure081523P
3.11
/ mg/L
/
OTW
09/27/2023
S PowerSecure092723Se
5.4
/ mg/L
/
if
Aug 2023
Week 3
3.11
/ mg/L
/
Sep 2023
Week 4
5.4
/ mg/L
/
Aug 2023
Average
3.11
/ mg/L
/
Sep 2023
Average
5.4
/ mg/L
/
2023
Quarter 3
4.255
/ mg/L
/
2023
2nd 6 Months (Avg)
4.255
/ mg/L
/
2023
2nd 6 ...(Max)
5.4
/ mg/L
/
2023
2nd 6 ...(Min)
3.11
/ mg/L
/
2023
2nd 6 ...(Count)
2
/
/
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2023
S
PowerSecure0723F1ow
0.003607
/
MGD /
08/31/2023
S
PowerSecure0823F1ow
0.004242
/
MGD /
09/30/2023
S
PowerSecure0923171ow
0.004469
/
MGD /
10/31/2023
S
PowerSecurc1023FIow
0.004475
/
MGD /
11/30/2023
S
PowerSecurel123171ow
0.006738
/
MGD /
12/31/2023
S
PowerSecurel223F1ow
0.003675
/
MGD /
Jul 2023
Week 4
0.003607
/
MGD /
Aug 2023
Week 4
0.004242
/
MGD /
Sep 2023
Week 4
0.004469
/
MGD /
Oct 2023
Week 4
0.004475
/
MGD /
Nov 2023
Week 4
0.006738
/
MGD /
Dec 2023
Week 4
0.003675
/
MGD /
Jul 2023
Average
0.003607
/ 0.006
MGD /
Aug 2023
Average
0.004242
/ 0.006
MGD /
Sep 2023
Average
0.004469
/ 0.006
MGD /
Oct 2023
Average
0.004475
/ 0.006
MGD /
Nov 2023
Average
0.006738
/ 0.006
MGD * /
Dec 2023
Average
0.003675
/ 0.006
MGD /
2023
Quarter 3
0.004106
/
MGD /
2023
Quarter 4
0.004963
/
MGD /
2023
2nd 6 Months (Avg)
0.004534
/
MGD /
2023
2nd 6 ...(Max)
0.006738
/
MGD /
2023
2nd 6 ...(Min)
0.003607
/
MGD /
2023
2nd 6 ...(Count)
6
/
/
Saturday, February 24, 2024 6:34:34PM * Indicates Violation ** Indicates TRC Violation Page 1 of 9

PowerSecure
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
6
Months Sampled :
6
Weeks Sampled:
6
Quarters Sampled :
2
# Over Daily C:
0
0.00
# Over Mo Avg C: 1
16.67
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
08/15/2023 P
PowerSecure081523P < 0.00008
/ 0.11
mg/L
<
/
OTW
09/27/2023 S
PowerSecure092723Se < 0.0005
/ 0.11
mg/L
<
/
if
Aug 2023
Week 3
< 0.00008
/
mg/L
<
/
Sep 2023
Week 4
< 0.0005
/
mg/L
<
/
Aug 2023
Average
< 0.00008
/ 0.07
mg/L
<
/
Sep 2023
Average
< 0.0005
/ 0.07
mg/L
<
/
2023
Quarter 3
< 0.00029
/
mg/L
<
/
2023
2nd 6 Months (Avg) < 0.00029
/
mg/L
<
/
2023
2nd 6 ...(Max)
< 0.0005
/
mg/L
<
/
2023
2nd 6 ...(Min)
< 0.00008
/
mg/L
<
/
2023
2nd 6 ...(Count)
2
Sample Count: 2
Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C:
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SampleLD Result/Limit Mass/Limit
Chloride
08/15/2023
P PowerSecure081523P
2310
/ mg/L /
OTW
09/27/2023
S PowerSecure092723Se
1230
/ mg/L /
if
Aug 2023
Week 3
2310
/ mg/L /
Sep 2023
Week 4
1230
/ mg/L /
Aug 2023
Average
2310
/ mg/L /
Sep 2023
Average
1230
/ mg/L /
2023
Quarter 3
1770
/ mg/L /
2023
2nd 6 Months (Avg)
1770
/ mg/L /
2023
2nd 6 ...(Max)
2310
/ mg/L /
Saturday, February 24, 2024 6:34:34PM * Indicates Violation ** Indicates TRC Violation Page 2 of 9

PowerSecure
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
Chloride
2023
2nd 6 ...(Min)
1230
/
mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
Chromium
08/15/2023 P
PowerSecure0815231? <
0.001
/ 2,77
mg/L
<
/
OTW
09/27/2023 S
PowerSecure092723Se <
0.003
/ 2,77
mg/L
<
/
if
Aug 2023
Week 3 <
0.001
/
mg/L
<
/
Sep 2023
Week 4 <
0.003
/
mg/L
<
/
Aug 2023
Average <
0.001
/ 1.71
mg/L
<
/
Sep 2023
Average <
0.003
/ 1.71
mg/L
<
/
2023
Quarter 3 <
0.002
/
mg/L
<
/
2023
2nd 6 Months (Avg) <
0.002
/
mg/L
<
/
2023
2nd 6 ...(Max) <
0.003
/
mg/L
<
/
2023
2nd 6 ...(Min) <
0.001
/
mg/L
<
/
2023
2nd 6 ...(Count)
2
Sample Count : 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0 0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC
:
0 0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M:
0 0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC
:
0 0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
Copper
08/15/2023 P
PowerSecure0815231?
0.049
/ 3.38
mg/L
/
OTW
09/27/2023 S
PowerSecure092723Se
0.019
/ 3.38
mg/L
/
if
Aug 2023
Week 3
0.049
/
mg/L
/
Sep 2023
Week 4
0.019
/
mg/L
/
Aug 2023
Average
0.049
/ 2.07
mg/L
/
Sep 2023
Average
0.019
/ 2.07
mg/L
/
2023
Quarter 3
0.034
/
mg/L
/
2023
2nd 6 Months (Avg)
0.034
/
mg/L
/
2023
2nd 6 ...(Max)
0.049
/
mg/L
/
2023
2nd 6 ...(Min)
0.019
/
mg/L
/
2023
2nd 6 ...(Count)
2
Saturday, February 24, 2024 6:34:34PM * Indicates Violation ** Indicates TRC Violation Page 3 of 9

PowerSecure
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
2
Months Sampled :
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
08/15/2023 P
PowerSecure081523P <
0.003
/ 0.60
mg/L
<
/
OTW
09/27/2023 S
PowerSecure092723Se <
0.004
/ 0.60
mg/L
<
/
if
Aug 2023
Week 3 <
0.003
/
mg/L
<
/
Sep 2023
Week 4 <
0.004
/
mg/L
<
/
Aug 2023
Average <
0.003
10.50
mg/L
<
/
Sep 2023
Average <
0.004
10.50
mg/L
<
/
2023
Quarter 3 <
0.003
/
mg/L
<
/
2023
2nd 6 Months (Avg) <
0.003
/
mg/L
<
/
2023
2nd 6 ...(Max) <
0.004
/
mg/L
<
/
2023
2nd 6 ...(Min) <
0.003
/
mg/L
<
/
2023
2nd 6 ...(Count)
2
Sample Count: 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C:
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SampleLD Result/Limit Mass/Limit
Fluoride
08/15/2023
P PowerSecure081523P
4.59
/ mg/L /
OTW
Aug 2023
Week 3
4.59
/ mg/L /
Aug 2023
Average
4.59
/ mg/L /
2023
Quarter 3
4.59
/ mg/L /
2023
2nd 6 Months (Avg)
4.59
/ mg/L /
2023
2nd 6 ...(Max)
4.59
/ mg/L /
2023
2nd 6 ...(Min)
4.59
/ mg/L /
2023
2nd 6 ...(Count)
1
Saturday, February 24, 2024 6:34:34PM * Indicates Violation ** Indicates TRC Violation Page 4 of 9

PowerSecure
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Lead
08/15/2023 P
PowerSecure081523P <
0.0003
/ 0.69
mg/L
<
/
OTW
09/27/2023 S
PowerSecure092723Se <
0.005
/ 0.69
mg/L
<
/
if
Aug 2023
Week 3
<
0.0003
/
mg/L
<
/
Sep 2023
Week 4
<
0.005
/
mg/L
<
/
Aug 2023
Average
<
0.0003
/ 0.43
mg/L
<
/
Sep 2023
Average
<
0.005
/ 0.43
mg/L
<
/
2023
Quarter 3
<
0.0026
/
mg/L
<
/
2023
2nd 6 Months (Avg) <
0.0026
/
mg/L
<
/
2023
2nd 6 ...(Max)
<
0.005
/
mg/L
<
/
2023
2nd 6 ...(Min)
<
0.0003
/
mg/L
<
/
2023
2nd 6 ...(Count)
2
/
/
Sample Count: 2
Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC
:
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury
09/27/2023 S
PowerSecure092723Se < 0.000001
/ 0.000142
mg/L
<
/
If
Sep 2023
Week 4
< 0.000001
/
mg/L
<
/
Sep 2023
Average
< 0.000001
/
mg/L
<
/
2023
Quarter 3
< 0.000001
/
mg/L
<
/
2023
2nd 6 Months (Avg) < 0.000001
/
mg/L
<
/
2023
2nd 6 ...(Max)
< 0.000001
/
mg/L
<
/
2023
2nd 6 ...(Min)
< 0.000001
/
mg/L
<
/
2023
2nd 6 ...(Count)
1
/
/
Sample Count: 1
Months Sampled:
1
Weeks Sampled:
1
Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Saturday, February 24, 2024 6:34:34PM * Indicates Violation ** Indicates TRC Violation Page 5 of 9

PowerSecure
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
Mercury - LL
10/03/2023
P
PowerSecurel00323P
0.000003
/
mg/L
/
OTWHg
Oct 2023
Week 1
0.000003
/
mg/L
/
Oct 2023
Average
0.000003
/
mg/L
/
2023
Quarter 4
0.000003
/
mg/L
/
2023
2nd 6 Months (Avg)
0.000003
/
mg/L
/
2023
2nd 6 ...(Max)
0.000003
/
mg/L
/
2023
2nd 6 ...(Min)
0.000003
/
mg/L
/
2023
2nd 6 ...(Count)
1
Sample Date
SamplelD
Result/Limit
Mass/Limit
Molybdenum
09/27/2023
S
PowerSecure092723Se
<
0.005
/
mg/L
<
/
if
Sep 2023
Week 4
<
0.005
/
mg/L
<
/
Sep 2023
Average
<
0.005
/
mg/L
<
/
2023
Quarter 3
<
0.005
/
mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.005
/
mg/L
<
/
2023
2nd 6 ...(Max)
<
0.005
/
mg/L
<
/
2023
2nd 6 ...(Min)
<
0.005
/
mg/L
<
/
2023
2nd 6 ...(Count)
1
Sample Date
SamplelD
Result/Limit
Mass/Limit
Nickel
08/15/2023
P
PowerSecure081523P
0.0088
/ 1.30
mg/L
/
OTW
09/27/2023
S
PowerSecure092723Se
<
0.0025
/ 1.30
mg/L
<
/
if
Aug 2023
Week 3
0.0088
/
mg/L
/
Sep 2023
Week 4
<
0.0025
/
mg/L
<
/
Aug 2023
Average
0.0088
/ 1.00
mg/L
/
Sep 2023
Average
<
0.0025
/ 1.00
mg/L
<
/
2023
Quarter 3
<
0.0057
/
mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.0057
/
mg/L
<
/
2023
2nd 6 ...(Max)
0.0088
/
mg/L
/
2023
2nd 6 ...(Min)
<
0.0025
/
mg/L
<
/
2023
2nd 6 ...(Count)
2
Saturday, February 24, 2024 6:34:34PM * Indicates Violation ** Indicates TRC Violation Page 6 of 9

PowerSecure
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
2
Months Sampled :
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
PH
08/15/2023 P
PowerSecure081523P
8.6
/ 6.0 - 10.0
SU
/
OTW
09/27/2023 S
PowerSecure092723Se
8.7
/ 6.0 - 10.0
SU
/
if
Aug 2023
Week 3
8.6
/
SU
/
Sep 2023
Week 4
8.7
/
SU
/
Aug 2023
Average
8.6
/
SU
/
Sep 2023
Average
8.7
/
Su
/
2023
Quarter 3
8.65
/
SU
/
2023
2nd 6 Months (Avg)
8.65
/
SU
/
2023
2nd 6 ...(Max)
8.7
/
SU
/
2023
2nd 6 ...(Min)
8.6
/
SU
/
2023
2nd 6 ...(Count)
2
Sample Count: 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C:
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SampleLD Result/Limit Mass/Limit
Silver
08/15/2023
P PowerSecure081523P
<
0.0003
/ 0.43
mg/L
< /
OTW
09/27/2023
S PowerSecure092723Se
<
0.0025
/ 0.43
mg/L
< /
if
Aug 2023
Week 3
<
0.0003
/
mg/L
< /
Sep 2023
Week 4
<
0.0025
/
mg/L
< /
Aug 2023
Average
<
0.0003
/ 0.24
mg/L
< /
Sep 2023
Average
<
0.0025
/ 0.24
mg/L
< /
2023
Quarter 3
<
0.0014
/
mg/L
< /
2023
2nd 6 Months (Avg)
<
0.0014
/
mg/L
< /
2023
2nd 6 ...(Max)
<
0.0025
/
mg/L
< /
Saturday, February 24, 2024 6:34:34PM * Indicates Violation ** Indicates TRC Violation Page 7 of 9

PowerSecure
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Over
2023
2nd 6
...(Min)
< 0.0003
/
mg/L <
/
2023
2nd 6
...(Count)
2
/
/
Sample Count :
2
Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit
Temperature
Mass/Limit
08/15/2023 P
PowerSecure081523P
28
/ 66
°C
/
OTW
09/27/2023 S
PowerSecure092723Se
22.5
/ 66
°C
/
if
Aug 2023
Week 3
28
/
°C
/
Sep 2023
Week 4
22.5
/
°C
/
Aug 2023
Average
28
/
°C
/
Sep 2023
Average
22.5
/
°C
/
2023
Quarter 3
25.3
/
°C
/
2023
2nd 6 Months (Avg)
25.3
/
°C
/
2023
2nd 6 ...(Max)
28
/
°C
/
2023
2nd 6 ...(Min)
22.5
/
°C
/
2023
2nd 6 ...(Count)
2
/
/
Sample Count : 2 Months Sampled
:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C:
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TTO
09/27/2023
S PowerSecure092723Se <
0.0025 / 2.13
mg/L <
/
if
Sep 2023
Week 4 <
0.0025 /
mg/L <
/
Sep 2023
Average <
0.0025 /
mg/L <
/
2023
Quarter 3 <
0.0025 /
mg/L <
/
2023
2nd 6 Months (Avg) <
0.0025 /
mg/L <
/
Saturday, February 24, 2024 6:34:34PM * Indicates Violation ** Indicates TRC Violation Page 8 of 9

PowerSecure
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
TTO
2023
2nd 6
...(Max)
< 0.0025 /
mg/L <
/
2023
2nd 6
...(Min)
< 0.0025 /
mg/L <
/
2023
2nd 6
...(Count)
1
Sample Count:
1
Months Sampled:
1
Weeks Sampled:
1
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
08/15/2023 P
PowerSecure081523P
0.008
/ 2.61
mg/L
/
OTW
09/27/2023 S
PowerSecure092723Se <
0.01
/ 2.61
mg/L <
/
If
Aug 2023
Week 3
0.008
/
mg/L
/
Sep 2023
Week 4 <
0.01
/
mg/L <
/
Aug 2023
Average
0.008
/ 1.48
mg/L
/
Sep 2023
Average <
0.01
/ 1.48
mg/L <
/
2023
Quarter 3 <
0.009
/
mg/L <
/
2023
2nd 6 Months (Avg) <
0.009
/
mg/L <
/
2023
2nd 6 ...(Max) <
0.01
/
mg/L <
/
2023
2nd 6 ...(Min)
0.008
/
mg/L
/
2023
2nd 6 ...(Count)
2
Sample Count : 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C:
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Saturday, February 24, 2024 6:34:34PM * Indicates Violation ** Indicates TRC Violation Page 9 of 9

SCM Metal Products, Inc.
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2023
S
SCM0723F1ow
0.031857
/ 0.080
MGD /
08/31/2023
S
SCM0823F1ow
0.024038
/ 0.080
MGD /
09/30/2023
S
SCM0923171ow
0.015668
/ 0.080
MGD /
10/31/2023
S
SCM1023F1ow
0.016729
/ 0.080
MGD /
11/30/2023
S
SCM1123F1ow
0.014121
/ 0.080
MGD /
12/31/2023
S
SCM1223Flow
0.01254
/ 0.080
MGD /
Jul 2023
Week 4
0.031857
/
MGD /
Aug 2023
Week 4
0.024038
/
MGD /
Sep 2023
Week 4
0.015668
/
MGD /
Oct 2023
Week 4
0.016729
/
MGD /
Nov 2023
Week 4
0.014121
/
MGD /
Dec 2023
Week 4
0.01254
/
MGD /
Jul 2023
Average
0.031857
10.050
MGD /
Aug 2023
Average
0.024038
10.050
MGD /
Sep 2023
Average
0.015668
10.050
MGD /
Oct 2023
Average
0.016729
10.050
MGD /
Nov 2023
Average
0.014121
10.050
MGD /
Dec 2023
Average
0.01254
10.050
MGD /
2023
Quarter 3
0.023854
/
MGD /
2023
Quarter 4
0.014463
/
MGD /
2023
2nd 6 Months (Avg)
0.019159
/
MGD /
2023
2nd 6 ...(Max)
0.031857
/
MGD /
2023
2nd 6 ...(Min)
0.01254
/
MGD /
2023
2nd 6 •..(Count)
6
Sample Count:
6
Months Sampled:
6
Weeks Sampled:
6
Quarters Sampled :
2
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass /Limit
Copper
07/28/2023
P SCM072823POTW
0.112
/ 0.75
mg/L
/
08/09/2023
S SCM080923Self
0.039
/ 0.75
mg/L
0.009987 /
Ibs/day
11/21/2023
S SCM1121223Self
0.29
/ 0.75
mg/L
0.045997 /
Ibs/day
Jul 2023
Week 4
0.112
/
mg/L
/
Aug 2023
Week 2
0.039
/
mg/L
0.009987 /
lbs/day
Nov 2023
Week 3
0.29
/
mg/L
0.045997 /
lbs/day
Jul 2023
Average
0.112
10.50
mg/L
/
Saturday, February 24, 2024 6:56:30PM * Indicates Violation ** Indicates TRC Violation Page 1 of 5

SCM Metal Products, Inc.
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Copper
Aug 2023
Average
0.039
10.50
mg/L
0.009987 / lbs/day
Nov 2023
Average
0.29
10.50
mg/L
0.045997 / lbs/day
2023
Quarter 3
0.076
/
mg/L
0.009987 / lbs/day
2023
Quarter 4
0.29
/
mg/L
0.045997 / Ibs/day
2023
2nd 6 Months (Avg)
0.147
/
mg/L
0.027992 / Ibs/day
2023
2nd 6 ...(Max)
0.29
/
mg/L
0.045997 / Ibs/day
2023
2nd 6 ...(Min)
0.039
/
mg/L
/
2023
2nd 6 •..(Count)
3
/
2 /
Sample Count: 3
Months Sampled:
3
Weeks Sampled:
3 Quarters Sampled :
2
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00 # Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00 # Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00 # Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass /Limit
Cyanide
07/28/2023 P
SCM072823POTW
0.005
/ 0.04
mg/L
/
08/09/2023 S
SCM080923Self
0.017
/ 0.04
mg/L
0.004353 /
Ibs/day
Jul 2023
Week 4
0.005
/
mg/L
/
Aug 2023
Week 2
0.017
/
mg/L
0.004353 /
lbs/day
Jul 2023
Average
0.005
/ 0.03
mg/L
/
Aug 2023
Average
0.017
/ 0.03
mg/L
0.004353 /
lbs/day
2023
Quarter 3
0.011
/
mg/L
0.004353 /
lbs/day
2023
2nd 6 Months (Avg)
0.011
/
mg/L
0.004354 /
Ibs/day
2023
2nd 6 ...(Max)
0.017
/
mg/L
0.004353 /
Ibs/day
2023
2nd 6 ...(Min)
0.005
/
mg/L
/
2023
2nd 6 ...(Count)
2
/
1 /
Sample Count: 2 Months Sampled
:
2
Weeks Sampled:
2 Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C:
0
0.00
# Over Wk Avg C : 0
0.00 # Over Qt Avg C :
0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00 # Over Qt Avg C TRC
: 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00 # Over Qtr Avg M :
0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Lead
Saturday, February 24, 2024 6:56:30PM * Indicates Violation ** Indicates TRC Violation Page 2 of 5

SCM Metal Products, Inc.
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Lead
07/28/2023 P
SCM072823POTW
0.0009
/ 0.20
mg/L
/
08/09/2023 S
SCM080923Self <
0.0005
/ 0.20
mg/L
<
0.000128 /
lbs/day
11/21/2023 S
SCM1121223Self <
0.0005
/ 0.20
mg/L
<
0.000079 /
lbs/day
Jul 2023
Week 4
0.0009
/
mg/L
/
Aug 2023
Week 2 <
0.0005
/
mg/L
<
0.000128 /
Ibs/day
Nov 2023
Week 3 <
0.0005
/
mg/L
<
0.000079 /
Ibs/day
Jul 2023
Average
0.0009
/ 0.10
mg/L
/
Aug 2023
Average <
0.0005
/ 0.10
mg/L
<
0.000128 /
Ibs/day
Nov 2023
Average <
0.0005
/ 0.10
mg/L
<
0.000079 /
Ibs/day
2023
Quarter 3 <
0.0007
/
mg/L
<
0.000128 /
lbs/day
2023
Quarter 4 <
0.0005
/
mg/L
<
0.000079 /
lbs/day
2023
2nd 6 Months (Avg) <
0.0006
/
mg/L
<
0.000104 /
Ibs/day
2023
2nd 6 ...(Max)
0.0009
/
mg/L
0.000128 /
Ibs/day
2023
2nd 6 ...(Min) <
0.0005
/
mg/L
<
/
2023
2nd 6 ...(Count)
3
/
2 /
Sample Count: 3 Months Sampled:
3
Weeks Sampled:
3 Quarters Sampled :
2
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00 # Over Qt Avg C :
0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC
:
0
0.00
# Over Wk Avg C TRC :
0
0.00 # Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00 # Over Qtr Avg M :
0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass /Limit
Mercury - LL
07/28/2023 P
SCM072823POTWHg
0.00001
/ 0.000142
mg/L /
08/09/2023 S
SCM080923Self
0.000006
/ 0.000142
mg/L /
Aug 2023
Week 2
0.000006
/
mg/L /
Jul 2023
Week 4
0.00001
/
mg/L /
Jul 2023
Average
0.00001
/
mg/L /
Aug 2023
Average
0.000006
/
mg/L /
2023
Quarter 3
0.000008
/
mg/L /
2023
2nd 6 Months (Avg)
0.000008
/
mg/L /
2023
2nd 6 ...(Max)
0.00001
/
mg/L /
2023
2nd 6 ...(Min)
0.000006
/
mg/L /
2023
2nd 6 ...(Count)
2
Saturday, February 24, 2024 6:56:30PM * Indicates Violation ** Indicates TRC Violation Page 3 of 5

SCM Metal Products, Inc.
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
2
Months Sampled :
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
PH
07/28/2023 P
SCM072823POTW
6.9
/ 6.0 - 10.5
SU
/
08/09/2023 S
SCM080923Self
7.55
/ 6.0 - 10.5
SU
/
11/21/2023 S
SCM1121223Setf
7.5
/ 6.0 - 10.5
SU
/
Jul 2023
Week 4
6.9
/
Su
/
Aug 2023
Week 2
7.55
/
SU
/
Nov 2023
Week 3
7.5
/
SU
/
Ju12023
Average
6.9
/
Su
/
Aug 2023
Average
7.55
/
SU
/
Nov 2023
Average
7.5
/
SU
/
2023
Quarter 3
7.23
/
SU
/
2023
Quarter 4
7.5
/
SU
/
2023
2nd 6 Months (Avg)
7.32
/
SU
/
2023
2nd 6 ...(Max)
7.55
/
SU
/
2023
2nd 6 ...(Min)
6.9
/
SU
/
2023
2nd 6 ...(Count)
3
Sample Count: 3 Months Sampled:
3
Weeks Sampled:
3
Quarters Sampled :
2
# Over Daily C:
0 0.00 # Over Mo Avg C :
0 0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0 0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0 0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0 0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
07/28/2023
P SCM072823POTW
28
/ 66
°C /
08/09/2023
S SCM080923Self
28
/ 66
°C /
11/21/2023
S SCM1121223Self
18.9
/ 66
c /
Jul 2023
Week 4
28
/
°C /
Aug 2023
Week 2
28
/
°C /
Nov 2023
Week 3
18.9
/
°C /
Jul 2023
Average
28
/
°C /
Aug 2023
Average
28
/
°C /
Saturday, February 24, 2024 6:56:30PM * Indicates Violation ** Indicates TRC Violation Page 4 of 5

SCM Metal Products, Inc.
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
Nov 2023
Average
18.9
/
°C
/
2023
Quarter 3
28
/
°C
/
2023
Quarter 4
18.9
/
°C
/
2023
2nd 6 Months (Avg)
25.0
/
°C
/
2023
2nd 6 ...(Max)
28
/
°C
/
2023
2nd 6 ...(Min)
18.9
/
°C
/
2023
2nd 6 ...(Count)
3
Sample Count: 3
Months Sampled:
3
Weeks Sampled:
3
Quarters Sampled :
2
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass /Limit
VOG
08/09/2023
S SCM080923Self
0.0213
/ mg/L /
Aug 2023
Week 2
0.0213
/ mg/L /
Aug 2023
Average
0.0213
/ mg/L /
2023
Quarter 3
0.0213
/ mg/L /
2023
2nd 6 Months (Avg)
0.0213
/ mg/L /
2023
2nd 6 ...(Max)
0.0213
/ mg/L /
2023
2nd 6 ...(Min)
0.0213
/ mg/L /
2023
2nd 6 ...(Count)
1
/ /
Saturday, February 24, 2024 6:56:30PM * Indicates Violation ** Indicates TRC Violation Page 5 of 5

Tergus Pharma
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
07/28/2023 P
Tergus072823POTW
0.067
/ 20.7
mg/L
/
09/26/2023 S
Tergus092623Self <
0.002
/ 20.7
mg/L <
/
Jul 2023
Week 4
0.067
/
mg/L
/
Sep 2023
Week 4 <
0.002
/
mg/L <
/
Jul 2023
Average
0.067
/ 8.2
mg/L
/
Sep 2023
Average <
0.002
/ 8.2
mg/L <
/
2023
Quarter 3 <
0.035
/
mg/L <
/
2023
2nd 6 Months (Avg) <
0.035
/
mg/L <
/
2023
2nd 6 ...(Max)
0.067
/
mg/L
/
2023
2nd 6 ...(Min) <
0.002
/
mg/L <
/
2023
2nd 6 ...(Count)
2
Sample Count: 2 Months Sampled
:
2
Weeks Sampled :
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Arsenic
07/28/2023
P Tergus072823POTW
<
0.001
/ mg/L
<
/
09/26/2023
S Tergus092623Self
<
0.0005
/ mg/L
<
/
Jul 2023
Week 4
<
0.001
/ mg/L
<
/
Sep 2023
Week 4
<
0.0005
/ mg/L
<
/
Jul 2023
Average
<
0.001
/ mg/L
<
/
Sep 2023
Average
<
0.0005
/ mg/L
<
/
2023
Quarter 3
<
0.0007
/ mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.0007
/ mg/L
<
/
2023
2nd 6 ...(Max)
<
0.001
/ mg/L
<
/
2023
2nd 6 ...(Min)
<
0.0005
/ mg/L
<
/
2023
2nd 6 ...(Count)
2
/
/
Sample Date
SamplelD
Result/Limit
Mass/Limit
Average Flow for Month
07/24/2023
S
Tergus0723F1ow
0.007445
/
MGD
/
08/31/2023
S
Tergus0823F1ow
0.01003
/
MGD
/
09/30/2023
S
Tergus0923F1ow
0.009809
/
MGD
/
10/31/2023
S
Tergusl023F1ow
0.009147
/
MGD
/
11/30/2023
S
Tergusll23F1ow
0.00557
/
MGD
/
Sunday, February 25, 2024 8:52:39AM * Indicates Violation ** Indicates TRC Violation Page 1 of 13

Tergus Pharma
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
12/20/2023 S
Tergusl223F1ow 0.003598
/
MGD
/
Jul 2023
Week 4
0.007445
/
MGD
/
Aug 2023
Week 4
0.01003
/
MGD
/
Sep 2023
Week 4
0.009809
/
MGD
/
Oct 2023
Week 4
0.009147
/
MGD
/
Nov 2023
Week 4
0.00557
/
MGD
/
Dec 2023
Week 3
0.003598
/
MGD
/
Ju12023
Average
0.007445
/ 0.006512
MGD *
/
Aug 2023
Average
0.01003
/ 0.006512
MGD *
/
Sep 2023
Average
0.009809
/ 0.006512
MGD *
/
Oct 2023
Average
0.009147
/ 0.006512
MGD *
/
Nov 2023
Average
0.00557
/ 0.006512
MGD
/
Dec 2023
Average
0.003598
/ 0.006512
MGD
/
2023
Quarter 3
0.009095
/
MGD
/
2023
Quarter 4
0.006105
/
MGD
/
2023
2nd 6 Months (Avg) 0.007600
/
MGD
/
2023
2nd 6 ...(Max)
0.01003
/
MGD
/
2023
2nd 6 ...(Min)
0.003598
/
MGD
/
2023
2nd 6 ...(Count)
6
Sample Count: 6
Months Sampled
: 6
Weeks Sampled :
6
Quarters Sampled :
2
# Over Daily C:
0 0.00
# Over Mo Avg C :
4 66.67
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0 0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0 0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC :
0 0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
BOD
07/28/2023
P Tergus072823POTW
31.5
/ mg/L /
09/26/2023
S Tergus092623Self
<
1
/ mg/L < /
Jul 2023
Week 4
31.5
/ mg/L /
Sep 2023
Week 4
<
1
/ mg/L < /
Jul 2023
Average
31.5
/ mg/L /
Sep 2023
Average
<
1
/ mg/L < /
2023
Quarter 3
<
16.3
/ mg/L < /
2023
2nd 6 Months (Avg)
<
16.3
/ mg/L < /
2023
2nd 6 ...(Max)
31.5
/ mg/L /
2023
2nd 6 ...(Min)
<
1
/ mg/L < /
2023
2nd 6 ...(Count)
2
/ /
Sunday, February 25, 2024 8:52:39AM * Indicates Violation ** Indicates TRC Violation Page 2 of 13

Tergus Pharma
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
07/28/2023
P Tergus072823POTW
<
0.00008
/ mg/L
<
/
09/26/2023
S Tergus092623Self
<
0.00004
/ mg/L
<
/
Jul 2023
Week 4
<
0.00008
/ mg/L
<
/
Sep 2023
Week 4
<
0.00004
/ mg/L
<
/
Jul 2023
Average
<
0.00008
/ mg/L
<
/
Sep 2023
Average
<
0.00004
/ mg/L
<
/
2023
Quarter 3
<
0.00006
/ mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.00006
/ mg/L
<
/
2023
2nd 6 ...(Max)
<
0.00008
/ mg/L
<
/
2023
2nd 6 ...(Min)
<
0.00004
/ mg/L
<
/
2023
2nd 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
07/28/2023
P Tergus072823POTW
30
/ mg/L
/
09/26/2023
S Tergus092623Self
15.2
/ mg/L
/
Jul 2023
Week 4
30
/ mg/L
/
Sep 2023
Week 4
15.2
/ mg/L
/
Jul2023
Average
30
/ mg/L
/
Sep 2023
Average
15.2
/ mg/L
/
2023
Quarter 3
22.6
/ mg/L
/
2023
2nd 6 Months (Avg)
22.6
/ mg/L
/
2023
2nd 6 ...(Max)
30
/ mg/L
/
2023
2nd 6 ...(Min)
15.2
/ mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
07/28/2023
P Tergus072823POTW
<
0.001
/ mg/L
< /
09/26/2023
S Tergus092623Self
<
0.001
/ mg/L
< /
Jul 2023
Week 4
<
0.001
/ mg/L
< /
Sep 2023
Week 4
<
0.001
/ mg/L
< /
Jul 2023
Average
<
0.001
/ mg/L
< /
Sep 2023
Average
<
0.001
/ mg/L
< /
2023
Quarter 3
<
0.001
/ mg/L
< /
2023
2nd 6 Months (Avg)
<
0.001
/ mg/L
< /
2023
2nd 6 ...(Max)
<
0.001
/ mg/L
< /
2023
2nd 6 ...(Min)
<
0.001
/ mg/L
< /
2023
2nd 6 ...(Count)
2
Sunday, February 25, 2024 8:52:39AM * Indicates Violation ** Indicates TRC Violation Page 3 of 13

Tergus Pharma
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Copper
07/28/2023
P Tergus072823POTW
0.041
/ mg/L
/
09/26/2023
S Tergus092623Self
0.051
/ mg/L
/
Jul 2023
Week 4
0.041
/ mg/L
/
Sep 2023
Week 4
0.051
/ mg/L
/
Jul 2023
Average
0.041
/ mg/L
/
Sep 2023
Average
0.051
/ mg/L
/
2023
Quarter 3
0.046
/ mg/L
/
2023
2nd 6 Months (Avg)
0.046
/ mg/L
/
2023
2nd 6 ...(Max)
0.051
/ mg/L
/
2023
2nd 6 ...(Min)
0.041
/ mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
07/28/2023
P Tergus072823POTW
0.007
/ mg/L
/
09/26/2023
S Tergus092623Self
<
0.001
/ mg/L
<
/
Jul 2023
Week 4
0.007
/ mg/L
/
Sep 2023
Week 4
<
0.001
/ mg/L
<
/
Jul 2023
Average
0.007
/ mg/L
/
Sep 2023
Average
<
0.001
/ mg/L
<
/
2023
Quarter 3
<
0.004
/ mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.004
/ mg/L
<
/
2023
2nd 6 ...(Max)
0.007
/ mg/L
/
2023
2nd 6 ...(Min)
<
0.001
/ mg/L
<
/
2023
2nd 6 ...(Count)
2
/
/
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
07/28/2023
P Tergus072823POTW
<
0.005
/ 20.7
mg/L
< /
09/26/2023
S Tergus092623Self
<
0.003
/ 20.7
mg/L
< /
Jul 2023
Week 4
<
0.005
/
mg/L
< /
Sep 2023
Week 4
<
0.003
/
mg/L
< /
Jul 2023
Average
<
0.005
/ 8.2
mg/L
< /
Sep 2023
Average
<
0.003
/ 8.2
mg/L
< /
2023
Quarter 3
<
0.004
/
mg/L
< /
2023
2nd 6 Months (Avg)
<
0.004
/
mg/L
< /
2023
2nd 6 ...(Max)
<
0.005
/
mg/L
< /
2023
2nd 6 ...(Min)
<
0.003
/
mg/L
< /
2023
2nd 6 ...(Count)
2
Sunday, February 25, 2024 8:52:39AM * Indicates Violation ** Indicates TRC Violation Page 4 of 13

Tergus Pharma
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
2
Months Sampled :
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
07/28/2023
P Tergus072823POTW
0.45
/ mg/L
/
09/26/2023
S Tergus092623Self
0.69
/ mg/L
/
Jul 2023
Week 4
0.45
/ mg/L
/
Sep 2023
Week 4
0.69
/ mg/L
/
Jul 2023
Average
0.45
/ mg/L
/
Sep 2023
Average
0.69
/ mg/L
/
2023
Quarter 3
0.57
/ mg/L
/
2023
2nd 6 Months (Avg)
0.57
/ mg/L
/
2023
2nd 6 ...(Max)
0.69
/ mg/L
/
2023
2nd 6 ...(Min)
0.45
/ mg/L
/
2023
2nd 6 ...(Count)
2
/
/
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
07/28/2023 P
Tergus072823POTW <
0.003
/ 20.7
mg/L
<
/
09/26/2023 S
Tergus092623Self <
0
/ 20.7
mg/L
<
/
Jul 2023
Week 4 <
0.003
/
mg/L
<
/
Sep 2023
Week 4 <
0
/
mg/L
<
/
Jul 2023
Average <
0.003
/ 8.2
mg/L
<
/
Sep 2023
Average <
0
/ 8.2
mg/L
<
/
2023
Quarter 3 <
0.001
/
mg/L
<
/
2023
2nd 6 Months (Avg) <
0.001
/
mg/L
<
/
2023
2nd 6 ...(Max) <
0.003
/
mg/L
<
/
2023
2nd 6 ...(Min) <
0.000
/
mg/L
<
/
2023
2nd 6 ...(Count)
2
Sample Count : 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sunday, February 25, 2024 8:52:39AM * Indicates Violation ** Indicates TRC Violation Page 5 of 13

Tergus Pharma
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Lead
07/28/2023
P Tergus072823POTW
<
0.0003
/ mg/L
<
/
09/26/2023
S Tergus092623Self
<
0.0001
/ mg/L
<
/
Jul 2023
Week 4
<
0.0003
/ mg/L
<
/
Sep 2023
Week 4
<
0.0001
/ mg/L
<
/
Jul 2023
Average
<
0.0003
/ mg/L
<
/
Sep 2023
Average
<
0.0001
/ mg/L
<
/
2023
Quarter 3
<
0.0002
/ mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.0002
/ mg/L
<
/
2023
2nd 6 ...(Max)
<
0.0003
/ mg/L
<
/
2023
2nd 6 ...(Min)
<
0.0001
/ mg/L
<
/
2023
2nd 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
Mercury - LL
07/28/2023 P
Tergus072823POTWH 0.00001
/ 0.000142
mg/L
/
g
09/26/2023 S
Tergus092623Self < 0.000001
/ 0.000142
mg/L
<
/
Jul 2023
Week 4 0.00001
/
mg/L
/
Sep 2023
Week 4 < 0.000001
/
mg/L
<
/
Jul 2023
Average 0.00001
/
mg/L
/
Sep 2023
Average < 0.000001
/
mg/L
<
/
2023
Quarter 3 < 0.000005
/
mg/L
<
/
2023
2nd 6 Months (Avg) < 0.000005
/
mg/L
<
/
2023
2nd 6 ...(Max) 0.00001
/
mg/L
/
2023
2nd 6 ...(Min) < 0.000001
/
mg/L
<
/
2023
2nd 6 ...(Count) 2
Sample Count: 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C:
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
07/28/2023 P Tergus072823POTW <
09/26/2023 S Tergus092623Self <
Jul 2023 Week 4 <
Sep 2023 Week 4 <
Jul 2023 Average <
0.003
/ 3.0
mg/L < /
0.002
/ 3.0
mg/L < /
0.003
/
mg/L < /
0.002
/
mg/L < /
0.003
/ 0.7
mg/L < /
Sunday, February 25, 2024 8:52:39AM * Indicates Violation ** Indicates TRC Violation Page 6 of 13

Tergus Pharma
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
Sep 2023
Average <
0.002
/ 0.7
mg/L
<
/
2023
Quarter 3 <
0.002
/
mg/L
<
/
2023
2nd 6 Months (Avg) <
0.002
/
mg/L
<
/
2023
2nd 6 ...(Max) <
0.003
/
mg/L
<
/
2023
2nd 6 ...(Min) <
0.002
/
mg/L
<
/
2023
2nd 6 ...(Count)
2
Sample Count:
2 Months Sampled
:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
Molybdenum
07/28/2023 P
Tergus072823POTW <
0.001
/
mg/L
<
/
09/26/2023 S
Tergus092623Self <
0.003
/
mg/L
<
/
Jul 2023
Week 4 <
0.001
/
mg/L
<
/
Sep 2023
Week 4 <
0.003
/
mg/L
<
/
Jul 2023
Average <
0.001
/
mg/L
<
/
Sep 2023
Average <
0.003
/
mg/L
<
/
2023
Quarter 3 <
0.002
/
mg/L
<
/
2023
2nd 6 Months (Avg) <
0.002
/
mg/L
<
/
2023
2nd 6 ...(Max) <
0.003
/
mg/L
<
/
2023
2nd 6 ...(Min) <
0.001
/
mg/L
<
/
2023
2nd 6 ...(Count)
2
/
/
Sample Date SamplelD Result/Limit Mass / Limit
n-Amyl acetate
07/28/2023 P
Tergus072823POTW
09/26/2023 S
Tergus092623Self
Jul 2023
Week 4
Sep 2023
Week 4
Jul 2023
Average
Sep 2023
Average
2023
Quarter
2023
2nd 6 Months (Avg)
2023
2nd 6 ...(Max)
2023
2nd 6 ...(Min)
< 0.005
/ 20.7
mg/L
< /
< 0
/ 20.7
mg/L
< /
< 0.005
/
mg/L
< /
< 0
/
mg/L
< /
< 0.005
/ 8.2
mg/L
< /
< 0
/ 8.2
mg/L
< /
< 0.003
/
mg/L
< /
< 0.003
/
mg/L
< /
< 0.005
/
mg/L
< /
< 0.000
/
mg/L
< /
Sunday, February 25, 2024 8:52:39AM * Indicates Violation ** Indicates TRC Violation Page 7 of 13

Tergus Pharma
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
n-Amyl acetate
2023
2nd 6 ...(Count)
2
Sample Count: 2 Months Sampled: 2
Weeks Sampled:
2
Quarters Sampled :
I
# Over Daily C :
0 0.00 # Over Mo Avg C :
0 0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0,00 # Over Mo Avg C TRC
: 0 0.00
# Over Wk Avg C TRC:
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0 0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0,00 # Over Mo Avg M TRC
: 0 0,00
# Over Wk Avg M TRC :
0
0,00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass /Limit
Nickel
07/28/2023 P
Tergus072823POTW
0.002 /
mg/L
/
09/26/2023 S
Tergus092623Self <
0.0025 /
mg/L
<
/
Jul 2023
Week 4
0.002 /
mg/L
/
Sep 2023
Week 4 <
0.0025 /
mg/L
<
/
Jul 2023
Average
0.002 /
mg/L
/
Sep 2023
Average <
0.0025 /
mg/L
<
/
2023
Quarter 3 <
0.0023 /
mg/L
<
/
2023
2nd 6 Months (Avg) <
0.0023 /
mg/L
<
/
2023
2nd 6 ...(Max) <
0.0025 /
mg/L
<
/
2023
2nd 6 ...(Min)
0.002 /
mg/L
/
2023
2nd 6 ...(Count)
2 /
/
Sample Date
SamplelD
Result/Limit
Mass/Limit
Nitrate -Nitrite
07/28/2023 P
Tergus072823POTW <
09/26/2023 S
Tergus092623Self <
Jul 2023
Week 4 <
Sep 2023
Week 4 <
Jul 2023
Average <
Sep 2023
Average <
2023
Quarter 3 <
2023
2nd 6 Months (Avg) <
2023
2nd 6 ...(Max) <
2023
2nd 6 ...(Min) <
2023
2nd 6 ...(Count)
Sample Date
SamplelD
Nitrogen, Total
07/28/2023 P
Tergus072823POTW
Sunday, February 25, 2024 8:52:39AM
0.1
/ mg/L
<
0.1
/ mg/L
<
0.1
/ mg/L
<
0.1
/ mg/L
<
0.1
/ mg/L
<
0.1
/ mg/L
<
0.1
/ mg/L
<
0.1
/ mg/L
<
0.1
/ mg/L
<
0.1
/ mg/L
<
2
/
Result/Limit
1.31 / mg/L
* Indicates Violation ** Indicates TRC Violation
Mass /Limit
Page 8 of 13

Tergus Pharma
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen, Total
09/26/2023 S
Tergus092623Self
1.58
/ mg/L
/
Jul 2023
Week 4
1.31
/ mg/L
/
Sep 2023
Week 4
1.58
/ mg/L
/
Jul 2023
Average
1.31
/ mg/L
/
Sep 2023
Average
1.58
/ mg/L
/
2023
Quarter 3
1.45
/ mg/L
/
2023
2nd 6 Months (Avg)
1.45
/ mg/L
/
2023
2nd 6 ...(Max)
1.58
/ mg/L
/
2023
2nd 6 ...(Min)
1.31
/ mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
Oil & Grease, Total
07/28/2023 P
Tergus072823POTW <
2.5
/ 200
mg/L
<
/
09/26/2023 S
Tergus092623Self <
2.5
/ 200
mg/L
<
/
Jul 2023
Week 4 <
2.5
/
mg/L
<
/
Sep 2023
Week 4 <
2.5
/
mg/L
<
/
Jul 2023
Average <
2.5
/
mg/L
<
/
Sep 2023
Average <
2.5
/
mg/L
<
/
2023
Quarter 3 <
2.5
/
mg/L
<
/
2023
2nd 6 Months (Avg) <
2.5
/
mg/L
<
/
2023
2nd 6 ...(Max) <
2.5
/
mg/L
<
/
2023
2nd 6 ...(Min) <
2.5
/
mg/L
<
/
2023
2nd 6 ...(Count)
2
Sample Count: 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M:
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
PH
07/28/2023
P Tergus072823POTW
Jul 2023
Week 4
Jul 2023
Average
2023
Quarter
2023
2nd 6 Months (Avg)
2023
2nd 6 ...(Max)
6.8
/6.0-10.0
SU /
6.8
/
Su /
6.8
/
Su /
6.8
/
Su /
6.8
/
SU /
6.8
/
SU /
Sunday, February 25, 2024 8:52:39AM * Indicates Violation ** Indicates TRC Violation Page 9 of 13

Tergus Pharma
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
pH
2023
2nd 6 ...(Min)
6.8
/
SU
/
2023
2nd 6 ...(Count)
1
Sample Count : 1 Months Sampled:
1
Weeks Sampled:
1
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC
:
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
Selenium
07/28/2023 P
Tergus072823POTW <
0.0005
/
mg/L
<
/
09/26/2023 S
Tergus092623Self <
0.0005
/
mg/L
<
/
Jul 2023
Week 4 <
0.0005
/
mg/L
<
/
Sep 2023
Week 4 <
0.0005
/
mg/L
<
/
Jul 2023
Average <
0.0005
/
mg/L
<
/
Sep 2023
Average <
0.0005
/
mg/L
<
/
2023
Quarter 3 <
0.0005
/
mg/L
<
/
2023
2nd 6 Months (Avg) <
0.0005
/
mg/L
<
/
2023
2nd 6 ...(Max) <
0.0005
/
mg/L
<
/
2023
2nd 6 ...(Min) <
0.0005
/
mg/L
<
/
2023
2nd 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
Silver
07/28/2023
P Tergus072823POTW
<
0.0003
/ mg/L
<
/
09/26/2023
S Tergus092623Self
<
0.0002
/ mg/L
<
/
Jul 2023
Week 4
<
0.0003
/ mg/L
<
/
Sep 2023
Week 4
<
0.0002
/ mg/L
<
/
Jul 2023
Average
<
0.0003
/ mg/L
<
/
Sep 2023
Average
<
0.0002
/ mg/L
<
/
2023
Quarter 3
<
0.0002
/ mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.0002
/ mg/L
<
/
2023
2nd 6 ...(Max)
<
0.0003
/ mg/L
<
/
2023
2nd 6 ...(Min)
<
0.0002
/ mg/L
<
/
2023
2nd 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass /Limit
Temperature
Sunday, February 25, 2024 8:52:39AM * Indicates Violation ** Indicates TRC Violation Page 10 of 13

Tergus Pharma
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
07/28/2023 P
Tergus072823POTW
30
/ 66
°C
/
09/26/2023 S
Tergus092623Self
29.5
/ 66
°C
/
Ju12023
Week 4
30
/
°C
/
Sep 2023
Week 4
29.5
/
°C
/
Ju12023
Average
30
/
°C
/
Sep 2023
Average
29.5
/
°C
/
2023
Quarter 3
29.8
/
°C
/
2023
2nd 6 Months (Avg)
29.8
/
°C
/
2023
2nd 6 ...(Max)
30
/
°C
/
2023
2nd 6 ...(Min)
29.5
/
°C
/
2023
2nd 6 ...(Count)
2
Sample Count: 2 Months Sampled
:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
07/28/2023
P Tergus072823POTW
1.31
/ mg/L
/
09/26/2023
S Tergus092623Self
1.58
/ mg/L
/
Jul 2023
Week 4
1.31
/ mg/L
/
Sep 2023
Week 4
1.58
/ mg/L
/
Jul 2023
Average
1.31
/ mg/L
/
Sep 2023
Average
1.58
/ mg/L
/
2023
Quarter 3
1.45
/ mg/L
/
2023
2nd 6 Months (Avg)
1.45
/ mg/L
/
2023
2nd 6 ...(Max)
1.58
/ mg/L
/
2023
2nd 6 ...(Min)
1.31
/ mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
Total Phosphorus
07/28/2023 P
Tergus072823POTW
0.522 /
mg/L
/
09/26/2023 S
Tergus092623Self
0.407 /
mg/L
/
Jul 2023
Week 4
0.522 /
mg/L
/
Sep 2023
Week 4
0.407 /
mg/L
/
Jul 2023
Average
0.522 /
mg/L
/
Sunday, February 25, 2024 8:52:39AM * Indicates Violation ** Indicates TRC Violation Page 11 of 13

Tergus Pharma
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
Total Phosphorus
Sep 2023
Average
0.407 /
mg/L
/
2023
Quarter 3
0.465 /
mg/L
/
2023
2nd 6 Months (Avg)
0.465 /
mg/L
/
2023
2nd 6 ...(Max)
0.522 /
mg/L
/
2023
2nd 6 ...(Min)
0.407 /
mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass /Limit
TSS
07/28/2023
P
Tergus072823POTW
12 /
mg/L
/
09/26/2023
S
Tergus092623Self
<
1.3 /
mg/L
<
/
Jul 2023
Week 4
12 /
mg/L
/
Sep 2023
Week 4
<
1.3 /
mg/L
<
/
Jul 2023
Average
12 /
mg/L
/
Sep 2023
Average
<
1.3 /
mg/L
<
/
2023
Quarter 3
<
6.6 /
mg/L
<
/
2023
2nd 6 Months (Avg)
<
6.6 /
mg/L
<
/
2023
2nd 6 ...(Max)
12 /
mg/L
/
2023
2nd 6 ...(Min)
<
1.3 /
mg/L
<
/
2023
2nd 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
VOC
07/28/2023
P
Tergus072823POTW
0.067 /
mg/L
/
09/26/2023
S
Tergus092623Self
0.002 /
mg/L
/
Jul 2023
Week 4
0.067 /
mg/L
/
Sep 2023
Week 4
0.002 /
mg/L
/
Jul 2023
Average
0.067 /
mg/L
/
Sep 2023
Average
0.002 /
mg/L
/
2023
Quarter 3
0.0345 /
mg/L
/
2023
2nd 6 Months (Avg)
0.0345 /
mg/L
/
2023
2nd 6 ...(Max)
0.067 /
mg/L
/
2023
2nd 6 ...(Min)
0.002 /
mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
Zinc
07/28/2023
P
Tergus072823POTW
0.144 /
mg/L
/
09/26/2023
S
Tergus092623Self
0.154 /
mg/L
/
Jul 2023
Week 4
0.144 /
mg/L
/
Sep 2023
Week 4
0.154 /
mg/L
/
Sunday, February 25, 2024 8:52:39AM * Indicates Violation ** Indicates TRC Violation Page 12 of 13

Tergus Pharma
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
Jul 2023
Sep 2023
2023
2023
2023
2023
2023
Average
0.144
/ mg/L /
Average
0.154
/ mg/L /
Quarter 3
0.149
/ mg/L /
2nd 6 Months (Avg)
0.149
/ mg/L /
2nd 6 ...(Max)
0.154
/ mg/L /
2nd 6 ...(Min)
0.144
/ mg/L /
2nd 6 ...(Count)
2
Sunday, February 25, 2024 8:52:39AM * Indicates Violation ** Indicates TRC Violation Page 13 of 13

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result/Limit Mass/Limit
Acetone
07/28/2023 P
TriPharm072823POT
0.156
/ 5.44
mg/L
0.0079 / Ibs/day
W
09/14/2023 S
TriPhartn091423Self
0.12
/ 5.44
mg/L
/
Jul 2023
Week 4
0.156
/
mg/L
0.0079 / lbs/day
Sep 2023
Week 2
0.12
/
mg/L
/
Jul 2023
Average
0.156
/ 2.15
mg/L
0.0079 / Ibs/day
Sep 2023
Average
0.12
/ 2,15
mg/L
/
2023
Quarter 3
0.138
/
mg/L
0.0079 / Ibs/day
2023
2nd 6 Months (Avg)
0.138
/
mg/L
0.0079 / Ibs/day
2023
2nd 6 ...(Max)
0.156
/
mg/L
0.0079 / Ibs/day
2023
2nd 6 ...(Min)
0.12
/
mg/L
/
2023
2nd 6 ...(Count)
2
/
1 /
Sample Count: 2 Months Sampled:
2
Weeks Sampled:
2 Quarters Sampled :
I
# Over Daily C :
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00 # Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC
:
0
0.00
# Over Wk Avg C TRC : 0
0.00 # Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00 # Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC : 0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SampleID
Result/Limit
Mass /Limit
Ammonia
07/28/2023
P TriPharm072823POT
0.3
/ mg/L
0.0152 /
Ibs/day
W
09/14/2023
S TriPharm091423Self
0.1
/ mg/L
/
Jul 2023
Week 4
0.3
/ mg/L
0.0152 /
lbs/day
Sep 2023
Week 2
0.1
/ mg/L
/
Jul 2023
Average
0.3
/ mg/L
0.0152 /
Ibs/day
Sep 2023
Average
0.1
/ mg/L
/
2023
Quarter 3
0.2
/ mg/L
0.0152 /
Ibs/day
2023
2nd 6 Months (Avg)
0.2
/ mg/L
0.0152 /
Ibs/day
2023
2nd 6 ...(Max)
0.3
/ mg/L
0.0152 /
Ibs/day
2023
2nd 6 ...(Min)
0.1
/ mg/L
/
2023
2nd 6 ...(Count)
2
/
1 /
Sample Date SampleID Result/Limit Mass I Limit
Average Flow for Month
07/31/2023
S
TriPhann0723FIow
08/31/2023
S
TriPharm0823FIow
09/30/2023
S
TriPharm0923FIow
10/31/2023
S
TirPharm1023F1ow
0.005494 /
MGD /
0.006163 /
MGD /
0.004371 /
MGD /
0.004654 /
MGD /
Saturday, February 24, 2024 9:20:33PM * Indicates Violation ** Indicates TRC Violation Page 1 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outttall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
11/30/2023 S
TriPharm1123Flow
0.005254
/
MGD
/
12/31/2023 S
TriPharm 1223 Flow
0.006182
/
MGD
/
Jul 2023
Week 4
0.005494
/
MGD
/
Aug 2023
Week 4
0.006163
/
MGD
/
Sep 2023
Week 4
0.004371
/
MGD
/
Oct 2023
Week 4
0.004654
/
MGD
/
Nov 2023
Week 4
0.005254
/
MGD
/
Dec 2023
Week 4
0.006182
/
MGD
/
Jul 2023
Average
0.005494
/ 0.008
MGD
/
Aug 2023
Average
0.006163
/ 0.008
MGD
/
Sep 2023
Average
0.004371
/ 0.008
MGD
/
Oct 2023
Average
0.004654
/ 0.008
MGD
/
Nov 2023
Average
0.005254
/ 0.008
MGD
/
Dec 2023
Average
0.006182
/ 0.008
MGD
/
2023
Quarter 3
0.005343
/
MGD
/
2023
Quarter 4
0.005363
/
MGD
/
2023
2nd 6 Months (Avg) 0.005353
/
MGD
/
2023
2nd 6 ...(Max)
0.006182
/
MGD
/
2023
2nd 6 ...(Min)
0.004371
/
MGD
/
2023
2nd 6 ...(Count)
6
Sample Count: 6
Months Sampled
: 6
Weeks Sampled:
6
Quarters Sampled :
2
# Over Daily C:
0 0.00
# Over Mo Avg C :
0 0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0 0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M:
0 0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC :
0 0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
BOD
07/28/2023
P TriPharm072823POT
17
/ mg/L
0.861
/ Ibs/day
W
09/14/2023
S TriPharrn091423Self
5.3
/ mg/L
/
Jul 2023
Week 4
17
/ mg/L
0.861
/ lbs/day
Sep 2023
Week 2
5.3
/ mg/L
/
Jul 2023
Average
17
/ mg/L
0.861
/ Ibs/day
Sep 2023
Average
5.3
/ mg/L
/
2023
Quarter 3
11.2
/ mg/L
0.861
/ Ibs/day
2023
2nd 6 Months (Avg)
11.2
/ mg/L
0.861
/ Ibs/day
2023
2nd 6 ...(Max)
17
/ mg/L
0.861
/ Ibs/day
2023
2nd 6 ...(Min)
5.3
/ mg/L
/
Saturday, February 24, 2024 9:20:33PM * Indicates Violation ** Indicates TRC Violation Page 2 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
BOD
2023 2nd 6 ...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
07/28/2023
P TriPharm072823POT
<
0.00008
/ mg/L
<
0.000004
/ lbs/day
W
09/14/2023
S TriPharm091423Self
<
0.00008
/ mg/L
<
/
Jul 2023
Week 4
<
0.00008
/ mg/L
<
0.000004
/ lbs/day
Sep 2023
Week 2
<
0.00008
/ mg/L
<
/
Jul 2023
Average
<
0.00008
/ mg/L
<
0.000004
/ lbs/day
Sep 2023
Average
<
0.00008
/ mg/L
<
/
2023
Quarter 3
<
0.00008
/ mg/L
<
0.000004
/ Ibs/day
2023
2nd 6 Months (Avg)
<
0.00008
/ mg/L
<
0.000004
/ lbs/day
2023
2nd 6 ...(Max)
<
0.00008
/ mg/L
<
0.000004
/ lbs/day
2023
2nd 6 ...(Min)
<
0.00008
/ mg/L
<
/
2023
2nd 6 ...(Count)
2
/
1
/
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
07/28/2023
P
TriPharm072823POT
W
09/14/2023
S
TriPharm091423Self
Jul 2023
Week 4
Sep 2023
Week 2
Jul 2023
Average
Sep 2023
Average
2023
Quarter 3
2023
2nd 6 Months (Avg)
2023
2nd 6 ...(Max)
2023
2nd 6 ...(Min)
2023
2nd 6 ...(Count)
Sample Date
SamplelD
COD
07/28/2023
P
TriPharm072823POT
W
09/14/2023
S
TriPharm091423Self
Jul 2023
Week 4
Sep 2023
Week 2
Jul 2023
Average
Sep 2023
Average
2023
Quarter 3
Saturday, February 24,2024 9:20:33PM
855 /
mg/L
1150 /
mg/L
855 /
mg/L
1150 /
mg/L
855 /
mg/L
1150 /
mg/L
1002.5 /
mg/L
1002.5 /
mg/L
1150 /
mg/L
855 /
mg/L
2 /
Result/Limit
45 /
mg/L
43 /
mg/L
45 /
mg/L
43 /
mg/L
45 /
mg/L
43 /
mg/L
44 /
mg/L
* Indicates Violation
** Indicates TRC Violation
43.2905
/
lbs/day
43.2905
/
lbs/day
43.2905
/
Ibs/day
43.2905
/
Ibs/day
43.2905
/
Ibs/day
43.2905
/
lbs/day
1
/
Mass /Limit
2.28
/
lbs/day
228
/
Ibs/day
2.28
/
lbs/day
2.28
/
lbs/day
Page 3 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
SarnpleDate SamplelD Result/Limit Mass/Limit
COD
2023
2nd 6 Months (Avg)
44 / mg/L
2.28 / lbs/day
2023
2nd 6 ...(Max)
45 / mg/L
2.28 / lbs/day
2023
2nd 6 ...(Min)
43 / mg/L
/
2023
2nd 6 ...(Count)
2 /
I /
Sample Date
SamplelD
Result/Limit
Mass/Limit
Ethyl acetate
07/28/2023 P
TriPhann072823POT <
0.005
/ 5.44
mg/L
<
0.0003 /
lbs/day
W
09/14/2023 S
TriPharm091423Self <
0.003
/ 5.44
mg/L
<
/
Jul 2023
Week 4
<
0.005
/
mg/L
<
0.0003 /
Ibs/day
Sep 2023
Week 2
<
0.003
/
mg/L
<
/
Jul 2023
Average
<
0.005
/ 2.15
mg/L
<
0.0003 /
lbs/day
Sep 2023
Average
<
0.003
/ 2.15
mg/L
<
/
2023
Quarter 3
<
0.004
/
mg/L
<
0.0003 /
lbs/day
2023
2nd 6 Months (Avg) <
0.004
/
mg/L
<
0.0003 /
lbs/day
2023
2nd 6 ...(Max)
<
0.005
/
mg/L
<
0.0003 /
Ibs/day
2023
2nd 6 ...(Min)
<
0.003
/
mg/L
<
/
2023
2nd 6 ...(Count)
2
/
I /
Sample Count: 2
Months Sampled:
2
Weeks Sampled:
2 Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00 # Over Qt Avg C :
0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC
:
0
0.00
# Over Wk Avg C TRC :
0
0.00 # Over Qt Avg C TRC
: 0
0.00
# Over Daily M:
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00 # Over Qtr Avg M :
0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
Fluoride
07/28/2023
P TriPharm072823POT
0.73 /
mg/L
0.037 /
Ibs/day
W
09/14/2023
S TriPharm09l423Setf
0.67 /
mg/L
/
Jul 2023
Week 4
0.73 /
mg/L
0.037 /
lbs/day
Sep 2023
Week 2
0.67 /
mg/L
/
Jul 2023
Average
0.73 /
mg/L
0.037 /
lbs/day
Sep 2023
Average
0.67 /
mg/L
/
2023
Quarter 3
0.7 /
mg/L
0.037 /
Ibs/day
2023
2nd 6 Months (Avg)
0.7 /
mg/L
0.0370 /
lbs/day
2023
2nd 6 ...(Max)
0.73 /
mg/L
0.0370 /
lbs/day
2023
2nd 6 ...(Min)
0.67 /
mg/L
/
2023
2nd 6 ...(Count)
2 /
1 /
Saturday, February 24, 2024 9:20:33PM * Indicates Violation ** Indicates TRC Violation Page 4 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
07/28/2023 P
TriPharm072823POT <
0.005
/ 5.44
mg/L
<
0.0003 / lbs/day
W
09/14/2023 S
TriPhartn091423Self <
0.003
/ 5.44
mg/L
<
/
Jul 2023
Week 4
<
0.005
/
mg/L
<
0.0003 / lbs/day
Sep 2023
Week 2
<
0.003
/
mg/L
<
/
Jul 2023
Average
<
0.005
/ 2.15
mg/L
<
0.0003 / Ibs/day
Sep 2023
Average
<
0.003
/ 2,15
mg/L
<
/
2023
Quarter 3
<
0.004
/
mg/L
<
0.0003 / Ibs/day
2023
2nd 6 Months (Avg) <
0.004
/
mg/L
<
0.0003 / Ibs/day
2023
2nd 6 ...(Max)
<
0.005
/
mg/L
<
0.0003 / Ibs/day
2023
2nd 6 ...(Min)
<
0.003
/
mg/L
<
/
2023
2nd 6 ...(Count)
2
/
1 /
Sample Count: 2
Months Sampled:
2
Weeks Sampled:
2 Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00 # Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00 # Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00 # Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
Mercury - LL
07/28/2023 P
TriPharm072823POT
0.000004
/ 0.000142
mg/L
/
WHg
09/14/2023 S
TriPharm091423Self
0.000002
/ 0.000142
mg/L
/
Jul 2023
Week 4
0.000004
/
mg/L
/
Sep 2023
Week 2
0.000002
/
mg/L
/
Jul 2023
Average
0.000004
/
mg/L
/
Sep 2023
Average
0.000002
/
mg/L
/
2023
Quarter 3
0.000003
/
mg/L
/
2023
2nd 6 Months (Avg)
0.000003
/
mg/L
/
2023
2nd 6 ...(Max)
0.000004
/
mg/L
/
2023
2nd 6 ...(Min)
0.000002
/
mg/L
/
2023
2nd 6 ...(Count)
2
Sample Count : 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C:
0 0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C :
0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0 0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC :
0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0 0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M :
0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0 0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC :
0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Saturday, February 24, 2024 9:20:33PM
* Indicates Violation
** Indicates TRC Violation
Page
5 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result/Limit Mass/Limit
Methylene Chloride
07/28/2023 P
TriPharm072823POT
<
0.003
/ 0.78
mg/L
<
0.000127 /
Ibs/day
W
09/14/2023 S
TriPhartn091423Self
0.002
/ 0.78
mg/L
/
Jul 2023
Week 4
<
0.003
/
mg/L
<
0.000127 /
lbs/day
Sep 2023
Week 2
0.002
/
mg/L
/
Jul 2023
Average
<
0.003
/ 0.18
mg/L
<
0.000127 /
Ibs/day
Sep 2023
Average
0.002
/ 0.18
mg/L
/
2023
Quarter 3
<
0.002
/
mg/L
<
0.000127 /
Ibs/day
2023
2nd 6 Months (Avg)
<
0.002
/
mg/L
<
0.000127 /
Ibs/day
2023
2nd 6 ...(Max)
<
0.003
/
mg/L
<
0.000127 /
Ibs/day
2023
2nd 6 ...(Min)
0.002
/
mg/L
/
2023
2nd 6 ...(Count)
2
/
1 /
Sample Count:
2
Months Sampled:
2
Weeks Sampled:
2 Quarters Sampled :
1
# Over Daily C :
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00 # Over Qt Avg C :
0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC
:
0
0.00
# Over Wk Avg C TRC :
0
0.00 # Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00 # Over Qtr Avg M :
0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SampleID
Result/Limit
Mass /Limit
Molybdenum
07/28/2023 P
TriPharm072823POT
<
0.001
/
mg/L
<
0.0001 /
Ibs/day
W
09/14/2023 S
TriPhatm091423Self
<
0.001
/
mg/L
<
/
Jul 2023
Week 4
<
0.001
/
mg/L
<
0.0001 /
lbs/day
Sep 2023
Week 2
<
0.001
/
mg/L
<
/
Jul 2023
Average
<
0.001
/
mg/L
<
0.0001 /
Ibs/day
Sep 2023
Average
<
0.001
/
mg/L
<
/
2023
Quarter 3
<
0.001
/
mg/L
<
0.0001 /
Ibs/day
2023
2nd 6 Months (Avg)
<
0.001
/
mg/L
<
0.0001 /
Ibs/day
2023
2nd 6 ...(Max)
<
0.001
/
mg/L
<
0.0001 /
Ibs/day
2023
2nd 6 ...(Min)
<
0.001
/
mg/L
<
/
2023
2nd 6 ...(Count)
2
/
1 /
Sample Date SampleID Result/Limit Mass/Limit
n-Amyl acetate
07/28/2023 P TriPhann072823POT
W
09/14/2023 S TriPhatm091423Self
Jul 2023 Week 4
Sep 2023 Week 2
< 0.005 / 5.44 mg/L < 0.0003 / lbs/day
< 0.025 / 5.44 mg/L < /
< 0.005 / mg/L < 0.0003 / Ibs/day
< 0.025 / mg/L < /
Saturday, February 24, 2024 9:20:33PM * Indicates Violation ** Indicates TRC Violation Page 6 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
Jul 2023
Average
<
0.005
/ 2.15
mg/L <
0.0003 / Ibs/day
Sep 2023
Average
<
0.025
/ 2.15
mg/L <
/
2023
Quarter 3
<
0.015
/
mg/L <
0.0003 / lbs/day
2023
2nd 6 Months (Avg) <
0.015
/
mg/L <
0.0003 / Ibs/day
2023
2nd 6 ...(Max)
<
0.025
/
mg/L <
0.0003 / Ibs/day
2023
2nd 6 ...(Min)
<
0.005
/
mg/L <
/
2023
2nd 6 ...(Count)
2
/
1 /
Sample
Count: 2
Months Sampled
:
2
Weeks Sampled:
2 Quarters Sampled :
I
# I%
#
%
#
% #
%
# Over Daily C :
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00 # Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00 # Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00 # Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC : 0
0.00 # Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
SampleDate SrnnplelD Result/Limit Mass/Limit
Nitrate -Nitrite
07/28/2023 P
TriPharrn072823POT
0.7
/ mg/L
0.034 /
Ibs/day
W
09/14/2023 S
TriPharm091423Self
0.9
/ mg/L
/
Jul 2023
Week 4
0.7
/ mg/L
0.034 /
Ibs/day
Sep 2023
Week 2
0.9
/ mg/L
/
Jul 2023
Average
0.7
/ mg/L
0.034 /
Ibs/day
Sep 2023
Average
0.9
/ mg/L
/
2023
Quarter 3
0.8
/ mg/L
0.034 /
Ibs/day
2023
2nd 6 Months (Avg)
0.8
/ mg/L
0.034 /
Ibs/day
2023
2nd 6 ...(Max)
0.9
/ mg/L
0.034 /
lbs/day
2023
2nd 6 ...(Min)
0.7
/ mg/L
/
2023
2nd 6 ...(Count)
2
/
I /
Sample Date SamplelD Result/Limit Mass /Limit
Nitrogen, Total
07/28/2023 P
TriPhartn072823POT
W
09/14/2023 S
TriPharm091423Self
Jul 2023
Week 4
Sep 2023
Week 2
Jul 2023
Average
Sep 2023
Average
2023
Quarter 3
2023
2nd 6 Months (Avg)
1.75
/ mg/L
0.089 /
Ibs/day
0.88
/ mg/L
/
1.75
/ mg/L
0.089 /
lbs/day
0.88
/ mg/L
/
1.75
/ mg/L
0.089 /
lbs/day
0.88
/ mg/L
/
1.32
/ mg/L
0.089 /
Ibs/day
1.32
/ mg/L
0.089 /
lbs/day
Saturday, February 24, 2024 9:20:33PM * Indicates Violation ** Indicates TRC Violation Page 7 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
SarnpleDate
SamplelD
Result/Limit
Mass/Limit
Nitrogen, Total
2023
2nd 6 ...(Max)
1.75 /
mg/L
0.089 / lbs/day
2023
2nd 6 ...(Min)
0.88 /
mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
pH
07/28/2023 P
TriPhann072823POT
6.8 / 5.5 - 10.5
SU
/
W
09/14/2023 S
TriPharm091423Self
7.2 / 5.5 - 10.5
SU
/
Jul 2023
Week 4
6.8 /
SU
/
Sep 2023
Week 2
7.2 /
SU
/
Jul 2023
Average
6.8 /
SU
/
Sep 2023
Average
7.2 /
SU
/
2023
Quarter 3
7 /
SU
/
2023
2nd 6 Months (Avg)
7 /
SU
/
2023
2nd 6 ...(Max)
7.2 /
SU
/
2023
2nd 6 ...(Min)
6.8 /
SU
/
2023
2nd 6 ...(Count)
2
Sample Count : 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C:
0 0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC
: 0 0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0 0.00 # Over Mo Avg M :
0 0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC
: 0 0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
Temperature
07/28/2023 P
TriPharm072823POT
30 / 66
°C
/
W
09/14/2023 S
TriPharm091423Self
30 / 66
°C
/
Jul 2023
Week 4
30 /
°C
/
Sep 2023
Week 2
30 /
°C
/
Jul 2023
Average
30 /
°C
/
Sep 2023
Average
30 /
°C
/
2023
Quarter 3
30 /
°C
/
2023
2nd 6 Months (Avg)
30 /
°C
/
2023
2nd 6 ...(Max)
30 /
°C
/
2023
2nd 6 ...(Min)
30 /
°C
/
2023
2nd 6 ...(Count)
2
Saturday, February 24, 2024 9:20:33PM * Indicates Violation ** Indicates TRC Violation Page 8 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Count:
2
Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C :
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0,00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Samplc Date SamplelD Result/Limit Mass/Limit
TKN
07/28/2023 P
TriPharm072823POT
1.07
/
mg/L
0.054 /
lbs/day
W
09/14/2023 S
TriPharm091423Self
<
0.1
/
mg/L
<
/
Jul 2023
Week 4
1.07
/
mg/L
0.054 /
Ibs/day
Sep 2023
Week 2
<
0.1
/
mg/L
<
/
Jul 2023
Average
1.07
/
mg/L
0.054 /
lbs/day
Sep 2023
Average
<
0.1
/
mg/L
<
/
2023
Quarter 3
<
0.59
/
mg/L
<
0.054 /
lbs/day
2023
2nd 6 Months (Avg)
<
0.59
/
mg/L
<
0.054 /
Ibs/day
2023
2nd 6 ...(Max)
1.07
/
mg/L
0.054 /
Ibs/day
2023
2nd 6 ...(Min)
<
0.1
/
mg/L
<
/
2023
2nd 6 ...(Count)
2
/
1 /
Sample Date
SamplelD
Result/Limit
Muss/Limit
Total Phosphorus
07/28/2023 P
TriPharm072823POT
0.48
/
mg/L
0.0243 /
Ibs/day
W
09/14/2023 S
TriPharm091423Self
0.381
/
mg/L
/
Jul 2023
Week 4
0.48
/
mg/L
0.0243 /
lbs/day
Sep 2023
Week 2
0.381
/
mg/L
/
Jul 2023
Average
0.48
/
mg/L
0.0243 /
Ibs/day
Sep 2023
Average
0.381
/
mg/L
/
2023
Quarter 3
0.431
/
mg/L
0.0243 /
Ibs/day
2023
2nd 6 Months (Avg)
0.431
/
mg/L
0.0243 /
Ibs/day
2023
2nd 6 ...(Max)
0.48
/
mg/L
0.0243 /
Ibs/day
2023
2nd 6 ...(Min)
0.381
/
mg/L
/
2023
2nd 6 ...(Count)
2
/
1 /
Sample Date SamplelD Result/Limit Mass/Limit
TSS
07/28/2023
P TriPhann072823POT
W
09/14/2023
S TriPharm091423Self <
Jul 2023
Week 4
Sep 2023
Week 2 <
Saturday, February 24,2024 9:20:33PM
3 / mg/L 0.151896 / lbs/day
1.3 / mg/L < /
3 / mg/L 0.151896 / Ibs/day
1.3 / mg/L < /
* Indicates Violation ** Indicates TRC Violation
Page 9 of 10

TriPharm Services, Inc. dba Alcami Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
TSS
Jul 2023
Average
3 /
mg/L
0.151896 /
Ibs/day
Sep 2023
Average <
1.3 /
mg/L
< /
2023
Quarter 3 <
2.1 /
mg/L
< 0.151896 /
lbs/day
2023
2nd 6 Months (Avg) <
2.1 /
mg/L
< 0.151896 /
Ibs/day
2023
2nd 6 ...(Max)
3 /
mg/L
0.151896 /
Ibs/day
2023
2nd 6 ...(Min) <
1.3 /
mg/L
< /
2023
2nd 6 ...(Count)
2 /
1 /
Sample Date
SamplelD
Result /Limit
Mass /Limit
VOC
07/28/2023
P TriPharm072823POT
0.156 /
mg/L
/
W
09/14/2023
S TriPharm091423Self
0.13 /
mg/L
/
Jul 2023
Week 4
0.156 /
mg/L
/
Sep 2023
Week 2
0.13 /
mg/L
/
Jul 2023
Average
0.156 /
mg/L
/
Sep 2023
Average
0.13 /
mg/L
/
2023
Quarter 3
0.143 /
mg/L
/
2023
2nd 6 Months (Avg)
0.143 /
mg/L
/
2023
2nd 6 ...(Max)
0.156 /
mg/L
/
2023
2nd 6 ...(Min)
0.13 /
mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
Zinc
07/28/2023
P TriPhartn072823POT
W
09/14/2023
S TriPharm091423Self
Jul 2023
Week 4
Sep 2023
Week 2
Jul 2023
Average
Sep 2023
Average
2023
Quarter 3
2023
2nd 6 Months (Avg)
2023
2nd 6 ...(Max)
2023
2nd 6 ...(Min)
2023
2nd 6 ...(Count)
0.553
/ mg/L
0.397
/ mg/L
0.553
/ mg/L
0.397
/ mg/L
0.553
/ mg/L
0.397
/ mg/L
0.475
/ mg/L
0.475
/ mg/L
0.553
/ mg/L
0.397
/ mg/L
2
/
0.028 /
lbs/day
0.028 /
lbs/day
0.028 /
Ibs/day
0.028 /
Ibs/day
0.028000 /
Ibs/day
0.028000 /
Ibs/day
Saturday, February 24, 2024 9:20:33PM * Indicates Violation ** Indicates TRC Violation Page 10 of 10

United Therapeutics Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
07/07/2023
S UT070723Setf
<
0.025
/
mg/L
<
0.0094 /
lbs/day
Jul 2023
Week 1
<
0.025
/
mg/L
<
0.0094 /
lbs/day
Jul 2023
Average
<
0.025
/
mg/L
<
0.0094 /
lbs/day
2023
Quarter 3
<
0.025
/
mg/L
<
0.0094 /
Ibs/day
2023
2nd 6 Months (Avg)
<
0.025
/
mg/L
<
0.0094 /
Ibs/day
2023
2nd 6 ...(Max)
<
0.025
/
mg/L
<
0.0094 /
Ibs/day
2023
2nd 6 ...(Min)
<
0.025
/
mg/L
<
0.0094 /
Ibs/day
2023
2nd 6 ...(Count)
1
/
1 /
Sample Date
SamplelD
Result/Limit
Mass /Limit
Ammonia
07/07/2023
S UT070723Self
1.8
/
mg/L
0.677 /
Ibs/day
09/26/2023
P UT092623POTW
2.6
/
mg/L
/
Jul 2023
Week 1
1.8
/
mg/L
0.677 /
lbs/day
Sep 2023
Week 4
2.6
/
mg/L
/
Jul 2023
Average
1.8
/
mg/L
0.677 /
lbs/day
Sep 2023
Average
2.6
/
mg/L
/
2023
Quarter 3
2.2
/
mg/L
0.677 /
Ibs/day
2023
2nd 6 Months (Avg)
2.2
/
mg/L
0.6770 /
Ibs/day
2023
2nd 6 ...(Max)
2.6
/
mg/L
0.6770 /
Ibs/day
2023
2nd 6 ...(Min)
1.8
/
mg/L
/
2023
2nd 6 ...(Count)
2
/
1 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2023
S
UT0723F1ow
0.041
/
MGD /
08/31/2023
S
UT0823F1ow
0.039
/
MGD /
09/30/2023
S
UT0923FIow
0.032
/
MGD /
10/31/2023
S
UT1023F1ow
0.032
/
MGD /
11/30/2023
S
UT1123F1ow
0.023
/
MGD /
12/31/2023
S
UT1223F1ow
0.024
/
MGD /
Jul 2023
Week 4
0.041
/
MGD /
Aug 2023
Week 4
0.039
/
MGD /
Sep 2023
Week 4
0.032
/
MGD /
Oct 2023
Week 4
0.032
/
MGD /
Nov 2023
Week 4
0.023
/
MGD /
Dec 2023
Week 4
0.024
/
MGD /
Jul 2023
Average
0.041
/ 0.060
MGD /
Aug 2023
Average
0.039
/ 0.060
MGD /
Sep 2023
Average
0.032
/ 0.060
MGD /
Oct 2023
Average
0.032
/ 0.060
MGD /
Nov 2023
Average
0.023
/ 0.060
MGD /
Sunday, February 25, 2024 5:57:14PM * Indicates Violation ** Indicates TRC Violation Page 1 of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outtall: 001
SampleDate SamplelD Result/Limit Mass/Limit
Average Flow for Month
Dec 2023
Average
0.024
/ 0.060
MGD
/
2023
Quarter 3
0.037333
/
MGD
/
2023
Quarter 4
0.026333
/
MGD
/
2023
2nd 6 Months (Avg) 0.031833
/
MGD
/
2023
2nd 6 ...(Max)
0.041
/
MGD
/
2023
2nd 6 ...(Min)
0.023
/
MGD
/
2023
2nd 6 ...(Count)
6
Sample
Count: 6
Months Sampled
:
6
Weeks Sampled:
6
Quarters Sampled :
2
# I%
#
%
#
%
#
%
# Over Daily C :
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0,00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
BOD
07/07/2023
S UT070723Self
141
/ mg/L
53.028
/ Ibs/day
09/26/2023
P UT092623POTW
112
/ mg/L
/
Jul 2023
Week 1
141
/ mg/L
53.028
/ Ibs/day
Sep 2023
Week 4
112
/ mg/L
/
Jul 2023
Average
141
/ mg/L
53.028
/ lbs/day
Sep 2023
Average
112
/ mg/L
/
2023
Quarter 3
126.5
/ mg/L
53.028
/ lbs/day
2023
2nd 6 Months (Avg)
126.5
/ mg/L
53.028
/ lbs/day
2023
2nd 6 ...(Max)
141
/ mg/L
53.028
/ Ibs/day
2023
2nd 6 ...(Min)
112
/ mg/L
/
2023
2nd 6 ...(Count)
2
/
1
/
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
07/07/2023
S UT070723Setf
09/26/2023
P UT092623POTW
Jul 2023
Week 1
Sep 2023
Week 4
Jul 2023
Average
Sep 2023
Average
2023
Quarter
2023
2nd 6 Months (Avg)
2023
2nd 6 ...(Max)
25
/ mg/L
9.4021
/ Ibs/day
28.6
/ mg/L
/
25
/ mg/L
9.4021
/ lbs/day
28.6
/ mg/L
/
25
/ mg/L
9.4021
/ lbs/day
28.6
/ mg/L
/
26.8
/ mg/L
9.4021
/ Ibs/day
26.8
/ mg/L
9.4021
/ Ibs/day
28.6
/ mg/L
9.4021
/ Ibs/day
Sunday, February 25, 2024 5:57:14PM * Indicates Violation ** Indicates TRC Violation Page 2 of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
Chloride
2023
2nd 6 ...(Min)
25 / mg/L
/
2023
2nd 6 ...(Count)
2 /
1 /
Sample Date
SamplelD
Result/Limit
Mass /Limit
COD
07/07/2023
S UT070723Self
234
/ mg/L
88 /
lbs/day
09/26/2023
P UT092623POTW
267
/ mg/L
/
Jul 2023
Week 1
234
/ mg/L
88 /
lbs/day
Sep 2023
Week 4
267
/ mg/L
/
Jul 2023
Average
234
/ mg/L
88 /
Ibs/day
Sep 2023
Average
267
/ mg/L
/
2023
Quarter 3
250.5
/ mg/L
88 /
Ibs/day
2023
2nd 6 Months (Avg)
250.5
/ mg/L
88.00 /
lbs/day
2023
2nd 6 ...(Max)
267
/ mg/L
88.00 /
lbs/day
2023
2nd 6 ...(Min)
234
/ mg/L
/
2023
2nd 6 ...(Count)
2
/
1 /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
09/26/2023
P UT092623POTW
0.018
/
mg/L
/
Sep 2023
Week 4
0.018
/
mg/L
/
Sep 2023
Average
0.018
/
mg/L
/
2023
Quarter 3
0.018
/
mg/L
/
2023
2nd 6 Months (Avg)
0.018
/
mg/L
/
2023
2nd 6 ...(Max)
0.018
/
mg/L
/
2023
2nd 6 ...(Min)
0.018
/
mg/L
/
2023
2nd 6 ...(Count)
1
Sample Date
SamplelD
Result/Limit
Mass/Limit
Ethyl acetate
07/07/2023
S UT070723Self
<
0.005
/
mg/L
<
0.0019 /
lbs/day
Jul 2023
Week 1
<
0.005
/
mg/L
<
0.0019 /
Ibs/day
Jul 2023
Average
<
0.005
/
mg/L
<
0.0019 /
Ibs/day
2023
Quarter 3
<
0.005
/
mg/L
<
0.0019 /
Ibs/day
2023
2nd 6 Months (Avg)
<
0.005
/
mg/L
<
0.0019 /
Ibs/day
2023
2nd 6 ...(Max)
<
0.005
/
mg/L
<
0.0019 /
lbs/day
2023
2nd 6 ...(Min)
<
0.005
/
mg/L
<
0.0019 /
lbs/day
2023
2nd 6 ...(Count)
1
/
I /
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
Sunday, February 25, 2024 5:57:14PM
* Indicates Violation ** Indicates TRC Violation
Page 3 of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
07/07/2023 S
UT070723Setf
<
0.005
/
mg/L
<
0.0019 /
lbs/day
Jul 2023
Week 1
<
0.005
/
mg/L
<
0.0019 /
lbs/day
Jul 2023
Average
<
0.005
/
mg/L
<
0.0019 /
lbs/day
2023
Quarter 3
<
0.005
/
mg/L
<
0.0019 /
Ibs/day
2023
2nd 6 Months (Avg)
<
0.005
/
mg/L
<
0.0019 /
Ibs/day
2023
2nd 6 ...(Max)
<
0.005
/
mg/L
<
0.0019 /
Ibs/day
2023
2nd 6 ...(Min)
<
0.005
/
mg/L
<
0.0019 /
Ibs/day
2023
2nd 6 ...(Count)
1
/
1 /
Sample Date
SamplelD
Result/Limit
Mass /Limit
Mercury - LL
07/10/2023 S
UT071023SelfHg 0.000018
/ 0.000142
mg/L
/
09/26/2023 P
UT092623POTWHg 0.000021
/ 0.000142
mg/L
/
Jul 2023
Week 2 0.000018
/
mg/L
/
Sep 2023
Week 4 0.000021
/
mg/L
/
Jul 2023
Average 0.000018
/
mg/L
/
Sep 2023
Average 0.000021
/
mg/L
/
2023
Quarter 3 0.00002
/
mg/L
/
2023
2nd 6 Months (Avg) 0.000020
/
mg/L
/
2023
2nd 6 ...(Max) 0.000021
/
mg/L
/
2023
2nd 6 ...(Min) 0.000018
/
mg/L
/
2023
2nd 6 ...(Count) 2
Sample Count : 2 Months Sampled
:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
07/07/2023 S
UT070723Setf
<
0.005
/ mg/L
<
0.00188 /
Ibs/day
Jul 2023
Week 1
<
0.005
/ mg/L
<
0.00188 /
lbs/day
Jul 2023
Average
<
0.005
/ mg/L
<
0.00188 /
lbs/day
2023
Quarter 3
<
0.005
/ mg/L
<
0.00188 /
lbs/day
2023
2nd 6 Months (Avg)
<
0.005
/ mg/L
<
0.001880 /
Ibs/day
2023
2nd 6 ...(Max)
<
0.005
/ mg/L
<
0.001880 /
Ibs/day
2023
2nd 6 ...(Min)
<
0.005
/ mg/L
<
0.001880 /
Ibs/day
2023
2nd 6 ...(Count)
1
/
1 /
Sunday, February 25, 2024 5:57:14PM * Indicates Violation ** Indicates TRC Violation Page 4 of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
07/07/2023 S
UT070723Setf
<
0.005
/
mg/L
<
0.0019 /
lbs/day
Jul 2023
Week 1
<
0.005
/
mg/L
<
0.0019 /
lbs/day
Jul 2023
Average
<
0.005
/
mg/L
<
0.0019 /
lbs/day
2023
Quarter 3
<
0.005
/
mg/L
<
0.0019 /
Ibs/day
2023
2nd 6 Months (Avg)
<
0.005
/
mg/L
<
0.0019 /
Ibs/day
2023
2nd 6 ...(Max)
<
0.005
/
mg/L
<
0.0019 /
Ibs/day
2023
2nd 6 ...(Min)
<
0.005
/
mg/L
<
0.0019 /
Ibs/day
2023
2nd 6 ...(Count)
1
/
1 /
Sample Date
SampleID
Result/Limit
Mass/Limit
Nitrate -Nitrite
07/07/2023 S
UT070723Self
0.3
/
mg/L
0.117 /
Ibs/day
09/26/2023 P
UT092623POTW
0.3
/
mg/L
/
Jul 2023
Week 1
0.3
/
mg/L
0.117 /
lbs/day
Sep 2023
Week 4
0.3
/
mg/L
/
Jul 2023
Average
0.3
/
mg/L
0.117 /
lbs/day
Sep 2023
Average
0.3
/
mg/L
/
2023
Quarter 3
0.3
/
mg/L
0.117 /
Ibs/day
2023
2nd 6 Months (Avg)
0.3
/
mg/L
0.117 /
Ibs/day
2023
2nd 6 ...(Max)
0.3
/
mg/L
0.117 /
Ibs/day
2023
2nd 6 ...(Min)
0.3
/
mg/L
/
2023
2nd 6 ...(Count)
2
/
1 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen, Total
07/07/2023 S
UT070723Self
12
/ mg/L
4.513 /
lbs/day
09/26/2023 P
UT092623POTW
12.2
/ mg/L
/
Jul 2023
Week 1
12
/ mg/L
4.513 /
Ibs/day
Sep 2023
Week 4
12.2
/ mg/L
/
Jul 2023
Average
12
/ mg/L
4.513 /
Ibs/day
Sep 2023
Average
12.2
/ mg/L
/
2023
Quarter 3
12.1
/ mg/L
4.513 /
Ibs/day
2023
2nd 6 Months (Avg)
12.1
/ mg/L
4.513 /
lbs/day
2023
2nd 6 ...(Max)
12.2
/ mg/L
4.513 /
lbs/day
2023
2nd 6 ...(Min)
12
/ mg/L
/
2023
2nd 6 ...(Count)
2
/
1 /
Sample Date SampleID Result/Limit Mass/Limit
Oil & Grease, Total
07/07/2023 S UT070723Self <
09/26/2023 P UT092623POTW <
Sunday, February 25, 2024 5:57:14PM
2.5 / 200 mg/L < /
2.5 / 200 mg/L < /
* Indicates Violation ** Indicates TRC Violation
Page 5 of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Lunit
Oil & Grease, Total
Jul 2023
Week 1
<
2.5
/ mg/L
< /
Sep 2023
Week 4
<
2.5
/ mg/L
< /
Jul 2023
Average
<
2.5
/ mg/L
< /
Sep 2023
Average
<
2.5
/ mg/L
< /
2023
Quarter 3
<
2.5
/ mg/L
< /
2023
2nd 6 Months (Avg)
<
2.5
/ mg/L
< /
2023
2nd 6 ...(Max)
<
2.5
/ mg/L
< /
2023
2nd 6 ...(Min)
<
2.5
/ mg/L
< /
2023
2nd 6 ...(Count)
2
/
/
Sample Count:
2
Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
I
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SampleID Result/Limit Mass /Limit
pH
07/07/2023
S UT070723Self
7.9
/ 5.5 - 10.0
SU /
09/26/2023
P UT092623POTW
7.8
/ 5.5 - 10.0
SU /
Jul 2023
Week 1
7.9
/
SU /
Sep 2023
Week 4
7.8
/
SU /
Jul 2023
Average
7.9
/
SU /
Sep 2023
Average
7.8
/
SU /
2023
Quarter 3
7.85
/
SU /
2023
2nd 6 Months (Avg)
7.85
/
SU /
2023
2nd 6 ...(Max)
7.9
/
SU /
2023
2nd 6 ...(Min)
7.8
/
SU /
2023
2nd 6 ...(Count)
2
Sample Count:
2
Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sunday, February 25, 2024 5:57:14PM * Indicates Violation ** Indicates TRC Violation Page 6 of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
SarnpleDate SamplelD Result/Limit Mass/Limit
Temperature
07/07/2023 S
UT070723Setf
28
/ 66
°C
/
09/26/2023 P
UT092623POTW
22
/ 66
°C
/
Ju12023
Week 1
28
/
°C
/
Sep 2023
Week 4
22
/
°C
/
Ju12023
Average
28
/
°C
/
Sep 2023
Average
22
/
°C
/
2023
Quarter 3
25
/
°C
/
2023
2nd 6 Months (Avg)
25
/
°C
/
2023
2nd 6 ...(Max)
28
/
°C
/
2023
2nd 6 ...(Min)
22
/
°C
/
2023
2nd 6 ...(Count)
2
Sample Count: 2
Months Sampled
:
2
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
07/07/2023
S UT070723Sclf
11.7
/ mg/L
4.4 /
lbs/day
09/26/2023
P UT092623POTW
11.9
/ mg/L
/
Jul 2023
Week 1
11.7
/ mg/L
4.4 /
lbs/day
Sep 2023
Week 4
11.9
/ mg/L
/
Jul 2023
Average
11.7
/ mg/L
4.4 /
lbs/day
Sep 2023
Average
11.9
/ mg/L
/
2023
Quarter 3
11.8
/ mg/L
4.4 /
lbs/day
2023
2nd 6 Months (Avg)
11.8
/ mg/L
4.400 /
lbs/day
2023
2nd 6 ...(Max)
11.9
/ mg/L
4.400 /
lbs/day
2023
2nd 6 ...(Min)
11.7
/ mg/L
/
2023
2nd 6 ...(Count)
2
/
I /
Sample Date
SamplelD
Result/Limit
Mass/Limit
Total Phosphorus
07/07/2023 S
UT070723Self
1.41 /
mg/L
0.5303 / lbs/day
09/26/2023 P
UT092623POTW
1.41 /
mg/L
/
Jul 2023
Week 1
1.41 /
mg/L
0.5303 / lbs/day
Sep 2023
Week 4
1.41 /
mg/L
/
Jul 2023
Average
1.41 /
mg/L
0.5303 / Ibs/day
Sunday, February 25, 2024 5:57:14PM * Indicates Violation ** Indicates TRC Violation Page 7 of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date
SamplelD
Result/Limit
Mass/Limit
Total Phosphorus
Sep 2023
Average
1.41 J
mg/L
/
2023
Quarter 3
1.41 /
mg/L
0.5303 /
lbs/day
2023
2nd 6 Months (Avg)
1.41 /
mg/L
0.5303 /
lbs/day
2023
2nd 6 ...(Max)
1.41 /
mg/L
0.5303 /
lbs/day
2023
2nd 6 ...(Min)
1.41 /
mg/L
/
2023
2nd 6 ...(Count)
2 /
1 /
Sample Date
SamplelD
Result/Limit
Mass /Limit
TSS
07/07/2023 S
UT070723Self
70 /
mg/L
26.325877 /
Ibs/day
09/26/2023 P
UT092623POTW
74 /
mg/L
/
Jul 2023
Week 1
70 /
mg/L
26.325877 /
Ibs/day
Sep 2023
Week 4
74 /
mg/L
/
Jul 2023
Average
70 /
mg/L
26.325877 /
lbs/day
Sep 2023
Average
74 /
mg/L
/
2023
Quarter 3
72 /
mg/L
26.325877 /
lbs/day
2023
2nd 6 Months (Avg)
72 /
mg/L
26.3259 /
Ibs/day
2023
2nd 6 ...(Max)
74 /
mg/L
26.325877 /
Ibs/day
2023
2nd 6 ...(Min)
70 /
mg/L
/
2023
2nd 6 ...(Count)
2 /
1 /
71112023
To 1213112023
Sample Type: Effluent Wastewater
Outfall: 002
Sample Date
SamplelD
Result/Limit
Mass /Limit
Acetone
07/11/2023 S
UTP2071123Self
0.104
/ 20.7
mg/L
/
Jul 2023
Week 2
0.104
/
mg/L
/
Jul 2023
Average
0.104
/ 8.2
mg/L
/
2023
Quarter 3
0.104
/
mg/L
/
2023
2nd 6 Months (Avg)
0.104
/
mg/L
/
2023
2nd 6 ...(Max)
0.104
/
mg/L
/
2023
2nd 6 ...(Min)
0.104
/
mg/L
/
2023
2nd 6 ...(Count)
1
Sample Count: 1
Months Sampled:
1
Weeks Sampled:
1
Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC:
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sunday, February 25, 2024 5:57:14PM * Indicates Violation ** Indicates TRC Violation Page 8 of 8

United Therapeutics Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 002
SarnpleDate SamplelD Result/Limit Mass/Limit
Ethyl acetate
07/11/2023 S
UTP2071123Self <
0.005
/ 20.7
mg/L
<
/
Jul 2023
Week 2
<
0.005
/
mg/L
<
/
Jul 2023
Average
<
0.005
/ 8.2
mg/L
<
/
2023
Quarter 3
<
0.005
/
mg/L
<
/
2023
2nd 6 Months (Avg) <
0.005
/
mg/L
<
/
2023
2nd 6 ...(Max)
<
0.005
/
mg/L
<
/
2023
2nd 6 ...(Min)
<
0.005
/
mg/L
<
/
2023
2nd 6 •..(Count)
1
Sample Count: 1
Months Sampled:
1
Weeks Sampled:
1
Quarters Sampled :
I
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass /Limit
Isopropyl acetate
07/11/2023 S
UTP2071123Self <
0.005
/ 20.7
mg/L
<
/
Jul 2023
Week 2
<
0.005
/
mg/L
<
/
Jul 2023
Average
<
0.005
/ 8.2
mg/L
<
/
2023
Quarter 3
<
0.005
/
mg/L
<
/
2023
2nd 6 Months (Avg) <
0.005
/
mg/L
<
/
2023
2nd 6 ...(Max)
<
0.005
/
mg/L
<
/
2023
2nd 6 ...(Min)
<
0.005
/
mg/L
<
/
2023
2nd 6 ...(Count)
1
Sample Count: I
Months Sampled:
1
Weeks Sampled:
1
Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
07/11/2023 S UTP2071123Self < 0.005 / 3.0 mg/L < /
Jul 2023 Week 2 < 0.005 / mg/L < /
Jul 2023 Average < 0.005 / 0.7 mg/L < /
Sunday, February 25, 2024 5:57:14PM * Indicates Violation ** Indicates TRC Violation Page 1 of 2

United Therapeutics Corporation
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 002
SampleDate SamplelD Result/Limit Mass/Limit
Methylene Chloride
2023
Quarter 3
<
0.005
/
mg/L <
/
2023
2nd 6 Months (Avg) <
0.005
/
mg/L <
/
2023
2nd 6 ...(Max)
<
0.005
/
mg/L <
/
2023
2nd 6 ...(Min)
<
0.005
/
mg/L <
/
2023
2nd 6 ...(Count)
1
Sample Count:
1
Months Sampled:
1
Weeks Sampled :
1
Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
07/11/2023 S
UTP2071123Self <
0.005
/ 20.7
mg/L
<
/
Jul 2023
Week 2
<
0.005
/
mg/L
<
/
Jul 2023
Average
<
0.005
/ 8.2
mg/L
<
/
2023
Quarter 3
<
0.005
/
mg/L
<
/
2023
2nd 6 Months (Avg) <
0.005
/
mg/L
<
/
2023
2nd 6 ...(Max)
<
0.005
/
mg/L
<
/
2023
2nd 6 ...(Min)
<
0.005
/
mg/L
<
/
2023
2nd 6 ...(Count)
1
Sample Count : 1
Months Sampled
:
1
Weeks Sampled:
1
Quarters Sampled:
1
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sunday, February 25, 2024 5:57:14PM * Indicates Violation ** Indicates TRC Violation Page 2 of 2

Wolfspeed 40 Moore
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2023
S
Wolfspeed40MoorePl
0.001842
/
MGD /
0723F1ow
08/31/2023
S
Wolfspeed40MoorePl
0.021341
/
MGD /
0823F1ow
09/30/2023
S
Wolfspeed40MoorePl
0.023054
/
MGD /
0923F1ow
10/31/2023
S
Wolfspeed40MooreP11
0.039844
/
MGD /
023F1ow
11/30/2023
S
Wolfspeed40MooreP11
0.051797
/
MGD /
123F1ow
Jul 2023
Week 4
0.001842
/
MGD /
Aug 2023
Week 4
0.021341
/
MGD /
Sep 2023
Week 4
0.023054
/
MGD /
Oct 2023
Week 4
0.039844
/
MGD /
Nov 2023
Week 4
0.051797
/
MGD /
Jul 2023
Average
0.001842
/ 0.056500
MGD /
Aug 2023
Average
0.021341
/ 0.056500
MGD /
Sep 2023
Average
0.023054
/ 0.056500
MGD /
Oct 2023
Average
0.039844
/ 0.056500
MGD /
Nov 2023
Average
0.051797
/ 0.056500
MGD /
2023
Quarter 3
0.015412
/
MGD /
2023
Quarter 4
0.045821
/
MGD /
2023
2nd 6 Months (Avg)
0.027576
/
MGD /
2023
2nd 6 ...(Max)
0.051797
/
MGD /
2023
2nd 6 ...(Min)
0.001842
/
MGD /
2023
2nd 6 ...(Count)
5
Sample Count:
5
Months Sampled:
5
Weeks Sampled:
5
Quarters Sampled :
2
# Over Daily C:
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury - LL
08/16/2023
11/27/2023
Aug 2023
Nov 2023
Aug 2023
Nov 2023
S Wolfspeed40MoorePl <
0.000001 / 0.000142
m9/1, < /
081623Self
P Wolfspeed40MooreP11
0.000002 / 0.000142
mg/L /
12723POTWHg
Week 3 <
0.000001 /
mg/L < /
Week 4
0.000002 /
mg/L /
Average <
0.000001 /
mg/L < /
Average
0.000002 /
mg/L /
Saturday, February 24, 2024 10:39:53PM * Indicates Violation ** Indicates TRC Violation Page 1 of 3

Wolfspeed 40 Moore
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Mercury - LL
2023
Quarter 3
< 0.000001
/
mg/L <
/
2023
Quarter 4
0.000002
/
mg/L
/
2023
2nd 6 Months (Avg) < 0.000001
/
mg/L <
/
2023
2nd 6 ...(Max)
0.000002
/
mg/L
/
2023
2nd 6 ...(Min)
< 0.000001
/
mg/L <
/
2023
2nd 6 ...(Count)
2
Sample Count: 2
Months Sampled
:
2
Weeks Sampled:
2
Quarters Sampled :
2
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC:
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
pH
08/16/2023 S
Wolfspeed40MoorePl
6.8
/ 6.0 - 10.0
SU
/
081623Self
11/27/2023 P
Wolfspeed40MoorePl l
7
/ 6.0 - 10.0
SU
/
12723POTW
Aug 2023
Week 3
6.8
/
SU
/
Nov 2023
Week 4
7
/
SU
/
Aug 2023
Average
6.8
/
SU
/
Nov 2023
Average
7
/
SU
/
2023
Quarter 3
6.8
/
SU
/
2023
Quarter
7
/
SU
/
2023
2nd 6 Months (Avg)
6.9
/
SU
/
2023
2nd 6 ...(Max)
7
/
SU
/
2023
2nd 6 ...(Min)
6.8
/
SU
/
2023
2nd 6 ...(Count)
2
Sample Count: 2 Months Sampled:
2
Weeks Sampled :
2
Quarters Sampled :
2
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M:
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
Saturday, February 24, 2024 10:39:53PM * Indicates Violation ** Indicates TRC Violation Page 2 of 3

Wolfspeed 40 Moore
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
08/16/2023 S
Wolfspeed40MoorePl
23
/ 66
°C
/
081623Self
11/27/2023 P
Wolfspeed40MooreP11
18
/ 66
°C
/
12723POTW
Aug 2023
Week 3
23
/
°C
/
Nov 2023
Week 4
18
/
°C
/
Aug 2023
Average
23
/
°C
/
Nov 2023
Average
18
/
°C
/
2023
Quarter
23
/
°C
/
2023
Quarter 4
18
/
°C
/
2023
2nd 6 Months (Avg)
20.5
/
°C
/
2023
2nd 6 ...(Max)
23
/
°C
/
2023
2nd 6 ...(Min)
18
/
°C
/
2023
2nd 6 ...(Count)
2
Sample Count : 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
2
# Over Daily C:
0 0.00 # Over Mo Avg C:
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC
:
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Muss/Limit
TTO
08/16/2023 S
Wolfspeed40MoorePl
0.003
/ 1.37
mg/L
081623Self
Aug 2023
Week 3
0.003
/
mg/L
Aug 2023
Average
0.003
/
mg/L
2023
Quarter 3
0.003
/
mg/L
2023
2nd 6 Months (Avg)
0.003
/
mg/L
2023
2nd 6 ...(Max)
0.003
/
mg/L
2023
2nd 6 ...(Min)
0.003
/
mg/L
2023
2nd 6 ...(Count)
l
/
Sample Count: 1 Months Sampled
:
1
Weeks Sampled:
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC : 0
# Under Daily:
0 0.00
# Under Daily TRC:
0 0.00
1
Quarters Sampled :
I
#
%
0.00
# Over Qt Avg C : 0
0.00
0.00
# Over Qt Avg C TRC : 0
0.00
0.00
# Over Qtr Avg M : 0
0.00
0.00
# Over Qtr Avg M TRC : 0
0.00
Saturday, February 24, 2024 10:39:53PM * Indicates Violation ** Indicates TRC Violation Page 3 of 3

Wolfspeed 40 Moore
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 002
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
12/31/2023 S Wolfspeed40MooreP2
0.134555
/
MGD /
1223F1ow
Dec 2023 Week 4
0.134555
/
MGD /
Dec 2023 Average
0.134555
/ 0.297500
MGD /
2023 Quarter 4
0.134555
/
MGD /
2023 2nd 6 Months (Avg)
0.134555
/
MGD /
2023 2nd 6 ...(Max)
0.134555
/
MGD /
2023 2nd 6 ...(Min)
0.134555
/
MGD /
2023 2nd 6 ...(Count)
1
Sample Count:
l
Months Sampled :
1
Weeks Sampled:
1
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Saturday, February 24, 2024 10:39:53PM * Indicates Violation ** Indicates TRC Violation Page 1 of 1

Wolfspeed Durham
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
08/16/2023
S WolfspeedP8081623Se
16.4
/ mg/L
/
if
10/27/2023
P WolfspeedP8102723P
15.2
/ mg/L
/
OTW
Aug 2023
Week 3
16.4
/ mg/L
/
Oct 2023
Week 4
15.2
/ mg/L
/
Aug 2023
Average
16.4
/ mg/L
/
Oct 2023
Average
15.2
/ mg/L
/
2023
Quarter 3
16.4
/ mg/L
/
2023
Quarter 4
15.2
/ mg/L
/
2023
2nd 6 Months (Avg)
15.8
/ mg/L
/
2023
2nd 6 ...(Max)
16.4
/ mg/L
/
2023
2nd 6 ...(Min)
15.2
/ mg/L
/
2023
2nd 6 ...(Count)
2
/
/
Sample Date SamplelD Result/Limit Mass /Limit
Average Flow for Month
07/31/2023
S
WolfspeedP80723F1ow
0.53729
/ MGD /
08/31/2023
S
WolfspeedP80823171ow
0.510761
/ MGD /
09/30/2023
S
WolfspeedP80923F1ow
0.5296
/ MGD /
10/31/2023
S
WolfspeedP81023F1ow
0.496955
/ MGD /
11/30/2023
S
WolfspeedP81123171ow
0.494867
/ MGD /
12/31/2023
S
WolfspeedP81223F1ow
0.505714
/ MGD /
Jul 2023
Week 4
0.53729
/ MGD /
Aug 2023
Week 4
0.510761
/ MGD /
Sep 2023
Week 4
0.5296
/ MGD /
Oct 2023
Week 4
0.496955
/ MGD /
Nov 2023
Week 4
0.494867
/ MGD /
Dec 2023
Week 4
0.505714
/ MGD /
Jul 2023
Average
0.53729
/ MGD /
Aug 2023
Average
0.510761
/ MGD /
Sep 2023
Average
0.5296
/ MGD /
Oct 2023
Average
0.496955
/ MGD /
Nov 2023
Average
0.494867
/ MGD /
Dec 2023
Average
0.505714
/ MGD /
2023
Quarter 3
0.525884
/ MGD /
2023
Quarter 4
0.499179
/ MGD /
2023
2nd 6 Months (Avg)
0.512531
/ MGD /
2023
2nd 6 ...(Max)
0.53729
/ MGD /
2023
2nd 6 ...(Min)
0.494867
/ MGD /
2023
2nd 6 ...(Count)
6
Saturday, February 24, 2024 9:50:17PM * Indicates Violation ** Indicates TRC Violation Page 1 of 6

Wolfspeed Durham
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 008
Sample Date
SamplelD
Result/Limit
Mass/Limit
Barium
08/16/2023
S WolfspeedP8081623Se
0.051 /
mg/L
/
if
Aug 2023
Week 3
0.051 /
mg/L
/
Aug 2023
Average
0.051 /
mg/L
/
2023
Quarter 3
0.051 /
mg/L
/
2023
2nd 6 Months (Avg)
0.051 /
mg/L
/
2023
2nd 6 ...(Max)
0.051 /
mg/L
/
2023
2nd 6 ...(Min)
0.051 /
mg/L
/
2023
2nd 6 ...(Count)
1
Sample Date
SamplelD
Result/Limit
Mass /Limit
Chloride
08/16/2023
S WolfspeedP8081623Se
90 /
mg/L
/
if
10/27/2023
P WolfspeedP8102723P
19l /
mg/L
/
OTW
Aug 2023
Week 3
90 /
mg/L
/
Oct 2023
Week 4
191 /
mg/L
/
Aug 2023
Average
90 /
mg/L
/
Oct 2023
Average
191 /
mg/L
/
2023
Quarter 3
90 /
mg/L
/
2023
Quarter 4
191 /
mg/L
/
2023
2nd 6 Months (Avg)
140.5 /
mg/L
/
2023
2nd 6 ...(Max)
191 /
mg/L
/
2023
2nd 6 ...(Min)
90 /
mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
Cyanide
08/16/2023
S WolfspeedP8081623Se
<
0.003
/
mg/L
<
/
if
10/27/2023
P WolfspeedP8102723P
<
0.003
/
mg/L
<
/
OTW
Aug 2023
Week 3
<
0.003
/
mg/L
<
/
Oct 2023
Week 4
<
0.003
/
mg/L
<
/
Aug 2023
Average
<
0.003
/
mg/L
<
/
Oct 2023
Average
<
0.003
/
mg/L
<
/
2023
Quarter 3
<
0.003
/
mg/L
<
/
2023
Quarter 4
<
0.003
/
mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.003
/
mg/L
<
/
2023
2nd 6 ...(Max)
<
0.003
/
mg/L
<
/
2023
2nd 6 ...(Min)
<
0.003
/
mg/L
<
/
2023
2nd 6 ...(Count)
2
Saturday, February 24, 2024 9:50:17PM
* Indicates Violation
** Indicates TRC Violation
Page 2 of 6

Wolfspeed Durham
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
08/16/2023
S WolfspeedP8081623Se
1.8
/ mg/L
/
if
10/27/2023
P WolfspeedP8102723P
2.32
/ mg/L
/
OTW
Aug 2023
Week 3
1.8
/ mg/L
/
Oct 2023
Week 4
2.32
/ mg/L
/
Aug 2023
Average
1.8
/ mg/L
/
Oct 2023
Average
2.32
/ mg/L
/
2023
Quarter 3
1.8
/ mg/L
/
2023
Quarter 4
2.32
/ mg/L
/
2023
2nd 6 Months (Avg)
2.06
/ mg/L
/
2023
2nd 6 ...(Max)
2.32
/ mg/L
/
2023
2nd 6 ...(Min)
1.8
/ mg/L
/
2023
2nd 6 ...(Count)
2
/
/
Sample Date SamplelD Result/Limit Mass /Limit
Mercury - LL
08/14/2023 P
WolfspeedP8081423P
0.000002
/ mg/L
/
OTWHg
08/16/2023 S
WolfspeedP8081623Se
0.000002
/ mg/L
/
if
10/26/2023 P
WolfspeedP8102623P
0.000005
/ mg/L
/
OTWHg
Aug 2023
Week 2
0.000002
/ mg/L
/
Aug 2023
Week 3
0.000002
/ mg/L
/
Oct 2023
Week 4
0.000005
/ mg/L
/
Aug 2023
Average
0.000002
/ mg/L
/
Oct 2023
Average
0.000005
/ mg/L
/
2023
Quarter 3
0.000002
/ mg/L
/
2023
Quarter 4
0.000005
/ mg/L
/
2023
2nd 6 Months (Avg)
0.000003
/ mg/L
/
2023
2nd 6 ...(Max)
0.000005
/ mg/L
/
2023
2nd 6 ...(Min)
0.000002
/ mg/L
/
2023
2nd 6 ...(Count)
3
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate -Nitrite
10/27/2023 P
WolfspeedP8102723P
OTW
Oct 2023
Week 4
Oct 2023
Average
2023
Quarter 4
2023
2nd 6 Months (Avg)
2023
2nd 6 ...(Max)
5.3
/ mg/L /
5.3
/ mg/L /
5.3
/ mg/L /
5.3
/ mg/L /
5.3
/ mg/L /
5.3
/ mg/L /
Saturday, February 24, 2024 9:50:17PM * Indicates Violation ** Indicates TRC Violation Page 3 of 6

Wolfspeed Durham
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 008
Sample Date
SamplelD
Result/Limit
Mass/Limit
Nitrate -Nitrite
2023
2nd 6 ...(Min)
5.3 /
mg/L
/
2023
2nd 6 ...(Count)
1
Sample Date
SamplelD
Result/Limit
Mass/Limit
Nitrogen, Total
08/16/2023 S
WolfspeedP8081623Se
27 /
mg/L
/
if
10/27/2023 P
WolfspeedP8102723P
23.1 /
mg/L
/
OTW
Aug 2023
Week 3
27 /
mg/L
/
Oct 2023
Week 4
23.1 /
mg/L
/
Aug 2023
Average
27 /
mg/L
/
Oct 2023
Average
23.1 /
mg/L
/
2023
Quarter 3
27 /
mg/L
/
2023
Quarter 4
23.1 /
mg/L
/
2023
2nd 6 Months (Avg)
25.05 /
mg/L
/
2023
2nd 6 ...(Max)
27 /
mg/L
/
2023
2nd 6 ...(Min)
23.1 /
mg/L
/
2023
2nd 6 ...(Count)
2 /
/
Sample Date
SamplelD
Result/Limit
Mass/Limit
Oil & Grease, Total
10/27/2023 P
WolfspeedP8102723P
<
2.5 /
mg/L
<
/
OTW
Oct 2023
Week 4
<
2.5 /
mg/L
<
/
Oct 2023
Average
<
2.5 /
mg/L
<
/
2023
Quarter 4
<
2.5 /
mg/L
<
/
2023
2nd 6 Months (Avg)
<
2.5 /
mg/L
<
/
2023
2nd 6 ...(Max)
<
2.5 /
mg/L
<
/
2023
2nd 6 ...(Min)
<
2.5 /
mg/L
<
/
2023
2nd 6 ...(Count)
1
Sample Date SamplelD Result/Limit Mass/Limit
pH
08/16/2023
S WolfspeedP8081623Se
if
10/27/2023
P WolfspeedP8102723P
OTW
Aug 2023
Week 3
Oct 2023
Week 4
Aug 2023
Average
Oct 2023
Average
2023
Quarter 3
Saturday, February 24, 2024 9:50:17PM
8.7
/5.0-10.5
SU /
8.7
/5.0-10.5
SU /
8.7
/
SU /
8.7
/
SU /
8.7
/
SU /
8.7
/
SU /
8.7
/
SU /
* Indicates Violation ** Indicates TRC Violation
Page 4 of 6

Wolfspeed Durham
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
PH
2023
Quarter 4
8.7
/
SU
/
2023
2nd 6 Months (Avg)
8.7
/
SU
/
2023
2nd 6 ...(Max)
8.7
/
SU
/
2023
2nd 6 ...(Min)
8.7
/
SU
/
2023
2nd 6 ...(Count)
2
Sample Count: 2
Months Sampled:
2
Weeks Sampled :
2
Quarters Sampled :
2
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
08/16/2023 S
WolfspeedP8081623Se
26
/ 66
°C
/
if
10/27/2023 P
WolfspeedP8102723P
24
/ 66
°C
/
OTW
Aug 2023
Week 3
26
/
°C
/
Oct 2023
Week 4
24
/
°C
/
Aug 2023
Average
26
/
°C
/
Oct 2023
Average
24
/
°C
/
2023
Quarter 3
26
/
°C
/
2023
Quarter 4
24
/
°C
/
2023
2nd 6 Months (Avg)
25
/
°C
/
2023
2nd 6 ...(Max)
26
/
°C
/
2023
2nd 6 ...(Min)
24
/
°C
/
2023
2nd 6 ...(Count)
2
Sample Count: 2 Months Sampled
:
2
Weeks Sampled :
2
Quarters Sampled :
2
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
10/27/2023 P WolfspeedP8102723P 17.8 / mg/L /
OTW
Saturday, February 24, 2024 9:50:17PM * Indicates Violation ** Indicates TRC Violation Page 5 of 6

Wolfspeed Durham
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 008
Sample Date
SamplelD
Result/Limit
Mass/Limit
TKN
Oct 2023
Week 4
17.8 /
mg/L
/
Oct 2023
Average
17.8 /
mg/L
/
2023
Quarter 4
17.8 /
mg/L
/
2023
2nd 6 Months (Avg)
17.8 /
mg/L
/
2023
2nd 6 ...(Max)
17.8 /
mg/L
/
2023
2nd 6 ...(Min)
17.8 /
mg/L
/
2023
2nd 6 ...(Count)
1
Sample Date
SamplelD
Result /Limit
Mass /Limit
Zinc
08/16/2023
S WolfspeedP8081623Se
0.926 /
mg/L
/
if
Aug 2023
Week 3
0.926 /
mg/L
/
Aug 2023
Average
0.926 /
mg/L
/
2023
Quarter 3
0.926 /
mg/L
/
2023
2nd 6 Months (Avg)
0.926 /
mg/L
/
2023
2nd 6 ...(Max)
0.926 /
mg/L
/
2023
2nd 6 ...(Min)
0.926 /
mg/L
/
2023
2nd 6 ...(Count)
1
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 009
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2023
S
WolfspeedP90723F1ow
0.029542 /
MGD /
08/31/2023
S
WolfspeedP90823F1ow
0.039041 /
MGD /
09/30/2023
S
WolfspeedP90923F1ow
0.031059 /
MGD /
10/31/2023
S
WolfspeedP91023F1ow
0.043506 /
MGD /
11/30/2023
S
WolfspeedP91123F1ow
0.050297 /
MGD /
12/31/2023
S
WolfspeedP91223F1ow
0.053281 /
MGD /
Jul 2023
Week 4
0.029542 /
MGD /
Aug 2023
Week 4
0.039041 /
MGD /
Sep 2023
Week 4
0.031059 /
MGD /
Oct 2023
Week 4
0.043506 /
MGD /
Nov 2023
Week 4
0.050297 /
MGD /
Dec 2023
Week 4
0.053281 /
MGD /
Ju12023
Average
0.029542 /
MGD /
Aug 2023
Average
0.039041 /
MGD /
Sep 2023
Average
0.031059 /
MGD /
Oct 2023
Average
0.043506 /
MGD /
Nov 2023
Average
0.050297 /
MGD /
Dec 2023
Average
0.053281 /
MGD /
Saturday, February 24, 2024 9:50:17PM * Indicates Violation ** Indicates TRC Violation Page 6 of 6

Wolfspeed Durham
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 009
Sample Date
SamplelD
Result/Limit
Mass/Limit
Average Flow for Mouth
2023
Quarter 3
0.033214
/
MGD
/
2023
Quarter 4
0.049028
/
MGD
/
2023
2nd 6 Months (Avg)
0.041121
/
MGD
/
2023
2nd 6 ...(Max)
0.053281
/
MGD
/
2023
2nd 6 ...(Min)
0.029542
/
MGD
/
2023
2nd 6 ...(Count)
6
Sample Date
SamplelD
Result/Limit
Mass /Limit
Fluoride
08/16/2023
S
WolfspeedP9081623Se
1.4
/
mg/L
/
if
10/27/2023
P
WolfspeedP9102723P
1.26
/
mg/L
/
OTW
Aug 2023
Week 3
1.4
/
mg/L
/
Oct 2023
Week 4
1.26
/
mg/L
/
Aug 2023
Average
1.4
/
mg/L
/
Oct 2023
Average
1.26
/
mg/L
/
2023
Quarter 3
1.4
/
mg/L
/
2023
Quarter 4
1.26
/
mg/L
/
2023
2nd 6 Months (Avg)
1.33
/
mg/L
/
2023
2nd 6 ...(Max)
1.4
/
mg/L
/
2023
2nd 6 ...(Min)
1.26
/
mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date
SamplelD
Result/Limit
Mass/Limit
Mercury - LL
08/14/2023
P
WolfspeedP9081423P
0.000002
/
mg/L
/
OTWHg
08/16/2023
S
WolfspeedP9081623Se
<
0.000001
/
mg/L
<
/
if
10/26/2023
P
WolfspeedP9102623P
0.000003
/
mg/L
/
OTWHg
Aug 2023
Week 2
0.000002
/
mg/L
/
Aug 2023
Week 3
<
0.000001
/
mg/L
<
/
Oct 2023
Week 4
0.000003
/
mg/L
/
Aug 2023
Average
0.000002
/
mg/L
/
Aug 2023
Average
<
0.000001
/
mg/L
<
/
Aug 2023
Average
<
0.000001
/
mg/L
<
/
Aug 2023
Average
0.000002
/
mg/L
/
Oct 2023
Average
0.000003
/
mg/L
/
2023
Quarter 3
0.000002
/
mg/L
/
2023
Quarter 3
<
0.000001
/
mg/L
<
/
2023
Quarter 3
<
0.000001
/
mg/L
<
/
2023
Quarter 3
0.000002
/
mg/L
/
Saturday, February 24, 2024 9:50:17PM * Indicates Violation ** Indicates TRC Violation Page 1 of 3

Wolfspeed Durham
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 009
Sample Date
SamplelD
Result/Limit
Mass/Limit
Mercury - LL
2023
Quarter 4
0.000003 /
mg/L
/
2023
2nd 6 Months (Avg)
<
0.000002 /
mg/L
<
/
2023
2nd 6 ...(Max)
0.000003 /
mg/L
/
2023
2nd 6 ...(Min)
<
0.000001 /
mg/L
<
/
2023
2nd 6 ...(Count)
3
Sample Date
SampleID
Result/Limit
Mass/Limit
Molybdenum
10/27/2023 P
WolfspeedP9102723P
0.002 /
mg/L
/
OTW
Oct 2023
Week 4
0.002 /
mg/L
/
Oct 2023
Average
0.002 /
mg/L
/
2023
Quarter 4
0.002 /
mg/L
/
2023
2nd 6 Months (Avg)
0.002 /
mg/L
/
2023
2nd 6 ...(Max)
0.002 /
mg/L
/
2023
2nd 6 ...(Min)
0.002 /
mg/L
/
2023
2nd 6 ...(Count)
1 /
/
Sample Date
SamplelD
Result/Limit
Mass/Limit
Oil & Grease, Total
10/27/2023 P
WolfspeedP9102723P
<
2.5 /
mg/L
<
/
OTW
Oct 2023
Week 4
<
2.5 /
mg/L
<
/
Oct 2023
Average
<
2.5 /
mg/L
<
/
2023
Quarter 4
<
2.5 /
mg/L
<
/
2023
2nd 6 Months (Avg)
<
2.5 /
mg/L
<
/
2023
2nd 6 ...(Max)
<
2.5 /
mg/L
<
/
2023
2nd 6 ...(Min)
<
2.5 /
mg/L
<
/
2023
2nd 6 ...(Count)
1
SampleDate
SamplelD
Result/Limit
Mass/Limit
pH
08/16/2023 S
WolfspeedP9081623Se
6.7 / 5.0 - 10.5
SU
/
If
10/27/2023 P
WolfspeedP9102723P
7.8 / 5.0 - 10.5
SU
/
OTW
Aug 2023
Week 3
6.7 /
SU
/
Oct 2023
Week 4
7.8 /
SU
/
Aug 2023
Average
6.7 /
SU
/
Oct 2023
Average
7.8 /
SU
/
2023
Quarter 3
6.7 /
SU
/
2023
Quarter 4
7.8 /
SU
/
2023
2nd 6 Months (Avg)
7.25 /
SU
/
Saturday, February 24, 2024 9:50:17PM * Indicates Violation ** Indicates TRC Violation Page 2 of 3

Wolfspeed Durham
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 009
Sample Date SamplelD Result/Limit Mass/Limit
PH
2023
2nd 6
...(Max)
7.8 /
SU
/
2023
2nd 6
...(Min)
6.7 /
SU
/
2023
2nd 6
...(Count)
2
Sample
Count:
2
Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled:
2
# Over Daily C :
0
0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
08/16/2023
S WolfspeedP9081623Se
28
/ °C
/
if
10/27/2023
P WolfspeedP9102723P
23
/ °C
/
OTW
Aug 2023
Week 3
28
/ °C
/
Oct 2023
Week 4
23
/ °C
/
Aug 2023
Average
28
/ °C
/
Oct 2023
Average
23
/ °C
/
2023
Quarter
28
/ °C
/
2023
Quarter 4
23
/ °C
/
2023
2nd 6 Months (Avg)
25.5
/ °C
/
2023
2nd 6 ...(Max)
28
/ °C
/
2023
2nd 6 ...(Min)
23
/ °C
/
2023
2nd 6 ...(Count)
2
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: All
Sample Date
SamplelD
Result/Limit
Mass/Limit
Average Flow for Month
07/31/2023
S
Wolfspeed0723FIow
0.566832
/
MGD
/
08/31/2023
S
Wolfspeed0823171ow
0.549802
/
MGD
/
09/30/2023
S
Wolfspeed0923FIow
0.560659
/
MGD
/
10/31/2023
S
Wolfspeedl023FIow
0.540461
/
MGD
/
11/30/2023
S
Wolfspeed1123171ow
0.545164
/
MGD
/
12/31/2023
Wolfspeed1223F1ow
0.558995
/
MGD
/
Jul 2023
Week 4
0.566832
/
MGD
/
Aug 2023
Week 4
0.549802
/
MGD
/
Sep 2023
Week 4
0.560659
/
MGD
/
Saturday, February 24, 2024 9:50:17PM * Indicates Violation ** Indicates TRC Violation Page 3 of 3

Wolfspeed Durham
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: All
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
Oct 2023
Week 4
0.540461
/
MGD
/
Nov 2023
Week 4
0.545164
/
MGD
/
Dec 2023
Week 4
0.558995
/
MGD
/
Ju12023
Average
0.566832
/ 0.591
MGD
/
Aug 2023
Average
0.549802
/ 0.591
MGD
/
Sep 2023
Average
0.560659
/ 0.591
MGD
/
Oct 2023
Average
0.540461
/ 0.591
MGD
/
Nov 2023
Average
0.545164
/ 0.591
MGD
/
Dec 2023
Average
0.558995
/ 0.591
MGD
/
2023
Quarter 3
0.559098
/
MGD
/
2023
Quarter 4
0.548207
/
MGD
/
2023
2nd 6 Months (Avg) 0.553652
/
MGD
/
2023
2nd 6 ...(Max)
0.566832
/
MGD
/
2023
2nd 6 ...(Min)
0.540461
/
MGD
/
2023
2nd 6 ...(Count)
6
Sample Count: 6
Months Sampled:
6
Weeks Sampled:
6
Quarters Sampled :
2
# Over Daily C:
0 0.00
# Over Mo Avg C :
0 0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0 0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0 0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC :
0 0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 013
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2023
S
WolfspeedP1307231710
W
08/31/2023
S
WolfspeedP1308231710
W
09/30/2023
S
WolfspeedP1309231710
W
10/31/2023
S
WolfspeedP131023F10
W
11/30/2023
S
WolfspeedP131123FIo
W
12/31/2023
S
WolfspeedP131223F10
W
Jul 2023
Week 4
Aug 2023
Week 4
Sep 2023
Week 4
Oct 2023
Week 4
0.000752
/ MGD /
0.000892
/ MGD /
0.000955
/ MGD /
0.000964
/ MGD /
0.001071
/ MGD /
0.001385
/ MGD /
0.000752
/ MGD /
0.000892
/ MGD /
0.000955
/ MGD /
0.000964
/ MGD /
Saturday, February 24, 2024 9:50:17PM * Indicates Violation ** Indicates TRC Violation Page 1 of 1

Wolfspeed Durham
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 013
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
Nov 2023
Week 4
0.001071
/
MGD
/
Dec 2023
Week 4
0.001385
/
MGD
/
Jul 2023
Average
0.000752
/ 0.030
MGD
/
Aug 2023
Average
0.000892
/ 0.030
MGD
/
Sep 2023
Average
0.000955
/ 0.030
MGD
/
Oct 2023
Average
0.000964
/ 0.030
MGD
/
Nov 2023
Average
0.001071
/ 0.030
MGD
/
Dec 2023
Average
0.001385
/ 0.030
MGD
/
2023
Quarter 3
0.000866
/
MGD
/
2023
Quarter 4
0.00114
/
MGD
/
2023
2nd 6 Months (Avg) 0.001003
/
MGD
/
2023
2nd 6 ...(Max)
0.001385
/
MGD
/
2023
2nd 6 ...(Min)
0.000752
/
MGD
/
2023
2nd 6 ...(Count)
6
Sample Count: 6
Months Sampled:
6
Weeks Sampled:
6
Quarters Sampled :
2
# Over Daily C:
0 0.00
# Over Mo Avg C :
0 0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0 0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0 0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC:
0 0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SampleID
Result/Limit
Mass/Limit
Cadmium
08/16/2023
S WolfspeedP13081623S
<
0.0005
/ 0.11
mg/L
<
/
elf
10/03/2023
P WolfspeedP13100323P
<
0.00008
/ 0.11
mg/L
<
/
OTW
Aug 2023
Week 3
<
0.0005
/
mg/L
<
/
Oct 2023
Week 1
<
0.00008
/
mg/L
<
/
Aug 2023
Average
<
0.0005
/ 0.07
mg/L
<
/
Oct 2023
Average
<
0.00008
/ 0.07
mg/L
<
/
2023
Quarter 3
<
0.0005
/
mg/L
<
/
2023
Quarter 4
<
0.00008
/
mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.00029
/
mg/L
<
/
2023
2nd 6 ...(Max)
<
0.0005
/
mg/L
<
/
2023
2nd 6 ...(Min)
<
0.00008
/
mg/L
<
/
2023
2nd 6 ...(Count)
2
Saturday, February 24, 2024 9:50:17PM * Indicates Violation ** Indicates TRC Violation Page 1 of 6

Wolfspeed Durham
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 013
Sample Count:
2
Months Sampled :
2
Weeks Sampled:
2
Quarters Sampled :
2
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
08/16/2023 S
WolfspeedP13081623S <
0.003
/ 2.77
mg/L
<
/
elf
10/03/2023 P
WolfspeedP13100323P <
0.001
/ 2.77
mg/L
<
/
OTW
Aug 2023
Week 3 <
0.003
/
mg/L
<
/
Oct 2023
Week 1 <
0.001
/
mg/L
<
/
Aug 2023
Average <
0.003
/ 1.71
mg/L
<
/
Oct 2023
Average <
0.001
/ 1.71
mg/L
<
/
2023
Quarter 3 <
0.003
/
mg/L
<
/
2023
Quarter 4 <
0.001
/
mg/L
<
/
2023
2nd 6 Months (Avg) <
0.002
/
mg/L
<
/
2023
2nd 6 ...(Max) <
0.003
/
mg/L
<
/
2023
2nd 6 ...(Min) <
0.001
/
mg/L
<
/
2023
2nd 6 ...(Count)
2
Sample Count: 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
2
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Copper
08/16/2023
S WolfspeedP13081623S
0.002
/ 3.38
mg/L /
elf
10/03/2023
P WolfspeedP13100323P <
0.001
/ 3.38
mg/L < /
OTW
Aug 2023
Week 3
0.002
/
mg/L /
Oct 2023
Week 1 <
0.001
/
mg/L < /
Aug 2023
Average
0.002
/ 2.07
mg/L /
Oct 2023
Average <
0.001
/ 2.07
mg/L < /
2023
Quarter 3
0.002
/
mg/L /
2023
Quarter 4 <
0.001
/
mg/L < /
Saturday, February 24, 2024 9:50:17PM * Indicates Violation ** Indicates TRC Violation Page 2 of 6

Wolfspeed Durham
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 013
Sample Date SamplelD Result/Limit Mass/Limit
Copper
2023
2nd 6 Months (Avg) < 0.002
/
mg/L <
/
2023
2nd 6 ...(Max)
0.002
/
mg/L
/
2023
2nd 6 ...(Min)
< 0.001
/
mg/L <
/
2023
2nd 6 ...(Count)
2
/
/
Sample Count: 2
Months Sampled
:
2
Weeks Sampled:
2
Quarters Sampled :
2
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M:
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass /Limit
Cyanide
08/16/2023 S
WolfspeedP13081623S <
0.003
/ 1.20
mg/L
<
/
elf
10/03/2023 P
WolfspeedP13100323P <
0.003
/ 1.20
mg/L
<
/
OTW
Aug 2023
Week 3 <
0.003
/
mg/L
<
/
Oct 2023
Week 1 <
0.003
/
mg/L
<
/
Aug 2023
Average <
0.003
/ 0.65
mg/L
<
/
Oct 2023
Average <
0.003
/ 0.65
mg/L
<
/
2023
Quarter 3 <
0.003
/
mg/L
<
/
2023
Quarter 4 <
0.003
/
mg/L
<
/
2023
2nd 6 Months (Avg) <
0.003
/
mg/L
<
/
2023
2nd 6 ...(Max) <
0.003
/
mg/L
<
/
2023
2nd 6 ...(Min) <
0.003
/
mg/L
<
/
2023
2nd 6 ...(Count)
2
Sample Count : 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
2
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M:
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00 # Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Lead
08/16/2023 S WolfspeedP13081623S < 0.0025 / 0.69 mg/L < /
elf
Saturday, February 24, 2024 9:50:17PM * Indicates Violation ** Indicates TRC Violation Page 3 of 6

Wolfspeed Durham
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 013
Sample Date SamplelD Result/Limit Mass/Limit
Lead
10/03/2023 P
WolfspeedP13100323P <
0.0003
/ 0.69
mg/L
<
/
OTW
Aug 2023
Week 3
<
0.0025
/
mg/L
<
/
Oct 2023
Week 1
<
0.0003
/
mg/L
<
/
Aug 2023
Average
<
0.0025
/ 0.43
mg/L
<
/
Oct 2023
Average
<
0.0003
/ 0.43
mg/L
<
/
2023
Quarter 3
<
0.0025
/
mg/L
<
/
2023
Quarter 4
<
0.0003
/
mg/L
<
/
2023
2nd 6 Months (Avg) <
0.0014
/
mg/L
<
/
2023
2nd 6 ...(Max)
<
0.0025
/
mg/L
<
/
2023
2nd 6 ...(Min)
<
0.0003
/
mg/L
<
/
2023
2nd 6 ...(Count)
2
/
/
Sample Count: 2
Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
2
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC
:
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
Nickel
08/16/2023
S WolfspeedP13081623S
0.519
/ 3.98
mg/L /
elf
10/03/2023
P WolfspeedP13100323P
0.152
/ 3.98
mg/L /
OTW
Aug 2023
Week 3
0.519
/
mg/L /
Oct 2023
Week 1
0.152
/
mg/L /
Aug 2023
Average
0.519
/ 2,38
mg/L /
Oct 2023
Average
0.152
/ 2.38
mg/L /
2023
Quarter 3
0.519
/
mg/L /
2023
Quarter 4
0.152
/
mg/L /
2023
2nd 6 Months (Avg)
0.3355
/
mg/L /
2023
2nd 6 ...(Max)
0.519
/
mg/L /
2023
2nd 6 ...(Min)
0.152
/
mg/L /
2023
2nd 6 ...(Count)
2
/
/
Saturday, February 24, 2024 9:50:17PM * Indicates Violation ** Indicates TRC Violation Page 4 of 6

Wolfspeed Durham
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 013
Sample Count:
2
Months Sampled :
2
Weeks Sampled:
2
Quarters Sampled :
2
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
Silver
10/03/2023 P
WolfspeedP 13100323P <
0.0003
/ 0.43
mg/L
<
/
OTW
Oct 2023
Week 1
<
0.0003
/
mg/L
<
/
Oct 2023
Average
<
0.0003
/ 0.24
mg/L
<
/
2023
Quarter 4
<
0.0003
/
mg/L
<
/
2023
2nd 6 Months (Avg) <
0.0003
/
mg/L
<
/
2023
2nd 6 ...(Max)
<
0.0003
/
mg/L
<
/
2023
2nd 6 ...(Min)
<
0.0003
/
mg/L
<
/
2023
2nd 6 ...(Count)
1
Sample Count: 1
Months Sampled:
1
Weeks Sampled :
1
Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C:
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC
:
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TTO
08/16/2023
S WolfspeedP13081623S
0.0027
/ 2.13
mg/L /
elf
Aug 2023
Week 3
0.0027
/
mg/L /
Aug 2023
Average
0.0027
/
mg/L /
2023
Quarter 3
0.0027
/
mg/L /
2023
2nd 6 Months (Avg)
0.0027
/
mg/L /
2023
2nd 6 ...(Max)
0.0027
/
mg/L /
2023
2nd 6 ...(Min)
0.0027
/
mg/L /
2023
2nd 6 ...(Count)
1
Saturday, February 24, 2024 9:50:17PM * Indicates Violation ** Indicates TRC Violation Page 5 of 6

Wolfspeed Durham
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 013
Sample Count:
1
Months Sampled :
1
Weeks Sampled:
1
Quarters Sampled :
1
# Over Daily C:
0
0.00
# Over Mo Avg C: 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0.00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
08/16/2023 S
WolfspeedP13081623S <
0.007
/ 2.61
mg/L
<
/
elf
10/03/2023 P
WolfspeedP13100323P <
0.003
/ 2.61
mg/L
<
/
OTW
Aug 2023
Week 3 <
0.007
/
mg/L
<
/
Oct 2023
Week 1 <
0.003
/
mg/L
<
/
Aug 2023
Average <
0.007
/ 1.48
mg/L
<
/
Oct 2023
Average <
0.003
/ 1.48
mg/L
<
/
2023
Quarter 3 <
0.007
/
mg/L
<
/
2023
Quarter 4 <
0.003
/
mg/L
<
/
2023
2nd 6 Months (Avg) <
0.005
/
mg/L
<
/
2023
2nd 6 ...(Max) <
0.007
/
mg/L
<
/
2023
2nd 6 ...(Min) <
0.003
/
mg/L
<
/
2023
2nd 6 ...(Count)
2
Sample Count : 2 Months Sampled:
2
Weeks Sampled:
2
Quarters Sampled :
2
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC
:
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Saturday, February 24, 2024 9:50:17PM * Indicates Violation ** Indicates TRC Violation Page 6 of 6

Wolfspeed RTP
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 012
Sample Date
SamplelD
Result/Limit
Mass/Limit
Ammonia
09/13/2023
S
WolfspeedRTPP12091
6.29
/
mg/L
/
323Self
Sep 2023
Week 2
6.29
/
mg/L
/
Sep 2023
Average
6.29
/
mg/L
/
2023
Quarter 3
6.29
/
mg/L
/
2023
2nd 6 Months (Avg)
6.29
/
mg/L
/
2023
2nd 6 ...(Max)
6.29
/
mg/L
/
2023
2nd 6 ...(Min)
6.29
/
mg/L
/
2023
2nd 6 ...(Count)
1
Sample Date
SamplelD
Result/Limit
Mass /Limit
Average Flow for Month
07/31/2023
S
WolfspeedRTPP12072
0.04971
/ 0.469
MGD
/
3Flow
08/31/2023
S
WolfspeedRTPP12082
0.060446
/ 0.469
MGD
/
3Flow
09/30/2023
S
WolfspeedRTPP12092
0.061093
/ 0.469
MGD
/
3Flow
10/31/2023
S
WolfspeedRTPP12102
0.042902
/ 0.469
MGD
/
3F1ow
11/30/2023
S
WolfspeedRTPP12112
0.069199
/ 0.469
MGD
/
3Flow
12/31/2023
S
WolfspeedRTPP12122
0.066013
/ 0.469
MGD
/
3Flow
Jul 2023
Week 4
0.04971
/
MGD
/
Aug 2023
Week 4
0.060446
/
MGD
/
Sep 2023
Week 4
0.061093
/
MGD
/
Oct 2023
Week 4
0.042902
/
MGD
/
Nov 2023
Week 4
0.069199
/
MGD
/
Dec 2023
Week 4
0.066013
/
MGD
/
Ju12023
Average
0.04971
/ 0.329
MGD
/
Aug 2023
Average
0.060446
/ 0.329
MGD
/
Sep 2023
Average
0.061093
/ 0.329
MGD
/
Oct 2023
Average
0.042902
/ 0.329
MGD
/
Nov 2023
Average
0.069199
/ 0.329
MGD
/
Dec 2023
Average
0.066013
/ 0.329
MGD
/
2023
Quarter 3
0.057083
/
MGD
/
2023
Quarter 4
0.059371
/
MGD
/
2023
2nd 6 Months (Avg)
0.058227
/
MGD
/
2023
2nd 6 ...(Max)
0.069199
/
MGD
/
2023
2nd 6 ...(Min)
0.042902
/
MGD
/
2023
2nd 6 ...(Count)
6
Saturday, February 24, 2024 10:34:49PM * Indicates Violation ** Indicates TRC Violation Page 1 of 7

Wolfspeed RTP
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 012
Sample Count:
6
Months Sampled:
6
Weeks Sampled:
6
Quarters Sampled :
2
# Over Daily C :
0
0.00
# Over Mo Avg C : 0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0
0,00
# Over Mo Avg C TRC : 0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0
0.00
# Over Mo Avg M : 0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0
0.00
# Over Mo Avg M TRC : 0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0
0.00
# Under Daily TRC:
0
0.00
Samplc Date SamplelD Result/Limit Mass/Limit
Chloride
09/13/2023
S WolfspeedRTPP12091
775
/ mg/L
/
323Self
09/29/2023
P WolfspeedRTPP12092
329
/ mg/L
/
923POTW
Sep 2023
Week 2
775
/ mg/L
/
Sep 2023
Week 4
329
/ mg/L
/
Sep 2023
Average
552
/ mg/L
/
2023
Quarter 3
552
/ mg/L
/
2023
2nd 6 Months (Avg)
552
/ mg/L
/
2023
2nd 6 ...(Max)
775
/ mg/L
/
2023
2nd 6 ...(Min)
329
/ mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass /Limit
Cyanide
09/13/2023
S WolfspeedRTPP12091
<
0.003
/ mg/L
<
/
323Self
09/29/2023
P WolfspeedRTPP12092
<
0.003
/ mg/L
<
/
923POTW
Sep 2023
Week 2
<
0.003
/ mg/L
<
/
Sep 2023
Week 4
<
0.003
/ mg/L
<
/
Sep 2023
Average
<
0.003
/ mg/L
<
/
2023
Quarter 3
<
0.003
/ mg/L
<
/
2023
2nd 6 Months (Avg)
<
0.003
/ mg/L
<
/
2023
2nd 6 ...(Max)
<
0.003
/ mg/L
<
/
2023
2nd 6 ...(Min)
<
0.003
/ mg/L
<
/
2023
2nd 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
09/13/2023
S WolfspeedRTPP12091
323Self
09/29/2023
P WolfspeedRTPP12092
923POTW
Sep 2023
Week 2
Sep 2023
Week 4
Saturday, February 24, 2024 10:34:49PM
3.5 / 8.0
mg/L /
3.06 / 8.0
mg/L /
3.5 /
mg/L /
3.06 /
mg/L /
* Indicates Violation ** Indicates TRC Violation
Page 2 of 7

Wolfspeed RTP
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
Sep 2023
Average
3.28
/ 7.0
mg/L
/
2023
Quarter 3
3.28
/
mg/L
/
2023
2nd 6 Months (Avg)
3.28
/
mg/L
/
2023
2nd 6 ...(Max)
3.5
/
mg/L
/
2023
2nd 6 ...(Min)
3.06
/
mg/L
/
2023
2nd 6 ...(Count)
2
Sample Count: 2
Months Sampled:
1
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC:
0 0.00
# Over Mo Avg M TRC:
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date
SamplelD
Result/Limit
Mass/Limit
Mercury - LL
09/13/2023 S
WolfspeedRTPP12091 0.000003
/
mg/L
/
323Self
11/27/2023 P
WolfspeedRTPP12112 0.000002
/
mg/L
/
723POTWHg
Sep 2023
Week 2 0.000003
/
mg/L
/
Nov 2023
Week 4 0.000002
/
mg/L
/
Sep 2023
Average 0.000003
/ 0.000142
mg/L
/
Nov 2023
Average 0.000002
/ 0.000142
mg/L
/
2023
Quarter 3 0.000003
/
mg/L
/
2023
Quarter 4 0.000002
/
mg/L
/
2023
2nd 6 Months (Avg) 0.000003
/
mg/L
/
2023
2nd 6 ...(Max) 0.000003
/
mg/L
/
2023
2nd 6 ...(Min) 0.000002
/
mg/L
/
2023
2nd 6 ...(Count) 2
Sample Count: 2 Months Sampled:
2
Weeks Sampled :
2
Quarters Sampled :
2
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M:
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
Saturday, February 24, 2024 10:34:49PM * Indicates Violation ** Indicates TRC Violation Page 3 of 7

Wolfspeed RTP
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
09/13/2023
S WolfspeedRTPP12091
0.016
/
mg/L
/
323Self
09/29/2023
P WolfspeedRTPP12092
0.014
/
mg/L
/
923POTW
Sep 2023
Week 2
0.016
/
mg/L
/
Sep 2023
Week 4
0.014
/
mg/L
/
Sep 2023
Average
0.015
/
mg/L
/
2023
Quarter 3
0.015
/
mg/L
/
2023
2nd 6 Months (Avg)
0.015
/
mg/L
/
2023
2nd 6 ...(Max)
0.016
/
mg/L
/
2023
2nd 6 ...(Min)
0.014
/
mg/L
/
2023
2nd 6 ...(Count)
2
/
/
Sample Date
SamplelD
Result/Limit
Muss/Limit
Nitrate -Nitrite
09/13/2023
S WolfspeedRTPP12091
5
/
mg/L
/
323Self
09/29/2023
P WolfspeedRTPP12092
1.1
/
mg/L
/
923POTW
Sep 2023
Week 2
5
/
mg/L
/
Sep 2023
Week 4
1.1
/
mg/L
/
Sep 2023
Average
3.1
/
mg/L
/
2023
Quarter 3
3.1
/
mg/L
/
2023
2nd 6 Months (Avg)
3.1
/
mg/L
/
2023
2nd 6 ...(Max)
5
/
mg/L
/
2023
2nd 6 ...(Min)
1.1
/
mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date
SamplelD
Residt/Limit
Mass/Limit
Nitrogen, Total
09/13/2023
S WolfspeedRTPP12091
17.16
/
mg/L
/
323Self
09/29/2023
P WolfspeedRTPP12092
2.39
/
mg/L
/
923POTW
Sep 2023
Week 2
17.16
/
mg/L
/
Sep 2023
Week 4
2.39
/
mg/L
/
Sep 2023
Average
9.78
/
mg/L
/
2023
Quarter 3
9.78
/
mg/L
/
2023
2nd 6 Months (Avg)
9.78
/
mg/L
/
2023
2nd 6 ...(Max)
17.16
/
mg/L
/
2023
2nd 6 ...(Min)
2.39
/
mg/L
/
2023
2nd 6 ...(Count)
2
Saturday, February 24, 2024 10:34:49PM * Indicates Violation ** Indicates TRC Violation Page 4 of 7

Wolfspeed RTP
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Oil & Grease, Total
09/29/2023 P
WolfspeedRTPP12092 <
2.5
/ 200
mg/L
<
/
923POTW
Sep 2023
Week 4
<
2.5
/
mg/L
<
/
Sep 2023
Average
<
2.5
/
mg/L
<
/
2023
Quarter 3
<
2.5
/
mg/L
<
/
2023
2nd 6 Months (Avg) <
2.5
/
mg/L
<
/
2023
2nd 6 ...(Max)
<
2.5
/
mg/L
<
/
2023
2nd 6 ...(Min)
<
2.5
/
mg/L
<
/
2023
2nd 6 ...(Count)
1
Sample Count: l
Months Sampled
:
1
Weeks Sampled:
1
Quarters Sampled :
1
# Over Daily C:
0 0.00
# Over Mo Avg C :
0
0.00
# Over Wk Avg C :
0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00
# Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC :
0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00
# Over Mo Avg M :
0
0.00
# Over Wk Avg M :
0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00
# Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC :
0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
09/13/2023 S
WolfspeedRTPP12091
7.1
/ 5.0 - 10.5
SU
/
323Self
09/29/2023 P
WolfspeedRTPP12092
7.4
/ 5.0 - 10.5
SU
/
923POTW
Sep 2023
Week 2
7.1
/
SU
/
Sep 2023
Week 4
7.4
/
SU
/
Sep 2023
Average
7.25
/
SU
/
2023
Quarter 3
7.25
/
SU
/
2023
2nd 6 Months (Avg)
7.25
/
SU
/
2023
2nd 6 ...(Max)
7.4
/
SU
/
2023
2nd 6 ...(Min)
7.1
/
SU
/
2023
2nd 6 ...(Count)
2
Sample Count: 2 Months Sampled:
1
Weeks Sampled:
2
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C:
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
Saturday, February 24, 2024 10:34:49PM * Indicates Violation ** Indicates TRC Violation Page 5 of 7

Wolfspeed RTP
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
09/29/2023 P
WolfspeedRTPP12092
21
/ 66
°C
/
923POTW
Sep 2023
Week 4
21
/
°C
/
Sep 2023
Average
21
/
°C
/
2023
Quarter
21
/
°C
/
2023
2nd 6 Months (Avg)
21
/
°C
/
2023
2nd 6 ...(Max)
21
/
°C
/
2023
2nd 6 ...(Min)
21
/
°C
/
2023
2nd 6 ...(Count)
1
Sample Count: l Months Sampled
:
1
Weeks Sampled:
1
Quarters Sampled :
1
# Over Daily C:
0 0.00 # Over Mo Avg C :
0
0.00
# Over Wk Avg C : 0
0.00
# Over Qt Avg C : 0
0.00
# Over Daily C TRC:
0 0.00 # Over Mo Avg C TRC :
0
0.00
# Over Wk Avg C TRC : 0
0.00
# Over Qt Avg C TRC : 0
0.00
# Over Daily M :
0 0.00 # Over Mo Avg M :
0
0.00
# Over Wk Avg M : 0
0.00
# Over Qtr Avg M : 0
0.00
# Over Daily M TRC :
0 0.00 # Over Mo Avg M TRC :
0
0.00
# Over Wk Avg M TRC : 0
0.00
# Over Qtr Avg M TRC : 0
0.00
# Under Daily :
0 0.00
# Under Daily TRC:
0 0.00
Sample Date SamplelD Result/Limit Mass /Limit
TKN
09/13/2023
S WolfspeedRTPP12091
12.16
/ mg/L
/
323Self
09/29/2023
P WolfspeedRTPP12092
1.26
/ mg/L
/
923POTW
Sep 2023
Week 2
12.16
/ mg/L
/
Sep 2023
Week 4
1.26
/ mg/L
/
Sep 2023
Average
6.71
/ mg/L
/
2023
Quarter 3
6.71
/ mg/L
/
2023
2nd 6 Months (Avg)
6.71
/ mg/L
/
2023
2nd 6 ...(Max)
12.16
/ mg/L
/
2023
2nd 6 ...(Min)
1.26
/ mg/L
/
2023
2nd 6 ...(Count)
2
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
09/29/2023 P
WolfspeedRTPP12092
923POTW
Sep 2023
Week 4
Sep 2023
Average
2023
Quarter 3
2023
2nd 6 Months (Avg)
2023
2nd 6 ...(Max)
2023
2nd 6 ...(Min)
1.68
/ mg/L /
1.68
/ mg/L /
1.68
/ mg/L /
1.68
/ mg/L /
1.68
/ mg/L /
1.68
/ mg/L /
1.68
/ mg/L /
Saturday, February 24, 2024 10:34:49PM * Indicates Violation ** Indicates TRC Violation Page 6 of 7

Wolfspeed RTP
SAMPLE OVERVIEW
71112023 To 1213112023 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SannplelD
Total Phosphorus
2023 2nd 6 ...(Count)
Result / Limit
Mass /Limit
Saturday, February 24, 2024 10:34:49PM * Indicates Violation ** Indicates TRC Violation Page 7 of 7

McClatchy
The Beaufort Gazette
The Belleville News -Democrat
Bellingham Herald
Centre Daiiv Times
Sun Herald
Idaho Statesman
Bradenton Herald
The Charlotte Observer
The State
Ledger -Enquirer
Durham I The Herald -Sun
Fort Worth Star -Telegram
The Fresno Bee
The Island Packet
The Kansas City Star
Lexington Herald -Leader
The Telegraph - Macon
Merced Sun -Star
Miami Herald
El Nuevo Herald
AFFIDAVIT OF PUBLICATION
The Modesto Bee
The Sun News - Myrtle Beach
Raleigh News & Observer
Rock Hill I The Herald
The Sacramento Bee
San Luis Obispo Tribune
Tacoma I The News Tribune
Tri-City Herald
The Wichita Eagle
The Olvmpian
Account #
Order Number
Identification
Order PO
Amount
Cols
Depth
36398
539590 i_
Print Legal Ad-IPL01678000 - IPLO167800
$165.75
1
50 L
Attention: STATE OF NORTH CAROLINA
DURHAM COUNTY ENGINEERING - UTILITY DIVISION COUNTY OF WAKE, COUNTY OF DURHAM
5926 HWY 55 EAST Before the undersigned, a Notary Public of Dallas
DURHAM, NC 27713 County, Texas, duly commissioned and authorized to
administer oaths, affirmations, etc., personally
[e-mail] appeared Tara Pennington, who being duly sworn or
affirmed, according to law, cloth depose and say that he
.------Public Notice ----------- p
-- -- --- --- --- -- - -- -- -- -- --- or she is Accounts Receivable S ecialistoftheNews&
Observer Publishing Company, a corporation organized
Durham County iaccordance with
Federal and State Regulations, is
and doing business under the Laws of the State of North
g
hereby giving public notice. Listed
Carolina, and publishing a newspaper known as The
below are users in significant non-
News &Observer, Wake and State aforesaid, the said
compliance
regultions (40 CFR Part 403),�state
newspaper in which such notice, paper, document, or
pretreatment regulations (15 NCAC
21-1.0900), or local pretreatment reg-
legal advertisement was published was, at the time of
ulations during January 2023 through
each and every such publication, a newspaper meeting
December 2023.
vic
all of the requirements and qualifications of Section 1-
Corporation, located at 627 Davis
597 of the General Statutes of North Carolina and was a
Drive, Suite 100, and regulated by sig-
qualified newspaper within the meaningof Section 1 597
Q
nificant industrial user permit number
DC-106 was in status of significant
of the General Statutes of North Carolina, and that as
noncompliance for late reporting in
the first semiannual period of January
such he or she makes this affidavit; and is familiar with
through June 2023. Monitoring results
the books, files and business of said corporation and by
for February 2023 were received more
reference to the files of said publication the attached
than 30 days past the requirements as
stated in the permit. A written notifi-
advertisement for DURHAM COUNTY ENGINEERING -
cation titled "Notice of Violation" was
sent to the user's authorized repre
UTILITY DIVISION was inserted in the aforesaid
sentative requiring them to notify the
newspaper on dates as follows:
County of the cause of the violation.
TriPhaml Services, Inc. dba Alcami
Corporation reported a change in staff
1 insertion(s) published on:
that lead to the violations and took
04/09/24
corrective action to return to compli-
ance in the second semiannual period
of 2023.
Cintas Corporation, located at 1003
Twin Creek Court, and regulated by
local industrial user permit number
DC-037 was in status of significant
noncompliance for failure to self -mon-
itor monthly parameters for biochem-
ical oxygen demand, total suspended
solids, total nitrogen and total phos-
, f+��1f►, p/t/1`�
'
phorus in the second semiannual alpe-
�alCN
riod of July through December 2023.
riod
A written notification titled "Notice of
I certify (or declare) under penalty of perjury that the
Violation" was sent to the user's au-
thorized representative requiring them
foregoing is true and correct.
to notify the County of the cause of the
violation.
IPLO167800
Apr 9 2024
Notary Public in and for the state of Texas, residing in
Dallas County
STEPHANIE WATCHER
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Expires anuary 14, 2026
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