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HomeMy WebLinkAboutWQ0007798_GW Monitoring_20081224�-o GROUNDWATER MONITORING REPORT Toastmaster, Inc. - Ingraham Time Products Facility December 2008 Groundwater Monitoring Report Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, North Carolina Permit No. WQ0007798 December 24, 2008 ERM NC, PC 1130 Situs Court, Suite 240 Raleigh, NC 27606 (919)233-4501 JAN 0 7 2009 OR-FAYEIfEVILLE REGIONALOFRCE RECEIVED / DENR,' Clda Aquiferprnf.-.;.,- c.,,,FIon JAN 05 2009 GROUNDWATER MONITORING REPORT Toastmaster, Inc. - Ingraham Time Products Facility December 2008 Groundwater Monitoring Report Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, North Carolina Permit No. WQ00O7798 December 24, 2008 Chris Cuomo, P.E. Project Manager t Rick Tarravechia, P.G. Principal -in -Charge ERM NC, PC . 1130 Situs Court, Suite 240 Raleigh, NC 27609 (919) 233-4501 I TABLE OF CONTENTS LIST OF FIGURES LIST OF TABLES LIST OF APPENDICES 1.0 INTRODUCTION 1.1 SCOPE OF WORK 1.2 REPORT ORGANIZATION 2.0 BACKGROUND INFORMATION 2.1 STTELOCATION 2.2 SPTEHISTORY& PREVIOUS INVESTIGATIONS 2.3 GEOLOGY& HYDROGEOLOGY 3.0 METHODOLOGY 3.1 GROUNDWATER ELEVATIONMEASUREMENTS 3.2 SAMPLE COLLECTION 4.0 GROUNDWATER MONITORING RESULTS 4.1 GROUNDWATER ELEVATIONSAND FLOW 4.2 VOLATILE ORGANIC COMPOUND ANALYSES 4.3 QUALITYASSURANCEIQUALITYCONTROL 5.0 DISCUSSIONAND CONCLUSIONS i 1 1 2 2 2 5 6 6 6 7 7 7 8 9 LIST OF FIGURES 1 Site Location Map 2 Monitor Well Locations 3 Groundwater Contour Map 4 Groundwater Analytical Residts LIST OF TABLES 1 Monitor Well Constniction Data 2 Groundwater Field Parameters 3 Groundwater Elevation Summary - November 2008 4 Groundwater Analytical Summary - November 2008 5 Historical Groundwater Analytical Summary 6 VOC Concentration Graphs vs. Time LIST OF APPENDICES A GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORMS B LABORATORY ANALYTICAL DATA SHEETS ii 1.0 INTRODUCTION This report presents the results of the November 2008 groundwater monitoring event conducted at the Toastmaster, Inc., Ingraham Time Products facility located at 17160 Plant Road in Laurinburg, North Carolina. Groundwater at the site has been affected by volatile organic compounds (VOCs). The site's remedial approach for the existing plume of VOC affected groundwater consists of a series of recovery wells through which VOC-impacted groundwater is extracted and transferred to an above -ground treatment system. The treated groundwater is then re- introduced to the surficial aquifer via an infiltration gallery. The groundwater extraction and treatment system operates under Non - Discharge Permit No. WQ0007798, originally issued by NCDENR on January 26,1998. An updated permit was re -issued on February 15, 2005, and has an expiration date of January 31, 2010. A requirement of the permit is semi-annual monitoring of seven monitor wells at the site. This report presents the results of the second of two semi-annual sampling events conducted during 2008. 1.1 SCOPE OF WORK Seven on -site monitor wells were sampled on November 13, 2008 by ERM NC, PC (ERM) of Charlotte, North Carolina. The scope of work for this project included:1) measurement of depth to water in seven groundwater monitor wells (MW-3, 5, 6, 9,10,11, and 14) and the subsequent calculation of groundwater elevations in these same wells; and 2) collection and analysis of groundwater samples from the above - referenced wells. The groundwater samples were analyzed for VOCs using EPA Method 8260B, nitrates by method 353.2, nitrites by method 354.1, sulfates by method 9056, total iron by method 6010B, and ferrous. iron by method 3500-Fe D. 1.2 REPORT ORGANIZATION The remainder of this report is divided into five sections. Section 2.0 provides background information, previous environmental investigations, and the site geology. Section 3.0 outlines field methodologies utilized during this sampling event. Section 4.0 presents the results of the field investigation and Section 5.0 provides a discussion and conclusion. ERM 1 T:\Projects\N-Z\Toastmaster 2.0 BACKGROUND INFORMATION 2.1 SITE LOCATION The Toastmaster facility is located at 17160 Plant Road in Laurinburg (Scotland County), North Carolina. Figure 1 presents a site location map. A detailed site map is included as Figure 2. The facility is situated approximately a quarter mile northwest of the intersection of US401 and US15/US501. The surrounding property land uses are primarily mixed commercial and industrial. The 50-acre property contains a single building, which is approximately 220,000 square feet in size. 2.2 SITE HISTORY & PREVIOUS INVESTIGATIONS The following section presents a summary of historical site activities and previous investigations. These details were obtained through a review of historical reports, discussions with facility and corporate personnel, and historical correspondence. The Toastmaster facility was originally developed in 1959 as Ingraham Time Products clock manufacturing facility. The following provides a summary of previous site ownership: 1959-1968 Ingraham Company 1968-1980 McGraw Edison Company 1980-1983 Toastmaster, Inc. 1983-1990 Magic Chef, Inc. 1990-Present Toastmaster, Inc. The Toastmaster facility ceased operations in 2002. Between 2002 and 2004, the site was operated as a warehouse. During 2004, all on -site operations ceased. Manufacturing operations formerly conducted on -site during the lifespan of the facility included the manufacture, assembly, and packaging of electrical clocks and timers, waffle bakers, and sandwich toasters. Operations associated with manufacturing included the following: • Plastic molding: where resins are molded into parts using machinery which heats and shapes the resin into the desired form, sans - 1 T.\Projects\N-Z\Toastmaster • Tooling operations: including stamping machines and drill presses, • Silk screening: where ink is applied to the clock faces, • Chromium and nickel electroplating: Electroplating operations were formerly conducted in association with the manufacture of metal clock parts, • Wood cutting and sanding operations: where wood blanks are formed, cut to size, and sanded, and • Spray and dipping operations: including three dry filter paint booths and one dip tank which are used to apply finishings to the clock bodies. An on -site wastewater treatment plant was constructed during initial site development in 1959. The wastewater treatment plant was used to treat plating wastewater formerly generated at the plant .Chromium and nickel electroplating wastewaters were treated to precipitate metals after hexavalent chromium had been reduced to trivalent chromium. The wastewater treatment plant included two large concrete settling tanks. Supernatant from the settling process was routed to a large unlined surface impoundment. Settled solids were spread in an unlined drying bed. Supernatant from the drying beds was collected and added to the effluent from the settling tank in the unlined surface impoundment Liquid from the unlined surface impoundment was discharged to Irvin Creek until 1980 when the discharge was re-routed to the sanitary sewer system. The wastewater treatment operations were discontinued in 1984, and the treatment plant underwent a RCRA closure. At that time, Toastmaster voluntarily installed monitor wells to confirm the absence of groundwater contamination. The monitor wells were sampled by both the state agency and Toastmaster. According to the Environmental Audit Report prepared by Water and Air Research, Inc. in 1990, no chromium, cadmium or cyanide has been detected in the groundwater samples collected from the wastewater treatment plant area. However, lead, nickel, and zinc have been detected at concentrations substantially above background levels. ERM . 3 T.\Projmt \N-Z\Toazh Wr A trichloroethene (TCE) recovery stillwas operated at the site by Toastmaster from the late 1960s until the early 1990s. A fire pit where the local fire department would practice extinguishing fires was also located behind the building. TCE was identified in groundwater at the site in the early 1990s. A Site Characterization Report (SCR) was prepared by Groundwater Technology in 1991 to define the lateral and vertical extent of TCE contamination identified in groundwater at the site. Results of the SCR suggested the presence of TCE and associated daughter compounds in the vicinity of the facility and extending to the south and southwest. Three potential source areas were identified, including:1) the area along the northwestern side of the plant; 2) an area to the southwest of the plant in the vicinity of the now removed waste treatment system; and 3) the area to the.extreme south of the site where the removed waste treatment system was relocated. TCE concentrations in groundwater at that time ranged from 25 to 12;000 parts per billion (ppb). No significant areas of affected soil were identified during the SCR. Nine soil samples were collected from seven locations across the site during the SCR. Soils were tested for TCE only using EPA Method 8010: No TCE was detected in any of the soil samples collected. Additionally, no free product has been detected in groundwater at the site. As mentioned is Section 1.0, a groundwater treatment system is currently in operation to address the TCE affected groundwater at the site. The system operates under Non -Discharge Permit No. WQ0007798, which has an expiration date of January 31, 2010. The treatment system includes three recovery wells which discharge to an aeration tank and carbon filtration system for effluent treatment. At the time of the system design, treated groundwater could not be discharged to the municipal wastewater treatment plant. Consequently, a 500-foot long infiltration gallery was constructed along the northwest portion of the site to accept the effluent discharge. Fourteen groundwater monitor wells exist at the site. In accordance with the permit, seven of these wells (MW-3, 5, 6, 9,10,11, and 14) are sampled two times a year to monitor TCE concentrations at the site. ERM 4 T:\Projects\N-Z\To tm ter A Corrective Action Plan (CAP), prepared by Richard Catlin and Associates, was approved by the North Carolina Department of Environment and Natural Resources (NCDENR) on July 2,1993. The CAP focused on mitigation of TCE in the three potential source areas identified in the SCR. The overall site remediation strategy consisted of the installation of three groundwater recovery wells. Based on the lack of detected TCE in soils, the proposed site remedy focused on the recovery and treatment of TCE affected groundwater. 2.3 GEOLOGY & HYDROGEOLOGY The Laurinburg area lies in the Flatwoods section of the Middendorf Formation. Drainage is accomplished through large, sluggish streams and swampy flood plains. The Middendorf is underlain by the Cretaceous age Blackwoods Formation, which primarily consists of alternating clay and fine-grained sand layers. Surficial soils consist of fine- to medium -grained sandy clay mixtures. The geology beneath the site is characterized by alternating clay and sand layers and is mapped as being underlain by several aquifers. Two significant zones of low permeability have been identified at the site. The upper aquifer, with a reported maximum thickness of 30 feet, is known as the Surficial Sand Aquifer. The lower aquifer is known as the Cretaceous Sand Aquifer. The first is present at a depth of approximately 15 feet below ground surface and appears to thin out towards the south end of the site. The second begins at a depth of approximately 45 to 50 feet below ground surface. During sampling conducted as part of the CSR, groundwater was encountered between 12 and 17 feet below the ground surface. Shallow groundwater velocity at the site was estimated to be 22.1 feet per year, with a general flow direction of south-southwest. ERM 0 T.\Projects\N.Z\Toastmaster 3.0 METHODOLOGY 3.1 GROUNDWATER ELEVATION MEASUREMENTS Water level measurements were obtained in each sampled monitor well using an electronic water level meter. These measurements were used to establish the depth to groundwater in order to calculate groundwater elevations and the hydraulic gradient across the site. 3.2 SAMPLE COLLECTION Seven monitor wells were sampled during the November monitoring event for VOCs, sulfate, nitrite, nitrate, total iron, and ferrous iron. Purging was accomplished using low -flow sampling procedures with a submersible stainless -steel pump, flow controller, and dedicated polyethylene tubing. A single well, MW-6, was purged using a dedicated submersible pump without a flow controller, since an apparent bend in the well casing prevents the insertion of the slightly larger stainless steel pump. This well was purged until parameters stabilized (indicating a connection with the aquifer) and then was sampled with a new disposable bailer. Each remaining monitor well was purged until field parameters stabilized or until at least three well bore volumes were extracted. Field measurements were collected for temperature, dissolved oxygen (DO), pH, oxidation reduction potential (ORP), specific conductance, and turbidity. Well construction details are presented in Table 1. A summary of field parameter measurements is presented as Table 2. Following purging, samples were collected in laboratory -provided containers. The samples were placed in chilled, insulated, shipping containers and delivered under the appropriate chain -of -custody protocol to Shealy Environmental Services, Inc., a North Carolina -certified laboratory, located in West Columbia, South Carolina. The collected samples were analyzed for VOCs, nitrate, nitrite, sulfate, total iron, and ferrous iron. After sampling each well, the water quality meter (Horiba U-22) and stainless -steel pump were properly decontaminated. Groundwater Quality Monitoring Compliance Report Forms (GW-59 and GW-59A) are included as Appendix A. earn G T.\Projects\N-Z\Toe hl ter 4.0 GROUNDWATER MONITORING RESULTS Groundwater elevations and depths to water are presented in Table 3. A groundwater elevation contour map is presented as Figure 3. 4.1 GROUNDWATER ELEVATIONS AND FLOW Depth to groundwater in the sampled monitor wells ranged from 9.50 feet below top of casing (BTOC) in MW-5 to 15.26 feet BTOC in MW-9. The top of casing elevations have historically been measured to an arbitrary datum of 100 feet. Based on this arbitrary datum, calculated groundwater elevations ranged from 100.18 in MW-6 to 110.28 feet MW-5. Groundwater flow in the surficial aquifer is to the south-southwest under an approximate hydraulic gradient of 0.0089, as measured between monitor wells MW-5 and MW-6 (see Figure 3). The groundwater flow direction is consistent with historical observations. 4.2 VOLATILE ORGANIC COMPOUND ANALYSES Groundwater analytical results for the current monitoring event are presented in Table 4 and illustrated on Figure 4. A historical summary of VOC data is presented as Table 5. A concentration versus time graph for TCE is presented as Table6. Laboratory analytical data sheets are presented in Appendix B. The following presents a summary of VOCs detected at each monitor wells that was sampled: MW-3/Duplicate • TCE: .180/180 µg/L • cis-1,2-DCE: 40/40 µg/L MW-5 • TCE: 5.2 µg/L • Chloroform 0.89 µg/L MW-6 • TCE: 59 µg/L • cis-1,2-DCE: 14 µg/L ERM 7 T.\Projects\N-Z\Tmtn ter MW-9 • TCE: 22 µg/L • cis-1,2-DCE: 2.2 µg/L MW-10 • TCE: 6.4 µg/L • cis-1,2-DCE: 2.1 µg/L MW-11 • TCE: 32 µg/L • cis-1,2-DCE: 1.6 µg/L MW-14 • TCE: 39 µg/L • cis-1,2-DCE: 3.0 µg/L • ' 1,1-DCE: 0.55 µg/L 4.3 QUALITYASSU ANCE/QUALITYCONTROL A blind duplicate sample was collected at monitor well MW-3 during the November 2008 monitoring event (see Table 4). The sample was identified as Duplicate. Both of the samples (MW-3 and Duplicate) were submitted to Shealy Environmental Services, Inc., of West Columbia, South Carolina. The duplicate sample results correlate well:180 and 180 µg/L TCE and 40 and 40 µg/L cis-1,2-DCE, indicating that the data are reproducible. A trip blank was analyzed for VOCs. No analytes were detected within the trip blank. ERM 8 T.\Projects\N-Z\Toastmaster 5.0 DISCUSSIONAND CONCLUSIONS Groundwater samples collected at the site during November 2008 detected four VOCs (TCE, cis-1,2-DCE,1,1-DCE, and chloroform). Of these detected VOCs, only TCE exceeded its North Carolina groundwater standard of 2.8 µg/L. Chloroform was only detected in one well (MW-5) at a concentration of 0.89 µg/L, which is below the North Carolina 2L groundwater quality standard (70 µg/L). 1,1-DCE was also detected in one well (MW-14) at a concentration of 0.55 µg/L, which is below the 2L groundwater quality standard of 7 µg/L. Cis-1,2-DCE was detected in 6 of 7 wells, but not in excess of the corresponding NC 21, groundwater standard (70 µg/L). Groundwater flow directions and hydraulic gradients during the November 2008 monitoring event were generally correlative with previous monitoring events conducted at the site. Field parameter values, including pH, specific conductance, ORP, and temperature are also correlative with past sampling events and are within realistic ranges for the area. TCE was detected in all seven monitor wells above the North Carolina groundwater standard of 2.8 µg/L. The highest concentration of TCE was detected in MW-3 (180,µg/L), which is located at the southeast corner of the property (one of the suspected source areas). This concentration is slightly lower than the concentration detected in MW-3 during the May 2007 sampling event (216 µg/L). Six of seven monitor wells sampled detected the degradation product cis- 1,2-DCE. In addition, the highest levels of cis-1,2-DCE correspond with the wells reporting the highest TCE concentrations (MW-3 and MW-6). The presence of 1,2 cis-DCE in these and other site monitor wells suggests that biotic reductive dechlorination of TCE is occurring throughout the affected area. Based on the continued presence of VOC concentrations above the North Carolina groundwater standards, continued groundwater monitoring of the seven monitor wells is warranted. Per the requirements of Non - Discharge Permit No. WQ0007798, the next groundwater monitoring event is tentatively scheduled for May 2009. ERM 9 T:\Projects\N-Z\Toastmaster Figures 79•Z890• 79'2 V 79'2r3P 79'27'0' 79.29M' 79•1613' 639000 6-I0e00 691000 612000 693000 % 4 w b Yl ' peT Hill t �/KK'a ffii s `�, gv nt .ram \%4 ��^-1�\ 1 A�.%�7�� ��,t���t•t �\��� ^ ��`���� p Y s a�ul \\ muU $ , . m ,`' . it i G' •. �j tT, $ At^ I +1 f tt! +Irk �� •' ✓ �, '., ti un • 'h d k c rt .+,fix +J. rOgrl. �... � � •Ma di n 0. {f' ala� �� 11.1� yi �- I <�t v ��'m` p Z �:..,_.,.,•� ,v X;' I[elg + ` ii�\'� ::'•'�i R1, tZ "' 8 win 1 ` , �:_a.iF) '' '— -yam � ✓ � l� �•` a qri� u} v - St m • 1 1� t\ F 1 i y t _ r3x % '• ��F t 1 08tL ` p i •w � all > ti i`` x .^� . ..��i . 1. 639000 650000 641000 697000 M3000 ' 79'2=1 79.260• 79'2730' 79.270' 79.26'JV 79.26V w I'.'[fi1009mb ' Ymu W Tm..wm W mb NM: M1:i.Ybs inrtf l E2M NC, PC FIGURE '�� f' - 8000 Corporate Center Drive Site Topographic Map Suite 200 Toastmaster, Inc. 1 E12M Charlotte, NC 28226 Laurinburg, North Carolina r\ 7 n MW- RW-3 ® FORMER INGRAHAM TIME PRODUCTS FACILITY MW-13 MW-9 ®. LEGEND ® Monitor/Recovery Well ERM NC, PC 8000 Corporate Center Drive ka e 200 ERM Charlootttt Chare, NC 28226 . WASTEWATER TREATMENT FACILITY MW-10 ® MW-11 �MW-1 MW-2 RW-1 MW-4 ® i i MW-6 Site Map (adapted from Richard Catlin & Associates,1993) Toastmaster, Inc. Laurinburg, North Carolina MW-12 0 40 80 120 FIGURE 2 107 (106.81) `RC-1 105 103 MW-9 (101.89) 101 MW-13 VW-7 LEGEND ® Monitor/Recovery Well 101 — Groundwater Contour Elevation based on an arbitrary datum of 100 feet ERM NC, PC . 8000 Corporate Center Drive ERM suite 200 Charlotte, NC 28226 MW-10 (,00.s7) a �11 ,soh Nip MW- 11% RW-1 ���� -MW-3 MW-4 ® (1oo.8s) i MW-6 (100.18) MW-12 0 40 80 120 FIGURE Groundwater Contour Map - November 2008 I Toastmaster, Inc. 3 Laurinburg, North Carolina is /M n ® MW-11 RC-1---__ TCE 39 5 \ TCE 32 cis-1,2-DCE 3.0 2 RW-2\ \ I :.........: I MW-13 \�\ kMW-1 MW-2 . RW-1 �) � -MW-3 MW-4 ® I MW-9 ® TCE 22 TCE 59 cis-1,2-DCE 2.2 cis-1,2-DCE 14 j)/1W-6 MW-12 LEGEND ® Monitor/Recovery Well Anal a (NC 2L Std) TCE (2.8 ug/L) cis-1,2-DCE (70 ug/L) 1,1-DCE (7 u9/L) Chloroform (70 ug/L) kaERM NC, PC 8000 Corporate Center Drive ERM Suite 200 Charlotte, NC 28226 MW-10 ® TCE 6.4 cis-1,2-DCE 2.1 0 40 80 120 FIGURE Groundwater Analytical Summary - November 2008 I Toastmaster, Inc. 4 Laurinburg, North Carolina Tables TABLE 1 MONITOR WELL CONSTRUCTION DATA TOASTMASTER, INC. INGRAHAM TIME PRODUCTS FACILITY LAURINBURG, NORTH CAROLINA -W MW-3 112.34 NA 24.84 2 NA MW-5 119.78 NA 27.49 2 NA MW-6 112.94 NA 37.89 NA NA MW-9 117.15 25 27.47 2 7-25 MW-10 110.83 25 26.80 4 6-25 117.57 25 23.15 4 6-27 IA 119.03 30 31.72 4 6-30 Notes: TOC = top of casing antsl = above mean sea level bgs = below ground surface NA = not available TAProjects N to Z%ToastrassterNToastmaster - Raleigh\JonuaTy 2009 Annual ReporATabl"Wable I - Monitor Well Construction Data,xis TABLE 2 NATURAL ATTENUATION AND FIELD MEASUREMENT PARAMETERS TOASTMASTER, INC. INGRAHAM TIME PRODUCTS FACILITY LAURINBURG, NORTH CAROLINA NOVEMBER 2008 S ID - ' r f t Tem Date Sample"de C) ' pg4. �, gi . at ri Cen'duettvt os/c qt) I{lt ,`�� (? ITT s ORP i3F r dr'4 -...(mtlltvolts),, : to O jp It) x {ttF , p k �'' 9 rtte. -;,S'ulfa,�tee{oe a M,. ahJrdlo n �'Parani ers'm /L ;. � + �' ` s2 ron Total Iron ) - MW-3 ll/13108 18.18 4.56 252 72 241 4.89 1.0 ND <0.02) 48 ND (<0.05) 0.13 MW-5 11/13/08 20.55 3.83 70 999+ 354 6.07 0.68 ND (<0.02) 9.1 ND <0.05) 6.9 MW-6 11/13/08 19.66 4.00 265 25 244 3.25 0.32 0.02 48 ND (<0.05) <0.1 MW-9 11/13/08 17.92 4.15 85 242 119 4.34 0.23 ND <0.02 9 3.7 9.2 MW-10 11/13/08 17.78 4.20 95 25 33 1.44 ND (<0.02) ND <0.02 20 2.7 3.0 MW-11 11/13/08 18.72 3.92 54 14 234 6.01 0.093 ND (<0.02) 8.7 ND (<0.05) ND <0.10 MW-14 11/13/08 17.76 5.02 214 303 -103 0.84 ND (<0.20) ND (<0.02) 24 5.4 7 General Criteria for Natural Attenuation >20 5 to 9 -- -- <-100' <0.5 < 1 --- <20 >1 --- Notes: Water chemistryparameters were taken in thefield after each well bore volume Data to this table represent the observed parameter values at completion of well development/purge. Bold data indicate positive conditions for natural attenuation processes ORP = Oxidation Reduction potential DO = Dissolved Oxygen ND - Not Detected above practical quantitation limits • Indicates likely reductive pathway T:%Projects N to Z\Toastmasteffoastmaster- Raleighl,lanuary 2009 Annual RepoMTables%Table 2 - Groundwater Field Parameters.xis TABLE 3 GROUNDWATER ELEVATIONS SUMMARY TOASTMASTER, INC. INGRAHAM TIME PRODUCTS FACILITY LAURINBURG, NORTH CAROLINA PAGE 1 OF 2 Well No. Top of Casing Elevation (feet)' 112.34 Well No. Top of Casing Elevation (Feet)* 119.78 Well No. Top of Casing Elevation (feet)- 112.94 Well No. Top of Casing Elevation (feet)• 117.15 MW-3 Dales: MW-5 Dates: MW-6 Dates: MW-9 - Dates: Water Depth (Ft BTOC) Water Elevation (Ft.) Water Depth (Ft. BTOC) Water Elevation (Ft.) Water Depth (Ft. B'fl)C) Water Elevation (Ft.) Water Depth (Ft BTOC) Water Elevation (Ft.) 11/17/06 11.33 101.01 11/17/06 8.21 111.57 11/17/06 13.15 99.79 11/17/06 15.23 101.92 5/3/07 10.16 102.18 5/3/07 - 8.72 111.06 513107 11.57 101.37 5/3/07 10.64 106.51 5/14/08 10.65 101.69 5/14108 8.21 111.57 5114109 11.93 101.01 5114109 14.66 102.49 11/13/08 11.45 100.89 11/13/08 9.50 110.28 11/13/08 12.76 100.18 11/13/08 15.26 101.89 Ft BTOC - Feet below top of casing • Top of Casing measured to an arbitrary datum of 100.00 feet. gArickkoalACAMWelevations Table9.xls TABLE 3 GROUNDWATER ELEVATIONS SUMMARY TOASTMASTER, INC. . INGRAHAM TIME PRODUCTS FACILITY LAURINBURG, NORTH CAROLINA PAGE 2 OF 2 Well No. Top of Casing Elevation (feet)* 110.83 Well No. Top of Casing Elevation (feet)* 117.57 Well No. Top of Casing Elevation (feet)" 119.03 MW-10 Dates: MW-11 Dates: MW-14 Dates: Water Depth (Ft. BTOC) Water Elevation (Ft.) Water Depth (Ft. BTOC) Water Elevation (Ft.) 7(F r [Elevfion 11/17/06. 11.34 99.49 HAWN •9.87 107.70 11/17/06 12.18 106.85 513107 8.31 102.52 5/3/07 10.64 106.93 5/3/07 10.92 108.11 5/14/08 8.56 102.27 5114109 9.95 107.62 5/14/08 ' 10.97 108.06 11/13/08 9.96 100.97 11/13/08 11.60 105.97 11/13/08 12.22 106.81 Ft BTOC = Feet below top of casing • Top of Casing measured to an arbitrary datum of 100.00 feet. TABLE 4 GROUNDWATER ANALYTICAL SUMMARY VOLATILE ORGANIC COMPOUNDS TOASTMASTER, INC. INGRAHAM TIME PRODUCTS FACILITY LAURINBURG, NORTH CAROLINA NOVEMBER 2008 .x. '.,��,`� EIr,,.qta x `nalvte Lai `°.' Imw3 �u hcate 0t" 5tiw+✓1�'1,1 6 L`MVR=9 "MV09ki " H 1'1 - M 1 °a TCE 2.8 ug/L 180 180 5.2 '59 22 6.4 32 39 Cis-1,2-DCE 70 u /L 40 40 ND 14 2.2 2.1 1.6 3.0 1,1-DCE 7 u /L ND ND ND ND. ND ND ND 0.55 Chloroform 70 u /L ND ND 0.89 ND ND ND ND ND Notes: TCE = trichloroethene DCE = dichloroethene ND = Not Detected above practical quantitation limit ug/1= micrograms per liter NC 2L Std = North Carolina 2L ground water quality standard "Duplicate" is a duplicate sample of MW-3 Detections in excess of the respective NC 2L standard are shown in bold Samples collected November 13, 2008 T:\Projects N to 2\Toastrnaster\Toastamter - Raleigh\January 2009 Annual Report\Tables\Table 4 - Groundwater Analytical Sumrnary.As TABLE 5 HISTORICAL ANALYTICAL SUMMARY VOLATILE ORGANIC COMPOUNDS TOASTMASTER, INC. INGRAHAM TIME PRODUCTS FACILITY LAURINBURG, NORTH CAROLINA PAGE 1 of 2 ig b, 1®i AgT CtiN r : i}/i* x DE P1 C19�PIL): PiCE.e; QIYGA7iT,CdMP©TINDS TC �7"1 DGiza $Y DPA a R1 " olet DCE t t ` dtofocm: 2/25/2005 ND 87.6 ND ND ND 5/18/2005 ND 74.8 ND ND ND 11/9/2005 ND 77.1 ND ND ND 5/25/2006 ND 101 ND ND ND M 3 11/17/2006 ND 116 ND ND ND 5/3/2007 ND 216 ND ND ND 11/30/2007 ND 155 ND ND ND 5/14/2008 1 0.73 180 1 ND 24 ND 11/13/2008 ND 180 ND 40 ND 2/2512005 ND 5.94 ND ND ND 5/18/2005 ND 10.4 ND ND ND 11/9/2005 ND 6.28 ND ND ND 5/25/2006 ND 6.59 ND ND ND A 5 11/17/2006 ND 7.2 ND ND ND 5/3/2007 ND 5.5 ND ND ND 11/30/2007 ND 8.3 ND ND ND 5/14/2008 ND 4.5 ND ND 1.7 11/13/2008 ND 5.2 ND ND 0.89 2/25/2005 ND 145 ND 21.1 ND 5/18/2005 ND 214 ND ND ND 11/9/2005 ND 184 ND ND ND 5/25/2006 ND 193 ND ND ND MW 6 11/17/2006 ND 181 ND ND ND 5/3/2007 ND 58.3 ND ND ND 11/30/2007 ND 173 ND ND ND 5/14/2008 ND 56 ND 17 ND 11/13/2008 ND 59 ND 14 ND 2/25/2005 ND ND ND ND ND 5/18/2005 ND 4.57 ND ND ND 11/9/2005 ND 3.2 ND ND ND 5/25/2006 ND 24.5 ND ND ND Nm-9 ll/17/2006 ND 6.2 ND ND ND 5/3/2007 ND 65.5 ND ND ND 11/30/2007 ND 1.76 ND ND ND 5/14/2008 ND 21 ND 3.0 ND 11/13/2008 ND 22 ND 2.2 ND TABLE 5 HISTORICAL ANALYTICAL SUMMARY VOLATILE ORGANIC COMPOUNDS TOASTMASTER, INC. INGRAHAM TIME PRODUCTS FACILITY LAURINBURG, NORTH CAROLINA PAGE 2 of 2 :R��TfON s aDAlI'Ei�s'�`� ��C1~; T1 2? Ground�xateY $tandar is + ON 0 2/25/2005 ND 17.6 ND 4.21 ND 5/18/2005 ND 11.3 ND 1.62 ND 11/9/2005 ND 72.1 ND ND ND AM-10 5/25/2006 ND 4.82 ND" ND ND 11/17/2006 ND 1290 ND 456 ND 5/3/2007 ND 6.73 ND ND ND 11/30/2007 ND 231 ND ND ND 5/14/2008 0.99 12 ND 2.5 ND 11/13/2008 ND 6.4 ND 2.1 ND 2/25/2005 ND 316 ND ND ND 5/18/2005 ND 396 ND ND ND 11/9/2005 ND 294 ND ND ND 5/25/2006 ND 163 ND ND ND MW-I1 11/17/2006 ND 76.2 ND ND ND 5/3/2007 ND 46.5 ND ND ND 11/30/2007 ND 126 1 ND ND ND 5/14/2008 ND 30 ND 1.7 ND 11/13/2008 ND 32 ND 1.6 ND 2/25/2005 ND 3.94 ND ND ND 5/18/2005 ND 4.68 ND ND ND 11/9/2005 ND 19.5 ND 4.28 ND 5/25/2006 ND ND ND ND ND MW-14 11/17/2006 ND 76.2 ND ND ND 5/3/2007 ND 6.69 ND ND ND 11/30/2007 ND 17 ND ND ND 5/14/2008 ND 16 ND 1.6 ND 11/13/2008 ND 39 0.55 3.0 ND 11/17/2006 NC GW STD 0.71 2.8 7 70 70 Notes: PCE= tetrachloroethene,TCE= trichloroethene,DCE= dichloroethene, VOC= volatile organic compound, ND = Not Detected (below quantization limits), ug/I = micrograms per liter, M W = monitor well, NC OW STD = North Carolina ground water standard, NA = not available TABLE 6 GRAPHS OF TCE AND cis-1,2-DCE CONCENTRATIONS VS. TIME TOASTMASTER, INC. INGRAHAM TIME PRODUCTS FACILITY LAURINBURG, NORTH CAROLINA Page 1 of 2 Well MW 3 -TCE 200 100 0 u g 9 g 9 3 so Well MW 3 - cis 1,2-DCE 40 30 20 -- 10 p 4 4 4 4 9 4 Well MW 5 - TCE 20 5 4 3 2 1 p Well'MW 5 - cis 1,2-DCE 15 10 -- 5- 0 E z £ z 2 2 i Well MW 6 -TCE 250 Well MW 6 - cis 1,2-DCE 200 40 30 150 20 100 so a 10 ' 0 i. 9. a tpo 7s a so � 25 0 Well MW 9 -TCE 10 e - s m 4 2 p Well MW 9 -cis 1,2-DCE — — — f TABLE 6 GRAPHS OF TCE AND cis-1,2-DCE CONCENTRATIONS VS. TIME TOASTMASTER, INC. INGRAHAM TIME PRODUCTS FACILITY LAURMURG, NORTH CAROLINA Page 2 of 2 Well MW 10 - TCE 00 600 400 300 200 100 0 Well MW 10 - cis 1,2-13CE 600 450 460 350 300 250 -- -_ 200 150 Ll 100 L-6- 50 0 f Z 3 2 F Z P 2 Well MW 11 -TCE 400 10Well MW 11 -cis 1,2-DCE 320 8 240 6 `d 160 4 80 2- 0 a pp ss R SO 60 - 40 20 0 $ �. Well MW 14 -TCE 10Well e 6 4 2 0 4 s MW 14 - cis 1,2-DCE b g 'a 3 a 3 q z s Appendix A Groundwater Quality Monitoring Compliance Report Forms . G`Jb'-59A COMPLIANCE REPORT FORM Permit # WQ0007798 (Suhmit one mde umnitaringpMod with GIV 59 f'am .) 1 Enter date monitoring results were due. (12-31-08) Will this monitoring report (GIN-59 and GW-59A) YES NO be submitted after the established due date? Was any required information missing on the GW-59 report forms? YES NO 2 IF the answer to question 1 or 2 is "YES" list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)?Ijthe answer is "Yes", contact the Regional Offrcefor guidance. Are any monitored constituents equal to or above the established standards? YES NO 4 If the answer to question 4 is "NO" skip to section B. If the answer to question 4 is 'NES"list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below., 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) In the same well(s) In the last two years? N/A If the answer to question 5 is "NO" skip to section B. If the answer to question 5 is 'YES", list in the space provided below, each well with constituents) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? N/A YES NO If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO" monitoring wells may be improperly located; contact the Regional Office. 7 Is the permlttee Implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? N/A If the answer to question 7 is 'YES", describe those actions in the space provided below. if the answer to question 7 is "NO", contact the Regional Office within 90 days, an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility, Failure to do so may subject the permittee to a Notice of Violation Fines and/or penalties. g The persomcompleting'this;portion (GW 59A} of Ef!e monttorng:report should s,grr below and,."submd this foim,;with GW 59 forms,fot �equtredtveells to the address provided at the`top of ihe-rurrenf GW-'S9 form 1 hereby icknovi(edge that the above Jnformation Vitas evaluatetl and the infonnabon submitted4V thJs report (Compliance Report GW-59A) is true and complete to y knowledge best of fn-77 -the Signature of Permittee (or Authorized Agent) Date GW-59A I V8/2003 SUBMIT FORM ON YFI I OW PAPER ONLY DEPARTMENT OF ENVIRONMENT& NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATERQUALITY-INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM a 1617 MAIL SERVICE CENTER; RALEIGH, NC27699-1617 Phone:(919)733.3221 FACILITY IN FORMATION Please print Clearly or Type PERMIT Number: Expiration Date: Facility Name: Toastmaster, Inc. - Ingraham Facility Non -Discharge WQ0007798 UIC NPDES Other Permit Name (if different): Facility Address: Plant Road TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery (5tre81) NC 28352 County Scotland icny) (state) 0p) ❑ Spray Field ❑ Remediation: Contact Person: Lisa Carstarphen Telephone#: 954-883-1025 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Lat 34o47'56.6" Long 79o2747.3" No. of wells to be sampled: 7 ❑ Water Source Heat Pump ❑ Other: (from Pemul SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-31 MW-3 DUP Date sample collected: 11-13-2008 FIELD ANALYSES: WAS Well Depth: 24.84 ft. Well Diameter: 2 in. pH 4.56 units Temp. 18.18 eC DRY at Depth to Water Level: 11.45 ft. below measuring point Screened Interval: NM ft. to NM ft. Spec. Cond. 252 µMhos time of sampling, Measuring Point is NM ft. above land surface Relative M.P. Elevation: 112.34 ft, Odor NM check Volume of water pumped/bailed before sampling: 1.5 gallons Appearance NM here: ❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 11/14-21/2008 LaboratoryName: Shealy Environmental Services, Inc. Certification No. 329 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD NA mg/l Nitrite (NO2) as N <0.02 mg/I Pb - Lead NA mgn Coliform: MF Fecal NA /100ml Nitrate (NO3) as N 1.0 mg/I Zn - Zinc NA mg/l Coliform: MF Total NA /100m1 Phosphorus: Total as P NA mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate NA mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total NA mg/I Al - Aluminum NA mg/I cis-1,2-DCE: 40 ug/L pH (when analyzed) NA units Be - Barium NA mg/l TICE: 180 ug/L TOC NA mg/I Ca - Calcium NA mg/l Chloride NA mg/l Cd- Cadmium NA mg/I Arsenic NA mg/I Chromium: Total NA mg/l Grease and Oils NA mg/l Cu - Copper NA mgn ORGANICS: (by GC, GC/MS, HPLC) Phenol NA mg/l Fe - Iron 0.13/ND mg/l (Specify test and method #. ATTACH LAB REPORT.) Sulfate 48 mg/I Hg - Mercury NA mg/I Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance NA µMhos K - Potassium NA mg/I VOC , method # 8260B Total Ammonia NA mg/l Mg - Magnesium NA mg/l Nitrate/Nitrite method # 353.2/354.1 (Ammonia Nitrogen; NH3as N;Amnwnla Nitrogen, Total) Mn- Manganese NAa l Sulfate ,method #9056 TKN as N NA mg/I Ni - Nickel NA nr ll Iron/Ferrous Iron method # 6010B/3500-Fe D GW-59 Rev. 1/2007 SUBMIT FORM ON YELLQW PAPER ONLY NDWATER QUALITY MONITORING: TY INFORMATION tneese runt usany, or type Name: Toastmaster, Inc. - Ingraham Facility Name (if different): ` Address: Plant Road sv��l NC County Scotland act Person: Lisa Carstarphen Telephone#:954-883.1026 I Location/Site Name: Lat 34047'56.6" Long 79o27'47.3" No, of wells to be sampled: 7 ' gram Permit) PLING INFORMATION = L ID NUMBER (from Permit): MW-5 _ Date sample collected: 11/13/2008 Depth: 27.49 ft. Well Diameter: 2 in. T to Water Level: 9.50 ft. below measuring point Screened Interval NM ft. to NM ft. luring Point is NM. ft. above land surface Relative M.P. Elevation:. 119.78 ft, ne of water pumpedibailed before sampling: 1.08 gallons sample COD NA mg/I Coliform: MF Fecal NA /100ml Coliform:.MFTotal NAmoom1 (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total - NA mg/I pH (when analyzed). NA units TOC Chloride Arsenic NA mg/l NA mg/I NA mg/I Grease and Oils NA mg/I Phenol NA mgA Sulfate 9.1.mg/l. Specific Conductance NA µMhos Total Ammonia NA mg/I (Ammnnie Nitrogen; NH3 as N: Ammonle Nitrogen, Total) TKN as N NA Number: ;harge W00007798 Expiration Date: UIC Other UNIT 'PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ RotaryDistributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: FIELD ANALYSES:' pH 3.83 units Spec. Cord. Odor NM Appearance NM Laboratory Name: Shealy. Environmental Services, Inc. Tidal concentrations. - Nitrite (NO2) as N <0.02 mgA Pb- Lead Nitrate (NO3) as N 0.68mg/I Zn - Zinc Phosphorus: Total as P NA mg/I Orthophosphate NA mg/I AI - Aluminum NA mgll Be - Barium _ NA nr l Ca - Calcium _. NA mgll Cd - Cadmium NA mg/I Chromium: Total NA mg/l Cu - Copper NA mgA Fe - Iron 6.9/ND mg/l Hg - Mercury NA mg/I K- Potassium NAni Mg - Magnesium NA mg/I Mn- Manganese NA mgA Ni - Nickel NA mg/I Temp. 20.55 eC DRY at 70 Whos time of Certification No. 329 NA mg/I NA mg/I Other (Specify Compounds and Concentration Units): Chloroform 0.89 ug/L . TCE , 5.2 ug/L ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Report Attached? ❑ Yes (1) ❑ No (0) VOC method # 8260B Nitrate/Nitrite method # 353.2/354.1 Sulfate method # 9056. Iron/Ferrous Iron method # 601OB/3500-Fe D For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Michael Pressley Permittee (or Authorized Agent) Name and Tige - Please print or type Signature of Permittee (or Authorized F GW-59 Rev. 112007 SUBMIT FORM ON YEI i OW PAPER ONLY EPARTMENT OF ENVIRONMENT B NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: IVISION OF WATER QUALITYdNFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 617MAIL SERVICE CENTER, RALEIGH.NC27699.1617 Phone:(919)733.3221 FACILITY INFORMATION - Please Pilaf Clearly or Type PERMIT Number: Expiration Date: Facility Name: Toastmaster, Inc. - Ingraham Facility Non -Discharge WQ0007798 UIC NPDES Other _ Permit Name.(if different): - _. Facility Address: Plant Road TYPE OF PERMITTED OPERATION: BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery (Street) NC 28352 - County Scotland (city) (lam) (zle) ❑ Spray Field ❑ Remediation: Contact Person: Lisa Carstarphen Telephone#:954-883-1025 ❑ Rotary Distributor Land Application of Sludge Well Location/Site Name: Let 34047'56.6" Long 79o27'47.3" No. of wells to be sampled: 7 ❑ Water Source Heat Pump ❑ Other: - from Permit SAMPLING INFORMATION - If WELL WELL ID NUMBER(from,Permit): MW-6 .. Date sample collected: 11/13/2008 FIELD ANALYSES: WAS Well Depth: 37.89ft. Well Diameter: NM in. pH 4.00 units Temp. 19;66 eC DRY at Depth to Water Level: 12.76 ft. below measuring point Screened Interval: NM ft. to NM ft. Spec. Cond. 265 µMhos time of Measuring Point is NM ft. above land surface Relative M.P. Elevation: 112.94ft. Odor NM_ sampling,check Volume of water pumped/bailed before sampling: 10 gallons Appearance NM here: ❑ Samples for metals were collected unfiltered: DYES ❑ NO and field acidified: ❑YES ❑ NO ' LABORATORY INFORMATION Date sample analyzed: 11114-21/2008 _ Laboratory Name: Shealy Environmental Services, Inc. Certification No. 329 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. - COD NA mg/I Nitrite (NO.) as N 0.02 mg/I Pb - Lead NA mg/l Coliform: MF Fecal NA /100ml Nitrate (NO3) as N 0.32 mg/I Zn - Zinc NA mg/I _ Coliform: MF Total NA moom1 Phosphorus: Total as P NA mg/I (Nots:'Use MPN method for highly turbid samples) Orthophosphate NA.mg/1 Other (Specify Compounds and Concentration Units): Dissolved Solids: Total .NA mg/I AI -Aluminum NA mgA cis-1,2-DCE 14ug/L pH (when analyzed) NA units Be - Barium NA mgA TICE 59 ug/L. TOC NA mg/I Ca - Calcium NA mgA _ Chloride NA mg/I Cd - Cadmium NA mg/I Arsenic NA mg/I Chromium: Total NA mg/I ' Grease and Oils NA mgA Cu - Copper NA mgA ORGANICS: (by GC, GC/MS, HPLC) Phenol _ NA mg/I Fe - Iron ND mgA (Specify test and method #. ATTACH LAB REPORT.), Sulfate 48 mg/l Hg - Mercury NA mgA Report Attached? ® Yes (1) ❑ No (0) ' Specific Conductance NA µMhos K —.Potassium NA mg/1 VOC , method # 8260B Total Ammonia NA mg/I, Mg - Magnesium NA mg/I Nitrate/Nitrite method # 353.2/354.1 (AmmonmPOmgen;NHsasNtAmmoolaNitrogen. Totel) Mn- Manganese NA mgA Sulfate method# 9056 TKN as N NA mg/I Ni - Nickel NA mgA Iron/Ferrous Iron method # 601 OB/3500-Fe D For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs:- mg/L Effluent Total VOCs: mg/L VOC Removal% Michael Pressley Permittee (or Authorized Agent) Name and Tide_- Please print or type - Signature of Permittee (or Authorized Agent) (Date) GW-59 Rev. 1/2007 UNLY 111aaMIJ EPARTMENT OF ENVIRONMENT &'NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: IVISION'OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 617MAIL SERVICE CENTER. RALEIGH.NC276994617 Phonoif9191733-3221 Name: Toastmaster, Inc. - IngrahamFacility Name (if different): Address: Plant Road (sire.) NC 28352 County Scotland act Person: Lisa Carstarphen Telephone#:954-883-1025 Location/Site Name: Let 34o47'56.6" Long 79o27'47.3" No. of wells to be sampled: L ID NUMBER (from Permit): -MW-9 Depth: 27.47 ft, 1 to Water Level: 15.26 ft. below measuring point uring Point is NM ft. above land surface ne of water pumped/bailed before sampling: sample COD _ NA mg/I Coliform: MF Fecal NA /100ml Coliform: MF Total NA /100m1 (Note: Use MPN method for highly turtld samples) Dissolved Solids: Total NA mgn pH (when analyzed) _. _ NA units TOC NA mg/I Chloride NA mg/I Arsenic NA.mg/I Grease and Oils NAmg/l, Phenol NA mg/1 Sulfate 9 mg/I Specific Conductance . NA µMhos Total Ammonia NA mg/I •(Ammonia Nitrogen; 1,11-13as N;Ammonie Nitrogen, Total) TKN as N NA Date sample collected: 11/13/2008 Well Diameter: 2 in. - Screened Interval: 7 ft. to 25 ft. Relative M.P. Elevation: 117.15 ft, 2.9 gallons Number: Expiration Date: harge WQ0007798 UIC_ Other 'PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation:.Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: FIELD ANALYSES: WAS pH 4.15 units Temp. 17.92 iOc DRY at Spec. Cond. 11.2 µMhos time of Odor NM samplin check Appearance NM here: ,r Laboratory Name: Shealy Environmental Services, Inc. colloidal concentrations. Nitrite (NO2) as N <0.02 mg/1 Pb - Lead Nitrate (NO3) as N 0.23 mg" Certification No. 329' NA mg/I Zn - Zinc PIA m9/1 Phosphorus: Total as P NA mgll Orthophosphate NA mg/I Other (Specify Compounds and Concentration Units): AI - Aluminum - NA mgn cis-1,2-DCE 2.2 ug/L Be,- Barium NA mg/I TICE - 22 ug/L Ca- Calcium NA mall Cd - Cadmium .. NA mg/1 Chromium: Total NA mg/I Cu - Copper _ NA mg/I Fe - Iron 9.2/3.7 mg/I. Hg - Mercury NA mg/I K- Potassium NA mg/1 Mg -Magnesium. NA mg4 Mn - Manganese _ NA n l Ni -Nickel NA mg/I ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Report Attached? ® Yes (1) ❑ No (0) VOC method # 8260B Nitrate/Nitrite method # 353.2/354.1 Sulfate method # 9056 Iron/Ferrous Iron method # 6010B/3500-Fe'D For Kernerllation systems Only (Attach Lab Reports): Intluent Total VOOs: mg/L Effluent Total VOIDS: mg/L VOC Removal% Michael Pressley_ -� 12/22I2008 Permittee (or Authorized Agent) Name and Tige - Please print or type Signature of Fermittee (or Authorized Agent) (Date) GW-59 Rev. 1/2007 SUBMIT FORM. ON YELLOW PAPER ONLY EPARTMENT OF ENVIRONMENT 3 NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: 7MVISION OFWATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM- - 617 MAIL SERVICE CENTER, RALEIGH, NC 276994617 Phone: (919) 7333221 FACILITY INFORMATION Please Print Clearly or Type IERMIT Number: Expiration Date: Facility Name: Toastmaster, Inc. - Ingraham .Facility on -Discharge WQ0007798 UIC - - -- -OtherFacility Permit Name(ifdifferent): - -_ - --�.. — -PDES Address: Plant Road YPE OF PERMITTED OPERATIONBEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery (si NC County Scotland (City) (sti (zip) ❑Spray Field El Remediation: ' Contact Person: Lisa Carstarphen Telephone#; 954-883-1025 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Lat 3401 Long 79o27'47.3" No. of wells to be sampled: 7.2/2.4 ❑ Water Source Heat Pump ❑ Other: fmm P-, ' SAMPLING INFORMATION - - - - If WELL WELL ID NUMBER (from Permit): MW-10 Date sample collected: 11/13/2008 FIELD ANALYSES: WAS Well Depth: 26.8ft.. Well Diameter: 4 in. pH 4.20 units Temp. 17.78 eC DRY of Depth to Waler.Level: 9.86 ft. below measuring point Screened Interval: ft. to ff. Spec. Cond. 95 µMhos time of Measuring Point is NM ft. above land surface Relative M.P. Elevation: _6 _L 110.83 ft. Odor NM 'check sampling, Volume of water pumped/balled before sampling: 1.0 gallons _ Appearance NM here: ❑ Samples for metals were collected unfiltered: OYES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 11/14-21/2008 Laboratory Name: _Shealy Environmental Services, Inc. Certification No. 329 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD NA mg/I Nitrite (NO.) as N ND mg/I Pb- Lead NA mg/I" Coliform: MF Fecal NA 1100mI. Nitrate (NO3) as N ND mgll Zn -Zinc NA mg/I - Colifonn: MF Total NA /100m1 Phosphorus: Total as NA mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate NAmg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total NA mg/1 AI - Aluminum NA mg/I cis-1,2-DCE _ 2.1 ug/L pH (when analyzed) NA units Be - Barium NA mg/I TICE 6.4 ug/L TOG NA mg/I - Ca - Calcium NA mg/I Chloride NA mg4 Cd - Cadmium NA mg/l Arsenic NA mg/I Chromium: Total NA mg/I Grease and Oils NA mg/l Cu-. Copper NA mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol NA mg4 Fe - Iron 3.0/2.7 mg/I (Specify test and method #. ATTACH LAB REPORT.) ' Sulfate - 20. mg/I Hg - Mercury NA mg/I Report Attached? ® Yes (1) ❑ No (0) - Specific Conductance NA µMhos K - Potassium NA-mg/I VOC , method # 8260B Total Ammonia _ NA mg/I Mg - Magnesium NA mg4 Nitrate/Nitrite method # 353.2/354.1 (Ammonia Nitrogen; NH,.. N;Ammerlla Nitrogen, Total) Mn- Manganese NA mg/I Sulfate ,method# 9056 TKN as N NA mg/I Ni - Nickel NA mg4 Iron/Ferrous Iron method # 6010B/3500FeD For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% .Michael Pressley I _ l� &��-aii 12/22/2008 Peneirae(orAuthonzed Agent) Name and Title -Please print or type Signature of Permittee(or Authorized Agent) - - (Dale) GW-59 Rev. 112007 SUBMIT FORM ON VFI I OW PAPER ONLY NDWATER QUALITY MONITORING: LIANCE REPORT FORM Name: Toastmaster, Inc. - Ingraham Facility Name (if different): Address: Plant Road (Svaap NC (z,P) county Scotland act Person: Lisa Carstarphen Telephone#:954-883-1025 Location/Site Name: Lat 34o47'56.6" Long 79o27'47.3" No. of wells to be sampled: 7 LID NUMBER (from Permit): MW-11 Depth: - 23.15 ft. i to Water Level: 11.60 ft. below measuring point uring Point is NM ft. above land surface ne of water pumped/bailed before sampling: 1.32 sample COD NA mg/I Coliform: MF Fecal NA /100ml Coliform: MF Total NA /10omi (Not.: Use MPN method for highly t.rbld samples) Dissolved Solids: Total NA mg/I pH (when analyzed) NA units TOG NA mg/I Chloride NA mg/I Arsenic NA mg/I Grease and Oils NA mg/1 Phenol NA ni Sulfate 8.7 ni Specific Conductance NA µMhos Total Ammonia NA mg/I (Ammonia Nitrogen; NHr as N; Ar monia Nitrogen, Total) TKN as N NA mg/I Date sample collected: 11/13/2008 Well Diameter: 4 in. Screened Interval: 6 ft. to Relative M.P. Elevation: 117.57 ft. TENT OF ENVIRONMENT S NATURAL RESOURCES OF WATER QUALITY -INFORMATION PROCESSING UNIT MAIL SERVICE Number: :harge WQ0007798 I. NC 27699.1617 Phone: Expiration Date: _ UIC Other 733-3221 'PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ FIELD ANALYSES: pH 3.92 units Temp. 18.72 "C DRY at 25 ft. Spec. Cond. 54 µMhos time of samplin Odor NM chart, Appearance NM Laboratory Name: Shealy Environmental Services, Inc. colloidal concentrations. Nitrite (NO2) as N ND mg/I Pb - Lead Certification No. 329 NA mg/l Nitrate (NO3) as N 0.093 mg" Zn - Zinc NA mg/I Phosphorus: Total as P NA mg/I Orthophosphate NA mg/I Other (Specify Compounds and Concentration Units): Al -Aluminum NA mg/I cis-1,2-DCE 1.6 ug/L Be - Barium NA mg/I TICE 32 ug/L Ca - Calcium NA Cd - Cadmium NA al Chromium: Total NA mg/I Cu - Copper NA mg/I Fe - Iron ND/ND mg/I Hg - Mercury NA mg/l K - Potassium NA mg/I Mg - Magnesium NA mg/I Mn - Manganese NA mg/I Ni- Nickel mg/I ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method M ATTACH LAB REPORT.) Report Attached? ® Yes (1) ❑ No (0) VOC , method # 8260B Nitrate/Nitrite , method # 353.2/354.1 Sulfate , method # 9056 Iron/Ferrous Iron method # 6010B/3500Fe D For Remediation Systems Only • • 1 certify that, to the best of my knowledge and belief, the Information submitted In this report is true, accurate; and complete, and that the laboratory analytical data was produced using approved methodsof analysis by a DWO-cenifiedlaboratory. I am aware that there are si nficant nenalties'for submittin false information, includinp the ssibili of fines and im risonment for knowino violations. Michael Pressley 11: Permittee (or Authorized Agent) Name and Tifle - Please print or type Signature of Perm iftee (or Authorized Agent) r. GW-59 Rev. 11 SUBMIT FORM ON YELLOW PAPER ONLY EPARTMENT OF ENVIRONMENT& NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: IVISION OF WATER QUALITY-INFORMATIONPROCESSING UNIT COMPLIANCE REPORT FORM 617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: (919) 7333221 FACILITY INFORMATION !lease Print Clearly or Type PERMIT Number: Expiration Date:. . Facility Name: Toastmaster, Inc. - Ingraham Facility Non -Discharge W00007798 UIC NPDES" Other ' Permit Name (if different): . Facility Address: Plant Road TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Ist,W) NC County Scotland (City) (stum) tap) • El Spray Field ❑Remediation: Contact Person: Lisa Carstarphen Telephone#:954-883-1025 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Let 34047'56.6" Long 79o2747.3" No. of wells to be sampled: 7 ❑ Water Source Heat Pump ❑ Other: (from Permit SAMPLING INFORMATION - If WELL WELL ID NUMBER (from Permit): MW-14 _ Date sample`collected: 11/13/2008. FIELD ANALYSES: WAS Well Depth: 31.72 ft. Well Diameter:. 4 in. _ pH 5.02 units Temp. 17.76 "C DRY at Depth to Water Level: 12.22 ft. below measuring point Screened Interval: 6 ft. to 25 ft. Spec. Cond. 17.8 µMhos time MeasuringPoint is NM ft. above land surface 119.03 Relative M.P. Elevation: ft. Odor NM li sampling, check . Volume of water pumpedlbailed before sampling: 1.37 gallons _ _ Appearance NM here:❑ Samples for metals were collected unfiltered: DYES ❑ NO - and field acidified: ElYES ❑ NO LABORATORY INFORMATION Date sample analyzed: 11/14-21/2008 - LaboratoryName: Shealy Environmental Services, Inc. Certification No. 329 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. _ COD. NA mg/I Nitrite (NO2) as N ND mg/I Pb-'Lead NA mg/I Coliform: MF Fecal NA A00ml Nitrate (NO3) as N ND mgA Zn - Zinc NA. mg/I Coliform: MF Total NA /100m1 Phosphorus: Total as P NA mg/I (Note: use MPN memod for highly tumid samples) Orthophosphate- NA mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total NA mg/l Al -Aluminum NA mg/l CIS-1,2-DCE 3 ug/L pH (when analyzed) = NA units Ba - Barium NA mg/l TICE 39 ug/L TOC NA ni Ca -Calcium NA mgA 1,1-DCE 0.55 ug/L Chloride NA mgll Cd - Cadmium NA mg/l Arsenic NA mg/I Chromium: Total NA mg/I Grease and Oils NA ri Cu - Copper NA mg/I ORGANICS`. (by GC, GC/MS, HPLC) Phenol NA ni Fe - Iron 7/5.4 mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate 24 mg/I Hg - Mercury NA mg/I Report Attached? ® Yes (1) ❑ No (0) Specific Conductance NA µMhos K- Potassium NA mgA VOC ,method '# 8260E . Total Ammonia NA mg/I Mg - Magnesium NA mg/l Nitrate/Nitrite method # 353.2/354.1 - (Ammonia Nitrogen; NHaaa N; A=onla Nitrogen, Total) Mn - Manganese NA mg/I Sulfate method # 9065 TKN as N NA mgA Ni - Nickel NA mg/l Iron/Ferrous Iron method # 601 OB/350OFe D For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Michael Pressley % r� 1- Pennittee (or Authorized Agent) Name and Title -Please print or type Signature of Perri GW-59 Rev. 112007 ` Appendix B Laboratory Analytical Data Sheets - Ground Water SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis ERM-Southeast, Inc 8000 Corporate Center Drive Suite 200 Charlotte, NC 28226 Attention: Michael Pressley Project Name: Toastmaster Project Number:0084651 Lot Number:JK14063 Date Completed:11/2512008 Michael Casalena Project Manager }E� 11t FCCago' o� a. yo w1 L�_�1r�6A.. i U This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist. Shealy Environmental Services, Inc. Page: 1 of 27 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-970D Fax (803) 791-9111 v .shealylab.ocm Level 1 Repon v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010 NELAC No: E87653 NC DEHNR No: 329 Case Narrative ERM-Southeast, Inc Lot Nuintier: JK14063 This Report of Analysis contains the analytical results) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented In the header information associated with each sample. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (CAMP), standard operating procedures (SOPS), and Shealy policies. Any exceptions to the NELAC standards, the CAMP, SOPS or policies are qualified on the results page or discussed below. If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page. Shealy Environmental Services, Inc. - Page: 2 of 27 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 mmv.shealylab.cum Level Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary ERM-Southeast, Inc Lot Number: JK14063 Sample Number Sample ID Matrix Date Sampled Date Received 001 MW-3 Aqueous 11113/20081725 11/14/2008 002. MW-5 Aqueous 11/13120081115 11/14/2008 003 MW-6 Aqueous 11/13/20081625 11/14/2008 004 MW-9 Aqueous 11/13/20081415 11/14/2008 005 MW-10 Aqueous 11/13/20081225 11/14/2008 006 MW-11 Aqueous 11/13120081520 11/14/2008 007 MW-14 Aqueous 11/13/20081315 11/14/2008 008 DUPLICATE Aqueous 11/13/2008 11/14/2008 009 TRIP BLANK Aqueous 11/14/2008 1525 11/14/2008 (9 samples) Shealy Environmental Services, Inc. Page: 3 of'27 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 vmnv.shealylab.com Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. Executive Summary ERM-Southeast, Inc Lot Number: JK14063 Sample Sample ID Matrix Parameter Method Result Q Units Page 001 MW-3 Aqueous Ferric Iron (calculation) SM3500/6010 0.12 mg/L 5 001 MW-3 Aqueous Nitrate -N 353.2 1.0 mg/L 5 ' 001 MW-3 Aqueous Sulfate 9056 48 mg/L 5 001 MW-3 Aqueous cis-1,2-Dichloroethene 8260B 40 ug/L 6 001 MW-3 Aqueous Trichloroethene 8260E 180 ug/L 6 001 MW-3 Aqueous Iron 6010B 0.13 mg/L 7 002 MW-5 Aqueous Ferric Iron (calculation) SM350016010 6.9 mg/L 8 002 MW-5 Aqueous Nitrate -N 353.2 0:68 mg1L 8 002 MW-5 Aqueous Sulfate 9056 9.1 mg/L 8 002 MW-5 Aqueous Chloroform 8260B 0.89 ug/L 9 002 MW-5 Aqueous Trichloroethene 8260E 5.2 ug/L 9 002 MW-5 Aqueous Iron 6010B 6.9 mg/L 10 003 MW-6 Aqueous Nitrate -N 353.2 0.32 mg/L 11 003 MW-6 Aqueous Nitrite - N 353.2 REV 2 0.020 mg/L 11 003 MW-6 Aqueous Sulfate 9056 48 mg/L 11 003 MW-6 - Aqueous cis-1,2-Dichloroethene 8260B 14 ug/L 12 003 MW-6 Aqueous Trichloroethene 8260B 59 ug/L 12 004 MW-9 Aqueous Ferric Iron (calculation) SM350016010 5.5 mg/L 14 004 MW-9 Aqueous Ferrous Iron SM 3500-Fe D 3.7 mg/L 14 004 MW-9 Aqueous Nitrate -N 353.2 0.23 mg/L 14 004 MW-9 Aqueous Sulfate 9056 9.0 mg/L 14 004 MW-9 Aqueous cis-1,2-Dichloroethene 8260E 2.2 uglL 15 004 MW-9 Aqueous Trichloroethene 8260B 22 ug/L 15 004 MW-9 Aqueous Iron 6010B 9.2 mglL 16 005 MW-10 Aqueous Ferric Iron (calculation) SM350016010 0.33 mg/L 17 005 MW-10 Aqueous Ferrous Iron SM 3500-Fe D 2.7 mg/L 17 005 MW-10 Aqueous Sulfate 9056 20 mg/L 17 005 MW-10 Aqueous cis-1,2-Dichloroethene 8260B 2.1 ug/L 18 005 MW-10 Aqueous Trichloroethene 8260B 6.4 ug/L 18 005 MW-10 Aqueous Iron 6010B 3.0 mg/L 19 006 MW-11 Aqueous Nitrate -N 353.2 0.093 mg/L 20 006 MW-11 Aqueous Sulfate 9056 8.7 mg/L 20 006 MW-11 Aqueous cis-1,2-Dichloroethene 8260B 1.6 ug/L 21 006 MW-11 Aqueous Trichloroethene 8260B 32 ug/L 21 007 MW-14 Aqueous Ferric Iron (calculation) SM350016010 1.6 mg/L 23 007 MW-14 Aqueous Ferrous Iron SM 3500-Fe D 5.4 mg/L 23 007 •MW-14 Aqueous Sulfate 9056 24 mg/L 23 007 MW-14 Aqueous 1,1-Dichloroethene 8260B 0.55 ug/L 24 007 MW-14 Aqueous cis-1,2-Dichloroethene 8260B 3.0 ug/L 24 007 MW-14 Aqueous Trichloroethene 8260B 39 ug/L 24 007 MW-14 Aqueous Iron 6010B 7.0 mg/L 25 008 DUPLICATE Aqueous cis-1,2-Dichloroethene 8260B 40 ug/L 26 008 DUPLICATE Aqueous Trichloroethene 8260B 180 ug/L 26 (43 detections) Shealy Environmental Services, Inc. Page: 4 of 27 106 Vantage Paint Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Inorganic non-metals Client: ERM-Southeast, Inc Laboratory ID: JK14063-001 Description: hill Matrix: Aqueous Dale Sampled:11/13120081725 Date Received: 1111412008 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Ferric Iron ) 1 11/18/2008 1502 MNM 1 (Ferrous Iron) SM 1 11/14/2008 2343 PMM 90189 1 (Nitrate - N) 353.2 1 11/15/2008 1040 RLM 90048 1 (Nitrite - N) 353.2 REV 2 1 11/15/2008 1040 RLM 90045 1 (Sulfate) 9056 1 11/21/2008 1521 DAS 90485 CAS Analytical Parameter Number Method Result Q PQL Units Run Ferric Iron (calculation) SM350016010B 0.12 0.10 mglL 1 Ferrous Iron SM 3500-Fe D ND 0.050 mg/L 1 Nitrate - N 353.2 1.0 0.020 mglL 1 Nitrite - N 353.2 REV 2 ND 0.020 mg/L 1 Sulfate 9056 48 1.0 mglL 1 PQL= Practical quantitation limit B= Detected in the method blank E= Quanta0on of compound exceeded the calibration range ND= Not detected at or above the PQL J=Estimated result <PQL and_I MDL P=The RPD between two GC columns exceeds 40% Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged wim avv. N= Recovery is out of criteria Shealy Environmental Services, Inc. Page: 5 of 27 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Volatile Organic Compounds by GC/MS Client: ERM-Southeast, Inc Laboratory ID: JK14063-001 Description: MW-3 Matrix: Aqueous Date Sampled:1111312008 1725 Date Received: 1111412008 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 50309 8260B 1 11/18/2008 1701 DLB 90194 CAS Analytical Parameter Number Method Result Q PQL Units Run Bromodichloromethane 75-27-4 8260B ND 0.50 ug/L 1 Bromoform 75-25-2 8260D ND 0.50 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 - 8260B ND 0.50 ug/L 1 Carbon tetrachloride 56-23-5 8260B ND 0.50 ug/L 1 Chlorobenzene 108-90-7 8260E ND 0.50 uglL 1 Chloroethane 75-00-3 8260B ND 0.50 ug/L 1 Chloroform 67-66-3 8260B ND 0.50 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260E ND 0.50 ug/L 1 Dibromochloromethane 124-48-1 8260E ND 0.50 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260B ND 0.50 ug/L 1 1,3-Dichlorobenzene 541-73-1 8260B ND 0.56 ug/L, 1 1,2-Dichlorobenzene 95-50-1 8260E ND 0.50 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260B ND 0.50 ug/L 1 1,1-Dichloroethane 75-34-3 8260B ND 0.50 ug/L 1 1,2-Dichloroethane 107-06-2 8260B ND 0.50 ug/L 1 trans-1,2-Dichloroethene 156-60-5 8260B ND 0.50 ug/L 1 1,1-Dichloroethene 75-35-4 8260B ND 0.50 ug/L 1 cis-1,2-Dichloroethene 156.59.2 8260B 40 0.50 uglL 1 1,2-Dichloropropane 78-87-5 8260B ND 0.50 ug/L 1 trans-1,3-Dichloropropene 10061-02-6 8260B ND 0.50 ug/L 1 cis-1,3-Dichloropropene 10061-01-5 8260B ND 0.50, ug/L 1 Methylene chloride 75-09-2 8260B ND 0.50 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 0.50 ug/L 1 Tetrachloroethene 127-18-4 8260E ND 0.50 ug/L 1 1,1,1-Trichloroethane 71-55-6 82608 ND 0.50 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260B ND 0.50 ug/L 1 Trichloroethane 79-01-6 8260E 180 0.50 ug/L 1 Trichlorof Lioromethane 75-69-4 8260B ND 0.50 ug/L 1 Vinyl chloride 75-01-4 8260B ND 0.50 uglL 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 110 52-138 Bromofluorobenzene 104 70-147 Toluene-d8 104 76-125 PCL= Practical quanlitatian limit a= Detected M the method blank E=Duantitation of compound exceeded the calibration range ND= Not detected at or above the PGL J=Estimated result <PGL and _>MDL P= The RPD between lwo GC columns exceeds 40% Vvhere applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a"W N= Recovery is out of coterie Shealy Environmental Services, Inc. Page: 6 of 27 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level Report v2.1 ICP-AES Client: ERM-Southeast, Inc Laboratory ID: JK14063.001 Description: MW-3 Matrix: Aqueous Date Sampled:1 111312008 1725 Date Received: 1111412008 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3005A 6010E 1 11/18120081502 MNM 11/14/20082025 90012 CAS Analytical Parameter Number Method Result Q PQL Units Run Iron 7439-89-6 6010B 0.13 0.10 mglL 1 PQL= Practical quantitation limit B= Detected in the method blank E= Quanbtaton of compound exceeded me caliballon range ND= Not detected at or above the PQL J=Estimated result <PQL and MDL P= The RPD between two GD columns exceeds 40% Mena appriwble, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' N = Recovery Is out of crileda Shealy Environmental Services, Inc. Page: 7 of 27 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 v .shealylab.com Level 1 Roped v21 Inorganic non-metals Client: ERM-Southeast, Inc Laboratory ID: JK14063.002 Description: MW-5 Matrix: Aqueous Date Sampled:11113120081115 Date Received: 1111412008 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Ferric Iron ) 1 11120/2008 1334 MNM 1 (Ferrous Iron) SM 1 11/14/2008 2343 PMM 90189 1 (Nitrate - N) 353.2 1 11/1512008 1041 RLM 90048 1 (Nitrite - N) 353.2 REV 2 1 11/15/2008 1041 RLM 90045 1 (Sulfate) 9056 1 11/21/2008 1543 DAS 90485 CAS Analytical Parameter Number Method Result Q PQL Units Run Ferric Iron (calculation) SM350016010B 6.9 0.10 nri 1 Ferrous Iron SM 3500-Fe D ND 0.050 mg/L 1 Nitrate -N 353.2 0.68 0.020 mglL 1 Nitrite - N 353.2 REV 2 NO 0.020 mg/L 1 Sulfate 9056 9.1 1.0 mglL 1 PCL = Practical quantitabon limit a = Detected In the method blank E = Quantitation of compound exceeded the calibration range ND= Not detected at or above We PQL J=Estimated result<PCL and MDL P= The RPD between two GC columns exceeds 40% Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a N= Recovery is out of criteria Shealy Environmental Services, Inc Page: 8 of 27 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-970o Fax (803) 791-9111 wwvv.shealylab.com Level i Report v2.1 Volatile Organic Compounds by GC/MS Client: ERM-Southeast, Inc Laboratory ID: JK14063-002 Description: MW-5 Matrix: Aqueous Date Sampled:11I13120081115 Date Received: 1111412008 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B 1 11118/2008 1722 DLB 90194 CAS Analytical Parameter Number Method Result Q PQL Units Run Bromodichloromelhane 75-27-4 8260B NO 0.50 ug/L 1 Bromoform 75-25-2 8260B NO 0.50 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260B NO 0.50 ug/L 1 Carbon tetrachloride 56-23-5 8260B NO 0.50 ug1L 1 Chlorobenzene 108-90-7 8260E NO 0.50 ug/L 1 Chloroelhane 75-00-3 8260B NO 0.50 ug/L 1 Chloroform 67-66-3 8260B 0.89 0.50 uglL 1 Chloromethane (Methyl chloride) 74-87-3 8260B NO 0.50 ug/L 1 Dibromochloromethane 124-48-1 8260E NO 0.50 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260B NO 0.50 ug1L 1 1,3-Dichlorobenzene 541-73-1 8260B NO 0.50 uglL 1 1,2-Dichlorobenzene 95-50-1 8260B NO 0.50 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260B NO 0.50 ug/L 1 1,1-Dichloroethane 75-34-3 8260B NO 0.50 ug/L 1 1,2-Dichloroethane 107-06-2 826013 NO 0.50 ug/L 1 trans-1,2-Dichloroethene 156-60-5 8260E NO 0.50 ug/L 1 1,1-Dichloroethene 75-35-4 8260B NO 0.50 ug/L 1 cis-1,2-Dichloroethene 156-59-2 8260B NO 0.50 ug/L 1 1,2-Dichloropropane 78-67-5 8260B NO 0.50 ug/L 1 trans-1,3-Dichloropropene 10061-02-6 8260E NO 0.50 ug/L 1 cis-1,3-Dichloropropene 10061-01-5 8260B NO 0.50 ug/L 1 Methylene chloride 75-09-2 8260B NO 0.50 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260B NO 0.50 ug/L 1 Tetrachloroelhene 127-18-4 8260B NO 0.50 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260B NO 0.50 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260B NO 0.50 ug/L 1 Trichloroethene 79.01-6 8260B 5.2 0.50 uglL 1 Tdchlorofluoromethane 75-69-4 8260E NO 0.50 ug/L 1 Vinyl chloride 75-01-4 8260E NO 0.50 ug/L 1 Run 1 Acceptance Surrogate 9 Q % Recovery Limits 1,2-Dichloroethane-d4 110 52-138 Bromofluorobenzene 104 70-147 Toluene-d8 103 76-125 PCL = Practical quanfitation limit S = Detected in the method blank E = Duantitabon of compound exceeded the calibration range - ND=NatdetectedatorabovethePDL J=Estimated result <PCL and >Not. P= The RPD between two GC columns exceeds 40% Where applicable, all soil sample analysis are reponed on a dry weight basis unless flagged with a N= Recovery is out of aitena Shealy Environmental Services, Inc. Page: 9 of 27 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level Report v2.1 ICP-AES Client: ERM-Southeast, Inc Laboratory ID: JK14063-002 Description: MW-5 Matrix: Aqueous Date Sampled:1111312008 1115 Date Received: 1111412008 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 3005A 6010E 1 11/20120081334 MNM 90267 CAS Analytical Parameter Number Method Result Q PQL Units Run Iron 7439.89-6 6010B 6.9 0.10 mgfL 2 PQL= Practical quantitation limit B = Detected In the method blank E = Q,mrttatian of compound exceeded the calibration range No Not detected at or above the POL J= Estimated result< PQL and> MDL P= The RPD between two GC mlumns exceeds 40% Where applicable, all soil sample analysis are reported on a dry weight basis unless Bagged with a'W' N = Recovery is out of enters Shealy Environmental Services, Inc. Page: 10 of 27 IDB Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 wvw.shealylaocom Level l Reponv2.1 Inorganic non-metals Client: ERM-Southeast, Inc Laboratory ID: JK14063-003 Description: MW-6 Matrix: Aqueous Date Sampled:11/13/2008 1625 Dale Received: 1111412008 'Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Ferric Iron ) 1 11/1812008 1508 MNM .. 1 (Ferrous Iron) SM 1 11/14/2008 2343 PMM 90189 " 1 (Nitrate - N) 353.2 1 11/15/2008 1042 RLM 90048 1 • (Nitrite - N) 353.2 REV 1 11/15/2008 1042 FILM 90045 1 (Sulfate) 9056 1 11/2112008 1606 DAS 90485 CAS Analytical Parameter Number Method Result Q PQL Units Run Ferric Iron (calculation) SM3500/6010B ND 0.10 mglL 1 Ferrous Iron SM 3500-Fe D ND 0.050 mglL 1 Nitrate -N 353.2 0.32 0.020 mglL 1 Nitrite - N 353.2 REV 2 0.020 0.020 mglL 1 Sulfate 9056 48 1.0 mglL 1. = Practical Quandtatlon limit B = Detected in ma method blank E = Cuantitation of compound exceeded the calibration range Not detected at or above the Put. J = Estimated result <PDL and >MDL P= The RPD between No GC columns exceeds 40% applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W N = Recovery Is out of cReda "nonmental Services, Inc, Page: 11 of 27 e Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803).791-9111 w .shealylab.com Level I Reponv2.1 Volatile Organic Compounds by GC/MS Client: ERM-Southeast, Inc Laboratory ID: JK14063.003 Description: MW-6 'Matrix: Aqueous Date Sampled:11/13/2008 1625 Date Received:[[/1412008 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260E 1 11/18/2008 1744 DLB 90194 Parameter CAS Analytical Number Method Result Q ' PQL Units Run Bromodichloromelhane 75-27-4 8260B NO 0.50 ug/L 1 Bromofonn 75-25-2 82608 NO 0.50 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260B NO 0.50 ug/L 1 Carbon tetrachloride 56-23-5 8260B NO 0.50 ug/L 1 Chlorobenzene - 108-90-7 8260B NO 0.50 ug/L 1 Chloroethane 75-00-3 8260B NO 0.50 ug/L 1 Chloroform 67-66-3 8260B ND 0.50 ug/L 1 Chloromelhane (Methyl chloride) 74-87-3 8260B NO 0.50 ug/L 1 Dibromochloromelhane 124-48-1 8260B NO 0.50 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260E NO 0.50 ug/L 1 1,3-Dichlorobenzene 541-73-1 8260B NO 0.50 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260B ND 0.60 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260E ND 0.50 ug/L 1 1,1-Dichloroethane 75-34-3 8260B NO 0.50 ug/L 1 1,2-Dichloroethane 107-06-2 8260B NO 0.50 ug/L 1 trans-1,2-Dichloroethene 156-60-5 82608 NO 0.50 ug/L 1 1,1-Dichloroethene 75-35-4 8260B NO 0.50 ug/L 1 cis-1,2-Dichloroethene 156-59-2 8260B 14 0.50 ug1L 1 1,2-Dichloropropane 78-87-5 8260B ND 0.50 ug/L 1 Vans-1.3-Dichloropropene 10061-02-6 8260B NO 0.50 ug/L 1 cis-1,3-Dichloropropene 10061-01-5 8260E ND 0.50 ug/L 1 Methylene chloride 75-09-2 8260B ND 0.50 ug/L 1 1,1,2,2-Tetrachloroelhane 79-34-5 8260B NO 0.50 ug/L 1 Telrachloroethene 127-18-4 8260B NO 0.50 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260B ND - 0.50 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260B NO 0.50 ug/L 1 Trichloroethene 79-01-6 8260E 59 0.50 uglL 1 Trichlcrofluoromethane 75-69-4 8260B NO 0.50 ug/L 1 Vinyl chloride 75-01-4 8260B NO 0.50 ug/L 1 Run 1 Acceptance Surrogate Q /, Recovery Limits 1,2-Dichloroethane-d4 111 52-138 Bromofluorobenzene 107 70-147 Toluene-d8 103 76-125 PGL= Practice[ quamitaron limit 9= Detached in the method blank E= ouantitation of compound exceeded the calibration range ND= Not detected at Or above the PGL J= Estimated result< PGL and >Mot. P= The RPD between two GC columns exceeds 40% Where applicable, all soJ sample analysis are reported on a dry weight basis unless flagged with a N= Recovery IS Out of cmena Shealy Environmental Services, Inc. Page: 12 of 27 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level Report v2.1 ICP-AES Client: ERM-Southeast, Inc Laboratory ID: JK14063.003 Description: MW-6 Matrix: Aqueous Date Sampled:1 111312008 1625 Date Received: 11114/2008 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3005A 6010B 1 11/18/2008 1508 MNM 11/14/2008 2025 90012 CAS Analytical Parameter Number Method Result Q PQL Units Run Iron 7439-89-6 6010B ND 0.10 mg/L 1 PQL= Practical quantitation limit 6= Detected in the method blank E= Quantitation of compound exceeded the calibration range ND= Not detected at or above the PQL J=Estimated result<POL and >MDL P= The RPD between Me GC columns exceeds 40% Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W N = Recovery Is cut of cnteda Shealy Environmental Services, Inc. Page: 13 of 27 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 w .shealylab.com Level I Report v21 Inorganic non-metals Client: ERM.Southeast, Inc Laboratory ID: JK14063-004 Description: MW-9 Matrix: Aqueous Date Sampled:11/1312008 1415 Date Received: 11/1412008 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Ferric Iron ) 1 11/2012008 1340 MNM 1 (Ferrous Iron) SM 2 11/14/2008 2343 PMM 90189 1 (Nitrate - N) 353.2 1 11/15/2008 1043 FILM 90048 1 (Nitrite - N) 353.2 REV 2 1 11/15/2008 1043 FILM 90045 1 (Sulfate) 9056 1 11/21/2008 1628 DAS 90485 CAS Analytical Parameter Number Method Result Q PQL Units Run Ferric Iron (calculation) SM350016010B 5.5 0.10 mglL 1 Ferrous Iron SM 3500-Fe D 3.7 0.10 mg/L. 1 Nitrate -N 353.2 0.23 0.020 mg/L 1 Nitrite - N 353.2 REV 2 ND 0.020 mgfL 1 Sulfate 9D56 9.0 1.0 mg1L 1 PQL = Practical guarb etlon limit B = Defected in the method blank E = Guantitation of ocmpound exceeded the calibration range NO= Not detected at or above the PQL J=Estimated result <PQL and_MDL P= The RPD between Me GC columns exceeds 40% Where applicable, all soli sample analysis are reported on a dry weight basis unless gagged with a"W N= Recovery is out of criteria Shealy Environmental Services, Inc. Page: 14 of 27 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 vnvw.shealylab.Wm Level 1 Report v21 Volatile Organic Compounds by GC/MS Client: ERM-Southeast, Inc Laboratory ID: JK14063-004 Description: MW-9 Matrix: Aqueous Date Sampled:1111312008 1415 Date Received: 11/14/2008 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 50308 8260B 1 11/18/2008 1805 DLB 90194 CAS Analytical Parameter Number Method Result Q PQL Units Run Bromodichloromethane 75-27-4 8260B NO 0.50 ug/L 1 Bromoform 75-25-2 8260B NO 0.50 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260B NO 0.50 ug/L 1 ' Carbon tetrachloride 56-23-5 8260B ND 0.50 ug/L 1 Chlorobenzene 108-90-7 8260B NO 0.50 ug/L 1 Chloroethane 75-00-3 8260B ND 0.50 ug/L 1 Chloroform 67-66-3 8260B ND 0.50 ug/L 1 Chloromelhane (Methyl chloride) 74-87-3 8260B ND 0.50 ug/L 1 Dibromochloromethane 124-48-1 8260B ND 0.50 ug/L 1 1,2-Dibromoethane (EDB) - 106-93-4 8260E NO 0.50 uglL 1 1,3-Dichlorobenzene 541-73-1 ' 8260B NO 0.50 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260B NO 0.50 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260B NO 0.50 ug/L 1 1,1-Dichloroelhane 75-34-3 82608 NO 0.50 ug/L 1 1,2-Dichloroelhane 107-06-2 8260B ND 0.50 ug/L 1 trans-1,2-Dichloroethene 156-60-5 8260E ND 0.50 ug/L 1 1,1-Dichloroethene 75-35-4 8260B ND 0.50 ug/L 1 cis-1,2-Dichloroethene 156-59-2 8260E 2.2 0.50 ug/L 1 1,2-Dichloropropane 78-87-5 8260B NO 0.50 ug/L 1 trans-1,3-Dichloropropene 10061-02-6 8260B NO 0.50 ug/L 1 cis-1,3-Dichloropropene 10061-01-5 8260E NO 0.50 ug/L 1 Methylene chloride 75-09-2 82608 NO 0.50 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260B NO 0.50 ug/L 1 Tetrachloroethene 127-18-4 8260B NO 0.50 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260E ND 0.50 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260B NO 0.50 ug/L 1 Trichloroethene 79-01-6 8260B 22 0.50 ug1L 1 Tdchlorofluoromethane 75-69-4 8260E ND 0.50 ug/L 1 Vinyl chloride 75-01-4 8260E ND 0.50 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 112 52-138 Bromofluorobenzene 104 70-147 Toluene-d8 102 76-125 PQL= Practical quantitation limit B= Detached in the method blank E=Quamtafion of compound exceeded the calibration range ND= Not detected at or above the PQL J=Estimated! result <PQL and _>MDL P=The RPD between two GC columns exceeds 40% vision, applicable, all soil sample analysis are reported on a dry weight basis unless flagged win a "W' N = Recovery is out of emeda Shealy Environmental Services, Inc. Page: 15 of 27 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.ccm Level Report v2.1 ICP-AES Client: ERM-Southeast, Inc Laboratory ID: JK14063.004 Description: MW-9 Matrix: Aqueous Date Sampled:1111312008 1415 Date Received: 11114/2008 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 3005A 6010E 1 11120120081340 MNM 90267 CAS Analytical Parameter Number Method Result Q PQL Units Run Iron 7439.89.6 6010B 9.2 0.10 mglL 2 PQL= Practical quantilation limit B= Detected in the method blank E= Quan6tabon of compound exceeded the calibration range ND= Not detected at or above the PQL J= Estimated result <POL and >MOL P=The RPD between We GC columns exceeds 40% Mere applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a RM N = Recovery, is out of cruise Shealy Environmental Services, Inc. Page: 16 of 27 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 viww.shealylab.com Level s Report v2.1 Inorganic non-metals Client: ERM-Southeast, Inc Laboratory ID: JK14063.005 Description: IIAW-10 Matrix: Aqueous Date Sampled:1 Ill 312008 1225 Date Received: 1111412008 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Ferric Iron ) 1 11/1812008 1513 MNM 1 (Ferrous Iron) SM 1 11/14/2008 2343 PMM 90189 1 (Nitrate - N) 353.2 1 11/15/2008 1044 RLM 90048 ' 1 (Nitrite - N) 353.2 REV 2 1 11/15/2008 1044 RLM 90045 1 (Sulfate) 9056 1 11/2112008 1651 DAS 90485 CAS Analytical Parameter Number Method Result Q PQL Units Run Ferric Iron (calculation) SM350016010B 0.33 0.10 mglL 1 Ferrous Iron SM 3500-Fe D 2.7 0.050 mg/L 1 Nitrate -N 353.2 ND 0.020 mg/L 1 Nitrite - N 353.2 REV 2 ND 0.020 ni 1 Sulfate 9056 20 1.0 mg/L 1 PQL= Practical quarntation limit B= Detected in the method blank E= Quantotien of compound exceeded the calibration range ND= Not detected at or above the PQL J=Estimated result <PQL and_MDL P=The RPD behveen two GC columns exceeds 40% Where applicable, all soft sample analysis are reported on a dry weight basis unless flagged with a'W N= Recovery is out of crioda Shealy Environmental Services, Inc. Page: 17 of 27 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.wm Level 1 Report v2.1 volaule vr9anic %�ompounus Lneiy)n] Client: ERM-Southeast, Inc Laboratory ID: JK14063-005 Description: MW-10 Matrix: Aqueous Date Sampled:1111312008 1225 Date Received: 1111412008 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260E 1 11118/20081827 DLB 90194 Parameter CAS Number Analytical Method Result Q PQL Units Run Bromodichloromelhane 75-27-4 8260B NO 0.50 ug/L 1 Bromoform 75-25-2 8260B NO 0.50 ug/L 1 Bromomelhane (Methyl bromide) 74-83-9 8260B NO 0.50 ug/L 1 Carbon tetrachloride 56-23-5 8260B ND 0.50 ug/L 1 Chlorobenzene 108-90-7 82608 NO 0.50 ug/L 1 Chloroethane 75-00-3 8260B NO 0.50 ug/L 1 Chloroform 67-66-3 8260B NO 0.50 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260B ND 0.50 ug/L 1 Dibromochloromethane 124-48-1 8260B NO 0.50 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260B NO 0.50 ug/L 1 1,3-Dichlorobenzene 541-73-1 8260E NO 0.50 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260B NO 0.50 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260E NO 0.50 ug/L 1 1,1-Dichloroethane 75-34-3 8260B ND 0.50 ug/L 1 1,2-Dichloroethane 107-06-2 8260E ND 0.50 ug/L 1 trans-1,2-Dichloroethene 156-60-5 8260B NO 0.50 ug/L 1 1,1-Dichloroethene 75-35-4 8260E NO 0.50 ug/L 1 cis-1,2-Dichloroethene 156.59-2 8260B 2.1 0.50 ug/L 1 1,2-Dichloropropane 78-87-5 8260B ND 0.50 ug/L 1 trans-1,3-Dichloropropene 10061-02-6 8260B ND 0.50 ug/L 1 cis-1,3-Dichloropropene 10061-01-5 8260B NO 0.50 ug/L 1 Methylene chloride 75-09-2 8260B ND 0.50 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260B NO 0.50 uglL 1 Tetrachloroethene 127-18-4 8260B NO 0.50 ug1L 1 1,1,1-Trichloroelhane 71-55-6 8260B NO 0.50 ug/L 1 1,1,2-Tichloroethane 79-00-5 8260B NO 0.50 ug/L 1 Trichloroethene 79-01-6 8260B 6.4 0.50 uglL 1 Trichlorofluoromethane 75-69-4 8260B NO 0.50 ug/L 1 Vinyl chloride 75-01-4 8260B NO 0.50 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 112 52-138 Bromofluorobenzene 106 70-147 Toluene-d8 101 76-125 PDL = Practical quantitation limit B = Detected in the method blank E = DuantitaGon of compound exceeded the calibration range ND= Not detected at or above the PDL J= Estimated result< PCL and_> M DL P= The RPD between two GC columns exceeds 40% Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a"W' N= Recovery is out of criteria Shealy Environmental Services, Inc. Page: 18 of 27 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Repodv2.1 ICP-AES Client: ERM-Southeast, Inc Laboratory ID: JK14063-005 Description: MW-10 Matrix: Aqueous Date Sampled:1111312008 1225 Date Received: 11/1412008 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3005A 6010B 1 11118/2008 1513 MINIM 11114/2008 2025 90012 CAS Analytical Parameter Number Method Result Q PQL Units Run Iron 7439-89.6 60108 3.0 0.10 mglL 1 PDL= Practical quantitation limit e= Detected in the method blank E= Duantitation of compound exceeded the calibration range ND= Not detected at or above the PDL J= Estimated result, PCL and, M DL P= The RPD between two GC columns exceeds 40% Where applicable, all soil sample analysis are reported on a dry weight basis unless nagged with a'W' N= Recovery is out of criteria Shealy Environmental Services, Inc. Page: 19 of 2.7 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Inorganic non-metals Client: ERM-Southeast, Inc Laboratory ID: JK14063-006 Description: MW-11 Matrix: Aqueous Date Sampled:1111312008 1520 Date Received: 11/14/2008 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Ferric Iron ) 1 11/18/2008 1525 MNM 1 (Ferrous Iron) SM 1 11/14/2008 2343 PMM 90189 1 (Nitrate - N) 353.2 1 11/15/2008 1045 RLM 90048 1 (Nitrite - N) 353.2 REV 2 1 11/15/2008 1045 RLM 90045 1 (Sulfate) 9056 1 11/2112008 1713 DAS 90485 CAS Analytical Parameter Number Method Result Q PQL Units Run Ferric Iron (calculation) SM350016010B ND 0.10 mglL 1 Ferrous Iron SM 3500-Fe D ND 0.050 mglL 1 Nitrate - N 353.2 0.093 0.020 mgfL 1 Nitrite - N 353.2 REV 2 ND 0.020 mg/L 1 Sulfate 9056 8.7 1.0 mglL 1 PDL= Practical quantitation limit a= Detected in the method blank E= Duantitabon of compound exceeded the calibration range ND= Not detected at or above the PDL J= Estimated result< PDL and _>Mot. P= The RPD between We GC columns exceeds 40% Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W N = Recovery is out of omens Shealy Environmental Services, Inc. Page: 20 of 27 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 w .shealylab.com Level 1 Report v21 Volatile Organic Compounds by GC/MS Client: ERM-Southeast, Inc Laboratory ID: JK14063-006 Description: MW-11 Matrix: Aqueous Date Sampled:1111312008 1520 Date Received:1111412008 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260E 1 11118/2008 1848 DLB 90194 CAS Analytical Parameter Number Method Result Q PQL Units Run Bromodichloromelhane 75-27-4 8260E NO 0.50 ug/L 1 Bromoform 75-25-2 82608 ND 0.50 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260B NO 0.50 ug/L 1 Carbon tetrachloride 56-23-5 8260B NO 0.50 ug/L 9 Chlorobenzene 108-90-7 8260E NO 0.50 ug/L 1 Chloroethane 75-00-3 8260B NO 0.50 ug/L 1 Chloroform 67-66-3 8260B ND 0.50 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260B NO 0.50 - ug/L 1 Dibromochloromelhane 124-48-1 8260B NO 0.50 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 82608 .ND 0.50 ug/L 1 1,3-Dichlorobenzene 541-73-1 8260B NO 0.50 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260B ND 0.50 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260B ND 0.50 ug/L 1 1,1-Dichloroethane 75-34-3 8260B NO 0.50 ug/L 1 1,2-Dichloroethane 107-06-2 8260B NO 0.50 ug/L 1 trans-1,2-Dichloroelhene 156-60-5 8260E ND 0.50 uglL 1 1,1-Dichloroelhene 75-35-4 8260B ND 0.50 ug/L 1 cis-1,2-Dichloroethene 156-59.2 8260B 1.6 0.50 uglL 1 1,2-Dichloropropane 78-87-5 8260B NO 0.50 ug/L 1 Vans-1,3-Dichloropropene 10061-02-6 8260B NO 0.50 ug/L 1 cis-1,3-Dichloropropene 10061-01-5 8260E NO 0.50 ug/L 1 Methylene chloride 75-09-2 8260B NO 0.50 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 0.50 ug/L 1 Tetrachloroethene 127-18-4 8260B NO 0.50 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260B NO 0.50 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260B NO 0.50 ug/L 1 Trichloroethene 79-01-6 8260B 32 0.50 ug/L 1 Trichlorofluoromethane 75-69-4 8260B ND 0.50 uglL 1 Vinyl chloride 75-01-4 8260B ND 0.50 ug/L 1 Run 1 Acceptance Surrogate 9 Q % Recovery Limits 1,2-Dichloroethane-d4 115 52-138 Bromofluorobenzene 106 70-147 Toluene-d8 104 76-125 POL= Practcal quantitation limit B= Detected in the method blank E= Ouantlatian of compound exceeded the calibrator, hangs ND= Not detected at or above the POL J=Estimated result <POL and >>MDL P= The RPD between two GC columns exceeds 40% More applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a"W N= Recovery is out of Walla Shealy Environmental Services, Inc. Page: 21 of 27 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 v .shealylab.com Level 1 Repodv .1 ICP-AES Client: ERM-Southeast, Inc Laboratory ID: JK14063-006 Description: MW-11 Matrix: Aqueous Date Sampled:1911312008 1520 Dale Received: 1111412008 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3005A 6010B 1 11/18/2008 1525 MINIM 11/14/2008 2025 90012 CAS Analytical Parameter Number Method Result Q PQL Units Run Iron 7439-89-6 60108 ND 0.10 mg/L 1 PDL= Practical quantdon limit B= Detected in the method blank E=Duan@abon of compound exceeded the calibration range ND= Not detected at or above the PGL J= Estimated result 4 PDL and> MDL P= The RPD between two GC columns exceeds 40% More applicable, all sail sample analysis ere reported on a dry weight basis unless gagged with a "W N = Recovery is out of criteria Shealy Environmental Services, Inc. Page: 22 of 27 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level Report vZ1 Inorganic non-metals Client: ERM-Southeast, Inc Laboratory ID: JK14063.007 Description: MW-14 Matrix: Aqueous Dale Sampled:1111312008 1315 Dale Received: 11/1412008 ' Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Ferric Iran ) 1 11/18/2008 1530 MNM 1 (Ferrous Iron) SM 5 11/14/2008 2343 PMM 90189 1 (Nitrate - N) 353.2 1 11/15/2008 1046 RLM 90048 1 (Nitrite - N) 353.2 REV 2 1 11/15/2008 1046 RLM 90045 1 (Sulfate) 9056 1 11/21/2008 1843 DAS 90485 CAS . Analytical Parameter Number Method Result Q PQL Units Run Ferric Iron (calculation) SM350016010B 1.6 0.10 mg/L 1 Ferrous Iron SM 3500-Fe D 5.4 0.25 mg/L 1 Nitrate -N 363.2 ND 0.020 mg/L 1 Nitrite - N 353.2 REV 2 ND 0.020 mg/L 1 Sulfate 9056 24 1.0 mg/L 1 PQL= Practical quantanion limit 8= Detected in the method blank E= Quantitaticn of compound exceeded the calibration range ND= Not detected at or above the PQL J=Estimated result <PQL and >MDL P= The RPD between two GC columns exceeds 40% More applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' N = Recovery is cut of crude Shealy Environmental Services, Inc. Page: 23 of 27 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 wwvy.shealylab.com Level 1 Report v2.1 Volatile Organic Compounds by GC/MS Client: ERM-Southeast, Inc Laboratory ID: JK14063.007 Description: MW-14 Matrix: Aqueous Date Sampled:1111312008 1315 Date Received: 11114/2008 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260E 1 11/18120081909 DLB 90194 • CAS Analytical Parameter Number Method Result Q PQL Units Run Bromodichloromethane 75-27-4 8260B ND 0.50 ug/L 1 Bromoform 75-25-2 8260B ND 0.50 uglL 1 Bromomethane (Methyl bromide) 74-83-9 8260B NO 0.50 ug/L 1 Carbon tetrachloride 56-23-5 8260B NO 0.50 ug/L 1 Chlorobenzene 108-90-7 8260B NO 0.50 ug/L 1 Chloroelhane 75-00-3 8260B ND 0.50 ug/L 1 Chloroform 67-66-3 8260B ND 0.50 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260B NO 0.50 ug/L 1 Dibromochloromethane 124-48-1 8260E NO 0.50 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260B ND 0.50 ug/L 1 1,3-Dichlorobenzene 541-73-1 8260B ND 0.50 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260B NO 0.50 ug/L 1 1,4-1)ichlorobenzene 106-46-7 8260B ND 0.50 ug/L 1 1,1-Dichloroethane 75-34-3 8260B NO 0.50 ug/L 1 1,2-Dichloroethane 107-06-2 8260E NO 0.50 ug/L 1 trans-1,2-Dichloroethene 156-60-5 8260B NO 0.50 ug/L 1 1,1-Dichloroethene 75-35-4 8260E 0.55 0.50 ug1L 1 cis-1,2-Dichloroethene 156-59-2 8260E 3.0 0.50 uglL 1 1,2-Dichloropropane 78-87-5 8260B NO 0.50 ug/L 1 trans-1,3-Dichloropropene 10061-02-6 8260E ND 0.50 ug/L 1 cis-1,3-Dichloropropene 10061-01-5 8260E ND 0.50 ug/L 1 Methylene chloride 75-09-2 8260B NO 0.50 ug/L 1 1,1,2,2-Tetrachloroethane . 79-34-5 8260E ND 0.50 ug/L 1 Tetrachloroethene 127-18-4 8260E ND 0.50 ug/L 1 1,1,1-Tdchloroethane 71-55-6 8260B NO 0.50 ug/L 1 1,1,2-Tdchloroethane 79-00-5 8260B NO 0.50 uglL 1 Trichloroethene 79-01-6 8260B 39 0.50 ug/L 1 Trichloro0uoromethane 75-69-4 8260B NO 0.50 ug/L 1 Vinyl chloride 75-01-4 8260B NO 0.50 ug/L 1 Run 1 Acceptance Surrogate 9 Q % Recovery Limits 1,2-Dichloroethane-d4 112 52-138 Bromofluorobenzene 106 70-147 Toluene-d8 102 76-125 PQL = Practical quantitalion limit B = Detected in the mehmtl blank E = Quantization or compound exceeded the calibration range ND= Not detected at or above the PDL J=Estimated result <PQL and, MDL P= The RPD between two GC columns exceeds 40% Where applicable, all soil sample analysis are teponed on a dry weight basis unless gagged with a'W N = Recovery is out of cabana Shealy Environmental Services, Inc. Page: 24 of 27 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Reponv2.1 ICP-AES Client: ERM-Southeast, Inc Laboratory ID: JK14063.007 Description: MWA4 Matrix: Aqueous Date Sampled:11/1312008 1315 Date Received: 11/14/2008 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3005A 6010E 1 11/18/20081530 MNM 11/14/20082025 90012 CAS Analytical Parameter Number Method Result Q PQL Units Run Iron 7439.89.6 6010B 7.0. 0.10 mg1L 1 PQL= Practical quanlitalion limit B= Detected in the method blank E= QuarMation of compound exceeded the cahlarmon range No= Not detected at or above Me PGL J= Estimated result< PQL and MDL P= The RPD between we GC columns exceeds 40% Mere applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a -W' N = Recovery is out of Were Shealy Environmental Services, Inc. Page: 25 of 27 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Volatile Organic Compounds by GC/MS Client: ERMSoutheast, Inc Laboratory ID: JK14063-008 Description: DUPLICATE Matrix: Aqueous Date Sampled:1Ill 312008 Date Received: 1111412008 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B 1 11/18/20081930 DLB 90194 Parameter CAS Analytical Number Method Result Q PQL Units Run Bromodichloromethane 75-27-4 8260E ND 0.50 ug/L 1 Bromoform 75-25-2 8260B ND 0.50 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260B ND 0.50 ug/L 1 Carbon tetrachloride 56-23-5 8260B ND 0.50 ug/L 1 Chlorobenzene 108-90-7 8260E ND 0.50 ug/L 1 Chloroelhane 75-00-3 8260B ND 0.50 ug/L 1 Chloroform 67-66-3 8260B ND 0.50 ug/L 1 Chloromethane (Methyl chloride) 74-37-3 8260B ND 0.50 uglL 1 . Dibromochloromelhane 124-48-1 8260B ND 0.60 uglL 1 1,2-Dibmmoethane (EDB) 106-93-4 8260B ND 0.50 uglL 1 1,3-Dichlorobenzene - 541-73-1 8260B ND 0.50 uglL 1 1,2-Dichlorobenzene 95-50-1 8260B ND 0.50 uglL 1 1,4-Dichlorobenzene 106-46-7 82608 ND 0.50 ug/L 1 1,1-Dichloroethane 75-34-3 8260B ND 0.50 uglL 1 1,2-Dichloroethane 107-06-2 8260B ND 0.50 ug/L 1 trans-1,2-Dichloroethene 156-60-5 8260E ND 0.50 ug/L 1 1,1-Dichloroelhene 75-35-4 8260B ND 0.50 ug/L 1 cis4,2-Dichloroethene 156.59.2 8260B 40 0.50 ugli- 1 1,2-Dichloropropane 78-87-5 8260B ND 0.50 uglL 1 trans-1,3-Dichloropropene 10061-02-6 8260B ND 0.50 ug/L 1 cis-1,3-Dichloropropene 10061-01-5 8260B ND 0.50 ug/L 1 Methylene chloride 75-09-2 8260B ND 0.50 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 0.50 uglL 1 Tehachloroethene 127-18-4 8260E ND 0.50 ug/L 1 1,1,1-Tichloroethane 71-55-6 8260B ND 0.50 uglL 1 1,1,2-Trichloroethane 79-00-5 8260B ND 0.50 ug/L 1 Trichloroethene 79-01-6 8260B 180 0.50 ug/L 1 Tdchlorofluoromethane 75-69-4 8260B ND 0.50 uglL 1 Vinyl chloride 75-01-4 8260B ND 0.60 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 113 52-138 Bromofluorebenzene 106 70-147 Toluene-d8 103 76-125 POL= Practical quanti[ation limit B= Detected in the method blank E= Guantitation of compound exceeded the calibration range N D = Not detected at or above the POL J= Estimated result< POL and >MDL P= The RPO between two GC columns exceeds 40% Where applicable, all soil sample analysis are reported on a dry weight basis unless fagged with a N= Recovery is out of criteria Shealy Environmental Services, Inc. Page: 26 of 27 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 vnvw.shealylab.cam Level 1 Report v2.1 Volatile Organic Compounds by GC/MS Client: ERM-Southeast, Inc Laboratory ID: JK14063-009 Description: TRIP BLANK Matrix: Aqueous Date Sampled:1111412008 1525 Date Received: 1111412008 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B 1 11/18/2008 1639 DLB 90194 CAS Analytical - Parameter Number Method Result - Q PCIL Units Run Bromodichloromelhane 75-27-4 8260B NO 0.50 uglL 1 Bromoform 75-25-2 8260B NO 0.50 ug/L 1 Bromomelhane (Methyl bromide) 74-83-9 8260B NO 0.50 ug/L 1 Carbon tetrachloride 56-23-5 8260B NO 0.50 ug/L 1 Chlorobenzene 108-90-7 8260B NO 0.50 ug/L 1 Chloroethane 75-00-3 8260B NO 0.50 ug/L 1 Chloroform 67-66-3 8260B NO 0.50 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260B NO 0.50 ug/L 1 Dibromochloromethane 124-48-1 8260B NO 0.60 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260E NO 0.50 ug/L 1 1,3-Dichlorobenzene 541-73-1 8260B NO 0.50 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260B NO 0.50 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260E NO 0.50 ug/L 1 1,1-Dichloroethane 75-34-3 8260B NO 0.50 ug/L 1 1,2-Dichloroethane 107-06-2 8260E NO 0.50 ug/L 1 Vans-1,2-Dichloroethene 156-60-5 8260B NO 0.50 ug/L 1 1,1-Dichloroethene 75-35-4 8260B NO 0.50 ug/L 1 cis-1,2-Dichloroethene 156-59-2 8260D NO 0.50 ug/L 1 1,2-Dichloropropane 78-87-5 8260B NO 0.50 ug/L 1 trans-1,3-Dichloropropene 10061-02-6 8260E NO 0.50 ug1L 1 cis-1,3-Dichloropropene 10061-01-5 82603 NO 0.50 ug/L 1 Methylene chloride 75-09-2 8260E NO 0.50 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260B NO 0.50 ug/L 1 Tetrachloroethene 127-18-4 8260B NO 0.50 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260B NO 0.50 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260B NO 0.50 ug/L 1 Trichloroethene 79-01-6 8260B NO 0.50 ug/L 1 Trichlorofluoromethane 75-69-4 8260B NO 0.50 ug/L 1 Vinyl chloride 75-01 4 8260E NO 0.50 ug/L 1 Runt Acceptance Surrogate q % Recovery Limits 1,2-Dichloroethane-d4 110 52-138 Bromofluorobenzene 103 70-147 Toluene-d8 103 76-125 POL = Practical cluan@ation limit 8 = Detected in the method blank E = Guantitation of compound exceeded the calibration range ND= Not detected at or above the POL J= Estimated result c POL and _>MDL P= The RPO between two GC columns exceeds 40% Mere applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W N= Recovery is out of cdleria Shealy Environmental Services, Inc. Page: 27 of 27 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Reponv2.1 s 3 f�1,11-N SHEAL:Y ENVIRONMENTAL SERVICES, INC. 1�,} 5 .[106Van:ago puinl Dnve Chain of Custody Record Wesi'Cotumhia,. South Car011na 29172 'v" Telophono No. (609) 791.97DO fax No: (803) 701-9111 Number 75209 1� 9A'a:i is Na. E-Mv 0- Ain, 1 o no:Vass 'S.scya'er s`� e'u:':a f K_ IGir1� I4:}b.'1 Nn CR}• GEfRF+�Gaf1T` s,�.a - In CcOs :$2Z�o Arurys't (A.rracl tisldmo!a ycara ra nttoedJ l =: • 1,m' W- 0 � Lc;fb. - V✓� �.7 a&a& ffmi '>: o! :aiitiNG B. Pmur:atitl ryGa Svml3 rDlva q.'.vn Daft JiL I ,'CnfehnYlurnsNi eaw?ewYde cmNunvfsn am P.,YJ i - fc 4 ? 9 / R•uwU: L_abr llA w-3 1 17 I +5 xX X X mw - 5 11=is . 15 MW-15 16 xxxxXX Mw— 1 •15 I .15 AXAX X X - f273 1 16 X XXX x 'XXXXXx w- 15 XXXXX 77z)? 31,AAI1Z, Z�tb kusrtl fa'��u!-ifrtry - - $1um:in 6.3rx.'vr Nam-AXsvy:ei&re h, . f 7.b>Hrean7 17.fGmrrvdb nswrwr ❑Aue;:n -'Un,r .. I"a=u V6icl 'j r%�nby:jb rv;k: s:'cn`vm+ar�,u•rYir�:aro �rea'ic.. iimratp.�rtl.rmp f?uf�ivpn (fYtir lvn gyrr�wdrcy�r.•n"'!n•F�µ+eare77AT.7 � Req:n%enrdvG{ },:µrrJj•) � I Siiv r,1 rl r7�^:(.�mJ119 1 R 49 :nF D&V 'mq LN YAY LWb' i T'w 6J . Y-P a nam v'a aW-Mru �/ . CAXr vrS• L19 D�[O.YLY Raaau'a.^aiicu lUsol �. hu knF•i�A R<a ,vr Tcap , 10 AJSififHUllDAE l'1H17b.R Ya;.lY.t+RsnmM wYK�t'+rivV xr'th SanmSitgl; A:.S'1: F4zKCCur.; Cr.}•ryr M CVuilalf:wwrD]r: FgD-0r? G'ies.N Lhtfa.Cbi�-fL T Z n She -A, I',viromnrn:al Smnas, Inc. pnn�men; Kcmb:r F-.iD-Ois Rc'"'M h;mn6_r E ?ze�a'I Replaces Da[::99�??:; S Effectiv: Dar,: DS 29:0 Sample Receipt Ciiecklisl(SRC:) Client 14 Cooler Inspected byid te: F! ( f ii. 16 Ur 4: .)". I EI D r� N9eans of receipt: Q"'SESI ❑ Client ❑ UPS ❑ FedEx ❑ Airbumc cep ❑ Othc: Yc4 ❑ No NA I. Wcrcclisrndyseals resent onthecooler? Yes No NP. 3. if cus[odV seals were PTCSCnl. •::err Ihry inlaeL and unhroken? Cooler M.-tcmperature upon muuipl 1.7 'C I C aC i 'C Method. EKTemperatuj� Blank ❑ Against Bottles 1 Method ofcoolant: • [,.j ICI Ice ❑ Blue Ice ❑ Dry [ce ❑ None If response is No for Yes for I4.:5. 16). an ex lanatienlicsohniun nu!st lie provided. Yes ❑ No ❑ \A l( i 3. rf temperature of any cooler exceeded 6.0'C, was PMjccL Mutmgcr notified? PM notiticd by SRC, phone; note (circic one), outer: . (For coolers received via commercial courier. PMs we to be notified inintediateh'. Yzs ❑ \u N:\ ± 4, fs rile commercial courier-i aaeking slip attached to this farm? Yes ❑ , No l NA ] 5. Were ropercu;todvorocedures(relir, ui:hedireccived) followed? Yes ❑ \u ❑ NA ❑ 1 6. Were smn le lDs listed? ' Fes ,o ❑ NA ?- Was collection da(c & time listed? Yes 0 No ❑ NA 3- Were (ells In be performed listed on :1r_ COC or was quote Tprovided? No NA ❑. 9. Did all samples arrive in the proper C(pn[ailiers fnr each test? _Yes Yes No I dA ❑ ; 0. llid all container label informstibn (ID, date. time) azee with COM ❑ l NA _ 1, Did all containers arrive in eood condition (uobroken. lids oil, etc.)? Yes Na N4 ❑ :. Was adequate. le voiumaavailable? Fes ❑ Nu ' E4 I NA -". Were all samples received within ii the, hoidin_t fine or-4 hours, whichever ❑ - came; first? 14. Were any samples container missing? N'A lhv NA I <i ! N.\ ❑ IJ. \Pere rhere an •excess samples utv )istc5 nn COC^ lb. \Vere'nuhblcs ^resent-"pA-size" rYi'or C+mm in diameter) in any VOA ❑ v:als'i L'Ne ❑ Y_s ❑ Np I NA ❑I''y I?. \\'crud) metzls+OKGMENL'ntaricnt Sam lea receiver- at a nl I of <=� Yea No NA IN IS. \\'ere all C}'Anlde alld'O[ snlhne ampiCs reCClcCd aI aytl i?" 19. \\'ere all appli ibleN'113; T1CN'cyanide phc ohBN.4:ccsl•'pC3.Le v (<0 _ut:.'L) and toxicity (<O.Imr U samples free of residual chlorine? Yes ❑ No ❑ NA ❑u Yes ❑ 'No ❑ [ 20, Wcrc collection temaeratures da.:umentt�d on the COC fxNC snnttiles7 1 _NA Sample Prewrvation (Nlust be c ptmpleted for any samples) incol. ectly prescn�ed or wish hcadspace.) Samplefs) were received incorrectly preserved -and were adjusted accordingly in sample receiving. with (H-SO4,HNO_j,HCl,NaQlD with die SR E(number) Sam 1e(s'I Lvem'received with buL•bles = 6 mm a diameter. Srnnple(s} z�•ere received wi'h'fRC?0.2 mg+L for NH3" TFV;cv:tnidr.'BNA% ..strPCf3Jhero. Toxicity sau:ple(s) were received a'itlt FFC = 0. i me'L and were analyzed hV method 3305. Corrective Action taken, if necrcxarv: Was client notified: Yes ❑ No ❑ S Sl cololoyee: _- _ Ctimmcnts- Did client respond: Datu of response: Ye's ❑ No ❑ Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 w .shealylab.ccm Level 1 Report v2.1