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Home My WebLink AboutWQ0000485_Monitoring - 03-2024_20240424Monitoring Report Submittal Permit Number#* WQ0000485 Name of Facility:* Darling Ingredients - Rose Hill Month: * March Year: * 2024 Report Information Type* Upload Document* GW-59 scan 2024-03 GW-59 3.56MB Grou ndwaterComplianceReportForm-WQ0000485 - DIRH.pdf PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Confirmation Email Address: * corey.lanier@darlingii.com Name of Submitter: * Corey Lanier Signature: Date of submittal: 4/24/2024 This will be filled in automatically Initial Review Reviewer: Wanda.Gerald Is the project number correct?* WQ0000485 Is the monitoring report accepted?* Yes NO Regional Office* Wilmington Reviewer: _anonymous Review Date: 5/13/2024 DARLING Addib- INGREDIENTS April 24, 2024 Division of Water Resources Attn: Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Re: Ground Water Quality Monitoring Report (GWQMR) Darling Ingredients — Rose Hill Permit WQ0000485 To whom it may concern, Please find enclosed the Groundwater Quality Monitoring Compliance Report for Surface Irrigation for the month of March 2024 for our Rose Hill Division. Should you require any additional information or wish to discuss this matter, please feel free to contact me at 910.289.2083 x 25119. Sincerely, Lar^ry Holt ' General Manager cc: DI Regional Corporate Office GW-59A COMPLIANCE REPORT FORM Permit # W00000485 (Submit one each monitoring period with GW-59 forma.) I Enter date monitoring results were due. (0413012024) Will this monitoring report (GW-59 and GW-59Af be submitted after the established due date? No 2 Was any required information missing on the GW-59 report forms? No IF the answer to question 1 or 2 is "YES'; list in the space provided below the well identification number(s) and explain the ,problems encountered in obtaining the required information. MW-8A was damaged by farm equipment and is scheduled to be closed and replaced by Register Well Co, INC; moving the replacement well 10' due North per DEQ direction 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing identification plate, area overgrown, etc.)? If the answer is "Yes ", contact the Regional Office for guidance. No 4 Are any monitored constituents equal to or above the established standards? YES If the answer to question 4 is "NO", skip to section B. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below., SEE ATTACHED GROUNDWATER MONITORING WELL 2 YR EXCEEDANCE HISTORY REPORT 5 IFor the constituents identified in question 4 above, have standards been exceeded previously for the same oonstituent(s) in the same well(s) in the last two years? YES If the answer to question 5 is "NO" skip to section B. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, wricentration(s) reported, and sample collection date for each occurrence (for the last two years). SEE ATTACHED GROUNDWATER MONITORING WELL 2 YR EXCEEDANCE HISTORY REPORT 6 .Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES N the answer is "YES", a groundwater qualify problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the Regional Office. 7 Is the perrnittee implementing previously approved actions required by the Division involving this groundwater quality problem? YES If the answer to question 7 is 'YES', describe those actions in the space provided below. If the answer to question 7 is "NO" contact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation, fines, and/or enatties. Additional monitoring was performed to identify constituents of TOC in MW No.9. The facility has been communicating with Mr. Geoff Kegley in the Wilmington Regional Office. 8 The person completing this portion (GIN--59A) of the monitoring report should sign below and submit this form with G W-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby acknowledge that the above information was evaluated and the information submitted in this report (Compliance Report GW-59A) is true and complete to the best of my knowledge. &�, fLGk .2L/12-:�Z Sjgnatufe of Po ittee (or Authorized Agent) Date GW-59A 12/8/2003 Darling Ingredients - Rose Hill (WQ0000485) Groundwater Monitoring Well 2 Year Exceedance History Report TDS 500 10A 12B 14A March-24 795 549 1420 November-23 793 1010 July-23 816 1270 March-23 804 1310 November-22 833 944 July-22 772 1280 March-22 783 1100 November-21 801 1230 pH 6.5-8.5 1 7A 8A 9 10A 11A 12B 13A 14A March-24 5.20 5.00 4.80 5.80 3.82 4.80 4.60 4.80 5.30 November-23 5.20 3.66 4.60 5.90 3.55 4.70 3.91 4.70 5.10 July-23 5.20 5.30 5.10 6.30 3.70 5.40 4.60 4.70 4.70 March-23 6.40 3.86 4.50 4.10 4.50 4.20 4.80 5.00 November-22 5.60 3.86 4.20 6.00 3.67 4.10 3.70 4.40 4.70 July-22 6.40 5.10 5.30 4.20 4.60 4.00 5.10 4.90 March-22 4.70 4.60 4.60 4.40 4.20 4.70 5.20 November-21 4.30 4.50 +--14.00 4.30 4.20 4.20 5.00 TOC 10 9 March-24 39.1 November-23 30.6 July-23 46.9 March-23 33 November-22 27.6 July-22 45.1 March-22 34.9 November-21 26.4 Chloride 250 10A 14A March-24 305 375 November-23 322 316 July-23 337 361 March-23 350 November-22 305 350 July-22 261 356 March-22 294 325 November-21 353 Sulfate 250 14A March-24 494 November-23 July-23 357 March-23 375 November-22 July-22 287 March-22 277 November-21 322 £LOZ/8'Aa2i 69-MJ (IuabV pazuoUnV ao) aaullwad 10 am;eubiS aan) JO;uud ase81d - aj;)1 pue aweN (;usbV pazuoglny jo) aagiwJad r1 J915eueINIWaua0-IIOH tuiel %lenouaGN OOA 1/6w :sOO/� Ielol luanl l3 /6w :sOOA Ie101 luenl;ul :(spodeN qel Uoe�1V) �(lu0 swa;s�(S uol;elpawa�l god # Pallaw ' 1/6n L90W 19�101N -!N 1/6w 8'0 9z900 N se Mil # poy;aw, ' 116n 99oLo asauebueW - uw (lelol'ua60j1!N eiuowwy'N seEHN'ua608N e!uowwV) # POUIaw , 1/6w LZ600 wnlsou6eVq - 61IU 1/6w Z'0> moo eluowwy lelol 00OZ9 INS # POUIaw ' :ZEL8L OOA 1/6w LS600 wnlsselod ->1 soyWT+ 96000 aouelonpuoO oi4loadc (0) ON ❑ (0) saA ■ ZpopegV podaN qel 1/6n 0o6LL AlnojaW - 61-1 1/6w 6L 9v600 ale;InS ('1210d3M EIV1 H3V11V '# poy;aw pue;sa; ApoadS) 1/6n 917ow ual - ad 1/6n o£LZ£ Ioua4d (O1dH 'SW/O0 'O0 Aq) :SOINVOM0 1/6w zt mo jaddoO - no 1/6w Z99oo sllO pue aseaJ0 1/6n v£0Lo Ielol :wnlwayO 1/6n zoo oluesay 1/6n Lzuo wnlwpeO - PO 1/6w 9 0600 aplJOIgD 1/6w 9L600 wnloleO - eO 1/6w Z, I, 08900 001 1/6n LooLo wnlaeg - eg sllun 0Z,9 £ovoo (qel) Hd 1/ w 8£,9 wnlpoS 1/6w 9oLLo wnulwnlV - IV 1/6w WWI, 00£OL 1e101:spIIOS paAlossl( :(s}IuN uollealuaouoO pue spunodwoO /4ioedS) jagjO 1/6w L090L alegdsogdoq:po (saldwes p!gjnl ANONJo; poglaw NdW asn :aloN) 1/6w 80'0 99900 d se lelol :sn.loLIdso4d 1w006/ vo9L£ lelol JIN moploO 1/6w Z60L0 oulZ - uZ 1/6w 69'0 oz9oo N se (EON) aIMM 1w006/ 0' > 9L9L£ leoad dW :wjo;!IoO 1/6n Lgmo peal - qd 1/6w Z0,0> 9L900 N se (zON) aIPM 1/6w 9££oo (]00 •su01;ea;ua0u03 IepIOIIO3 pue paAIOSslp;oal;aa pinoLis sanlen:310N SN313WVHVd 176#0M(] 'ON uo1le01;l}JaO 'oul 's;slwaLIO Ie;uawuonnu3 :aweN kolejoge-I t7Z0Z/8Z/£0-vZ0Z/Z6/£0 :pazAleue aldwes ale(] NOIIVW80-ANI AM01"OEIV1 �'l aiaq ON SAA X :Paljlploe play PUB ON S3A X :paaa;ll;un poloalloo ajem sle;aw joi sal weS I—Jloago aealO aouejeaddV suolle6 O g :6ulldwes ajolaq palleq/padwnd aalemn o awnIOA '6ulldwes auON :99000 JopO .11 :uollena13 'd'W aAllela2i aoepns puel anoge .4 LI 6 s1 lulod 6uljnseaW ;o awl; sogvgTi :v6000 -puoO -oadS 4 917,Z of '4 917'ZI, :IeAJalul pauaaJoS £-£ :9179Z9 Ianal joleM of Lylda(] le AM(3 75-7 —,,, :m000 -dwal sllun OZ-9 SH009vHd ul Z :Jalawel(] IIaM 'll 9b'Z6 4lda(] IIaM SVM :S3SAIVNV (3131d 17707/Z6/£ :paloalloo aldwes ale(] VMW :(;IwJad wa;) M39wnN al 113M 113M31 NOIlVWHO-AN1 JNI1dWVS :jagl0 ❑ dwnd leaH aoinoS jaleM ❑ I.I. :paldwes aq of sllem jo oN aweN Gl!S/uolleool IIaM 96pnlS to uolleollddV pue-I ❑ joingljlsl(] tielo2j ❑ £LI, 6-099 066) :#auogdalal aalue-j Aajoo :uosaad loeluOO :uollelpawa�j ❑ plaid AejdS X (dlz) (alels) u,,> /vaIIe0 uogedllllul :uollelpawa�l ❑ uoo6el ❑ ull n(] f(lunoO 89v8Z ON 'IIIH aso�l 43MMINOW ON139 N0I1"3dO 43111WN3d =10 3dA1 Pia lnO MollaA 69b ssaippV Alllloed JGglO S3(]dN :(IuGJa}j1P M aweN llwlad Olfl a6Jeg0s14-uON IIIH asO�J - sluG1PGJI5uI I5u1IJeG :aweN A4111oed 9ZOZ/6£/£ :ale(] uol;endx3 M700000M :jegwnN llWH3d adA_LjoAliea/o NOIlVWMO-ANl "110Vd 90£9-L09-666.au04d L496-669LZON'HE)13lVN'M31N3333IAa3S-IIVWLL9L WM0J 1210d3M 30NV11dW00 11NnONI99330HdNOI1VWMOdNI-S3ounOS mM31VMA0NOISWO • • • :9N1N011N0W A11 vn6 H31VMdNnouo S3OMnosau lVan1VN °81N3WNONIAN3 d01N3WISVd3a • • • AINO a3dVd MO -MIA NO mo=i inmenS SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Please Print Clearly or Type Facility Name: Darling Ingredients - Rose Hill Permit Name (if different): Facility Address: 469 Yellow Cut Rd. Rose Hill, NC 28458 (State) (zip) County Duplin act Person: Corey Lanier Telephone#: (910) 660-1173 Location/Site Name No. of wells to be sampled: 11 (from Permlh DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Non -Discharge UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery X Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-2 Date sample collected: 3/12/2024 FIELD ANALYSES: WAS Well Depth: 31.00 ft. Well Diameter: 2 in. pH4500HB 6.70 units Temp. 00010: 149 eC DRY at Depth to Water Level 92546: 10.8 ft. below measuring point Screened Interval: 30.15 ft. to 20.15 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 3 ft above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear here: El Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 03/12/2024-03/28/2024 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1.0 /100mL Nitrate (NO3) as N 00620 0.58 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.07 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): )issolved Solids -Total 70300 20700 mg/L Al -Aluminum o1105 mg/L Sodium 11.9 mg/L pH (Lab) 00403 6.70 units Ba - Barium 01007 ug/L TOC 00680 1 mg/L Ca - Calcium 00916 mg/L Chloride 00940 18 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 37 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? E Yes (0) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 <0 5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs. mg/L VOC Removal% Larry Holt - General Manager `--,- 1LA1J Permittee (or Authorized Aqent) Name and Title - Please print or type Siqnature of Permittee Z /2p2 (Date) GW-59 Rev 8/2013 SUBMIT FORM ON YELLOW PAPER ONLY • • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485Expiration Date: 3/31/2025 Facility Name: Darling Ingredients - Rose Hill Non -Discharge UIC Permit Name (if different): NPDES Other Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED Rose Hill, INC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery (City) (St:110) (zip) X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-4 Date sample collected: 3/12/2024 FIELD ANALYSES: WAS Well Depth: 28.93 ft. Well Diameter: 2 in. pH4500HB 7.40 units Temp o0010: 14.4 oC DRY at Depth to Water Level 82546: 1.4 ft. below measuring point Screened Interval: 28.93 ft. to 18.93 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear here: Samples for metals were collected unfiltered: X YES ❑1 NO and field acidified: X YES ElNO LABORATORY INFORMATION Date sample analyzed: 03/12/2024-03/28/2024 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.10 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 219.00 mg/L Al -Aluminum 01105 mg/L Sodium 8.4 mg/L pH (Lab) 00403 7.40 units Ba - Barium 01007 ug/L TOC 00680 0.70 mg/L Ca - Calcium o0916 mg/L Chloride 00940 <5.0 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 <5.0 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? E Yes (0) ❑ No (0) pedfic Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev.8/2013 I MIN DEPARTMENT OF ENVIRONMENTS NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISIONOFWATERRESOURCES- INFORMATIONPROCESSINGUNIT COMPLIANCE REPORT FORM 161 'MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: VY00000485 Expiration Date: 3/31/2025 Facility Name: Darling Ingredients - Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 284.58 County Duplin tc„y) (State) rr:. X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-7A Date sample collected: 3/12/2024 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 5.00 units Temp. 000lo: 15.8 °C DRY at Depth to Water Level 82546: 5.2 ft. below measuring point Screened Interval: 16 ft. to 6 ft. Spec. Cond. mm: "Mhos time of sampling, Measuring Point is 2.42 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None checl� Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear/Tan here: Samples for metals were collected unfiltered: X YES NO and field acidified: X YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 03/12/2024-03/28/2024 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100ml- Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.08 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 122.00 mg/L Al - Aluminum 01105 mg/L Sodium 24.4 mg/L pH (Lab) 00403 5.00 units Ba - Barium 01007 ug/L TOC 00680 0.7 mg/L Ca - Calcium 00916 mg/L Chloride 00940 83 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 26 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? i Yes (0) ❑ No (0) Specific Conductance 00095 "Mhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOGs: mg/L Effluent Iota) VOCs: TIIY�L vkj� rceiriuvai,o Larry Holt - General Manager Perrnittee (or Authorized Agent) Name and Title - Please print or type DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807.6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: VVQO000485 Expiration Date: 3/31/2C25 Facility Name: Darling Ingredients - Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill NC 28458 County Duplin (city) (Stale) (zip) X Spray Field ❑ Remediation- Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Field 5 - damaged by farm equip / to replace No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-8A Date sample collected: 3/12/2024 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH45ooH8 4.80 units Temp. 000lo: 15.1 °C DRY at Depth to Water Level 82546: 5.9 ft. below measuring point Screened Interval: 16 ft. to 6 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 2.5 ft. above land surface Relative M.P. Elevation: ft. Odor 00065: None sampling, Volume of water pumped/bailed before sam 0 5.0 gallons Appearance Clear/Tan check Samples for metals were collected unfiltered: X YES LJ NO and field acidified: X YES ❑ NO here:❑ LABORATORY INFORMATION Date sample analyzed: 03/12/2024-03/28/2024 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1.0 /100mL Nitrate (NO3) as N 00620 0.58 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.06 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 157.00 mg/L Al - Aluminum ol1o5 mg/L Sodium 1.21 mg/L pH (Lab) 00403 4.80 units Ba - Barium 01007 ug/L TOC 00660 0.70 mg/L Ca - Calcium 00916 mg/L Chloride 00940 <5 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 24 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? 0 Yes (0) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 76732: method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOGs: mg/L trrtuent I oral vuus: ll,ylL V Vl✓ r[CIIIVVO170 Larry Holt - General Manager Permittee (or Authorized Agent) Name and Title - Please print or type • • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: • • • DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Darling Ingredients - Rose Hill Non -Discharge UIC Permit Name (if different): NPDES Other Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin tcay> (Slate) (zip) X Spray Field ❑ Remediation Contact Person Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): Ill Date sample collected: 3/12/2024 FIELD ANALYSES: WAS Well Depth: 13.73 ft. Well Diameter: 2 in. pH4500HB 5.80 units Temp. 000lo: 13 °C DRY at Depth to Water Level 62546: 3.8 ft. below measuring point Screened Interval: 13.73 ft. to 3.73 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 3.80 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear/Tan here: Samples for metals were collected unfiltered: X YES NO and field acidified: X YES NO LABORATORY INFORMATION Date sample analyzed: 03/12/2024-03/28/2024 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1.0 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.11 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 151.00 mg/L Al - Aluminum 01105 mg/L Sodium 2.65 mg/L pH (Lab) 00403 5.80 units Ba - Barium 01007 ug/L TOC oosso 39.1 mg/L Ca - Calcium 00916 mg/L Chloride 00940 6 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 8 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? E Yes (0) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 1.4 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent t otal vucs: mg/L t-muent l ocal vow. tltylL ,O Larry Holt - General Manager Permittee (or Authorized Agent) Name and Title - Please print or type DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485Expiration Date: 3/31/2025 Facility Name: Darling Ingredients - Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin (City) (State) (zp) X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-10A Date sample collected: 3/12/2024 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 3.82 units Temp. 000ic 14.3 °C DRY at Depth to Water Level 82546: 3.8 ft. below measuring point Screened Interval: 16 ft. to 6 ft. Spec. Cond. 00094: l_Mhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 000a5: None checii, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear here: Samples for metals were collected unfiltered: X YES NO and field acidified: X YES M NO LABORATORY INFORMATION Date sample analyzed: 03/12/2024-03/28/2024 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.04 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.10 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): )issolved Solids:Total 70300 795.00 mg/L Al -Aluminum 01105 mg/L Sodium 119 mg/L pH (Lab) 00403 3.82 units Ba - Barium 01007 ug/L TOC oo68o 3.6 mg/L Ca - Calcium 00916 mg/L Chloride 00940 305 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 156 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? E Yes (0) ❑ No (0) Specific Conductance 00095 p.Mhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 0.40 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 0.80 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Innuent t otal vvus: I11911— CIIIUCIIt I UU9 Vvw. 1.1y1 L- - Larry Holt - General Manager Permittee (or Authorized Agent) Name and Title - Please print or type Signature of DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485Expiration Date. 3,13112025 Facility Name: Darling Ingredients - Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin (Orly) (Stale) (Z!F.: X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-11A Date sample collected: 3/12/2024 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 4.80 units Temp. oo01c 1a.s °C DRY at Depth to Water Level 82546: 4.8 Screened Interval: 16 ft. to 6 ft. Spec. Cond. 00094: uMhos time of sampling, Measuring Point is 3.3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None checl Volume of water pumped/bailed before sampling 5.0 gallons Appearance Clear ._, here: Samples for metals were collected unfiltered: X YES NO and field acidified: X YES NO LABORATORY INFORMATION Date sample analyzed: 03/12/2024-03/28/2024 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1.0 /100mL Nitrate (NO3) as N 00620 0.41 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.05 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 489.00 mg/L Al - Aluminum 01105 mg/L Sodium 60.3 mg/L pH (Lab) 00403 4.80 units Ba - Barium 01007 ug/L TOC 00680 2.30 mg/L Ca - Calcium 00916 mg/L Chloride 00940 129 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS. HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 163.0 mg/L Hg - Mercury 71900 ug1L Lab Report Attached? Yes (0) ❑ No(0) Specific Conductance 00095 uMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 <0.50 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Inruent I otal vuL;s: mgrL crnuem I olds vv1s. I.V" • r Larry Holt - General Manager Pennittee (or Authorized Agent) Name and Title - Please print or type DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Darling Ingredients - Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin (state) (zip) X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-12B Date sample collected: 3/12/2024 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB: 4.60 units Temp. 000lo: 15.1 °C DRY at Depth to Water Level 82546: 5.5 ft. below measuring point Screened Interval: 20 ft. to 10 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear here: Samples for metals were collected unfiltered: X YES NO and field acidified: X YES M NO LABORATORY INFORMATION Date sample analyzed: 03112/2024-03128/2024 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.09 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.90 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 549.00 mg/L Al - Aluminum 01105 mg/L Sodium 68.7 mg/L pH (Lab) 00403 4.60 units Ba - Barium 01007 ug/L TOC 00680 2.10 mg/L Ca - Calcium 00916 mg/L Chloride 00940 135 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 183 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? 0 Yes (0) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese o1o55 ug/L , method # TKN as N 00625 0.60 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent 1 otal VUGs: mg/L Effluent I otai Vvus: 111y'L V., 1. Larry Holt - General Manager Pennittee (or Authorized Agent) Name and Title - Please print or type DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please PnnfCleadyorType PERMIT Number: VVO0000485 Expiration Date: 3/31/2025 Facility Name: Darling Ingredients - Rose Hill Non -Discharge UIC Permit Name (if different): NPDES Other Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, INC 28458 County Duplin (:iy) (state) (Z,p) X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-13A Date sample collected: 3/12/2024 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 4.80 units Temp. 000lo: 15.7 oC DRY at time of Depth to Water Level 82546: 5.5 ft. below measuring point Screened Interval: 16 ft. to 6 ft. Spec. Cond. 00094: itMhos sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Mikly White here: Samples for metals were collected unfiltered: X YES I —I NO and field acidified: X YES NO LABORATORY INFORMATION Date sample analyzed: 03/1212 )24-03/28/2024 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.05 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.14 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 30.00 mg/L Al - Aluminum 01105 mg/L Sodium 4.43 mg/L pH (Lab) 00403 4.80 units Ba - Barium 01007 ug/L TOC 00680 0.70 mg/L Ca - Calcium 00916 mg/L Chloride 00940 <5 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 7.00 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? E Yes (0) ❑ No (0) Specific Conductance 00095 uMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.20 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 <0.50 mg/L Ni - Nickel 01067 ug/L method # For Remedlation Systems Only (Attach Lab Reports): mnuent I oial vuL s: fnyrl- C111=11t l vtnl V v�O- v - �•••�- Larry Holt - General Manager Permittee (or Authorized Agent) Name and Title - Please print or type DEPARTMENT OF ENVIRONMENT B NATURAL RESOURCES GROUNDWATER QUALITY MONITORING:WN DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date 3/31/2025 Facility Name: Darling Ingredients - Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin (city) (stag) (4) X Spray Field ❑ Remediation Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-14A Date sample collected: 3/12/2024 FIELD ANALYSES: WAS Well Depth 16 ft. Well Diameter: 2 in. pH4500HB 5.30 units Temp. 000lt 16.2 °C DRY at Depth to Water Level 82546: 3.5 ft. below measuring point Screened Interval: 10 ft. to 2.5 ft. Spec. Cond. 00094: uMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear /Tan here:[:] Samples for metals were collected unfiltered: X YES 1- i NO and field acidified: X YES NO - LABORATORY INFORMATION Date sample analyzed: 03/12/2024-03/28/2024 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0 02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1.0 /100mL Nitrate (NO3) as N 00620 3.71 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.16 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 1420.00 mg/L Al - Aluminum o1105 mg/L Sodium 188 mg/L pH (Lab) 00403 5.30 units Ba - Barium 01007 ug/L TOC oomo 5.60 mg/L Ca - Calcium oo916 mg/L Chloride 00940 375 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 494 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? N Yes (0) ❑ No (0) Specific Conductance 00095 uMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.20 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 8.00 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): mtluent loyal vucs: m91L r-nluern tutor vwb. ...V" .__ Larry Holt - General Manager Permittee (or Authorized Agent) Name and Title - Please print or type ro"07 k Environmental Chemists, Inc. enviroChem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info(u environmentalchemistscom Darling Ingredients - Rose Hill Date of Report: Mar 28, 2024 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2024-06051 Project ID: March - Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 24-14335 Site: MW-1 3/12/2024 10:25 AM Water jcb/envirochem Test Method Results Date Analyzed Color Color Clear 03/12/2024 Depth to water, ft. Depth to Water, Ft. 3.3 feet 03/12/2024 Sodium EPA 200.7, Rev 4.4,1994 5.38 mg/L 03/17/2024 Sulfate EPA 300.0, Rev. 2.1, 1993 79 mg/L 03/14/2024 Ammonia Nitrogen EPA 350.1, Rev. 2.0,1993 < 0.2 mg/L 03/19/2024 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/12/2024 Odor Qualitative None 03/12/2024 Total Dissolved Solids (TDS) SM 2540 C-2015 138 mg/L 03/13/2024 Temperature SM 2550 B-2010 15.1 C 03/12/2024 pH SM 4500 H B-2011 5.2 units 03/12/2024 Total Phosphorus SM 4500 P (F-H)-2011 0.08 mg/L 03/20/2024 Total Organic Carbon (TOC) SM 5310 B-2014 1.2 mg/L 03/13/2024 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 03/12/2024 Chloride SM4500 Cl E-2011 6 mg/L 03/15/2024 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev 2.0, 1993 < 0.02 mg/L 03/12/2024 Nitrate Nitrogen Subtraction Method 0.59 mg/L 03/28/2024 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 3512, Rev. 2.0, 1993 0.8 mg/L 03/20/2024 Total Nitrogen Total Nitrogen 1.4 mg/L 03/28/2024 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 24-14335A Site: MW-1 3/12/2024 10:25 AM 'Water jcb/envirochem Test Method Results Date Analyzed Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0, 1993 0.59 mg/L 03/15/2024 Report #:: 2024-06051 Page 1 of 11 [env7irochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 71.0 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax i nfoC-envi ronmen talchemists.com Darling Ingredients - Rose Hill Date of Report: Mar 28, 2024 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2024-06051 Project ID: March - Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 24-14338 Site: MW-2 3/12/2024 10:05 AM Water jcb/envirochem Test Method Results Date Analyzed Color color Clear 03/12/2024 Depth to water, ft. Depth to water, Ft 10.8 feet 03/12/2024 Sodium EPA 200.7, Rev 4.4,1994 11.9 mg/L 03/14/2024 Sulfate EPA 300.0, Rev. 2 1,1993 37 mg/L 03/14/2024 Ammonia Nitrogen EPA 350.1, Rev. 2.0,1993 < 0.2 mg/L 03/19/2024 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/12/2024 Odor Qualitative None 03/12/2024 Total Dissolved Solids (TDS) SM 2540 C-2015 207 mg/L 03/13/2024 Temperature SM 2550 B-2010 14.9 C 03/12/2024 pH SM4500 H B-2011 6.7 units 03/12/2024 Total Phosphorus SM 4500 P (F-H)-2011 0.07 mg/L 03/20/2024 Total Organic Carbon (TOC) SM 5310 B-2014 1.0 mg/L 03/13/2024 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 03/12/2024 Chloride SM4500 Cl E-2011 18 mg/L 03/15/2024 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 < 0.02 mg/L 03/12/2024 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0, 1993 0.58 mg/L 03/13/2024 Nitrate Nitrogen Subtraction Method 0.58 mg/L 03/28/2024 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 2.0,1993 < 0.5 mg/L 03/20/2024 Total Nitrogen Total Nitrogen 0.6 mg/L 03/28/2024 Report #.: 2024-05051 Page 2 of 11 :envirocehem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Mar 28, 2024 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2024-06051 Project ID: March - Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 24-14339 Site: MW-4 3/12/2024 9:30 AM Water jcb/envirochem Test Method Results Date Analyzed Color Color Clear 03/12/2024 Depth to water, ft. Depth to water, Ft. 4.4 feet 03/12/2024 Sodium EPA 200.7, Rev 4.4,1994 8.40 mg/L 03/17/2024 Sulfate EPA 300.0, Rev. 2.1, 1993 <5 mg/L 03/14/2024 Ammonia Nitrogen EPA 350.1, Rev.2.0, 1993 < 0.2 mg/L 03/19/2024 Gallons bailed before sampling Gallons Bailed before sampl'mg 5.0 gallons 03/12/2024 Odor Quardative None 03/12/2024 Total Dissolved Solids (TDS) SM 2540 C-2015 219 mg/L 03/13/2024 Temperature SM 2550 B-2010 14.4 C 03/12/2024 pH SM 4500 H B-2011 7.4 units 03/12/2024 Total Phosphorus SM 4590 P (F-H)-2011 0.10 mg/L 03/20/2024 Total Organic Carbon (TOC) SM 5310 B-2014 0.7 mg/L 03/13/2024 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 03/12/2024 Chloride SM4500 CI E-2011 < 5 mg/L 03/15/2024 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0,1993 < 0.02 mg/L 03/12/2024 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev.2.0,1993 < 0.02 mg/L 03/13/2024 Nitrate Nitrogen Subtraction Method <0.02 mg/L 03/28/2024 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev.2.0.1993 < 0.5 mg/L 03/20/2024 Total Nitrogen Total Ndrogen <0.5 mg/L 03/28/2024 Report #:: 2024-06051 Page 3 of 11 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab • 910.392.4424 Fax L All- 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info;iUenvironmentalchemists.com Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Date of Report: Mar 28, 2024 Customer PO #: Customer ID: 08100027 Report #: 2024-06051 Project ID: March - Monitoring Wells Lab ID Sample ID: Collect DatelTime Matrix Sampled by 24-14340 Site: MW-7A 3/12/2024 11:05 AM Water jcb/envirochem Test Method Results Date Analyzed Color Color Clear/Tan 03/12/2024 Depth to water, ft. Depth to Water, Ft. 5.2 feet 03/12/2024 Sodium EPA 200.7, Rev 4.4, 1994 24.2 mg/L 03/14/2024 Sulfate EPA 300.0, Rev. 2.1, 1993 26 mg/L 03/14/2024 Ammonia Nitrogen EPA 350.1, Rev. 2.0. 1993 < 0.2 mg/L 03/19/2024 Gallons bailed before sampling Gallons Balled before sampling 5.0 gallons 03/12/2024 Odor Qualitative None 03/12/2024 Total Dissolved Solids (TDS) SM 2540 C-2015 122 mg/L 03/13/2024 Temperature SM 2550 B-2010 15.8 C 03/12/2024 pH SM 4500 H B-2011 5.0 units 03/12/2024 Total Phosphorus SM 4500 P (F-H)-2011 < 0.04 mg/L 03/20/2024 Total Organic Carbon (TOC) SM 5310 B-2014 0.7 mg/L 03/13/2024 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 03/12/2024 Chloride SM4500 Cl E-2011 83 mg/L 03/15/2024 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA3532, Rev 20. 1993 < 0.02 mg/L 03/12/2024 Nitrate+Nitrite-Nitrogen EPA 3532, Rev. 2 0, 1993 0.08 mg/L 03/14/2024 Nitrate Nitrogen Subtraction Method 0.08 mg/L 03/28/2024 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 2.0. 1993 < 0.5 mg/L 03/20/2024 Total Nitrogen Total Nltrogen <0.5 mg/L 03/28/2024 Report #:: 2024-06051 Page 4 of 11 'L. enviroehem.,J ANALYTICAL & CONSULTING CHEMISTS Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Lab ID Sample ID: 24-14341 Site: MW-8A Test Color Depth to water, ft. Sodium Sulfate Ammonia Nitrogen Gallons bailed before sampling Odor Total Dissolved Solids (TDS) Temperature pH Total Phosphorus Total Organic Carbon (TOC) Fecal Coliform Chloride Nitrate Nitrogen (Calc) Nitrite Nitrogen Nitrate+N itrite-Nitrogen Nitrate Nitrogen Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) Total Nitrogen Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Mar 28, 2024 Customer PO #: Customer ID: 08100027 Report #: 2024-06051 Project ID: March - Monitoring Wells Collect Date/Time Matrix 3/12/2024 11:15 AM Water Method Color Depth to Water, Ft EPA 200.7, Rev 4.4, 1994 EPA 300.0, Rev. 2.1, 1993 EPA 350.1, Rev. 2.0, 1993 Gallons Bailed before sampling Qualitative SM 2540 C-2015 SM 2550 B-2010 SM 4500 H B-2011 SM 4500 P (F-H)-2011 SM 5310 B-2014 SM 9222 D-2015 MF SM4500 Cl E-2011 EPA 353.2, Rev. 2.0, 1993 EPA 353.2, Rev. 2.0,1993 Subtraction Method EPA 351.2, Rev. 2.0, 1993 Total Nitrogen Results Sampled by jcb/envirochem Date Analyzed Clear/Tan 03/12/2024 5.9 feet 03/12/2024 1.21 mg/L 03/14/2024 24 mg/L 03/14/2024 < 0.2 mg/L 03/19/2024 5.0 gallons 03/12/2024 None 03/12/2024 157 mg/L 03/13/2024 15.1 C 03/12/2024 4.8 units 03/12/2024 0.06 mg/L 03/20/2024 0.7 mg/L 03/13/2024 <1 Colonies/100ml- 03/12/2024 < 5 mg/L 03/15/2024 < 0.02 mg/L 03/12/2024 0.58 mg/L 03/14/2024 0.58 mg/L 03/28/2024 < 0.5 mg/L 03/20/2024 0.6 mg/L 03/28/2024 Report #:: 2024-06051 Page 5 of 11 -- --:-7 Environmental Chemists, Inca F"17 envirochem6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab 9 910.392.4424 Fax _ 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax _ M 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Date of Report: Mar 28, 2024 Customer PO #: Customer ID: 08100027 Report #: 2024-06051 Project ID: March - Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 24-14342 Site: MW-9 3/12/2024 9:45 AM Water jcb/envirochem Test Method Results Date Analyzed Color Color Clear/Tan 03/12/2024 Depth to water, ft. Depth to water, Ft. 3.8 feet 03/12/2024 Sodium EPA 200.7, Rev 4.4, 1994 2.65 mg/L 03/14/2024 .Sulfate EPA300.0, Rev.2.1, 1993 8 mg/L 03/14/2024 Ammonia Nitrogen EPA 350.1, Rev. 2.0, 1993 < 0.2 mg/L 03/19/2024 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/12/2024 Odor Qualitative None 03/12/2024 Total Dissolved Solids (TDS) SM 2540 C-2015 151 mg/L 03/13/2024 Temperature SM 2550 B-2010 13.0 C 03/12/2024 pH SM 4500 H 3-2011 5.8 units 03/12/2024 Total Phosphorus SM 4500 P (F-H)-2011 0.11 mg/L 03/20/2024 Total Organic Carbon (TOC) SM 5310 B-2014 39.1 mg/L 03/13/2024 Fecal Coliform SM 9=2 D-2015 MF <1 Colonies/100ml- 03/12/2024 Chloride SM4500 Cl E-2011 6 mg/L 03/15/2024 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 < 0.02 mg/L 03/12/2024 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0, 1993 < 0.02 mg/L 03/14/2024 Nitrate Nitrogen Subtraction Method <0.02 mg/L 03/28/2024 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 2,0, 1993 1.4 mg/L 03/20/2024 Total Nitrogen Total Nitrogen 1.4 mg/L 03/28/2024 Report ift: 2024-W51 Page 6 of 11 envirochem sM ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info(a environmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Mar 28, 2024 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2024-06051 Project ID: March - Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 24-14343 Site: MW-10A 3/12/2024 12:10 PM Water jcb/envirochem Test Method Results Date Analyzed Color Color Clear 03/12/2024 Depth to water, ft. Depth to Water, Ft. 3.8 feet 03/12/2024 Sodium EPA200.7, Rev 4.4.1994 119mg/L 03/14/2024 Sulfate EPA 300.0, Rev. 2.1,1993 156 mg/L 03/14/2024 Ammonia Nitrogen EPA 350.1, Rev. 2.0, 1993 0.4 mg/L 03/19/2024 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/12/2024 Odor Qualitative None 03/12/2024 Total Dissolved Solids (TDS) SM 2540 C-2015 795 mg/L 03/13/2024 Temperature SM 2550 B-2010 14.3 C 03/12/2024 pH SM 4500 H B-2011 3.82est units 03/12/2024 Estimated, below calibration range. Total Phosphorus SM 4500 P (F-H)-2011 0.10 mg/L 03/20/2024 Total Organic Carbon (TOC) SM 5310 B-2014 3.6 mg/L 03/13/2024 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 03/12/2024 Chloride SM4500 Cl E-2011 305 mg/L 03/15/2024 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 < 0.02 mg/L 03/12/2024 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 20, 1993 0.04 mg/L 03/14/2024 Nitrate Nitrogen Subtraction Method 0.04 mg/L 03/28/2024 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 2.0, 1993 0.8 mg/L 03/20/2024 Total Nitrogen Total Nitrogen 0.8 mg/L 03/28/2024 Report A: 2024-05051 Page 7 of 11 F"�' -- 77 Environmental Chemists, Inc. envirochem6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax M 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS infotaenvironmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Mar 28, 2024 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2024-06051 Project ID: March - Monitoring Wells Lab ID Sample ID: Collect DatelTime Matrix Sampled by 24-14344 Site: MW-11A 3/12/2024 12:00 PM Water jcb/envirochem Test Method Results Date Analyzed Color Color Clear 03/12/2024 Depth to water, ft. Depth to water, Ft 4.8 feet 03/12/2024 Sodium EPA 200.7, Rev 4.4,1994 60.3 mg/L 03/17/2024 Sulfate EPA 300.0, Rev. 2.1, 1993 163 mg/L 03/14/2024 Ammonia Nitrogen EPA 350.1, Rev. 2.0, 1993 < 0.2 mg/L 03/19/2024 Gallons bailed before sampling Gallons Balled before sampling 5.0 gallons 03/12/2024 Odor Qualitative None 03/12/2024 Total Dissolved Solids (TDS) SM 2540 C-2015 489 mg/L 03/13/2024 Temperature SM 2550 B-2010 14.5 C 03/12/2024 pH SM 4500 H B-2011 4.8 units 03/12/2024 Total Phosphorus SM 4500 P (F-H)-2011 0.05 mg/L 03/20/2024 Total Organic Carbon (TOC) SM 5310 B-2014 2.3 mg/L 03113/2024 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 03/12-12024 Chloride SM4500 ci E-2011 129 mg/L 03/15/2024 Nltmte Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 < 0.02 mg/L 03/13/2024 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0, 1993 0.41 mg/L 03/14/2024 Nitrate Nitrogen Subtraction Method 0.41 mg/L 03/28/2024 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 2.0. 1993 < 0.5 mg/L 03/20/2024 Total Nitrogen Total Nitrogen <0.5 mg/L 03/28/2024 Report #.: 202448051 Page a of 11 envirochem6602 sM ANALYTICAL & CONSULTING CHEMISTS Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Environmental Chemists, Inc. Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ^ 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Mar 28, 2024 Customer PO #: Customer ID: 08100027 Report #: 2024-06051 Project ID: March - Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 24-14345 Site: MW-12B 3/12/2024 11:45 AM Water jcb/envirochem Test Method Results Date Analyzed Color Color Clear 03/12/2024 Depth to water, ft. Depth to Water, Ft 5.5 feet 03/12/2024 Sodium EPA 200.7, Rev 4.4, 1994 59.8 mg/L 03/14/2024 Sulfate EPA 300.0, Rev. 2.1. 1993 183 mg/L 03/14/2024 Ammonia Nitrogen EPA 350.1, Rev. 2.0,1993 < 0.2 mg/L 03/19/2024 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/12/2024 Odor Qualitative None 03/12/2024 Total Dissolved Solids (TDS) SM 2540 C-2015 549 mg/L 03/13/2024 Temperature SM 2550 B-2010 15.1 C 03/12/2024 pH SM 4500 H B-2011 4.6 units 03/12/2024 Total Phosphorus SM 4500 P (F-H)-2011 0.90 mg/L 03/20/2024 Total Organic Carbon (TOC) SM 5310 B-2014 2.1 mg/L 03/13/2024 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 03/12/2024 Chloride SM4500 Cl E-2011 135 mg/L 03/15/2024 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 < 0.02 mg/L 03/13/2024 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0, 1993 0.09 mg/L 03/14/2024 Nitrate Nitrogen Subtraction Method 0.09 mg/L 03/28/2024 Total Nitrogen (Cale) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev, 2.0, 1993 0.6 mg/L 03/20/2024 Total Nitrogen Total Nitrogen 0.7 mg/L 03/28/2024 Report *: 2024-06051 Page 9 of 11 F"000--- -77 envirochem 6M ANALYTICAL & CONSULTING CHEMISTS Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Mar 28, 2024 Customer PO #: Customer ID: 08100027 Report #: 2024-06051 Project ID: March - Monitoring Wells Lab ID Sample ID: 24-14346 Site: MW-13A Test Collect DatelTime 3/12/2024 11:35 AM Method Matrix Sampled by Water jcb/envirochem Results Date Analyzed Color Color Milky White 03/1212024 Depth to water, ft. Depth to water. Ft 5.5 feet 03/12/2024 Sodium EPA 200.7, Rev 4.4,1994 4.43 mg/L 03/14/2024 Sulfate EPA 300.0, Rev. 21, 1993 7 mg/L 03/14/2024 Ammonia Nitrogen EPA 350.1, Rev. 2.0,1993 < 0.2 mg/L 03/19/2024 Gallons bailed before sampling Gallon Belted before sampling 5.0 gallons 03/12/2024 Odor Qualitative None 03/12/2024 Total Dissolved Solids (TDS) SM 2540 c-2015 30 mg/L 03/13/2024 Temperature SM 2550 B-2010 15.7 C 03/12/2024 pH SM 4500 H B-2011 4.8 units 03/12/2024 Total Phosphorus SM 4500 P (F-H)-2011 0.14 mg/L 03/20/2024 Total Organic Carbon (TOC) SM 5310 B-2014 0.7 mg/L 03/13/2024 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 03/12/2024 Chloride SM4500 CI E-2011 < 5 mg/L 03/15/2024 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0,1993 0.05 mg/L 03/13/2024 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0, 1993 0.02 mg/L 03/14/2024 Nitrate Nitrogen subtraction Method <0.02 mg/L 03/28/2024 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 2-0, 1993 < 0.5 mg/L 03/20/2024 Total Nitrogen Total Nitrogen <0.5 mg/L 03/28/2024 Report*: 2024-06051 Page 10 of 11 [envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 e 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Mar 28, 2024 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2024-06051 Project ID: March - Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 24-14347 Site: MW-14A 3/12/2024 10:55 AM Water jcb/envirochem Test Method Results Date Analyzed Color Color Clear/Tan 03/12/2024 Depth to water, ft. Depth to Water, Ft 3.5 feet 03/12/2024 Sodium EPA200.7, Rev4.4, 1994 188 mg/L 03/14/2024 Sulfate EPA 300.0, Rev. 2.1, 1993 494 mg/L 03/14/2024 Ammonia Nitrogen EPA 350.1, Rev. 2.0, 1993 < 0.2 mg/L 03/19/2024 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/12/2024 Odor Qualitative None 03/12/2024 Total Dissolved Solids (TDS) SM 2540 c-2015 1420 mg/L 03/13/2024 Temperature SM 2550 B-2010 16.2 C 03/12/2024 pH SM 4500 H B.2011 5.3 units 03/12/2024 Total Phosphorus SM 4500 P (F-H)-2011 0.16 mg/L 03/20/2024 Total Organic Carbon (TOC) SM 5310 B-2014 5.6 mg/L 03/13/2024 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 03/12/2024 Chloride SM4500 Cl E-2011 375 mg/L 03/15/2024 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA353.2. Rev. 2.0, 1993 < 0.02 mg/L 03/13/2024 Nitrate+Nitrite-Nitrogen EPA353.2, Rev. 2.0,1993 3.71 mg/L 03/15/2024 Nitrate Nitrogen Subtraction Method 3.71 mg/L 03/28/2024 Total Nitrogen (Cale) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 20, 1993 0.8 mg/L 03/20/2024 Total Nitrogen Total Nitrogen 4.5 mg/L 03/28/2024 Comment: Reviewed by: Report it: 2024-06051 Page 11 of 11 Date: 3 Lz 1 2-4 Analyst: Jav Baker -i-, Certification # 94 Facility Name: � ► 1� I I rl!�q Permit #: C>,A f l Li - pH Reference Method SM4500 H+B -201 1 instrument ID STARA221 : K06795 Calibration Time Cal Buffer4.0 s_u. Cal Buffer 10.0 s.0 Check Buffer 7.0 s.u. Comments 8:I0 14.02. (4) 1O.0( ") -1.CD (�) 'pH check buffer must read within t 0.1 pH units of the buffer's true value. 4 su buffer Lot#/. Ricca 1304N61 Exp 0425 7 su buffer Lot#/: Ricca 2? 10G40 Iixp. I Oi24 10 su buffer Lot#: RICCA 1304P74 Exp 1024 Sample location Sample Collection Time* Sample Analysis Time♦ pH Result s.0 ►Post -analysis Buffer Check value s.u. Comments/Data Qualifiers I Q 2-S 02. .M V'1- Z 100S 100S 6.13 IM, W - LA 9 SD Rr60 -7, 35 Mw--IR I i 11o5 49S M -vF} ( 4.87- ► Post analysis buffer check is required when performing analyses at multiple sampling locations and must be within f 0.1 units of the buffer's true value All pH values in pH units (i.e., sm.). Record all data to the nearest 0.01 s.u. and report to the nearest 0.1 s.u. Total Residual Chlorine (TRC) Reference Method: SM 4500 CI-G201 I Hach 8167 HR' ( Please circle applicable Method) Instrument ID: HACH Colorimeter 1512OE289091 Daily Check Standard Result Post -analysis Check Std. Time check Standard Sample Sample Collection Sample Analysis TRC Result Comments/Data Qualifiers or mg/L (when analyzing Analyzed Location Time Time µPS- or mg/Lµg/L at multiple sites) TRC Daily Check Standard true value µg/L or rng/L acceptance range µg/L or mg/L GEL STDS HACH A0038 Check standards must recover within f 10% of the check standard's true value Annual Calibration Curve Verification Date: 11/25/23 IDEXX (Free) 230901 Exp. Date:10/31/24 IDEXX (Total) 230757 Exp, Date'08/3124 Reagent Blank Value: When applicable. Analyze and document a reagent blank when standards, sample dilutions or PT Samples are prepared) Dissolved Oxygen (DO) Reference Method SM 4500 0 G -2016 instrument ID: YSI PRO 20 22D 100065_ Calibration/ Calibration variable Meter reading ♦Post -analysis calibration verification (when necessary) Verification Time or % efficiency after calibration Comments Temp °C Barometric re pressure Salinity, ppt Theoretical Value mg/L Calculated Value mg/L Use this row when performing a verification instead of calibration Sample Location Sample Collection Time *SampleAnalysis Time DO reading m Comments/Data Qualifiers ♦ When performing analyses at multiple locations, the meter must be recafibrated at each site before analysis or a post -analysis calibration verification must be performed + If sample is measured directly in the stream and/or onsite, only time analyzed would be recorded with a note that they are measured in situ or immediately Temperature Reference Method- SM 2550 B-2010 Instrument 1D: STARA221 : K06795 Sample Location Sample Collection Time 'Sample Analysis Time Temperature °C Comments/Data Qualifiers W - oz5 1025 ,1 - 2 1 DOS 1 S \14 .q r-1 w-y o N .y V\A J --711 [IDS I los 1 •$ ►tits- gprl 11►s I IIIS I5.1 " If sample is measured directly in the stream and/or on site, only time analyzed would be recorded, with a note that they are measured in situ or immediately Annual Verification Date 11-25-23 Field Personnel Note: QA.001 12/01/22 Rev 1-2022 Date: 3 I 12 i 2L� Analyst: Jav Baker Certification # 94 Facility Name- a d 1 t 21 Permit #: F I t if pH Reference Method- SM4500 H+A -2011 Instrument ID STARA221 : 1(06795 Calibration Time Cal Buffer 4 0 sm Cal Buffer 10 0 s u Check Buffer 7.0 sm Comments �' I u y oz (d) 10.01 ") —l. Do ") *PH check buffer must read within t 0,1 pH units ofthe buffer's true value. 4 su buffer Lot#/: Ricca 1304N61 Expo4/25 7 su buffer Lot#/: Ricca 221 OG40 Exp. 10l24 10 su buffer Lot#: RICCA 1304P74 En. 10124 Sample location Sample Collection Time* Sample Analysis Time• pH Result s.0 ►Post -analysis Buffer Check value s.u. Comments/Data Qualifiers s 5--% w-II7A- IZIC) 121p 3�2� W-Illr') 1200 17p 4.15 HVJ- IZ13 114S I14S 4 -�_-5 MW 13 P, 113c_-, 113s 14.1?5 ► Post analysis buffer check is required when performing analyses at multiple sampling locations and must be within f 0.1 units ofthe buffer's true value All pH values in pH units (i.e., sm.). Record all data to the nearest 0.01 s u, and report to the nearest 0,1 s.u. h�l 1r`1-14 A- I ASS IDss 5-3D Total Residual Chlorine (TRC) Reference Method: SM 4500 CI-G201 I: Hach 8167 HR: ( Please circle applicable Method) Instniment ID. HACH Colorimeter 15120E289091 Daily Check Standard Result Post -analysis Check Std. Time check Standard Sample Sample Collection Sample Analysis TRC Result Comments/Data Qualifiers µg/L or mg/L (when analyzing Analyzed Location Time Time pg/L or mg/L at multiple sites) TRC Daily Check Standard true value µg/L or mg/L acceptance range µg/L or mg, L GEL STDS HACH AUU3g Check standards must recover within ;L10% of the check standard's irue value Annual Calibration Curve Verification Date: 11/25/23 IDEXX (Free) 230901 Exp. Date:10/31/24 IDEXX (Total) 230757 Exp Date:08/310-4 Reagent Blank Value: When applicable. Analyze and document a reagent blank when standards, sample dilutions or PT Samples are prepared) Dissolved Oxygen (DO) Reference Method:SM 4500 O G -2016 Instrument ID. YSI PRO 20 22D100065 Calibration/ Calibration variable Meter reading •Post -analysis calibration verification (when necessary) Verification Time or%efficiency after calibration Comments Temp °C Barometric pressure Salinity, ppt Theoretical Value mg/L Calculated Value mg/L Use this row when performing a verification instead or calibration Sample Location Sample Collection Time *Sample Analysis Time DO reading me/L Comments/Data Qualifiers • When performing analyses at multiple locations, the meter must be recalibrated at each site before analysis or a post -analysis calibration verification must be performed. • If sample is measured directly in the stream and/or onsite, only time analyzed would be recorded with a note that they are measured in situ or immediately Temperature Reference Method SM 2550 D-2010 Instrument ID STARA221 : K06795 Sample Location Sample Collection Time *Sample Analysis Time Temperature °C Comments/Data Qualifiers Ck 4Sq4SIca •D 1 Vi]-Ib11- IZ10 I7-10 ILI-3 M ) I N vwo I wo 14. N W -12e k 14,5 1 ML3 15. N I3 p I t 35 1135 • I f sample is measured directly in the stream and/or on site, only time analyzed would be recorded, with a note that they are measured in situ or immediately Annual Verification Date 11-25-23 Field Personnel Note: V' r^ ,r W! I 1 I k 10C 5 1 6 ,Z Y r'1- I J QA.00l 12ro1n2 Rev 1-2022 Environmental Chemist, Inc., Wilmington, NC Lab #94 Sample Receipt Checklist 6602 Windmill Way Wilmington, NC 28405 910.392.0223 Client: U �j1y �11n Date: Report Number: _ 2024- O U G 1:I Receipt of sample: ECHEM Pickup Client Delivery ❑ I UPS ❑ FedEx ❑ Other O ❑ YES ❑ NO ❑x N/A 1. Were custody seals present on the cooler? ❑ YES JE3 NO (] N/A 12. If custody seals were present, were they intact/unbroken? Original temperature upon receipt °C Corrected temperature upon receipt °C How temperature taken: ❑ Temperature Blank ❑x Against Bottles IR Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor °C: 0.0 ❑x YES ❑ NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified? Z YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed? 0 YES ❑ NO S. Were sample ID's listed on the COC? 0 YES ❑ NO 6. Were samples ID's listed on sample containers? 0 YES ❑ NO 7. Were collection date and time listed on the COC? 0 YES ❑ NO 8. Were tests to be performed listed on the COC? 0 YES ❑ NO 9. Did samples arrive in proper containers for each test? 0 YES ❑ NO 10. Did samples arrive in good condition for each test? 9 YES ❑ NO 11. Was adequate sample volume availableT YES ❑ NO 12. Were samples received within proper holding time for requested tests? YES ❑ NO 13. Were acid preserved samples received at a pH of <2? ❑ YES ❑ NO 14. Were cyanide samples received at a pH >12? ❑ YES ❑ NO 15. Were sulfide samples received at a pH >9? YES ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? ** ❑ YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? 11 YES ❑ NO 18. Were orthophosphate samples filtered in the field within 15 minutes? * TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet. ** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) Sample(s) were received incorrectly preserved and were adjusted accordingly by adding (circle one): H2SO4 HNO3 HCI NaOH Time of preservation: If more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or notify the state lab If directed to analyzed by the customer. Who was notified, date and time: Volatiles Sample(s) were received with headspace COMMENTS: DOC. QA.002 Rev 1 dmill Way Wilminon, NC ENVIRONMENTAL CHEMISTS, INC OFFI En 103 2-0223FAX910392- 4245 Analytical &Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: Darling Ingredients -Rose Hill PROJECT NAME: Monitoring Wells (Mar/Jul/Nov) REPORT NO: ELT 60� ADDRESS: CONTACT NAME: PO NO: REPORT TO: Corey Lanier PHONE/FAX: COPY TO: email: Sampled By: j-<4 SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection m y �a ui 2mw m E `o G c t7 co o a "" c U E Y! z PRESERVATION ANALYSIS REQUESTED Date Time Temp z o z = o z c a z ° MW: I �'f MW 1� r1 X NO2, Chloride, TDS, Sulfate G G .i Depth to water: `f C P �� La X NO3, NH3, TP, TN (calc G G gallons bailed: s C P �a X Na G G pH(field): S f� C P X Fecal Coliform G G color(field): C P X ITOC G G odor: AP A C P lx� VOC (November only) G G C P G G C P G G C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature wh Delivered By:_ Comments: °C: -1. () Accepted: Rejected: Resampl Re ested: By: P/ Date: t c4 Time: 3 L T ROUND: mington ENVIRONMENTAL CHEMISTS, IN C OFFICE: 10 I392-02 3i1FAX 910-392-44245 Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: Darling Ingredients -Rose Hill PROJECT NAME: Monitoring Wells (Mar/Jul/Nov) REPORT NO: ADDRESS: CONTACT NAME: PO NO: REPORT TO: Corey Lanier PHONEIFAX: COPY TO: email: Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification p Collection m coa E T h� a `o E c 0 m cC7 `o oa " m c� c-a t E " ow m m g� z PRESERVATION ANALYSIS REQUESTED D e Time Temp m o Z s '� = Z = a Z o W i` o MW: MW C P X NOZ Chloride, TDS, Sulfate G G Depth to water: %ZS C P 1.0'5 as X NO3, NH3, TP, TN (calc) G G / gallons bailed: s C P I X I INa G G pH(field): �• C P X Fecal Coliform G G color(field): C P X TOC G G odor: C P X VOC (November only) G G C P G G C P G G C P FFF G G Transfer Relinquished By: DatelTime Received By: DateTme 1. 2. Temperature when Received °C: • G7 Accepted: / Rejected: Resample Requested: Delivered By: Received By: bbl Date: Time: Comments: TURNAROUND: 6602 Windmill Way NC mington ENVIRONMENTAL CHEMISTS, INC OFFICE: 9103 2-02 3i1FAX910� 92- 4245 Analytical 8 Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchamists.com COLLECTION AND CHAIN OF CUSTODY Client: Darling Ingredients -Rose Hill PROJECT NAME: Monitoring Wells (Mar/Jul/Nov) REPORT NO: aw - won ADDRESS: CONTACT NAME: PO NO: REPORT TO: Corey Lanier PHONEIFAX: COPY TO: email: Sampled By:_ SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection m m W F a a E ii ! ci d _ ct7 Ts `o lu m �= r E rc Ow m 5 z PRESERVATION ANALYSIS REQUESTED Pate Time Temp z z u $ _ o o Z ° = o �j MW: 7 04 < �V'� MW C P �y��a X NO2, Chloride, TDS, Sulfate G G y Depth to water: J 3 C P �0� X NO3, NH3, TP, TN (calc) G G gallons bailed: � C P X Na G G � pH(field): y C P X Fecal Coliform G G color(field): o%te-i C P I X TOC G G odor: AAW-& C P X VOC (November only) G G C P G G C P G G C P G G Transfer Relinquished By: Daterrime Received By: Daterrime 1. 2. Temperature when Received °C: Accepted: / Rejected: Resample Requested: Delivered By: Received By: ` c/ I Date:� I jdI a�l _Time: Comments: TURNAROUND: 6602 Way mington 'r ENVIRONMENTAL CHEMISTS, INC OFFICE: 0-3 2-0223'iFAX910392-4245 Analytical &Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: Darling Ingredients -Rose Hill PROJECT NAME: Monitoring Wells (Mar/Jul/Nov) REPORT NO: ADDRESS: CONTACT NAME: PO NO: REPORT TO: Corey Lanier PHONE/FAX: COPY TO: email: Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection E a 0 `o 0 m _ `o "` o m m 00 z PRESERVATION ANALYSIS REQUESTED at Time Temp w z � � x ., = x z C W o MW: } MW C P l� X NO2, Chloride, TDS, Sulfate f G G Depth to water: b L C P Lal X NO3, NH3, TP, TN (calc) G G / gallons bailed: S C P I �a X I INa G G / pH(field): •�'J C P X Fecal Coliform G G color(field): o�(fJ C P X TOC G G odor: A C P X VOC (November only) G I G C P G G C P G G C P G G Transfer Relinquished By: Date/Time Received By: Dateffime 1. 2. Temperature when Received °C: 0 Accepted: Rejected: Resample Requested: Delivered By: Received By: I✓G l Date: J at ay Time: Comments: TURNAROUND: 44M ENVIRONMENTAL CHEMISTS, INC OFFICE: 910I392-02 3iIFAX 910392-44245 Analytical 8 Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info&nvironmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: Darling Ingredients -Rose Hill PROJECT NAME: Monitoring Wells (Mar/Jul/Nov) REPORT NO: " ADDRESS: CONTACT NAME: PO NO: REPORT TO: Corey Lanier PHONEIFAX: COPY TO: email: Sampled By: L O'`J SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection m m E a ~ 2 A n o` E C7 d _ C U' 9 `o C1 v m C J c t E i7 W m 2 PRESERVATION ANALYSIS REQUESTED D to Time Temp z z = c _ o = 0 z 0_ W O MW: d / / MW C P �y�� X NO2. Chloride, TDS. Sulfate G G � Depth to water: 714 C P c LO ' I �X NO3, NH3, TP, TN (calc) G G gallons bailed: C P to X Na G G pH(field): y.� L c P X Fecal Coliform G G color(field): G e.-J L4o. C P X TOC G G odor: C P X VOC(November only) G G C P G G C P G G C P G G Transfer Relinquished By: DateITime Received By: Daterrime 1. 2. Temperature when Received °C: Accepted: ✓ Rejected: Resample Requested: Delivered By: Received By: /Gj Date: Time: Comments: TURNAROUND: mington ENVIRONMENTAL CHEMISTS, I N C OFFICE: 910 I392-02 3,IFAX 910 392.4245 Analytical &Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: Darling Ingredients -Rose Hill PROJECT NAME: Monitoring Wells (Mar/Jul/Nov) REPORT NO: a N " ADDRESS: CONTACT NAME: PO NO: REPORT TO: Corey Lanier PHONE/FAX: COPY TO: email: Sampled By: 7Z71 SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection E F H E `o 0 m _ `o "" m U E 3 z PRESERVATION ANALYSIS REQUESTED Date Time Temp Z z 3 o c z o q MW: 1 ' c' MW AW X NO2, Chloride, TDS, Sulfate G G •/ Depth to water: cK C P ` 10''+ I.� X NO3, NH3, TP, TN (calc) G G gallons bailed: S C P X I INa G G H(field): , a C P X Fecal Coliform G G color(field): 4� �G� C P X TOC G G odor: A. - — C P I X IVOC (November only) G G C G C I— G C G Transfer Relinquished By: Date/Time Received By: Date/Time 7. 2. Temperature when Received °C: Accepted: ✓ Rejected: Resample Requested: Delivered By: Received By: U1 Date: Time: Comments: TURNAROUND: 6602 Way mington ENVIRONMENTAL CHEMISTS, I N C OFFICE: win 910 392.44245 Analytical &Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 Info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: Darling Ingredients -Rose Hill PROJECT NAME: Monitoring Wells (Mar/Jul/Nov) REPORT NO: d60051 ADDRESS: CONTACT NAME: PO NO: REPORT TO: Corey Lanier PHONE/FAX: COPY TO: email: Sampled By: ,j ,4 SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection — m a F H :9 M E `o V id _ cLl `o a V CJ .2 E V O W m 2 PRESERVATION ANALYSIS REQUESTED Date Time Temp z 2 x c o = o Z p ~ O MW: fl A, (4.3 MW C P X NO2, Chloride, TDS, Sulfate G G � Depth to water: �� C P Ld ' S e2, X IN03. NH3, TP, TN (talc) G G 1 gallons bailed: S C P La X Na G G pH(field): S'� Ll C P X Fecal Coliform G G color(field): `' C P X I I ITOC G G odor: ^I' C P X I IVOC (November only) G G C P G G C P G G C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received °C: h . Q Accepted: ✓ Rejected: Resam pie Requested: Delivered By: Received By: e4�A Date: 3 ! 12 Iay Time: rnmmpn+c• TURNAROUND: 6602 Windmil Way Wilmington, NC ENVIRONMENTAL CHEMISTS, IN C OFFICE: 9101392-0223 FAX 910 392-44245 Analytical &Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@envlronmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: Darling Ingredients -Rose Hill PROJECT NAME: Monitoring Wells (Mar/Jul/Nov) REPORT NO: ADDRESS: CONTACT NAME: PO NO: REPORT TO: Corey Lanier PHONE/FAX: COPY TO: email: Sampled By: 7 �f SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection d m E F �' m a E' m .. e(7 c° c°� a m �� 0 E �w m g 'z PRESERVATION ANALYSIS REQUESTED to Time Temp z z "= o T 0 z o w o MW: 7 MW C P 'I �! X NO2, Chloride, TDS, Sulfate G G Y Depth to water: C P LU 4a X IN03, NH3, TP, TN (calc) G G gallons bailed: C P I ci X Na G G pH(field): C P X Fecal Coliform G G color(field): C, 106J C P X TOC G G A�1 odor: C P X VOC (November only) G G C P G G C P _ G G C P G G Transfer Relinquished By: DatelTime Received By: Datefrime 1. 2. Temperature when Received °C: Accepted: V Rejected: Resample Requested: Delivered By: Received By: Date: Time: Comments: TURNAROUND: 41M mington ENVIRONMENTAL CHEMISTS, I N C OFFICE: 9 0' 392-02231FAX 910 392-44245 Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 Info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: Darling Ingredients -Rose Hill PROJECT NAME: Monitoring Wells (Mar/Jul/Nov) REPORT NO: (� ADDRESS: CONTACT NAME: PO NO: REPORT TO: Corey Lanier PHONE/FAX: COPY TO: email: Sampled By: �SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection w m W F m r m E `o ff o 0 m ec7 `o oa " _ r r E " ow m g� Z PRESERVATION ANALYSIS REQUESTED ate Time Temp z o Z o x H �+ = e Z xo o = = r MW: IL 1 11Y3 i S ' ( MW C P q �y7 X NO2, Chloride, TDS, Sulfate ' G G Depth to water: (O C P < . � c2 X NO3, NH3, TP, TN (calc) G G / gallons bailed: f� C P Z X Na G G pH(field): y C P X Fecal Coliform G G color(field): G k4j C P X I ITOC G G odor: A D^ C P X I ivoc (November only) G G C P G G C P G G C P G G Transfer Relinquished By: Date/Time Received By: Daterrime 1. 2. Temperature when Received `C: UAccepted: V Rejected: Resample Requested: Delivered By: Received BY: flee Date: a -Time: Comments: TURNAROUND: 4M ENVIRONMENTAL CHEMISTS, INC OFFICE: 910I392-02 3iIFAX 910392-44g245 Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentaichemists.com COLLECTION AND CHAIN OF CUSTODY Client: Darling Ingredients -Rose Hill PROJECT NAME: Monitoring Wells (Mar/Jul/Nov) REPORT NO: ~- OUKLI ADDRESS: CONTACT NAME: PO NO: REPORT TO: Corey Lanier PHONEIFAX: COPY TO: email: Sampled By: S!1) SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection m m F W a a E' `o V m _ c t7 `o U c .2 E U W m Z PRESERVATION ANALYSIS REQUESTED Pate Time Temp Z z = = o x a0 4z 0 p �1 MW: / 3 } MW C P 1u'n (y 'I l4' X NO2, Chloride, TDS, Sulfate G G . Depth to water: C P �/ LO'�1 L A. X NO3. NH3, TP, TN (calc) G G gallons bailed: C P La X Na G G H(field): y' C P X Fecal Coliform G G color(field): M. f `j �' C P X TOC _ G G odor: 19 DAc. C P X VOC (November only) G G C P G G C P G G C P G G Transfer Relinquished By: DateMme Received By: DatelTime 1. 2. Temperature when Received °C: "h . �� Accepted: ✓ Rejected: Resample Requested: Delivered By: Received By: �/ Date: 4-1 dq Time: Comments: TURNAROUND: 6602 Way , NC 4 mington MENVIRONMENTAL CHEMISTS, I N C OFFI E: 910-1392-02 3IFAX 910 392-44245 Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentaichemists.com COLLECTION AND CHAIN OF CUSTODY Client: Darling Ingredients -Rose Hill PROJECT NAME: Monitoring Wells (Mar/Jul/Nov) REPORT NO: ADDRESS: CONTACT NAME: PO NO: REPORT TO: Corey Lanier PHONE/FAX: COPY TO: email: Sampled Bv: = SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection m ad A i; Ca m _ �c� o` m c=� a E " c w m 5'z PRESERVATION ANALYSIS REQUESTED D to Time Temp z z lu _ o _ c $ O W c MW: 1N 3 v p� /6 L MW X NO2, Chloride, TDS, Sulfate / G G ,► Depth to water: �L C P t d " L 9 X NO3, NH3, TP, TN (talc) G G gallons bailed: S C P 1p� X Na G G pH(field): �' 3-- C P X Fecal Coliform G G color(field): Cte.J J C P X I ITOC G G odor: C P X VOC (November only) G G C P G G C P G G C P GIG Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received °C: h V Accepted: ✓ Rejected: Resampie Requested: Delivered By: Received By: Date: Time: Comments: TURNAROUND: