NCG080590_DMR_20240503

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APEXApril 30, 2024 /�I- Environmental Quality
Received
NC DEMLR MAY 0 3 2024
Winston-Salem Regional Office ! Winston-Salem
450 Hanes Mill Road, Suite 300 Regional Office
Winston-Salem, North Carolina 27105
RE: NCG 080000 Discharge Monitoring Report
Southeastern Freight Lines —GBO
8718 West Market Street
Greensboro, North Carolina 27409
Permit No. NCG080590
To whom it may concern:
Apex Companies, LLC (Apex) has prepared the attached Discharge Monitoring Report (DMR) on
behalf of Southeastern Freight Lines for samples collected at the above referenced facility in Q1
2024. Samples were collected for pH, Total Suspended Solids, and Oil & Grease analysis.
Analysis of samples collected indicated no exceedances of benchmark values. A copy of the
DMRs is included as Attachments 1 & 2. The laboratory report has been included as
Attachment 3, and a photo log showing the pH measurement for these samples has been
included as Attachment 4.
Apex understands that NC DEMLR has implemented electronic reporting systems and DMRs are
to be submitted via these systems. In Q1 2024, Apex coordinated with Southeastern Freight
Lines to register with NC eDMR and Southeastern Freight Lines has submitted the applicable
eDMR registration forms to DEMLR. Access to this facility's eDMR page is still pending, therefore
Apex has prepared a hard-copy DMR to ensure that DEMLR has been provided with monitoring
reports as required per the permit.
If you have any questions regarding this matter, please contact Apex at [phone].
Sincerely,
Apex Companies, LLC
//,fast
Josh McClintic, PE
Engineer 3
Attachments:
Attachment 1 — Ouffall 1 DMR
Attachment 2— Ouffall 2 DMR
Attachment 3—Laboratory Report
Attachment 4— Photo Log
Apex Companies,LLC• 5909 Breckenridge Pkwy,Suite E•Tampa,FL 33610•T 813.248.8558 ApexCos.com

Discharge Monitoring Report—NCG080590 April 30, 2024
Southeastern Freight Lines— G8O Page 2
Attachment 1
Duffel! 1 DMR
Apex Companies,LLC•5909 Breckenridge Pkwy,Suite E Tampa,FL 33610 T 813.248 8558 ApexCos com

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Discharge Monitoring Report—NCG080590 April 30, 2024
Southeastern Freight Lines—GBO Page 3
Attachment 2
Outfall 2 DMR

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Discharge Monitoring Report—NCG080590 April 30, 2024
Southeastern Freight Lines—GBO Page 4
Attachment 3
Laboratory Report

Pace Analytical Services,LLC
9800 Kincey Ave. Suite 100
ace
Huntersville,NC 28078
[phone]
January 16, 2024
Andrew Street
Apex Companies
5900-0 Northwoods Business
Parkway
Charlotte, NC 28269
RE: Project: SOUTHERNEASTERN FREIGHT-GREENS
Pace Project No.: 92707501
Dear Andrew Street:
Enclosed are the analytical results for sample(s)received by the laboratory on January 10,2024. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services-Asheville
• Pace Analytical Services-Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
'A)
Bonnie yang V
[e-mail]
704-977-0968
Project Manager
Enclosures
cc: Kevin Cooke,Apex Comapnies, LLC
Kaitlyn Nootens,Apex Companies
Devin Politoske,Apex Companies,LLC
Q PC�FO
4 \tb REPORT OF LABORATORY ANALYSIS
, / 1 This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 1 of 13

Pace Analytical Services,LLC
Pace. 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
[phone]
CERTIFICATIONS
Project: SOUTHERNEASTERN FREIGHT-GREENS
Pace Project No.: 92707501
Pace Analytical Services Charlotte
South Carolina Laboratory ID:99006 South Carolina Certification#:99006001
9800 Kincey Ave.Ste 100, Huntersville,NC 28078 South Carolina Drinking Water Cert.#:99006003
North Carolina Drinking Water Certification#:37706 Florida/NELAP Certification#:E87627
North Carolina Field Services Certification#:5342 Kentucky UST Certification#:84
North Carolina Wastewater Certification#: 12 Louisiana DoH Drinking Water#: LA029
South Carolina Laboratory ID:99006 Virginia/VELAP Certification#:460221
Pace Analytical Services Asheville
2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030
Florida/NELAP Certification#:E87648 South Carolina Certification#:99030001
North Carolina Drinking Water Certification#:37712 Virginia/VELAP Certification#:460222
North Carolina Wastewater Certification#:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 2 of 13

Pace Analytical Services,LLC
9800 Kincey Ave. Suite 100
ace. Huntersville,NC 28078
[phone]
SAMPLE SUMMARY
Project: SOUTHERNEASTERN FREIGHT-GREENS
Pace Project No.: 92707501
Lab ID Sample ID Matrix Date Collected Date Received
92707501001 OUTFALL 1 Water 01/09/24 10:39 01/10/24 08:50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 3 of 13

Pace Analytical Services,LLC
9800 Kincey Ave. Suite 100
Pace® Huntersville,NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: SOUTHERNEASTERN FREIGHT-GREENS
Pace Project No.: 92707501
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92707501001 OUTFALL 1 EPA 1664B DVR 1 PASI-C
SM 2540D-2015 RVS 1 PASI-A
EPA 9040C SMS 1 PASI-A
PASI-A=Pace Analytical Services-Asheville
PASI-C=Pace Analytical Services-Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 4 of 13

Pace Analytical Services,LLC
9800 Kincey Ave. Suite 100
ace® Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: SOUTHERNEASTERN FREIGHT-GREENS
Pace Project No.: 92707501
Sample: OUTFALL 1 Lab ID: 92707501001 Collected: 01/09/24 10:39 Received: 01/10/24 08:50 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
HEM,Oil and Grease Analytical Method:EPA 1664E
Pace Analytical Services-Charlotte
Oil and Grease 1.2J mg/L 4.9 1.1 1 01/15/24 14:00
2540D Total Suspended Solids Analytical Method:SM 2540D-2015
Pace Analytical Services-Asheville
Total Suspended Solids <2.5 mg/L 2.5 2.5 1 01/11/24 01:31
9040 pH Analytical Method:EPA 9040C
Pace Analytical Services-Asheville
pH at 25 Degrees C 6.5 Std.Units 0.10 0.10 1 01/11/24 17:59 H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:01/16/2024 09:33 AM without the written consent of Pace Analytical Services,LLC. Page 5 of 13

Pace Analytical Services,LLC
9800 Kincey Ave. Suite 100
aced Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: SOUTHERNEASTERN FREIGHT-GREENS
Pace Project No.: 92707501
QC Batch: 825389 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM,Oil and Grease
Laboratory: Pace Analytical Services-Charlotte
Associated Lab Samples: 92707501001
METHOD BLANK: 4269283 Matrix: Water
Associated Lab Samples: 92707501001
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Oil and Grease mg/L <5.0 5.0 1.1 01/15/24 14:00
LABORATORY CONTROL SAMPLE: 4269284
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Oil and Grease mg/L 40 33.3 83 78-114
MATRIX SPIKE SAMPLE: 4269285
92707495002 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Oil and Grease mg/L ND 38.8 35.1 83 78-114
SAMPLE DUPLICATE: 4269286
92707501001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Oil and Grease mg/L 1.2J 1.3J 30
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:01/16/2024 09:33 AM without the written consent of Pace Analytical Services,LLC. Page 6 of 13

Pace Analytical Services,LLC
ace 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: SOUTHERNEASTERN FREIGHT-GREENS
Pace Project No.: 92707501
QC Batch: 824717 Analysis Method: SM 2540D-2015
QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92707501001
METHOD BLANK: 4265953 Matrix: Water
Associated Lab Samples: 92707501001
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Total Suspended Solids mg/L <2.5 2.5 2.5 01/11/24 01:26
LABORATORY CONTROL SAMPLE&LCSD: 4265954 4265963
Spike LCS LCSD LCS LCSD %Rec Max
Parameter Units Conc. Result Result %Rec %Rec Limits RPD RPD Qualifiers
Total Suspended Solids mg/L 250 240 240 96 96 90-110 0 25
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:01/16/2024 09:33 AM without the written consent of Pace Analytical Services,LLC. Page 7 of 13

Pace Analytical Services,LLC
ace. 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: SOUTHERNEASTERN FREIGHT-GREENS
Pace Project No.: 92707501
QC Batch: 824974 Analysis Method: EPA 9040C
QC Batch Method: EPA 9040C Analysis Description: 9040 pH
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92707501001
SAMPLE DUPLICATE: 4267174
92706177001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
pH at 25 Degrees C Std.Units 7.2 7.2 0 10 H3
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:01/16/2024 09:33 AM without the written consent of Pace Analytical Services,LLC. Page 8 of 13

Pace Analytical Services,LLC
ace 9800 Kincey Ave. Suite 100
Hunlersville,NC 28078
[phone]
QUALIFIERS
Project: SOUTHERNEASTERN FREIGHT-GREENS
Pace Project No.: 92707501
DEFINITIONS
DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot.
ND-Not Detected at or above adjusted reporting limit.
TNTC-Too Numerous To Count
J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL-Practical Quantitation Limit.
RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S-Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is
a combined concentration.
Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values.
LCS(D)-Laboratory Control Sample(Duplicate)
MS(D)-Matrix Spike(Duplicate)
DUP-Sample Duplicate
RPD-Relative Percent Difference
NC-Not Calculable.
SG-Silica Gel-Clean-Up
U-Indicates the compound was analyzed for,but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as
"Total"may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes.
TNI-The NELAC Institute.
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:01/16/2024 09:33 AM without the written consent of Pace Analytical Services,LLC. Page 9 of 13

Pace Analytical Services,LLC
9800 Kincey Ave. Suite 100
ace. Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SOUTHERNEASTERN FREIGHT-GREENS
Pace Project No.: 92707501
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92707501001 OUTFALL 1 EPA 1664E 825389
92707501001 OUTFALL 1 SM 2540D-2015 824717
92707501001 OUTFALL 1 EPA 9040C 824974
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:01/16/2024 09:33 AM without the written consent of Pace Analytical Services,LLC. Page 10 of 13

DC#_Title: ENV-FRM-HUN1-0083 v03 Sample Condition Upon Receipt
fl
ace
Effective Date: 11/29/2023 4:16:30 PM
Laboratory receiving samples: -.,/
Asheville❑ Eden❑ Greenwood❑ Huntersville[11 Raleigh Mechanicsville❑ Atlanta❑ KernersvilleD
Sample Condition Client Name: WO# 92?07501
Upon Receipt ; / Project#:
Courier: ‘__,Fed Ex X ❑UPS ❑USPS ❑Client 11111111 1111111111
❑ Commercial Q.Pace ❑Other: 92707501
Custody Seal Present? DYes v No Seas Intact? ❑Yes ❑No 21 /A
Date/Initials Person Examining Contents•: C 44—/('
Packing Material: 0 Bubble Wrap Bubble Bags 0 None ❑ Other Biological Tissue F ozen?
Thermometer: qz-co ❑Yes ❑No UN/A
❑ IR Gun ID: 10 Type of Ice: 17)4 et 0 Blue ❑None
' Correction Factor: _
Cooler Temp: - Add/Subtract('C) + I Temp should be above freezing to 6'C
0 Samples out of temp criteria.Samples on ice,cooling process
Cooler Temp Corrected (jLA: 3,\ has begun
USDA Regulated Soil(M N/A,water sample)
Did samples originate in a quarantine zone within the United States:CA,NY,or SC Did samples originate from a foreign source(internationally,
(check maps)?Oyes No including Hawaii and Puerto Rico)?❑Yes ❑No
J Comments/Discrepancy:
Chain of Custody Present? di es 0 No ]N/A 1.
Samples Arrived within Hold Time? Yes ❑ o ❑N/A 2.
Short Hold lime Analysis(<72 hr.)? Oyes QDo ❑N/A 3.
Rush Turn Around Time Requested? Oyes OdNo ON/A 4.
Sufficient Volume? dyes, ❑No ON/A S.
Correct Containers Used? 1pyes ❑No ON/A 6.
-Pace Containers Used? �f-b�/es 0 No ❑N/A
Containers Intact? nrgYes 0 yo ❑N/A 7.
Dissolved analysis:Samples Field Filtered? ❑ es d No ❑N/A 8.
Sample Labels Match COC? yof es ❑No ❑N/A 9.
-Includes Date/Time/ID/Analysis Matrix: V1/ _
Headspace in VOA Vials(>5.6mm)? ❑Yes ❑No GYr/A 10.
Trip Blank Present? ❑Yes ❑Na (;'N/A 11.
Trip Blank Custody Seals Present? ❑Yes 0 No Ld N/A
COMMENTS/SAMPLE DISCREPANCY Field Data Required? ❑Yes 0 No
Lot ID of split containers:
CLIENT NOT1FICATION/RESOLUTION
Person contacted: Date/Time:
•
Project Manager SCURF Review: Date:
Project Manager SRF Review: Date:
Qualtrax ID:69614 Paoe 1 of 2
Page 11 of 13

I — Effective Date: 11/14/2022
111 'Check mark tophalf of box ifpH and/or dechlorination is verified and ��70 1 ®�
/ Project 4
within the acceptance range for preservation samples. PM: BV Due Date: 01/17/24
Exceptions:VOA,Colierm,TOE'.Oil and Grease,ORO/8015(water)DOC LLtic CLIENT: 92-APEX MOOR
"Bottom half of box is to list number of bottles
J
•"Check all unpreserved Nitrates for chlorine
I ; v-r-- - I ---, v 1
7.
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u v y v v *1 = v , d rr v r. Z — I 1 Qri: a v
T. s = v X a N •, x a o v z a a < c.i Y a
✓ u Oi ' ? n A v ° n 2 Z m Z I 2 ON t =^ d
n n c aP to al . O O `a' T A d c c v ON v p v 2 e+ m = To
N er d
c c c a '^ 2 a O ° g- c ON N v 2 N ' a = c c a
N 2 '° c V nr 2 = vl .. O ? > m m Z z Q
a_ u ,: 2 ry z S , = 2 V A c M 7 a a ., iv A -
. ii e .n io A ry q o A a E a E A a a . v. A
a ra a 9 S a a a E E E E E O O 0 O v a`+ " F.0 < ,c—, E
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E E E r, E E E E Si v y c y E -+ N J
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rt N N ti H N N N ..�1 .M rj ...1 O O O n V O 21 r N O— N O
7 N M ' N a w N NE O H N C v C G UG G U0 G UG 0t1d �l m G 7 .
m 6m % Cm % d m m 3 a a a o o o = > C v 1 a la N U
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pH Adjustment Log for Preserved Samples _ 1
Sample ID Type of Preservative i pH upon receipt Date preservation adjusted Time preservation Amount of Preservative Lot$1
adjusted added
i_ _ .
Note Whenever there 1s a discrepancy affecting Nortlr Carolina compliance samples.a copy of this form will be sent to Ow North Carolina DENR certification Office lI e
Out of hold.incorrect preservative,out el temp.incorrect containers.
Qualtrax ID. 69151-1 Page 2 of 2
Page 12 of 13

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Pace Analytical Services,LLC
Pace 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
[phone]
January 16, 2024
Andrew Street
Apex Companies
5900-0 Northwoods Business
Parkway
Charlotte, NC 28269
RE: Project: SOUTHERNEASTERN FREIGHT-GREENS
Pace Project No.: 92707503
Dear Andrew Street:
Enclosed are the analytical results for sample(s)received by the laboratory on January 10,2024. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services-Asheville
• Pace Analytical Services-Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
"% JZ `/Ucu4a----
Bonnie Vang
[e-mail]
704-977-0968
Project Manager
Enclosures
cc: Kevin Cooke,Apex Comapnies, LLC
Kaitlyn Nootens,Apex Companies
Devin Politoske,Apex Companies, LLC
ICGR
2 " • REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
H/, without the written consent of Pace Analytical Services,LLC. Page 1 of 13

Pace Analytical Services,LLC
9800 KinceyAve. Suite 100
(/ ! ace Huntersville,NC 28078
[phone]
CERTIFICATIONS
Project: SOUTHERNEASTERN FREIGHT-GREENS
Pace Project No.: 92707503
Pace Analytical Services Charlotte
South Carolina Laboratory ID:99006 South Carolina Certification#:99006001
9800 Kincey Ave.Ste 100, Huntersville,NC 28078 South Carolina Drinking Water Cert.#:99006003
North Carolina Drinking Water Certification#:37706 Florida/NELAP Certification#:E87627
North Carolina Field Services Certification#:5342 Kentucky UST Certification#:84
North Carolina Wastewater Certification#:12 Louisiana DoH Drinking Water#:LA029
South Carolina Laboratory ID:99006 Virginia/VELAP Certification#:460221
Pace Analytical Services Asheville
2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030
Florida/NELAP Certification#:E87648 South Carolina Certification#:99030001
North Carolina Drinking Water Certification#:37712 Virginia/VELAP Certification#:460222
North Carolina Wastewater Certification#:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 2 of 13

Pace Analytical Services,LLC
ace9800 Kincey Ave. Suite 100
Huntersville,NC 28078
[phone]
SAMPLE SUMMARY
Project: SOUTHERNEASTERN FREIGHT-GREENS
Pace Project No.: 92707503
Lab ID Sample ID Matrix Date Collected Date Received
92707503001 OUTFALL 2 Water 01/09/24 11:15 01/10/24 08:50
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services,LLC. Page 3 of 13

Pace Analytical Services,LLC
ace 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: SOUTHERNEASTERN FREIGHT-GREENS
Pace Project No.: 92707503
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92707503001 OUTFALL 2 EPA 1664B DVR 1 PASI-C
SM 2540D-2015 RVS 1 PASI-A
EPA 9040C SMS 1 PASI-A
PASI-A=Pace Analytical Services-Asheville
PAST-C=Pace Analytical Services-Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 4 of 13

Pace Analytical Services,LLC
9800 Kincey Ave. Suite 100
ace` Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project: SOUTHERNEASTERN FREIGHT-GREENS
Pace Project No.: 92707503
Sample: OUTFALL 2 Lab ID: 92707503001 Collected: 01/09/24 11:15 Received: 01/10/24 08:50 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
HEM,Oil and Grease Analytical Method:EPA 1664E
Pace Analytical Services-Charlotte
Oil and Grease <4.9 mg/L 4.9 1.1 1 01/15/24 14:00
2540D Total Suspended Solids Analytical Method:SM 2540D-2015
Pace Analytical Services-Asheville
Total Suspended Solids 3.4 mg/L 2.5 2.5 1 01/11/24 01:31
9040 pH Analytical Method:EPA 9040C
Pace Analytical Services-Asheville
pH at 25 Degrees C 6.8 Std. Units 0.10 0.10 1 01/11/24 18:02 H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:01/16/2024 09:33 AM without the written consent of Pace Analytical Services,LLC. Page 5 of 13

Pace Analytical Services,LLC
9800 Kincey Ave. Suite 100
Pace. Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: SOUTHERNEASTERN FREIGHT-GREENS
Pace Project No.: 92707503
QC Batch: 825389 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM,Oil and Grease
Laboratory: Pace Analytical Services-Charlotte
Associated Lab Samples: 92707503001
METHOD BLANK: 4269283 Matrix: Water
Associated Lab Samples: 92707503001
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Oil and Grease mg/L <5.0 5.0 1.1 01/15/24 14:00
LABORATORY CONTROL SAMPLE: 4269284
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Oil and Grease mg/L 40 33.3 83 78-114
MATRIX SPIKE SAMPLE: 4269285
92707495002 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Oil and Grease mg/L ND 38.8 35.1 83 78-114
SAMPLE DUPLICATE: 4269286
92707501001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Oil and Grease mg/L 1.2J 1.3J 30
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:01/16/2024 09:33 AM without the written consent of Pace Analytical Services,LLC. Page 6 of 13

Pace Analytical Services,LLC
ace` 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: SOUTHERNEASTERN FREIGHT-GREENS
Pace Project No.: 92707503
QC Batch: 824717 Analysis Method: SM 2540D-2015
QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92707503001
METHOD BLANK: 4265953 Matrix: Water
Associated Lab Samples: 92707503001
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Total Suspended Solids mg/L <2.5 2.5 2.5 01/11/24 01:26
LABORATORY CONTROL SAMPLE&LCSD: 4265954 4265963
Spike LCS LCSD LCS LCSD %Rec Max
Parameter Units Conc. Result Result %Rec %Rec Limits RPD RPD Qualifiers
Total Suspended Solids mg/L 250 240 240 96 96 90-110 0 25
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:01/16/2024 09:33 AM without the written consent of Pace Analytical Services,LLC. Page 7 of 13

Pace Analytical Services,LLC
aced 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA
Project: SOUTHERNEASTERN FREIGHT-GREENS
Pace Project No.: 92707503
QC Batch: 824974 Analysis Method: EPA 9040C
QC Batch Method: EPA 9040C Analysis Description: 9040 pH
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92707503001
SAMPLE DUPLICATE: 4267174
92706177001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
pH at 25 Degrees C Std. Units 7.2 7.2 0 10 H3
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:01/16/2024 09:33 AM without the written consent of Pace Analytical Services,LLC. Page 8 of 13

Pace Analytical Services,LLC
ace 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
[phone]
QUALIFIERS
Project: SOUTHERNEASTERN FREIGHT-GREENS
Pace Project No.: 92707503
DEFINITIONS
DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot.
ND-Not Detected at or above adjusted reporting limit.
TNTC-Too Numerous To Count
J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL-Practical Quantitation Limit.
RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S-Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is
a combined concentration.
Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values.
LCS(D)-Laboratory Control Sample(Duplicate)
MS(D)-Matrix Spike(Duplicate)
DUP-Sample Duplicate
RPD-Relative Percent Difference
NC-Not Calculable.
SG-Silica Gel-Clean-Up
U-Indicates the compound was analyzed for,but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as
"Total"may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes.
TNI-The NELAC Institute.
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:01/16/2024 09:33 AM without the written consent of Pace Analytical Services,LLC. Page 9 of 13

Pace Analytical Services,LLC
Pace. 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SOUTHERNEASTERN FREIGHT-GREENS
Pace Project No.: 92707503
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92707503001 OUTFALL 2 EPA 1664B 825389
92707503001 OUTFALL 2 SM 2540D-2015 824717
92707503001 OUTFALL 2 EPA 9040C 824974
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:01/16/2024 09:33 AM without the written consent of Pace Analytical Services,LLC. Page 10 of 13

DC# Title: ENV-FRM-HUN1-0083 v03_Sample Condition Upon Receipt
lace
Effective Date: 11/29/2023 4:16:30 PM
Laboratory receiving samples:
Asheville❑ Edenf Greenwood❑ Huntersville Qh Raleigh❑ MechanicsvillPf-1 A+l ...a-n
Sample Coition",CoArtG",77 Client Name:
n WO : 9270750
Upon,Receipt. A I X; / Project#:
Courier: ❑/Fed Ex ❑UPS ❑USPS ❑Client tin I U tUU I L1It
❑ Commercial Q Pace ❑Other: 92707503
I_ I
Custody Seal Present? ❑Yes L✓J(No Seals Intact? Oyes ❑No l'N/A -1
Date/Initials Person Examining Contents: //TV/1...
Packing Material: 0 Bubble Wrap Bubble Bags ❑None ❑ Other Biological Tissure�Fdozen?
[
Thermometer: r7 ^ ❑Yes ❑No N/A
❑ IR Gun ID. n l ,—/'
,, i'/ /•f Type of Ice: 0/Net ❑Blue ❑None
`-) Correction Factor: .
Cooler Temp: "� Add/Subtract(SC) i Temp should be above freezing to 6°C
0 Samples out oftemp criteria.Samples on ice,cooling process
Cooler Temp Corrected: .): 1 has begun
USDA Regulated Soil ( N/A,water sample)
Did samples originate in a quarantine zone within the United States:CA,NY,or SC Did samples originate from a foreign source(internationally,
(check maps)?❑Yes ❑No including Hawaii and Puerto Rico)?❑Yes 0 No
Comments/Discrepancy:
Chain of Custody Present? dies 0 No ]N/A 1.
Samples Arrived within Hold Time? VYes 0 No ❑N/A 2.
Short Hold Time Analysis(<72 hr.)? Dyes G] oo ❑N/A 3.
Rush Turn Around Time Requested? 0rlyes Q/No ❑N/A 4.
Sufficient Volume? Lrv(l'es
JYes ❑No ❑N/A 5.
Correct Containers Used? 0 No ❑N/A 6. ,
-Pace Containers Used? es 0 No ❑N/A
Containers Intact? Vies ❑ o ❑N/A 7.
Dissolved analysis:Samples Field Filtered? ❑ es W No ❑N/A 8.
Sample Labels Match COC? 1 dYes 0 No ❑N/A 9.
-Includes Date/Time/ID/Analysis Matrix: V1/ ------- /
Headspace in VOA Vials(>5-6mm)? Dyes ❑No L„t!/M/A 10.
E
Trip Blank Present? ❑yes ❑No N/A 11.
Trip Blank Custody Seals Present? Dyes ❑No Gd N/A
COMMENTS/SAMPLE DISCREPANCY Field Data Required? ❑Yes ❑No
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: Date/Time:
Project Manager SCURF Review: Date:
Project Manager SRF Review: Date:
Qualtrax ID: 69614 Paae 1 of 2
Page 11 of 13

Effective Date: 11/14/2022
'Check mark top half of box if pH and/or dechlorination is verified and Project s wo : 92707503
within the acceptance range for preservation samples. PM: BV Due Date: 01/17/24
Exceptions:VOA,Coutorm,TOC,Oil and Grease,Dft0/8015(water)DOC.Uric CLIENT: 92—APEX MOOR
°°Bottom half of box is to list number of bottles
""Check all unpreserved Nitrates for chlorine
z
1 � i _ = _ zip _ z
Z 2 Z Q U A ? �r d ` ; o Z
a Q Z a
Z ry �` .N+ C = a �r y lJ 7 z = I i o' 'a U
u 09 v v dS O v l _ Y v S 4 a x Q q v EP F. w
aZi u cZi Z.c LP n' a m y z z J y l7 Z �' O V io N
01 G N R I+1 r ,n = V (a Q M ♦' Z 1 u - N a > 2
a c. c u O O d p A c O `'^, v p ? xa .' x c c a
c c a N Z Z m e v O �r x x ^ c n m ? O c E
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pH Adjustment Log for Preserved Samples
Sample ID Type of Preservative j pH upon receipt I Date preservation adjusted Time preservation amount of Preservative T Lot It
adjusted added
\ \
rlote- Whenever there is a discrepancy affecting North Carolina compliance sarsp!es.a copy of this form will be sect to the North Carolina DENS Certification Office(i c
Out of hold,ocorrect preservative,out of temp.incorrect conla:nors.
Qualtrax ID. 6961.1 Page 2 of 2
Page 12 of 13

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sample. ;II Pogo 13 of 13

Discharge Monitoring Report—NCG080590 April 30, 2024
Southeastern Freight Lines—GBO Page 5
Attachment 4
Photo Log

Site Photographs - 01/09/2024 8718 West Market St.
Apex Companies, LLC Greensboro , NC
Photograph 1 i
Description: Overview of a 1 � �`,
outfall /'.; `
y riv� c,y,Y, Y',.
1:Or T'..‘ 14.'113''------- 7.'',75.,,,k 7;''. ,'
y G,
Y ''� 7/4 4 _ im 4
J
t $k
�,d fw aJr Yi ,
•
r y sir. , r
Photograph 2M
Description: Sample bottle for
outfall 1 44
IIIIIIIIIII
Photograph 3
Description: PH reading for
outfall 2
I. II 71 ' 1 ' 1 ' 1 l 1
11 t, i'I .; NN►II !,I r.
~'v
'`
APEX

Site Photographs - 01/09/2024 8718 West Market St.
Apex Companies, LLC Greensboro , NC
Photograph 4 a ,
Description: Overview of
outfall 2
4 w4 0.A k .'� z f 14
.1 �, '" Akan ' "�'` f >' r`h .ii ',`.,' .",
e�
NwAto
v' `rjr, ,, 'fir i •;S" clliv'3 ,-,,-
° a •
Photograph. 5 � a
Description: Sample from
outfall 2 ,.
' % -
Photograph. 6
Description: PH Reading from `>a.` ^=b (aa
outfall2 �" .
1,4 -, #-, I 24.4„ ,,,z,ii.iit)
,gx �l
`yri ,a
. , 11!i,,
,,r,,t .
APEX