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Home My WebLink AboutNCG200344_DMR_20220502 NC Department of Environmental Qualit Received Y NCDEQ Division of Energy, Mineral and Land Resources ��`;�Y o 2 20�2 Stormwater Discharge Monitoring Report(DMR) Form for NCG200000 Winston-5:I:em Scrap Metal R" Tonal Gtiice Click here for instructions Complete,sign,scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report(DMR)Upload form within 30 days of receiving sampling results. Mail the original,signed hard copy of the DMR to the appropriate DEMLR Regional Office. Certificate of Coverage No. NCG20 0344 Person Collecting Samples: Beverly King Facility Name:Cranford Iron and Metal Company Laboratory Name: Pace Analytical Facility County: Randolph Laboratory Cert. No.: 12 Discharge during this period: ✓❑ Yes ❑ No (if no,skip to signature and date) Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances?❑✓ Yes ❑ No If so, which Tier(I, II,or III)? I A copy of this DMR has been uploaded electronically via https://edocs.deq.nc.gov/Forms/SW-DMR ❑ Yes ❑ No Date Uploaded: Analytical Monitoring Requirements for Outfalls with Industrial Activities—Benchmarks in(Red) Parameter Parameter Outfall 1 Outfall Outfall Outfall Outfall Code N/A Receiving Stream Class WS.II HQW N/A Date Sample Collected MM/DD/YYYY 3/17/2022 46529 24-Hour Rainfall in inches C0530 TSS in mg/L(100 or 50*) 4.0 00340 Chemical Oxygen Demand (120) 34.2 00552 Non-Polar Oil&Grease in mg/L(15) <5.0 01119 Copper,total recoverable in mg/L (0.010 FW,0.005 SW) 0.0262 01051 Lead,total recoverable(as Pb)in <0.005 L(0.075 FW,0.220 SW) 0.005 C0034 Zinc,total recoverable in mg/L(0.126 0.121 FW,0.095 SW) Additional parameters for outfalls in drainage areas that use>55 gallons per month of new hydraulic oil on average NCOIL Estimated New Motor/Hydraulic Oil N/A Usage in gal/month *Outfalls to Outstanding Resource Waters(ORW),High Quality Waters(HQW),Trout Waters(Tr)and Primary Nursery Areas(PNA) have a benchmark TSS limit of 50 mg/L.All other water classifications have a benchmark of 100 mg/L FW(Freshwater)SW(Saltwater) Notes(optional): "I certify by my signature below,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who manage the system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations." � 1-/- aU. aoas Signatur of Per ' tee or Delegated Authorized Individual Date Email Address Phone Number Pace Analytical Services,LLC ® 9800 Kincey Ave. Suite 100 aceAnalyfical Huntersville,NC 28078 www.pecelebs.com (704)875-9092 CERTIFICATIONS Project: CRANFORD IRON AND METAL Pace Project No.: 92594214 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 South Carolina Certification#:99006001 9800 Kincey Ave.Ste 100, Huntersville, NC 28078 South Carolina Drinking Water Cert.#:99006003 North Carolina Drinking Water Certification#:37706 Florida/NELAP Certification#: E87627 North Carolina Field Services Certification#:5342 Kentucky UST Certification#:84 North Carolina Wastewater Certification#: 12 Louisiana DoH Drinking Water#:LA029 South Carolina Laboratory ID:99006 VirginiaNELAP Certification#:460221 Pace Analytical Services Asheville 2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030 Florida/NELAP Certification#: E87648 South Carolina Certification#:99030001 North Carolina Drinking Water Certification#:37712 VirginiaNELAP Certification#:460222 North Carolina Wastewater Certification#:40 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC, Page 2 of 15 Pace Analytical Services,LLC ® 9800 Kincey Ave. Suite 100 aceAnalytical Huntersville,NC 28078 www.pacelabs.com (704)875-9092 SAMPLE ANALYTE COUNT Project: CRANFORD IRON AND METAL Pace Project No.: 92594214 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92594214001 OUTFALL 001 EPA 1664B ICO 1 PASI-C EPA 1664E ICO 1 PASI-C EPA 200.7 Rev 4.4 1994 KH 3 PASI-A SM 2540D-2015 MAB2 1 PASI-A EPA 9040C YEG 1 PASI-A SM 5220D-2011 JP1 1 PASI-A PASI-A=Pace Analytical Services-Asheville PASI-C=Pace Analytical Services-Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 3 of 15 Pace Analytical Services,LLC 9800 Kincey Ave. Suite 100 aceAnalytical Huntersville,NC 28078 www.pecelebs.com (704)875-9092 ANALYTICAL RESULTS Project: CRANFORD IRON AND METAL Pace Project No.: 92594214 Sample: OUTFALL 001 Lab ID: 92594214001 Collected: 03/17/22 12:50 Received: 03/18/22 09:40 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM,Oil and Grease Analytical Method:EPA 1664E Pace Analytical Services-Charlotte Oil and Grease ND mg/L 5.0 1 03/21/22 23:53 1664 SGT-HEM,TPH Analytical Method:EPA 1664E Pace Analytical Services-Charlotte Total Petroleum Hydrocarbons ND mg/L 5.0 1 03/21/22 23:53 200.7 MET ICP Analytical Method:EPA 200.7 Rev 4.4 1994 Preparation Method:EPA 200.7 Rev 4.4 1994 Pace Analytical Services-Asheville Copper 26.2 ug/L 5.0 1 03/19/22 18:47 03/21/22 22:55 7440-50-8 Lead ND ug/L 5.0 1 03/19/22 18:47 03/21/22 22:55 7439-92-1 Zinc 121 ug/L 10.0 1 03/19/22 18:47 03/21/22 22:55 7440-66-6 2540D Total Suspended Solids Analytical Method:SM 2540D-2015 Pace Analytical Services-Asheville Total Suspended Solids 4.0 mg/L 2.8 1 03/21/22 13:07 9040 pH Analytical Method:EPA 9040C Pace Analytical Services-Asheville pH at 25 Degrees C 8.1 Std.Units 0.10 1 03/22/22 12:57 H3 5220D COD Analytical Method:SM 5220D-2011 Preparation Method:SM 5220D-2011 Pace Analytical Services-Asheville Chemical Oxygen Demand 34.2 mg/L 25.0 1 03/25/22 01:28 03/25/22 04:31 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/25/2022 02:30 PM without the written consent of Pace Analytical Services,LLC. Page 4 of 15 Pace Analytical Services,LLC ® 9800 KinceyAve. Suite 100 aceAnalytical Huntersville,NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: CRANFORD IRON AND METAL Pace Project No.: 92594214 QC Batch: 686263 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 HEM,Oil and Grease Laboratory: Pace Analytical Services-Charlotte Associated Lab Samples: 92594214001 METHOD BLANK: 3588113 Matrix: Water Associated Lab Samples: 92594214001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 03/21/22 23:53 LABORATORY CONTROL SAMPLE: 3588114 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Oil and Grease mg/L 40 35.4 88 78-114 MATRIX SPIKE SAMPLE: 3588115 92594214001 Spike MS MS %Rec Parameter Units Result Conc. Result %Rec Limits Qualifiers Oil and Grease mg/L ND 40 34.5 83 78-114 SAMPLE DUPLICATE: 3588116 35704294001 Dup Parameter Units Result Result RPD Qualifiers Oil and Grease mg/L 1.1U 1.2J Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/25/2022 02:30 PM without the written consent of Pace Analytical Services,LLC. Page 5 of 15 Pace Analytical Services,LLC ace Analytical® 9800 KinceyAve. Suite 100 Huntersville,NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: CRANFORD IRON AND METAL Pace Project No.: 92594214 QC Batch: 686269 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM,TPH Laboratory: Pace Analytical Services-Charlotte Associated Lab Samples: 92594214001 METHOD BLANK: 3588125 Matrix: Water Associated Lab Samples: 92594214001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 03/21/22 23:53 LABORATORY CONTROL SAMPLE: 3588126 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 17.8 89 64-132 MATRIX SPIKE SAMPLE: 3588127 92594214001 Spike MS MS %Rec Parameter Units Result Conc. Result %Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 20 14.4 66 64-132 SAMPLE DUPLICATE: 3588128 35704294001 Dup Parameter Units Result Result RPD Qualifiers Total Petroleum Hydrocarbons mg/L 5.0U ND Results presented on this page are in the units Indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/25/2022 02:30 PM without the written consent of Pace Analytical Services,LLC. Page 6 of 15 Pace Analytical Services,LLC 9800 KinceyAve. Suite 100 aceArialytical® Huntersville,NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: CRANFORD IRON AND METAL Pace Project No.: 92594214 QC Batch: 685960 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92594214001 METHOD BLANK: 3586865 Matrix: Water Associated Lab Samples: 92594214001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper ug/L ND 5.0 03/21/22 21:18 Lead ug/L ND 5.0 03/21/22 21:18 Zinc ug/L ND 10.0 03/21/22 21:18 LABORATORY CONTROL SAMPLE: 3586866 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Copper ug/L 500 505 101 85-115 Lead ug/L 500 485 97 85-115 Zinc ug/L 500 476 95 85-115 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3586867 3586868 MS MSD 92593976001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Copper ug/L 69.8 500 500 586 585 103 103 70-130 0 Lead ug/L ND 500 500 444 447 88 89 70-130 1 Zinc ug/L 238 500 500 708 714 94 95 70-130 1 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3586869 3586870 MS MSD 92594264001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Copper ug/L ND 500 500 494 491 99 98 70-130 1 Lead ug/L ND 500 500 482 479 96 96 70-130 1 Zinc ug/L 114 500 500 588 584 95 94 70-130 1 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/25/2022 02:30 PM without the written consent of Pace Analytical Services,LLC. Page 7 of 15 Pace Analytical Services,LLC 9cac100 _.( eAnalytical® 9800Hunte sville,NCKincey Ave. 1te 280778 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: CRANFORD IRON AND METAL Pace Project No.: 92594214 QC Batch: 686030 Analysis Method: SM 2540D-2015 QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92594214001 METHOD BLANK: 3587064 Matrix: Water Associated Lab Samples: 92594214001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 03/21/22 13:05 LABORATORY CONTROL SAMPLE: 3587065 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Total Suspended Solids mg/L 250 244 98 90-110 SAMPLE DUPLICATE: 3587261 92594270001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 251 266 6 SAMPLE DUPLICATE: 3587262 92594330001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 126 107 16 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/25/2022 02:30 PM without the written consent of Pace Analytical Services,LLC. Page 8 of 15 Pace Analytical Services,LLC ® 9800 Kincey Ave. Suite 100 aceAnalytical Huntersville,NC 28078 www.pacelabs.cem (704)875-9092 QUALITY CONTROL DATA Project: CRANFORD IRON AND METAL Pace Project No.: 92594214 QC Batch: 686344 Analysis Method: EPA 9040C QC Batch Method: EPA 9040C Analysis Description: 9040 pH Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92594214001 SAMPLE DUPLICATE: 3588259 92593860001 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std.Units 7.2 7.2 0 H3 SAMPLE DUPLICATE: 3588260 92594248002 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std.Units 7.8 7.8 0 H3 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/25/2022 02:30 PM without the written consent of Pace Analytical Services,LLC. Page 9 of 15 Pace Analytical Services,LLC aceAnalytical® 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 www.pacslabs.cem (704)875-9092 QUALITY CONTROL DATA Project: CRANFORD IRON AND METAL Pace Project No.: 92594214 QC Batch: 686904 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92594214001 METHOD BLANK: 3590887 Matrix: Water Associated Lab Samples: 92594214001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 03/25/22 04:26 LABORATORY CONTROL SAMPLE: 3590888 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 786 105 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3590889 3590890 MS MSD 92593364001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Chemical Oxygen Demand mg/L 92.6 100 100 188 186 96 93 90-110 1 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3590891 3590892 MS MSD 92593511002 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Chemical Oxygen Demand mg/L 41.2 100 100 139 139 98 98 90-110 0 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/25/2022 02:30 PM without the written consent of Pace Analytical Services,LLC. Page 10 of 15 Pace Analytical Services,LLC aceAnalytical 9800 Kincey Ave. Suite100 Huntersville,NC 28078078 www.pecelebs.com (704)875-9092 QUALIFIERS Project: CRANFORD IRON AND METAL Pace Project No.: 92594214 DEFINITIONS DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot. ND-Not Detected at or above adjusted reporting limit. TNTC-Too Numerous To Count J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL-Practical Quantitation Limit. RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S-Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is a combined concentration. Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values. LCS(D)-Laboratory Control Sample(Duplicate) MS(D)-Matrix Spike(Duplicate) DUP-Sample Duplicate RPD-Relative Percent Difference NC-Not Calculable. SG-Silica Gel-Clean-Up U-Indicates the compound was analyzed for,but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as "Total"may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes. TNI-The NELAC Institute. ANALYTE QUALIFIERS H3 Sample was received or analysis requested beyond the recognized method holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/25/2022 02:30 PM without the written consent of Pace Analytical Services,LLC. Page 11 of 15 Pace Analytical Services,LLC ® 9800 Kincey Ave. Suite 100 _ aceAnalytical Huntersville,NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: CRANFORD IRON AND METAL Pace Project No.: 92594214 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92594214001 OUTFALL 001 EPA 1664B 686263 92594214001 OUTFALL 001 EPA 1664E 686269 92594214001 OUTFALL 001 EPA 200.7 Rev 4.4 1994 685960 EPA 200.7 Rev 4.4 1994 685977 92594214001 OUTFALL 001 SM 2540D-2015 686030 92594214001 OUTFALL 001 EPA 9040C 686344 92594214001 OUTFALL 001 SM 5220D-2011 686904 SM 5220D-2011 687211 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/25/2022 02:30 PM without the written consent of Pace Analytical Services,LLC. Page 12 of 15 Document Name: Document Revised:November 15,2021 Sample Condition Upon Receipt(SCUR) Page 1 of 2 i aceAnalytical Document No.: Issuing Authority: F-CAR-CS-033-Rev.08 Pace Carolinas Quality Office Laboratory receiving samples: • Asheville❑ EdenE Greenwood E Huntersville❑ Raleigh❑ Mechanicsville❑ Atlanta❑ Kernersville❑ Sample Condition Client Name: Upon Receipt f'll/ I d ,�] I j�,� t C_ ��( ProjecWOE 92594214Courier: ❑/Fed Ex L❑IUPS ❑LISPS ❑Client 0 Commercial ❑Pace ❑Other: II I II'I Iilll I I II I II III Custody Seal Present? Des ❑No Seals intact? ❑Yes ONo 92594214 Date/initials Person Examining Contents; 1 i) 5. �,7 Packing Material: ❑Bubble Wrap ❑Bubble Bags ❑None ❑ Other Biological Tissue Frozen? Thermometer; Eves ❑No ON/A IR Gun ID: l ` (.' ❑Wet ❑Blue ❑None / Type of Ice: • Correction Factor: Cooler Temp: 3."1 Add/Subtract(CC) ; ) Temp should be above freezing to 6°C ❑Samples out of temp criteria.Samples on ice,cooling process Cooler-Temp-Corrected-('CI: tin-bERTB USDA Regulated Soli(❑N/A,water sample) Did samples originate in a quarantine zone within the United States:CA,NY,or SC(check maps)? Did samples originate from a foreign source(internationally, Des END including Hawaii and Puerto Rico)?Elves ENo Comments/Dlscrepa ncy: Chain of Custody Present? Oyes ONo ON/A 1. Samples Arrived within Hold Time? ( Yes ONo ON/A 2. Short Hold Time Analysis(<72 hr.)? Oyes [No_ ON/A 3. Rush Turn Around Time Requested? Dyes ONo ON/A 4. Sufficient Volume? Oyes ONo ON/A 5. Correct Containers Used? Oyes ONo ' ON/A 6. •Pace Containers Used? Oyes ONo ❑N/A Containers Intact? Dyes [No ❑N/A 7. Dissolved analysis:Samples Field Filtered? Des ❑No ON/A 8. Sample Labels Match CDC? Oyes ONo ON/A 9. -Includes Date/Time/ID/Analysis Matrix: Headspace in VOA Vials(>5.6mm)? Oyes ONo ON/A 10. Trip Blank Present? Oyes ONo ON/A 11. Trip Blank Custody Seals Present? Des ONo ON/A COMMENTS/SAMPLE DISCREPANCY Field Data Required? Dyes ONo Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Date/Time: Project Manager SCURF Review: Date: Project Manager SRF Review: • Date: Page 13 of 15 Document Name: Document Revised:November 15,2021 Sample Condition Upon Receipt(SOUR) Page 2 of 2 • 7/7:6aceAnalytical a Document No,: Issuing Authority: f-CAR•C5.033•Rev.08 Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is Project d . W��`# ��,�w 4214 verified and within the acceptance range for preservation y samples. Due Date: 03/29/22 Exceptions:VOA,Coliform,TOC,Oil and Grease,DRO/8015(water)DOC,LLHg PM: TIH **Bottom half of box is to list number of bottles CLIENT: 92-MID ATLAN Z Q a -- I v \ z ; . s R 2 2 Z z ry N 2 8. Z - N ` 4 2 ro m '5 "> v a, aa' v oa .o a�i N a C I I °" u , m 2 2 a n = ° = m N w % a Z v ? \ \ 8 . '' a, a,, ar Z ro a a z al, a 2 rc 2 z 0 v v N v m u '^ r T v iu i z l7 N r a a n v ON O a =D v a a S a O °� 44 m 2 .� N a '> T > > > CC I▪ Z N z 3 C U N N a ? vNi a O v, > . z j oC n u u 7 u u u _ w 2 T U , m , « a el - 7. " t'n •euu .. Y '« y a`i a, E = 2 O i le Y v v iu ,o io ro .- n :o v o' d L E a E ° a a a a y a, A E .c - a a J J a a J a a E. E a a J E ^i O 0 O O ri G ,n an ' a ,n a n o o v E E E E v a E u E .an E E E E % E E E of E E 0 ryry 3 ,e V0 N0N N VI N ,N-, N _rl ti "' ,-I r, N rl N L] I O Y Y � „N.� 4 N - O O i r ,ti N m LL _ — —d x gm m m m m m m m3 aV aL ea 4' V '4 2 > > V > a 'i-- 1a. Ft > O I. ,' 2 3 4 7 gglill .- 6 gli RgRil 1110‘111 1, igh h gl 1116„ 1.0 g gg 11 12 f pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative Lot 1a adjusted added • Note: Whenever there is a discrepancy affecting North Carolina compliance samples,a copy of this form will be sent to the North Carolina OEHNR Certification Office(I.e. Out of hold,incorrect preservative,out of temp,incorrect containers, Page 14 of 15 ci \\\\\\ S • (N/A) W G :: :: cv 0 0 a` y 4) c. gill— 0 L L u > CO .S to y d (p 2 N (N/A)sal uo ael No 0: P aue2f N w • 3 (N/A)aupo140 Ienplse8II o 0,ui dale' Q E N\ i U a. Z p W Z CW.1 U cc X >- L L F re o W R >- cr E v = Z D y > `y cg out x r. v § L. L .0 r .eddo0 x 1 O v > peel x 4-1 E z } COO x O cn CO 8 F ° v g. .v r asa p pue coI x • F. f a cr a, CC SS x a / o CD m o o IN/A peel slsAteuy I 8 Uti ° CZ Q 3 I0ue41eW 1111 0 g c o 5 7 No :• , v a a t(YSeN a • ! a Y HQeEHIIIIIIIIIII oY oC Q 7 rncu co 10III af `-) a E O € OSH0 u Z p e0 ew, ,L,,,,a - pa/uasaidun N w H 0m `. o v "` m S2i3NIVINOO dO t/ (o 1 ` V) ` ¢ U a a¢a a n V y NO110311001V dW31 31dWVS j ( z, /- J L'' U- U U, W -/o Q F E l^,S Qa Qrai ti Z ? c • z o o a h{ a W U m in Pia < ^ 2 Z )-E CC o U L E c 0 z Z i (31 z •c ... W O a En" c a) _1 W cD (0 "") w - F J aP. E c 1 r g O co h W } d (a a o3 - o u I- 1 A. m Fa e E • a ° TO U c o O f Y o U CZ 8V219=9) 3dA131dWVS U' a U Z Z e U p d (yal o)sepoa peen eas) 3000 XIalVW s CO i. Oa U E I o um) Z ro gE S O '' a y ? 3 q C.) a a eU S a ho �or 'aU ( w W w ` c in O G a it 2 W W 4 =C W J co V K Z 7 c E o >� o33auob3a8P O N O co ' O N C U W F (0 70 c 0)• E 00 W - C 0 U o 'c • ' 0 z = f Q > N Eko `s LLJ m J n U N U - J 0 I- a. Q o N Z o O (D c C N F. Z Q 0€ � a —oQ = a .� u o m ❑ u uJ roc v 1 ) N o `o p E p U .. _O O 0 c N 4 \ ¢ 9 v rn d rns O ry d L c E a m o a #Van N M a )n W n. W W ? iN- • (n& 0 a 1 a et Page 15 of 15 N C Department of Pace Analytical Services,LLC ® aceAnalyt Environmental Quality 9800 KinceyAve. Suite 100 ical Received Huntersville,NC 28078 2 www.pecelebs.eom MAY 0 2022 (704)875-9092 Winston-Salem Regional Office March 25, 2022 • Chuck Hoffman Mid-Atlantic Associates, Inc 409 Rogers View Court Raleigh, NC 27610 RE: Project: CRANFORD IRON AND METAL Pace Project No.: 92594214 Dear Chuck Hoffman: Enclosed are the analytical results for sample(s)received by the laboratory on March 18, 2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services-Asheville • Pace Analytical Services-Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, I-li s— Tyriek Hooks tyriek.hooks@pacelabs.com (704)875-9092 • Project Manager Enclosures cc: Ron Davis,Mid Atlantic Associatees, Inc. . AC \�/►'' REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 1 of 15