NCS000315 DMR SW (Report - Not on DMR) (2)

neAvveo"
solutions
January 8, 2015
Division of Water Quality
Surface Water Protection Section
Attention: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
9-.0 '5 3Waterwaya
Square Place
Suite 1000
Re: Semi -Annual Storm Water Sampling Results for Year 5, Period 2
Nexeo Solutions, LLC
3930 Glenwood Avenue
Charlotte, Mecklenburg County, North Carolina
EPA ID #NCD 061 263 315
Dear Ms. Cannon:
The Woodlands, TX 77380
I/ C's aa03/S�
JAN 14 2015
CENTRAL FILES
SWR SECTION
Nexeo Solutions, LLC (Nexeo) conducted the semi-annual analytical monitoring event for Year 5, Period
2 at the Nexeo facility located at 3930 Glenwood Drive in Charlotte, Mecklenburg County, North
Carolina, on December 6, 2014 as prescribed in the National Pollutant Discharge Elimination System
(NPDES) permit (NCS000315). Per the requirements, the storm water sample was collected from the
storm water disc arge outfall (SDO) 001 during a representative storm event that consisted of 0.13 inches
of total rainfall, as measured by the local United States Geological Survey (USGS) rain gage (number
351412080541245 CRN -53). More than 72 hours of 0.00 inches of rainfall occurred prior to the sampling.
During the sampling event, a visual inspection for qualitative monitoring was conducted as specified in
Table 4 of the NPDES permit. No atypical conditions were noted during the field inspection. In
accordance with Section C. of the permit, in the event that an atypical condition is noted at a stormwater
discharge outfal I, the permittee shall document the suspected cause of the condition and any actions taken
in response to the discovery in the Stormwater Pollution Prevention Plan (SPPP). The inspection results
are presented in Table 1.
Table 1
Discharge Characteristic
Inspection Result
Color
Clear
Odor
No odor detected
Clarity
Clear
Floating Solids
None observed
Suspended Solids
None observed
Foam
None observed
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Table 1 (cont.)
3 Waterway Square Place
Suite 1000
The Woodlands, TX 77380
Discharge Characteristic
Inspection Result
Oil Sheen
None observed
Erosion/Deposition at the
Outfall
None observed
Other Obvious Indicators
of Storm water Pollution
None observed
The sample was collected in laboratory -supplied bottles, preserved with ice, and transported with a trip
blank to the Test America, Inc. laboratory in Savannah, Georgia. The sample was then analyzed for total
suspended solids, oil and grease, chemical oxygen demand, toluene, total xylenes, and pH. None of the
results exceeded its corresponding benchmark value. The results of the storm water sample analyses along
with their corresponding benchmark values as listed in the permit are presented below in Table 2, and the
laboratory results are included as Enclosure 1.
Table 2
Discharge Characteristic
Result
Benchmark Value
Total Suspended Solids
6.5 milligrams/liter (mg/L)
100 mg/L
Oil and Grease
<2.5 mg/L
30 mg/L
Chemical Oxygen Demand
25 mg/L
120 mg/L
Toluene
<0.0010 mg/L
0.055 mg/L
Xylenes, Total
<0.0020 mg/L
6.7 mg/L
H
7.20
6-9
Total Rainfall
0.13 inches
Required to be >
0.1 inches
Nexeo will continue semi-annual monitoring under the expired permit NCS000315 until the new permit
is issued. We will conduct the next monitoring event (Year 6, Period 1) between January 1 and June 30,
2015, and will submit the results per the requirements of the permit. Should you have any questions or
require additional information, please contact me at 704-392-2121.
Sincerely,
Nexeo Solutions, LLC
�*A:a alA�
Michael Trull
Plant Manager
NexeoSolutions.com I Connect.

,Enclosure 1

TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
TestAmerica Job ID: 680-108001-1
Client Project/Site: Nexeo Solutions LLC Charlotte
For:
Nexeo Solutions, LLC
3 Waterway Square Place
Suite 1000
The Woodlands, Texas 77380
Attn: Ms. Hanh Duong
Authorized for release by:
12/19/2014 8:34:00 AM
Bernard Kirkland, Manager of Project Management
[phone] e.3238
[e-mail]
Designee for
Jerry Lanier, Project Manager 1
[phone] e.3410
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Definitions/Glossary
Client: Nexeo Solutions, LLC
Project/Site: Nexeo Solutions LLC Charlotte
Qualifiers
General Chemistry
Qualifier Qualifier Description
HF Field parameter with a holding time of 15 minutes Test performed by laboratory at client's request.
C
Abbreviation These commonly used abbreviations may or may not be present in this report.
n Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Job ID: 680-108001-1
TestAmerica Savannah
Page 2 of 16 12/19/2014

Sample Summary
Client: Nexeo Solutions, LLC
Project/Site: Nexeo Solutions LLC Charlotte
TestAmerica Job ID: 680-108001-1
TestAmerica Savannah
Page 3 of 16 12/19/2014
L
Lab Sample ID
680-108001-1
680-108001-2
Client Sample ID
Outfall 001
Trip Blank
Matrix
Water
Water
Collected
12/06/14 14 30
12/06/14 00.00
Received
12/09/14 09 59
12/09/14 09.59
TestAmerica Savannah
Page 3 of 16 12/19/2014
L

Method Summary
Client: Nexeo Solutions, LLC
Project/Site: Nexeo Solutions LLC Charlotte
TestAmerica Job ID: 680-108001-1
Method Method Description
Protocol
Laboratory
624 Volatile Organic Compounds (GC/MS)
40CFR136A
TAL SAV
1664A HEM and SGT -HEM
1664A
TAL SAV
SM 2540D Solids, Total Suspended (TSS)
SM
TAL SAV
SM 4500 H+ B pH
SM
TAL SAV
SM 5220D COD
SM
TAL SAV
Protocol References:
1664A = EPA -821-98-002
40CFR136A = "Methods for Organic Chemical Analysis of Municipal Industrial Wastewater', 40CFR,
Part 136, Appendix A, October 26, 1984 and
subsequent revisions.
SM = "Standard Methods For The Examination Of Water And Wastewater',
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Page 4 of 16
TestAmerica Savannah
12/19/2014
C

Case Narrative
Client: Nexeo Solutions, LLC
Project/Site: Nexeo Solutions LLC Charlotte
TestAmerica Job ID: 680-108001-1
Job ID: 680-108001-1
Laboratory: TestAmerica Savannah a
Narrative
CASE NARRATIVE
Client: Nexeo Solutions, LLC
Project: Nexeo Solutions LLC Charlotte
Report Number: 680-108001-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the
reporting limits are adjusted relative to the dilution required.
RECEIPT
The samples were received on 12/09/2014; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 2.9 C.
VOLATILE ORGANIC COMPOUNDS (GC -MS)
Samples Outfall 001 (680-108001-1) and Trip Blank (680-108001-2) were analyzed for Volatile Organic Compounds (GC -MS) in
accordance with EPA Method 624. The samples were analyzed on 12/10/2014.
Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with batch 362619.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
OIL AND GREASE AND TPH
Sample Outfall 001 (680-108001-1) was analyzed for Oil and Grease and TPH in accordance with EPA Method 1664A. The samples were
prepared and analyzed on 12/18/2014.
Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate (MS/MSD/DUP) associated
with batch 363886.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TOTAL SUSPENDED SOLIDS
Sample Outfall 001 (680-108001-1) was analyzed for total suspended solids in accordance with SM 2540D. The samples were analyzed
on 12/11/2014.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CHEMICAL OXYGEN DEMAND
Sample Outfall 001 (680-108001-1) was analyzed for chemical oxygen demand in accordance with SM 5220D. The samples were
analyzed on 12/15/2014.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CORROSIVITY (PH)
Sample Outfall 001 (680-108001-1) was analyzed for corrosivity (pH) in accordance with SM 4500 H+ B. The samples were analyzed on
12/10/2014.
TestAmerica Savannah
Page 5 of 16 12/19/2014

Case Narrative
Client: Nexeo Solutions, LLC
Project/Site: Nexeo Solutions LLC Charlotte
TestAmerica Job ID: 680-108001-1
Job ID: 680-108001-1 (Continued)
Laboratory: TestAmerica Savannah (Continued)
This analysis is normally performed in the field and has a method -defined holding time of 15 minutes. This sample(s) was performed in ,
the laboratory outside the 15 minute timeframe.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TestAmerica Savannah
Page 6 of 16 12/19/2014

TestAmerica Savannah
Page 7 of 16 12/19/2014
Client Sample Results
Client: Nexeo Solutions, LLC
TestAmerica Job ID: 680-108001-1
Project/Site: Nexeo Solutions LLC Charlotte
Client Sample ID: Outfall 001
Lab Sample ID: 680-108001-1
Date Collected: 12/06/1414:30
Matrix: Water
Date Received: 12/09/14 09:59
Method: 624 - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D
Prepared Analyzed
Dil Fac
Toluene
<1.0
1.0
ug/L
12110/14 2389
1
Xylenes, Total
<2.0
2.0
ug/L
12/10/14 2339
1
Surrogate
%Recovery Qualifier
Limits
Prepared Analyzed
Dil Fac
Toluene -d8 (Surr)
102
79-119
12/10/14 23:39
1
Dibromofluoromethane (Surf)
106
77-129
12/10/14 2339
1
1,2-Dichloroethane-d4 (Sun-)
104
70-130
12/10/14 23:39
1
4-Bromofluorobenzene (Surr)
95
71-121
12/10/14 23:39
1
General Chemistry
Analyte
Result Qualifier
NONE
NONE Unit
D
Prepared Analyzed
Dil Fac
pH
7.20 HF
SU
12/10/1417:55
1
Analyte
Result Qualifier
RL
MDL Unit
D
Prepared Analyzed
Dil Fac
HEM (Oil & Grease)
<2.5
2.5
mg/L
12/18/14 12:04 12/18/14 12:48
1
Chemical Oxygen Demand
25
10
mg/L
12/15/14 12:55
1
Analyte
Result Qualifier
RL
RL Unit
D
Prepared Analyzed
Dil Fac
Total Suspended Solids
6.5
5.0
mg/L
12/11/14 13 46
1
Lab Sample ID: 680-108001-2
Client Sample ID: Trip Blank
Date Collected: 12/06/14 00:00
Matrix: Water
Date Received: 12/09/14 09:59
Method: 624 - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D
Prepared Analyzed
Dil Fac
Toluene
<1.0
1.0
ug/L
-T2-/10/1423 11
1
Xylenes, Total
<2.0
2.0
ug/L
12110/14 23:11
1
Surrogate
%Recovery Qualifier
Limits
Prepared Analyzed
Dil Fac
Toluene -d8 (Surr)
96
79-119
12/10114 23:11
1
Dibromofluoromethane (Surr)
112
77-129
12/10/14 23.11
1
1,2-Dichloroethane-d4 (Surr)
115
70-130
12/10/14 23.11
1
4-Bromofluorobenzene (Surr)
95
71-121
12/10/14 23:11
1
TestAmerica Savannah
Page 7 of 16 12/19/2014

QC Sample Results
Client: Nexeo Solutions, LLC
Project/Site: Nexeo Solutions LLC Charlotte
Method: 624 - Volatile Organic Compounds (GC/MS)
Lab Sample ID: MB 680-36261917
Matrix: Water
Analysis Batch: 362619
MB MB
Analyte Result Qualifier
Toluene
Xylenes, Total
Surrogate
Toluene -d8 (Surf)
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
4-Bromofluorobenzene (Surr)
Lab Sample ID: LCS 680-362619/3
Matrix: Water
Analysis Batch: 362619
Spike
Analyte Added
<1 0
<2.0
M8 MB
%Recovery Qualirrer
99
106
102
93
RL
1.0
2.0
Limits
79-119
77-129
70-130
71-121
Toluene
20.0
Xylenes, Total
40.0
MDL Unit
LCS LCS
D Prepared Analyzed Dil Fac
Surrogate
%Recovery Qualifier
Limits
Toluene -d8 (Surr)
97
79-119
Dibromofluoromethane (Surr)
113
77-129
1,2-Dichlomethane-d4 (Surr)
117
70-130
4-Bromofluorobenzene (Surr)
102
71-121
Lab Sample ID: LCSD 680-36261914
Matrix: Water
Analysis Batch: 362619
Analyte
Toluene
Xylenes, Total
Surrogate
Toluene -d8 (Surr)
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
4-Bromofluorobenzene (Surr)
LCSD LCSD
%Recovery Qualifier
99
113
116
98
Method: 1664A - HEM and SGT -HEM
Spike
Added
20.0
40.0
Limits
79-119
77-129
70-130
71-121
TestAmerica Job ID: 680-108001-1
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
LCSD LCSD %Rec. RPD
Result Qualifier Unit D %Rec Limits RPD Limit
22.2 uglL 111 47-150 2 30
40.0 ug/L 100 78-119 1 30
Lab Sample ID: MB 680-363875121-A
Matrix: Water
Analysis Batch: 363886
MB MB
Analyte Result Qualifier RL MDL Unit
HEM (Oil & Grease) <5.0 5.0 mg/L
Page 8 of 16
Client Sample ID: Method Blank
Prep Type: TotalINA
Prep Batch: 363875
D Prepared Analyzed Dil Fac
12/18/14 12.04 12/18/14 12.48 1
TestAmerica Savannah
12/19/2014
Client Sample ID: Method Blank
Prep Type: Total/NA
MDL Unit
D Prepared Analyzed Dil Fac
ug/L
12/10/14 19 42 1
ug/L
12110/1419:42 1
Prepared Analyzed Dil Fac
12/10/14 19:42 1
12/10/14 19:42 1
12/10/14 19:42 1
12/10/14 19:42 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
LCS LCS
%Rec.
Result Qualifier
Unit
D %Rec Limits
21.8
ug/L
109 47-150
40.3
ug/L
101 76-119
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
LCSD LCSD %Rec. RPD
Result Qualifier Unit D %Rec Limits RPD Limit
22.2 uglL 111 47-150 2 30
40.0 ug/L 100 78-119 1 30
Lab Sample ID: MB 680-363875121-A
Matrix: Water
Analysis Batch: 363886
MB MB
Analyte Result Qualifier RL MDL Unit
HEM (Oil & Grease) <5.0 5.0 mg/L
Page 8 of 16
Client Sample ID: Method Blank
Prep Type: TotalINA
Prep Batch: 363875
D Prepared Analyzed Dil Fac
12/18/14 12.04 12/18/14 12.48 1
TestAmerica Savannah
12/19/2014

Client: Nexeo Solutions, LLC
Project/Site: Nexeo Solutions LLC Charlotte
QC Sample Results
TestAmerica Job ID: 680-108001-1
Method: 1664A - HEM and SGT -HEM (Continued)
Lab Sample ID: LCS 680-363875/22-A
Matrix: Water
Client Sample ID: Lab Control Sample
Matrix: Water
Analysis Batch: 362824
Prep Type: Total/NA
Analysis Batch: 363886
MB MB
Prep Batch: 363875
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit D %Rec Limits
HEM (Oil & Grease)
399
34.5
mg/L 86 78.114
Lab Sample ID: LCSD 680-363875/23-A
Matrix: Water
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Analysis Batch: 362824
Prep Type: Total/NA
Analysis Batch: 363886
Spike
Prep Batch: 363875
%Rec.
Spike
LCSD LCSD
%Rec. RPD
Analyte
Added
Result Qualifier
Unit D %Rec Limits RPD Limit
HEM (Oil & Grease)
-410
34.4
mg/L 84 78.114 0 18
Method: SM 2540D - Solids, Total Suspended (TSS)
Lab Sample ID: MB 680-362824/1
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 362824
MB MB
Analyte
Result Qualifier
RL RL Unit
D Prepared Analyzed Dil Fac
Total Suspended Solids
<5.0
5.0 mg/L
12/11/14 13:43 1
Lab Sample ID: LCS 680-362824/2
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 362824
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit D %Rec Limits
Total Suspended Solids
20.0
20.0
mg/L 100 80. 120
Lab Sample ID: LCSD 680-362824/3
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 362824
Spike
LCSD LCSD
%Rec. RPD
Analyte
Added
Result Qualifier
Unit D %Rec Limits RPD Limit
Total Suspended Solids
20.0
22.5
mg/L 113 80-120 12 25
Lab Sample ID: 680-108001-1 DU
Client Sample ID: Outfall 001
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 362824
Sample Sample
DU DU
RPD
Analyte
Result Qualifier
Result Qualifier
Unit D RPD Limit
Total Suspended Solids
6.5
5.50
mg/L 17 25
Method: SM 4500 H+ B - pH
Lab Sample ID: LCS 680-362679/7
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 362679
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit D %Rec Limits
_pH
7.00
7.020
SU 100 63.158
Page 9 of 16
I
TestAmerica Savannah
12/19/2014

Client: Nexeo Solutions, LLC
Project/Site: Nexeo Solutions LLC Charlotte
Method: SM 4500 H+ B - pH (Continued)
Lab Sample ID: 680-108001-1 DU
Matrix: Water
Analysis Batch: 362679
Sample Sample
Analyte Result Qualifier
pH 7.20 HF
Method: SM 5220D - COD
Lab Sample ID: MB 680-363238/3
Matrix: Water
Analysis Batch: 363238
Analyte
Chemical Oxygen Demand
Lab Sample ID: LCS 680-363238/4
Matrix: Water
Analysis Batch: 363238
Analyte
Chemical Oxygen Demand
QC Sample Results
MB MB
Result Qualifier
<10
TestAmerica Job ID: 680-108001-1
Client Sample ID: Clutfall 001
Prep Type: Total/NA
DU DU RPD
Result Qualifier Unit D RPD Limit
7.200 SU 0 40
Client Sample ID: Method Blank
Prep Type: Total/NA
RL MDL Unit D Prepared Analyzed Dil Fac
10 mg/L 12/15!1412'55 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
50.0 48.2 mg/L 96 90-110
TestAmerica Savannah
Page 10 of 16 12/19/2014

QC Association Summary
Client: Nexeo Solutions, LLC
Project/Site: Nexeo Solutions LLC Charlotte
GC/MS VOA
Analysis Batch: 362619
Prep Type
Matrix
Method Prep Batch
Lab Sample ID
Client Sample ID
Prep Type
Matrix
680-108001-1
Outfall 001
Total/NA
Water
680-108001-2
Trip Blank
Total/NA
Water
LCS 680-362619/3
Lab Control Sample
Total/NA
Water
LCSD 680-362619/4
Lab Control Sample Dup
Total/NA
Water
MB 680-362619/7
Method Blank
Total/NA
Water
General Chemistry
Analysis Batch: 362679
Lab Sample ID
680-108001-1
680-108001-1 DU
LCS 680-362679/7
Analysis Batch: 362824
FLab Sample ID
680-108001-1
680-108001-1 DU
LCS 680-362824/2
LCSD 680-362824/3
MB 680-362824/1
Analysis Batch: 363238
FLab Sample ID
TestAmerica Job ID: 680-108001-1
Method Prep Batch
624
624
624
624
624
Client Sample ID
Prep Type
Matrix
Method Prep Batch
Outfall 001
Total/NA
Water
SM 4500 H+ B
Outfall 001
Total/NA
Water
SM 4500 H+ B
Lab Control Sample
Total/NA
Water
SM 4500 H+ B
Client Sample ID
Prep Type
Matrix
Method Prep Batch
Outfall 001
Total/NA
Water
SM 2540D
Ouffall 001
Total/NA
Water
SM 2540D
Lab Control Sample
Total/NA
Water
SM 2540D
Lab Control Sample Dup
Total/NA
Water
SM 2540D
Method Blank
Total/NA
Water
SM 2540D
Client Sample ID
680-108001-1
Ouffall 001
LCS 680-363238/4
Lab Control Sample
MB 680-363238/3
Method Blank
Prep Batch: 363875
Lab Sample ID
Client Sample ID
680-108001-1
Ouffall 001
LCS 680-363875/22-A
Lab Control Sample
LCSD 680-363875/23-A
Lab Control Sample Dup
MB 680-363875/21-A
Method Blank
Analysis Batch: 363886
Prep Batch
Lab Sample ID
Client Sample ID
680-108001-1
Outfall 001
LCS 680-363875/22-A
Lab Control Sample
LCSD 680-363875/23-A
Lab Control Sample Dup
MB 680-363875/21-A
Method Blank
Prep Type
Matrix
Method
Prep Batch
Total/NA
Water
SM 5220D
Total/NA
Water
SM 5220D
Total/NA
Water
SM 5220D
Prep Type
Matrix
Method
Prep Batch
Total/NA
Water
1664A
Total/NA
Water
1664A
Total/NA
Water
1664A
Total/NA
Water
1664A
Prep Type
Matrix
Method
Prep Batch
Total/NA
Water
1664A
363875
Total/NA
Water
1664A
363875
Total/NA
Water
1664A
363875
Total/NA
Water
1664A
363875
TestAmerica Savannah
Page 11 of 16 12/19/2014

Lab Chronicle
Client: Nexeo Solutions, LLC TestAmerica Job ID: 680-108001-1
Project/Site: Nexeo Solutions LLC Charlotte
Client Sample ID: Outfall 001 Lab Sample ID: 680-108001-1
Date Collected: 12106/1414:30 Matrix: Water
Date Received: 12/09/14 09:59
Batch Batch
Prep Type Type Method
Total/NA Analysis 624
Instrument ID CMSAD
Total/NA Prep 1664A
Total/NA Analysis 1664A
Instrument ID: NoEquip
Total/NA Analysis SM 2540D
Instrument ID, NOEQUIP
Total/NA Analysis SM 4500 H+ B
Instrument ID. MANTECH
Total/NA Analysis SM 5220D
Instrument ID. SPC3
Client Sample ID: Trip Blank
Date Collected: 12/06/14 00:00
Date Received: 12/09/14 09:59
Dil
Initial
Final
Batch
Prepared
i ..
Run Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
1
5 mL
5 mL
362619
12/10/14 23:39
TF1
TAIL SAV
996 mL
500 mL
363875
12/18/14 12 04
ALC
TAL SAV
1
996 mL
500 mL
363886
12/18/14 12.48
ALC
TAL SAV
i
1
200 mL
200 mL
362824
12/11/14 13.46
LBH
TAL SAV
1
362679
12/10/14 1755
LBH
TAIL SAV
1
2 mL
2 mL
363238
12/15/14 12.55
JRJ
TAL SAV
Lab Sample ID: 680-108001-2
Matrix: Water
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor . Amount Amount Number or Analyzed Analyst Lab
Total/NA Analysis 624 1 5 mL 5 mL 362619 12/10/14 23:11 TF1 TAL SAV
Instrument ID: CMSAD
Laboratory References:
TAIL SAV = TestAmenca Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Page 12 of 16
TestAmerica Savannah
12/19/2014

Page 13 of 16
12/19/2014
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Page 13 of 16
12/19/2014
0

Client: Nexeo Solutions, LLC
Login Number: 108001
List Number: 1
Creator: Banda, Christy S
Question
Login Sample Receipt Checklist
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a
N/A
surrey meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
N/A
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time.
True
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
Job Number: 680-108001-1
List Source: TestAmerica Savannah
TestAmerica Savannah
Page 14 of 16 12/19/2014

Client. Nexeo Solutions, LLC
Project/Site: Nexeo Solutions LLC Charlotte
Laboratory: TestAmerica Savannah
The certifications listed below are applicable to this report.
Authority Program
North Carolina (WWISVV) State Program
Certification Summary
EPA Region Certification ID
4 269
Page 15 of 16
TestAmerica Job ID: 680-108001-1
TestAmerica Savannah
12/19/2014

Method Summary
Client: Nexeo Solutions, LLC
Project/Site: Nexeo Solutions LLC Charlotte
TestAmerica Job ID: 680-108001-1
Method Method Description
Protocol
624 Volatile Organic Compounds (GC/MS)
40CFR136A
1664A HEM and SGT -HEM
1664A
SM 2540D Solids, Total Suspended (TSS)
SM
SM 4500 H+ B pH
SM
SM 5220D COD
SM
Protocol References:
1664A = EPA -821-98-002
40CFR136A = "Methods for Organic Chemical Analysis of Municipal Industrial Wastewater', 40CFR,
Part 136, Appendix A, October 26, 1984 and
subsequent revisions.
SM = "Standard Methods For The Examination Of Water And Wastewater',
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Page 16 of 16
Laboratory
TAL SAV
TAL SAV
TAL SAV
TAL SAV
TAL SAV
TestAmerica Savannah
12/19/2014
F12