HomeMy WebLinkAboutNCG030535_2024 DMR_20240422 (2) Pace Analytical Services,LLC
ace. 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
(704)875-9092
April 10, 2024
William Edens
ZF Chassis Components LLC
1570 E. P St. Ext.
Newton, NC 28658
RE: Project: Stormwater Sampling
Pace Project No.: 92721952
Dear William Edens:
Enclosed are the analytical results for sample(s)received by the laboratory on March 28, 2024. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services-Asheville
• Pace Analytical Services-Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyriek Hooks
tyriek.hooks@pacelabs.com
704-977-0947
Project Manager
Enclosures
2' • REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
qeo
without the written consent of Pace Analytical Services,LLC. Page 1 of 14
Pace Analytical Services,LLC
ace/� 9800 Kincey Ave. Suite 100
/// e, Huntersville,NC 28078
�!V (704)875-9092
CERTIFICATIONS
Project: Stormwater Sampling
Pace Project No.: 92721952
Pace Analytical Services Charlotte
South Carolina Laboratory ID:99006 South Carolina Certification#:99006001
9800 Kincey Ave.Ste 100,Huntersville,NC 28078 South Carolina Drinking Water Cert.#:99006003
North Carolina Drinking Water Certification#:37706 Florida/NELAP Certification#: E87627
North Carolina Field Services Certification#:5342 Kentucky UST Certification#:84
North Carolina Wastewater Certification#: 12 Louisiana DoH Drinking Water#:LA029
South Carolina Laboratory ID:99006 VirginiaNELAP Certification#:460221
Pace Analytical Services Asheville
2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030
Florida/NELAP Certification#: E87648 South Carolina Certification#:99030001
North Carolina Drinking Water Certification#:37712 Virginia/VELAP Certification#:460222
North Carolina Wastewater Certification#:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 2 of 14
Pace Analytical Services,LLC
ace. 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
(704)875-9092
SAMPLE ANALYTE COUNT
Project: Stormwater Sampling
Pace Project No.: 92721952
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92721952001 3-2024#1 ABCD EPA 1664E YY 1 PASI-C
EPA 200.7 Rev 4.4 1994 SBW 3 PASI-A
SM 2540D-2015 JMH1 1 PASI-A
EPA 9040C YEG 1 PASI-A
92721952002 3-2024#2 ABCD EPA 1664E YY 1 PASI-C
EPA 200.7 Rev 4.4 1994 SBW 3 PASI-A
SM 2540D-2015 JMH1 1 PASI-A
EPA 9040C YEG 1 PASI-A
PASI-A=Pace Analytical Services-Asheville
PASI-C=Pace Analytical Services-Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 3 of 14
Pace Analytical Services,LLC
ace. 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Stormwater Sampling
Pace Project No.: 92721952
Sample: 3-2024#1 ABCD Lab ID: 92721952001 Collected: 03/27/24 11:30 Received: 03/28/24 09:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM,Oil and Grease Analytical Method: EPA 1664E
Pace Analytical Services-Charlotte
Oil and Grease 6.5 mg/L 4.8 1 03/29/24 12:27
200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services-Asheville
Copper ND mg/L 0.0050 1 03/29/24 12:55 04/09/24 15:54 7440-50-8
Lead ND mg/L 0.0050 1 03/29/24 12:55 04/09/24 15:54 7439-92-1
Zinc 0.031 mg/L 0.010 1 03/29/24 12:55 04/09/24 15:54 7440-66-6
2540D Total Suspended Solids Analytical Method:SM 2540D-2015
Pace Analytical Services-Asheville
Total Suspended Solids 5.8 mg/L 2.8 1 04/03/24 17:49
9040 pH Analytical Method: EPA 9040C
Pace Analytical Services-Asheville
pH at 25 Degrees C 7.3 Std.Units 0.10 1 04/08/24 12:37 H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:04/10/2024 05:15 PM without the written consent of Pace Analytical Services,LLC. Page 4 of 14
Pace Analytical Services,LLC
ace. 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Stormwater Sampling
Pace Project No.: 92721952
Sample: 3-2024#2 ABCD Lab ID: 92721952002 Collected: 03/27/24 11:45 Received: 03/28/24 09:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM,Oil and Grease Analytical Method: EPA 1664E
Pace Analytical Services-Charlotte
Oil and Grease ND mg/L 4.8 1 03/29/24 12:27
200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services-Asheville
Copper ND mg/L 0.0050 1 03/29/24 12:55 04/09/24 15:57 7440-50-8
Lead ND mg/L 0.0050 1 03/29/24 12:55 04/09/24 15:57 7439-92-1
Zinc 0.020 mg/L 0.010 1 03/29/24 12:55 04/09/24 15:57 7440-66-6
2540D Total Suspended Solids Analytical Method:SM 2540D-2015
Pace Analytical Services-Asheville
Total Suspended Solids 2.9 mg/L 2.5 1 04/03/24 17:49
9040 pH Analytical Method: EPA 9040C
Pace Analytical Services-Asheville
pH at 25 Degrees C 6.6 Std.Units 0.10 1 04/08/24 12:48 H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:04/10/2024 05:15 PM without the written consent of Pace Analytical Services,LLC. Page 5 of 14
Pace Analytical Services,LLC
ace. 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Stormwater Sampling
Pace Project No.: 92721952
QC Batch: 842864 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM,Oil and Grease
Laboratory: Pace Analytical Services-Charlotte
Associated Lab Samples: 92721952001,92721952002
METHOD BLANK: 4352868 Matrix: Water
Associated Lab Samples: 92721952001,92721952002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L ND 5.0 03/29/24 12:25
LABORATORY CONTROL SAMPLE: 4352869
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Oil and Grease mg/L 40 32.3 81 78-114
MATRIX SPIKE SAMPLE: 4352870
35869109002 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Oil and Grease mg/L 1.2J 39.6 33.5 81 78-114
SAMPLE DUPLICATE: 4352871
35869109001 Dup
Parameter Units Result Result RPD Qualifiers
Oil and Grease mg/L 1.1U ND
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:04/10/2024 05:15 PM without the written consent of Pace Analytical Services,LLC. Page 6 of 14
Pace Analytical Services,LLC
ace. 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Stormwater Sampling
Pace Project No.: 92721952
QC Batch: 842852 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92721952001,92721952002
METHOD BLANK: 4352836 Matrix: Water
Associated Lab Samples: 92721952001,92721952002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Copper mg/L ND 0.0050 04/09/24 15:15
Lead mg/L ND 0.0050 04/09/24 15:15
Zinc mg/L ND 0.010 04/09/24 15:15
LABORATORY CONTROL SAMPLE: 4352838
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Copper mg/L 0.5 0.49 97 85-115
Lead mg/L 0.5 0.48 96 85-115
Zinc mg/L 0.5 0.48 96 85-115
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4352839 4352840
MS MSD
92721916001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Copper mg/L 121 0.5 0.5 0.52 0.53 79 82 70-130 3
ug/L
Lead mg/L ND 0.5 0.5 0.41 0.42 79 82 70-130 3
Zinc mg/L 2330 0.5 0.5 2.6 2.7 53 65 70-130 2 M1
ug/L
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4352841 4352842
MS MSD
92721971001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Copper mg/L ND 0.5 0.5 0.50 0.51 100 101 70-130 1
Lead mg/L ND 0.5 0.5 0.50 0.50 99 100 70-130 1
Zinc mg/L 19.7 0.5 0.5 0.52 0.53 100 101 70-130 1
ug/L
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:04/10/2024 05:15 PM without the written consent of Pace Analytical Services,LLC. Page 7 of 14
Pace Analytical Services,LLC
ace. 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Stormwater Sampling
Pace Project No.: 92721952
QC Batch: 843908 Analysis Method: SM 2540D-2015
QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92721952001,92721952002
METHOD BLANK: 4358213 Matrix: Water
Associated Lab Samples: 92721952001,92721952002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 04/03/24 17:49
LABORATORY CONTROL SAMPLE: 4358214
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Total Suspended Solids mg/L 251 242 96 90-110
SAMPLE DUPLICATE: 4358474
92721938001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 2920 2840 3
SAMPLE DUPLICATE: 4359959
92721914001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 211 220 4
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:04/10/2024 05:15 PM without the written consent of Pace Analytical Services,LLC. Page 8 of 14
Pace Analytical Services,LLC
ace. 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Stormwater Sampling
Pace Project No.: 92721952
QC Batch: 845082 Analysis Method: EPA 9040C
QC Batch Method: EPA 9040C Analysis Description: 9040 pH
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92721952001,92721952002
SAMPLE DUPLICATE: 4364077
92721984001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 6.3 5.8 9 D6,H3
SAMPLE DUPLICATE: 4364332
92721984007 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 4.3 4.3 0 H3
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:04/10/2024 05:15 PM without the written consent of Pace Analytical Services,LLC. Page 9 of 14
Pace Analytical Services,LLC
( ace® 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
(704)875-9092
QUALIFIERS
Project: Stormwater Sampling
Pace Project No.: 92721952
DEFINITIONS
DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot.
ND-Not Detected at or above adjusted reporting limit.
TNTC-Too Numerous To Count
J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL-Practical Quantitation Limit.
RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S-Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is
a combined concentration.
Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values.
LCS(D)-Laboratory Control Sample(Duplicate)
MS(D)-Matrix Spike(Duplicate)
DUP-Sample Duplicate
RPD-Relative Percent Difference
NC-Not Calculable.
SG-Silica Gel-Clean-Up
U-Indicates the compound was analyzed for,but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as
"Total"may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes.
TNI-The NELAC Institute.
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample(LCS)recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:04/10/2024 05:15 PM without the written consent of Pace Analytical Services,LLC. Page 10 of 14
Pace Analytical Services,LLC
ace. 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
(704)875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Stormwater Sampling
Pace Project No.: 92721952
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92721952001 3-2024#1 ABCD EPA 1664B 842864
92721952002 3-2024#2 ABCD EPA 1664B 842864
92721952001 3-2024#1 ABCD EPA 200.7 Rev 4.4 1994 842852 EPA 200.7 Rev 4.4 1994 842922
92721952002 3-2024#2 ABCD EPA 200.7 Rev 4.4 1994 842852 EPA 200.7 Rev 4.4 1994 842922
92721952001 3-2024#1 ABCD SM 2540D-2015 843908
92721952002 3-2024#2 ABCD SM 2540D-2015 843908
92721952001 3-2024#1 ABCD EPA 9040C 845082
92721952002 3-2024#2 ABCD EPA 9040C 845082
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:04/10/2024 05:15 PM without the written consent of Pace Analytical Services,LLC. Page 11 of 14
DC#_Title: ENV-FRM-HUN1-0083 v03_Sample Condition Upon Receipt
' ace
Effective Date: 11/29/2023 4:16:30 PM
Laboratory receiving samples:
Asheville❑ Eden Greenwood❑ Huntersville _ Raleigh❑ Mechanicsville❑ Atlantan Kernersville❑
WO* : 9272
Sample Condition Client Name: 1952
Upon Receipt 7 r �� �n.('c.s^ �,I p( l n Project #:
Courier: 11 Fed Ex ❑UPS 11 LISPS ❑Client I III I 111111 11111
III
❑ Commercial ❑Pace ❑Other:
92721952
Custody Seal Present? CI Yes ❑No Seals Intact? Elves El No ❑N/A I.1L1
Date/Initials Person Examining Contents:
L
Packing Material: ❑Bubble Wrap ❑Bubble Bags ❑None ❑ Other Biological Tissue Frozen?
Thermometer: �( Yes El No ❑N/A
❑ IR Gun ID: 11 110
lllJJl Type of Ice: ❑Wet ❑Blue ❑None
Correction Factor:
Cooler Temp: Add/Subtract('C) Temp should be above freezing to 6°C
❑Samples out of temp criteria.Samples on ice,cooling process
Cooler Temp Corrected (CC): has begun
USDA Regulated Soil ( N/A, water sample)
Did samples originate in a quarantine zone within the United States:CA, NY, or SC Did samples originate from a foreign source (internationally,
(check maps)?❑Yes ❑No including Hawaii and Puerto Rico)?❑Yes 0 No
Comments/Discrepancy:
Chain of Custody Present? ❑Yes ❑No ]N/A 1.
Samples Arrived within Hold Time? ❑Yes 0 No ❑N/A 2.
Short Hold Time Analysis (<72 hr.)? ❑Yes ❑No ❑N/A 3.
Rush Turn Around Time Requested? ❑Yes ❑No ❑N/A 4.
Sufficient Volume? Oyes 0 No ❑N/A 5.
Correct Containers Used? :Pies ❑No ON/A 6.
-Pace Containers Used? ❑Yes 0 No ❑N/A
Containers Intact? ❑yes ❑No ❑N/A 1
Dissolved analysis:Samples Field Filtered? [Dyes 0 No ❑N/A 8.
Sample Labels Match COC? ❑Yes 0 No ❑N/A 9.
-Includes Date/time/ID/Analysis Matrix:
Headspace in VOA Vials(>5-6mm)? ❑Yes ❑No ❑N/A 10.
Trip Blank Present? ❑Yes CI No ON/A 11.
Trip Blank Custody Seals Present? ❑Yes ❑No ❑N/A
COMMENTS/SAMPLE DISCREPANCY Field Data Required? ❑Yes ❑No
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: Date/Time:
Project Manager SCURF Review: Date:
Project Manager SRF Review: Date:
Page 12 of 14
Qualtrax ID: 69614
Paae 1 of 2
DC#_Title: ENV-FRM-HUN1-0083 v02_Sample Condition Upon Receipt
,filace
Effective Date: 11/14/2022 WO#
: 92721952
*Check mark top half of box if pH and/or dechlorination is verified and Project t1 PM: TIN Due Date:
within the acceptance range for preservation samples. CLIENT: 92—ZFLemferd 04/1 1/24
Exceptions:VOA,Coliform,TOC,Oil and Grease,DRO/8015(water)DOC.LLHg
**Bottom half of box is to list number of bottles
***Check all unpreserved Nitrates for chlorine
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pH Adjustment Log for Preserved Samples
Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative Lot ft
adjusted added
Note: Whenever there is a discrepancy affecting North Carolina compliance samples,a copy of this form will he sent to the North Carolina DENR Certification Office{i.e.
Out of hold,incorrect preservative,out of temp,incorrect containers.
Page 13 of 14
Qualtrax ID:69614 Page 2 of 2
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