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HomeMy WebLinkAboutNCG030669_2024 DMR_20240416 NCDEQ Division of Energy, Mineral and Land Resources Stormwater Discharge Monitoring Report(DMR) Form for NCGO3OOOO Metal Fabrication Click here for instructions Complete,sign,scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report(DMR) Upload form within 30 days of receiving sampling results. Mail the original,signed hard copy of the DMR to the appropriate DEMLR Regional Office. Certificate of Coverage No. NCG03 0669 Person Collecting Samples: Robert Hensley Facility Name: AFS MFG LLC Laboratory Name: Pace Analytical Facility County: ROWAN Laboratory Cert. No.: DW#37706,WW#12, DW#37712,WW#40 Discharge during this period: Yes Q No (if no,skip to signature and date) Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances?EIYes E No If so,which Tier(I, II, or Ill)? A copy of this DMR has been uploaded electronically via https://edocs.deq.nc.gov/Forms/SW-DMR Eyes No Date Uploaded: 1.4)I Analytical Monitoring Requirements for Outfalls with Industrial Activities—Benchmarks in(Red) Parameter Parameter Outfall 1B Outfall 2 Outfall Outfall Outfall Code N/A Receiving Stream Class C C N/A Date Sample Collected MM/DD/YYYY 3/15/2024 3/15/2024 46529 24-Hour Rainfall in inches 0.45" 0.45" CO530 TSS in mg/L(100 or 50*) <2.5 mg/L <2.5 mg/L 00400 pH in standard units(6.0-9.0 FW, 7.31 7.46 6.8-8.5 SW) 01119 Copper,total recoverable in mg/L <0,0050 m mg/L (0.010 FW,0.0058 SW) g/L <0.0050 01051 Lead,total recoverable in mg/L <0.0050 mg/L <0.0050 mg/L (0.075 FW,0.22 SW) 01094 Zinc,total recoverable in mg/L(0.126 <0.0100 mglL <0.0100 mglL FW,0.095 SW) Chemical Oxygen Demand(COD)in 00340 <25.0 mg/L <25.0 mg/L mg/L(120) 00552 Non-Polar Oil&Grease in mg/L(15) <4.8 mglL <4.8 mg/L *Outfalls to Outstanding Resource Waters(ORW),High Quality Waters(HOW),Trout Waters(Tr)and Primary Nursery Areas(PNA) have a benchmark TSS limit of SO mg/L.All other water classifications have a benchmark of 100 mg/L FW(Freshwater)SW(Saltwater) Notes(optional): "I certify by my signature below,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who manage the system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,accurate,and complete.I am aware that there are significant penalties for submitting false inf rmation,including the possibility of fines and imprisonment for knowing violations." Sign ure of Permittee or elegate Authorized Individual Dat KiAt . mC+ a,{ 9 11e• -,A9 Pk5 t k t c 0 1 D - $1 0 --3 5 f , Email Address Phone Number Pace Analytical Services,LLC aceo 9600 Kincey Ave. Suite 100 Huntersville,NC 28078 (704)875-9092 March 22, 2024 Robert Hensley Agility Fuel Systems 1010 Corporate Center Drive Salisbury, NC 28146 RE: Project: Stormwater Pace Project No.: 92719773 Dear Robert Hensley: Enclosed are the analytical results for sample(s)received by the laboratory on March 19, 2024. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: •Pace Analytical Services-Asheville •Pace Analytical Services-Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyriek Hooks tyriek.hooks@pacelabs.com 704-977-0947 Project Manager Enclosures cc: Kulema McKoy,Hexagon Agility REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, re � without the written consent of Pace Analytical Services,LLC. Page 1 of 15. Pace Analytical Services,LLC acEr 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 (704)875-9092 CERTIFICATIONS Project: Stormwater Pace Project No.: 92719773 Pace Analytical Services Charlotte South Carolina Laboratory ID:99006 South Carolina Certification#:99006001 9800 Kincey Ave.Ste 100,Huntersville,NC 28078 South Carolina Drinking Water Cert.#:99006003 North Carolina Drinking Water Certification#:37706 Florida/NELAP Certification#:E87627 North Carolina Field Services Certification#:5342 Kentucky LIST Certification#:84 North Carolina Wastewater Certification#: 12 Louisiana DoH Drinking Water#:LA029 South Carolina Laboratory ID:99006 VirginiaNELAP Certification#:460221 Pace Analytical Services Asheville 2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030 Florida/NELAP Certification#:E87648 South Carolina Certification#:99030001 North Carolina Drinking Water Certification#:37712 VirginiaNELAP Certification#:460222 North Carolina Wastewater Certification#:40 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 2 of 15 Pace Analytical Services,LLC ace. 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Stormwater Pace Project No.: 92719773 Analytes Lab ID Sample ID Method • Analysts Reported Laboratory 92719773001 OUTFALL 2 GRAB EPA 1664E YY 1 PASI-C EPA 200.7 Rev 4.4 1994 DBB1 3 PASI-A SM 2540D-2015 JAY 1 PASI-A SM 5220D-2011 JP1 1 PASI-A 92719773002 OUTFALL 1B GRAB EPA 1664B YY 1 PASI-C EPA 200.7 Rev 4.4 1994 DBB1 3 PASI-A SM 2540D-2015 RVS 1 PASI-A SM 5220D-2011 JP1 1 PASI-A PASI-A=Pace Analytical Services-Asheville PASI-C=Pace Analytical Services-Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 3 of 15 Pace Analytical Services,LLC ace. L m 9B00 Kinaey Ave. Suite 100 Huntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Stormwater Pace Project No.: 92719773 Sample: OUTFALL 2 GRAB Lab ID: 92719773001 Collected: 03/15/24 17:00 Received: 03/19/24 12:36 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM,TPH Analytical Method:EPA 16648 Pace Analytical Services-Charlotte Total Petroleum Hydrocarbons ND mg/L 4.8 1 03/20/24 11:50 200.7 MET ICP Analytical Method:EPA 200.7 Rev 4.4 1994 Preparation Method:EPA 200.7 Rev 4.4 1994 Pace Analytical Services-Asheville Copper ND ug/L 5.0 1 03/20/24 12:35 03/20/24 20:37 7440-50-8 Lead ND ug/L 5.0 1 03/20/24 12:35 03/20/24 20:37 7439-92-1 Zinc ND ug/L 10.0 1 03/20/24 12:35 03/20/24 20:37 7440-66-6 2540D Total Suspended Solids Analytical Method:SM 2540D-2015 Pace Analytical Services-Asheville Total Suspended Solids ND mg/L 2.5 1 03/20/24 16:14 5220D COD Analytical Method:SM 5220D-2011 Preparation Method:SM 5220D-2011 Pace Analytical Services-Asheville Chemical Oxygen Demand ND mg/L 25.0 1 03/21/24 03:24 03/21/24 06:36 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/22/2024 03:54 PM without the written consent of Pace Analytical Services,LLC. Page 4 of 15 Pace Analytical Services,LLC 9800 Kincey Ave. Suite 100 ace. Huntersville,NC 28078 V (704)875-9092 ANALYTICAL RESULTS Project: Stormwater Pace Project No.: 92719773 Sample: OUTFALL 1B GRAB Lab ID: 92719773002 Collected: 03/15/24 18:00 Received: 03/19/24 12:36 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM,TPH Analytical Method:EPA 1664E Pace Analytical Services-Charlotte Total Petroleum Hydrocarbons ND mg/L 4.8 1 03/20/24 11:50 200.7 MET ICP Analytical Method:EPA 200.7 Rev 4.4 1994 Preparation Method:EPA 200.7 Rev 4,4 1994 Pace Analytical Services-Asheville Copper ND ug/L 5.0 1 03/20/24 12:35 03/20/24 20:46 7440-50-8 Lead ND ug/L 5.0 1 03/20/24 12:35 03/20/24 20:46 7439-92-1 Zinc ND ug/L 10.0 1 03/20/24 12:35 03/21/24 11:52 7440-66-6 2540D Total Suspended Solids Analytical Method:SM 2540D-2015 Pace Analytical Services-Asheville Total Suspended Solids ND mg/L 2.5 1 03/21/24 05:39 5220D COD Analytical Method:SM 5220D-2011 Preparation Method:SM 5220D-2011 Pace Analytical Services-Asheville Chemical Oxygen Demand ND mg/L 25.0 1 03/21/24 03:24 03/21/24 06:36 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/22/2024 03:54 PM without the written consent of Pace Analytical Services,LLC. Page 5 of 15 Pace Analytical Services,LLC 9800 Kincey Ave. Suite 100 ace(' Huntersville,NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92719773 QC Batch: 840339 Analysis Method: EPA 1664B QC Batch Method: EPA-1664B Analysis Description: 1664 SGT-HEM,TPH Laboratory: Pace Analytical Services-Charlotte Associated Lab Samples: 92719773001,92719773002 METHOD BLANK: 4340330 Matrix: Water Associated Lab Samples: 92719773001,92719773002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 03/20/24 11:50 LABORATORY CONTROL SAMPLE: 4340331 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 15.9 80 64-132 MATRIX SPIKE SAMPLE: 4340332 92719613002 Spike MS MS %Rec Parameter Units Result Conc. Result %Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 19.4 17.5 74 64-132 SAMPLE DUPLICATE: 4340333 92719613005 Dup Parameter Units Result Result RPD Qualifiers Total Petroleum Hydrocarbons mg/L ND ND Results presented on this page are In the units Indicated by the"Units"column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/22/2024 03:54 PM without the written consent of Pace Analytical Services,LLC. Page 6 of 15 Pace Analytical Services,LLC ace. 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92719773 QC Batch: 840356 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92719773001,92719773002 METHOD BLANK: 4340417 Matrix: Water Associated Lab Samples: 92719773001,92719773002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper ug/L ND 5,0 03/20/24 20:03 Lead ug/L ND 5.0 03/20/24 20:03 Zinc ug/L ND 10.0 03/20/24 20:03 LABORATORY CONTROL SAMPLE: 4340418 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Copper ug/L 500 493 99 85-115 Lead ug/L 500 496 99 85-115 Zinc ug/L 500 505 101 85-115 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4340419 4340420 MS MSD 92719556001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Copper ug/L 32.9 500 500 567 566 107 107 70-130 0 Lead uglL ND 500 500 537 537 107 107 70-130 0 Zinc ug/L 0.087 500 500 635 635 110 110 70-130 0 mg/L MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4340421 4340422 MS MSD 92719603001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Copper ug/L 0.30 500 500 887 878 118 116 70-130 1 mg/L Lead ug/L 0.018 500 500 542 539 105 104 70-130 1 mg/L Zinc ug/L 4.7 500 500 5010 4910 54 34 70-130 2 M1 mg/L Results presented on this page are In the units Indicated by the"Units"column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/22/2024 03:54 PM without the written consent of Pace Analytical Services,LLC. Page 7 of 15 Pace Analytical Services,LLC ace. 9800 Kincey Ave. Suite 100 Huntersville,NC 28978 (704)875-9092 QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92719773 QC Batch: 840451 Analysis Method: SM 2540D-2015 QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92719773001 METHOD BLANK: 4341050 Matrix: Water Associated Lab Samples: 92719773001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 03/20/24 16:05 LABORATORY CONTROL SAMPLE: 4341051 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Total Suspended Solids mg/L 250 256 102 90-110 SAMPLE DUPLICATE: 4341481 92719292001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 244 244 0 SAMPLE DUPLICATE: 4341482 92719292003 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mglL 3230 3180 2 Results presented on this page are In the units Indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/22/2024 03:54 PM without the written consent of Pace Analytical Services,LLC. Page 8 of 15 Pace Analytical Services,LLC ace'. 9800 Kincey Ave. Suite100 Huntersville,NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92719773 QC Batch: 840585 Analysis Method: SM 2540D-2015 QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92719773002 METHOD BLANK: 4341882 Matrix: Water Associated Lab Samples: 92719773002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 03/21/24 05:32 LABORATORY CONTROL SAMPLE: 4341883 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Total Suspended Solids mg1L 250 252 101 90-110 SAMPLE DUPLICATE: 4341884 92720056001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 318 342 8 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/22/2024 03:54 PM without the written consent of Pace Analytical Services,LLC. Page 9 of 15 Pace Analytical Services,LLC ace. 9800 Kincey Ave. Suite 100 Huntersviile,NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92719773 QC Batch: 840623 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92719773001,92719773002 METHOD BLANK: 4341983 Matrix: Water Associated Lab Samples: 92719773001,92719773002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 03/21/24 06:30 LABORATORY CONTROL SAMPLE: 4341984 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 804 107 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4341985 4341986 MS MSD 92717965001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Chemical Oxygen Demand mg/L 620 100 100 718 754 98 133 90-110 5 M1,R1 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4341987 4341988 MS MSD 92718461002 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Chemical Oxygen Demand mg/L 84.7 100 100 189 197 105 112 90-110 4 M1,R1 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/22/2024 03:54 PM without the written consent of Pace Analytical Services,LLC. Page 10 of 15 Pace Analytical Services,LLC (/ iace 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 (704)875-9092 QUALIFIERS Project: Stormwater Pace Project No.: 92719773 DEFINITIONS DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot. ND-Not Detected at or above adjusted reporting limit. TNTC-Too Numerous To Count J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL-Practical Quantitation Limit. RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S-Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is a combined concentration. Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values. LCS(D)-Laboratory Control Sample(Duplicate) MS(D)-Matrix Spike(Duplicate) DUP-Sample Duplicate RPD-Relative Percent Difference NC-Not Calculable. SG-Silica Gel-Clean-Up U-Indicates the compound was analyzed for,but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as "Total"may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes. TNI-The NELAC Institute. ANALYTE QUALIFIERS M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample(LCS)recovery. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/22/2024 03:54 PM without the written consent of Pace Analytical Services,LLC. Page 11 of 15 Pace Analytical Services,LLC (/! ace Huntersville,NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Stormwater Pace Project No.: 92719773 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92719773001 OUTFALL 2 GRAB EPA 1664B 840339 92719773002 OUTFALL 1 B GRAB EPA 1664E 840339 92719773001 OUTFALL 2 GRAB EPA 200.7 Rev 4.4 1994 840356 EPA 200.7 Rev 4.4 1994 840484 92719773002 OUTFALL 1 B GRAB EPA 200.7 Rev 4.4 1994 840356 EPA 200.7 Rev 4.4 1994 840484 92719773001 OUTFALL 2 GRAB SM 2540D-2015 840451 92719773002 OUTFALL 1 B GRAB SM 2540D-2015 840585 92719773001 OUTFALL 2 GRAB SM 5220D-2011 840623 SM 5220D-2011 840651 92719773002 OUTFALL 1B GRAB SM 5220D-2011 840623 SM 52200-2011 840651 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/22/2024 03:54 PM without the written consent of Pace Analytical Services,LLC. Page 12 of 15 DC## Title: ENV-FRM-HUN1-0083 v03_Sample Condition Upon Receipt .. ace Effective Date: 11/29/2023 4:16:30 PM Laboratory receiving samples: Asheville❑ Eden❑ Greenwood❑ Huntersville Raleigh❑ Mechanicsville❑ Atlanta❑ KPrnercviIIan WO# . 92719773 Sample C:ondittan���� Client Name: • upon Rece) hY044 Project#: � pt ��a Courier. ❑Fed UPS ❑USPS ❑Client 1111 � ' I Ell II !11 ❑ Commercial Pace ❑Other: 92719773 11 !!! ll �—y�' �_ Custody Seal Present? DYes -ENO- Seals Intact? ❑Yes ONO N A � C) 1r Date/Initials Person Examining Content's: I `DJ l 3�f��f:9 Packing Material: 9ubble Wrap ❑Bubble Bags ❑None ❑ Other Biological Tissue Frozen? ❑Yes Q2N/A m Theromet No lR Gun ID: `.� cy? ( ✓ Type of Ice: Wet ❑Blue 0 None Correction Factor: Cooler Temp: Add/Subtract('C) L/ Temp should be above freezing to 6'C ❑Samples out of temp criteria.Samples on ice,cooling process Cooler Temp Corrected i'C): has begun USDA Regulated Soil N/A,water sample) Did samples originate in a uarantine zone within the United States:CA,NY,or SC Did samples originate from a foreign source(internationally, (check maps)?❑yes/�No including Hawaii and Puerto Rico)?0Yes —011a Comments/Discrepancy: Chain of Custody Present? s D No 3 N/A 1. Samples Arrived within Hold Time? -Yes ❑Na ❑N/A 2. Short Hold Time Analysis(<72 hr.)? 0 Yes ,i�No ❑N/A 3. Rush Turn Around Time Requested? Oyes trNo CI N/A 4. Sufficient Volume? Yes ❑No O N/A 5. Correct Containers Used? 'es ❑No ❑N/A 6. -Pace Containers Used? C,1=tes 0 No ❑N/A Containers Intact? es ❑No ©N/A 7. Dissolved analysis:Samples Field Filtered? pps ©No N/A B. Sample Labels Match COC? Zall Yes ❑No ©rr/A 9. VI 1- -Includes Date/Time/ID/Analysis Matrix: Headspace in VOA Vials(>5-6mm)? El Yes No i/A 10. Trip Blank Present? ❑Yes ❑No Hare/A 11. Trip Blank Custody Seals Present? ❑Ycs ONo LdN/A COMMENTS/SAMPLE DISCREPANCY Field Data Required? ©yes 0 No Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Date/Time: Project Manager SCURF Review: Date: Project Manager SRF Review: Date: Qualtrax ID: 69614 Paae 1 of 2 Page 13 of 15 t Ulil., Effective Date: 11/1L1/2022 • `Check mark top half of box if pH and/or dechlorination is verified and Project o WO : 92719773 within the acceptance range for preservation samples. PM: TIN Due Date 03/26/24 Exceptions:VOA,Cotiforrn,TOC.Oil and Grease.DRO/8O15{water)DOC.LLHc CLIENT: 92_Ag g i i ty F "Bottom half of box is to list number of bottles i *"Check all unpreserved Nitrates for chlorine i 0 4'. i ,..4. i t) —... --.. U -0 y —1:1y V pa A 5 r l Y v .. Q E '� : ' I i x d 1 u Cdi T 21 G n a J Qr 6 _a: \ F. J G rya \ 1 O a .n Z .Z.+ ` % ...... . , r tv Si ` ` ..4. In N ,- 7• U R r e; o Q M U — 1 � v. i l > .4.. ca v • ,'- N m ,. S v ! n m ,. E a I Z ca . I w W _ m c`r A y s i 2 = a .7.. a q . n I A A .. C D �; Q C . I � y - z E C A n. a. c- n a c y g. c 1 4 f, I K Q 7 ° > > y a K w a• t vi: C .. • E `v C E c e , ro z f a } E ' c 1 E e c To E E 'c of .v'.r ,^ o , = :I a r; = I 1 rn I - uQ, l .. a o o a o .r, 1 0 o y O o r ti N H ... ry rti i -1 I 4 t I .., N 4 •O q 'r 1. — r7.. rr N 6 V ▪ .• 1. ry _.. V1 Z N 4 W T4 T t I V1 Jf cn S cn at > R Y ,., t" . : 7 n a m c Q } V : r m .� en m m Q, m m n _ r� u< ry ^� . � � u n_ a 0 rr 0 0 0 a L7 4 4 V' t7 0 > ) d o. % p, a U N U m m m m m I o m I m y ¢ d <t ( d K G C 7 > �c ; ? w v, I m 4 > 0 p , i Ni\\--7, -:--,, r , \ `, T \1 \, \ \�'•., ‘:I 1 ,i N\1�..1 _ —;—; ( l '\ \. \ \'�, \ \ \ i i \\I:\is, ,... i is \ ` \ \ ` 1 + I\ i\.. 1 \i _LI. 1 \ i \ \. \ \` _ i — ` L \. \,1 NI7 \ \ " — 4\ 1 \ \\\v,L__,\. II I '57\ ' 1\ \ \\ • i 1 [\\\I K I 1 .t \ i \. I \ \ \ 1 \ `�,....\. \ . l \\I\\‘I>\L \\ I 1 \ r\Is\•,l'•, r , \IN 1 El\ \ \ j , '4 s• s' ^••1 \ \ I I . � i t II \ ' \ \\ \\P h `\ —1-- ... L -'—' pH Adjustment Log for Preserved Samples Sample ID k Type of Preservative pH upon receipt ( Date preservation adjusted 1 Time preservation Amount of Preservative lot I adjusted added �` d ! •I 1 1 1 I__ _ • Note Whenever there is a discrepancy affecting North Carolina compliance samples.a copy of the;tom will be sent to thn Wirth Carolina OENR Certdicatron Office(i e Out of hold.incorrect preservative.out el temp.incorrect conlarn rt Qualtrax ID.69614 Page 2 of 2 Page 14 of 15 w E Ci �` Q ,,,..9 A n a g z = iti c3 M e _ S g 1 n n » .%.• °� of 3 wi. y. Y o w a� a ob 15 La X V �r N o Ei 3 _ <" ° _ $ " � `� r �., a A a 3 x a „ r Y A N N En 1 n Q 11 01 iC ' n _ a f� a o .1 a u.�'. t at •at s v . 3 :• x m o c c ..it" C o Z d ra \\ u 1 - ry • NI yr G> im ` ro N n 5 0.3 3 4 3 i n of r `2 v A • ^ m K •G N O 12 9 c C m 7 p n O a • 7 O b O O m yi O O y�� _a O rt n of 4 b ‹. y G u n n st d , n S Y • ip m b vs ^ 1. K G _ ^ 0. = �1 O O O IA a ` —a w' �- o - %V P. f1n �. o roI' o C Lel ,� O ` K `S' •N W m G1 a 2 n n n �J Ff1 0a g. n w1 _10 2.. 1Ry %"'VVV3 i � = no N" u ro m a �Q1 0. C n^ m • — �{ rr n C o > > n _W ro Er' M U �, 7t':2'.;•-• COD $ x ;111111.111111111.111111M11 Metals, Fatal Cu P6 ZnJ` — El d:1 �d �L�_tt�� Z■■■■■.■.�� _ Oil and Grease by 1664 8 `n off• N IZZINEMISIDERBIOIT ' .n�Y_n`�JY i — o u ■.■■■■■■■� < 0 0 m `` sj D■■.■..■■■■ ro�_ O j ? O c ra 91 ....- it '27= x■U■11i•Ui1■ a"ri • 12 I J c ■■■■■.... _ n• ro0 al ^` x Z v Z N o ■■■..■■■■. — 1 r o a Al an p o c• _ - Lab use Only = m l� — ._ _ — Mro Oaro a —1 ro" o Gop i. No r- p — ; n U �5 0 n 0 O _F 4 P M o `o N o G e• ^ H _ 2 r N i y B. O _av Q.0 ft, O n'4. Preservation non•conformance Identified for — r Page 15 of 15 Sample _ r