WQ0014885_2015 Annual Report_20160226

4
HARNETT COUNTY, NC
CLASS A RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0014885
2015 ANNUAL REPORT

° Harnett County Wi'P, NC
Residuals Land Application Program
2015 Annual Report
TABLE OF CONTENTS
1. Certification Form, Annual Operations Summary, Facility and
Land Applier Contact Information
2. Annual Residual Sampling Summary Forms, Residuals Analyses,
& SAR Calculation Pages
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen Reduction/Vector Attraction Reduction
t `�

ANNUAL LAND APPLICATION CERTIFICATION FORM
I WQPermit#: W00014885 County Harnett Year2015
Facility Name (as shown on permit) Harnett Countv Utilities Regional WTP PWS ID No. 00-076-84
Land Application Operator Synagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, slip Part A, and PartB and proceed to Part C. Also, if residuals were generated but not landapplied,
please attach an explanation on how the residuals were handled.
Part A— Residuals Application Summary:
Total number of application fields in the permit: N/A
Total number of fields utilized for land application during the year: 3
Total amount of dry tons applied during the year for all application sites: 914.39
Total number of acres utilized for land application during the year: 100.9
Part B —Annual Compliance Statement:
Facility was compliant during calendar year 2015 with all conditions of the land application permit (including but not limited to items
1-13, below) issued by the Division of Water Quality X YES N0.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils -analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .11 I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, in;lulingj possibility of fines and imprisonment for
knowing violations."
aL-16— q
Steve Ward. Director of Public Utilities
Pe e an it n E}- , Si a reAP�i
�/ D e Z��G
ignatureofPreparerk Date S atureofLand plier Date
(if different from Pemy tee) (if different in Permittee and Preparer)
•Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)
C3

2015. ANNUAL OPERATIONS SUMMARY -LAND APPLICATION
,AARNETT CO. UTILITIES, NC
HARNETT CO. UTIL., NC COH REGIONAL WTP LIQUID
DRY METRIC
MONTHNEAR
AMOUNT
UNIT
DRY TONS
UNIT
TONS
January 2015
762,600.00
G
61.39
D
55.66
March 2015
1,078,800.00
G
98.97
D
89.77
April 2015
787,400.00
G
88.00
D
79.81
May 2015
843,200.00
G
94.23
D
85.47
June 2015
1,302,000.00
G
145.50
D
131:97
July 2015
868,000.00
G
96.99
D
87.97
August 2015
830,800.00
G
68.59
D
62.22
September 2015
868,000.00
G
71.66
D
64.99
October 2015
198,400.00
G
16.38
D
14.86
November 2015
954,800.00
G
112.68
D
102.20
December 2015
508,400.00
G
60.00
D
54.42
YEARLY TOTAL
9,002,400.00
G
914.39
D
829.34
2142016

2015 ANNUAL REPORT
PROJECT: Harnett County, NC
FACILITY: Harnett County Regional WTP
310 West Duncan St
Lillington, NC 27546
[phone]
HARNETT CO. REGIONAL WTP:
1:7 Dfyale W"Die7W-W Col CYIF
FACILITY OPERATOR:
NC 00-076-84
Steve Ward, Director of Public Utilities
PO Box 1119
700 McKinney Parkway
Lillington, NC 27546
[phone]
Allan O'Briant, Superintendent (WTP)
310 West Duncan St
Lillington, NC 27546
[phone] ext. 3238
LAND APPLIER AND PREPARER OF LAND
APPLICATION ANNUAL REPORT: Synagro Central, LLC
284 Boger Road
Mocksville, N.C. 27028
Contact: Marshall Puryear
[phone] ext. 17

�. +.. , , ... .. .�z i'� i :r . r ,"� r i': .e� fad wK �(v7i
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0014885
Laboratory
Facility Name: HARNETT CO. UTILITIES,
INC
A&L Eastern Laboratories Inc.
NPDES#: NC0007684
WAYPOINT ANALYTICAL
or WQ# (residual only)
WWTP Name: COH REGIONAL WTP
Residuals Analysis Data
Product Type WPL
WPL
WPL
WPL
Date Sampled (grab) or 02/23/15
04/22/15
07/28/15
11/03/15
Date Composited
Percent Solids 2.20
2.68
1.98
2.03
PARAMETERS (mg/kg dry weight)
Arsenic 8
8
16
9
Cadmium <2
<2
<2
<2
Mercury <0.4
<0.4
<0.4
<0.4
Chromium 30
35
31
43
Copper 155
69
261
342
Lead 8
9
5
7
Molybdenum <5
8
18
8
Nickel 13
16
16
17
Selenium <5
<5
<5
<5
Zinc 91
175
54
56
Total Phosphorus 2850
2490
3010
1620
TKN 14100
10400
13100
11700
Ammonia -Nitrogen 455
1120
3030
1770
Nitrate and Nitrite <2
<2
<2
<2
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluatecJ.tthe information submitted. I am aware that there are
significant penalties for subr9jtting false information, including the possibiloAf fines and imprisonment for knowing violations."
��r✓/ Date
DENR FORM RSSF (5/2003) Printed: Thursday- February 4 2016 at 13:28:28 for: 2037 01

1 Y /1. 1 � 1 � ��� % . ` ' ? Y ice.. `•. 1�
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0014885
Laboratory
Facility Name: HARNETT CO. UTILITIES, NC
A&L Eastern Laboratories Inc.
NPDES# : NC0007684
WAYPOINT ANALYTICAL
or WQ# (residual only)
WWTP Name: COH REGIONAL WTP
Residuals Analysis Data
Product Type WPL
WPL
WPL
WPL
Dale Sampled (grab) or 02/23/15
04/22/15
07/28/15
11/03/15
Date Composited
Percent Solids 2.20
2.68
1.98
2.83
PARAMETERS (mglkg dry weight)
Aluminum 113000
116000
130000
112000
Calcium 1170
1450
1380
769
Magnesium 985
1370
925
947
pH 5.44
5.58
5.82
5.50
Potassium 637
459
766
824
Sodium 420
381
751
483
"I certify, under penalty of law, that this document was prepared under my ction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evalu the information submitted. I am aware that there are
significant penalties for submitting fats@ trtfer(natio eWing the p. of fines and imprisonment for knowing violations."
RN
NR - Data Not Reported or Data
Date l eY
y
DENR FORM RSSF-B (7/2002)
Printed: Thursday - February 4. 2016 at 13:28:51 for 2037 01

Page: 1 of 2
Report Number: 15-063-020B
Account Number: 46460
Submitted By., WILL VARNER
Send To: SYNAGRO CENTRAL LLC/HARNETT
Mary Brewer
COUNTY
284 BOGER RD
MOCKSVILLE, NO 27028
Lab Number: 6049E
Sample Id : HARNETT WTP
�rL A&L Eastern Laboratories, Inc.
' 7621 Whltopine Road RIAMQ .Vlr0In1423237 Ie04t7434401 Fax[phone]
m
wwwaWastern.4orn
Project: HARNETT WTP
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 2/23/2015 12:00:00
Date Received: 03/04/2015 00:00
Date Reported:03/09/2015
Total Solids `
2.20
22000
100.0
JM
03/04/2015 14:10
SM-2540G
Moisture'
97.80
100.0
JM
03/04/201514:10
SM-2540G
Total Kjeldahl Nitrogen
1.41
:V 14100
10.0
JM
03/0512015 08:24
SMA500-NH3C-TKN
Total Phosphorus
0.29
2850
100
KM
03105/201512:30
SW 6010C
Total Potassium
0.06
637
100
KM
03/05/2015 12:30
SW 6010C
Total Sulfur
1.18
11800
100
KM
03/05/2015 12:30
SW 6010C
Total Calcium
0.12
1170
100
KM
031051201512:30
SW 6010C
Total Magnesium
0.10
985
100
KM
03/05/2015 12:30
SW 6010C
Total Sodium
0.04
420
100
KM
03/05/2015 12:30
SW 601OC
Total Iron
25100
100
KM
03/05/2015 12:30
SW 6010C
Total Aluminum
113000
100
KM
03/05/2015 12:30
SW 6010C
Total Manganese
709
5
KM
03/051201612:30
SW 6010C
Total Copper
155
5
KM
03/05/2015 12:30
SW 6010C
Total Zinc
91
5
KM
03/05/2015 12:30
SW 6010C
Ammonia Nitrogen
0.05
A� 456
10.0
JM
03/05/2015 08:24
SM-4500-NH3C
Organic N
1.36
-X13645
10.0
03/05/2015 08:24
CALCULATION
Nitrate+Nitrite-N
<2.00
2.00
JM
03/05/2015 08:25
SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
03/05/2015 12:30
SW 601CC
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series Is on a wet basis.
Our repads and letters are forthe exclusive and conridential use ofaact/ants, and maynot bo mpmduawl in whole orpad, normay any minrencs he made
to the wade, the results, orthe company in any advedlctng, news release. orotherpub6c announcements wilhout obtalnlnp ourodor wriltan authorization. ,
Debbie Holt

Page: 2 of 2
Report Number: 15-063-0208
AccountNumber: 46460
Submitted By: WILL VARNER
Send To: SYNAGRO CENTRAL LLC/HARNETT
Mary Brewer
COUNTY
284 BOGER RD
MOCKSVILLE, NC 27028
Lab Number: 6049B
Sample Id : HARNETT WTP
AFL A&L Eastern Laboratories, Inc.
N21 Whltepine Road Richmond, Virglnla 23237 1004)7434401 Fox [phone]
a
wwwaleostern.cam
Project: HARNETT WTP
NC CERT#257
REPORT OFANALYSIS
Total Chromium
30
5
Total Nickel
13
5
Total Lead
8
5
Total Arsenic
8.0
3.0
Total Mercury
<0.4
0.4
Total Selenium
<5.0
5.0
pH (Standard Units)' 5.44
2.00
Total Molybdenum
<5
5
Chloride
860
200
Comments:
CHLORIDE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MSD WAS OUT OF LIMITS FOR "Se".
ALL OTHER QC DATA IS ACCEPTABLE.
Date Sampled: 2/23/2016 12:00:00
Date Received: 03/04/2015 00:00
Data Reported: 03/09/2015
KM
03/05/201512:30
SW 6010C
KM
03/05/201512:30
SW 6010C
KM
03/05/201512:30
SW 6010C
KM
03/05/201612:30
SW 6010C
KM
03105/201509:00
SW-7471B
KM
03/05/2015 12:30
SW 6010C
JM
03/05/2015 08:24
SW-9045D
KM
03/06/201612:30
SW 6010C
JM
03/06/201509:10
SM4500CI-D
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our wports and totters ere forme "clusiva and conrdendal use of ourctients, and may not be mproducod in whole or pan, nor may any reference be made
to the work, the result., or the company In any advat ising, news release, or other public a nounranlents without obtaining ourpror wrtlen oulhoubmiton.
Debbie Holt

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2037-01-WPL-NC HARNETT CO. UTIL., NC COH REGIONAL 212312015 211/2015-313112015 0.3231
WTP LIQUID
Na mg/l = (Na mglkg x % Solids) + 100 = (420 x 2.2000) + 100 = 9.24
Ca mgA = (Ca mg/kg x % Solids) + 100 = (1170 x 2.2000) + 100 = 25.74
Mg mgA = (mg mg/kg x % Solids) + 100 = (985 x 2.2000) + 100 = 21.67
Na meq = Na mgA + Molec.Wgt.Na =9.24 + 23 = 0.401739
Ca meq = Ca mg/l + Molec.Wgt.Ca = 25.74 + 20 = 1.287
Mg meq = Mg mg/l + Molec.Wgt.Mg = 21.67 + 12 = 1.80583
SAR = Na meq + SgrRoog0.5 x (Ca meq + Mg meq)] = 0.401739 + SgrRoog0.5(1.287+1.80583)] = 0.323058
Printed: 2/4/2016
Page 1 14:09

Page: 1 of 2
Report Number: 15-114-0204
Account Number: 46460
Submitted By: WILLVARNER
Send To: SYNAGRO CENTRAL LLC/HARNETT
Mary Brewer
COUNTY
284 BOGER RD
MOCKSVILLE, NC 27028
Lab Number: 61590
Sample Id: HARNETT WTP
�L A&L Eastern Laboratories, Inc.
7621 VRdtoplpe Road Rionnone, Virainla 232a7 (804) 7434%01 Fax [phone]
e
www,aleastem om
Project: HARNETT WTP
NC CERT#257
REPORT OFANALYSIS
Date Sampled: 4/22/2015 14:45:00
Date Received: 04/24/2015 00:00
Date Reported: 04/29/2015
Total Solids
2.68
26800
100.0
BW
04/24/201515:00
SM-254OG
Moisture'
97.32
100.0
BW
04/24/201515:00
SM-2540G
XTotal KJeldahl Nitrogen
1.04
Jr 10400
10.0
JM
04/27/2015 09:24
SM-4500-NH3C-TKN
Total Phosphorus
0.25
2490
100
KM
04/27/2015 13:15
SW 6010C
Total Potassium
0.05
459
100
KM
04/27/2015 13:15
SW 6010C
Total Sulfur
1.12
11200
100
KM
04/27/2015 13:15
SW 601OC
Total Calcium
0.15
1450
100
KM
04/27/2015 13:15
SW 601OC
Total Magnesium
0.14
1370
100
KM
04/27/2015 13:15
SW 6010C
Total Sodium
0.04
381
100
KM
04/27/2015 13:15
SW 6010C
Total Iron
23200
100
KM
04/27/2015 13:15
SW 6010C
Total Aluminum
116000
100
KM
04/27/2015 13:15
SW 6010C
Total Manganese
1710
5
KM
04/27/2015 13:15
SW 6010C
Total Copper
69
5
KM
04/27/2015 13:15
SW 601OC
Total Zinc
175
5
KM
04/27/2015 13:15
SW 6010C
Ammonia Nitrogen
0.11
)t 1120
10.0
JM
04/27/2015 09:24
SM4500-NH3C
Organic N
0.93
* 9280
10.0
04/27/2015 09:24
CALCULATION
Nitrate+Nitrite-N
<2.00
2.00
JM
04/27/2015 09:25
SM450ONO3F
Total Cadmium
<2.0
2.0
KM
04/2712015 13:15
SW 6010C
All values are on a dry weight
basis except as noted by asterisk. Detectibn limit on all N series Is on a wet basis.
Our reports and tellers are for the exclusiro and confidential use of ourclients, and may not be reproduced to whole orped, normay any Waroneo be. made
(4i
to the work, the results, or the company in any advertising, news release, or otherpublic announcements wthout obtaining ourprior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 15-114-0204
Account Number: 46460
Submitted By: WILL VARNER
Send To: SYNAGRO CENTRAL LLC/HARNETT
Mary Brewer
COUNTY
284 BOGER RD
MOCKSVILLE, NC 27028
Lab Number: 61590
Sample Id : HARNETT WTP
NA&L Eastern Laboratories, Inc.
7621 Whitepina Road Rloltmond, Vlrglnla 20237 (304)7434401 Fax 1@041 Z71-6440
wwweleastern.Gom
Project: HARNETT WTP
NC CERT#257
REPORT OFANALYSIS Date Sampled: 4/22/2015 14:46:00
Date Received: 04/24/2015 00:00
Date Reported: 04/29/2015
Total Chromium
35
5
KM
04/27/2015 13:15
SW 6010C
Total Nickel
16
5
KM
04/27/201513:15
SW-6010C
Total Lead
9
5
KM
04/27/2015 13:15
SW 6010C
Total Arsenic
8.0
3.0
KM
04/27/201513:15
SW 6010C
Total Mercury
<0.4
0.4
KM
041281201509:00
SW-7471B
Total Selenium
<5.0
5.0
KM
04/27/2015 13:15
SW 6010C
pH (Standard Units)" 5.58
2.00
JM
04/27/2016 09:24
SW-9045D
Total Molybdenum
8
5
KM
04/27/2016 13:15
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE RPD WAS OUT OF LIMITS FOR "NO3/NO2-N".
THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al".
"Cr", AND "Ni". ALL OTHER QC DATA
IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Ourrepons and letters am for the excfusiva and confidential use ofourrlients, and maynot be mpmduced in whole orped, normay any mfetonco be made
to the work, the remlls, orthe company in any advertising, news mlease. nrotherpublic announcements without obmining our pdor written authorization.
Debbie Holt

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
2037-01-WPL-NC HARNETT CO. UTIL., NC COH REGIONAL 4/2212015 411/2016-713112015 0.2807
WTP LIQUID
Na mg/I = (Na mg/kg x % Solids) + 100 = (381 x 2.6800) + 100 = 10.2108
Ca mg/I = (Ca mg/kg x % Solids) + 100 = (1450 x 2.6800) + 100 = 38.86
Mg mg/I = (mg mg/kg x % Solids) + 100 = (1370 x 2.5800) + 100 = 36.716
Na meq = Na mgA +Molec.Wgt.Na = 10.2108+23 = 0.443948
Ca meq = Ca mgA + Molec.Wgt.Ca = 38.86 + 20 = 1.943
Mg meq = Mg mgA + Malec.Wgt.Mg = 35.716 + 12 = 3.05967
SAR = Na meq + SgrRoot(0.5 x (Ca meq + Mg meq)] = 0.443948 + SgrRoot[0.5(1.943+3.05967)] = 0.280702
Printed: 2/4/2016
Page 1 14:09

Page: 1 of 2
Report Number: 15-212-0205
Account Number: 46460
Submitted By: WILL VARNER
Send To: SYNAGRO CENTRAL LLC/HARNETT
Mary Brewer
COUNTY
284 BOGER RD
MOCKSVILLE, NC 27028
Lab Number: 63248
Sample Id : HARNETT WTP
I
1
a G
Waypoint.
ANALYTICAL
7621 Whitepine Road, Richmond, VA23237
Main 804-743-9401 a Fax [phone]
www.waypointana lyticai.cbm
Project: HARNETT WTP
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 7/28/2015 11:00:00
Date Received: 07/31/2015 00:00
Date Reported: 08/05/2015
Total Solids
1.98
19800
100.0
RD
0713112015.00:00
SM-2540G
Moisture'
98.02
100.0
RD
07/31/201500:00
SM-2540G
*'Total Kjeldahl Nitrogen
1.31
k 13100
10.0
SB
08/04/2015 08:05
SM-4500-NH3C-TKN
Total Phosphorus
0.30
3010
100
KM
08/0312015 13:52
SW 6010C
Total Potassium
0.08
766
100
KM
08/03/2015 13:52
SW 6010C
Total Sulfur
1.26
12600
100
KM
08/03/2015 13:62
SW 6010C
Total Calcium
0.14
1380
100
KM
08/03/2015 13:52
SW 601CC
Total Magnesium
0.09
926
100
KM
08/03/2015 13:52
SW 601CC
Total Sodium
0.08
751
100
KM
08/03/2015 13:52
SW 6010C
Total Iran
21000
100
KM
08103/201513:52
SW 6010C
Total Aluminum
130000
100
KM
08/03/2015 13:52
SW 6010C
Total Manganese
1610
5
KM
08/03/2015 13:52
SW 6010C
Total Copper
261
5
KM
08/0312015 13:52
SW 6010C ,
Total Zinc
54
5
KM
08/03/2015 13:52
SW 6010C
�YAmmonlaNitrogen
0.30
3030
10.0
SB
08/03/20150BA5
SM-4500-NI3C
-XOrganlc N
1.01
%V10070
10.0
08/03/2015 08:15
CALCULATION
Nitrate+Nitrite-N
<2.00
2.00
SB
08/03/2015 08:15
SM-460ONO3F
Total Cadmium
<2.0
2.0
KM
08/03/2015 13:52
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series
is on a wet basis.
9'&aa��
Ourmpods and lacers are forthe exclusive and ronfidonflat use ofourdionts, andmaynotbe mpaducadin
whole orpad, normay anymfemnce be made
to Me work, the resulls, ortho company in any advertising, news release, or otherpi blIc announrements wtthout obla6Ung ourpdorwdttm authod2aflon.
Debbie Holt
I

Page: 2 of 2
Report Number: 15-212-0205
Account Number: 46460
Submitted By: WILLVARNER
Send To: SYNAGRO CENTRAL LLC/HARNETT
Mary Brewer
COUNTY
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 63248
Sample Id : HARNETT WTP
Total Chromium
Total Nickel
Total Lead
Total Arsenic
Total Mercury
Total Selenium
pH (Standard Units)
Total Molybdenum
5.82
is0
Way„®' ■ ■tn 7621 ain 80 -7 3-94 Richmond, 27 -6446
��••yy Maln 804-743-9401 °Fax [phone]
ANALYTICAL www.waypointanalytical.com
Project: HARNETT WTP
NC CERT#257
REPORT OFANALYSIS
Date Sampled: 7/28/2015 11:00:00
Date Received: 07/31/2015 00:00
Date Reported: 08/05/2015
31
5
KM
08103/201513:52
16
5
KM
08/03/2016 13:52
5
5
KM
081031201513:52
16.0
3.0
KM
08/031201513:52
<0.4
0.4
KM
08103/2015 09:00
<5.0
5.0
KM
08103/201513:52
2.00
SB
08/03/2015 08:15
18
5
KM
08/03/2015 13:52
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW-7471 B
SW 6010C
SW-9045D
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "Na" AND "Zn". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "AI", "As", "Fe", AND "Se". ALL OTHER
QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for Maoxclusive and confidential use of our clients, and may not be ml>mducod In whole orpart, nor may any lolomoco be made
to the work, the insult.^„ orthe company in anyadvenising, news in/ease, or otharpublic announcements without obtaining ourpdorwnden authorization.
Debbie Holt

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
2037-01-WPL-NC HARNETT CO. UTIL., NC COH REGIONAL 7/28/2015 8/1/2015-10/31/2015 0.5376
WTP LIQUID
Na mgll = (Na mg/kg x % Solids) + 100 = (751 x 1.9800) + 100 = 14.8698
Ca mg/I = (Ca mg/kg x % Solids) + 100 = (1380 x 1.9800) + 100 = 27.324
Mg mg/I = (mg mg/kg x % Solids) + 100 = (925 x 1.9800) + 100 = 18.315
Na meq = Na mg[l +Molec.Wgt.Na = 14.8698 +23 = 0.646513
Ca meq = Ca mg/I + Molec.Wgt.Ca = 27.324 + 20 = 1.3662
Mg meq = Mg mg/I + Molec.WgLMg = 18.315 + 12 = 1.52625
SAR = Na meq + SgrRoct(0.5 x (Ca meq + Mg meq)] = 0.646513 + SgrRoot(0.5(1.3662+1.52625)] = 0.5376
Printed: 2/4/2016
Page 1 14:10

Page: 1 of 2
.Report Number: 15-309-0205
Account Number: 46460
Submitted By: WILL VARNER
Send To: SYNAGRO CENTRAL LLC/HARNETT
Mary Brewer
COUNTY
284 BOGER RD
MOCKSVILLE, NC 27028
Lab Number: 65124
Sample Id: HARNETT WTP
Waypoint.
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 a Fax [phone]
www.waypointanalytical.com
Project: HARNETT WTP
NC CERT#257
REPORT OF ANALYSIS
k Date Sampled: 11/3/2015 13:15:00
Date Received: 11/05/2015 00:00
Date Reported: 11/12/2015
Total Solids
2.83
28300
100.0
JM
11/06/2015 08:44
Moisture.
97.17
_
100.0
JM
11/061201508:44
_t
S Total Kjeldahl Nitrogen
1.17
11700
10.0
JM
11/06/2015 08:35
Total Phosphorus
0.16
1620
100
KM
11/06/2015 14:38
Total Potassium
0.08
824
100
KM
11106/201514:38
Total Sulfur
1.15
11500
100
KM
11106/201514:38
Total Calcium
0.08
769
100
KM
11/06/2015 14:38
Total Magnesium
0.09
947
100
KM
11/06/2015 14:38
Total Sodium
0.05
483
100
KM
11/06/2015 14:38
Total Iron
21600
100
KM
11106/201514:38
TolalAluminum
112000
100
KM
11/06/2015 14:38
Total Manganese
1260
5
KM
11/06/2015 14:38
Total Copper
342
5 _
KM
11/06/2015 14:38
Total Zinc
56
5
KM
11/06/2015 14:38
y
->r Ammonia Nitrogen
0.18
1770
10.0
JM
11/06/2015 08:35
Organic N
0.99
�V`9930
10.0
11/06/2015 08:35
Nitrate+Nitrite-N
<2.00
2.00
JM
11/06/2015 08:35
Total Cadmium
<2.0
2.0
KM
11/06/2015 14:38
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series Is on a wet basis.
Our reports and /attars are for the exclusive end confidential use or our clients, and may not be mcmduced in whole orpad, normay any reference be made
to Ilia wale, tha results, orthe company In any advenislnp, news release. or olherpublic announcements wittiout obtalning ourpdor writtan authorization.
SM-2540G
SM-2540G
SM-4500-NH3C-TKN
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 601OC
SW 601OC
SW 6010C
SW 6010C
SW 6010C
SM-4500-NH3C
CALCULATION
SMA60ONO3F
SW 6010C
Debbie Holt

Page: 2 of 2
Report Number: 15-309-0205
Account Number: 46460
Submitted By: WILL VARNER
Send To: SYNAGRO CENTRAL LLCIHARNETT
Mary Brewer
COUNTY
284 BOGER RD
MOCKSVILLE, NC 27028
Lab Number: 65124
Sample Id : HARNETT WTP
0 10.
Waypoint
ANALYTICAL
7621 Whltepine Read,Richmond. VA 23737
Main 804-743-94010Fax [phone]
www.waypolntanalytica I. cam
Project: HARNETT WTP
NC CERT#257
REPORT OFANALYSIS
Date Sampled: 11/312015 13:15:00
Date Received: 11/05/2015 00:00
Date Reported: 11/12/2016
Total Chromium
43
5
KM
11/06/2015 14:38
SW 6010C
Total Nickel
17
5
KM
11/06/2015 14:38
SW 6010C
Total Lead
7
5
KM
11/06/2015 14:38
SW 6010C
Total Arsenic
9.0
3.0
KM
11/06/201614:38
SW 6010C
Total Mercury
<0.4
0.4
KM
11/06/2015 09:00
SW-7471B
Total Selenium
<5.0
5.0
KM
11/06/2015 14:38
SW 6010C
pH (Standard Units) •
6.50
2.00
JM
11/06/2015 08:35
SW-9045D
Total Molybdenum
8
5
KM
11/06/2015 14:38
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "Mo" AND "Na". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al" AND "S". ALL OTHER QC DATA IS
ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series Is on a wet basis.
Ourrepods and Isitam am lbrtho oxc/usiva and confidential use of ourclients, and maynot be mpreduced in whole or part, normay any relevance be made
to the work, the results, or the company in any advertising, news mtease, orother public announcements without obtaining ourpdor, written outhmintion.
Debbie Holt

t
6r
SAMPLING LOG#
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Phone:
SAMPLER
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SAMPLING
SAMPLE
# OF
SAMPLING METHOD
METHOD
LAB # SAMPLE I.D.
LOCATION
TYPE
CONTAINERS
DATE TIME PRESERVED
SHIPPED I
Relinquished by
by:
//-3-iS Y., 2z'
Relinquished by: pa Time Reclev
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Relinquished by: DAate Time Recleved by:
SPECIAL INSTRUCTIONS:
n5� For T.� monitaring purposes. PO#:
REMARKS:
SAMPLE
ANALYSIS REQUEST
I.D.
SL1
SL2
NH4-N
NO3 N
OrgNAnic
Cd
Cr
NI
Pb
As
Hg
So
pH
CaCO3
eul
Solids Volatile
Me
CI
NOz N
,
wiP
SL1: Total Solids (Moisture), Total Neldahl Nitrogen, Phosphorus, and Potassium
SU- Basic Test SL1 plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Capper and Zinc

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2037-01-WPL-NC HARNETT CO. UTIL., NC COH REGIONAL 11/3/2015 111112015-12131/2015 0.4612
WTP LIQUID
Na mg/l = (Na mg/kg x % Solids) + 100 = (483 x 2.8300) + 100 = 13.6689
Ca mgA = (Ca mglkg x % Solids) + 100 = (769 x 2.8300) + 100 = 21.7627
Mg mgA = (mg mglkg x % Solids) + 100 = (947 x 2.8300) + 100 = 26.8001
Na meq = Na mgA + Moleo. WgtNa = 13.6689 + 23 = 0.5943
Ca meq = Ca mgA + Molec.WgLCa = 21.7627 + 20 = 1.08813
Mg meq = Mg mg/I + Molec.Wgt.Mg = 26.8001 + 12 = 2.23334
SAR = Na meq + SgrRcot[0.5 x (Ca meq + Mg meq)] = 0.5943 + SgrRoct[0.5(1.08813+2.23334)] = 0.461164
Printed: 2/4/2016
Page 1 14:11

J `
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: HARNETTCO. UTR.ITIES, NC PREDOMINANT SOIL SERIES: LAKELAND
OWNER: HARNETTCOUNTY PERMIT N: W00014885 ANNUAL DRY TONS APPLIED: 725.26
SITE N: NC HA OOX43 FIELDA : HA OOX43 0001 OPERATOR: HARNETP COUNTY CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):• See list at bottom Of report ACRES UTILIZED: 39.30 ACRES PERMITTED: 39.30
Page: 1
Lime Applied •••
Date Lbs/Ac
allons (0) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
MONTH
Solids
per
Residual
Dry,
D Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
Total
Per Acre
1115115
272,800.00 (G)
�6941.476
1.93
0.559
HCUCOHV
DRY
0-<l2"
SUR
0.5
0.20
IS,000.p
2,590.00 p
130.00 p
3907
BERMUDAGRASS
1/16/15
148,800.00 (G)
3786.260
1.93
0.305
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
15,000.p
2,590.00 p
130.00 p
3907
BERMUDAGRASS
129/15
260.400.00 (G)
6625.954
1.93
0.533
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
15,000.p
2,590.00 p
130.00 p
3907
BERMUDAGRASS
1/30/15
80,600.00 (G)
2050.891
1.93
0.165
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
15,000.p
2,590.00 p
130.00 p
3907
BERMUDAGRASS
J1111-15
762,600.00 (G)
19,404.581
3/4115
303,800.00 (G)
7730.280
2.20
0.709
HCUCOHV
DRY
0•<12"
SUR
0.5
0.20
14,100.p
455.00 p
2.00 p
2959
BERMUDAGRASS
3/5/15
155,000.00 (G)
3944.020
2.20
0.362
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
14,I00.1)
455.00 p
2.00 p
2959
BERMUDAGRASS
3/19/15
198,400.00 (G)
5048.346
2.20
0.463
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
14,100.p
455.00 p
2.00 p
2959
BERMUDAGRASS
323/15
223,200.00 (G)
5679.389
2.20
0.521
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
14, 100.p
455.00 p
2.00 p
2959
BERMUDAGRASS
324/15
198,400.00 (0)
5048.346
2.20
0.463
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
14, 100.p
455.00 p
2.00 p
2959
BERMUDAGRASS
Mar-15
1,078,800.00 (G)
27,450.381
4/13/15
235,600.00 (0)
5994.911
2.68
0.670
HCUCOHV
DRY
O-<12"
SUR
0.5
0.20
10,400.p
1,120.00 p
2.00 p
2418
BERMUDAGRASS
4/14/15
99,200.00 (G)
2524.173
2.68
0.282
HCUCOHV
DRY
0-<I2"
SUR
0.5
0.20
10,400.p
1,120.00 p
2.00 p
2418
BERMUDAGRASS
Apr-15
334,800.00 (G)
8,519.084
5/12/15
322,400.00 (G)
8203.562
2.68
0.917
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
10,400.p
1,120.00 p
2.00 p
2418
BERMUDAGRASS
5113115
99,200.00 (G)
2524.173
2.68
0.282
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
10,400.p
1,120.00 p
2.00 p
2418
BERJv UDAGRASS
528115
198,400.00 (0)
5048.346
2.68
0.564
HCUCOHV
DRY
0-<I/2"
SUR
0.5
0.20
10,400.p
1,120.00 p
2.00 p
2418
BERMUDAGRASS
529/15
155.000.00 (0)
3944.020
2.69
0.441
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
10,400.p
1,120M p
2.00 p
2418
BERMUDAGRASS
May-15
775,000.00 (G)
19,720.101
619115
223,200.00 (0)
5679.389
2.68
0.635
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
10,400.p
1,120.00 p
2.00 p
2418
BERMUDAGRASS
6110115
223,200.00 (0)
5679.389
2.68
0.635
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
10,400.p
1,120.00 p
2.00 p
2418
BERMUDAGRASS
Jun-15
446,400.00 (G)
11,358.778
7/9/15
223,200.00 (G)
5679.389
2.68
0.635
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
10,400.p
1,120.00 p
2.00 p
2418
BERMUDAGRASS
7/10/15
223.200.00 (G)
5679.389
2.68
0.635
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
10,400.p
1,120.00 p
2.00 p
2418
BERMUDAGRASS
720/15
198,400.00 (0)
5048.346
2.68
0.564
HCUCOHV
*DRY
0-<1/2"
SUR
0.5
0.20
10,400.p
1,120.00 p
2.00 p
2418
BERMUDAGRASS
7/21/15
223,200.00 (0)
5679.389
2.68
0.635
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
10,400.p
1,120.00 p
2.00 p
2418
BERMUDAGRASS
Jul-15
968.000.00 (G)
22,086.513
821/15
235,600.00 (G)
5994.911
1.91t
0.495
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
13, 100.p
3.030.00 p
2.00 p
3531
BERMUDAGRASS
824/15
167,400.00 (G)
4259.542
1.98
0.352
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
13,100.p
3,030.00 p
2.00 p
3531
BERMUDAGRASS
Aug-15
403,000.00 (G)
10,254.453
9/9/15
111,600.00 (G)
2839.695
1.98
0.234
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
13,IOO.p
3,030.00 p
2.00 p
3131
BERMUDAGRASS
9/10/15
248,000.00 (0)
6310.433
1.98
0.52]
HCUCOHV
DRY
0-<l2"
SUR
0.5
0.20
13,IOO.p
3,030.OD p
2.00 p
3531
BERMUDAGRASS
9/11115
105,400.00 (G)
2681.934
1.98
0.221
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
13, 100.p
3,030.00 p
2.00 p
3531
BERMUDAGRASS
928115
266,600.00 (0)
6783.715
1.98
0,560
HCUCOHV
DRY
0-<1/2"
SUR
0.5
0.20
13,100.p
3,030.00 p
2.00 p
3531
BERMUDAGRASS
929/15
136,400.00 (0)
3470.738
1.98
0.287
HCUCOHV
DRY
0-<I2"
SUR
0.5
0.20
13,100.p
3,030.00 p
2.00 p
3531
BERMUDAGRASS

FACILITYNAME: HARNETTCO.UTILITIES,NC
OWNER: HARNETT COUNTY
SITE #: NC HA OOX43 FIELD# : HA OOX43 0001
RESIDUAL SOURCE(S):• See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: LAKELAND
PERMIT#: W00014885 ANNUAL DRY TONS APPLIED: 725.26
OPERATOR: HARNETT COUNTY CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 39.30 ACRES PERMITTED: 39.30
Page: 2
Lime Applied ••' .
Date Lbs/Ac
allons (0) or Cubic Yards ICY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or. Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
till-
eli-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(PP-)
Crop
MONTH
Total
Per Acre
Solids
Sep-15
868,000.00 (G)
22,086.515
10/14/15
198,400.00 (G)
5048.346
1.98
0.417
HCUCOHV
DRY
0-<1/2"
SUR
0.5
0.20
13,100.p
3.030.00 p
2.00 p
3531
BERMUDAGRASS
Oct-15
198.400.00 (G)
5,048-346
11/5/15
260,400.00 (G)
6625.954
2.83
0.782
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
11,700.p
1.770.00 p
2.00 p
2873
BERMUDAGRASS
1116115
105,400.00 (G)
2681.934
2.83
0.316
HCUCOHV
DRY
0-<1211
SUR
0.5
0.20
11,700.p
1,770.00 p
2.00 p
2873
BERMUDAGRASS
11/13/15
272,800.00 (G)
6941.476
2.83
0.819
HCUCOI-IV
DRY
0-<12"
SUR
0.5
0.20
11,700.p
1.770.00 p
2.00 p
2873
BERMUDAGRASS
11/14/15
99,200.00 (G)
2524.173
2.83
0.298
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
11,700.p
1.770.00 p
2.00 p
2873
BERMUDAGRASS
11/30/15
2t7,000.00 (G)
5521.628
2.83
0.652
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
11,700.p
1,770.00 p
2.00 p
2873
BERMUDAGRASS
Nov-15
954.800.00 (G)
24,295.165
12/1/15
148,800.00 (G)
3786.260
2.83
0.447
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
11,700.p
1,770.00 p
2.00 p
2873
BERMUDAGRASS
12/15/15
223,200.00 (G)
5679.389
2.83
0.670
HCUCOHV
MOIST
0-<12"
SUR
0.5
0.20
11,700.p
1,770.00 p
2.00 p
2873
BERMUDAGRASS
12/16/15
136,400.00 (G)
3470.738
2.83
0.410
HCUCOHV
MOIST
0-<12"
SUR
0.5
0.20
11,700. p
1,770.00 p
2.00 p
2873
BERMUDAGRASS
Dec-15
508,400.00 (G)
12,936.387

! 1
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: HARNETT CO. UTILITIES, NC
OWNER: HARNETTCOUNTY
SITE N: NC HA 0OX43 FIELDN : HA 0OX43 0001
RESIDUAL SOURCE(S):• See list at bottom of report
PREDOMINANT SOIL SERIES: LAKELAND
PERMIT H: W00014885
OPERATOR: HARNETT COUNTY
ANNUAL DRY TONS APPLIED: 725.26
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 39.30 ACRES PERMITTED: 39.30
I
Page: 3
Lime Applied...
Date Lbs/Ac
allons (0) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner-
orWet Tons (WT)(specify)
%
Tons
Cottd.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
TDATE
or
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
ntion
TKN
Nitrogen
and
Total
MONTH
PerAcre
1 am UauonstAc: 183,16 t-31
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
107
0.372
0.074
1.278
8.007
0.272
0.015
0.376
0.575
0.185
4.259
91.22
Cumulative lbs/acre
0.694
0.118
2.057
15.975
0.453
0.024
0.680
0.943
0.296
10.606
'
M777=r
Permit PAN Limit s/acre lst Cro nd Crop
Ib
( ) I P
'*
°t "t
�w,mr`E
l
R
�.�.�iw�Fr
147
i��tl
SurFfl
l+'YJJhfIFr
�41
�1�
J,.'.Ir4v �Y
fI.�LN4lµ .yl Ua friV I�.':11T�'
111 miv.t:
�iVM'-t'Ihr�
P�
AV h.11
, JTr.F.r�w� ,r-W
id.}
�.� F i. lnf �
PD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
Yi a
1339.0
267.9
15.0 1't ^fir 375.0
89.0
2500.0 r � '"'
�NJt{i
ixQ 11 IYLf4:�r
ir'
pIrlr`.tltY
rj
HCUCOHWPL= HARNETT CO. UTIL., NC COH REGIONAL WTP LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with asystem designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A =Not Applicable NR=Not Reportedor Not Required %=percent p=ppm or mg/kg •• Volatilizntion Rate: Surface 0.5. Injection/Incorporation 1.0
Application Method: SUR - Surface. 'INJ - Injection, SURIN - Incorporation ••• See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2016

i
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
ACB.H'YNAME: HARNETT CO. UTILITIES, NC PREDOMINANT SOIL SERIES: GILEAD
WNER: JAMES FARRAR PERMIT#: W00014885 ANNUAL DRY TONS APPLIED: 129.57
:TE #: NC HA OX124 FIELD# : HA OX124 0005 OPERATOR: JAMES FARRAR CATION EXCHANGE CAPACITY (NON-503):
ESIDUAL SOURCE(S):' See list at bottom of report ACRES UTILIZED: 26.90 ACRES PERMITTED: 26.90
Page: 1
Lime Applied "•
Date Lbs�Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Mincr-
orWet Tons(VM(specify)
"�"
Tons
Con
cation
till-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
427/15
260,400.00 (G)
9680.297
2.68
1.082
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
10,400.p
1,120.00 p
2.00 p
2418
BERMUDAGRASS
428/15
192,200.00 (G)
7144.981
2.68
0.798
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
10,400.p
1,120.00 p
2.00 p
2418
BERMUDAGRASS
Apr-15
452,600.00 (G)
16,825.278
528115
43,400.00 (G)
1613.383
2.68
0.180
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
10,400.p
1,120.00 p
2.00 p
2418
BERMUDAGRASS
529/15
24,800.00 (G)
921.933
2.68
0.103
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
10,400.p
1,120.00 p
2.00 p
2418
BERMUDAGRASS
May-15
68,200.00 (G)
2,535.316
623115
111,600.00 (G)
4148.699
2.68
0.464
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
10,400.p
1,120.00 p
2.00 p
2418
BERMUDAGRASS
624/15
291,400.00 (G)
10832.714
2.68
1.211
HCUCOHV
DRY
O- 12"
SUR
0.5
0.20
10,400.p
.1,120.00 p
2.00 p
2418
BERMUDAGRASS
625/15
235,600.00 (G)
8758.364
2.68
0.979
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
10,400.p
1,120.00 p
2.00 p
2418
BERMUDAGRASS
Jun-15
638.600.00 (G)
23,739.777

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
'ACILITY NAME: HARNETTCO. UTILTTIES, NC
PREDOMINANT SOIL SERIES: GILEAD
WINER: JAMES FARRAR
PERMIT #: W00014885
ANNUAL DRY TONS APPLIED: 129.57
ITE #: NC HA OX124 FIELD# : HA OX124 0005
OPERATOR: JAMES FARRAR
CATION EXCHANGE CAPACITY (NON-503):
tESIDUAL SOURCE(S):• See list at bottom of report
ACRES UTILIZED: 26.90 ACRES PERMITTED: 26.90
Page: 2
Lime Applied •••
Date Lbs/Ac
allons (G) or Cubic Yards (Cy)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Prec2
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
pef
Residual
Dry, Wet,
Pazt 24
Method
nation
nation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
Total Gallons/Ac: 43,10037
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
23
Annual Ibs/acre
0.077
0.019
0.337
0.665
0.087
0.004
0.077
0.154
0.048
1.686
23.99
Cumulative Ibs/acre
0.145
0.036
0.633
5.214
0.171
0.007
0.119
0.298
0.090
4.733
,crmit PAN Limit (lbs/acre) 1st Crop2nd Crop
�
120
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
HCUCOHWPL = HARNETT CO. UTIL, NC COH REGIONAL WTP LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for Mowing violations."
N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppm or mgflcg '• Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
• Application Method: SUR - Surface, INJ - Injection, SURIN- Incorporation ••• See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2016

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: HARNETT CO. UTILITIES, NC PREDOMINANT SOIL SERIES: GILEAD
OWNER: LAMES FARRAR PERMIT 4: W00014885 ANNUAL DRY TONS APPLIED: 59.57
SITE Ik NC HA OX124 FIELDP : PIA OX124 0006 OPERATOR: JAMES FARRAR CATION EXCHANGE CAPACITY QI ON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 34.70 ACRES PERMITTED: 34.70
Page: I
Lime Applied •*•
Data Lbs/Ae
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tom (WT)(specify)
%
Tons
Cond
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE orH
Per
Residual
Dry, Wet,
Past 24
Method
zatimr
zation
M
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
6/26115
217,000.00 (G)
6253.602
2.68
0.699
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
10,400.p
1,120.00 p
2.00 p
2418
BERMUDAGRASS PASTURE
Jun-15
217.000.00 (G)
6,253.602
816/15
297,600.00 (0)
8576.369
1.98
0.708
HCUCOHV
DRY
0-<I/2" '
SUR
0.5
0.20
13,100, p
3,030.00 p
2.00 p
3531
BERMUDAGRASS PASTURE
8/7/15
130,200.00 (G)
3752.161
1.98
0.310
HCUCOHV
DRY
0-<12"
SUR
0.5
0.20
13,100.p
3,030.00 p
2.00 p
3531
BERMUDAGRASS PASTURE
Aug-15
427,800.00 (G)
12,328.530
Total Gallons/Ac: 18,582.13
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual Ibs+acre
0.044
0.007
0.112
0.628
0.023
0.001
0.048
0.055
0.017
0.355
9.61
11
Cumulative Ibs/acre
0.056
0.010
0.166
1.458
0.036
0.002
0.056
0.081
0.025
0.910
Permit PAN Limit (lbs(acre) Ist Cropand Crop
n,
r 1
r t
N�
1 r
2 -'ly tt,;,
r } * r t ,
,, •«
y� �r �r r;
, tTt.'-,rt a :
120
.
a
T, ii
FD Cumulative Pollutant Loading Role Limit (lbs+nere)
36.6
34 8
}5. r)PI+ ''
1339.0
267.9
15.0 }' I It" 375.0
89.0
2500.0
HCUCOHWPL= HARNETT CO. UTIL., NC COH REGIONAL WTP�LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the informntion submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations,"
N/A=Not Applicable NR=Not Reported orNot Required %=percent p=ppm or mg/kg "• Volatilization Rate: Surface 0.5, InjectioNlncorporalion LO
Application Method: SUR- Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2016

R lA Suntans Environmental Technologies, Inc.
surs �Ky]' yr 3310 Win Sr.
MIFONMENTFL T24:HN0L—:;G4_S, T c Cuyahoga Falls, Ohio 44223
.0..:a:pG_.:i LsL•granres TEL: [phone] FLY.[phone]
Website., hrro:/Avw v.settekcam
February 28, 2015
Will Varner
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
Dear Will Varner: Order No.: 15021921
Summit Environmental Technologies, Inc. received 1 sample(s) on 2/20/2015 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
©�
Dr. Mo Osman
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
A2LA 0724.01, Alahema 41600, Arizom AZ0788, A&=" 88.M5, Caliramia 07256CA. Coloredo, Co®eWd PH-0105, Delaware, Florida NELAC
E97688, Georoa E87688 and 943. Who OH00923, Mhois 200061 and Reg.5, Indiana C-011-13, Kansas E-I0347, Kentucky (Uvdergound Storage Tack)
3, Keuft,ky 90146, L,16,iann 04061 and LA12004, Marne 2012015, Maryland 339, Massachusetes M-0PH92i, Mim.mm 4097I1, Monona CERT0099,
New Hampshire 2996. New Jersey OH006, New York 11777, North Carslina 39705 and631, Ohio Drinking Water 4170. Ohio VAP C1,0052, Oklahoma
9940, Oregon OIU00001, Pennsylvania 6&01335, Rhode isLavd LA000317, South Cerolina 92016001. Tenuessee TN04018, Teccs T104704466-11-5.
Region S STMS-L, USDA/APHIS P330-11-00244, Utah OH009232011.1, Vermont VT-87688, V-nginia 00440 and 1591, Washington C891, West
Vfi&ia 248 and 9957C and E87688, Wisconsin 399013010
Page 1 of 6

♦t` f„ Summit Emrroroaen(ol Technologies, Inc.
3310 Win St.
FN�9RU�h1E.L'ML r2C3�+iOL3C= , :x�, Cuyahoga Falls, Ohio 44223
A..3iytS::?FLatS.^.a'-=.rati.a TEL: [phone] FAX.. [phone]
Website: hao.,Av ,seuek.com
Workorder
Sample Summary
WOH: 15021921
28-Feb-I5
CLIENT: Synagro
Project: Harrett WTP
Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix
15021921-001 Hanett WT? 2/19PO 1511:00:00 AM 2-0/201512:50:OOPM Solid
Page 2 of 6

Summit Environmental Technologies, Inc. 33hWinCase NarrativeNarrative�1VC
w
.
16 P-vlgpN!dE^lT.t14"_'C .tahLO� �; e. Cuyahoga Falls Ohio 4422323 }yp({: 15021921
+^sn(i cz l TEL [phone] FAX: [phone]
Wehsite: huy.lAnnv.settekcom Date: 228/2015
CLIENT: Synagro
Project: Harrett WTP _
This report in its entirety consists of the documents listed below. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Paginated Report including Cover Letter, Case Narrative, Analytical Results, Applicable Quality
Control Summary Reports, and copies of the Chain of Custody Documents are supplied with this
sample set.
Concentrations reported with a J-Flag in the Qualifier Field are values below the Limit of Quantitation
(LOQ) but greater than the established Method Detection Limit (MDL).
Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods.
-, Estimated uncertainty values are available upon request.
' All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report.
Any comments or problems with the analytical events associated with this report are noted below.
( Original
Page 3 of 6

_
Srmunit Environmental Technolo es. Inc.
gr
3310 Win St.
WO#:
15021921
s
L-4
PVY1fiOt1T8E;SALT=CHi3t]�t?^�-,'eS..14C
Cuyahoga Falls, Ohio 44113 Date Reported:
P
2/282015
_
Anarvtasl Lsccrzmo:r.:;
TEL: [phone]JI FAX., [phone]
Company:
Synagro
Website: hno.,11 x vsenekcom
Address:
284 Boger Rd.
Mocksville NC 27028
Received:
2/20/2015
Project#:
Harrett WTP
TCLP Metals Analysis (6010)
Client ID#
Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
.DF
RegLvl
Run
Analyst
Harrett WTP
001
2/192015 TCLP Arsenic(As)
0.500
NO mg/L
Solid
EPA 6010 C
1
5.00
2/24/2015
WK
Harrett WTP
001
2119/2015 TCLP Badum(Ba)
5.00
NO mg/L
Solid
EPA 6010 C
1
100
2124/2015
WK
Harrett WTP
001
2/19/2015 TCLP Cadmium(Cd)
0.100
NO mg/L
Solid
EPA 6010 C
1
1.00
2124/2015
WK
Harrell WTP
001
2/19/2015 TCLP Chromium(Cr)
0.200
NO mg/L
Solid
EPA 6010 C
1
5.00
224/2015
WK
Harrell WTP
001
2/1912015 TCLP Lead(Pb)
0.500
ND mg/L
Solid
EPA 6010 C
1
5.00
2/24/2015
WK
Hartett WTP
001
2/192015 TCLP Selenium(Se)
0.500
NO mgli-
Solid
EPA 6010 C
1
1.00
21242015
WK
Harnett WTP
001
2/192015 TCLP Slver(Ag)
0.500
NO mg/L
Solid
EPA 6010 C
1
5.00
2.r24/2015
WK
TCLP Mercury Analysis (1311/7470)
Client ID# Lab HW Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
Harrell WTP 001 2/'19/2015 TCLP Mercury 0.00200 NO mg/L Solid EPA 7470 A 1 0.200 2/23/2015 ALJ
a
r
SVOC SW-846: 8081-TCLP Pesticides
Client ID#
Lab IDN
Collected Analyte
Rep Lunt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Harrett WTP
001
21192015 Chlordane, total
0.0250
ND mg/L
Solid
EPA 8081 B
1
0.0300
2252015
JRT
Harrett WTP
001
2119/2015 Toxaphene
0.0500
NO mglL
Solid
EPA 8081 B
1
0.500
2252015
JRT
Harrell WTP
001
2/19/2015 Enddn
0.00250
ND mgfi-
Solid
EPA 8081 B
1
0.0200
2/2512015
JRT
Harnett WTP
001
2119/2015 gamma-BHC
0.00250
ND mg/L
Solid
EPA 8081 B
1
OA00
2252015
JRT
Harrell WTP
001
7JI912015 Heptachlor
0.00250
NO mg/L
Solid
EPA 8081 B
1
0.00800
2r25/2015
JRT
Harrell WTP
001
2119/2015 Heptachlor epoxide
0.00250
ND mg/L
Solid
EPA 8081 B
1
0.00800
2/25/2015
JRT
Harrett WTP
001
21192015 Methoxychlor
0.00250
ND mg/L
Solid
EPA 8081 B
1
10.0
2125/2015
JRT
VOC by GC/MS (8260)-TCLP
Client M#
Lab ID#
Collected Analyte,
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Hartett WTP
001
2/192015 M-Dichlomethene
0.100
NO mg/L
Solid
EPA 8260 B
1
0.700
2242015
JCR
Harrell WTP
001
2I192015 1,2-Dichloroethane
0.100
NO mg/L
Solid
EPA 8260 B
1
0.500
2124/2015
JCR
Harnett WTP
001
2/19/2015 Benzene
0.100
NO mg/L
Solid
EPA 8260 B
1
0.500
2124/2015
JCR
Harrell WTP
001
2/1912015 Carbon tetrachlodde
0.100
ND mglL
Solid
EPA 8260 B
1
0.500
224/2016
JCR
HarrettWTP
001
2/19/2015 Chlorobenzene
0.100
NO mglL
Solid
EPA 8260 B
1
100
212412015
JCR
Harrell: WTP
001
2/1912015 Chloroform
0.100
NO mglL
Solid
EPA 8260 8
1
6.00
224/2015
JCR
Hartett WTP
001
2119I2015 Tetrachlomethene
0.100
NO mglL
Solid
EPA 8260 B
1
0.700
2124/2015
JCR
Hartett WTP
001
21192015 Trichlorcethene
0.100
ND mg/L
Solid
EPA 8260 B
1
0.500
2242015
JCR
Harnett WTP
001
2119/2015 Vinyl chloride
0.200
NO mg/L
Solid
EPA 8260 B
1
0200
2242015
JCR
Harrett WTP
001
2/192015 MEK
2.00
NO mg/L
Solid
EPA 8260 B
1
200
22412015
JCR
Page 4 of 6

}�
Srm nit Emn ironmental Technologies, Inc.
�'
3310 Win St.
wo#:
lsozlvzi
CLry#IROM7,1f7JTAc
T_trreOlOGi`c ,.:INC
Cuyahoga Falls, Ohio 44213
Date Reported:
2/282015
rSrz;V CSl ca^urarm8a.5
TEL: [phone] FIX.' [phone]
Company:
Synagro
Website: hm.-Il�nv.senekcom
Address:
284 Boger Rd.
Mocksville NC 27028
Received: 2/20/2015
Project#: HarrettWTP
SVOC 8270 TCLP BNA List
Client ID#
Lab ID#
Collected Analyte
Rep Lint Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Harrell WTP
001
V19I2015 1,4-01chlorobenzene
0.100
ND mg/L
Solid
EPA 8270 C
1
7.50
2/24/2015
JBN
Harrell WTP
001
W19/2015 2,4,5-Tdchlcrophenol
0.250
ND mg/L
Solid
EPA 8270 C
1
400
2/24/2016
JBN
Harnett WTP
001
2/1912015 2,4,6-Tdchloraphenol
0.250
ND mg/L
Solid
EPA 8270 C
1
2.00
2/24/2015
JBN
Harrell WTP
001
2/19/2015 2,4-Dinitrotoluene
0.100
ND mg/L
Solid
EPA 8270 C
1
0.130
2/24/2015
JBN
Harrett WTP
001
2119/2015 Cresols, Total
5.00
ND mg/L
Solid
EPA 8270 C
1
200
2124/2015
JBN
Harnett WTP
001
2/19/2015 Hexachloro-1,i
0.100
ND mg/L
Solid
EPA 8270 C
1
0.500
2124/2015
JBN
butadiene
Harrell WTP
001
2119/2015 Hexachlorobenzene
0.100
ND mg/L
Solid
EPA 8270 C
1
0.130
2124/2015
JON
Harrell WTP
001
2/19/2015 Hexarhlomethane
0.100
ND mg/L
Solid
EPA 8270 C
1
3.00
212412015
JBN
Hamett WTP
001
2/19/2015 Nitrobenzene
0.100
ND mg/L
Solid
EPA 8270 C
1
2.00
212412015
JBN
Harnett WTP
001
2/19/2015 Pentachlarophenol
0.250
ND mg/L
Solid
EPA 8270 C
1
100
2/24/2015
JBN
Harrett WTP
001
2/19/2015 Pyridine
0.250
ND mg/L
Solid
EPA 8270 C
1
5.00
2124/2015
JBN
SVOC SW-846: 8321 Herbicides-TCLP
Client IN
Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Harnett WTP
001
2119/2015 2,4-D
5.00 ND mg/L
Solid
EPA 8321 A
1
10.0
2/23/2015
AMZ
Harnett WTP
001
2/19/2015 2,4,5-TP
0.500 ND mg/L
Solid
EPA 8321 A
1
1.00
2/23/2015
AMZ
Page 5 of 6

t' _ a
�a t
Smmnit Environmental Technologies, Inc.
3Win
WO#:
15021921
Date Reported:
2282015
t
_JFMONi.LNTaL rErYVOLCr;s,3�[O
Cayaho g aFdls, Ohio 44223
P
TEL: [phone] FLY: [phone]
Company:
Synagro
Website: hnP.'1A w ,settekcom
Address:
284 Boger Rd.
Mocksville NC 27028
Received:
2/20/2015
Project#:
Harrett WTP
Client ID#
Lab ID# Collected Analyte
Result Units
Matrix
Method DF RL
Harnett WTP
001
2/19/2015
Flashpoint (140'F)
Harrett WTP
001
2/19/2015
Cyanide, Reactive
Harreft WTP
001
2/19/2015
pH
Harrett WTP
001
2/19/2015
Sulfide, Reactive
F j"
Run Analyst
>140 °F
Solid
EPA 1010
1 223/2015
TAH
ND ppm
Solid
EPA 9014
1 0.500 2/24/2015
TIR
5.21 s.u.@21.3
Solid
EPA 9045 D
1 2127/2015
DHC
C
ND pprn
Solid
EPA 9034
1 25.0 224/2015
TIR
Page 6 of 6

�J
n "„iveec-RPOUest/Chain.of CusiodY

Rev. 12
Dail_ 0727',3-
Summit Environmental Tecfinolcgies, Inc.
Cooler Receipt Forte
:ritais;f,.,sr,.:+n ,SL
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usm+ediatEty adloixica(SaiE'y
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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
r
Facility Name: Harnett CountyWTP WQ Permit Number: W00014885
WWTPName: Harnett County Regional WTP NPDESNumber: 00-076-84
Monitoring Period: From 01/01/15 To 3/31115
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) -Please indicate level achieved and alternative performed:
Class A: Fecal Coliform Testing
Alt. l/A (time/temp) X
Alt. 2/B (Alk Treatment) _ Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) _ AIL 5/Process to Further Reduce Pathogens _ Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost _ Heat Drying _ Heat Treatment _ Thermophilic
Beta Ray _ Gamma Ray _ Pasteurization
Class B:
AIL (1) Fecal Density AIL (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization _ Air Drying _ Composting _ Aerobic Digestion
Anaerobic Digestion _
if nnnlirahle to alternative nerfnrmed (Class A or Clnss B) comnlete the following mnnitorinv data -
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6
CFU
MPN/g
Colifomt
power per gram
of total solids
CFU
CFU/g
1000 MPN per gram of
22.1
22.1
CFU/g
0
4/yr
Grab
9222D
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed: - N/A
0ption/AIL 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(V S reduction) _
(40-day bench) _
(30-day bench) _ (Spec. 02 uptake)
Option/Alt 5
Option/Alt. 6
Option/AIL 7 Option/Alt. 8
(14-Day Aerobic) _
(AlkStabilization) _
(Drying —Stable) _ (Drying —Unstable)
Option/Alt 9
Option/Alt. 10
(Injection) _
(Incorporation) _
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement rn 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment"
Allan Rex O'Briant WTPSu Superintendent
P er and ti ( p ' Land Applier Name and Title (if applicable) (type or print)
f ���
_ ignature of Preparer* at Signature of Land Applier (if applicable)
•Preparer is defined in 40 Part 503.9(r) and 15A N AC T.1102 (2 6)
Date

aceAna�ical
w»mz{u-aN3hsom
March 02, 2015
Marshall Puryear
Synagro Technologies, Inc.
284 Boger Rd
Mocksville, NC 27028
RE: Project: Harnett WTP 2/19
Pace Project No.: 92238449
Dear Marshall Puryear:
Pace Analytical Services, Inc.
98001(incey Ave. Suite too
Huntersviile, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on February 20, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
—�
Chris Derouen
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Ir yO without the vrdtten consent of Paw Analytical Services, Inc.. Page 1 of 11
Bp

Pace Analytical Services, Inc.
® 9800Hun
�;ZeMalyfical ntersvi le, NC 28078
n w¢pacdabr= [phone]
r'
1 �
5
CERTIFICATIONS
Project Harnett WTP 2/19
Pace Project No.: 92238449
Raleigh Certification IDs
6701 Conference Drive, Raleigh, NC 27607
North Carolina Bioassay Certification #: 16
North Carolina Wastewater Certification #: 67
North Carolina Drinking Water Certification #: 37731
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Flodda/NELAP Certification #: E87627
North Carolina Drinking Water Certification M. 37706
Kentucky UST Certification M. 84
North Carolina Field Services Certification * 5342
West Virginia Certification # 357
North Carolina Wastewater Certification #: 12
Virginla/VEIAP Certification P. 460221
South Carolina Certification #: 99006001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page 2 of 11

ace Analygao
wxn!Pace�ahsmm
SAMPLE ANALYTE COUNT
Pmject Harnett WTP 2N9
Pace Project No.: 92238449
Pace Analytical Services, Inc.
980010ncey Ave. Sufte100
Huntersville, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92238449001 HARNETT WTP 1 ASTM D2974-87
EX
1
PASI-C
SM9221C E (MPN) 503
JW1
1
PASI-R
92238449002 HARNETT WTP 2 ASTM D2974-87
EJK
1
PASI-C
SM9221C E (MPN) 503
JW1
1
PASI-R
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc. Page 3 of 11

nrn:po^cd30.smm
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
980010ncey Ave. Suite 100
Huntersviile, NC 28078
[phone]
Project Harnett WiP 2119
Pace Project No.: 92238449
Sample: HARNETT WTP 1 Lab ID: 92238449001 Collected: 02119/15 15:30 Received: 0220/15 00:00 Matrix: Solid
Results reported on a 'dry-weight"basis
Parameters Results Units Report Umit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 97.7 % 0.10 1 0227115 10:25
92210E Fecal Colifonn, MPN RAL Analytical Method: SM9221C E (MPN) 503
Fecal Colifonns, MPN 22.1 MPN/g 0.018 1 02/20/15 13:58
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/0212015 04:55 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 11

�20,�apace!ats.com
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
98001Gncey Ave. Sutte100
Huntersviile, NC 28078
(704)875-9a92
Project Hamett WTP 2/19
Pace Project No.: 92238449
Sample: HARNETT WfP 2 Lab ID: 92238449002 Collected: 0211911515:35 Received: 02120/15 00:00 Matrbc Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 97.0 % 0.10 1
92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503
Fecal Colifonns, MPN 17.0 MPN/g 0.018 1
Prepared Analyzed CAS No. Qual
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 03/0212015 04:55 PM without the written consent of PaceAnalydcal Services, Inc.
02127/15 10:25
02120115 13:58
Page 5 of 11

ace Analytical
wmv.Pacela0smm
r-�
QUALITY CONTROL DATA
Project Harnett W)P 2/19
Pace Project No.: 92238449
QC Batch: PMSTl7560 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92238449001., 92238449002
SAMPLE DUPLICATE 1398558
92238449001 Cup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 97.7 96.4 1
Pace Analytical Services, Inc.
980010ncey Ave. SuRe100
Huntersviile, NC 28078
[phone]
SAMPLE DUPLICATE 1398659
92238876002 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 17.7 17.7 0
i
-' � Results presented on this page are In the units Indicated by me 'Units -column except where an alternate unit Is presented to the right of the result
i�
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 03/02J2015 04:55 PM without the written consent of Pace Analytical Services, Inc.
Page 6 of 11

Pace Anatytical Services, Inc.
a 9800 Kncsy Ave. Sude WOaee .Analytical Huntersville, NC 20078
u wapacda0smm [phone]
QUALITY CONTROL DATA
Project Harnett WiP 2/19
Pace Project No.: 92238449
QC Batch: RBIOf4855 Analysis Method: SM9221C E (MPN) 503
QC Batch Method: SM9221C E (MPN) 503 Analysis Description: 92210E Fecal Cortfonn, MPN Solid
Associated Lab Samples: 92238449001, 92238449002
METHOD BLANK 1397678 Mabiic Solid
Associated Lab Samples: 92238449001, 92238449002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms, MPN MPN/g NO 0.018 0220/15 13:58
SAMPLE DUPLICATE: 1397679
92238449002 Dup
Parameter Units Result Result RPD Qualifiers
Fecal Colifonns, MPN MPN/g 17.0 7.4 79 1g
Results presented on this page are In the units Indicated by the 9rnits' column a mptvhem an alternate unit b presented W in. right of the resuR
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 0310212015 04:55 PM wilhart the written consent of Pare Analytical Services, Inc.
Page 7 of 11

QUALIFIERS
Project Harnett WlP 2119
Pace Project No.: 92238449
DEFINITIONS
Pace Analytical Services, Ina
9800 IGncey Ave. Sude 100
Huntersville, NC 28078
[phone]
OF- Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
NO - Not Detected at or above adjusted reporting limit
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL-Adjusted Method Detection Limit
PQL- Practical Quantitation Limit.
RL - Reporting Limit
S- Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matra Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonithle by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
Add preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the conent list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
PAST-R Pace Analytical Services - Raleigh
ANALYTE QUALIFIERS
1g This is a less than value.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/02/2015 04:55 PM without the written consent cf PaceAnalytical Services, Ina. Page 8 of 11

QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project Harnett WiP 2119
Pace Project No.: 92238449
Lab ID
Sample ID
QC Batch Method
QC Batch
92238449001
HARNETT WTP 1
ASTM 02974-87
PMST17560
92238449002
HARNETT WTP 2
ASTM D2974-87
PMSTl7560
92238449001
HARNETT WTP 1
SM9221C E (MPI) 503
RBI0/4855
92238449002
HARNETT WTP 2
SM9221C E (MPN) 503
RBIOA855
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 0310212015 04:55 PM without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Ino.
98001Gncey Ave. Suite100
Huntersville, NC 28078
[phone]
Analytical
Analytical Method Batch
Page 9 of 11

IceArralytical"
w vw pacelah i,
870T Conference Drive, Raleigh, NC 27607
C(1MCeAff6rNN't WCer)tN3 4-64
Chain. of Custody
W10. #
Report Results To_: 6111 To:�
Company: 1//'I-f � el �C'e,J Project Reference:
Address: 7 : r�� ✓^ti i
Project Number:
Attn: t u Ctid/ �i Purchase Order #:
Phone: �� �U9 8rr �. O Standard Report Delivery
11. rr // ❑ Rush Report Delivery. (w/surcharge)
W Fax: I V'r VAr<4 l_t G L.� hGi �+rc "Rush projectsam subject W prior appiavarby
l� � Ihefeboramry
Sampfedby(signature):
Requested Due Date:
ReM shed by (sgriaiuref
ivied
lure
�D a
Time
�geFML fished by (OgnaFure)
R ivied -fry (stgnamre �
O
Time
e
�Relrrrqu(shedby(signature)
Received by(signatum)
Date
TM
Recalpr.Conditions(L�¢eL�9 O.Ny)
❑ 4±2°C O.TBMPVI7 _°C
Res..Chfarine_
OAbsent ❑Present Orda
AcIdpredery <2?
Q Yes O-No ❑ n/&
Basapresew.>12?
❑ Yes O No 11 ofa
Page 10 of 11

�1
Document No.: laeumgnumvuuc?•
F-RAL-GS=001.4ev.02 PacsAsheifille Quality Office
Client Name:
Where Received: ❑ Huntersviltep Asheville El Fden Raleigh
Coudor (Circle): • FedEx UPS LISPS Client Commercial Pace .Other
Custody Seal art CoolenSax Present: I] yes no Seats intact 'yes, E]`no
Packing.Materfal: 0 Bubble.YVrap ' Bubble Bags None otter
Circle Thermometer UsedriR Gun N:1220653677 Of Ice: Wet Blue None ElSamptas on ice, cooling processh" begun
e.-e ., vonacn�t
Temp Correction Factor:V Add 1- ubtract
. Z G
Date and initials ot'persen examining
co to i Prey ati
CorrectedCoolerTemp.:. C
Biological TlssueisFrozen:
Yea No NiA
- cl,
Temp should be above freezing to 6'43
Comments:
-
hdin of Cestod- Present:
P<s -ONo
OWA
1: .• -- - •• - -
.Chain ofCustodyFilled Out:
Yes ONO
OWA
2 '
Chalk of CustodyRelln luished:
yes ON.
OtilA
3.
Sam rerName&.Si nature onCOG.
es ONO
OWA
4.
Sant las7MVsd within Hold Time:
Yes ONO,
ON/A
5.-
ShortHold Time Anal fs <72hr:'
VfY,. [IN.
ONIA
6."
Rush Turn Around Time Requested:
OYes No
ONfA
7.
SufficientVolume:
yos ONO
OWA
8.
�Corredfcontstners Used:
Yes ONO
OWA
9. ..
=PacaConfafnersUsed.
ae ONO
OWA
Containers Inlact
Yes ONO
OWA
10. '
Fliteredvolume"tecefvedfor Dlssolvedtests
ElYas ONO.
WA
It-
Sampie.Labels match COC:
Y ONO .OWA
�
V.
-Includes date4itne/IDfAnatysis Matffxt
A¢mntaNem needing preserva,Nan have bean ched(ed.
v-�w ONO
�Ve,
OWA
13.
AD bontainers"needing preservation am found to be In
compliance with EPA rerommendatian.
ONO
OWA
emepVons:y0A, 4ardonrt TOC. o&G,WI-0Reivaferl
!�� ON.
'
Samples checked-fordechlodnatlan
ea. ON.
OWA
14•
Headspdcein-VOAVials(>6mm):
Oyes ONO
- A
15. "
Trip Blank Present
Trip Blank Custody Seals Present
OYes ONo
OYes ONo,
WA
AA
16.
Pace Trip Blank lot # Iff purchased):
Client Notification/Resolution: Field Data .Required? Y'I N
PersorrContacteds DafelTme:
Commonfef Resolution:
SCURF/SRF Date: , WO#,: 92238449 "
Review:. '
Note: Wheneverthemisadrscfepancyaffeding-North fma comptlance
samples; a copy ofnas f %ill'be santto the North Carolina DEHNR
ceN6cation"ofica(i.e cot othold,incorrect.preservailve,outoftemp, 92238449' '
income ctcontalners) ".
Page 11 of.ii

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
T^ Facility Name: Harnett County WTP WQ Permit Number: W00014885
WWTPName: Harnett County Regional WTP NPDESNumber: 00-076-84
Monitoring Period: From 4/01/15 To 6/30/15
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A: Fecal Coliform Testing
Alt. 1/A (time/temp) X
Alt. 2/13 (Alk Treatment) _ Alt. 3/C (Prior Testing) _
Alt. 4/D (No Prior Test) _ Alt. 5/Process to Further Reduce Pathogens _ Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost _ Heat Drying _ Heat Treatment Thermophilic
Beta Ray _ Gamma Ray _ Pasteurization
Class B:
Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6
CFU
CFU/g
Coliform
power per gram
of total solids,
CFU/g
CFU
1000 MPN per gram of
6.6
6.6
CFU/g
0
4/yr
Grab
9222D
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: - N/A
0ption/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt. 4
(VS reduction) (40-day bench) (30-day bench) (Spec. 02 uptake)
Option/AIL 5
(14-Day Aerobic)
Option/Alt. 9
(Injection)
Option/Alt 6
(Alk Stabilization)
Option/Alt. 10
(Incorporation)
STATEMENT (please check the appropriate statement)
Option/Alt. 7 Option/Alt. 8
(Drying —Stable) (Drying —Unstable)
No vector attraction reduction alternatives were performed
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFk 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met" (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.) — See Tab 91
`"this determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met.I am aware that there are significant penalties for false certification including fine and imprisonment"
fJ/Land Applier Name and Title (if applicable) (type or print) —
ate� Signature of Land Applier (if applicable) Date
'Preparer is defined in 40 CFR Pa%'56.9(r) and 15A NCAC 2T.1102 (26)

aceAnalytical
www.pa-ca'aAamm
April29, 2015
Marshall Puryear
Synagro Technologies, Inc.
284 Boger Rd
Mocksville, NC 27028
RE: Project: Harnett Fecals 4/22
Pace Project No.: 92246808
Dear Marshall Puryear:
Pace Analytical Services, Inc.
980010ncey Ave: Suite,00
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on April 23, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location' indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
4—
Chris Derouen
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This repart shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pagel of 11

e
swwpsca!aEamrn
Project: Harnett Fecals 4122
Pace Project No.: 92246808
Raleigh Certification IDs
6701 Conference Drive, Raleigh, NC 27607
North Carolina Wastewater Certification At: 67
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification # 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
I
CERTIFICATIONS
North Carolina Bioassay Certification A 16
North Carolina Drinking Water Certification #: 37731
FloridaINELAP Certification #: E87627
Kentucky UST Certification #. 84
West Virginia Certification #: 357
VrginiaNELAP Certification#: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except In full,
withoutthe written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hurttersville, NC 28078
[phone]
Page 2 cf 11

Pace Analytical Services, Inc.
aceMalytical" 9800 Huncey Ave. Suite IDO
ntersville, NC 28078
k Pacelatexm [phone]
I'
SAMPLE ANALYTE COUNT
Project
Pace Project No.:
Harnett Fecals 4/22
92246808
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92246808001
HARNETT 1
ASTM D2974-87
EX
1
PASI-C
SM9221C E (MPN) 503
JW1
1
PASI-R
92246808002
HARNETT 2
ASTM D2974-87
EX
1
PASI-C
SM9221 C E(MPN) 503
JW1
1
PASI-R
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 11

/�570I Analyfleal e
9 wwwpacalabamm
ANALYTICAL RESULTS .
Pace Analytical Services, Inc.
9800 Kncey Ave. Suite 100
HuntersWle, NC 28078
[phone]
Project Hamett Facets 4122
Pace Project No.: 92246808
Sample: HARNETT 1 Lab ID: 92246808001 Collected: 04/22/15 14:45 Received: 04/23/15 09:10 Matdx: Solid
Results reported on a 'dry weight- basis and are adjusted forpercent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 97.0 % 0.10 1 04/29/15 13:26
9221 CE Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503
Feral Colifonns, MPN 6.6 MPN/g 0.018 1 04/2311511:10
Date: 04/29l2015 05:22 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page of 11

Pace Analytical Services, Inc.
98001Qncey Ave. Su00100
Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project Harnett Fecals 4/22
,Pace Project No.: 92246808
Sample: HARNETT 2 Lab IO: 92246808002 Collected: 04/22/15 14:50 Received: 04/23/15 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM 02974-87
Percent Moisture 97.5 % 0.10 1 04/29/15 13:27
92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN 8.0 MPN/g 0.018 1 04/23/1511:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 04/2912015 05:22 PM without the written consent of Pace Analytical Services, Inc.
Page 5 of 11

aceAnalytical
iwnapacetaDsmm
t F
QUALITY CONTROL DATA
Project - Harnett Fecals 4/22
Pace Project No.: 92246808
QC Batch: PMSTr7786 - Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight(Percent Moisture
Associated Lab Samples: 92246808001, 92246808002
Pace Analytical Services, Inc.
98001Gncey Ave. Suite too
Huntersville, NC 28078
[phone]
SAMPLE DUPLICATE: 1446054
92247220001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture ere 10.9 11.2 3
SAMPLE DUPLICATE: 1446055
92246808002 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 97.5 96.7 1
i
Results presented on this page are in the units indicated by the'0niW column except whem an alternate unit Is presented to the right of the rerun.
i
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/29/201506:22 PM without the written consent of Pace Analytical Services, Inc,.
Page 6 of 11

Paco Analytical services, Inc.
Analytical
l+.,I® 9800Kncey Ave. SUfte1U0
F1nalytical HuMersMle, NC 28078
vnnvpace!a6srnrrr [phone]
QUALITY CONTROL DATA
Project Harnett Facets 4/22
Pace Project No.: 92246808
QC Balch: RSIO15038 Analysis Method: SM9221C E (MPN) 503
QC Batch Method: SM9221C E (MPN) 503 Analysis Description: 92210E Fecal Coliform, MPN Solid
Associated Lab Samples: 92246808001,92246808002
METHOD BLANK: 1444262 Matrix: Solid
Associated Lab Samples: 92246808001, 92246808002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms, MPN MPN/g NO 0.018 041/2311511:10
SAMPLE DUPLICATE: 1444263
92246808002 Dup
Parameter Units Result Result RPD Qualifiers
Fecal Coliforms, MPN MPNfg 8.0 7.2 11
I Results presented on We page am in the units Indicated by the "Units• column except where an alternate unit Is presented to the right of the result
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/29/2015 05:22 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 11

Pace Analytical Services, Inc.
41181 IC�Id 980016ncey Ave. Suite 100
Hwrtersville, NC 28078
mwRp?cNaCsmm [phone]
QUALIFIERS
Project Harnett Fecals 4122
Pace Project No.: 92246808
DEFINITIONS
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL- Practical Quantilation Limit
RL- Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPAguidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matra Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
t
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
i Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Yrryl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylcn!Wle by EPA
Method 8260.
N-Nitrosadiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each anaiyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services - Chadotte
PASI-R Pace Analytical Services - Raleigh
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/2912015 05:22 PM without the written consent of Pace Analytical Services, Inn. Page 8 of 11

Analytical
w ..Pacdadaaan
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
98001GnceyAve. Suhe 100
Huntersville, NC 28078
[phone]
Project
Pace Project No.:
Hamett Fecals 4/22
92246808
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method Batch
92246808001
HARNETT 1
ASTM D2974-87
PMSTI7786
92246808002
HARNEW 2
ASTM D2974-87
PMSTf7786
92246808001
HARNETT 1
SM9221 C E (MPN) 503
RBIO/5038
92246SU8002
HARNETT 2
SM9221 C E (MPN) 503
RBIO/5038
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/29/2015 05:22 PM without the written consent of Pace Analytical Services, Inc. Page 9 of 11

Y4 �yA a Chain of Custody
a eAnalvtical w.O: #
Bill Ta
4-1
Project Reference: g22(-(6r69
Project Number. -
Purchase Order M.
❑ Standard Report Delivery
❑ Rush Report Delivery (wlsurcharge)
"Flush Ptajecthm sut$ecttu prlarepproval by .
the taeomtory
Requested Due Date:
YFAd
^�__®
• r x
yA'4
tr �.
i >n
-Y
ti
t
! ti
•� ,
v LL r I
'
Page 10of 11

DecumenfNamexSemplsGcmditloaUpon
Document Revised: April04,2916
Receipt ($CUR)
page fof 2
Document W1,
issuing Authorities:
FRAL-GS-001-rey.02
Pace Asheville Quali Office
Client Name: J'
] Huntersville [i Ashevill E] den Raleigh
:x UPS USPS Client • Commercial Pace Other
1xPresent: I] yes J�rno, Seals.lntact ,dyes 0 no .
Ile Wrap Q, Bubble Bags rt,-"f( Other
IR G� SN:122065387T Iof Ice: Wet Blue None �Samplesomice, .wo0r>p process has begun
���.
'^ Fjemp Cajvection Factor: Add 1 ubtract U�.C'. -
Date and initials of per arte aminrng
cc to / P rva
CoYrecEe�' Cooter Temp.: l� G
Blologfcal,Tlssue is Frozen:
Yes 11qNIA._
aheale i
;'�Temgshohld be above freezing to 6'0
Comments:
Chaln64 66stod Present:. •
es ON. -OWA
4 -
-
CheinofCustod -Filled Out•
as ONO OWA
2. '
�-[ COf CUstody Relln U(shed:
9fY. [IN. OWA
3.
!` SAffioiI rJai me & Signature on COC7
Yes ONO ❑WA
4.
'
s- Sa"ro Ariived within Hold Tlme:
Yes ONO 'dwA
5,
.los
Sljort.HolB:Tlme Analysis' <12hr :
roe ONo OWA
6.
Rtisfi�7urn.Around Time Requested:
OYsa NO OWA
7_
.
'SLfftclerit:Volume:
Yw ONo ONrA
8.
Ce2e61Containers Used:
as ONO OWA.
9. -
`.:-Aiaonfainers Used:
(L.IYes ONO OWA
elders Intact:
4as ONO OWA.10.
-
Fill'etedr$oluirfa`raceived for Dissolved tests
I7Yes ONO ..f )WA
11.
`..,"': •:.
Samplo L•abals match COG
Yes Qj o OWA
12.
Includes dateltimalID/Analysis ivlahlx:
C'
•! Nl.cohfainers needfAg preservariarthave bean Chadred.
as ONO [TWA
13,
All cgntalgers needing preservation are found to be in
Ces ONO OWA
cempaancE WIII' EPA recommendation.
aly. ONO
'
, ezcapaons:_VOh m5form.TOC,OBG,INMR0(Water)
rs
Sam les;oheckedfordecfi:odnatlon:
os ONO OWA
14,
[
Hoadsprcri Ih VOA Vials '�6mm :
Oyes ONO A
16.
OYas ONO FkA 16.
Tnp.Blant .Present•
6WA
Tr p,Btaftk.Cusfody Seals Present
Oyes ❑ko
PaceTdpP Blank Lot# (if purchased):
cilentNdtiflcatlonj Resolution:
Field Data Required? Y '/ N- -
r't~Pehori;Contacteds
.Gominenls/�Resotu0on:
- -_ DateMme:
i SCURF I$RF Date:
140
922468O8
r
`Wh'enever there is adisrrepsncy affecting Noith Ca Tina compl!ance
`II�II��I�I
III�II��IIII
fNoto
_ NsaO;nias's mov of ibis fortn.vrilfbnsentlo fhallodh Carolina prFNR
La out of held, incorrect presMsUve, our Or ramp,
ihwrrectcontafners)
92246808: ..
Page 11 of 91

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Harnett CountyWTP WQ Permit Number: W00014885
W WTP Name: Harnett County Regional WTP NPDES Number: 00-076-84
Monitoring Period: From 07/01/15 To 09/30/15
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A: Fecal Coliform Testing
Alt. 1/A (time/temp) X Alt 2B (Alk Treatment) _ Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) _ Alt. 5/Process to Further Reduce Pathogens _ Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost _ Heat Drying _ Heat Treatment _ Thermophilic
Beta Ray _ Gamma Ray _ Pasteurization
Class B:
Alt (1) Fecal Density Alt (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization _ Air Drying _ Composting _ Aerobic Digestion
Anaerobic Digestion _
�.�..... _u__..., a:.... ......0 ---A tol... A n. r'l— M rmmntnfp fhp fnllnwinv mnnifnrinv dafne
.... .... ...
Parameter
............. .-
Allowable Level in Sludge
Pathogen Density
No. of
Excee-
Frequency
of
Sample
Type
Analytical
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10to the 6
CFU
CFU/g
Coliform
power per gram
of total solids
CFU/g
CFU
1000 MPN per gram of
12.1
12.1
CFU/g
0
4/yr
Grab
9222D
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: - N/A
0ption/Alt 1
Option/Alt. 2
Option/Alt 3 Option/Alt 4
(VS reduction) _
(40-day bench) _
(30-day bench) _ (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic) _
(AlkStabilization) _
(Drying —Stable) _ (Drying —Unstable)
Option/Alt 9
(Injection) _
Option/Alt. 10
(Incorporation) _
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the ppathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement to 40 CFR 503.33/15A NCAC 02T.1107 have been met"
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met" (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties fpr false certification including fine and imprisonment."
Pre ern title (ty r ri '— Land Applier Name and Title (if applicable) (type or print)
g6a& re of Prep are rA Dat Signature of Land Applier (if applicable)
•Preparer is defined in 40 CFR Part 503.9(r) and 15A CAC 2T.1102 (26)
Date

PawAna"val Services, Inc.
9800 Kncey Ave. Suite 100
Huntersville, NC 28078
[phone]
August 07, 2015
Marshall Puryear
Synagro Technologies, Inc.
284 Boger Rd
Mocksville, NC 27028
RE: Project: Harnett 7/27
Pace Project No.: 92260491
Dear Marshall Puryear:
Enclosed are the analytical results for sample(s) received by the laboratory on July 27, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
ll 'Q;; C:�u
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 11

ly4:11 If W l_y_AIII Ill k'&.
Project Harnett 7/27
Pace Project No.: 92260491
Raleigh Certification IDs
6701 Conference Drive, Raleigh, NC 27607 North Carolina Bioassay Certification#: 16
North Carolina Wastewater Certification #: 67 North Carolina Drinking Water Certification #: 37731
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Florida/NELAP Certification #: E87627
North Carolina. Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
West Virginia Certification #: 357
North Carolina Wastewater Certification #: 12
Virginia/VELAP Certification #: 460221
South Carolina Certification #: 99006001
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, Inc.
9800 I0ncey Ave. Suite 100
Hurnersvi9e, NC 28078
(704)878-g092
This report shall not he reproduced, except in full,
Whout the written consent of Pace AnalyBW services, Inc.
Page 2 of 11

Pace Ana"cal Services, Ina
Analytical a 9800 Kncey Ave. Suite 100
Hurdersw9e, NC 28078
aM1sw.Paaaba= [phone]
SAMPLE ANALYTE COUNT
Project
Pace Project No.:
Hamett 7127
92260491
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92260491001
HARNETT WTP 1
ASTM D2974-87
CLW
1
PASI-C
SM9221C E (MPN) 503
JW1
1
PASI-R
92260491002
HARNETT WTP 2
ASTM D2974-87
CLW
1
PAS(-C
SM9221C E (MPN) 503
JW1
1
PASI-R
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Ina. Page 3 of 11

Pace Analytical Services, Inc.
a 9800Huntefsville, NC 28078 ace>4nalyfieal
twnepacerafaaoxn [phone]
s^�
ANALYTICAL RESULTS
Project Harnett 7127
Pace Project No.: 92260491
Sample: HARNETT WTP 1
Lab ID: 92260491001 Collected: 07/27/15 12:32
Received: 07/27/15 14:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF
Prepared Analyzed CAS No. Qual
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
98.5 % 0.10 1
08/05/15 13:09
92210E Fecal Coliform, MPN RAL
Analytical Method: SM9221C E (MPN) 503
Fecal Colifonns, MPN
12.1 MPN/g 0.018 1
0728115 09:25
Date: 08/07/2015 05:14 PM
REPORT OF LABORATORY ANALYSIS
This report shall not he repmduced, except in full,
without the written consent of Pam Analytical Services, Inc..
Page 4 of 11

ace -Analytical e
vmepoz'adsom
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kmcey Ave. SuBe too
Hunterswlle, NC 28078
(704)9759092
Project: Harnett 7127
Pace Project No.: 92260491
Sample: HARNETT WTP 2
Lab lD: 92260491002 Collected: 07/271/5 12:36
Received: 07/27115 14:40 Matra: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit OF
Prepared Analyzed CAS No. Qual
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
98.1 % 0.10 1
08/06/15 13:10
92210E Fecal Coliform, MPN RAL
Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN 1
23.6 MPN/g 0.018 1
07/28/15 09:25
Date: 08/07/2015 05:14 PM
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page 5 of 11

hmvpamlabscon
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 ICncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project
Harnett 7/27
Pace Project No.:
92260491
QC Batch:
PMST/8206 Analysis Method: ASTM D2974-87
QC Batch Method:
ASTM D2974-87 Analysis Description: Dry Weight(Percent Moisture
Associated Lab Samples: 92260491001, 92260491002
SAMPLE DUPLICATE: 1525895
M60491001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 98.5 98.6 0
SAMPLE DUPLICATE: 1525896
92261503011 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 16.9 16.4 3
�,. Results presented on this page am in Me units indicated by the 'Units' column except where an altemate unit is presented to the right of the mealt.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 081071201505:14 PM without the written wnsent of Pan Analytical Services,Ina.
Page 6 of 11

a
xswwpa'celablmm
QUALITY CONTROL DATA
Project Harnett 7127
Pace Project No.: 92260491
QC Batch: RBI0/5323 Analysis Method: SM9221C E (MPN)503
QC Batch Method: SM9221C E (MPN) 503 Analysis Description: 92210E Fecal Califonn, MPN Solid
Associated tab Samples: 92260491001, 92260491002
METHOD BLANK 1522057 Matrix: Solid
Associated Lab Samples: 92260491001,92260491002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms, MPN MPN/g ND 0.018 07/28/15 09:25
Pace Analytical Services, Inc.
9800 Kinney Ave. Suite 100
Huntemwlle, NC 28078
[phone]
SAMPLE DUPLICATE: 1522058
92260491002 Dup
Parameter Units Result Result RPD Qualifiers
Fecal Colifonns, MPN MPN/g 23.6 10.5 77
w
1
\ Resuffs presented on We page are In the unite inClcated by Me'Unifs' calumn except where an alternate unit to presented to the right of the nmu1L
REPORT OF LABORATORY ANALYSIS
This report shal not be reproduced, except in full.
Date: 08/07/2015 05:14 PM without the written consent of Pace Analytical Services, Inc.
Page 7 of 11

wvnvpaoyabawar
QUALIFIERS
Project Hamett 7127
Pace Project No.: 92260491
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL- Practical Quantitation Limit.
RL- Reporting Limit.
Pace Analytical Services, Inc.
9800 lGncey Ave. Suite too
Huntersvlle, NC 28078
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unfounded data are displayed and have been used to calculate % recovery and RPO values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPO - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
\ Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
PaceAnalytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
PASI-R Pace Analytical Services - Raleigh
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 08/07/2015 05:14 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11

w wpaceuacvrr
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project Hameft 7127
Pace Project No.: 92260491
Lab ID
Sample ID
QC Batch Method
QC Batch
92260491001
HARNETT WTP 1
ASTM D2974-87
PMST/8206
92260491002
14ARNETT WTP 2
ASTM D2974-87
PMST/8206
92260491001
HARNETT WTP 1
SM9221C E (MPN) 503
R8I015323
92260491002
HARNETT WTP 2
SM9221C E (MPN) 503
R91015323
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 08/07/2015 05:14 PM without the written consent of Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
98001Gncey Ave. Suite too
Huntersville, NC 28078
[phone]
Analytical
AnaWcaf Method Batch
Page 9 of 11

CHAIN -OF -CUSTODY I Analytical Request Document
The Chal"r-CUS10*1s a LEA LDOCUMENT; pli relewnt(Iebs il'wsl be tpmpleiW aOt�lptey,
nnbM.<en

ttCl a Name: 1(`C;t4 � Tage2 of 21S for Internal Use Only
Ccurter (Clrclgj: Fed Ex UPS- USPS gD -
CustodySea' on CoOferISOX Present: y no Comment: Pace Other
es Seafslntact: 171• yes no
Packing Materlalr ❑ Bubble Wiap. bra Bags J`-'
Mete Thermometer Used: IR Gun •122065387TU of 1 N Other
1R Gun 06 371 we., Blue, None Q Samples on Ica, cool
Temp Correction Fa�P'� S Ing pracass has begun
clot: Ad,r,� �.F.__. 1r 1 �.
rersorr contacted:
Cemmenfs/RssolPtlon: D'ate/Rme:
SCURF/SRF
Review::
Nafe: whenever there .Il a discrepancy.afrecdng Nodh.CaroOn p nce
samples, a copy ofthis form w1Q he sent toths.North Camllne DERNR
GeNpcafforiance(re ou(oftiold;fncorrect preservaeve, out offelop.
fhcmmct containers)
new, uara RequfredT- Y f N
®It
# W=92260491
IIIIIIIIIIIIIIIIIIIIII
92260g91
Page 11

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Harnett CountyWTP WQ Permit Number: W00014885
WWTPName: Hamett County Regional WTP NPDESNumber: 00-076-84
Monitoring Period: From 10/01/15 To 12/31/15
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) -Please indicate level achieved and alternative performed:
Class A: Fecal Coliform Testing
Alt. I/A (time/temp) X Alt. 2B (Alk Treatment) _ Alt 3/C (Prior Testing)
Alt. 4/D (No Prior Test) _ Alt 5/Process to Further Reduce Pathogens _ Alt 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost _ Heat Drying _ Heat Treatment _ Thermophilic
Beta Ray _ Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density Alt (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting _ Aerobic Digestion
Anaerobic Digestion
If .,..-H—hlu s.. nun.oaf:vn oo.fnr.,.nd !!`Inee A nr f Inca Rl rmm.lwf 4hn fnllnmino mnnitnrino da4ae
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
'
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the
CFU
CFU/g
Coliform
power per gram
of total solids
CFU
CFU/g
1000 MPN per gram of
71.1
71.1
CFU/g
0
41yr
Grab
9222D
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
colifonn
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed: - N/A
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction) _
(40-day bench) _
(30-day bench) _ (Spec. 02 uptake)
Option/Alt 5
Option/Alt. 6
Option/Alt 7 Option/Alt. 8
(14-Day Aerobic) _
(AlkStabilization) _
(Drying —Stable) _ (Drying —Unstable)
Option/Alt 9
Option/Alt. 10
(Injection) _
(Incorporation) _
No vector attraction reduction alternatives were performed
STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement In 40 CFR 503.33/15A NCAC 02T.1107 have been met"
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met" (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
��--� Allan Rex O'Briant, WTP Superintendent
Pre r n titl o pn t)r Land Applier Name and Title (if applicable) (type or print)
lgoature of Prepared D Signature of Land Applier (if applicable) Date
•Preparer is defined in 40 CF art 503.9(r) and 15A NCA 2T.1102 (26)

Pace Analytical Services, Inc.
98001Gncey Ave. Suite 100
Huntersville, NC 28078
[phone]
November 11, 2015
Marshall Puryear
Synagro Technologies, Inc.
284 Boger Rd
Mocksville, NC 27028
RE: Project: Harnett 11/3
Pace Project No.: 92274492
Dear Marshall Puryear:
Enclosed are the analytical results for sample(s) received by the laboratory on November 03, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Endosures
REPORT OF LABORATORY ANALYSIS
This report shall not be repmduce4 except in full,
without the written consent of Pace Analytical Services, Inc.
Page 1 of 11

aceAnalytical o
tvwwpacelabsmm
I
CERTIFICATIONS
Project: Harnett 1113
Pace Project No.: 92274492
Paca Analytical Services, Inc.
9800 Kncey Ave. Suite too
Hunterswlle, NC 28078
[phone]
Raleigh Certification IDS
6701 Conference Drive, Raleigh, NC 27607
North Carolina Bioassay Certification #: 16
North Carolina Wastewater Certification #: 67
North Carolina Drinking Water Certification #: 37731
Charlotte Certification IDS
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Rodda/NELAP Certificafion #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification P. 84
North Carolina Feld Services Certification #: 6342
West Virginia Certification #: 357
North Carolina Wastewater Certification #: 12
VirginialVELAP Certification #: 460221
South Carolina Certification* 99006001
REPORT OF LABORATORY ANALYSIS
This report shall net be repreduced, except in full,
without the written consent of Pace AnalyBd Services, Inc.
Page 2 of 11

Pace Analytical Services, Inc.
9800 KGncey Ave. Suite 100
Huntersvdle, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project
Hamelt 1 V3
Pace Project No.:
92274492
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92274492001
HARNETT WTP1
SM 254OG
KDF
1
PASI-C
ASTM D2974-87
KDF
1
PASI-C
SM9221C E (MPN) 503
RC
1
PASI-R
92274492002
HARNETT WTP2
SM 254OG
KDF
1
PASI-C
ASTM 02974-87
KDF
1
PASI-C
SM9221C E (MPN) 503
RC
1
PASI-R
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc. Page 3 of 11

Pace Analytical Services, Inc.
9800 KincsyAve. Suite Soo
Hu terswlte, NC 28078
[phone]
ANALYTICAL RESULTS
Project Harnett 11/3
Pace Project No.: 92274492
Sample: HARNETT WfP1
Lab ID: 92274492001 Collected: 1110311513:15
Received: 11/03/15 14:54 Matrix: Solid
Results reported on a 'dry weight" basis and are adjusted for percent moisture, s nrpfe size and any dilutions.
Parameters
Results Units Report Limit DF
Prepared Analyzed CAS No. Qual
2540G Total Percent Solids
Analytical Method: SM 2540G
Total Solids
2.8 % 0.000010 1
11/04/15 18:51
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
. 97.2 % 0.10 1
11/0511512:30
92210E Fecal Colifonn, MPN RAL
Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN
72.6 MPN/g 0.018 1
11/0311515:39 1g
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/11/2015 09:53 AM without the written consent of Pace Analytical Services, Ina. Page 4 of 11

aceAnalyfical e
txmpaoyaCsmm
1
I
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
98001Gnary Ave. Suite 100
Huntersnlle, NC 28078
[phone]
Project Harnett 11/3
Pace Project No.: 92274492
Sample: HARNETTINTP2
Lab ID: 92274492002 Collected: 11103/1613:20
Received: 1V03/1514:54 Matrix: Solid
Results reported on a 'dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF
Prepared Analyzed CAS No. Qual
2540G Tonal Percent Solids
Analytical Method: SM 254OG
Total Solids
2.8 % 0.000010 1
11/04/15 18:51
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
97.2 % 0.10. 1
11/05/15 12:31
92210E Fecal Coliform, MPN RAL
Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN
71.7 MPN/g 0.018 1
11/03/15 15:39 tg
Date: 11/11/2015 09:53 AM
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page 5 of 11

2cemalytical ®
�1
f
Project Harnett 11/3
Pace Project No.: 92274492
QUALITY CONTROL DATA
Pace Analytical services, Inc.
I(Incey Ave. Suite 100
9800Huntersvi le, NC 8078
[phone]
QC Batch: PMST/8533
Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87
Analysis Description: Dry Weight(Percent Moisture
Associated Lab Samples: 92274492001,
92274492002
SAMPLE DUPLICATE: 1599248
92274345008 Dup
Parameter
Units Result Result RPD Qualifiers
Percent Moisture
% 85.4 85.4 0
�}
Restate presented on this page are In 0e units indicated by the "Units' column except where an alternate unit is presented to the fight of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 1111112015 09:53 AM
without the written consent of Pace Analytical Services, Ina.
Page 6 of 11

Pace Analytical Services, Inc.
980010ncey Ave. Suitet00
Hunternnile, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harnett 11/3
Pace Project No.: 92274492
QC Batch: RBIO/5665 Analysis Method: SM9221C E (MPN) 503
QC Batch Method: SM9221C E(MPN) 503 Analysis Description: 92210E Fecal.Coliform, MPN Solid
Associated Lab Samples: 92274492001, 92274492002
METHOD BLANK 1598235 Matrix: Solid
Associated Lab Samples: 92274492001, 92274492002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Colifonns, MPN MPN/g NO 0.018 1110311615:39
SAMPLE DUPLICATE: 1598236
92274492002 Dup
Parameter Units Result Result RPD Qualifiers
Fecal Coliforms, MPN MPN/g 71.7 71.7 0
Results presented on We page are In the units indimted bythe "omits" column except where an alternate unB is presented to the tight of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11111201509:53AM vAthaut the written consent at Pace Analytical services, Inc..
Page 7 of 11

5a'ceAnalytical"'
rwwrpaceradsram
QUALIFIERS
Pmject Harnett 1113
Pace Project No.: 92274492
DEFINITIONS
Pace Analytical Services, Inc.
980010ncey Ave. Suite 100
Huntersville, NC 28078
[phone]
DF - Di ution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL-Adjusted Method Detection Limit.
PQL- Practical Quantitation Limit.
RL- Reporting Limit
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azabenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data am displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Add preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
R' f Aseparate vial preserved to a pH of 4-5 is recommended In SW846 Chapter 4 for the analysis ofAcmlein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
PASI-R Pace AnalyticalServices- Raleigh
ANALYTE QUALIFIERS
1g This is a less than value
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 11/11/2015 09:53 AM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11

wwtpaoftlo n
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
980010ncey Ave. Suite 100
Huntersvile, NC 28078
VO4)875-9092
Project
Pace Project No.:
Hamett 11/3
92274492
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method Batch
92274492001
. HARNETT WTP1
SM 2540G
OEXT/38893
92274492002
HARNETT WTP2
SM 254OG
OEXT/38893
92274492001
HARNETT WTPi
ASTM D2974-87
PMST/8533
92274492002
HARNETTWTP2
ASTM D2974-87
PMST/8533
92274492001
HARNETT WTP1
SM9221C E (MPN) 503
RBIO/5665
92274492002
HARNETT WTP2
SM9221C E (MPN) 503
RBI0/5665
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/1112015 09:63 AM without the written consent of PaceAnalocal Services, Inc.. Page 9 of 11

I
%�`'',.°�"� CHAIN -OF -CUSTODY % Analytical. Request Document
i`3CE41Yd lQBl I TheChaioof-CmtddyIsaLEGAL DOCUMENT. All Wava OchsmValbbcompleteda rdl¢ly.
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bocurrjentName: Sample Copditlon.Upon
Docume
.Revised; May15.2U15
-aseAnalytifxl�
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Page tofr
DocumentNo.:'-
Is
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F-RAC-CS UOi. rev.03
Pace
afef h Quali Ofgce
Page 2
Client (Name:
f 2 is for-Intemal Use Only.
`
Courler(Circie): Fed Ex UPS USPS Client Commercial Pace Other
Custody Seal on Cooler/Box present yes no Seals Inlacir yes 0 no
_
Packing Material-. Bubble Wrap Bub-te BagsNone Other
Used, lRGun 5122865387T
-
`Clrcle.Thermometer
a flce:. Wet Blue None QSamples on
has begun-.—
IRGurifia
e65374
Temp Correction Factor: Add/ b1m � � G Dataan
CorrecteddCeolar Temp: 3. C Bfologlcal Tissue is Frozen: Yea No1.wA °
Initlafsofp rson=Mining
t !p a at(en
-[J
Temp be freezing
!J chec
•
should above to 6-c
Comments:
Cfia[nofCusfodyPresent:
Yes ONO OwA
i..
CharnofCustod Filled Out:
es ONO O�
2
Chain ofCustad Relin ulshed:'
Yea ON.ONIA
3.
Sam Ier Name&'Signature on COC:
Yes ONo OwA
4_
Sam ras Arrivedwithin Hold Time:
vas pNo OwA
S.
Short Hold Time Anal ls(<72hr:
Yes ❑No OeuA
6.- -
RushrTum Around Time Request=13yes
ON/A
7.
Sufficient Volume:
OWA
S.
Correct Containers Used.OwA
9.
-Pace Containers Used:DING
ONIA
Containers Intact:
OWA
10.
Mitered volume received for Dissolved.wA
11.
Sample Labels match COC:
has ONO ON/A
12.
-Includes dateltimello/Anal sis Malft .
All containers heeding presmadon have been checked ,../
yiYos ON- ON/A
13.
Allcontainers -needing preservation are found
tobein [{Yes
compirancewgh EPA.reeommendauem.
ONO OwA
!O//
rs: pumm.. VOA coldomn. TOC. O&G, WI-0RO(Water) es: 17Na
Samples checked for dechlorinatfont
IJY.s ONo ❑NIA
14.
Heads ace in VOA Mats >6mm):
Oyce ONO. IINIA
15,
Trip BlankPresenE
Ores ONa
16.
Trip Blank Custody Seals Present
/NfA
DYea ONo ,OWA
_
Pace Trip Blank Lotif ifpurchased):
Client Notification/ Resotuflon:
Rerd Data Req
Ired7 Y 1 N
Person Contacted:
DateMme:
.Commentsf Resolution:
- -
SCURF/SRF
Date- tf WQ# : 92274492
S
Revlew::
`h
Note: Whenever there Is dlscrepancy affectingNadh Carolina wmpirance II II�.'I I I I�II�
samples, a copy of this form.vdil be sent tolhe
NorlflCarolina DEHNR III I'll
__._....... r. ............. ..
r Incorrect corltalners)
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