WQ0014868_2017 Annual Report_20180227

o� Resources, L1c.
February 27, 2018
DENR/Water Quality Section
Non -Discharge Compliance Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2017 Annual Report — Smithfield Packing Co.
Treatment and Land Application of Residuals
Permit No. WQ0014868
Dear Sir or Madam:
Enclosed are three copies of the 2017 Annual Report for the above referenced land
application permit.
During 2017 EMA Resources, Inc. land applied 193.1 dry tons of wastewater residuals to
143.4 acres of private farmland. Please contact Brent Collins - Director of Technical
Services if you have any further questions regarding this report.
Sincere
lad
Brent Collins
Director of Technical Services
[e-mail]
Phone [phone] — Fax [phone]
755 Yadkinville Road — Mocksville, NC 27028

0
Smithfield Packing Co., Inc.
Tar Heel Facility
2017 Annual Report
Residuals Land Application
Permit No. WQ0014868
Prepared By:
EMA Resources, Inc.
{
Phone[phone]*1441 — Fax[phone]
{ 755 Yadkinville Rd ,.. Mocksville, NC 27028
�f

ANN UAL LAND APPLICATION CERTIFICATION FORM
C
WQ Permit#: WQ0014868 County: Bladen Year:
Facility Name (as shown on permit): Smithfield Fresh Meats Cort
Land Application Operator:
Resources
Phone:
Land application of residuals as allowed by the permit occurred during the past calendar year?
El Yes ❑ No - If No, slip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summarv:
2017
r,
Total number of application fields in thepermit: 37
L
Total number of fields utilized for land application during the year: 9
Total amount of dry tons applied during the year for all application sites: 193.1
Total number of acres utilizes for land application during the year: 143.4
Pod R _ A......-1 n..-..______ o._.___ __�-
_ - oavaauce oanaCWCLLa" ,
Facility was compliant during calendar year 2017 with all conditions of the land application permit
r� (including but not limited to items 1-13 below) issued by the Division of Water Quality, El Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
_i 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T 1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .I I05(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T. I 111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and iemediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing.residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties, for submittin false information, including the
6 possibility of fines and imprisonment for knowing violations." JJ
Donovan Owens - General Manager
ti Perm' a Name and Ti (type or print) Signature of Pennittee Date
2/6/2018
i Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
DENR FORM ACF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0014868 Laboratory: 1) Waypoint Analytical
Facility Name: Smithfield Fresh Meats Corp. 2)
Residual Source WQ # or NCO078344 3)
NPDES #: 4)
WWTP Name: Tarheel Plant WWTP 5)
Residual Analvsis Data
Parameter
(mg/kg)
Ceiling
Conc.
Limit
Sample or Com osite Date
North
4/24/17
I North
6/15/17
Average
South
10/25/17
Percent Solids (%)
NA
2.2
3.31
2.755
0.43
Arsenic
75
3
3
3
3
Cadmium
85
2
2
2
2
Copper
4,300
1220
1040
1130
897
Chromium
NA
43.1
52.4
47.8
32.7
Lead
840
11
9.91
10.46
6.64
Mercury
57
0.4
0.4
0.4
0.4
Molybdenum
75
14.1
13.6
13.9
7.86
Nickel
420
31.6
34.6
33.1
17.8
Selenium
100
5.58
5
5.3
5
Zinc
7,500
2950
2620
2785
1700
Total Phosphorus
NA
19200
18000
18600
9820
TKN
NA
95500
71400
83450
95500
Ammonia -Nitrogen
NA
24900
15100
20000
63600
Nitrate and Nitrite
NA
2.44
2.26
2.35
1.94
'For surface disposal facilities the ceiling concentration limits listed in this forth are not applicable. Reference the individual permit for metals limits. -
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submittin false information, including the possibility of fines and imprisonment for knowing violations."
k 2 *Ig
Signature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

---'
ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: - WQ0014868 Laboratory: 1) Waypoint Analytical
Facility Name: Smithfield Fresh Meats Corp. 2)
Residual Source NCO078344 3)
NPDES # or WQ#: 4)
WWTP Name: Tarheel Plant WWTP
Residual Analvsis Data
5)
Parameter
'
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM RSSF - 8 (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
_ Facility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual): 50.78
,Permit #: WQ0014868 Cation Exchange Capacity (non 503 only): 6.2
'-Operator: Steve Dunham Owner: Steve Dunham Predominant Soil Series: LaB
-Acres Used: 21.6 Acres Permitted: 21.6 Site #: SF03 Field #: I
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
1
2j
3
4,
5
6
7
8
9
10 -
11
12
Com-
Avg
10/25/17
posite
I Date
%Solids
2.755
0.43
Arsenic
3
3
Cadmium
2
2
Copper
1130
897
�hromiu
47.75
32.7
Lead
10.455
6.64
;Mercury
0.4
0.4
Molyb-
27.7
7.86
1
denum
Nickel
33.1
17.8
Selenium
5.29
5
j
- Zinc
2785
1700
Total
Phos-
18600
9820
horns
;annual Heavy Metal Field Loadings
(Calculated in lbs/acre):
Total
1
2j
3j
4
5
6
7
8
9
10
11
12
I DT/Ac./
App.
Event
2.18
0.17
y
_ Arsenic
0.013
0.001
0.000
0.000
0.000
0.000
0.000
0:000
6.000
0.000
0.000
0.000
0.014
Cadmium
0.009
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000-
0:000
0.000
0.009
Copper
4.922
0.310 .1
0.000
0.000
_ 0.000
0.000
0.000i
0.000
0.000
0.000
0.000
0.000
5.233
f�hromi
0.208
0.011
0.000
0.000
0.000
0.600
0.000
0.000.
0.000-
0.000
" 0.000
0.000
0.219
Lead
0.046
0.002
0.000
0.000
0.000
0.000
0.000
.0.000
0.000
0.000
0.000
0.000
0.048
ercury
0.002
0:000
0.000
0.000
0.000,
0.000
0.0ft
. 0.000
0.000
0.000
0.000
0.000
0.002
0.121
0.003
0.000
0.000
0.000
0.000
0.000
0.000
. 0.000 .
0.000
0.000
0.000
0.123
enyb-
um
(Nickel
-
0.144
0.006
0.000
0.000
0.000
.0.000.
0.000'
0.000
0.000
0.000
0.000
0.000
0.150
_lenium
0.023
0.002
0.000 .
0.000 .
0.000
0.000
, 0.000
0.000
0.000
0.000
0.000-
0.000
0.025
Zinc
12.131
0.588
0.000
,0.000'
0.000
0.000
0.000!
0.000
0.000
0.000
0.000
0.000
12.720
Total
Phos-
81.022
3.398
0.000
0.000
. 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
84.419
horns
-11 certily, under penalty of law, that this document was prepared under my direction.or supervision in accordance
_with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
I , � �`� 2/6/2018
Signature of Land Applier Date
it
DENR FORM MFLSF (1212006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Smithfield Farmland Corp.
Land Owner: Steve Dunham
Operator: Steve Dunham
WQ Permit #: WQ0014868 Field #: 1
Annual Dry Tons Applied: 50.78 Site #: SF03
Predominant Soil Series:
Crop I Name: Bermuda -Pasture Crop 1 Max. PAN:
147
Acres Utilized:
Acres Permitted:
LaB Cation Exchange Capacity (non 503):
Crop 2 Name: Crop 2 Max. PAN:
21.6
21.6
6.2
..
° 5
° c
°
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
'Acre
(DryTons/Ao)
Residual Sources
PDES #, W #,
(N Q
FerG, Animal
Waste, etc)
$0il
Cond.
(Dry'
Moist)
Precip.
Past 24
firs.
inches
D
b
a ,ew
o
;v »
m �,
a �'
5
N.
w '°
t �'
+
TKN
mg/kg
Z I
dr
w.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(]bs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop.2
5/24
84500
2.755
0.449 '
Tarheel WWTP
Dry
<5"
S
0.5
0.2
83450
20000
2.35
20.307
NA
Bennuda
5/30
97500
2.755
0.519
Tarheel WWTP
Dry
<•5"
S
0.5
0.2
83450
20000
2.35
23.535
NA
Bermuda
5/31
195000
2.755
1.037
Tarheel WWTP
I Dry
<•5"
S
0.5
0.2
83450
20000
2.35
47.070
NA
Bermuda
611
32500
2.755
0.173
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
83450
20000
2.35
7.845
NA
Bermuda
10/24
65000
0.43
0.054
Tarheel WWTP
Dry
<•5"
S
0.5
0.2
95500
63600
1.94
4.121
NA
Bermuda
10/25
143000
0.43
0.119
Tarheel WWTP
Dry
<•5"
S
0.5
0.2
95500
63600
1.94
9.065
NA
Bermuda
0.000,
0.000
0:000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
-0.000._
--
----
-0:000--
-0.000--
0:000
0.000
0.000
-
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
.
TOTALS:
- 0
617500
::::: ; ::
As
Cd
Cu
Cr
Pb
H
Mo
Ni
Se
Zn -
P
112.034
.0.000
Lime A lied.
Annuallbs/acre
0.014
0.009
5.233
0.219:
0.048
0.002
0.123
0.150
0.025
12.720
84.419
%> ;::
Date
Ibs/ac
Prior Years Cumulative Ibs/ac
0.169
0.183
0.075
0.084
9
33.242
38.475
250
1.951
2.170
0.548
0.596
1000
0.019
0.021
1.061
1.184.:
3.336
3.486
250
0.232
0.257
150.594
163.314
500
: :::> ':::: :: >::: > >
:::::::::::::::>::::::;::i:::>::::::;::: ::
:::::::.:.....................
Current Cumulative lbs/ac
Permitted C. P. L. R****
PAN Limit Ist/2nd Crop
14Permit 7
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/6/2018 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (1212006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
II
L` Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual): 3.03
lermit #: WQ0014868 Cation Exchange Capacity (non 503 only): 4.1
Jperator: Steve Dunham Owner: Steve Dunham Predominant Soil Series: Ce
Acres Used: 13.3 Acres Permitted: 13.3 Site #: SF03 Field #: 2
?.esidual Analysis Data (He4a Metals and Total Phosphorus use mgLkg, % Solids use Raw Percent #):
0
m
m
INNEIIIII
.,,
©�
,
I
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"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
am aware that there are significant penalties for submitting false information, including the possibility of fines and
Imprisonment for knowing violations".
Signature of Land Applier
2/6/2018
Date
L'
DENR FORM MFLSF (1212006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Smithfield Farmland Corp. WQ Permit#: WQ0014868 Field #:
Land Owner: Steve Dunham Annual Dry Tons Applied: 3.03 " Site #:
Operator: Steve Dunham Predominant Soil Series: Ce
Crop I Name: Bermuda -Pasture Crop I Max. PAN: 168 Crop 2 Name:
2 Acres Utilized: 13.3
SF03 Acres Permitted: 13.3
Cation Exchange Capacity (non 503): 4.1
Crop 2 Max. PAN:
o
A
Volume applied
(enter one) Solids/
Liquid
Cu. Yds .Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert.,Animal
W��= etc)
Soil
Cond.
(Dry,
Wet,
Moist)
Precip•
Past 24
ilrs.
inches
� ,o
�,
o� c
°ten
o
} ^
z „
�.K,:
w
TKN
mgikg
95500
z 9
x
?
❑ w
mglkg
63600
Nitrate
and
Nitrite
mg/kg
1.94
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop I
Crop 2
Crop 1
Crop.2
11/1
169000
0.43
0.228,
Tarheel WWTP
Dry
<•5"
S
0.5
0.2
17.399
NA
Bermuda
0.000
0.000
0.000
0.000 .
0.000
0.000
0.1000
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0:000
0.000'
0.000
0.000:
0.000
0.000 "
0.00.0
0.000
0.000
0.000
0.000
A000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp (attach FORM FSF supp
to this form):
.........
..........
TorA1s:
' " 0
169000
::: :
As
Cd
Cu
Cr
Pb
I Hg
I Me
I Ni
I Se
I Zn
P
17.399
0:000
Lime Applied
Annual lbs/acre
0.001
0.001'
0.409
0.015
. 0.003.]
0.000
0.004
1 0.008
1 0.002
0.775
4.478...........
: ;:::y::::'::::::::`:::
::
;;`.................•.....::
..........................
bate
lbslac
Prior Years Cumulative lbs/ac
0.174 -
0.062
37.41
1.65
0.648
0.019
1.037
3.743
0.216
152.736
2000
Current Cumulative lbs/ae
0.175
0.063
37.819
1.665
" 0.651
0.019
1.041
3.751
0.218
153.511
Permitted C. P. L. R****
9
250
1000
250
500
Pehnit PAN Limit lst(2nd Cro P
168
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/6/2018 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (1212006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
'ermit #:
-Operator:
keres Used:
Smithfield Farmland Corp. Total Dry Tons Applied (Annual): 4.43
WQ0014868 Cation Exchange Capacity (non 503 only): 2.9
Steve Dunham Owner: Steve Dunham Predominant Soil Series: Cc
21.3 Acres Permitted: 21.3 Site #: SF03 Field #: 3
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
i
on,©
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o
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0
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m
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1111
:,,,�
r 'I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
-- with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
— am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
�!Z�zz 2/6/2018
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL. LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Smithfield Farmland Corp. WQ Permit #: W00014868 Field #: 3 Acres Utilized: 213
Land Owner: Steve Dunham Annual Dry Tons Applied: 4A3 - Site #: SF03 Acres Permitted: 21.3
Operator: Steve Dunham Predominant Soil Series: Ce Cation Exchange Capacity (non 503): 2.9
Crop 1 Name: Bermuda -Pasture Crop 1 Max. PAN: 168 Crop 2 Name: Crop 2 Max. PAN:
0.
'�
c, c
i
La
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
o/a
Solids
Volume
Applied per
Acre
(Dry7ons/Ac)
Residual Sources
pDES N, W #
Q
Fero, Animal
Waste, etc)
Sod
Cond
(Dry,
e '
Moist)
Pcecip.
Past 24'd
Iirs.
inches
,o
a 41w^_,•
µme^
o
»
c
+ m
$
��•
,
m
: ^
=
T[CN
mg/kg
95500
z �
q
w° o
5 Z.
mg/kg
63600
Nitrate
and
Nitrite
mg/kg
1.94
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop I
Crop 2
11/1
52000
0.43
0.044
Tarheel WWTP
Dry
<•5"
S
0.5
0.2
3.343.
NA
Bermuda
11/2
195000
0.43
0.164
Tarheel WWTP
Dry
<•5"
S
0.5
0.2
95500
63600
1.94
12.536
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000.
0.000
0.000
0.000
0.000
0.000.
0.000
0.000
.0.600
0.000
0.000
0.000.
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
QD
TOTALS:
0
247000
::::::::
As
Cd
Cu
Cr
Pb
A
Mo
Ni
Se'
Zn
P
15.879
0.000
Annual lbs/acre
0.001
0.001
- 0.373
0.014
0.003
0.000
0.003
0.007
0.002
0.707
4.085.;:;;:;:;;Prior
::>;:>::.`;;:; :>::::::>::::;::: :':
:::::::`;i::::::::::::::::::
;.
Years Cumulative lbs/ac
0.142
0.07
29.847
1.201
0.488
0.015
0.817
2.842
0.171
122.375
Current Cumulative lbs/ac
0.143
0.071
30.220
1.215
0.491
0.015
0.820
2.849
0.173
123.082
Permitted C. P. L. R.****
9
250
1000
250
500
Permit PAN Limit lst/2nd Cro P
168
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/6/2018 "Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date
*"Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
i` Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
'ermit #:
Operator:
Icres Used:
Smithfield Farmland Corp. Total Dry Tons Applied (Annual):
W00014868 Cation Exchange Capacity (non 503 only):
Steve Dunham Owner: Steve Dunham Predominant Soil Series:
19 Acres Permitted: 19 Site #: SF03 Field #:
4.43
4.9
Wh
2esidual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
ample or
1
2
3
4
5 -
6
7
8
9'
10
11
12
Com-
10/25/17
posite
Date
Solids
OA3
Arsenic
3
admium
2Copper
897
hromi
32.7
Lead
1phorus
6.64
Mercury
0.4
Molyb-
7 86
denum
Nickel
17.8
elenium
5
Zinc
1700
Total
Phos-
9820
annual Heavy Metal Field Loadings
(Calculated in lbs/acre):
Ill
2j
3j
4
5j
6j
7j
8
9j
10
11
12
ITotal
_DT/AcJ
o
App.
m
Event
0.23
_Arsenic
O.00 ,;
0.000,:.
0:000 ,
-6.000'
A 000 ,
A 00 ,
-'- ;000
0:000.,
.-0:000'<
0 000'
; 0 000
;admium
0:001
0.000'.;
0 000
°0.000 ;
20:000,,
`,0 000 .
.'600
0i000,
. 0 000`
0.000,:
' 0 OOQ
°, 0 000
001"
Copper
0:418
. 0 000;°
, 0 006
,t-0.000
: 0 000
Of000.,,
0.000
r'0A00.
_ 0.000
0:000,4
; 0 000 :.'0.000
=0 438:
- ^hromi
0:O15z
0.000
0 000
y'0.000;
�� 0 000,
"-O 000_
0 000';
'0.000
0:000:_
000'.a
000
'IO 000 '
`.'Oi0,15'�
; -
,a
,0
,0
Lead
0.003".
,6J000
°, 0 000_
`d0.000=
'0 000
4.0f000 ..
;0 000'-
' 0:000.
.0.000`
=0.000 ,
w.0.000`�
=0.000 ,
r 0 003 ;
Mercury
`0:000
0.000;
0 000 >
y'0:000,'
.-0 000
"-Ot000
"'OA00
_'AO .
0 000'i
0 000;°'
:t 0.000.:
`0 0001.
'`0:000J°
-Molyb-
0 004.
0 000'
0 000
0 000
- '0 000
0 000
O'000
0 000
0 OOOf,
O 000
0 000
`0 000
r
=0;004':
denum
,
Nickel
0.008
,0 000<.`
` 0.000:
<0 000
i:;0 000
J6.000
: 0.000
0.000
O'.000.;
0.000.
'° 0.000:
; -0 000
;Oi008
-Selenium
:0.002'
3 O.000','
0 000
0 000 `
._'0. 000 ,
s0;000
06000
.:O:OQO,
, 0.000.
0 00,0 r
:�10.000-;
. 0 000
:; 0,:002 ,
Zinc
0.792s
,r0.006
0.000
'0.000.
`. 0 000 ,
;0 000
:Op000 .
,'•0:000,
0:000:;
0.000;:'
0 000:
t 0.000'
0 792`.
Total
�-
a
,
;,rv,-
Phos-
4 576,'
0 000 '
0 000
�0 000
0 000
0 000
0.000
O'000
0 000=,
0 0001J
t 0 000` _
000
:�'0 4:576
horus
'I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
-with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
zfz 2/6/2018
Signature of Land Applier Date
i
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN. A BLANK OR BOX WHEN NOT APPLICABLE. 1
Facility Name: Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 4 Acres Utilized: 19
Land Owner: Steve Dunham Annual Dry Tons Applied: 4.43 Site #: SF03 Acres Permitted: 19
Operator: Steve Dunham Predominant Soil Series: Wh Cation Exchange Capacity (non 503): 4.9
Cron 1 Name: Wheat Crop 1 Max. PAN: 121 Crop 2 Name: Crop 2 Max. PAN:
Volume applied
(enter one)
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
' Acre
(DryronstAc)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)Moist)
Soil
Cord.
Wei�•
Precip.
Past 24.
inches
Y
K by
�
o
_
m
*w�•
5mg/kg
TICN
95500
z
o
w o
mglkg
63600
Nitrate
and
Nitrite
mglkg
1.94
PAN Applied
(ibs/acre)
Name of Crop Type
ReceivingResidual
Application
Crop I
Crop 2
Crop I
Crop 2
13000
0.43
0.012
Tarheel WWTP
Dry
<•5"
S
0.5
0.2
0.937
- NA
Bermuda
234000
0.43
0.221.
Tarheel WWTP
Dry
<•5"
S
0.5
0.2
95500
63600
1.94
16.864
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
[ZAnnual
0.000
0.000
0.000
0.000
0.000
6.000
0.000
0.000
0,000
0.000
0.000
0.0ti0
0:000
0.000
0.000
0.000
0.000
0.000
0000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM_
FSF supp
tothis form):
....
..........
o
za7000::....
A
Cd
Cu
Cr
Pb
H
Mo
Ni
Se
Zn
P-17.801
0.000
Lime A lied
lbs/acre
0.001:_ '
. 0.001 '
0.418
0.015
0.003
0.000
0.004
0.008
0.002
0.792
4.576
Date
Ibs/ac
Prior Years Cumulativelbs/ac
0.0993
0.0485
15.9461
1.5398
0.2884
0.0104
0.6275
1.8858
0.1254
85.I038
Current Cumulative lbs/ac
0.101
0.049
16.364
I.555
0.291
1 0.011
0.631
1-.894
0.128
85.896
Permitted C. P. L. R.****
9
250
1000
250
500
Permit it PAN Limit Is t/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed_to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/6/2018 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
Signature of Land Applier Date
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R:: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
µ Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
'ermit #:
Operator:
Acres Used:
Smithfield Farmland Corp. Total Dry Tons Applied (Annual): 1.86.
W00014868 Cation Exchange Capacity (non 503 only): 3.9
Steve Dunham Owner: Steve Dunham Predominant Soil Series: LaB
Acres Permitted:
Site #: SF03 Field #:
'tesidual Analvsis Data (Heavy Metals and Total Phosphorus use mg/kg, % SoGds use Raw Percent #):
ID
e
e e►
► ee►
► ►ee
a ►►e
► ►►►
► ee►
► e►e
► ee►
a e►►
a eee
► ►►►
►eee
► ►►
. �
e e►
►eee
► e►e
a ►►►
► ►►►
► e►►
a eee
a eee
a e►e
►eee
► ►e►
a eee
a ►►
...
► �
► ee►
► ►ee
►eee
► ►ee
a e►e
a ►►►
eee►
► 11e
► 11e
► ►►►
a eee
..
e ►
e ►ee
a eee
a eee
a ►ee
a e►e
a ►ee
a eee
► ►ee
► ee►
a eee
a eee
e e
e ►e
a ►e►
eee►
eee►
a eee
a ►►e
a eee
a ►ee
► 11►
► ►e►
a eee
► ee►
eee
e ►ee
► e►e
a oee
a eo►
a eee
a oee
a eee
► eeo
a eee
► ►e►
a eee
► ►ee
► ►e►
•
eee-
► ►ee
a e►e
a e►e
eee►
a eee
► ►e►
► ►ee
► ee►
a ►e►
a e►e
► ►ee
eee- '
e e►:
►eee
► ►ee
a ►►e
eee►
►eee
eee►
a eee
eee►
e e►►
e e►►
► e►e
e e►:
► e►
eee►
► ►►e
a e►e
► ►ee
a e►►
a e►e
a e►►
eee►
a e►e
eee►
a e►e
a e►
► �
eee►
a eee
a eee
► ►►e
a e►e
a eee
a eee
a eee
a ►ee
►eee
a e►e
e
�
e ►►e
eee►
oee►
a ►ee
a eee
► ►ee
► ►ee
eee►
eee►
a eee
► ►e►
...
-'I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
I
2/6/2018
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 5 Acres Utilized:
Steve Dunham Annual Dry Tons Applied: 1.86 Site #: SF03 Acres Permitted:
Steve Dunham
Crop 1 Name: Bermuda -Hay
Predominant Soil Series: LaB
Crop 1 Max. PAN: 196 Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
8
8
3.9
=
m
Ca
Volume applied
(enter one) Solids/
Liquid
Cu Yds Gallons
%
Solids
Volume
Applied per
Acre
(DryTons Ac)
Residual Sources
(NPDGS #, W #,
Fert., Animal
Waste, etc)
Sod
Cond.
dry'
Moist)
Precip.
Past 24
Hrs.
inches
Y
� 9
" ti
c a:
; °
o
} »
a
5'
=°
,�, -�,'
* tF
TKN
mg/kg
Z
o g
a '-�•
mg/kg
Nitrate
and
Nitrite
mpg
PAN Applied
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
10131
104000
0.43
-. 0.233
Tarheel WWTP
Dry
<,5"
S
0.5
0.2
104625
39947.5
2
15.343
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000.
0.000
0.000
0.000
0.000
. 0.000
0.000.
0.000
- 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000.
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
.........
..........
TOTALS:
- 01
As
Cd
I Cu
Cr
I Pb
Hg
Mo
Ni
I Se
Zn
P
15.343
0.000
Lime Applied
Annual lbs/acre
0.001
0.001
0.418
0.015
0.003
0.000
0.004
0.008
0.002 °
0.792
4:576
::
Date
lbs/ac
Prior Years Cumulative Ibs/ac
0.098
0.051
18.988
0.969
0.283
0.011
0.577
1.924
0.127
85.925
2000
Current Cumulative lbs/ac
0.099
' 0.052
19.406
0.984
0.286
0.01 t
0.581
1.932
0.129
86.717
Permitted C. P. L. R.****
9
250
1000
250
500
2 C ro
P ermit PAN Limit 1st/ nd P
196
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
Lv� - *Application Method: S - Surface, IN - Injection, INC - Incorporation
2/6/2018 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual): 45.82
'ermit #: W00014868 Cation Exchange Capacity (non 503 only): 16.2
Operator: Steve Dunham Owner: JW Burney Predominant Soil Series: WmB
lcres Used: 19.3 Acres Permitted: 19.3 Site #: SF07 Field #: 6
tesldual Analysis Data (Heavy Metals and total rnospnorus use mg/Kg,
"/o aonus
use
xaw rercent s):
Sample or
Com-
posite
Date
11
Avg
2 '
10/25/17
3j
4
5
6
7
8
9j
10
IIJ
12
Yo Solids
2.755
0.43
Arsenic
3
3
�admium
2
2
Copper
1130
897
Chromi
47.75
32.7
Lead
10.455
6.64
Mercury
0.4
0.4
I Molyb-
denum
27.7
7.86
Nickel
33.1
17.8
Selenium
5.29
5
Zinc
2785
1700
Total
IPhos-
horus
18600
9820
annual Heavy Metal Field Loadings
(Calculated in Ibs/acre):
ITotal
DT/AcJ
App.
-' Event
1
2.21
_2j
0.17
3j
4j
5
6j
7j
8
9j
LOJ
11
12
_ Arsenic
0:013
0.001
0.000
0.000
0.000
0.000
0.000
0.006
0.000
0.000
.0.000
0.000-
0.014
Cadmium
0.009
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.009
Copper
4.983
0.303
1 0.000
0.000 ,
0.000
0.000
0.000
0.000
0.000
0.000
0:000
0.000
5.286.
^hromi
0.211
OAll
0.000
0.000
0.000'
0.000
0.000
0.000
0.000
0.000
0.000
0.000'
0.222
Lead
0.046
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.048
Mercuy
0.002
0.000,
0.000.
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000,
0.002,
,. Molyb-
denum
0.122
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.125
Nickel
0.146
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.152
,Selenium
0.023
0.002
0.000
0.000
0.000
0000
0.000
0.000
0.000
0.000
0'.000
0.000
025
0]83
Zinc
12.282
0.575
0.000
0.000.
0.000
0.000
0.000
0.000 `
0.000
0.000
0.000
0.000
�. Total
Phos-
' 82.026
3.319
-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
horns
,-,'I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance ,
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
[ am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/6/2018
Date
Signature of Land Applier
is
i,
DENR FORM MFLSF (12/2006)

J
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 6 Acres Utilized:
Land Owner: JW Burney Annual Dry Tons Applied: 45.82 Site #: SF07 Acres Permitted:
Operator: Steve Dunham Predominant Soil Series: WmB Cation Exchange Capacity (non 503):
Crop 1 Name: Bermuda -Pasture Crop 1 Max. PAN: 210 Crop 2 Name: Crop 2 Max. PAN:
19.3
19.3
16.2
o r�
°3 0
m
q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(DryTonslAc)
Residual Sources
(NPDES #, WQk,
Fer., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
Past 24
Hrs.
inches.
9
n v
oa m
.0
>
0
;v m
+ ^
>
w
N
w
c
TKN
mg/kg
z
o B
a
mglkg
Nitrate
and
Nitrite
mgtkg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop I
Crop 2
Crop I
Crop 2
5119
149500
2.755
0.890
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
83450
20000
2.35
40.388
NA
Bermuda
5/20
182000
2.755
1.083
Tarheel WWTP
Dry
<,5.
S
0.5
0.2
83450
20000
2.35
49.168.
NA
Bermuda
5/21
39000
2.755
1 0.232
Tarheel WWTP
Dry
<,5"
S
0.5
1 0.2
83450
20000
2.35
10.536
NA
Bermuda
10/27
182000
0.43
0.169
TarheclWWTP
Dry
<•5"
S
0.5
0.2
95500
63600
1.94
12.912
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
6.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
NTOTALSf,
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp (attach FORM FSF supp
to this form):
`
01
552500
::::::::;:::
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
I P
113.0041
0.000
Lime Applied
Annual lbs/acre
0.014
0.009
5.286
0.222
0.048
0.002
0.125 -
0.152
-0.025
12.856
85.345 :: ;:;
::: ;: ;:;:.:::: ::::::::;:
::::::::..... :::::... .....
Date
Ibs/ac
Prior Years Cumulative (bs/ac
0.247
0.242
105.018
6.176
1.783
0.027
1.552
14.846
0.331
366.291
Current Cumulative Ibs/ac
0.261
0.251
110.304
6.398
1.83 t
0.029
1.G77
14.998
0.356
379.147
Permitted C.P. L. R.****
9'
250
1000
250
500
Perm it PAN Limit Ist/2nd CroP
210
"I certify, under penalty of taw, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/6/2018 **Volatilization Rate: Surface- 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R: Cumulative Pollutant Loading Rate
DENR FORM FSF (1212006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual): 27.59
'ermit #: W00014868 Cation Exchange Capacity (non 503 only): 12.7
Operator: Steve Dunham Owner: JW Burney Predominant Soil Series: AaA '
t-cres Used: 12.1 Acres Permitted: 12.1 Site #: SF07 Field #: 8
_Xesluuat analysts
iiata trteavy ivietais ana it otat rnospnorus use mgixg,
ro bons use tcaw rercent 11:):
Sample or
_ '
Com-
posite
Date
1
Avg
2
10/25/17
3
4
5
a
7
8
9
10
11
12
I%u Solids
2.755
0.43
Arsenic'
3
3
Cadmium
2
2
Copper
1130
897
lChromiurn
47.75
32.7
Lead
10.455
6.64
'Mercury
0.4
0.4
IMolyb-
- denum
27.7
7.86
Nickel
33.1
17.8
Selenium
5.29
5
Zinc
2785
1700
Total
Phos-
-, hours
18600
9820
knnual
Heavy Metal Field Loadings
(Calculated in lbs/acre):
ITotal
DT/Ac./
. App.
- _, Event
11
2.22
2j
0.06
3
_4j
5j
6j
7j
a
9
10
11
12
o
m
nic
0.013
0.000
0.000.
0.000
0.000
0.000
0.000
0.000
0.000
.0.000-
0.000
0.000
0.014
(atmiurn
0.009.
0.000
0.000
0.000
0.000.
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.009'
per
5.022:
0.104
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.126
romi
0.212
0.004
0.000
: 0.000
0.000
0.000
0.000
0.000
.0.000
0.000--
' 0.000
0.000
0.216
i Lead
0.046
0.001
0.000
0.900
0.000
0.000
. 0.000
0.000
0.000
0.000
0.000
0.000
0.047
Mercury
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.'000.
0.000
0.000
0.000
0.000
0.002
Molyb-
demur
0.123
0.001
0.000
0.006
0.000
0.000
0.000
6.000'.
0.000
0.000
0.000
0.000.
0.124
Nickel
0.147
0.002.
0.000
.0.000
0.000
0.000
0.000
0.000
0.000
0.000
0:000
0.000.
0.149
Selenium
0.024
0.001
1 0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.024
Zinc
12.377'
0.197
0.000
0.000
0.000
0.000
0:000
0.000
0.000
0.000.1
0.000
1 0.000
1 12.574
Total
Phos-
horus
82.658
1.139
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0:000
0.000
83.798
-''I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
-with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
� am aware that there are significant penalties for submitting false information, including the possibility of fines and
-imprisonment for knowing violations".
2/6/2018
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

l_-,
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 8 Acres Utilized: 12.1
Land Owner: JW Barney Annual Dry Tons Applied: 27.59 - Site #: SF07 Acres Permitted: 12.1
Operator: Steve Dunham Predominant Soil Series: AaA Cation Exchange Capacity (non 503): 12.7
Crop 1 Name: Bermuda -Pasture Crop I Max. PAN: 207 Crop 2 Name: Crop 2 Max. PAN:
o
q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
APPlied per
Acre
(DryTonslAc)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry'
Wet,
Moist)
Precip.
Past 24
Hrs.
inches
Y
3'v
m
o -"w,
; 6'
❑
o
,n °:
m _,
: �'
`_
eZ.
�.
ti
: N•
.' Pi
TKN
mg/kg
z
x
o
5
❑ °
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(Ibs(acre)'
Name of Crop Type
Receiving Residual
g
Application
PP
Crop I
Crop 2
Crop 1
Crop 2
5/17
39000
2.755
0.370.
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
83450
20000
2.35
16.805
NA
Bermuda
5/18
182000
2.755
1.728
Tarheel WWTP
Dry
<•5"
S
0.5
0.2
83450
20000
2.35
78.425
NA
Bermuda
5/19
13000
2.755
0.123
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
83450
20000
2.35
5.602
NA
Bermuda
10/28
39000
OA3
- 0.058
Tarheel WWTP
Dry
1 <.5"
S
1 0.5
0.2
1 95500
1 63600
1.94
4.413
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 _
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
- -
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
.Annuallbs/acre
TOTALS:
-0
273000:::;:
As
Pb
H
Mo
Ni
Se
Zn
P
105.245
0.014
16
0.047
0.002
0.124
0.149
0.024
12.574
83.798Prior
Years Cumulative lbs/ac
0.142
0.156
MCd
4
0
0.666
0.713 .
lm0
0.016
0.018
087
0.994
2.692
2.841
250
0.207
0.231
119.293l
131.Permitted
500
Current Cumulative lbs/ac
C. P. L. R.****
Permit PAN Limit Ist/2nd Crop
207
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/6/2018 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
'ermit #:
Operator:
- lcres Used:
Smithfield Farmland
W00014868
Richard Dunham
Total Dry Tons Applied (Annual): 37.98
Cation Exchange Capacity (non 503 only):
Owner: JW Burney Predominant Soil Series:
21.3 Acres Permitted: 21.3 Site #: SF07 Field #:
4.7
WmB
9
.Zesidual Analysis Data (Heavy Metals and Total Phosphorus use me/km % Solids use Raw Percent ft
Sample or
1
_2j
3J
4
5j
6j
L 7
8
9
10
j1j
12
Com-
Avg
10/25/17
posite
Date
% Solids
2.755
0.43
Arsenic
3
3
2
1130
897
47.75
32.7
radmiuml2
10.455
6.64
0.4
0.4
27.7
7.86
denum
Nickel
33.1
17.8
Selenium
5.29
5
- Zinc
2785
1700
Total
Phos-
18600
9820
horus
11kiinual
Heavy Metal Field Loadings
(Calculated in lbs/acre):
Total
1
3j
1 4
5j
6j
7
8
9
10
11
12 .
DT/AcJ
_2j
App.
m
-a Event
1.61
0.17
Arsenic
0.010
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000-
0.000
.0.000
0.000
0.011
';admium
0.006
0.001
0.000
0.000
0.000
,0.000
0.000
0.000
0.000
0.000
0.000-
0.000
0.007
Copper
3.645
0.305
0.000
0.000
0.000.
0X0-
0.000
0.000
0.000
1 0.000.
0.000
0:000.
3.950
Ir.hromhur
0.154
0.011
0.000
0.000-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.165
Lead
0.034
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0:000
0.000
0.000
0.036
Mercury
0.001
0.000
0.000
0.000
0.600
0.000
0.000
0.000
0.000
0.000
'0.000
0.000
'0.001
-,Molyb-
0.089
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.060
0.000
0.000
0.000
0.092
denum
Nickel
0.467
0.006
0.000
0.000
0.000
' 0.000
0:000
0.000
0.000
0.000
0.000
0.000
0.113
Selenium
0.017
0.002
0.000
0.000
0.000
0.000
0.000
0.000
' 0000
0.000
0.000
0.000
0.019
Zinc
8.984
0:578
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
'0.000
0.000
9.562
" Total
-, Phos-
60.604
3.339
0.000
0.000
0.000
0.000
0.000
0.000
0:000
0.000
'0.000
0.000
63.342'
horus
-'I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
i am aware that there are significant penalties for submitting false information, including the possibility of fines and
-imprisonment for knowing violations".
2/6/2018
Signature of Land Applier
I
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE.MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Smithfield Farmland Corp. WQ Permit #: WQ0014868
Land Owner: 1W Burney Annual Dry Tons Applied: 37.98
Operator: Richard Dunham Predominant Soil Series: WmB
Crop 1 Name: Bermuda -Pasture Crop 1 Max. PAN:
210
Field #:
Acres Utilized: 21.3
Site #: SF07 Acres Permitted:
Cation Exchange Capacity (non 503):
Crop 2 Name:
Crop 2 Max. PAN:
21.3
4.7
...a
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(DryTons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cord.
Wets
Moist)
Precip.
Past 24
Hrs•
inches
,D
5 'd
o• w,
0
o
m �L,
t w
0
`a'
`•;
;�,'
x
5
TIUJ
mg/kg
z gag
o 9
0 �•
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
Pp
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
5/21
123500
2.755
0.666
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
83450
20000
2.35
30.231
_ NA
Bermuda
5/22
175500
2.755
0.947
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
83450
20000
2.35
42.960
NA
Bermuda
10/27
45500
0.43
0.038
Tarheel WWTP
Dry
<.5"
S
0.5
1 0.2
95500
63600
1.94
1925
NA
Bermuda
10/28
156000
0.43
0.131
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
95500
63600
1.94
10.029
NA
Bermudo
0.000
0.000'
0.000
0.000
0.000
0.000
0.000
0.060
0.600
0.000
0.000
0.660
0.000
0.000
0.000
0.000
0.000
.0.000
0.000
0.000
0.000
0.000
0.000
0.000
FAnnual
-
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
`. 0
500500
:::: :
As
Cd
Cu
Cr
Pb
H
Mo
Ni
Se
Zn
P
86.145
uo0
Lime Applied
lbs/acre
0.011
0.007
3.950
0.165
0.036
0,001
0.092
0.113
0.019
9.562
.63.342 ;:
:::::::::::::::::::�::;::::::::::;:::::::�:
:::::•'::: :>::` i::2::22:::::: i
Date
Ibs/ac
ears Cumulative lbs/ac
0.164
0.094
28.289
3.742
0.721
0.017
0.946
3.101
0.201
138.145
2000
Cumulative lbs/ac
0.175
0.101
32.239
3.907
0.757
0.018
1.038
3.214
0.220
147.707
Permitted C. P. L. R.****
9
250
1000
250
500
Permit PAN Limit Ist/2nd Crop
210
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/6/2018 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
'ermit #:
-Jperator:
,ores Used:
Smithfield Farmland Corp. Total Dry Tons Applied (Annual): 17.18
WQ0014868 Cation Exchange Capacity (non 503 oily): 3.9
Steve Dunham Owner: JW Burney Predominant Soil Series: LaB
7.5 Acres Permitted: 7.5 Site #: SF07 Field #: 14
iesidual Analysis Data (Heavy Metals and Total.Phosnhorus use me/ke. % Solids use Raw Percent #1:
®®®®®®®®®®®®®
WMA
► ►►
► ►►►
► ►►►
► ►►►
► ►►►
► ►►►
► ►►►
► ►►►
► ►►►
► ►►►
► ►►►
► ►►►
► ►►
-'1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
`ware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/6/2018
Signature of Land Applier
Date
DENR FORM MFLSF (1212006)

- --- �--- �- - - - L_ -�
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 14 Acres Utilized: 7.5
Land Owner: JW Burney Annual Dry Tons Applied: 17.18 Site M SF07 Acres Permitted: 7.5
Operator:
Steve Dunham
Predominant Soil Series:
Crop 1 Name: Bermuda -Pasture Crop 1 Max. PAN:
147
LaB
Crop 2 Name:
Cation Exchange Capacity (non 503): 3.9
Crop 2 Max. PAN:
w t
I
C]
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry TonslAc)
Residual Sources
(NPDES #, WQN,
Fert., Animal
Waste, etc)
Sod
Cond.
(Dry'
Moist)
Precip•
Past 24
Hrs.
inches
,b
'�
a d.
o
?:
_
o
g
; 5
TKN
mg/kg
Z
o S
o
mg/kg
Nitrate
and
Nitrite
mglkg
PAN Applied
Ibs/acre
( )
Name of Crop Type
Receiving Residual
Application
Crop I
Crop 2
Crop 1
Crop 2
5/16
39000
2.755
0.597
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
83450
20000
2.35
27.113
NA
Bermuda
5/17
110500
2.755
1.693
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
83450
20000
2.35
76.819
NA
Bermuda
0.000
1
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
. 0.000
0.000
0.000
'0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000.
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp (attach FORM FSF supp
to this form):
..........
..........
TOTALS:
- 01
149500
i::::
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
103.9310.000
Lime Applied
Annual lbs/acre
0.014
0.009
5.175
0.219
0.048
0.002
0.127
0.152
0.024
12.755
85.188 ;::
2::i::::::::i>:i:>::;::::
;::.':::.:...................
Date
lbs/ac
Prior Years Cumulativelbs/ac
0.13
0.056
28.732
2.114
0.578PE
0.84
2.859
0.184
121.953:::;:::;:2:;:'>:;':;:;:;:':;:
2000
Current Cumulative lbs/ac
0.144
0.065
33.907
2.333
0.626
0.967
3.011
0.208
134.708
Permitted C.P. L. R.****
9
250
1000
250
500
Permit PAN Limit lst/2nd Cro p
147
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/6/2018 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anacrobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (1212006)

Page: 1 of 2
Report Number: 17-115-0203
Account Number: 46245
Send To, EMA Resources Inc
755 Yadkinville Road
Mocksville , NC 27028
Lab Number: 63557
Sample Id : North Lagoon
s
•
Waypoi nt. 7621 ain 80 -7, Road, Richmond, 27 -6446
Main 804-743-9401 0Fax [phone]
ANALYTICAL www.waypointanalytical.com
Project : Smithfield Tar Heel
NC Certff257
REPORT OFANALYSIS
Date Sampled: 4/24/201716:00:00
Date Received:04125/2017 00:00
Date Reported: 05101/2017'
Total Solids
2.20
22000
100.0
R D
04/25/2017 14:50
Moisture'
97.79
100.0
R D
04/25/201714:50
Total Kjeldahl Nitrogen
9.55
95500
50.0
R D
04/26/2017 08:30
Total Phosphorus
1.92
19200
100
MOS
04/26/2017 18:58
Total Potassium
0.46
4590
100
MOS
04/271201712:36
Total Sulfur
1.98
19800
100
MOS
04126/201718:58
Total Calcium
1.79
17900
100
MOS
04126/201718:58
Total Magnesium
0.20
1950
100
MOS
04/26/201718:58
Total Sodium
1.27
12700
1000
MOS
04/27/201713:08
Total Iron
13600
100
MOS
04/26/201718:58
Total Aluminum
9530
100
MOS
04/26/201718:58
Total Manganese
375
5.00
MOS
04126/201718:58
Total Copper
1220
5.00
MOS
04/26/201718:58
Total Zinc
2950
50.0
MOS
041271201713:08
Ammonia Nitrogen
2A9
24900
50.0
R D
04/2612017 08:30
Organic N
7.06
70600
50.0
04/26/2017 08:30
Nitrate+Nitrite-N
<2.44
2.44
SJB
04/28/201714:42
All I d
ht b t t d b t' k
D t t' 1' 't II N
b'
SM-254OG
SM-254OG
SM-4500-NH3C-TKN
6010C
6010C
6010C
6010C
6010C
6010C
6010C
6010C
6010C
6010C
6010C
SM-4500-NH3C
CALCULATION
4500NO3F-2011
va ues are on a ryweig as excep as no e y as ens . e ec an imi on a serves is on a we, asis. 4wa
�7Ourreportsandleltem arefortheexclusive and confidential use o/our clients, and may not be reproducedin whole orport, normay any reference be made mg
to the wodc, the results, or the company in any advertising, news release, orotherpublic announcements without obtaining ourpdor written authorization.
Debbie Holt
Laboratory Supervisor

L_. r-I --� —' f _—) _J 1_J 1_,_i l__—1 1_ -I - --� ---I
Page: 2 of 2
Report Number: 17-115-02030Account Number: 46245 7621 Whitepine Road, Richmond, VA 23237
Waypoi nt� Main 804.743-9401 a Fax [phone]
ANALYTICAL www.waypointanalytical.com
Send To: EMA Resources Inc
755 Yadkinville Road
Mocksville , NC 27028
Lab Number: 63557
Sample Id : North Lagoon
Project : Smithfield Tar Heel
NC Cert#257
REPORT OFANALYSIS
Total Cadmium
<2.00
Total Chromium
43.1
Total Nickel
31.6
Total Lead
11.0
Total Arsenic
<3.00
Total Mercury
<0.400
Total Selenium
5.58
pH (Standard Units)
7.91
Total Volatile Solids
76.36 763600
Total Molybdenum
14.1
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
Date Sampled: 4/24/2017 16:00:00
Date Received: 04/25/2017 00:00
Date Reported: 05/01/2017
2.00
MOS
04/26/201718:58
6010C
6.00
MOS
04/26/201718:58
601OC
5.00
MOS
04/26/201718:58
601OC
5.00
MOS
_ 04/26/201718:58
601OC
3.00
MOS
04/26/201718:58
6010C
0.400
SJB
05/01/201709:49
SW-7471B
5.00
MOS
04126/201718:58
6010C
1.00
R D
04/26/2017 08:30
SW-9045D
100.0
R D
04/25/201714:50
SM-2540G
5.00
MOS
04/26/201718:58
601OC
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole orpad, nor may any reference be made
to the wm$ the results, or the company in any advertising, news release, or otherpublicannouncements without obtaining ourpnorwnflen authorization.
"
Debbie Holt
Laboratory Supervisor

r - —1 '—J -- 1 3— -- i I— - I ( —I I_ J ' -- 1 I__—i I — I I, J
-J - - I ,__I I__ { I - _I
BIOSOLIDS SAMPL] CUSTODY
17-1 c.
7621 Whitepine Road F IIMII�III�EMA urcI I1Ill1lll'��IIuI�IIIuII�I'lull'l1 nc �25-2017 ce203 �al-Inbs�slem.crum
Account rf
amnnuem mrmeei
Submitted By Charge To Copy To
EMA Resources Inc
EMA Resources Inc
755 Yadkinville Rd
755 Yadkinville Rd
Mocksville, NC 27028 Mocksville, NC 27028
Project
�2
Z.7r1 FTZG L
Sample Information
Lab Number
Collection Information
Container Information
Please Check Dashed Tests
Sample ID
(Lob Use
Number
503
Nlhagen
Volatile
Only)
Type
of Bottles
Type
Volume
SL1
S/ede/s
ptt
CCE
All
CI
Solids
Others
�tfic- 4
C Composite
p/D'atte �7
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/Time
D0 f v
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plastic
oz
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7.
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—Grab
_Glass
— oz
pint
Composite
_Plastic
Roll I e SI n ra
Time
Received(Signature)Date
'Brie
25 ,Z
/Ua
Test Package Details
Special Instructions or Remarks
SLI: Total Solids (Moisture) Total Kjeldohl Nitrogen, Phosphorus and Potassium -
-
SL2r Dnslc Test SLt plus Sulfur, Calcium, Magnesium,Sodlum,Iron,Aluminum, Manganese, Copper And Zinc
603 Motels; Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel,. Selenium.
(Copper & Zinc Included In SL2)
Nlirogeu Serlexr'Iblal Kjcldnal, Ammonium, Nitrate & Orgunic Nitmgen.
CCa: Calcium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge)
I

Page: 1 of 2
Report Number: 17-170-0203
Account Number: 46245
Send To: EMA Resources Inc
755 Yadkinville Road
Mocksville , NC 27028
Waypoint_10.
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 a Fax [phone]
www.waypoin,tanalytical.com
Project: Smithfield Tar Heel
REPORT OFANALYSIS Date Sampled: 6/15/2017 18:00:00
Lab Number: 64410 Date Received: 06/19/2017 00:00
Sample Id : North Lagoon Date Reported: 06/2312017
Moisture
96.68
100.0
JM
06/19/201716:20
Total Kjeldahl Nitrogen
7.14
71400
50.0
JM
061201201712:05
Total Phosphorus
1.80
18000
100
MOS
06/23/2017 12:39
Total Potassium
0.37
3680
100
MOS
06/23/2017 12:39
Total Sulfur
1.74
17400
100
MOS
06/23/2017 12:39
Total Calcium
1.97
19700
100
MOS
06/23/2017 12:39
Total Magnesium
0.16
1620
100
MOS
06/23/2017 12:39
Total Sodium
0.84
8390
1000
MOS
06/23/2017 14:25
Total Iron
11300
100
MOS
06/23/2017 12:39
Total Aluminum
9250
100
MOS
06/23/2017 12:39
Total Manganese
376
5.00
MOS
06/23/2017 12:39
Total Copper
1040
5.00
MOS
06/23/2017 12:39
Total Zinc
2620
50.0.
MOS
06123/201714:25
Ammonia Nitrogen
1.51
15100
50.0
R D
06/21/2017 08:40
Organic N
5.63
56300
50.0
06/201201712:05
Nitrate+Nitrite-N
<2.26
2.26
SJB
06121/201713:34
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
SM-254OG
SMA500-NH3C-TKN
6010C
6010C
6010C
6010C
6010C
6010C
6010C
6010C
6010C
6010C
6010C
SM-4500-NH3C
CALCULATION
4500NO3F-2011
per,« Ourrepods sad fatten are 7orihe excfusive and confidential use atom d/ants, and may nat be reproduced In whole orpad, normay any m(emnco be made mC owr
to the work, the results, orthe company in anyadvertising, news release, or otherpublic announcements without obtaining ourpdor written aufhodza6on.
Pauric McGroary
Agronomist

Page: 2 of 2
Report Number: 17-170-0203 �
Account Number. 46245
Waypoint_
ANALYTICAL
Send To: EMA Resources Inc
755 Yadkinville Road
Mocksville , NC 27028
Lab Number: 64410
Sample Id : North Lagoon
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 a Fax [phone]
www.waypointanalytical.com
Project: Smithfield Tar Heel
REPORT OFANALYSIS Date sampled: 6/15/2017 18:00:00
Date Received: 06/19/2017 00:00
Date Reported: 06/2312017
Total Cadmium
<2.00
Total Chromium
52.4
Total Nickel
34.6
Total Lead
9.91
Total Arsenic
<3.00
Total Mercury
<0.400
Total Selenium
<5.00
pH (Standard Units)
7.93
Total Volatile Solids
77.64 776400
Total Molybdenum
13.6
Comments:
NC CERT#257, SC.CERT#9300 7001
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
2.00
MOS
06/23/201712:39
6010C
5.00
MOS
06/23/201712:39
6010C
5.00
MOS
06/23/201712:39
6010C
5.00
MOS
06/23/201712:39
6010C
3.00
MOS
06/23/201712:39
6010C
0.400
SJB
06/21/201715:59
SW-7471B
5.00
MOS
06/23/201712:39
6010C
1.00
R D
06/21/2017 08:40
SW-9045D
100.0
JM
06/191201716:20
SM-254OG
5.00
MOS
06123/201712:39
6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Ourtepods and leltersare for the exclusive and comidenRal use of our clients, and may not be reproduced In whole orpod, normayany rofersnce be made
to the watk the results, orthe company in any advertising, news telease, orotherpublic announcements without obtaining ourptior written authodzaboa.
Pauric McGroary
Agronomist

BIOSOLIDS SAMPLE n' _pNSNRTTA ^
6-gd,'Paste— rn' iIIuIHt�IHl�lul�lW�l����lNI411
7621 Whitapine!toad Richmond VA 23237 Tel: 8W, EMARes°urcas Inc
Smilhricld Tar Had
¢ Customer In.w .... io
S
ubmittedBy
EMEi Resources Inc
rces Inc
Rd 755 Yadlunville Rd
ato Nc 27028
Lab Number
Sampelp (Lab Use
- only)
L{tMco/t%
7�m f. f
$affl le lflformallofl',..•' Please Ched(De
Container Information '
Collodion lnfortna8on - - 503,. Nitrogen
Number Type Volume;. SL1,' SI2 Metals Series
Type Dale Time of Bowes
oz
GI �i t
Grab IasUcdt
_Composite oz
.Glass
3omposne
oz
_Glass
—:n'
Grab
_Plastic
Composite
z
Glass
�ir
Grab
_Plasfio
of
composite
Sodium iron, lron, Aluminum,Mangonrse, Copper And Zinc
Tntd Solids (Moisture) Tom
1(jddahl Nitrogen, phosp torus a.
Dmic•rest SLI plus SuINr, Calcium.l�'Mercury, Molybdenum, Lead, Nickel. Selenium.
M°tals: Arsenic, Cadmium, Chromium,
(Copper & Z nc included in SL2) Ni,mtc & arsenic Nitrog°,,.
"gcn series: Total I(joldahl, Ammonium,
:• rAlcium Carbonate Equivalent of Total neubaliza8on Value (For Lime Treated Sludge)
pH I GLE I Ag I Cl

Page: 1 of 2
Report Number: 17-299-0203
Account Number: 46245
Send To: EMA Resources Inc
755 Yadkinville Road
Mocksville , NC 27028
Lab Number: 56870
Sample Id : South Lagoon
e
Waypoi nt_ 7621 ain' 804-7 Road, Richmond, 27 -6446
Main 804.743-9401 0Fax [phone]fi
ANALYTICAL www.waypointanalytical.com
Project : Smithfield Tar Heel
REPORT OF ANALYSIS
Date Sampled: 10/25/2017 07:00:00
Date Received: 10/26/2017 00:00
Date Reported: 11102/2017
Total Solids •
0.43
4300
100.0
JM
10/26/2017 15:00
Moisture •
99.56
100.0
JM
10126/201715:00
Total Kjeldahl Nitrogen
9.55
95500
50.0
R D
10/27/2017 08:90
Total Phosphorus
0.98
9820
100
MOS
11/01/2017 15:30
Total Potassium
0.98
9780
1000
MOS
11/01/201717:18
Total Sulfur
1.14
11400
100
MOS
11/01/2017 15:30
Total Calcium
1.38
13800
100
MOS
11/01/2017 15:30
Total Magnesium
0.28
2800
100
MOS
11/01/2017 15:30
Total Sodium
5.69
56900
1000
MOS
11/01/2017 17:18
Total Iron
7230
100
MOS
11/01/201715:30
Total Aluminum
4250
100
MOS
11101/201715:30
Total Manganese
160
5.00
MOS
11/011201715:30
Total Copper
897
5.00
MOS
11/01/2017 15:30
Total Zinc
1700
50.0
MOS
11101/201717:18
Ammonia Nitrogen
6.36
63600
50.0
R D
10/27/2017 08:30
Organic
3.19
31900
50.0
10/27/201708:30
Nitrate+Nitrite-N
<1.94
1.94
SJB
10/31/201713:48
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series Is on a wet basis
SM-2540G
SM-2540G
SM4500-NH3C-TKN
6010C
6010C
6010C
6010C
6010C
6010C
6010C
6010C
6010C
6010C
6010C
SM4500-NH3C
CALCULATION
4500NO3F-2011
poo,« P owr
Our reports and letlers are tor the exclusive and confidential use orourclients, and may not be reproduced in whole orpart, nor may any reference be made
to the work, the results, or the company In any advertising, news release, or otherpublicannouncoments;without obtaining ourpdor mitten authodution.
Pauric McGroary
Agronomist

Page: 2 of 2
Report Number: 17-299-0203 �
Account Number: 46245 7621 Whitepine Road, Richmond, VA 23237
Waypoi nt� Main 804-743-9401 a Fax [phone]
ANALYTICAL www.waypointanalytical.com
Send To: EMA Resources Inc
755 Yadkinville Road
Mocksville , NC 27028
Lab Number: 56870
Sample Id : South Lagoon
Total Cadmium
<2.00
Total Chromium
32.7
Total Nickel
17.8
Total Lead
6.64
Total Arsenic
<3.00
Total Mercury
<0.400
Total Selenium
<5.00
pH
7.97
Total Volatile Solids
72.72 727200
Total Molybdenum
7.86
Comments:
NC CERT#257, SC CERT#9300 7001
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
Project: Smithfield Tar Heel
REPORT OF ANALYSIS Date Sampled: 10/25/2017 07:00:00
Date Received: 10/26/2017 00:00
Date Reported: 11/0212017
2.00 -
MOS
11/01/2017 15:30
6010C
5.00
-MOS
11/01/201716:30
6010C
5.00
MOS
11101/201715:30
6010C
5.00
MOS
11/01/201715:30
6010C
3.00
MOS
11/02/201711:56
6010C
0.400
SJB
11/01/201714:32
SW-7471B
5.00
MOS
11/021201711:56
6010C
1.00
R D _
10/27/2017 08:30
SW-9045D
100.0
JM
10/26/201715:00
SM-254OG
5.00
MOS
11/01/201715:30
6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letfersore /orthe exclusive and confidential use o/our clients, and may not be reproduced in whole orpdrt, normay any re/erence be made
to the work, the results, orthe companyin anyadvedising, news release, orotherpublic announcements without obtaining ourprior wnflen authonzah'on..
Pauric McGroary
Agronomist

l "-____ I__N )-_-' a- - I- 2—_ I -_- t_-_' - I -'
I,-, !__I
AFLA&L
Eastern
�IIIIImn �I„_2_= -2d3
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755 Yadkinville Rd 755 Yadkinville Rd
Mocksville,
le, NC 27028
NC 27028 MocksvilAJ
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SLi: Total Solids(Moisture) Total KjeldahlNitmgen,Phosphomsand Po[assium
SL2: Buie Test SLl plus Sulfur, Calcium, Magncsimn,Sodium, Iron, Aluminum, Manganese, Copper And Zinc
503 Metals: Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel,
Selenium.
(Copper & Zink included in SL2)
Nitrogen Series: Total Kjeldahl, Ammonium, Nitmlc& Organic Nitrogen.
,
CCE: Calcium Carbonate Equivalent orTotal neutralization Value (For Lime Treated Sludge)

myESC
ANALYTICAL REPORT
May 03, 2017
EMA Resources
Sample Delivery Group: L904770
Samples Received: 04/25/2017
Project Number.
Description: Sludge
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC,27028
Entire Report Reviewed By:
Janet Hensley
Technical Service Representative
Results relate only to the Items tested or calibrated and are reported as rounded values This test report shag not be
reproduced, eviceptln full,vdthout written approval of the laboratory. Whereappllcable.sampring conducted by ESCis
performed per guidance pravlded in laboratory standard operating procedures: 060302, 060303. and 060300. �
IDTt

TABLE OF CONTENTS ONELAB.NAMONWIDE.
'Cp: Cover Page
1
2Tc; Table of Contents
2
3Ss: Sample Summary
3
4Cn: Case Narrative
4
'Sr: Sample Results
5
SMITHFIELD TARHEEL L904770-01
5
6Qc: Quality Control Summary
7
Wet Chemistry by Method 9012 B
7
Wet Chemistry by Method 9034-9030B
8
Wet Chemistry by Method 9045D
9
Wet Chemistry by Method D93/1010A
10
Mercury by Method 7470A
11
Metals (ICP) by Method 6010D
12
Volatile Organic Compounds (GC/MS) by Method 8260B
13
Chlorinated Acid Herbicides (GC) by Method 8151A
15
Pesticides (GC) by Method 8081B
16
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
17
'GI: Glossary of Terms
19
"Al: Accreditations & Locations
20
9Sc: Chain of Custody
21
ACCOUNT: PROJECT: SDG: DATEMME: PAGE:
I EMA Resources L904770 05/03016:45 2 of 21

SAMPLE
SUMMARY
ONE LAB. NATIONWIDE.
Collected by
Collected dateltime
Received dateltime
_
SMITHFIELD TARHEEL L9O477O-01 Waste
RoywhRaker
04124/1716:45
04/25/1709:00
Cp
- Method
Batch
Dilution
Preparation
Analysis
Analyst
_
date/time
clateNme
ZTC
Preparation by Method 1311
WG975100
1
04129A708:24
04129/1708:24
BG
1 Preparation by Method 1311
WG975122
1
04/29/1709:55
04129/1709:55
BG
Wet Chemistry by Method 9012 B
WG974348
1
04126/1715:18
04127/1700:31
ASK
Wet Chemistry by Method 9034-9030B
WG974049
1
04126/1716:30
0412611716:30
KK
Wet Chemistry by Method 9045D
WG974066
1
04127/1711:34
042711713:03
MA
4Cn
Wet Chemistry by Method D9311010A
WG974041
1
0412611718:35
0426/1718:35
MAJ
Mercury by Method 7470A
WG975480
1
05/0111714:24
OSIOV1715:52
NJB
sSf
Metals(ICP( by Method 6010D
WG975496
1
05101/1713:15
05101/1714:45
CCE
Volatile Organic Compounds (GC/MS( by Method 8260B
WG975465
1
05/01/1714:35
05/0111714:35
BMB
Chlorinated Acid Herbicides (GC) by Method 815tA
WG975648
1
05102/1706:27
05/02/1719:47
KLM
aQC
Pestiddes(Gq by Method 8081E
WG975572
1
0510111720:44
05102J1712:24
VKS
I Semi Volatile Organic Compounds (GC/MS( by Method 8270D
WG975569
1
0510111723:07
05102A713:03
JF
7GI
--,
9
Sc
I ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EMA Resources
L904770
0510311716:45
3 of 21

CASE NARRATIVE ONE LAB. NATIONWIDE.
All sample aliquots were received at the correct temperature, in the proper containers, with the ch
appropriate preservatives, and within method specified holding times. All MDL (LOD) and RDL (LOO)
values reported for environmental samples have been corrected for the dilution factor used In the Tc
analysis. All Method and Batch Quality Control are within established criteria except where addressed
in this case narrative, a non-conformance form or properly qualified within the sample results. By my
digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the Ss
laboratory as having the potential to affect the quality of the data have been identified by the
laboratory, and no information or data have been knowingly withheld that would affect the quality of
the data.
6Sr
6
QC
[GI
Janet Hensley cAl
Technical Service Representative
Project Narrative 9Sc
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012B. ,
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/9030B.
ACCOUNT: PROJECT: SDGr DATE/TIME: PAGE:
EMA Resources L904770 05103A716:45 4 of 21

SMITHFIELD TARHEEL SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. 41�
h Collected date/time: 04/24/17 iGA5 L904770
Preparation by Method 1311
Result
Qualifier
Prep
Batch
C p
-J Analyte
-. TCLP Extraction -
dateltime
412912017824:34 AM
WG975100
zTC
TCLP ZHE Extraction -
4129/2017 9:55:31 AM
WG975122
Fluid 1
4129/20178:24:34 AM
WG975100
a$S
Initial pH 6.79
4/29/2017 8:24:34 AM
WG975100
Final pH 4.76
412920178:24:34 AM
WG975100
4Cn
Wet Chemistry by Method 9012 B
Result
Qualifier
RDL Dilution
Analysis Batch
Analyse mg/kg
mg/kg
date/lime
l Reactive Cyanide ND
0250 1
041271201700:31 WG974348
C
Wet Chemistry by Method 9034-9030B
7
'— Result
Qualifier
RDL Dilution
Analysis Batch -
GI
- Analyse mg/kg
mg/kg
dateltime
Reactive Sulfide ND
25.0 1
04/261201716:30 WG974049
~I
Wet Chemistry by Method 9045D
eSc
g Result
Qualifier
Dilution Analysis
Batch -
_Analyte su
date/time
CovosNity, by pH 7.74
T8
1 04127/201713:03 WG974066
Sample Namable:
'
- ' 9045D L904770-01 WG974065: 7.74 at 21.9c
Wet Chemistry by Method D93/1010A
-' - Result
Qualifier
Dilution Analysis
Batch
_ Analyte Deg.F
date/time
'
Ignitability ONI at 170
1 04126/201718:35 WG974041
Mercury by Method 7470A
Result
Qualifier'
RDL Limit
Dilution Analysis Batch
_ Analyte mgA
mgA mgn
date/time
Mercury ND
0.0100 0.20
1 05/01/201715:52 WG975480
Metals (ICP) by Method 6010D
Result
Qualifier RDL
Limit
Dilution
Analysis
Balch
I Analyse
mgA
mgA
mgA
-
dateltime
Arsenic
ND
0.100
5
1
05/01/201714:45
WG975496
— Barium
ND
0.100
100
1
051011201714:45
WG975496
_ 4 Cadmium
ND
0.100
1
1
051OV201714:45
WG975495
: Chromium
ND
0.100
5
1
05/011201714:45
WG975496
Lead
ND
0.100
5
1
05/011201714:45
WG975496
Selenium
NO
0.100
1
1
05101/201714:45
WG975496
Silver
ND
0.100
5
1
05/01/201714:45
WG975496
Volatile Organic Compounds (GUMS) by Method 8260B
,
Result
Qualifier RDL
Limit
Dilution
Analysis
Batch
jCAnalyle
mgA
mgfi
mgn
date/time
-' Benzene
ND
0.0500
0.50
1
05/011201714:35
WG975465
Carbon tetrachloride
ND
0.0500
0.50
1
05/01/201714:35
WG975465
I Chlorobenzene
ND
0.0500
100
1
05/01/201714:35
WG975465
i Chloroform
ND
0.250
6
1
051011201714:35
WG975465
i ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
�, EMA Resources L904770 05103/1716:45 6 of 21

. SMITHFIELD TARHEEL
SAMPLE
RESULTS - 01
ONE LAB. NATIONWIDE.
-'
Collected date/time: 04/24/17 16:45
L904770
Volatile Organic Compounds (GC/MS) by Method 8260E
I�
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
- Cp
Analyte mgA
mgA
mgA
date/time
,
1,2-Dichloroethane ND
0.0500
0.50
1 05/01/201714:35
WG975465
2TC
_y
1,1-Dichioreethene ND
0.0500
0.70
1 05101/201714:35
WG975465
2-Butanone(ME10 ND
0.500
200
1 051011201714:35
WG975465
a$S
Tetrachloroethene ND
0.0500
0.70
1 05/01/20171435
WG975465
_
r j
Trichloroeihene ND
0.0500
0.50
1 05/01/201714:35
WG975465
Vinyl chloride ND
0.0500
0.20
1 05/01/201714:35
WG975465
Cn
/SJToluene-d8 121
A80.0-120
120
05101/201714.35
WG975465
(5) Dlbromo8uoromethone 702
76.0.123
123
OSlOY201714135
WG975465
(S) om'o-wfiuorofoluene 120
80.0-120
120
05101120171425
WG975465
IS)4-BromoBuorobenzene 102
80.0-120
f20
051011201714:35
WG975465
_
'
6QC
Chlorinated Acid Herbicides (GC) by Method 8151A
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
7GI
Analyte mgA
mgA
mgA
date/time
-1
2,4,5-TP(Silvex( ND
0.00200
1
1 051021201719:47
WG975648
a
2,4-D ND
0.00200
10
1 05/021201719:47
WG975648
AI
(S)2,4-D/ch/orophenylAceficAdd 97.6
14.0-158
158
051021201719:47
WG975648
Pesticides
9Sc
(GC) by Method 8081E
,.-.
Result Qualifier RDL
Dilution
Analysts Batch
'Analyze mgfl
mgA
date/time
Chlordane ND
0.00500
1
05102/201712:24 WG975572'
Endrin ND
0.00500
1
05102201712:24 WG975572
-
Heptachlor ND
0.00500
1
05/021201712:24 WG975572
.-,
Undane ND
0,00500
b
05102f201712:24 WG975572
Methoxychlor ND
0.00500
1
05102f201712:24 WG975572
--
Toxaphene ND
0.0100
1
05/02/201712:24 WG975572
(S) Decochloroblphenyl 61.2
10.0-144
05/02201712:24 WG975572
f
(SJTetrochloro-ranglene 45.6
10.0-135
05/0220171224 WG975572
I
Semi Volatile Organic Compounds
(GC/MS) by Method 8270D
-"�
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyze mgA
mgA
mgfi
dateitime
1,4-Dichlorobenzene ND
0.100
7.50
1 051021201713:03
WG975569-
,-.
2,4-Dinitrotoluene ND
0.100
0.13
1 051021201713:03
WG975569
I
Hexachlorobenzene ND -
0.100
0.13
1 05102/201713:03
WG975569
Hexachlor0,3-butadiene ND
0.100
0.50
1 061021201713:03
WG975569
Hexachloroethane ND
0.100
3
1 05/021201713:03
WG975569
Nitrobenzene ND
0.100
2
1 05/02/201713:03
WG975569
il_ r
Pyridine ND
0.100
5
1 05/021201713:03
WG975569
3&4-Methyl Phenol ND
0.100
400
1 05102/201713:03
WG975569
2-Methylphenol ND
0.100
200
1 05/021201713:03
WG975569
Pentachlorophenol ND
0.100
100
1 05/02/201713:03
WG975569
I_i
2,4,5-Trichlorophenol ND
0.100
400
1 05102/201713:03
WG975569
2,4,6-Trichlorophenol ND
0.100 "
2
1 051021201713:03
WG975569
(S) 2-Fluorophenol 55.1
10.0-120
120
05102201713:03
WG975569
(S)Ahenol-05 43
10.0-120
120
051021201713:03
WG975569
IS)Nitrobenzene-6 70.7
10.0-126
126
051021201713.03
WG975569
(S)2-Fluorobiphenyl 82.3
220-127
127
05r0212017.13:03
WG975569
IS)2,4,6-Tribrothophenof 79.4
10.0-153
153
051021201713:03
W6975569
Np-Terphenyl-d14 95.8
29.0-141
141
0.51021201713.03
WG975569
ACCOUNT.
PROJECT:
SDG:
DATE/TIMe
PAGE:
EMA Resources
L904770
05103A716:45
6 of 21

WG974348 QUALITY CONTROL SUMMARY
ONE LAB. NATIONWIDE.
Wet Chemistry by Method 9012 B L904770-01
Method Blank (MB)
i Cp
(MB) R3213833-1 04/27/17 00:11
MB Result MB Qualifier MB MDL MB RDL
a
Analyte mg/kg mg/kg mglkg
Reactive Cyanide U 0.039 0 250
SS
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
El
(LCS) R3213833-2 04/27A7 00:12 - (LCSD) R3213933-3 04/27/17 00:13
Spike Amount LCS Result LCSD Result LCS Rec LCSD Rec Rec Limits LCS Qualifier LCSD Qualifier RPD
RPD Limits
5$r
Analyte mg/kg mg/kg mg/kg % % % %
%
Reactive Cyanide 2:50 2:60 2.52 109 101 50-150 3
20
L9O4458-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
7 GI
(OS) L904458-02 04/27M 00:18 - (MS) R3213833-4 04/27/17 00:19 - (1VISD) R3213833-5 04/27/17 00:20
Spike Amount Original Result MS Result MSD Result MS Rec MSD Rec. Dilution Rec Umits MS Qualifier
Analyte mg/kg mg/kg mg/kg mg/kg % % %
MSD Qualifier RPD
%
RPD Limits
% aAl
Reactive Cyanide 167 ND 1.53 1.53 92 92 1 75125
0
20
9$C
ACCOUNT: PROJECT: SDG:
EMA Resources L904770
DATEMME:
05103A716:45
PAGE:
7 0121

WG974049 QUALITY CONTROL SUMMARY ONE LAB. NATION\AADE.
Wet Chemistry by Method 9034-90308 L904770-01
Method Blank (MB)
(MB) WG974049-1 0412611716:30
MB Result MB Qualifier MB MDL MB RDL
Anayte mg/kg mg/kg mg/kg
Reactive Sulfide U 7.63 250
L9O477O-01 Original Sample (OS) • Duplicate (DUP)
(OS) L904770-01 04/26A716:30 • (DUP) WG974049A 04/2611716:30
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Anayte mg/kg mpg % %
Reaclrve Sulfide ND ND 1 0.000 20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(1-CS) WG974049-2 04/2611716:30 • (LCSD) WG974049-3 04/26/1716:30
Spike Amount LCS Result LCSD Result LCS Rea LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg % % % % %
Reacuve Sulfide 100 80.6 74A 80.6 744 700130 8.00 20
ACCOUNT: PROJECT: SDG: DATE/TIME PAGE:
EMA Resources L904770 05/03/1716:45 8 of 21

WG974066 T� QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE �
Wet Chemistry by Method 9045D L90477041
L9O4611-02 Original Sample (OS) • Duplicate (DUP)
(OS) L904611-02 04/27/1713:03 - (DUP) WG974066-3 0412711713:03 Cp
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD - 2
Limits TC
Analyte _ su su % %
CorrosivitybypH 7.95 7.93 i 0.252 T8 1 ss
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) WG974066-1 04/27/1713:03 • (LCSD) WG974066-2 0412711713:03
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte Su su su % % % % %
ComosivilybypH 7.50 7.55 7.56 101 101 9841D2 0.132 1
ACCOUNT: PROJECT: SOG:
EMA Resources L904770
DATErnME
05/03n716:45
PAGE:
9 of 21

WG974041 - - - J - - - QUALITY CONTROL SUMMARY__
Wet Chemistry by Method D93/1010A L904770-01
L904947-01 Original Sample (OS) • Duplicate (DUP)
--
ONE LAB. NATIONWIDE.
Cp
(OS) L904947-01 04126/1718:35 • (DUP) R3213780-3 04/26/1718:35
Original Result DUP Result Dilufion DUP RPD DUP Qualifier DUP RPD
Umds
ETC
Analyte Deg. F Deg. F % %
Ignitabiliry 108 108 1 0.000 10
?SS
4Cn
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3213780-1 04/26/1718:35 - (LCSD) R3213780-2 0412611718:35
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
s
Sf
Analyte Deg. F Deg. F Deg. F % % % % %
Ign'M1abdity 82.0 82.4 824 101 101 96.0404 0.000 10 -
7GI
aAl
9Sc
ACCOUNT: PROJECT: SDG:
EMA Resources L904770
DATE/rlME:
05/03A716:45
PAGE:
10 or21

'
WG975480 QUALITY C0NTR0L4 SUMMARY
oNELAe. NAT16F4 IDE.
Mercury by Method 7470A L904770-01
Method Blank (MB)
Cp
(MB) R3214727-1 05/01/1715:41
MB Result MB Qualifier MB MDL MB RDL
ZTC
Analyte mgA mgA mgA
Mercury U 0.00333 0.0100
3$$
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
4Cn
(LCS) R3214727-2 05/01A715.48 • (LCSD) R3214727-3 05/OV1715:50
Spike Amount LCS Result LCSD Result LCS Rec LCSD pea Rec. Limits LCS Qualifier LCSD Qualifier RPD
RPD Limits
6$r
Analyte mg/l mgA mgA % % % %
---,,.._..__
%
._'r__._,. _ _....._. _.._.....,._...
Mercury 0.0300 0.0287 0.0287 96 96 80d20 0
20
L9O477O-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
7Gl
(OS) L9D4770-01 OS/01/1715:52 - (MS) R3214727-4 05/01/1715:55 • (MSD) R3214727-5 0SIOIK715:57
Spike Amount Original Result MS Result . MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier
MSDOualifier RPD
RPD Limits
Analyte mgA mgA mgA % % %
%
_mgA
Mercury _ 0.0300 ND 0.0264 0.0267 88 89 1 75-125
1
20
9Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE
EMA Resources L904770 05/03A716:45 11 of21

CONTROL SUMMARY
ONE LAB. NATIONWIDE 41�-
WG975496
QUALITY
Metals (ICP) by Method 6010D
L904770-01
Method Blank (MB)
Cp
(MB) R3214735.1 05/0111714:37
MB Result
MB Qualifier MB MDL
MB ROL
2TC
Analyze--.-•__,__..,_._ mg/1....._._--'-'----._
r
_. mgA
T
mgA
...
Arsenic U
0.0333
0.100
a$S
Barlum U
0.0333
0.100
Cadmium U
0.0333
0.100
Chromium U
0.0333
0.100
4^n
Lead U
0.0333
0.100
Selenium U
0.0333
0.100
sSr
Silver U
0.0333
0.100
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3214735.2 05/01/1714:40 • (LCSD) R3214735-3 05/0111714:42
i
7
Spike Amount
LCS Result LCSD Result
LCS Rec.
LCSD Rec
Rec. Limits LCS Qualifier LCSD Qualifier
RPD
RPD Limits
GI
Analyte mgA
mgA mgA
%
%
%
%
%
ArseNc •-- --10.0 .-_.- --9.87-W
.-.- '9.90
99
99
80-120-
0
20
oAI
Badum 10.0
9.89 9.96
99
100
80-120
1
20
Cadmium 10.0
9.95 10.0
99
100
80-120
1
20
y
Chromium 10.0
9A3 9.51
94
95
80-120
1
20
SC
Lead 10.0
9.76 9.84
98
98
80-120
1
20
Selenium 10.0
10.2 10.2
102
102
80-120
0
20
Silver 2.00
1.86 1.87
93
93
80-120
0
20
L904770-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS)L904770-01 05/0117714:45 • (MS) R3214735-5 051OU1714:51 • (MSD) R3214735-6 05/OV1714:54
Spike Amount
Original Result
MS Result
MSD Result
MS Rec
MSD Rec.
Dilution
Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
Analyte
mg/I_
mgA
%
%
...
-
%
-
%
-
Arsenic
_--,---._mgll,
- - 10.0
„.mgA
ND
.
10.2
10.2
102
102
1
75425
0.
20
Badum
10.0
ND
9.85
9.84
98 -
98
1
75425
0
20
Cadmium
10.0
NO
10.2
10.1
102
101
1
75-125
0
20
Chromium
10.0
NO
9A4
9.49
94
95
1
75-125
1
20
Lead
10.0
ND
9.94
9.93
99
99
1
75-125
0
20
Selenium
10.0
,ND
10.7
10.6
107
106
1
75-125
1
.20•
Silver
2.00
NO
1.89
L90
94
95
1
75425
1
20
ACCOUNT: PROJECT: SDG:
EMA Resources L904770
DATErrIME:
05/03/1716:45
PAGE:
12 of 21

WG975465 QUALITY CONTROL SUMMARY ONELAe.MATIONWLE.
Volatile Organic Compounds (GC/MS) by Method 8260E L904770.01
Method Blank (MB)
(MB) R32146893 051OV17
--
MB Result
Anaiyte
mg/I
Benzene
U
Carbon tetrachloride
U
Chlorobenzene
U
Chloroform
U
1,2-Dlchloroethane
U
1,1-Dichloroethene
U
2-Butanone(MEK)
U
Tetmchlomethene
U
Trichooroethene
U
Vinyl chloride
U
(5) To1uened8
103
(S) Dlbromo8uoromethane
104
IS)acta-70wrofoluene
103
(S)4-Bromoffucrobenzene
702
MB Oualifier MB MDL
MS RDL
mgn
mg
0.0167
0.0500
0.0167
0.0500
0.0167
0.0500
0.0833
0.250
0.0167
0.0500
0.0167
0.0500
0.167
0.500
0.0167
0.0500
0.0167
0.0500
0.0167
0.0500
8ao-120
76.0-123
8a0.120
80.0.120
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(1.CS) R32146894 05/01/1711:46 - (LCSD) R3214689-2 051OV1711:59
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
Analyte
mgn
mgn
mgA
%.
%
%
Benzene
0.0250
0.0257
0.0211
103
109
69.0-123
Carbon tetrachloride
0.0250
0.0257
0.0274
103
110
63.0-122
Chlorobenzene
0.0250
0.0262
0.0268
105
107
79.0-121
Chloroform
0.0250
0.0256
, 0.0269
102
108
72.0421
1,2-Dichloroethane
0.0250
0.0259
0.0277
103
111
67.0426
1,1-Dichloroethene
0.0250
0.0246
0.0262
98.5
105
64.0-129
2-Butanone(MEK)
0.125
0.139
0.133
Ili
107
37.0458
Te0achloroelhene
0.0250
0.0266
0.0271
107
108
70.0-127
Trichloroelhene
0.0250
0.0263
0,0270
' 10S
108
78.0-120
Vinyl chloride
0.0250
0.0255
0.0289 -
102
116
64.0-133
(S)Toluene-d8
101
102
80.0-120
p)Dibromo8uaromethone
101
104
76.4123
IS)a,o,o-Affluorotoluene
102
102
80.0-120
IS)4-BromoBuorobenzene
99.6
98.4
80.0-110
LCS Oualifier LCSD Oualifier RPD
RPD Limits
532
20
6.28
20
239
20
5.07
20
6.92
20
6.25
20
4.32
20
1.56
20
2.54
20
12.5
20
ACCOUNT: PROJECT: SOG: DATEMME: PAGE:
EMA Resources L904770 05/03/1716:45 13 of 21

WG975465
QUALITY CONTROL
SUMMARY
ONE LAB. NA-nommDL
Volatile Organic Compounds (GC/MS) by Method 8260B
1904770.01
L904785-01 Original Sample (OS) . Matrix Spike (MS) • Matrix Spike Duplicate (MSD) '
Cp
(OS) L904785-01 05/01/1714:48 • (MS) R3214689-4 05/OV1715:14 • (MSD) R3214689-5 OSIOV1715:27
Spike Amount Original Result MS Result
MSD Result MS Rec MSD Rec. Wallop
Rec. Limits MS Qualifier
MSD Qualifier RPD
RPD Limits
zTC
Analyte mg/I mgn mgn
mgn % %
%
%
%
Benzene 1.25 ND 1.12
1.12 89.4 89.4 1
34.0-147
0.0100
20
35S
Carbon tetrachloride 1.25 ND 1.21
1.21 96.6 '96.7 1
41.0-138
0.180
20
Chlorobenzene 1.25 ND 1.16
1.15 92A 91.8 1
52.0-141
0.670
20
Chloroform 1.25 ND 1.21
1.19 97.1 95.5 1
50.0439
1.68
20
qCn
1,2-Dichloroethane 1.25 ND 1.17
1.21 93.9 96.7 1
47.0-141
2.92
20
1,1-Dichloroethene 1.25 ND 1.04
1.03 83.0 82.0 1
31.0-148
1.12
20
ssr
2-Butanone(MEit) 6.25 ND 3:76
4.68 60.2 74.9 1
12.0-149
21.8
24
Tehachloroethene 1.25 ND 1.12
1.09 89.7 87.1 1
38.D-147
2.86
20
Trlchlotoethene 1.25 ND 1.10
1.09 88.1 86.6 1
32.0-156
1.71
20
Vinyl chloride 1.25 ND 1.01
1.05 80.8 84.0. 1
24.0-153
3.94
20
(5)Toluene-18
117 102
80.0420
7Gi
(SJDibromo8uoromethone
106 104
76.0-123
(S) o o.o-Trinuorololuene
(S)4-Biomonuorobenzene
10 101
99.3 97.6
80.0-120
80.0420
eAl
aSC
ACCOUNT: PROJECT: SDG: DATE/TIME PAGE
EMA Resources L904770 05/03/1716:45 14 of 21

T
WG975648
QUALITY
CONTROL SUMMARY
ONE LAB. NATIONWIDE.
Chlorinated Acid Herbicides (GC) by Method 8151A
L904770.01
Method Blank (MB)
Cp
(MB) R3215334-1 0510211719:07
MB Result MBQualifier MB MDL
M8 RDL
ZTC
Analyte mg/I mgA
__._..
mgA -
.. _
- ..
2,4-0 .__....... U.
0.000667
0.00200
3S5
2,4,5-TP(SINex) u 0.000667
0.00200
(5'J2,4-DichlorophenylAcetic 949
f4.4158
Acid
4Cn
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
SSr
(LCS) R3215334-2 05/02/171920 • (LCSD) R3215334-3 05/02/1719.34
Spike Amount LCS Result LCSD Result
LCS Rec. LCSD Rec
Rec. Limits LCS Qualifier LCSD Qualifier
RPD
RPD Limits
Analyte mgA mgA mgA
% %
%
%
% -
2,4-D 0.00500 0.00492 0.00471
98.3 94.2
56.0-120
4.30
20
761.
2A,5-TP(Silve4 0.00500 0.00451 0.00423
903 84.5
55.0420
6.59
20
95.9 88.5
20.0-138
Add)2,4-0IchlorophenyfAceBc
aAl
9Sc
ACCOUNT: PROJECT: SDG: DATE/OME: PAGE
EMA Resources L904770 05/0311716:45 15 of 21

--)�'---1-1,-� _ - _ 1 -� w-
WG975572 QUALITY CONTROL SUMMARY oNE LA8NATIOMW10hi.
Pesticides (GC) by Method 8081B L904770-01
Method Blank (MB)
(MB) R3214997-1 0510211712:10
MB Result
MB Oualifer MB MDL
Analyte -
mgR .
mg8
Gamma BHL
U
0.00167
Enddn
U
0.00167
Heptachlor
U
0.00167
Methoxychlor
U
0.00167
Chlordane
U
0.00167
Toxaphene
U
0.00333
(S) Demchlamblphenyl
69.2
-
(5)Tetrarh1oro-m-xylene
622
MB RDL
m9^
0.00500 _
0.00500
0.00500
0.00500
0.00500
0.0100
10.0-144
10.0-135
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3214997-2 05/02/17ll:26 • (LCSD) R3214997-3 05102/1711:41
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec
Rec Limits
Analyte
ml;A
mg/1
mgn
%
%
%
Gamma BHL
0.6O10
0.000733
0.000897
. 73.3
88.7
56.0433
Enddn
0.00100
0.000760
0.000887
76.0
8B.7
58.0-135
Heptachlor
0.00100
0.000686
0.000809
68.6
80.9
37.0434-
Methoxychlor
0.00100
0.000824
0.000951
82A
95.1
44.0-160
(S) Decachlomblphenjd
-
68.7
78.8
10.0456
(S)Tearachloro-m-xylene
48.8
69.7
13.9-137
L904770-01 Original Sample (OS) • Matrix Spike (
(OS) L904770-01 05/02/1712:24 - (MS) R3214997-4 05/02/1712:38
Spike Amount
Original Result
MS Result
Analyte
mg/I
mgll
mgll
Gamma BHC
0.0100
ND
0.00778
Endrin
0.0100
ND
0.00794
Heptachlor
0.0100
ND
0.00736
Methouychlor
0.0100.
ND
0.00844
(S) Decochloroblphen)4
(S) TetraMoro-m-xy/ene
• Matrix Spike Duplicate (MSD)
LCS Qualifier LCSD Qualifier RPD RPD Limits
19.0 20
1SA 20
16.5 24
14A 22
• (MSD) R3214997-5 05/0211712:53
MSD Result MS Rec. MSD Rec.
Dilullon
Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
mgn % %
%
%
%
0.00758 77.8 75.8
1
56.0-133
2.55
20
0.00765 79A 76.5
1
58.0.135
3.66
20
0.00720 73.6 72.0
1
37.0-134
2.17
24
0.00822 ' 84A 82.2
1
44.0-160
2.71
22
70.5 64.2
-
10.0-144
58.5 55.1
10.0-135
I
ACCOUNT: PROJECT: SDG:
EMA Resources L904770
DATE/TIME:
05/03/t716:45
PAGE:
16 or 21

J ,r,,..-_�- Z _J �___) I-_ -) �`_--- ONSLA9 NATIONWIDE
CONTROL SU-�
WG975569 QUALITY MMARY
Seml Volatile Organic Compounds (GC/MS) by Method 8270D L904770.01
Method Blank (MB)
Cp
(MB) R3215006-3 05102/1712:40
MB Result
MB Qualifier MB MDL
MB RDL
2TC
Anaiyte mg8
m98
mg8 ..
1,4-0ichlorohenzene U
0.0333
0.100
aS5
2,4Dinibotoluene U
0.0333
0.100
Hexachlombeazene U
0.0333
0.100
Hexachloro-1,3-butadiene U
0.0333
0.100
4Cn
Hexachloroelhane U
0.0333
0.100
Nitrobenzene U
Pyridine U
0.0333
0.0333
0.100
0.100
s$r
2-Methylphenol U
0.0333
-0.100 -
3&4-Methyl Phenol U
0.0333
0.100
Pentachlorophenol U
0.0333
0.100
2,4,5-Trichlorophenol U
0.0333
0.100
7GI
2,4,6-Trichlorophenol. U
0.0333
0.100
(S)Nitrobenzene-05 858
10.0-126
(S)2-Fluorobtphenyf 956
22.0-127
oAI
(S)p-Teiphenyl-04 99.4
29.0-141
IS)Phenohd5 47.2
10.0-120
aSC
(S)2-Fluorophenul 59.6
10.0-120
(S)1,4,6-Tnbromophenol 86.3
10.0.153
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3215006-1 05102M 11:30 • (LCSD) R3215006-2 05/0211711:53
Spike Amount
LCS Result
LCSD Result
LCS Rec
LCSD Rec
Rec Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
Analyte
mg8
mg8
mgll
%
%
%
%
%
1,4 Ichiorobenzene
0.0500
0.0365
0.0364
73.0
72.8
26.0-120
0.310
30
2,4-Dinitrotoluene
0.0500
0.0507
0.0501
101
100
47.0427
1.21
21
Hexachlorobenzene
0.0500
0.0453
0.0441
90.6
88.2
41.0-124
2.64
-21
Hexachloro-t3butadlene
0.0500
0.0374
0.0377
74.8
75.4
26.0.120
0.800
31
Hexachloroethane
0.0500
0.0366
0.0377
73.2
75.3
22.0-120
2.93
34 -
Nitrobenzene
0.0500
0.0381
0.0390
76.2
78J
31.0-120
- 2.51
28
Pyridine
0.0500
0.0165
0.0153
33.0
30.7
10.0-120
7.45
39
2-Methylphenol
0.0500
0.0368
0.0376
73.7
75.3
26.0-120
2.17
27
3&4-Methyl Phenol
0.0500
0.0427
0.0430
85.3
85.9
27.0420
0.690
28
Pentachlorophenol
0.0500
0.0412
0.0412
82.4
82.5
20.0-126
0.0900
32
2,4,5-Tdchlorophenol
0.0500
0.0446
0.0450
89.3
89.9
44.0-124
0.730
24
2,4,6-Trichlorophenol
0.0500
0.0434
0.0444
86.7
88.8
40.0-122
2.34
24
IS) Ninobenzened5
79.7
77.8
10.0426'
-
IS)2-Fluoroblphenyl
-
92.5
91.1
220.127
(S)p-Teiphenyldl4
99.0
97.8
29.0-141
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE
EMA Resources L904770 05/034716:45 . 17 of 21

WG975569 QUALITY CONTROL SUMMARY DMEI4 NA-ria vroti.
Semi Volatile Organic Compounds (GC7MS) by Method 8270D L904770-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(1-CS) R3215006-1 05/02/1711:30 • (LCSD) R3215006-2 05/02/1711:53
Spike Amount LCSResult
LCSD Result Rec
LCSD Rec.
Rec. Limits
Analyte mgA mgA
-_LCS
mgn % -T
%
%
(5/PhenaFdS
50.2
52.0
10.0-120
(SJ 2-Fluorophenol
63.5
65.7
10.0-120
(S) g4,6-Trlbromophenol
98.1
93.8
10.0-153
L904770-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
LCS Qualifier LCSD Qualifier RPD RPD Limits
(OS) L904770-01 05/02/1713:03 • (MS) R32150064 05/02/1713:26 • (MSD) R3215006-5 05102/1713:49
Spike Amount
Original Result
MSResult
MSD Result
MS Rec
MSD Rec.
Dilution
Rec Limits
Analyte
mgn..,.
mgn
_mgn
mgn .r.._.___%
%
%
_
1,4-OiWbrohenzene
_._
0.500
..__.._
ND
0.328
0.308
65.6
61.6
1
12.0-125
2,4-Dlnitrotoluene
0.500
ND
0.478
0.489
95.5
97.9
1
30.0-156
Hexachlorobenzene
0.500
ND
OA22
OA27
84.5
85.4
1
29.0-144
Hexachlare-1,3-butadiene
0.500
ND
0.349
0.342
693
68A
1
18.0-122
Hexarhloroethane
0.500
ND
0.332
0.316
66.3
63.1
1
12.0-120
Nitrobenzene
0.500
ND
0358
0352
7L5
70.3
1
14.0434
Pyddine
0.500
ND
0.0994
0.0884
19.9
17.7
1
10.0-120
2-Methylphenol
0.500
NO
0.345
0.338
68.9
67.6
1
14.0-120
3&4-Methyl Phenol
0.500
ND
0.387
0387
77.5
77A
1
13.0-124
Pentachlorophenel
0.500
ND
OAl2
OA35
82A
87.0
1
10.0-160
2,4,5-Trichlorophenol
0.500
ND
0.432
0.441
86.5
88.2
1
15.0-160
2,4,6-Tdchlomphenol
0.500
ND
OA33
OA25
86.6
85.0
1
10.0-153
(5)N7vobenzene-6
77.6.
70.9
70.0-126
(S)2-Fluordblphenyl
95.9
87.4
22.0-127
(S)p-Terphenyl-04
101
93.9
29.0-141
(5)PhenoFdS
49.3
41.2
10.0-120
(5)2-Fluorophenol
60.3
53.9
10.0-120
13)2,4,6-Tiibromophenol
98.4
92.8
10.0.153
MS Oualifer
MSD Oualifier' RPD
6.17
2A6
1.14
1.89
5.00
132
11.7
1.99
0.110
5.46
1.93
1.91
RPD Limits
23
29
33
35
36
32
40
29
26
40
27
29
ACCOUNT: PROJECT: SDG: DATE/rIME: PAGE:
EMA Resources L904770 05/0311716:45 18 or21

( GLOSSARY OF TERMS ONELAB.NATIONWDE.
Abbreviations and Definitions
SDG
Sample Delivery Group.
MDL
Method Detection Limit.
RDL
Reported Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
U
Not detected at the Reporting Limit (or MDL where applicable).
RPD
Relative Percent Difference.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD)
from a quality control sample. The Original Sample may not be included within the reported SDG.
(S)
Surrogate (Surrogate Standard)-Analytes added to every blank, sample, Laboratory Control
Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring
recovery. Surrogates are not expected to be detected in all environmental media.
Rec.
Recovery.
jAf
Qualifier Description
it Surrogate recovery limits have been exceeded; values are outside upper control limits.
T8 Sample(s) received pastltoo close to holding time expiration.
li
i
Li
i I
i I
'J
1Cp
ZTc
3Ss
4Cn
SSr
eQC.
EAI
9Sc
ACCOUNT: PROJECT: SDG: DATHTIME:
EMA Resources L904770 05/03/1716:45
PAGE:
19 of 21

ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE.
ESC Lab Sciences Is the only emironmenlal laboratory accredited1cer0fed to support your work nationwide from one location. One phone call, one pent of contact, one laboratory. No Omer
lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capabiatyfrom our single location laboratory is comparable to the collective totals ofthe 'C
network laboratories in our industry. The most significant benefit to bur'oae location' design is the design of our laboratory campus. The model is cenduWe to accelerated productiviy, p
decreasing tumamund rime, and preventing cross contamination, thus protecting sample Integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE
Not all cerifcallons held by the laboratory are applicable to the results reported in the attached report ' 2
State Accreditations Tc
Alabama
40660 -
Nevada
TN-03.2002-34
Alaska
UST-080
New Hampshire
2975
Arizona
AZ0612
New Jersey-NELAP
TNO02
Arkansas
88-0469
New Mexico
TN00003
California
01157CA
New York
11742
Colorado
TN00003
North Carolina
Env375
Conneticut
PH-0197
North Carolina
DW21704
Florida
E87487
North Carolina °
41
Georgia
NELAP
North Dakota
R-140
Georgia'
923
Ohio-VAP
CL0069
Idaho
TN00003
Oklahoma
9915
Illinois
200008
Oregon
TN200002
Indiana
C-TN-01
Pennsylvania -
68-02979
Iowa
364
Rhode Island
221
Kansas
E-10277
South Carolina
84004
Kentucky'
90010;
South Dakota
n/a '
Kentucky'
16
Tennessee"
2006
Louisiana
A130792
Texas
T104704245-07-TX
Maine
TN0002
Texas'
LABO152
Maryland
324
Utah
6157585858
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
109
Minnesota
047-999-395
Washington
C1915
MISSISsippl
TN00003
West Virginia
233
Missouri
340
Wisconsin
9980939910
Montana
CERT0086
Wyoming
A2LA
Nebraska
NE-OS-15-05
Third Party & Federal Accreditations
A2LA-ISO 17025
1461.01 -
AIHA-IAP,U-C 100789
A2LA-ISO 17025'
1461.02
DOD 1461.01
Canada
1461.01
USDA S-67674
EPA-Crypto
TN00003
`Drinking Water LUnderground storageTanks ' Aquadclexlclty 'ChemimtrMicrobeloglcal 'Mold NAccreditation not applicable
Our Locations
ESC Lab Sciences has silty -four client support centers that provide sample pickup andfor the delivery of sampling supplies. Ifyou would like assistance from one of our support offices, please
contact our main office. ESC Lab Sciences performs all testing at our central laboratory.
$ WA
MT NO
T ID SO
WY
M/ T NE
UT Q CO
KS
T�
ACCOUNT:
.EMA Resources
NM O�
T TJC T
T
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HI
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ZAN
T WI
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IA T T PA
T IL Ip OH VJI/
MO VA
NT
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SDG: DATERIME
L904770 05/03A716:45
PAGE
20021

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
;i
Facility Name: Smithfield Fresh Meats Corp. WQ Permit Number: W00014868
V#/WTP Name: Tarheel W WTP NPDES Number: NCO078344
Monitoring Period: From 4/25/2017 To 4/25/2017
Pathogen Reduction (15A NCAC 02T .1100) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑ 1 Alt B (Alk Treatment) ❑ Alt. C (Prior Testin )❑
Alt.D (No Prior Test) ❑ Process to Further Reduce Patho ens ❑
''
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑ Thermo hilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
JAIt. (1) Fecal Density El
Alt. (2) Process to Significantly Reduce Patho ens ❑
If applicable to alternative performed (Class$ only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑ I
Aerobic Digestion ❑
Anaerobic Digestion ❑
;:::;::r:>.":it3[EtE i'::E<
If applicable to alternative pe med (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
um ero
Excee
Frequency
of Analysis
Sample
'type
Analytical
Tech-nique
im
Geo. Mean
aximu
Units
Fecal Coliform
2 x to to the
6th power
per gam of
total solids
MPN
680
931
1356
MPN/G
0
Quarterly
G
SM92210E-
2006
CFU
1000 mpn per gram
of total solid (dry'
weight)
Salmonella bacteria
(in lieu of fecal
wliform)
3 MPN per 4 grams
total solid (dry
weight)
Veetnr Attraetinn Rednetion f15A NCAC 02T .11071- Please indicate alternative performed:
Alt.1 (VS reduction)
El
Alt. 2 (40-day bench) [I,
Alt. 3 (30-day bench) El Alt. 4 (Spec. OZ uptake)
❑
Alt. 5 (14-Day Aerobic)
[IAlt.
6 (Alk. Stabilization El
Alt 7 (Drying - Stable) El JAR. 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
El
]Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were erformed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
re uirements.)
This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment"
Dwayne Russ - ORC Brent Collins; Director of Technical Services
Preparer Name and itle (type or print) Land Applier Nam Ti�if.applicable)(type or print)
f y '9, 2/6/2018
Signature of Preparer* Date Signature of Land Applier (if applicable) , Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
j�
i
Facility Name: Smithfield Fresh Meats Corp.
WWTPName: Tarheel WWTP
Monitoring Period: From` 6/16/2017 To
WQ Permit Number: W00014868
NPDES Number: NCO078344
6/16/2017
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/tem) ❑ 1
A1tB (Alk Treatment) ❑
Alt. C (Prior Testing)❑
f
ix
AIt D (No Prior Test) ❑
Process to Further Reduce Patho en ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 111
Heat Drying ❑
Heat Treatment ❑
Thermo hilic ❑
"
Beta R'
❑
Gamma Ra ❑
Pasteurization ❑Ray
_
Class B:
Alt. (1) Fecal Density El
I Alt. (2) Process to Significantly Reduce Pathogens ❑ 17777,777
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
1 Aerobic Digestion ❑
Anaerobic Digestion
st on ❑
If applicable to alternative performed Class A or Class B) complete the followin
monitor' g data:
Parameter
Allowable Level
Pathogen Density
NUMDer °
Excee- '
Frequency
Sample
Analytical
'nim
Gen. Mean
axim
Units
Sludgein
of Anal sis
y
Type
Tech-ni ue
q
z x to to the
MPN
755
813
870
MPN/g
0
Quarterly
G
SM-
6thpower
2006
006
per gram of
Fecal Coliform
total solids
CFU
1000 mpn per gram
of total solid (dry
Wei t
Salmonella bacteria
3 NTN per 4 grams
(in lieu of fecal
total solid (dry
coliform)
wei t
Vector Attraction Reduction (15A NCAC 02T .1107) -Please indicate alternative performed:
Alt.l (VS reduction) El
Alt. 2 (40-day bench) ❑
jAlt. 3 (30-day bench) El
jAlt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
1Alt 7 (Drying - Stable) 111
Alt. 8 (Drying -Unstable) ❑
Alt. 9 (Injection) ❑
JAIL 10 (Incorporation) ❑
INo vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
"This determination has been made under my direction and supervision in accordance, with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Dwayne Russ - ORC Brent Collins; Director of Technical Services
Preparer Name an Title (type or print) Land Applier Name and Title(ifapplicable)(type or print)
tat 1 —il ^j' 2/6/2018
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) , ,
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
I
f
.t
j
Facility Name: Smithfield Fresh Meats Corp.
W WTP Name: Tarheel W WTP
Monitoring Period: From 10/25/2017 To
WQ Permit Number: W00014868
NPDES Number: NCO078344
10/2512017
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/tent) ❑ I
Alt (Alk Treatment) ❑
Alt. C (PriorTestin )❑
A1t.D (No Prior Test) El
Process to Further Reduce PathogenPathogengs El
If applicable to alternative performed (Class A only) Indicate "Process to Further Reduce Pathogens":
Compost ❑
I Heat Drying ❑
I Heat Treatment ❑
Thermo h c ❑ " ;
Beta Ra ❑
I Gamma Ra ❑
Pasteurization ❑
-
Class B:
lAlt. (1) Fecal Density El
I Alt. (2) Process to SignificantlyReduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑ I Composting ❑ lAerobic
Digestion ❑
Anaerobic Diestion 11If
applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Allowable Level
Pathogen Density
um er oFrequency
Sample
Analytical
Parameter
in Sludge
Excee
of Analysis
Type
Tech -pique
inim
Geo. Mean71235
u
Units
2 x 10 to the
MPN
952
1062
MPN/G
0
Quarterly
G
SIvI9206
6th power
2006
per gram of
Fecal Coliform
total solids
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacterial
3 WN per 4 grams
(in lieu of fecal
total solid (dry
coliform
weight)
Vector Attraction Reduction (15A NCAU UTI .IIU7) - Please indicate alternative performed:
Alt.1 (VS reduction) El
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) El
Alt. 4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
JAR. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
JAR. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑ ]Alt.
10 (Incorporation) ❑
No vector attraction reduction alternatives were erformed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the.
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
"This determination has been made under my direction and supervision to accordance wtm ine system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am, aware that there are
significant penalties for false certification including fine and imprisonment."
Dwayne Russ - ORC Brent Collins; Director of Technical Services
Preparer, (me and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
2/6/2018
Signature of Preparer* DateSignature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Smithfield Farmland - Tar Heel
ANL Volatile Solids In
Month-
'DAFEE6
tssmigfl
.. mgll'
DAFEc
jTvSS mg/IP,
_ _ mgll_
Digesterin
Volatile Solids+%
Jan 2017...
- 40,700
`_ 47,200
- 93--
Feb 2017
47,750
44,500
93
Mar 2017
_ 57,550
54,450
_ - 95
Apr 2017
56,300
52,375
93
May 2017
.. _. 50.600
46;700
_. _ 92,
Jun 2017
56.600
52,225
92
Jul 2017.
-_ 7,2,800
68,025
:- 93
Aug 2017
59,975
66,526
94
Sep 2017
_ _ +56,650
_. 53,950
' ;-_ `__`95
Oct 2017
50,100
46,550
93
Noy 201_7
53,700
. 50,400
' - 94
Dec 2017
55,100
53,975
98
Minimumi
47;750
72,800
4'4i500
68,025
Maximum
Total _
_-667,825
626;875
52,240
96
Average
55,652

Volatile Solids Out
Volatile Solids IN average
% Reduction
3/31/16 North
76.36
96
86.54
4/21/16 South
77.64
96
85.53
4/21/16 North
72.72
96
88.89

Analytical Results
EMA Resources, Inc.
755 Yadklnvlile Rd.
Mocksville, NC 27028
Receive Date:
04212017
Reported:
04/2612017
For:
Smithfield TarHeel
Comments:
Geometric Mean 931 MPNIg
Sample Number
Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
170425-09-01
Fecal Coliforms
1
680
MPNIg
Sh192210E•2005
04/25/2017
WC
170425.09-01
Percent Solids
1
2.94
%
SM2540eA997
04125/2017
WC
170425.09-02
Fecal Coliforms
2
1356
MPNIg
sm9zzlcE.zoos
04/2512017
WC
170425-09-02
Percent Solids
2
2.95
odd
SM2549e-1997
04/2512017
WC
170425-09-03
Fecal Coliforms
3
<722
MPNIg
SM92210E- ON
0412512017
WC
170425-09-03
Percent Solids
3
2.77
ova
SM25d98-1W
04/2512017
WC
170425-09.04
Fecal Coliforms
4
1238
MPNIg
SM92210E-2000
04/25/2017
WC
170425.09-04
Percent Solids
4
3.23
%
51115OSA997
04/25/2017
WC
170425-09.05
Fecal Coliforms
5
<735
MPN/g
sm9m1cE-l006
04125/2017
WC
170425.09-05
Percent Solids
5
2.72
%
SM2540a-1997
04/25/2017
WC
170425-09.06
Feral Coliforms
6
781
MPNIg
8M92]10E-M
04125/2017
WC
170425-09-05
Percent Solids
6
2.56
%
SWUOs-1997
04/2512017
WC
170425-09-07
Fecal Coliforms
7
1286
MPN/g
. SM92210E-M
04/25/2017
WC
170425-09-07
Percent Solids.
7
3.11
%
BW6408.1997
04/25/2017
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 170425-09-01 Temp on Arrival: 3
Parameter Schedule: Percent Solids
i
Received on Ice
Parameter Schedule:
Fecal Collforms
i Sodium Thiosulfate
Received on Ice
Sample Number 170425-09-02 Temp on Arrival: 3
f
I Parameter Schedule:
Percent Solids
Received on Ice
-1 Parameter Schedule:
Fecal Coliforms
_i Sodium Thiosulfate
Received on Ice
i
Sample Number 170425-09-03 Temp on Arrival: 3
Parameter Schedule:
Percent Solids
Received on Ice
Parameter Schedule:
Fecal Collforms
Sodium Thlosulfate
Received on Ice
Sample Number 170425-09-04 Temp on Arrival: 3
Parameter Schedule:
i
Percent Solids
Received on Ice
Parameter Schedule: Fecal Collforms
Sodium Thiosulfate Received on Ice
j Sample Number 170425-09-05 Temp on Arrival: 3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Collforms
i Sodium Thiosulfate Received on Ice
Sample Number 170425-09-06 Temp on Arrival: 3
i
PO Box 228 • Statesville, NC 28687.704/872/4697
Page 2 of 4

_I
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 170425 09-07 Temp on Arrival: 3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Pago 3 of 4

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Analytical Results
I EMA Resources, Inc.
755 Yadkinville Rd.
—� Mocksville, NC 27028
Receive Date:
06/16/2017
Reported:
0611912017
For:
Smithfield Tarheel
Comments:
Geometric Mean <813 MPN/g
Sample Number
parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
170616-02-01
Fecal Coliforms
1
<840
MPN/g
SM92210E-2006
0611612017
WC
W0616-02-01
Percent Solids
1
2.38
%
SM2540B-1997
06/16/2017
WC
170616-02-02
Fecal Coliforms
2
<813
MPN/g
BM92210E-2006
06116/2017
WC
170616-02-02
Percent Solids
2
2.46
%
5Al2S4°s'1997
06/16/2017
WC
170616-02-03
Fecal Coliforms
3
<755
MPNIg
SM92210E-2008
0611612017,
WC
170616-02-03
Percent Solids
3
2.65
%
SM25400.1997
0611612017
WC
170616-02-04
Fecal Coliforms
4
<870
MPN/g
SM92210E-2005
06/16/2017
WC
170616-02-04
Percent Solids
4
2.30
%
SN125408-1997
06116/2017
WC
170616-02-05
Fecal Coliforms
5
<840
MPN/g
SM92210E-2006
0611612017
WC
170616-02-05
Percent Solids
5
2.38
%
SM2540B-19W
06/16/2017
WC
170616-02-06
Fecal Coliforms
6
<794
MPN/g
SM92210E-2006
06/16/2017
WC
170616-02-06
Percent Solids
6
2.52
%
SM2540B.1097
06/1612017
WC
170616-02-07
Fecal Coliforms
7
<784
MPN/g
SN192210E-2006
06/1612017
WC
170616-02-07
Percent Solids
7
2.55
%
SM2540B-1997
06/16/2017
WC
Respectfully submitted,
Dena Myers
NC Cart #440,
NCDW Cert#37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687.704/872/4697
Page 1 of 1

Contact Person:
Phone #
Chain of
Custody Record
PI* '5dtcr Requisitioned by: (Time umei
customer
Tinto Sampled
wEs bampled
Mstrl�
Parameters requested for analysIs
Received by:
Au
Relinquished by:
Time — am, pm Date
Holding times meet--:
Received by:
Time am, pm Date _j__J—
Compliance work:
Composite Sampling
#1:
Time begin_
am. prn Date
Non-compliance work:
Time end_am,
pm Date
Lab Comments:
Time begin—
am, pm Date
Time end —am,
pm Date
^~

Analytical Results
EMA Resources, Inc.
755 Yadkinville Rd.
L
I� Mocksville, NC 27028
4
-
Receive Date:
10125/2017
Reported:
10/26/2017
1
,
For:
Smithfield Tar Heel
Comments:
Geometric Mean <1062 MPNIg
- Sample Number
Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
171025-12-01
Fecal Coliforms
1
<1064
MPN/g
SM92210E-2005
10/2512017
WC
171025-12-01
Percent Solids
1
1.88
0/,
SM2540B-1997
10125/2017
WC ,
177025-12.02
Fecal Coliforms
2 ,
<1156
MPN/g
' SMSUICE-2006
10126/2017
WC
171025-12-02
Percent Solids
2
1.73
%
SM2540B-1997
10125/2017
WC
171025-12-03
Feral Coliforms
3
<995
MPN/g,
SMMICE-2006
1012512017
WC
171025-1243
Percent Solids
3
2.01
%
SM2540B-1997
10/25/2017
WC
171025-12-04
Feral Coliforms
4
<1000
MPN/g
SM92210E-2006
-10/25/2017
WC
171025-12-04
Percent Solids
4
2.00
%
SM2540B-1997
10/25/2017
WC
171025-12-05
Fecal Coliforms
5
<1058
MPN/g
SM92210E-2006
10/25/2017
WC
171025-12-05
Percent Solids
5
1.89
%
SM2540B-1997
10125/2017
WC
171025-12-06
Fecal Coliforms
6
<1235
MPN/g
SM92210E-2006
1012512017
WC
- 171025-12-06
Percent Solids
6
1.62
%
SM254OB-1997
10/25/2017
WC
,-_ 171025-12-07
Fecal Collfonns
7
<952
MPN/g
SM92210E-2006
1012512017
WC
171025-12-07
Percent Solids
7
2.10
%
SM25408-1997
10125/2017
WC
Respectfully submitted,
I�
Dena Myers
NC Carl #440,
NCDW Cert #37755,
EPA #NC00909
i'
PO Box 228 • Statesville, NC,28687 • 704/87214697
Page 1 of 4

Condition of Receipt
Sample Number 171025-12-01 Temp on Arrival: 2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab•
Sample Number 171025-12-02 Temp on Arrival:.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Collforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab.
Sample Number 171025-12-03 Temp on Arrival: 2
Parameter Schedule: Percent Solids
Received on Ice
i Parameter Schedule: Fecal Coliforms
ii
- Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
i
Sample Number 171025-12-04 Temp on Arrival: 2 .
Parameter Schedule: Percent Solids
Received on Ice
,t
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab .
Sample Number 171025-12-05 Temp on Arrival: 2
Parameter Schedule: Percent Solids
Received on Ice
i PO Box 228 • Statesville, NC 28687 o 704/872/4697
Page 2 of 4
1 I -

i I
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
i Sample Number 171025-12-06 Temp on Arrival: 2
I_
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 171025-12-07 Temp on Arrival: 2
Parameter Schedule: Percent Solids
- Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC286B7 • 704/872/4697
Page 3 of 4
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Page 1 of 1
Report No. 17-171-0501 to 7621 Whitepine Road, Richmond, VA 23237
Account No: 46245 Waypoi ■■Y■ t, Main 804-743-94016 Fax [phone]
��II ANALYTICAL www.waypointanalytical.com
Advisor: EMA Resources Inc Client: Steve Dunham Farm to: SF03
755 Yadkinville Road
Mocksville NC 27028 Date Received: 06/20/2017
Date of Report: 06/21/2017
Lab No Reid ID
Sample ID
Soft Class
HM%
WN pH
Ac
P-I
K-1
S-1
Mn4
Zn4
Zn-AI
Cu-1
CEC
BS%
Ca%
Mg%
ESP
Na
SS-1 NO3 N
06221
1
MIN
1.1.
6.5
0.5
287
20
12
150
1095
1095
200
6.2
92
76
13
1.3
0.1
Comment:
Test result units = CEC and Na in meg/10gcm3; NO3-N in mgldm3; WN in g/cm3
North Carolina Division of Water Quality Certification 9257, Analysis and fertility recommendations shown on this report are pedormed in accordance within NCOA guidelines, Analysis prepared hy. W aypoint Analytical Virginia, Inc.

Page 1 of 1
Report No: 17-361-0537
Account No: 46245
Advisor: EMA Resources Inc
755 Yadkinville Road
Mocksvllle NC 27028
o
Waypoint_
ANALYTICAL
Client: William Dunham
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 a Fax [phone]
www.waypointanalytical.com
Farm ID/Name: SF03
'Date Received: 12/27/2017
Date of Report: 01/02/2018
Lab No Field /D
Sample ID
Soil Class HM% WN
pH
Ac
P-1
K-1
S-1
Mn-I
Znd
Zn-AI
Cu-1
CEC
BS%
Ca%
-Mg%
ESP
Na
SS-1 ND3 N
07072
2
MIN
5.9
0.7
469
36
40
69
1068
1068
520
4.1
82
57
18
2.4
0.1
12
07073
3
MIN
5.7
0.6
368
25
31
63
800
800
395
2.9
80
57
16
2.7
0.1
10
07074
4
MIN
6.5 _
0.4
107
9
8
56
230
-230
55
4.9
91
70
19
1.1
0.1
6
07075
5
MIN
5.8
0.7
427
26
15
69
980
980
465
3.9
82
58
17
2.9
0.1
11
Comment:
Test result units = CEC and No in megllixi=3; NO3 N in mg/dm3; WN in g/om3
North Carolina Division of Water Quality Certification #257, Analysis and fedility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by. Waypoint Analytical Virginia, Inc.

Page 1 of 1
Report No: 1462450502 Waypoi nt, 7621 Main
80 -7 Road, Richmond, 27 23237
-6446
Account No: 46245 � Maln 804-743-9401 °Fax [phone]
ANALYTICAL www.waypointanalytical.com
Advisor: EMA Resources Inc Client: J.F Burney Farm ID: SF07
755 Yadkinville Road
Mocksville NC 27028 Date Received: 06/20/2017
Date of Report: 06012017
Lab No Fleld lD
Sample ID
Sol! Class
HM%
WN pH
Ac
P-1
K-1
S-1
Mn-I
Zn4
Zn-Al
Cu-1
CEC
BS%
Ca%
Mg%
ESP
Na SS-1 NOS N
06222
6
M-0
3.6
6.6
1.0
590
199
60
481
1850
2313
1055
162
94
74
13
1.0
0.2
06223
8
MIN
1.9
6.4
1.1
456
36
37
' 331
1855
1855
695
12.7
92
84.
6
0.8
6.1
06224
9 _
MIN
0.8
5.6
1.2
533
63
19
175
1328
1328
720
4.7
75
57
9
1.8
0.1
06225
14
MIN
1.1
5.7
0.8
219
9
8
75
848
848
225
3.9
81
67
12
1.2
0
Comment:
Test result units = CEC and Na in meg/taocm;; NC3 N in mg/dm3; W1vin g/cm3
North Carolina Division of Water Quality Certification N257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared oy. Waypoint Analytical Virginia, Inc.