HomeMy WebLinkAboutWQ0014452_2017 Annual Report_20180215Town of Bladenboro, NC
RESIDUALS LAND APPLICATION PROGRAM
Perffiit No. WQ0014452
2017 ANNUAL REPORT
a
Town of Bladenboro, NC
Residuals Land Application Program
2017 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms, Residuals Analysis,
& SAR Calculation Page
3. Annual Land Application field Summary Forms
4. TCLP Analysis
5. Pathogen ReductionNectgr Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses
ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00014452 County Bladen Year 2017
Facility Name (as shown on permit) Bladenboro W WTP NPDES No. NCO026352
Land Application Operator, Svnaero Phone# (336) 998-7150
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X 'YES NO. NNO, skip Part A, and Part Band proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A —Residuals Application Summary:
Total number of application fields in the permit: 4 .
Total number of fields utilized for land application • during the year: 2
Total amount of dry tons applied during the. year for all application sites: 25.43
Total number of acres utilized. for land application during the year: 16
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2017 with all conditions of the land application permit (including but not limited to
items 1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates,. and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified is the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory resultsare attached. - '
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached. I
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .I 105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities). 1
8. All monitoring and reporting requirements in• 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations' and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at monitoring well or explanations of violations are
attached to include appropriate actions and remediatioas.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified'
in the permit
12. No runoff of residuals from the application 'sites onto adjacent property or nearby surface watershas occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations." '
2uRA6 P. Mr-Y-I, Z� M -TL
Permittee Name and Title (type or print)
Signature of Preparer* Date
(if different from Permittee)
_k'U�on K-1_ JGtCltc>Ut 15^t8
Signature ofPe ri Date
SignatMe of Land App rDate
(if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)
2017 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION
BLADENBORO,NC
BLADENBORO, NC AEROBICALLY DIGESTED LIQUID
MONTHNEAR
December 2017
YEARLY TOTAL
DRY METRIC
AMOUNT UNIT DRY TONS UNIT TONS
204,600.00 G 25.43 D 23.06
204,600.00 G 25.43 D 23.06
2/8/2018
ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0014452
Facility Name: BLADENBORO, NC
NPDES# : NCO026352
or WQ# (residual only)
WWTP Name: BLADENBORO
Residuals Analysis Data
Product Type
AEDLIQ
Date Sampled (grab) or 11/13/17
Date Composited
Percent Solids
2'. 98
PARAMETERS (mg/kg dry weight)
Arsenic
4.02
Cadmium
<2
Mercury
0.497
Chromium
84.5
Copper
435
Lead
24.6
Molybdenum
<5
Nickel
41.1
Selenium
<5
Zinc
556
Total Phosphorus
14300
TKN
42800
Ammonia -Nitrogen
9700
Nitrate and Nitrite
99
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this'document was prepared under my direction or'supervision in accordance with a system
designed to as urg;tjat qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant pea r suboitting false information, including the possibility of fines and imprisonment for knowing violations."
Date
DENR FORM RSSF (5/2003) Printed: Thursday- February 8 2018 at 16:54:41 for: 2004 01
ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0014452
Facility Name: BLADENBORO, NC
NPDES# : NCO026352
or WQ# (residual only)
WWTP Name: BLADENBORO
Residuals Analysis Data
Product Type AEDLIQ
Date Sampled (grab) or _ 11/13/17
Date Composited
Percent Solids 2.98
PARAMETERS (mg/kg dry weight)
Aluminum
7520
Calcium
13600
Magnesium
1590
pH
7.69
Potassium
1800
Sodium
710
"I certify, under
designed to
significant p n6
Fq
Laboratory
Waypoint Analytical Virginia Inc.
ilty of law, that this document was prepared under my direction or supervision in accordance with a system
:hat qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
for sub/nitting false information, including the possibility of fines and imprisonment for knowing violations."
NR - Data Not Reported or Data Not Required
Date
DENR FORM RSSF-B (7/2002) Printed: Thursday - February 8. 2018 at 16:55:05 for: 2004 01
Page: 1 of 2
Report Number: 17-318-0203
Account Number: 46437
Send To: Synagro Central LLC/ Bladenboro
Marshal Puryear
284 Boger Road
Mocksville , NC 27028
Lab Number: 57101
Sample Id : bladenboro wwtp
Waypoint.
(D
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Project: Bladenboro W WTP
REPORT OFANALYSIS
Date Sampled: 11/13/2017 11:30:00
Date Received: 11/14/2017 00:00
Date Reported: 11/21/2017
Total Solids
2.98
29800
100.0
JM
11/14/201715:00
SM-2540G
Moisture'
97.01
_
.100.0
JM
11/14/201715:00
SM-254OG
Total Kjeldahl Nitrogen
428
42800
50.0
R D
11/15/2017 08:30
SM-4500-NH3C-TKN
Total Phosphorus
1.43
14300
100
MOS
11/15/2017 15:34
6010C
Total Potassium
0.18
1800
100
MOS
11/1612017 12:34
6010C
Total Sulfur
0.78
7800
100
MOS
11/15/2017 15:34
6010C
Total Calcium
1.36
13600
100
MOS
11/15/2017 15:34
6010C
Total Magnesium
0.16
1590
100
MOS
11/15/2017 15:34
6010C
Total Sodium
0.07
710
100
MOS
11/15/2017 15:34
6010C
Total Iron
14300
100
MOS
11/151201715:34
6010C
Total Aluminum
7520
100
MOS
11/16/2017 12:34
6010C
Total Manganese
145
5.00
MOS
11/15/2017 15:34
601OC
Total Copper
435
5.00
MOS
11/15/2017 15:34
601OC
Total Zinc
556
5.00
MOS
11/15/2017 15:34
6010C
Ammonia Nitrogen
0.97
9700
50.0
R D
11/15/2017 08:30
SM-4500-NI3C
Organic N
3.31-
33100
50.0
11/15/2017 08:30
CALCULATION
Nitrate+Nitrite-N
99.0
2.37
MMT
11/16/201714:45
450ONO3F-2011
All values are on a dry weight basis except as noted
by asterisk.
Detection limit on all N series
is on a wet basis.
�«
Ourrepons and letters am forthe exclusive and cnnfidenliel use of ourclienfs, and
may not be reproduced In whole organ, normay any reference be made
to the work, the results, orthe company in any advedising, news release, orotherpublic announcements without obtaining ourpdorwritten authorization. ,
Pauric McGroary
Agronomist
Page: 2 of 2
Report Number: 17-318-0203
Account Number: 46437
Send To: Synagro Central LLC/ Bladenboro
Marshal Puryear
284 Boger Road
Mocksville , NC 27028
Lab Number: 57101
Sample Id : bladenboro wwtp
Waypoint..
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 a Fax 804-271-6446
www.waypointanalytical.com
Project: Bladenboro W WTP
REPORT OFANALYSIS
Total Cadmium
<2.00
Total Chromium
84.5
Total Nickel
41.1
Total Lead
24.6
Total Arsenic
4.02
Total Mercury
0.497
Total Selenium
<5.00
pH `
7.69
Total Volatile Solids
45.33 _ 453300
Total Molybdenum
<5.00
Comments:
NC CERT#257, SC CERT#9300 7001
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
Date Sampled: 11/13/2017 11:30:00
Date Received: 11/14/2017 00:00
Date Reported: 11/21/2017
2.00
MOS
11/15/201715:34
6010C
5.00
MOS
11/15/201715:34
6010C
5.00
MOS
11/15/201715:34
6010C
5.00
MOS
11/15/201715:34
6010C
3.00
MOS
11/15/201715:34
6010C
0.400
SJB
11/20/201710:51
SW-7471B
5.00
MOS
11115/201715:34
6010C
1.00
R D
11/15/2017 08:30
SW-9045D
100.0
JM
11114/201715:00
SM-2540G
5.00
MOS
11/15/201715:34
6010C
All values are on a dry weight basis except as noted by.aster sk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any mfemnce be made
to the wodr, the results, or the company in any advertising, news release, or otherpublic announcements without obtaining ourpnor written authodution.
Pf« AV Ga°"�
Pauric McGroary
Agronomist
Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
2004-01-AEDLIQ-NC BLADENBORO, NC AEROBICALLY - • 11/13/2017 1/112017-12131/2017 0:2644
DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) +100 = (710.x 2.9800) + 100 = 21.158
Ca mg/I = (Ca mg/kg x % Solids) + 100 = (13600 x 2.9800) 100 = 405.28
Mg mg/l = (mg mg/kg x % Solids) + 100 = (1690 x 2.9800) + 100 = 47.382
Na meq = Na mg/I + Molec.Wgt.Na = 21.158 + 23 = 0.919913
Ca meq = Ca mg/I + Molec.Wgt.Ca = 405.28 + 20 = 20.264
Mg meq = Mg mg/I--+ Molec.Wgt.Mg = 47.382 + 12 = 3.9485
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 0.919913 + SgrRoot[0.5(20.264+3.9485)] = 0.264388 .
Printed: 2/8/2018
Page 1 16:56
f�
ACILITYNAME: BLADENBORO,NC
)WNER: TOWN OF BLADENBORO
iITE #: NC BL 00003 FIELD# : BL 00003 0003
3ESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIE LD SUMMARY FORM
PREDOMINANT SOIL SERIES: GOLDSBORO
PERMIT #: W00014452 ANNUAL DRY TONS APPLIED: 10.02
OPERATOR: TOWN OF BLADENBORO CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 6.10 ACRES PERMUTED: 6.10
Page: 1
Lime Applied
Date iLbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
"�"
Tons
Cond.
Precip.
cation
till-
all-
Ammonia
Nitrate
PAN
DATE or
Solids
pet
Residual
DWet,
Dry,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pp m)
Crop
p
Total
MONTH
Per Acre
1215/17
80,600.00 (G)
13213.115
2.98
1.642
BLAEDL
DRY
0-<I/2"
SUR
0.5
0.30
42,800.p
9,700.00 p
99.00 p
14879
WHEAT
Dec-17
80,600.00 (G)
13,213.115
Total Gallons/Ac: 13,213.11
As
Cd
Cr
Cu
Pb
Fig
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annual lbs/acre
49
0.013
0.007
0.277
1.428
0.081
0.002
0.016
0.135
0.016
1.826 46.96
Cumulative lbs/acre
0.139
0.067
3.346
19.126
1.009
0.034
0.167
1.551
0.161
23.164
'emit PAN Limit (lbs/acre) 1st Crop/2nd Crop
r "'''
J
'
M 1 i M
t
Ill.
136
c'�
FD Cumulative Pollutant Loading Rate Limit (lbs/nre)
36.6
34.8
r an
1339.0
267.9
15.0 375.0
89.0
2500.0 !
! l
BLAEDL = BLADENBORO, NC AEROBICALLY DIGESTED LIQUID
X a 2 Z15I$
(SIGNATURE OF LAND APPLIER) - DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppm or mgdrg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
° Application Method: SUR-Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018
FACILITYNAME: BLADENBORO,NC
JWNER: TOWN OF BLADENBORO
81TE #: NC BL 00003 I =# : BL 00003 0004
RESIDUAL SOURCE(S) * See list at bottom of report
0
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GOLDSBORO
PERMIT#: W00014452
OPERATOR: TOWN OF BLADENBORO,
ANNUAL DRY TONS APPLIED: 15.41
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 9.90 ACRES PERMITTED: 9.90
Page: 1
Lime Applied *•*
Date Lbs/Ac
jallons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (VM (specify)
^/o
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
.MONTH
Solids
Per
Residual
'Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
Total
Per Acre
12/4/17
124,000.00 (G)
12525.253
2.98
1.556
BLAEDL
- DRY
0- 1/2"
SUR
0.5
0.30
42,800.p
9,700.00 p
99.00 p
14879
WHEAT
Dec-17.
124,000.00 (G)
12,525.253
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
46
0.013
0.006
0.263
1.354
0.077
0.002
0.016
0.128
0.016
1.731
44:51
Cumulative lbs/acre
0.300
0.041
2.243
12.215
0.682
0.021
0.102
1.000.
0.113
15.077
t
]r
,emit PAN Limit (lbs/acre) 1st Crop2nd Crop
;
t
, ,� '(
t: t
�.
` f
l -
136
J
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34 8
1339.0
267.9
""f a" 'i
15.0 �„
375.0
89.0
2500.0
DDD
BLAEDL = BLADENBORO, NC AEROBICALLY DIGESTED LIQUID
x
(SIGNATURE OF LAND APPLIER) DATE
- "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A=Not Applicable NR=Not Reported or Not Required .%=percent p=ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR- Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018
��
EPR9agN1dENYALiE6a0.+OlAefE5, lN0
hrtalptical fabetatorles
November 28, 2017
Chad M. Hayes ,
Synagro
284 Boger Rd.
Mocksville; NC 27028
TEL: (336) 998-7150
FAX: (336) 998-8450
RE: Bladenboro WWTP
Dear Chad M. Hayes:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX.- (330) 253-4489
Websht: httn://www:settekcom
Order No.: 17110701
Summit Environmental Technologies, Inc. received 1 sample(s) on 11/14/2017 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.'
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St:,
Cuyahoga, Falls, Ohio 44223
Arkansas 88-0735, Califomia 07256CA, Colorado, Comecticut PH-0108, Delaware, Florida NELAC E87688, GeorgiaE87688, Idaho 01100923, Illinois
200061, Indiana C-011-13, Kaasss E-10347, Kennmky (Underground Storage Took) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Miaresota
409711, New Hampshire 2996, New Jersey 011006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Oklahoma 9940, Oregon
OH2O0001, Rhode Island LA000317, South Carolina 92016001, Texas TI047044664 1-5, Utah OH009232011-1, Virginia 00440 and 1591, Washington
C991
Page 1 of 36
"y
Summit Environmental Technologies, Inc. Case Narrative
ui iur 3310 Win St. 1\
RMIRONWENTALTECBNOLOCIES, INC-. CayahogaFalls, Ohio 44223 WO#: 17110701
AnalyBcal Laboratories TEL: (330) 253-8211 FAX: (330),253-4489
Website: haol/www.settekemn Date: 11/2S/2017
CLIENT: Synagro
Project: Bladenboro WWTP
WorkOrder Narrative:
17110701: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit EnvironmentalTechnologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not certified."
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
t� Summit Environmental Technologies, Inc. or the customer for which this report was issued.' The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units. .
This report is believed, to meet all of the requirementsof the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
WorkOrder Comments:
17110701: Sample Receipt Temperature= 5.8°C
Analytical Sequence Sample Notes:
17110701-001A SVOC-BNA_TCLP(8270): The BNA 8270 CCV (Batch R77398) exhibited high
recoveries for several analytes and low recovery for Surrogate: Phenol-d6; Associated samples are ND
for all analytes of interest.
17110701-001a tclp-svoc-epest_tclp(8081): TCLP Pesticide Sample MS and MSD pair exhibited high
RPDs for all analytes of interest.
Original
Page 2 of 36
U I T Smmait Environmental Tec3310 haolWS. Case Narrative
10 win st.
MVIRONMENTAL ISCMOLOGI'cS, 19C. Cuyahoga Falls, Ohio 44223 wo#: 17110701
Anaiytica! Laboratories TEL: (330) 253-8211 FAX.. (330) 253-4489
website: huoda� /wv.seaekcom Date: 11/28/2017
CLIENT: Synagro
Project: Bladenboro WWTP
Analytical Sequence QC Notes: .
NM-29700 SVOC-BNA_TCLP(8270): The BNA TCLP Method Blank (Batch 29700) exhibited high
recovery for Surrogate: Nitrobenzene-d5; the MB is ND for all analytes of interest.
LCS-29700 SVOC-BNA_TCLP(8270): The BNA TCLP LCS (Batch 29700) exhibited low recovery for
Phenol-d6; All analytes of interest exhibited recoveries within acceptance limits.
17110701-00IAMS SVOC-BNA TCLP(8270): The BNA TCLP Sample MS exhibited low recovery
for Phenol-d6; All analytes of interest exhibited recoveries within acceptance limits.
17110701-OOIAMSD SVOC-BNA_TCLP(8270): MSD not reported due to Internal Standard failing
Original
Page 3 of 36
� w Summir Environmental Technologies, In Qualifiers and Acronyms
3310 /owms
`
ENVIROMMENTALTECHUCLOCIZ5,
INC. Cuyahoga Falls, Ohio 4422 WO#: 17110701
Analytical I aborstorfes TEL: (330) 253-8211 FAX.- (330) 253-445
•
Website: hup.-lAvlvtv.settek.co. Date:. 11/28/2017
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers •-
" U
The compound was analyzed for but was not detected.
J
The reported value is greater than the Method Detection Limit but less than the Reporting Limit: ,
H .
The hold time for sample preparation and/or analysis was exceeded. ,
D
The result is reported from a dilution. '
E
The result exceeded the linear range of the calibration or is estimated due to interference.
MC
The result is below the Minimum Compound Limit. -
*
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in
Manual integration was used to determine the area response. -
' it •
Manual integration in which peak was deleted
N
The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P
The second column confirmation exceeded 25% difference.
C
The result has been confirmed by GC/MS.
X
The result was not confirmed when GC/MS Analysis was performed
B/MB+
The analyte was detected in the associated blank
G
The ICB or CCB contained reportable amounts of analyte. - .
QC-/+
The CCV recovery failed low (-) or high (+). '
R/QDR
The RPD was outside of accepted recovery limits.
QL-/+
The LCS or LCSD recovery failed low (-) or high (+).
QLR
The LCS/LCSD RPD was outside of accepted recovery limits. •,
QM-/+
The MS or MSD recovery failed low (-) or high (+).
QMR
The MS/MSD RPD was outside of accepted recovery limits. .,
_
QV-/+
The ICV recovery failed low (-) or lrigh (+). -
° • S
'�
The spike result was outside of accepted recovery limits..
.
Z
Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected RL Reporting Limit
QC
Quality Control MDL Method Detection Limit
MB
Method Blank LOD Level of Detection _
LCS
Laboratory Control Sample LOQ Level ofQuanfitation '
LCSD
Laboratory Control Sample Duplicate PQL Practical Quantitation Limit
QCS
Quality Control Sample CRQL Contract Required Quantitation Limit
DUP
Duplicate PL Permit Limit .
MS
Matrix Spike - RegLvl Regulatory Limit '
MSD
Matra Spike Duplicate MCL Maximum Contamination Limit '
RPD
Relative Percent Different MinCL Min m= Compound Limit '
ICV
Initial Calibration Verification RA Reanalysis
ICB
Initial Calibration Blank RE Reextraction
CCV
Continuing Calibration Verification TIC Tentatively Identified Compound
CCB
Continuing Calibration Blank RT Retention Time
_
RLC
. Reporting Limit Check CF Calibration Factor
DF '
Dilution Factor RF Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting..
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
�) Original
Page 4 of 36
Sronmit Environmental Technologies,Inc. WOrkorder
3310 Win St.
RIVIRONMENTAL TECHNOLOGIES, INC. Cuyahoga Falls, Ohio 44223 Sample Summary
Analytical laboratories TEL: (330) 253-8211 FAX. • (330) 253-4489, WO#: 17110701
Websile: hu .-IA lv.seuekcom 28-Nov-17
CLIENT: Synagro
Project: Bladenboro WWTP
Lab SampleID Client Sample D) Tag No Date Collected Date Received Matrix
17110701.001 Bladenboro W WiP 11/13=17 11:30:00 AM 11/14=17 10:00:00 AM Sludge
Page 5 of 36
�8
> � -, ��
sam+rEnvironmental Teehnar10WinStInc.
3310 Win St.
Analytical Report
ENVIRONMENTAL TECHNOLOGIES, IPiC.
Cuyahoga Falls, Ohio 44213
(basereport)
/rrelytical Laboratories TEL: (330) 253-8211 FAX.-. (330) 253-4489
WO#: 17110701
Website: htta://www.settekeom
Date Reported: 11/28/2017
CLIENT:
Synagro
Tag Number:
Matrix:
SLUDGE
Collection Date:
11/13/2017 11:30:00 AM
Lab ID:
17110701-OOIA
Project:
Bladenboro WWTP
Client Sample ID Bladenboro W WTP
Analyses Result
RL
Qual Units
DF .
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW7470A
SW7470A Analyst ALJ '
. TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury NO
0.00200
mg/L
1
11/16/2017 5:05:00 PM
TCLP METALS, VOC, BNA, PEST,.HERBSOLID
SW6010C
SW3010A
Analyst KMS
TCLP METALS ANALYSIS (SW131116010)
TCLP Arsenic(As) ND
0.500
mg/L
1
11/16/2017 5:29:25 PM
TCLP Badum(Ba) - ND
5.00
mg/L
1
11/16/2017 5:29:25 PM
TCLP Cadmium(Cd) ND
0.1.00
mg/L
1
11/16/2017 5:29:25 PM
- TCLP Chromium(Cr) - ND
0.200
mg/L
1
11/16/2017 5:29:25 PM
_
TCLP Lead(Pb) - ND
0.500
mg/L
1
11/16120175:29:25 PM
- TCLP Seler ium(Se) ND
0.0500
mg/L
1
11/16/2017 5:29:25 PM
TCLP Silver(Ag) ND
0.500
mg/L
1
11/16/2017 5:29:25 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270C
SW3510C , Analyst: BJH
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene , ND
0.0800
mg/L
2
11/17/2017 2:47:00 AM
2,4,5-Tiichlorophenol ND
0.200
QC+ mgtL
2
11117120172:47:OOAM
2,4,6-Trichlorophenol ND
0.200
QC+ mg/L
2
11/17/20172:47:OOAM
' 2,4-Dinitrotoluene ND
0.100
QC+ ingil-
2
1 Ill 7/20172:47:00 AM
Cresols, Total - ND
4.00
mg/L
2
11/17120172:47:00AM
Hexachlorc-1,3-butadiene ND
0.100
mg/L
2
11/17120172:47:00'AM
Hexachlorpbenzene ND
0.100
mg/L
2
11/17/20172:47:00AM
Hexachloroethane ND
0.0800
mglL
2
11/17/20172:47:OOAM
Nitrobenzene ND
0.0800
mg/L
2
11/17/20172:47:OOAM
Pentachlorophenol • ND
0:200
mg/L
2"
11/17120172:47:OOAM
Pyridine ND
0.200
mg/L
2
11/17/20172:47:OOAM
Sum 2-Fluorophenol 57.3
10-109
%Rec
2
11/17/20172:47:OOAM
Sum Phenol-d6 60.2
10-109
%Rec
2
11/17/20172:47:00AM
Surr Nitrobenzene-d5 95.5
'19-120
%Rec
2
11/17/20172:47:OOAM
Surr:2,4,6-Tdbromophenol 60.3
10 -120
%Rec
2
11/17/2017 2:47:00 AM
Surr: 2-Fluorobiphenyl 74.0
22 - 117
%Rec
2
11/17/2017 2:47:00 AM
Surf: p-Terphenyl-d14 88.4
34 -116
%Rec
2
11/172017 2:47:00 AM
QualiSers• " Value exceeds Maximum Contaminant Level.
E Value above quantitation range
H Holding times for preparation or analysis exceeded
M 'Manuel Integration
used to detemilne area response
/ MC Value is below Minimum Compound Limit.
N Tentatively identified compounds
ND Not Detected
0 • RSD is greater than RSDIimit
' P Second column confirmation exceeds
PL Permit Limit
I
Original
R RPD outside accepted recovery limits
RL Reporting Detection Limit
Page 6 of 36
Summit Environmental Technologies, Ina - Analytical Report
3310 Win St.
RiVIROWENTAL TECHNOLOGIES, IxR Cuyahoga Falls, Ohio 44223 (basereport)
Analyffcaf Lahorarorjes TEL. (330) 253-8211 FAX.-. (330) 253-4489 WO#:17110701
Websile: h ry.-IAnmvsettekcom Date Reported: 11/28/2017
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 11AV201711:30:00 AM
Lab ED: 17110701-001A
Project: Bladenboro WWTP
Client Sample lD Bladenboro W WTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8270C SW3510C Analyst BJH
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
_ NOTES:
The BNA 8270 CCV (Batch R77398) exhibited high recoveries for several analytes and low recovery for Surrogate: Phenol-d6; Associated
samples are ND for all analytes of interest.
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8081A SW3510C Analyst JBN
TCLP PESTICIDES ANALYSIS (SW131118081)
Chlordane, total ND 0.0100 mg/L 1 11/22/2017 9:53:00 PM
Toxaphene -ND - 0.0200 ni 1 11122/20179:53:06 PM
Enddn ND 0.00100 QMR mg/L 1 11/22/2017 9:63:00 PM '
{, gamma-BHC ND 0.00100 QMRd mg/L 1 11/22/20179:53:00 PM
-` Heptachlor No 0.00100 QMR mg/L 1 11/22/2017 9:53:00 PM
Heptachlor epoxide ND 0.00100 QMR mg/L 1 11/22120176:53:00 PM
Methoxychlor ND 0.00100 QMR mg/L 1 11/22120179:53:00 PM
Sum TCMX 93.3 10 -119 %Rec 1 11/22/2017 9:53:00 PM
Sum DCB 85.4 10 -119 %Rec 1 11/22/2017 9:53:00 PM
NOTES:.
TCLP Pesticide Sample MS and MSD pair exhibited high RPDs forall analytes of interest.
TCLP METALS; VOC, BNA, PEST, HERB -SOLID SW8151A SW8151A Analyst: JBN
SVOC SW-846: 8151 HERBICIDES-TCLP _
2,4-D ND 11.3 d ri 1 11/21/2017 9:23:00 PM
2,4,5-TP ND 11.3 d mg/L 1 11/2112017 9:23:00 PM
Sum 2,4-Dichlorophdnylacetic aci 92.0 20 - 140 %Rea 1' 11/21/2017 9:23:00 PM
TCLP METALS, VOC, BNA, PEST, HERBSOLID - SW8260B SW1311M Analyst MES
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene ND 0.100 mg/L 1 11/16120174:07:00 PM
1,2-Dichloroethane ND 0.100 mg/L 1 11116/20174:07:00 PM
MEK ND 2.00 mg/L 1 11116/20174.07:00 PM
Benzene ND 0.100 mg/L 1 11/16120174:07:00 PM
Carbon tetrachloride , ND 0.100 ri 1 11/16/2617 4:07:00 PM
Chlorobenzene - ND 0.100 mg/L 1 11116120174:07:00 PM
Qualifiers: " Value exceeds Maximum Contaminant Level. E Value above quantitation range
�_-- H Holding times for preparation of analysis exceeded M Manual Integration used to determine area: response
1 ) MC Value is below Minimum Compound Limit. N Tentatively identified compounds
\._ 1 ND Not Detected O RSD is greater than RSDlirnit
P Second column confirmation exceeds , PL Permit Limit Original'
R RPD outside accepted recovery limits RL Reporting Detection Limit ,
Page 7 of 36
Summit Environmental Technologies, Inc.
3310 Win St.
Analytical Report
ENVIRONMENTAL TECONO LOCI25, NC.
Cuyahoga Falls, Ohio 44223
(basereport)
Analytical lshcrafories 'TEL:.. (330) 253-8211 FAX.- (330) 253-4489
WO#: 17110701
Website: htra://ivwrvsenekcom
Date Reported- 1128/2017
CLIENT:
Synagro
Tag Number:
Matrix:
SLUDGE
Collection Date:
11/13/2017 11:30:00 AM
Lab ED:
17110701-001A
Project:
Bladenboro WWTP
Client Sample ID Bladenboro W WTP
Analyses
Result' ' RL Qual Units
DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERBSOLID
SW8260B
SW1311M Analyst MES
TCLP VOLATILES ANALYSIS
Chloroform
ND
. 0.100
mg/L
1
11/16/2017 4:07:00 PM
Tetrachloroethene
ND
0.100
mg/L
1
11/16/20174:07:00 PM
Trichlorcethene
ND
0.100
mg/L
1
1.1/16/20174:07:00 PM
Vinyl chloride
ND
0.200
mglL
1
11/16/2017 4:07:00 PM
Sum 4-Bromofluorobenzene
104
70-130
%Rec
1
11/1612017 4:07:00 PM
Surr: Dibromofluoromethane
94.0
70 -130
%Rec
1
11/16/2017 4:07:00 PM
Surr. Toluene-d8
95.3
70 - 130
%Rec
1
11/16/2017 4:07:00 PM
- RCISOLID-W/IGNITABILITY1030
SW9014
Analyst MS
/
REACTIVE CYANIDE (9014/7.3.3.2)SOLID
l
J�
Cyanide, Reactive
ND
0.500
mg/Kg
1
11/21/2017
RCI-SOLID-W/ IGNITABILITY1030
SW1030
Analyst AJT
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability non-flammable
1
11/16/2017 10:00:00 AM
RCISOLID-W/ IGNITABILITY1030
SW9045D
Analyst: DHC
PH (SW9045D)
pH
7.0
s.u.@19.0C
1
11/14120172:64:00 PM
RCISOLID-W/IGNITABILITY1030
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)17.3.4.2
Sulfide, Reactive _
30.0
25.0
mg/Kg
1
11/21/2017 12:35:00 PM
Qualifiers: "
Value exceeds Maximum Contaminant Level.
.E
Value above quantitation range ,
H
Holding times for preparation or analysis exceeded
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound Limit.
N,
Tentatively identified compounds
._ ND
Not Detected
O
RSD is greater than RSDlimit
- P
Second column confirmation exceeds
PL
Permit Limit Original
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 8 of 36
ms"MmIst
9amnrilEnvironmental TeahnalainSt.
33I0Win St.
QC SUMMARY REPORT
tr;vlNVMn4NMAL I LCHNOLUr11bS, INC.
Analyltcal Laborraroriea
Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX.- (330) 253-4489
WO#: 17110701
Websile: hawlAvrvw..rettelccom
28-Nov-17
Client:
Synagro
Project:
Bladenboro WWTP
BatchID: 29666
Sample ID mb-29666=10
SampType:
MBLK
TestCode: tclp-voc-mstr Units: mg/L
Prep Date: 11/15/2017
RunNo: 77399
"lient ID: PBS
Batch to:
29666
TeslNo: SW8260B SW1311M
Analysis Date: 1111612017
SegNo: 1324639
4nalyle
Result
PQL SPK value SPK Ref Val
%REC LowLimit HlghUrnit RPD Ref Val
%RPD RPDLimil Qual
1,1-Dichloroethene
ND
0.100
1,2-Dichloroelhane
ND
0.100
MEK
ND
.2.00
Benzene
ND
0.100
Carbon tetrachloride
ND
0.100
Chlorobenzene
ND
0.100
Chloroform
ND
0.100
Tetrachloroethene
ND
0.100
Trichloroethene
ND
0.100
Vinyl chloride
ND
0.200
Surr: 4-Bromofluorobe6zene
526
Surr: Dibromofluoromethane
_
471
Surr: Toluene-d8
483
500.0 105 70 130,
500.0 94.2 70 130
500.0 96.7 70 130
Sample ID Ics 20ppb 4059
SampType: LCS
TestCode: tclp-voc-mstr Units: mglL
Prep Date:
RunNo: 77399
"lient ID: LCSS
Batch ID: 29666
TestNo: SW8260B SW1311M
Aralysis Date: 11/1612017
SegNo: 1324659
4nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighUrnit ' RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.0227
0.0100
0.0200 0 114
79.4
131
1,2-Dichloroethane
0.0230
0.0100
0.0200 0 115
73.6
137
MEK
0.0995
0.0506
0.100 0 99.5
55.1
163
Benzene
0.0215
0.0100
0.0200 0 107
73.1
132
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND Not Detected
Q
RSD is greater than RSDlimit .Original
P
Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits
Page 9 of 36
a � IT
t�
SnmmirEar,.aan,eatarTeehaafaWinSInc.
3310Win St.,
QC SUMMARY REPORT
eKVIKIINrA9NIALrecewoLVOLS.,.ANC. Cuyahoga Falls, Ohio44223
AnsiyUcal taboratorfes ,. TEL: (330) 253-8211 FAX.- (330) 253-4489
WO#: 17110701
'
Website: hoo:Oww v.seeekcom
28-Not-17
Client:
Synagro
-
Project:
Bladenboro WWTP
BatchED: 29666
Sample ID Ics 20ppb 4059
SampType:
LCS
TestCode: tclp-voc-mstr Onils: mg/L
Prep Date: -
RunNo: 77399
Client ID: LCSS
Batch ID:
29666
TestNo: SW8260B SW1311M
Analysis Date: 11/16/2017
SegNo: 1324659
Analyte ..
Result
PQL SPK value SPK Ref Val
%REC LowUmit HIghLlmit RPD Ref Val
%RPD RPDLImlt Qual
carbon tetrachloride
0.0192
0.0100
0.0200
0
96.2
63.7
139
Chlorobenzene. -
0.0195
0.0100
0,0200
0
97.4 -
72.3
139
Chloroform
'• 0.0208
-0.0100
0.0200
0
104
79.3
129
Tetrachloroelhene _
0.0218
Ao100
O.D200
0
109
56.2
187
Trichloroethene
0.0206
0.0100-
0.0200
0
103
64.1
138
Vinyl chloride
0.0209 "
0.0100
0.0200
0
104
22.1
147
Surr: 4-Bromofluorobenzene
52.3
50.00
105
80.4
126
Surr: Dibromofluoromethane
45.0
50.00
90.0
70.3
125
. Surr: Toluene -dB
49.7
50.00
,. 99.4
82
117
Sample ID Icsd 20ppb 4059
SampType:
LCSD
TestCode: tclp-voc-mstr Units: mg/L
Prep.Date:
RunNo: 77399
Client ID: LCSS02
'Batch ID:
29666
TestNo: SW8260B SW1311M
Analysis Dale: 11/1612017
SegNo: 1324660 '
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLlmit HighUmit RPD Ref Val
%RPD RPDLimit Qual
i,i-ulcmoroemene
u.u224
0.01uu
0.0200
0
112
79.4
131
0.0227 1.64
25
1,2-Dichloroethahe
_ 0.0228
0.0100
0.0200
.0
114
73.6
137
0.0230 0.960
25- -
MEK
0.0968
0.0500 •
0.100 ..
0 ,
96.8. -
55.1
163
0.0995 2.82
25
Benzene
0.0208
0.0100,
0.0200
0
104 -
73.1
132
0.021 5' 2.88
25
Carbon tetrachloride
0.0196.
0.0100
0.0200 -
0 _
98.2
63.7
139
0.0192 2.11
25
Chlorobenzene
0.0191
0.0100
0.0200
0
95.6
72.3
139
'0.0195 1:92
25
Chloroform -
0.0197
0.0100
0.0200
0
98.4
79.3
129
0.0208 5.29
25
Tetrachloroethene
0:0225
0.0100
0.0200
0-
-112
56.2
187
0.0218 3.02
25 -
Qualifiers: •
Value exceeds Maximum Contaminant Level.
B ' Analyte detected in the associated Melhod Blank
E
Value above quantitation range
-
H
Holding times for preparation or analysis exceeded .
J- Analyte detected
below quantitation limits
M
Manual Integration used to determine
`
MC
.
Value is below MinimumCom oundLimit..
P
ND Not Detected
O
RSDis greater than RSDlimit
Original '
P
Second column confirmation exceeds
'PL Permit Limit
_
R
RPD outside accepted recovery limits
Page 10 of 36
1 � �
UIT
Summit Environmental Technologies, Inc.ffIS
3310 Wirs S<.
QC SUMMARY REPORT
L1VIRU1NIabN I Al. I LGi14UWQuL5INC.
Arialyifeal tabolotorles
Cuyahoga Falls, Ohio 44223
TEL:_ (330) 253-8211 FAX.- (330) 253-4489
- WO#: 17110701
'
Website: hawlAnnv.settelr.eom
28 Not,17
Client:
Synagro
Project:
Bladenboro WWTP
BatchlD: 29666
Sample ID Icsd 20ppb 4059
SampType: LCSD
TestCode: tclp-voc-mstr _Units: mg/L
Prep Date:
RunNo: 77399
:lient to: LCSS02
Batch ID: 29666
TestNo: SW8260B SW1311M .
Analysis Date: 11/16/2017
SegNo: 1324660
lnalyte
Result
PQL SPK value SPK Ref Val
%REC Lowlimit Hlght-lmit RPD Ref Val
%RPD RPDLlmit Qual
inchloroethene -
0.0204
0.0100-0.0200
0 102
64.1
138 0.0206
1.02
25
Vinyl chloride
0.0196
0.0100 0.0200
0 98.0
22.1
147 0.0209
6.32
25
Sun: 4-13romofluorobenzene
52.2
50.00
104
80.4
- 126 -
0
25
Sutr: Dibromofluoromethane
45.5
50.00
90.9,
70.3
125
0
'25
Surr: Toluene-d8,
49.6 "
50.00
- 99.2
82
117
0
25
Qualifiers: • Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value. above quantitation range
H Holding times for: preparation or analysis exceeded I Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below. Minimum Compound Limit. ND Not Detected - 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit - R RPD outside accepted recovery limits '
Page 11 of 36
u i�
Win St. Inc.
vd 3BammhEnvironmental Technologies,
QC SUMMARY REPORT
LRWINrrdtlAMAL. I WHH0LVG11:S,1NQ Cuyahoga Falls, Ohio 44223
Anatyllcal Laboratories TEL: (330) 253-8211 FAX:: (330) 253-4489
WO#: 17110701
Webstte: humMvinvaettekcom
28-Nov-17
Client:
Synagro
-
Project:
Bladenboro WWTP
BatchID: 29690
Sample ID MB-29690
SampType:
MBLK
TestCode: MTL-TCLP-7( Units: mg1L
Prep Date: 11116/2DI7
RunNo: 77394
client ID: PBS
Batch ID:
29690
TestNo: SW6010C SW3010A
Analysis Date: 11116/2017
SegNo: 1324512
Malyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit Hlghl-imit RPD Ref Val
%uRPD RPDUmlt Qual
TCLP Arsenic(As)
ND
0.500
TCLP Barium(Ba)
ND
5.00
TCLP Cadmium(Cci)
ND
0.100
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pb)
ND
0.500
TCLP Selenium(Se)
ND
0.0500
TCLP Silver(Ag)
ND
0.500
Sample ID LCS-29690
SampType:
LCS
TestCode: MTL-TCLP-7( Units: mg/L
Prep Date: 11/1612017
RunNo: 77394
client ID: LCSS
.Batch ID:
29690
TestNo; SW6010C SW3010A
Analysis Dale: 11/1612017
SegNo: 1324613
Malyte
Result
PQL SPK value SPK Ref Val
%REC LowLlmit HighLimit RPD Ref Val
%RPD RPDUmit Dual
TCLP Arsenic(As)
1.93
0.500
2.000
0
96.4
80
120
TCLP Barium(Ba)
ND
5.00
2.000
0
- 99.1
80
120
TCLP Cadmlum(Cd)
1.83
0.100
2.000
0
91.5
80
120
TCLP Chromium(Cr)
2.01
0.200
2.000
0
100
80
120
TCLP Lead(Pb)
- 1.98
0.500
2.000
0
99.0
80-
120
TCLP Selenium(Se)
2.00
0.0500
2.000
0
100
80 -
120
TCLP Silver(Ag)
2.03
0.500
2.000,
0
101
80
120
Qualifiers: • Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDhrmt
R RPD outside accepted recovery limits
Original
Page 12 of 36
fn
u l�
Inc
Smm�,tEmirnamemarTea331010 Win SShaarWt. .
QC SUMMARY REPORT
W4V1KV,NlnhN I Al. 1 bCHFI0 G1tS, INC. Cuyahoga Falls, Ohio 44223 -
Analytleal Laboratories TEL: (330) 253-8211 FAX.- (330) 253-4489
WO#: 17110701
Webslte: ham:/Fvwwseuekcom
28 Now17
Client:
Synagro
Project:
Bladenboro WWTP
BatchID: 29690
Sample ID 17110703-001AMS
SampType:
MS
TestCode:
MTL-TCLP-7( Units: mg/L
Prep Date: 11/1612017
RunNo: 77394
Client ID: BatchQC
Balch ID:
29690
TestNo:
SW6010C SW301 DA
Analysis Date: 1111612017
SegNo: 1324517
Analyte'
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HlghLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsemc(As)
2.11
0.500
2.000
0.04748
103
70
130
TCLP Barium(Ba)
ND
5.00
2.000
0.5291
92.7
70
130
TCLP Cadmium(Cd)
1.83
0.100
2.000
0.0005364
91.7
70
130
TCLP Chromium(Cr)
1.93
0.200
2.000
0.004083
96.3
70
130
TCLP Lead(Pb)
1.81
0.500
2.000
0.0D4672
90.4
70
130
TCLP Selenium(Se)
2.17
0.0500
2.000
0
109
70
130
TCLP Silver(Ag)
2.08
0.50D
2.000
0
104
70
130
Sample ID 17110703-OD1AMSD
SampType:
MSD
TestCode: MTL-TCLP-7(, Units: mg/L
Prep Date: 1111612017
RunNo: 77394
Client ID: BatchQC
Batch ID:
29690
TestNo: SW6010C SW301 DA
Analysis Date: 1111612017
SegNo: 1324518
4nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimitt HighLimit RPD Ref Val
%RPD RPDLimit Quay
TCLP
Arsenic(As)
2.12
0,500
2.000
0.04748
103
70
130
2.108
0.318
20
TCLP
Barium(Ba)
ND
5.00
2.000
0.5291
92.1
70
130
0
0
20
TCLP
Cadm1um(Cd)
1.82
0.100
2.000
0.0005364
91.0
70
130
1.834
0.716
20
TCLP
Chromium(Cr)
1.92
0.200
2.000
0.004083
95.7
70
130
1.930
0.646
20
TCLP
Lead(Pb)
1.81
0.500
2.000
0.004672
90.5
70
130
1.813
0.0748
20
TCLP
Selenium(Se)
2.16
0.0500
2.000
0
108
70
130
2.171
0.715
20
TCLP
Silver(Ag)
2.06
0.500
2.000
0
103
70
130
2.084
0.944
20
Qualifiers: ' Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 13 of 36
En
uur
33Win SSamnr,Env;.anneata,Teahnar10WinSt. .
QC SUMMARY REPORT
trGVlagVtlrrlaN l F4 t tunNUL4Q1b S, lRC. Cuyahoga Falls, Ohio 44223
�ittaryffcal [at1af910!!e6 TEL: (330) 253.8111'FAX.• (330) 253-4489
WO#: 17110701
Websuei httn://www..seuekcom
28-Nou17
Client:
Synagro
Project:
Bladenboro WWTP
BatchID: 29690
Sample ID MB-29684
SampType:
MBLK
TestCode: MTL-TCLP-7( Units: mglL
Prep Date: 11/16/2017
_ RunNo: 77394
Client ID: PBS
Batch ID:
29690
TestNo:, SW6010C SW3010A
Analysis Date: 11/16/2017
SegNo: 1324523
Analyte
Result
PQL. SPK value SPK Ref VaI
%REC LowLimit HIghLlmit RPD Ref Val
%RPD RPDLlmit Qual
TCLP Arsenlc(As)
ND
0.500
TCLP Barium(Ba)
ND
5.00 '
TCLP Cadmlum(Cd)
- ND.
- 0.100 -
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pla)
ND
0.500
TCLP Selenlum(Se)
ND
0.0500
TCLP Silver(Ag)
ND
0.500
Qualifiers: " Value exceeds Maximum Contaminant Level.
H.. _Holding times for preparation or arialysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit '
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits'
Original
Page 14 of 36
i
f
l �
3310/0 Win St.
Summit Environmental TeehnarWinSInc.91
QC SUMMARY REPORT
tr4UNUPJrneNIRL t LU"NuLUCltt:S, 1NC.
Cuyahoga Falls, Ohio 44223
WO#: 17110701
Analyitcaf Laboratories TEL: (330) 253-8211 FAX (330) 253-4489
Webslte: haa:/fw m, settek.com
28-Nov-17
Client:
Synagro
Project:
Bladenboro WWTP
BatchID:, 29693
Sample ID MS-29693
SampType:
MBLK
TestCode: HG TCLP(74 Units: PPM
Prep Date: 11116/2017
RunNo: 77387
Client ID: PBS
Batch ID:
29693
TestNo: SW7470A SW7470A
Analysis Date: 1111612017
SegNo: 1324359 '
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
TCLP Mercury ND 0.00200
Sample ID LCS-29693
SampType:
LCS
TestCode:
HG_TCLP(74 Units: PPM
Prep Date: 11116/2017
RunNo: 77387
Client ID: LCSS
Batch to:
29693
TestNo:
SW7470A SW7470A
Analysis Date: 11116/2017
SegNo: 1324360
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowUmit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury, 0.00434 0.00200 0.00400 0 108 80 120
Sample ID 171.10703-001AMS
SampType:
MS
TestCode:
HG TCLP(74 Units: PPM
Prep Dale:. 11/1612017
RunNo: 77387-
Client ID:. BatchQC
Batch to:
29693
TestNo:
SW7470A SW7470A
Analysis Date: 11/1612017
SegNo: 1324363
Analyte
.
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDUmit oust
TCLP Mercury 0.00402 0.00200 0.00400 0 101 75 125
Sample to 17110703-001AMSD
SampType:'MSD
TestCode: HG TCLP(74 Units: PPM
Prep Date: 11/1612017
RunNo: 77387
Client ID: BatchQC
Batch ID: 29693
TestNo: SW7470A SW7470A
Analysis Date: 11116/2017
SegNo: 1324364
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimil HighLimit RPD Ref Val
%RPD RPDUm[t Qual
TCLP Mercury 0.00397 0.00200
0.00400 0 99.2 75
125
0.00402 1.25 20
Qualifiers: * Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
1 Analyte detected below quantitation limits
ND Not Detected
M
O
Manual Integration used to determine
RSD is greater than RSDImut Original
P Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits
Page 15 of 36
1 - r
� ��
Summit Environmental Technologies, Inc.
3310 Wm &.
QC SUMMARY REPORT
trMHUInrnbry i Ai. I menaatuarbs,+rac. Cuyahoga Falls, Ohio 44223
AnsiyNcal Laboratories TEL: (330) 253-8211 FAX., (330) 253-4489
WO#: 17110701
Website: httwll wrv..seaelccom
28-Nov-17
Client:
Synagro
Project:
Bladenboro WWTP
Bateh D: 29693
Sample ID 17110703-001AMSD
SampType:
MSD
TeslCode: HG TCLP(74 Units:PPM
Prep Date: 1111612017
RunNo: 77387
Client ID: BatchQC
Batch ID:
29693
TestNo: SW7470A SW7470A
Analysis Date: 1111612017
SegNo: 1324364
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowrUmit HlghUrnit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: • Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation"range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 16 of 36
6
91
ummur331OinSt.
Summit Environmental Technologies, ner
QC SUMMARY REPORT
emvlRWrtl ldkNltIL IYCHRULVU1�5, itYC.
Cuyahoga Falls, Ohio 44223
WO#: 17110701
Analytical Laboratorle5 TEL: (330) 253.8211 FAX.-. (330) 253-4489
Wehsite: htto:/Aviviv..Teltelc.com
28-Nov-17
Client:
Synagro
Project:
Bladenboro WWTP
BatchID: 29698
Sample ID mb-29698
SampType:
mblk
TestCode: tclp-svoc-cpe Units: mg1L
Prep Date: 11/1612017
RunNo: 77731
Client ID: PBS
Batch ID:
29698
TestNo: SW8081A SW3510C
Analysis Dale: 11/2212017
SegNo: 1332175
4alyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLlmil RPD Ref Val
%RPD RPDLimit Qual
Chlordane, total
ND
0.0100
Toxaphene
ND
0.0200
Endrin
ND
0.00100 d
gamma-BHC
ND
0.00100
Heptachlor
ND
0.00100
Heptachlor epoxide
ND
0.00100
Methoxychlor
NO
0.00100
Sum: TCMX
16.6
20.00 83.2 10 119
Surr: DCB
17.9
20.00 89.7 10 119
Sample ID Ics-29698
SampType:
Ics
TestCode: tclp-svoc-cpe Units: mglL
Prep Date: 11/1612017
RunNo: 77731
Client ID: LCSS
Batch ID:
29698
TestNo: SW8081A SW3510C
Analysis Date: 11/2212017
SegNo: 1332176
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLlmit RPD Ref Val
%RPD RPDLimit Qua]
Endrin
0.00874
0.00100
0.0100
0
87.4
20
157
gamma-BHC
0.00804
0.00100
0.0100
0
80.4
22
137
Heptachlor
0.00843
0.00100
0.0100
0
84.3
24
121
Heptachlor epoxide
0.00869
0.00100
0.0100
.0
86.9
27
152
Methoxychlor
0.00836
0.00100
0.0100
0
83.6
10
199
Surr: TCMX
13.4
20.00
66.9
10
119
Surr: DCB
13.4
20.00
67.2
10
119
Qualifiers: • Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantilation range
H Holding times for preparation or analysis exceeded I Analyte detected below quantilation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit.. ND Not Detected O RSD is greater than RSDlimit Original
P Second column confirmation exceeds _ PL Permit Limit R RPD outside accepted recovery limits
Page 17 of 36
n1suMMIT
Summit Enviromuen[al Technologies, Inc.
3310 Win St
QC SUMMARY REPORT
WAVIaV'NMUN IRL I LCHNVIRCH.b.S" Ma,
Cuyahoga Falls, Ohio 44223
WOS: 17110701
Artaryilcal Laboralories
TEL: (330) 253-8211 FAX.- (330) 253-4489
Wehsite: hup.*lApww.seaefccom
28-Not 17
Client:
Synagro
Project:
Bladenboro WWTP
BatchID: 29698
Sample ID 17110701-001ams
SampType:
has
TestCode: tclp-svoc-cpe Units: mg/L
Prep Date: 11/1612017
RunNo: 77731
Client ID: Bladenboro WWTP
Batch ID:
29698
TeslNo: SW8081A SW3510C
Analysis Date: 1112212017
SegNo: 1332177
Analyte
. Result
PQL SPK value SPK Ref Val
%REC LowLlmit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
0.00419
0.00100
0.0100
0
41.9
20
157
QMR
gamma-BHC
0.00502
0.00100
0.0100
0
50.2
22
137
QMR
Heptachlor
0.00509
0.00100
0.0100
0
50.9
24
121
QMR
Heptachlorepoxide
0.00440
0.00100
0.0100
0
44.0
27 -
152
QMR
Methoxychlor
0.00502
0.00100
0.0100
0
50.2
10
199
QMR
Sur: TCMX
8.04
20.00
40.2
10
119
Sum: DCB
8.54
20.00
42.7
10
119
Sample ID 17110701-001amsd
SampType:
msd
TestCode: telp-svoc-cpe. Units: mglL
Prep Date: 1111612017
RunNo: 77731
Client ID: Bladenboro WWTP
Batch ID:
29698
TestNo: SW8081A-SW3510C
Analysis Dale: 11122f2017
SegNo: 1332178
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit oust
Endrin
0.00953
0.00100
0.0100
gamma-BHC
0.00988
0.00100
0.0100
Heptachlor
0.0105
0.00100
0.0100
Heptachlor epoxide
0.00968
0.00100
0.0100
Methoxychlor
0.0119
0.00100
0.0100
•- Sur: TCMX ,
17.4
20.00
Sum: DCB
17.5
20.00
NOTES:
The TCLP Pesticide Sample MS and MSD pair exhibited high RPDs for all analytes of Interest.
Qualifiers: • Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
0 95.3
20
157
0.00419
77.9
0 98.8
22
137
0.00502
65.2
0 105
24
121
_
0.00509
69.3
0 96.8
27
152
0.00440
- 75.1
0 119
10
199
0.00502
81.4
86.9
10
119
0
87.7
10
119
0
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
30 R
30 R
3D R
30 R
30 R
Original
Page 18 of 36
Bunvnil Environmental Technologies,QC
3310t.
/0 Win SSt.
SUMMARY REPORT
trsvlarJN rn uN l Al. t LCHUL) LUU14: S, Mc.
Analytical Gabartalories
Cuyahoga Fails, Ohio 44223
TEL: (330) 253-8211 FAX. (330) 253-4489
WO#: 17110701
-
Webslle: hup.,lAnvivaettekcam
28-Nov-17
Client:
Synagro
Project:
Bladenboro Wl TP
BatchED: 29700
Sample ID MB-29700
SampType:
MBLK
TestCode: SVOC-BNA T Units: mg1L
'Prep Date: 11116/2017
RunNo: 77398
Client to: PBS
Batch ID:
29700
TestNo: SW8270C SW3510C
Analysis Date'. 1111712017
SegNo: 1324620
Analyte -
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HlghLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
ND
0.0400
2,4,5-Trichlorophenol
ND
0.100
2,4,6-Trichloropheno_I
- ND
0.100
2,4 Dinitrotoluene..
ND.
- 0.0200
o-Cresol
ND
0.100
m/p-Cresol(s),
ND
0.100
Cresols, Total
ND
2.00
Hexachloro-1,3-butadiene
ND
0,00800
Hexachlorobenzene
ND
0.0200
Hexachloroelhane
ND
0.6400
Nitrobenzene
ND
0.0400
Pentachlorophenol
- ND
0.100
Pyridine
'ND
0.100
Surr: 2-Fluorophen ol
0.825
Surr: Phenol-d6
0.836
Surr: Nitrobenzene-d5
1.22
Surr: 2,4,6-Tribromophenol
0.838
Surr: 2-Fluorobiphenyl
0.930
Surr: p-Terphenyl-d14
_
Qualifiers: • Value exceeds Maximmn Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P ' Second column confirmation exceeds
1.000
82.5
10
109 ,.
1.000
83.6
10
109
1.000
122
19
120
1.000 -
83.8
10
120
1.000
93.0
22
117
1.000
-111
34
- 116 -
B Analyte detected in the associated Method Blank E Value above quantitation range
J . Analyte detected below quantitation limits M Manual Integration used to determine
ND Not Detected - 0 RSDJs greater than RSDlimit
PL Permit Limit R RPD outside accepted recovery limits
QC+
QC+
QC+
6
Original
Page 19 of 36,
rya U M MIT
Summit Ersvironmenta[Technolo0 Inc.WinSr
QC.SUMMARYREPORT
trIVIKULN rAIIN I AL 14UHNULOU11:5, INC,
Cuyahoga Falls, Ohio 44223
`
" - WO#: 17110701
1lnalyll:=I tabarslafteo
TEL: (330) 2S3-8211 FAX. • (330) 253-4489
Websue: hum-11 viv.settekaam
28-Nov-17
Client:
Synagro
Project:
Bladenboro WWTP
BatchED: 29700
Sample ID LCS-29700
SampType:
LCS
TestCode: SVOC-BNA T Units: mglL
Prep Date: 1111612017 -
RunNo: 77398 '
Client to: LCSS
Balch to:
29700
TeslNo: SW8270C SW3510C
Analysis Date: 1111712017
SegNo: 1324621
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLlmit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.619
0.0400
0.8000
0
77.4
19.1
126
2,4,5-Trichlorophenol
0.768
0.100.
0.8000
0
96.0
11.7.
- 151
2,4,6-Trichlorophenol
0.741
0.100
0.8000
0
92.6
12.4
150
2,4-Dinitrotoluene
- 0.777
0.6200 - '
0.8000
0
97.1
20:6
140
o-Cresol
0.661
0.100
0.8000
0
82.6
13.8
137
mlp-Cresol(s)
0.674'
0.100
0.8000
0
84.2
10
134
Cresols, Total
. ND
2.00
1,600 '
0
83A
10
129
Hexachloro-1,3-butadiene
6.626
0.00800
0.8000-
0
78.2
14.7
137
Hexachlorobenzene
0.640
0.0200
0.8000
0
80.0
12
139
Hexachloroethane
0.606
0.0400
0.8000
0
75.8
14.8
132
Nitrobenzene
0.726 '
0.0400
0.8000
0
' 90.8
15.6
138
Pentachlorophenol
- 0.755
0.100
0.8000
- 0
94.4
10
156
Pyridine
0.121
0.100
0.8000
0
15.1
- 1
130
Burr: 2-Fluorophenol _
0.651
1.000
65.1
10
147
Surf: Phenol-d6
0.0316
1.000
3.16
10
140
Suir: Nitrobenzene-d5
1.02
1.000
102
10
169
Burr: 2,4,6-Tdbromophenol
- 0.718
1.000
71.8
10
185
Surr: 2-Fluorobiphenyl
0.806
1.000
80.6
10
169
Surr: p-Terpherryld14
- 0.968 -
1.000
96.8
10
179
Qualifiers: ° Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded 1 'Analytedetected below quantitationlimits -
MC Value is below Minimum Compound Limit. ND Not Detected
P Second column confirmation exceeds PL Permit Limit. -
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
QC+.
QC+
QC+
In
S
Original
Page 20 of 36
��
331010 Win sr.
suaanirEavi.aameararTeahaarWinSInc.fn
QC SUMMARY REPORT
LNInHUNUMN IAL I W"rlUt Gn;S, INC. Cuyahoga Falls, Ohio 44223
Aaalyftral Laboralarles TEL: (330) 253-8211 FAX.- (330) 253-4489
Wolf: 17110701
Webstle: hap://wlny.sellelccom
28 Nov-17
Client:
Synagro
Project:
Bladenboro WWTP
BatchlD: 29700
Sample ID 17110701-D01AMS
SampType:
MS
TeslCode: SVOC-BNA T Units: mg/L
Prep Date: 11/1612017
RunNo: 77398
Client ID: Bladenboro WWTP
Batch ID:
29700
TestNo: SW8270C SW3510C
Analysis Date: 11/1712017
SegNo: 1324622
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLlmit HIghLlmil RPD Ref Val
%RPD RPDLImit Coal
1,4-Dichlorobenzene 0.674
0.0800
0.8000
0
84.3
15.2
124
2,4,5-Trichlorophenol 0.838
0.200
0.8000
0
105
30.6
152
QC+
2,4,6-Trichlorophenot 0.768
0.200
0.8000
0
96.0
27.6
150
QC+
2,4-Dinitrotoluene 0.856 _
0.0400
0.8000
0
107
58
_
141
QC+
o-Cresol 0.708 -
0.200
0.8000
0
88.4
26.9
132
m/p-Cresol(s) 0,729
0.200
0.8000
0
91.2
27.4
134
Cresols, Total NO
4.00
1.600
0
89.8
27.6
132 '
Hexachloro-1,3-butadiene 0.658 -
0.0160
0,8000
0
_ 82.2
-5.3
156
Hexachlorobenzene 0.6B1
0.0400
0.8000
0
85.2
54.3
142
Hexachloroethane 0,680
0.0800
0.8000
0
85.1
1.92
131
Nitrobenzene - 0.762 -
0.0800
0.8000
0
95.2
21
135
In
Pentachlorophenol 0.934
0.200
0.8000
0
117
47.4
134
Pyridine NO
0.200
0.8000
0
15.2
-10.3
64.2
Surr: 2-Fluorophenol 0.696
1.000
69.6
9.77
146
Surr: Phenol-d6 0.0356
1.000
3.56
20.7
130
S
Surr: Nitrobenzene-d5 1.15
1.000
115
13.9
156
_
Surr: 2,4,6-Tdbromophenol 0.849
1.000
84.9
27.3
183
Surr: 2-Fluorobiphenyl 0.887
1.000
88.7
21.4
153
Surr: p-Terphenyl-d14 1.07
1.000
107
54.8
154
NOTES:
The BNA TCLP Sample MS exhibited low recovery for Phenol-d6; All analytes of interest exhibited recoveries within acceptance limits.
Qualifiers: * Value exceeds Maximum Contaminant Level.
B Analyte detected
in the associated Method Blank
E Value above quantitation range
H Holding times for preparation or analysis exceeded
J Analyte detected
below quantitation limits
M Manual Integration used to determine
MC Value is below Minimum Compound Limit.
ND Not Detected
O RSD is greater than RSDlimit
Original
P Second column confirmation exceeds
PL Permit Limit
R RPD outside accepted recovery limits
Page 21 of 36
u lirrn s
SunvnifErsvhanmersralTeahr3310Wirs SY.en&
3310
QC SUMMARY REPORT
tr4vIHU1NN1kN IAL I hCHNUWCnES, tNc.
Anarytfcal tabornforles
Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX: (330) 253-4489
WO#: 17110701
'
Website: hap:/Avtnv sehekcom
28-Nov-17
Client:
Synagro
Project:
Bladenboro VFWI?
BatehID: 29708
Sample ID mb-29708
SampType:
mblk
TestCode: telp-svoc-her Units: mg/L
Prep Date: 11/1612017
RunNo: 77587
Client ID: PBS
Batch ID:
29708
TestNo: SW8151A SW8151A
Analysts Date: 11/2112017
SegNo: 1328684
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HlghLimil RPD Ref Val
%RPD RPDUmlt Qual
2,4-U ND 1.00 0 0 d
2,4,5-TP ND 0.500 0 0 d
Surr: DCAA 423 500.0 84.6 20 140
Sample ID Ics-29708
SampType:
Ics
TestCode: tclp-svoc-her Units: mg/L
Prep Date: 1111612017
RunNo: 77587
Client ID: LCSS
Batch ID:
29708
TestNo: SW8151A SW8151A
Analysis Date: 11121/2017
SegNo: 1328695
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D ND 1.00
2,4,5-TP ND 0.500
Surr. CCAA 511
Qualifiers: • Value exceeds Maximum Contaminant Level. .
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
0.500 0 97.1 62.6
0.500 0 84.9 52.5
500.0 102 20
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
125
128
140
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 22 of 36
frSMMU Summit Environmental. Technologies, Inc. 'QC SUMMARY REPORT
IT 3310 Win St.
eraviKUWr1 ery iAu hCMgULOCn:s, tne. Cuyahoga Falls, Ohio 44223
Analyllcal taboretories TEL: (330) 253-8211 FIX.- (330) 253-4489 WO#: 17110701
- Website: htt�://www.seuelccmn 28-Nov-17
Client: Synagro
Project: Bladenboro WWTP BatchID: 29708
Sample ID 17110656.006ams
"SampType:
ms
- TestCode: tclp-svoc-her Units: mglL
Prep Date: 1111612017
RunNo: 77567
Client ID: BatchQC
Batch ID:
29708
TestNo: SW8151A SW8151A
Analysis Dale: 11/2112017
SegNo: 1328685
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HlghLimit RPD Ref Val
%RPD RPDLimit Qual
t,v-u
NU
11.3 0.500
0 103
37
105 -
2,4,5-TP
ND
11.3 0.500
0 90.5
36
106 -
Surr:2,4-Dlchlorophenylacelcacid
544
500.0
109
20
.- 140
Sample ID 17110656-006amsd
SampType:
msd
TestCode: telp-svoc-her Units: mg/L '
Prep Date: 11116/2017
RunNo: 77587
Client ID: BatchQC
Batch ID:
29708
TestNo: SW8151A SW8151A
Analysis Date: 11121/2017
SegNo: 1328686
Analyte
- Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLlmit RPD Ref Val
%RPD RPDLimit Qual
2,4-D.
ND
11.3 - 0.500
0 87.8
37
105
0 0
30
2,4,5,TP
ND
11.3 0.500
0 77.9
38
106
0 0.
30
'Surr: 2,4-Dichlorophenylacetic acid
472
600.0
94.3
20
140
0
30
Qualifiers: • Value exceeds Maximum Contaminant Level. B . Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded •J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected Q RSD is Original
p greater than RSDlimil
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits -
Page 23 of 36
AgEm
Ill' 1 ly
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
trevlHUNrOMAL rtiMNOLGCnt3, a'1C,
rinalylical Laboralorieo
Cuyahoga Falls, Ohio 44223fn
TEL: (330) 253-8211 FAX (330) 253-4489
WO#: 17110701
Webshe: hay.,1Aovw.seaek.com/Avtvw.seuek.com
28-Nov-17
Client:
Synagro
Project:
Bladenboro WWTP
BatchID: R77252
'ample ID LCS-R77252
SampType: LCS
TestCode: pH O11(9045 Units: s.u.@20.3C
Prep Date:
RunNo: 77252
:lient to: LCSW
Batch ID: R77252
TestNo: SW9045D
Analysis Date: 11/1412017
SegNo: 1322134
4nalyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imil HighLimit RPD Ref Val
%RPD RPDLImit Qua[
pH 7.0 7.0 0 100 90 110
Sample ID 17110691-001ADUP
SampType:
DUP
TestCode: pH 011(9045 Units: s.u.@20.4C
Prep Date:
RunNo: 77252
:;lient ID: BatchQC
Batch ID:
R77252
TestNo: SW9045D
Analysis Date: 11/14/2017
SegNo: 1322136
4nalyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH
5.9
Qualifiers: " Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit,
P Second column confirmation exceeds
0 0
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
5.9 0 10
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 24 of 36
p" f�.
I'G�''?7�
33/0 Win St.
Summit Environmental Technologies, St.FE
QC SUMMARY RL' PORT
crcv IHU w rm u n l AL r LCHNO LU 011:5, m¢6.
Cuyahoga Falls, Ohio 44223
WO#: 17110701
Analytical Laboratories TEL: (330) 253-8211 FAX:: (330) 253-4489
Website: huy.,1AvrnP.se1tekcom
28-Nov-17
Client:
Synagro
Project:
Bladenboro WWTP
BatchED: R77351
Sample ID 17110701-001ADUP
SampType:
DUP
TestCode: Ignitahility_S Units:
Prep Date:
RunNo: 77351
,lient ID: Bladenboro WWTP
Batch to:
R77351
TestNo: SW1b30
Analysis Dale: 11/1612017
SegNo: 1323859
4nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HlghLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
Sample ID 17110701-001ATRIP
SampType:
DUP
TestCode:
Ignitability_S Units:
Prep Date:
RunNo: 77351
,lient ID: Bladenboro WWTP
Batch ID:
R77351
TestNo:
SW1030
Analysis Dale: 11/1612017
SegNo: 1323860
4nalyte
-
Result
PQL
SPK value SPK Ref Val
%REC LowUrnit HighLlmit RPD Ref Val
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
Sample ID 17110779-001ADUP
SampType:
DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 77351
:lient ID: BatchQC
Batch ID:
R77351
TestNo: SW1030
Analysis Date: 11/16/2017
SegNo: 1323862 "
4nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimlt RPD Ref Val
%RPD RPDLimit Qual
gn0aon0y non-mammaole o 0 20
Sample ID 17110779-001ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 77351
Client ID: BatchQC
Batch ID: R77351
TestNo: SW1030
Analysis Date: 11/16/2017
SegNo: 1323863
Analyle
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighUmit RPD Ref Val
%RPD RPDLimit oust
Ignitability non-flammable 0 0 20
Qualifiers: ° Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 25 of 36
SUMMIT
SnmmitEnvirmmnenalTechnologies,
WinSIna
331010 Win St.
QC SUMMARY REPORT
trAVINUNrneN IAL I WHNULQUTSs, INC.
Analytical Laborasarfa5
Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX.. (330) 253-4489
WO#: 17110701
Website: hay.,1 ww.seaekcom
'28 Nov-17
Client:
Synagro
"
Project:
Bladenboro WWTP
BatchID: R77351
Sample ID 17110779-001ATRIP
'SampType:
DUP
TestCodes
Ignitability_S Units:
Prep Date:
RunNo: 77351
Client ID: Batch=
Batch ID:
R77351
TestNo:
SW103D
Analysis Date: 1111612017
SegNo: 1323863
Analyte
Result,
PQL "SPK
value SPK Ref Val
%REC LowLlmit HlghUrnit RPD Ref Val
%RPD RPDLimit Qtial
Qualifiers: • Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded "J Analyte detected below quantimtion limits
MC Value is below Minimum Compound Limit. ND Not Detected '
P Second column confirmation exceeds PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine -
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original -
Page 26 of 36
s u m"I N T
Summit Environmental Technologies, St.
3310 l0 Win St.
QC SUMMARY REPORT
tsVIRVNrmeNUtl. rtcHNV LS7G1tt5, JNC,
AnalyUcaf Lobarnforlos
Cuyahoga Falls, Ohio 44223
TEL: (330) 253.8211 FAX: (330) 253-4489
WO#: 17110701
Website: hity.-Mvinvsetrelccom
28-Nou17
Client:
Synagro
Project:
Bladenboro WWTP
BatchED: R77544
Sample ID MB.R77544
SampType:
MBLK
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 77544
Client ID: PBS
Batch ID:
R77544
TestNo: SW9034
Analysts Date: 1112112017
SegNo: 1327622
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
iulfitle, Reactive ND 25.0
Sample ID LCS-R77544
SampType:
LCS
TestCode:
Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 77544
Client ID: LCSS
Batch ID:
R77544
TestNo:
SW9034
Analysis Date: 1112112017
SegNo: 1327623
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
iulfitle, Reactive 4560 25.0 4800 0 95.0 85 130115
Sample ID 17110481-001AMS
SampType:
MS
TestCode: Sulfide,React Units: mglKg
Prep Date:
RunNo: 77544
Client ID: BatchQC
Batch ID:
R77544
TestNo: SW9034
Analysis Date: 11/2112017
SegNo: 1327625
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
iulfide, Reactive 4470 25.0 4800 0 93.1 SD 120
Sample ID 17110481-001AMSD
SampType:
MSD
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 77544
Client ID: BatchQC
Batch ID:
R77544
TestNo: SW9034
Analysis Date: 11/2112017
SegNo: 1327626
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
4510 25.0
4800 0 . 94.0 80
120
4470 0.891 30
Qualifiers: •
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
I
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
O
RSD is greater than RSDlimit Original
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Page 27 of 36
r�
tRI
sa,,,a;lEnvironmental Technologies, Inc. 3310 Win St.
QC SUMMARY REPORT
cravIaUTunCNia4 t t:CMULUOLS,aG
Cuyahoga Falls, Ohio 44223
WO#: 17110701
Analytdcal Laboralcries TEL: (330) 253-8211 FAX.- (330) 253-4489
Websile: hUR.-Mvinv.sellekcon,
28-NoY 17
Client:
Synagro
Project:
Bladenboro WWTP
BatchID: R77544
Sample ID 17110481-001AMSD
SampType:
MSD
TestCode:
Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 77544
Client ID: BatchQC
Batch ID:
R77544
TestNo:
SW9034
Analysis Dale: 11/2112017
SegNo: 1327626
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLlmit RPD Ref Val
%RPD RPDUrrdt Qual
Qualifiers: • Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation mnge
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected 0 RSD is Original
p greater than RSDlimit
P Second column confirmation exceeds - PL Pormit Limit R RPD outside accepted recovery limits
Page 28 of 36
Ef
LT,
Surmnit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY ^LoRl
crcvlHVNrakNlAL t LCHNat.0a6.5, P;C Cuyahoga Falls, Ohio 44223
Anatyfl:cal taboralwlec TEL: (330) 2S3-8211 FAX.- (330) 253-4489
WO#: 17110701
Website: hun.,114,mv.seaekeom
28-Nov-17
Client:
Synagro
Project:
Bladenboro WWTP
BatchID: R77599
Sample ID MB-R77599
SampType:
MBLK
TestCode: Cyanide,Rea Units: mg]Kg
Prep Dale:
RunNo: 77599
Client ID: PBS
Batch to:
R77599
TestNo: SW9014
Analysis Date: 11/21/2017
SegNo: 1328886
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
;yanide, Reactive ND 0.500
Sample ID LCS-R77599
SampType:
LCS
TestCode:
Cyanide,Rea Units: mglKg
Prep Date:
RunNo: 77599
Client ID: LCSS
Batch ID:
R77599
TestNo:
SW9014
Analysis Date: 11/21/2017
SegNo: 1328887
Analyte
Result.
POL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
;yanide, Reactive 1.03 0.500 1.000 0 103 85 110
Sample ID 17110481.001AMS
SampType:
MS
TestCode: Cyanide,Rea Units: mglKg
Prep Date:
RunNo: 77599
Client to: BatchQC
Batch ID:
R77599
TestNo: SW9014
Analysis Dale: 11/21/2017
SegNo: 1328889
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
:yamde, Reactive 0.973 0.500 1.000 0 97.3 81.6 122
Sample ID 17110481-001AMSD
SampType:
INSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 77599
Client ID: BatchQC
Batch ID:
R77599
TestNo: SW9014
Analysis Date: 1112112017
SegNo: 1328890
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowUndt HighLimit RPD Ref Val
%RPD RPDLimit Qual
yanide, Reactive
0.973 0.500
1.000 0 97.3 81.6
122.
0.9730 0 5
Qualifiers: °
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
O
RSD is greater than RSDlimit Original
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Page 29 of 36
\ � r
[,1�
surdrd
33/0WWInin St.
Svmmtt Envirottmen[al Technologies, Inc.rn
QC SUMMARY REPORT
trMHUMA rN W. t br:HW000IL5, RIG
Analyn=l Labaraforleo TEL:.(330)
Cuyahoga Falls, Ohio 44223
253-8211 FAX. (330) 253-4489
V✓0#: 17110701
Website: ht1P.-1A rvtv.se[lekcom
28-Nov-17
Client:
Synagro
Project:
Bladenboro WWTP
BatchID: R77599
Sample ID 17110481-001AMSD
SampType:
MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 77599
Client ID: BatchQC
Batch ID:
R77599
TeslNo: SW9014
Analysis Dale: 11/21/2017
SegNo: 1328890
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HlghUmit RPD Ref Val
%RPD RPDLimit oust
Qualifiers: • Value exceeds Maximum Contaminant Level, B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits
MC Value is below Minimum Compound Limit. ND Not Detected
P Second column confirmation exceeds PL Permit Limit
E Value above quantitationrange
M Manual Integration used to determine
Q RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 30 of 36
Page 31 of 36
CID
M
N
0
O
N
M
N
a)
SOP: Sample Receipt rn
to
Revision:13 m
C.
fL
Effective Date: 07/17/17
Figure 1— Summit Environmental Technologies, Inc.
Cooler Receipt Form, Page 7
Initials of person lnspeciing cooler earl samples:'
Client: r/ �'�` D Order Number, I —2 �( 0] a I
Date Recemad: -1 - / cr-/T a ReceYi,ed: (000 Date cooler(B) opened and samples Inspected: I Lt
Number of Cool-mMoxes: M NIA
Shlpper, di PS DHL Atoms US Postal Walk-in Pickup Other.
Packaging: Peanuts B ISMS Paper Foam None Other.
TapeonwaW_rlbor. /'� N WA
Custody Seals intact Y N QA
C•0.0 in glesfe 0 N . WA
ice_Blue lw resenl bsenl matted WA
Cooler Temperalum IR Gun #16020 Sag CFI°C Temp: S,S-O WA
Ratrological Tesfsglnstnmentsedatpd5127• Y N Nr _ (seepage2forscanresurs)
Use shear par sample. If sample IS> 100 cpm, the Radiological SafetyOffleer must be notified Immediately.
PO-C filled out property L:P N WA
Samples in separate bags Y N - WA
Sample containers intact* D N WA
'If na, list broken samplo(a
Sample laber(s) complete (to; date, eta)
Y
N
NIA
Label(s) agree with CO•C
Y
N
WA
Correct containers used
YO
N
WA
Suisnnt sample received
0
WA
/N�
Sufficient sample for OC
Y
NIA
Samples received wit" holding time
(Y
N
WA
RDonny 40rnL vials=maln bubbles•'
•°Samples
Y
N
WA
with bubbles SSmm are acceptable.
Indicate bubble size
Was client contacted about samples
Y
N
Will client sand new Samples
Y
N
Logged
Page 10 of 12
North Carolina WastewaterlGroundwater Laboratory Certification
Certified Paramete76 Listing
L-aO Nama. SLwar Eq'HroArrlenlor-roehn=g es lnn Cedlf[mle Numirci. 531
Address: 3310 Win Slrect --EReplim Dale. 111 Pi.01T'
Cuyahoga Fall., OH 44223- Expiration 7atu. 92.3f12097
Dote Cf Last Amerdment: Ell, W120 r
[no eoyr.m•-a=b6mate'7. havingduly met:Fu roqui-ampn:a$15ANGAG 21-.7206,Is burrcyeo•tlfcd rc11k. Ile parsrneMsils.ad DDIVA
CERTIFIED PARAMETERS
11ORGANIC
FHp6PWAYE ORTHC
Boo
S W-846 0056 A (Aqucoue)
SM 521 1) B•2001 iAgjetus)
SW646905G A (Non-Aqueousl
CHI ORI()E
_ PHOSPHORL:S, TOTAL
SW345 9056 P. (AJuaoutl
EPA nC 7 Rev 44(1994) (Acueous)
SW -MU 9056 A (Non -Aqueous)
5 W-846 (i070 D (Aquecus)
GO0
- 9W-mu SDtO D(Non.Aqueous;
Ski 5220 C- 397 ±Aq jeous)
F.EEIOJ=_ DISSOLVED 180 O
rLLORfr)E
3M 2540 0.199' (Acueoas)
CPA 300 0• Rev : 1• 1993 (Aqueous)
RESIOJ=. SUSPENDED
SVV-846 gG.96 A :Aluenus}
SM KAD D-199' (.AcueoJS)
SW-84390AF A ;Nnn-AgUeauS)
SILICA
IGNITA.6ILIT'i -
EPA2C0-7•ReV 4.4. IS841AqueaLA7
SW-846 10m (Nor Aqueous)
S W-946 6010 D (Agaaaus I
INORGANIC PHENOLS
S W-S46 6010 D (Non,Aqueous;
EPA L20 1• Rev ' 078 IAQjtcLS)
SULFATE
NITROGEN. NITRATE
EPA NO.D. Rev. 2.1. 1G03 (Aqueous)
EPA 300 0. Ruv. 2 1 • ; S931A i2mus)
SW-840 S050 A (Aqueous)
SVJ-845 9056 A ;Aqueuu5;
9W.R46 A0 61 A (Non-Aqueaus)
SW-045 0056 A:Non,Aquerus)
9ULPIOF
NITROGEN. NITRITE
5W-046 0034 (Aqueous)
I:FA 300 0. Rev. 2 1 :993 (Agjeolls)
S W-846 0084 (Non-Ageeouy;
9W-045 905E A ;Aqueous;
RIETAL
SVV-843 905E A ;Na1-A.queoue)
TCLP METALS
N17RQmEN. NOS ^ NO2 '
31*440 1311 (Aqueaus)
F.PA3000 R,v.21 19931Agacvuu;
AL IWINL'M
SW-946 9C5E A ;ASueoms:
FPA. 900 7, Rev. 4.4 1994 (P.yuruus)
SVd4e6 DL'Sti A ;NL••1-Aquaaus)
SW.049 6013 D rkwou5)
NI'; HOO(:.L. I0-AL KJELDAHL
S'N-849 b013 D (Nan-AgLeuuM
SM 4500 No,g 9-' 907 (GM 4500 NH3 D-I D07) (Aqueous)
EPA 200.8, Rev. 9.4 1994 (Aqueous)
OIL 8 GREASE
SIN 046 6021) R (AquewE)
CPA 11104 Rev B-;Acuepu$)
S'N•84660205(Nan-Ayoeousj
9w-848 9071 F. {Nno-Aquenus)
ANTIMONY
PH
EPA 200.7• Rev. 4.4 1994 (Aqueous)
SW-846 904E E•;Non-Aqueous)
S'N-04E 601;1 D (Aqunrn.$)
Tres u.»Sc;?r rrc. 25raiamne; Manaweptaoa valiyasa.ra-pe p-aq:em Sae OFappM0. rr-ll de'a=y per enesanlbr:matt-al;nn Fr•idmrAarc
e_.q:Port1- in lEA nCAC2h.0BU.
(v
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North Carolina Wastewater/Groundwater Laboratory Certification
CerNfied Parameters Listing
Lab• Narrz. Surmi: Fmironi -mtal TeChraloDees Inc.
Address: 231a Wm Str=el
Cuyahoga -ally. CH 4422i-
lne 2:a'e named IM 2t0ry h.uine 4U} mul the rMuirpr is of 1bA N::AC:2H)dW.0'10TP7yaadBled to•Ce mBsaah-raaM ellhe pa3no%ri lw.w babw.
CERTIFIED PARAMETERS
SW-84E 6010 D (Von-Aq,+ecue)
EPA 2W.8, Rev, 54, 1994 (Aqueousl
SW-946 6020 B (Aqueoua;
SLV-94C 6020 B (Ncr•AuuaoL�)
ARSEN C
FPA Inn 7, Rev. 4A. 1094 (Aquauas)
5L4.646 5210 Or(AgLeau4)
SLY-150 8010 D (Ncn-AquaOLs)
LPA 200 8, 9ev. 5.4, 1994 (Aqueous)
SW-846 6020 B (Aqueousl
SW-540 G720 6 (Hon-AgveoUs)
BARIUM
EPA 2007. Rev 4.4. 1994 Aquenl,$)
SW-80 6010 D (Aqueousl
SW-846 6010 D (Nor -Aqueous}
EPA 200.3. Rev. 5.4, 1994'AgUQou.1)
SVJ-846 W2C E ;Aqueous!
SW-846602C S'Non-Aqueous)
BERYLLILM
EPA 200.$.Rev. 5A. 1934 ;Aquecus)
.i W-845 602C E {Aqueous;
SW-S46602C S;Nq Aquecus)
BURUN
EPA 200.61 Rev'. 5 4 1994 {AgjeC6.9)
S1N-845 6020 E ;Aqueous;
SLV-845 6020 0:Non•A.queousS
CADMIUTA
EOAi00 Y. Rev 44.1994iAq.,QC.S)
SVJ.848 % C. :AgUfauSi
SW-S4S BU70 C jNcnAquequs)
EbA 20u e, Rev 5.4. 1994 (Aq.acsl
SW 84& 6020 9 fAqucaus;
SYd•046 U020 a (Nnn-Aqueo05)
CALCIU%I
EPA 200.7. Rev. 4.4. '9241Aqu=n.$)
SW-346 6010 D {Aqueous}
S•M-3+66010 D INcrinNucous)
CI IROMIUh4 TOTAL
EPA200.7, P,ev. 4.4, 1994 (Aquuuus)
S W-346 6010 D iAq.reau s)
S W-B4fi 6010 0 (Non-Aqueousl
EPA.200.8, Rev. 5.4, 1994 (Aqueous)
SW B46 602D 8 (Aqu: We)
$W-846 60200 (Non-A4Leous)
COBALT
EPA 20.7. Rev 4.4. IS94 (Aqueous)
Svy-346 601C r3 (Agjwua)
SW-840 en1C n (NnnagLeousl
EPA 2LO.e. Rev 5 4.1994 (Aqueous)
SIV!•iti 802D B (Aquooue)
SW-846 602C 13 (Hai-Aaueouei
COPPER
EPA.2 OJ- ROv. 4.4 1994 ;Aqueous)
SW446 GO'" D (Aqueous)
SW-846 60-2 D (Nnn-ACLEOUS)
EPAXO.5. R=_v. 5.4. 199A (Aqueous)
6W-646 6WU B 1A6UeCU8)
SW-846 6020 B (Non Aqucousi
IRON
EPA 2Ce.7. f iev. 4.4. 1994 ;Aq ue Sus)
SW-246 60' 7 D fgquaous)
SW-246 = 3 D fNo:l-AuLeaus)
LEAD
EPA 2C0.7. Rev. 4-d. 1954 (Aqueous)
SW d46 6C10 D fAgneousl
SW 846 6013 0 (Non Aal..ous)
EPA2C0& Rev 53 1594 {Agveousl
SW-646 6023 B ;Aqueous)
SWd46 6023 B ;No,+ Aqueous;
MAGNFSII•;IJ
Carif+cale Nu7,be•
631
Effective Dole
1f1)2017
EBoiraticr. Date:
12f3fy2017
Date o1 Last Armndmen:'
WI W2017
Iris Cer4tealal•C.cuirc�rrtair{j�oa'.•a' a::BF-tdb� 4ualtyai;ct ante pmGram,use of aup!oved Md:"o4obgy ei-j 1s-adoy pe&r-iwoow9%awlloq eame eE Ltmtoree are Subjec. xr:lua pwal( vx d!nr dvm:tiG::allon fo• mlrlGLCm
as Se19' :. 15f, NCA� 2H.CEo:,
North Caroliiia Wasti water/Groundwater Laboratory Certification
Certified Parameters Listing
Lab News Summit Environmen:et Tecnnologle5111C.
Acdre99: 3310 Win SUM..t
Cuy211a97. Falls, 0?1 44?23.
P:e ate+r nsroR1 NScre:oq, naWt9 tluy n el I::e m,;aur,:n,::. d l-A N('Af aFpsOq, �s heres/<'enifie:'nr Na measuremant aft Parenns;'3 fis>=d 1e4+r.
EPA?00 7, Rev. 4.4, 1994 iAqueous;
-RW-UP 5011) D (Aqueousl
SUC-a40 •301D D (Ncr-Aqueous)
MANUANEEE
EPA.200.7 Rey 4,4,'994fAgteous)
SW'-D40 6010 0 (Aqueous)
Sw-840 6010 D Mar•Aqueou+)
EPA 20f. A Rev 5.4. ' 934 CAqueous)
SW-346 6:21T 0 (Aqueous;
SW-9461iU;N 9:Nor,Aqusous)
NERCl1RY
EDA?45 1. Rcv. 3.C, 1094 CAqueous)
SW-346 7470 A :Aqueous;
SW345 747: B :Ncrl-A.queousl
EPA t 531 E (Aqueous)
M(71 V51DENU4
FPA 2D07, Rev. 4.4. 1994 CAgoeous)
SW445601C C:Agt'cqus;
SYJ-a15 GWC C :Non Aqueous)
EPA 2:0.8 Ro 5.4. -W4 CAgjaoI;S)
SW-W 602C B {lwueous)
S'PJ-E4.3 6C2C B (Non -Aqueous)
NICaF1
5'uV.84%i 6C+C D :No"A.queous)
EPA 20U.6. Rev 5.4, 1994 (Ag1EeUR)'
SU'1.845 5C25 9 (Agjeouo )
SW546 SU22 3 M3n-ACUeo:s)
PO i AESIUM
C'A 20D 7. Rep 4.4, 1304 (Aqutc.$)
S'rl-840 W1.1 I iAnl.F Vs)
S'N-845 El M 'I (Nlr-Jlqueq.I8)
SELENIUM
SYJ•S46 bQl J -1 iNun-Aqunojs)
LPA 200 0, Rov. 5.4, '.9D4 (Aqueous)
G'N-846 6020 3 SAquccus)
CERTIFIED PARAMETERS
S47-646 6U'LU B (Non -Aqueous)
SILVER
EPA 20.7, Rcv. 4.4 1004 (Acucous)
SW-640 601110 (Aqusaus)
5W-6400010 D Wqn-AqueaV5'
EPA 2C0.8. R=_v. 5.4 1994 (Acueous}
SW84660 AR(AquP.nus1
SW.846 G020 B(Non•Aqueous)
SOUIUM
EPA 2C0.7. Rev. 4.4 19a4 (Aoueo.lol.
6W6466010 D (Aqueo.ls]
6WLE46 6012 D (Non-Aqutaos;
STRONTIUM
EPA 2C0?, Rdv. 4.4 1S94 (Agoau.-sl
SW-2466U 17 D (AgU8Ou4)
SW-E46 601 J D (Non-AaLeous;
EPA 200.6. Roo. 6.4 1994 (Aqueous)
SW-E46 602D B tAquaoua)
$W,,466023 E (Non-Aquecus)
THALLIUM
FPA 200 7, Rex 44 1494 (Aguen.as)
SW-846 60101)(ACne,)Us]
SW-e46 601 J D (Non -Aqueous;
EPA -ICU U. ttw b.4 1544 CAgueo.ls)
SW-E46602J 9 (Aqucnus)
GW246 602) B (Non-Aquccus)
TIN
EPA 200 7, Rea 4.4 1994 (Aqueous)
S W246 601:1 D (Aquama)
SAr246 6010 D (Non•Aqueous)
VANADIUM
EPA 200 5, Rev 5.4 1994 (Aaueaasl
SW-546 602) B (Agl••eous)
SVJ-50 602D B (Non•A•wecus)
ZI•VO
Certif we NUm:er:
031
Fff,' .rlve NIP,
111120/7
Explratior :lwF,
19:310.117
Date of Last Amendment-
9A91401t
T'ia tl1r19[at!pl gd?SI"dI111nMf.ffa'arr.Pn!.:nle4}it1=s3V4rKe naaraM, gsE et xa::a'2tl mENOEao9i,alJ sah518[Eory pe'Orrtalcea^Eva4•a:cn sar[155.Lam•a:ar ssarE so".;e¢Ic q7n Fera�:R£antlrn•aa;E^iL'xlim fnr PlrtrimS
eL+se: W.111 • °A NOW. N111N..7
North Carolina Wastewater/Groundwater Laboratory Certification
Codified Parameters Listing
Lab Narra: Summi; Envhonmeval Tedlnalogiea Ix.
Address 3310win Street
Cnyahop Falls, Ott 44223-
T•e aoeve n�rmJ r�L.anLrrta�i la ilnly rol:•t^n lr..7iin�nnraa.n :SF Nf,.AC .N Iwm SlrerFCY Lenlflay'rp: IfP mAF.:'YI-"�'�: nrll'F nAIArrINiY.rV Iti:I.fI IY:INI
SW-846 6310 0 (Non -Aqueous)
EPA 200.6, Rev. 5.4 1294 (Ag4e0VS)
SYJ-M 5 902CI B (Aqueous)
EV1-8466020 B(Non-Apueouai
ORGANIC
TCLP ORGANICS
SW-8461311 iAq.leu. )
,AWORBABLE ORGANIC HALIDES
EPA 1650, Rev. C, 1997 (Aqueous)
BAe6 NEVI HA-m mo. ORGANICS
EPA 826 (Aaucous)
.SW9466270 D (Aqueous)
3W-04Gb270 D (Non-AqueoVS)
01ILQRI VATED ACID HFRP.ICIDFR
SW-84G 8151 A (Asuan.Is7.
SW-640 8151 A (Nan AgjeoLS)
CHLORINATED PHENOLICS
EPA 1BE$ Rev. A 1 U67 (Apcovoj
EXTRACTABLE PETROLEUM HYDROCARBONS
MADEP. rdsq 20L'4, Rev. 1.1 :Aqueous)
NONHA,LOGCNAI'CD VOLATILE. OR:ANIC.S
SkV•846 EWE C (AgLuo4s)
PESTICIDES, 0RGA.NOCHLORINE
EFA 608 �,AgLEOLS)
S1'Y•CJ68081 B(Acueoosf
SVV-VG 8G81 6 (Non AaUCoua1
PO.-YCHLORINATED 6,Pi-ENYLS (P03s!
. EPA 008 (Aqueous)
a^W-846 8082 A (Ruucuusl '
SW-P46 8087 A (Non-Aelleo,S)
PIIR(i=AXLE QRGANICS
EPA ti24.AqueOus)
SW 84G6260 B'AuLcousl
SLV 8488260 B (Aon,AqueDus)
TOTAL ORGANIC rIAL10ES
_ — CERTIFIED PARAMETERS
SV!-84d 9U2L• B!Ag3ecusl
IPh U hStL RANGE, ORGANICS
SX-846 8818 C'Aqueous;
S W-648 8012 O ;Nor•A.quewsl
7PFi GASOLIAERANGE, GR3ANICS
Sif!-&58 8010 C :Aqueuux;•
SV!-H40 801 E C ;Nur-Ayueoux)
VOLATILE FETROLEUM HYDROCARBONS
t.4ADEP May 2004, Rev. 1.1 (Agjamsj
Certificate NLmbcr:
631
Effective Dam-
111/2017
Fxpim ion Ode
12C1r2017
Date of Las! Amendment
9t 912017
m1s renlrL^9l:er'equrux-mwwj.ror.'Hear;eplkle gl.alp•xssl'ra"orppp. ise ete_prW.dmellxxdoap era sel 5ari•)pertnmarc+A^.nual:mil•:n R'-...--y Ixhnclu:n•Saio CullrCl uoevl pP.rRdieS 6rffiftlPC.P.n'le3ao'ro!l:'•'dG11an5
59 9P.1-wh in l5A v:4 JH nm,
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Bladenboro WQ Permit Number: W00014452
r WWTPName: BladenboroWWTP NPDESNumber: NC0026352
Monitoring Period: From OU01/2017 To 12/31/2017
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106)- Please indicate level achieved and alternative performed:
Class A:
Alt. I/A (time/temp)
Alt. 4/D (No Prior Test)
Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 5/Process to Further Reduce Pathogens _ ,Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only). indicate "Process to Further Reduce Pathogens":
Compost _ Heat Drying _ Heat Treatment _ Thermophilic
Beta Ray _ Gamma Ray — Pasteurization —
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting _ Aerobic Digestion
Anaerobic Digestion
at appitcame to arernanve periormea ku
ass A or umss ticom iere me InHowing monnorm
t ama:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2xl0 to the 6
MPN
MPN/g
Coliform
power per gram
of total solids
67600
110000
145000
CFU/g
0
Once a
grab
9222D -
CFU
year
MF
1000 MPN per gram of
MPN/g
total solids (dryweight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
'
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
Option/Mt. 6
Option/Alt 7 Option/Alt. 8
(14-Day Aerobic)
(A1kStabthzation)
(Drying —Stable) (Drying —Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection) _
(Incorporation) X
No vector attraction reductionalternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met I am aware that there are significant. penalties for false certification including fine and imprisonment."
A/ L, 3n ktz=r� D �C Todd LWaftftAftAirckor
t' Pr Lland�i[le (type or print _ Lan ie Q applicably pr'
6WYa?6re ofPreparer* Date Signature of Land Applier (if applicable) Date
*Prepares is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Cameron Testing Services, Inc.
Laboratory Report
NO OENR#554
NCPHHS#37799
Glrenf'
Synagro
C3S Prod 171930
US EPA #NC01918
ro�ect
t
Bladenboro
�L2ebb Ot�orry ' Yes
!
-
0M_ *
Sample
Information
_
Sam�led'S1
C. Hayes x� bate,;
"11/13/173iecelvgd j G. Cameron 1 date'
11/13/17
Analyses and Results
171930 01
a Sludge Gr •-
Fec:Colifcrrn-S
• <125000
cWts
125000 11/14/17 ERP 9222D-MF
r
b
<67600
OFUfg
676.00
'
C
<125000
CFUfg
125000
d
<92600
MID
92600
e
<145000
CFU/g,
145000
'
f
<122000
CFUfg
122000
9
<116000
cFU19
116000
Geomean
<110000
LL�
rf 1 171930 01
a sludge or
TS (e/u)
2.84%
0.01 11/14/17 ERP 2540 G -TS
b
5.29%
o.0f
C
2.30%
0.01
d
3.66%
0.01
e
2.87%
0.01
f
2.830W
0.01
g
2.86%
0.01 ..
- Report
ReviewY12Q�
Project Manager
.210. S. Steele Ste.
914-2084240
Sanford NC 27330
chds& merentesting,com
219S.Steele str. Cameron Testing Services, Inc. Chain of Custody
Sanford, NC 27330
Phone: 919-208.4240 NC WW(GW Cent. 9654 NC PHHS cent #37799 US EPA NC01918 Page of t
C m an
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gadstclty;
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Email
I
Phone•
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Notes
Cha es s na ro.com
_ Y °Q Y 9
919-799-0766�-
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Pro) :i' q 7
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rover
ore "
tf , . o;4ViN C�-0
ce�]»e..n-ere.r 0. ed
284 Boger Rd.
Mocksville, NC 27028
Bladenboro
�rColleeted��Name:
CIAJ 14 � Signature:
{h�,Jn'Itl]9
r�ti
I-Z.+. _.t:7`>'.+i,,Idx
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m o I r °
Preservatives (U)np(esenved H(C)J' rill
`(S 1 , 3
H2(S)04iIH(N)g3 ,(Na)7hmsulfate Na(0)N{),I1rD�
S+�rt`t,a,l+ '�Olher(X),Indlcate' N`�
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Rush work will require prior approval. Additional charges will apply
1 ) Agricultural Lime Application Log
Year: 2017
Project:
Town of Bladenboro
Field
(state -county -site -field code)
Soil pH
Lime Requirement,
(from soil analysis)
Tons/Acre
Applied
Date Applied
NC-BL-03-03
6.6 1 0.0
NC-BL-03-04
6.0 0.0
Page 1 of 2 '-
Report Number: 18-033-0519
Account Number:46437
Send To: Synagro Central LLC/ Bladenboro
Marshal Puryear
284 Boger Road
Mocksville NC 27028
j
Waypoint_
ANALYTICAL
"Every acre ... Everyyear."rxr
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 p Fax 804.271.6446
www.waypointanalytical.com
Grower: Bladenboro
Farm ID/Name: Bladenboro
SOIL ANALYSIS REPORT AnalyticalMethod(s): Mehlich3 SMPBufferpH LossOnlgnition WaterpH
Date Received: 02/02/2018 Date Of Analysis: 0210512018 Date Of Report: 02/07/2018
OM
WN
ENR-
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Field ID
Lab
Number
Rate
Soil
Class
Ibs1A
M3
ppm Rate
ppm Rate
ppm Rate
K
ppm Rate
M 9
ppm Rate
Ca
ppm Rate
Na
ppm Rate
Soil
PH
Buffer
Index
H
meq/106g
meq/100g
3
01196
2.0
L
84
285 VH
NC=237
66 M
NC=34
70 M
672 H
12 VL
6.6
0.3
4.5
MIN
4 1
01197
2.5
L
94
226 VH
NC=188
89 M
NC=46
54 M
542 M
19 VL
6.0
0.6
4.1
MIN
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble salts
Sample
FieID ID e
K
%
Mg
%
Ca
%
No
%
H
%
NO3 N
ppm Rate
S
ppm Rate
Zn
ppm Rate
Mn
ppm Rate
Fe
ppm Rate
Cu
ppm - Rate
B
ppm Rate
SS
ms/cm Rate
3
3.8
13.0
74.7
1.2
6.7
9 VL
NC=19
12.0 VH
NC=300.0
5 L
NC=31
256 VH
7.3 VH
NC=365.0
0.5 L
0.12 VL
4
5.6
1 11.0
1 66.1
1 2.0
14.6
17 M
NC=35
9.4 VH 1
NC=235.0
6 L
NC=38
245 VH
6.1 VH
NC=305.0
0.5 L
0.11 VL
Values on this report represent the plant available nutrients in the
soil. Rating after each value: VL (Very Low), L (Low), M (Medium),
H (High), VH (Very High). ENR- Estimated Nitrogen Release..
C.E.C. - Calton Exchange Capacity.
Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retaineda
(pounds per acre), ms/cm(milli-mhos per centimeter),meq/t00g maximum ofthirty days after testing. by. Ppuric m°��
(milli -equivalent per 100 grams). Conversions: ppm x 2= Ibs/A, Soluble Salts ms/cm x 640 = ppm. Analysis prepared by. WaypointAnaly(Ical Nrginie, Inc.
Pauric McGroary
. j
Page 2 of 2
Report Number: 18-033-0519
Account Number:46437
Send To: Synagro Central LLC/ Bladenboro
Marshal Puryear
284 Boger Road
Mocksville NC 27028
Date Received: 02/02/2018
Date Of Report: 02/07/2018
7621 Whitepine Road, Richmond, VA 23237
Waypoi ■■M■ t Main 804-743-9401 a Fax 804-271-6446
ANALYTICAL www.waypointanalytical.com
"Every acre...Everyyear.",v Grower: Bladenboro
Farm ID/Name: Bladenboro
SOIL FERTILITY RECOMMENDATIONS
Nitrogen
Phosphate
Potash
Magnesium
Sulfur
Zinc
Manganese
Iron
Copper
Boron
FFiemldp7ID
Intended Crop
Yield Goal
Lime
N
P205
K20
Mg
S
Zn
Mn
Fe
Cu
B
TonslA
Ib/A
IbIA
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
lb/A.
IbIA
Ib/A
3
Adjust pH to 6.0
0
0.0
0
3
0
4
Adjust pH to 6.0
0
1 0.0
11
3
0
Comments:
Sample(s) : 4 Crop: Adjust pH to 6.0
Apply required magnesium with magnesium oxide, Epsom Salts, K-Mag or Sul-PO-Mag.
'The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or Implied, concerning crop performance is made."
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced In whole or part, nor may any reference be made to the Pod. me 600"
work,lhe results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Paul McGroary