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WQ0000672_2016 Annual Report_20170214
FEB 2 7 2017 Iriormat crn Froc ;u,� Unit .. G'a'u R :i3C:1011 RECEIVED DEQIDWR MAR 0 S 2017 WQROS CITY OF LUMBERTON, NC FAYEI7EVILLEREGIONAL OFFICE RESIDUALS LAND APPLICATION PROGRAM Permit No. WQ0000672 2016 ANNUAL REPORT City of Lumberton, NC Residuals Land Application Program 2016 Annual Report TABLE OF CONTENTS 1. Certification Form and Annual Operations Summary 2. Annual Residual Sampling Summary Forms, Residuals Analyses, & SAR Calculation Pages 3. Annual Land Application Field Summary Forms r 4. TCLP Analysis a J 5. Pathogen Reduction/Vector Attraction Reduction 6. Soil pH & Lime Application Records 7. Soil Analyses ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit #: W00000672 County Robeson Year 2016 ' Facility Name (as shown on permit) City of Lumberton W WTP &WTP NPDES No. NC0024571& 03-78-010 Land Application Operator Svnaero Phone# (336) 998-7150 Land application of residuals as allowed by the above permit occurred during the past calendar year? X YES NO. IfNO, slip PartA, and Part B and proceed to Part C. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A — Residuals Application Summary: Total number of application fields in the permit: 83 Total number of fields utilized for land application during the year: 18 - Total amount of dry tons applied during the year for all application sites: 843.62 Total number of acres utilized for land application during the year: 366.5' Part B — Annual Compliance Statement: Facility was compliant during calendar year2016 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality X YES No. If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit 3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .I 105(b) (Applicable to 40 CFR Part 503 regulated facilities). ,.� 7. AN general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All monitoring and reporting requirements in 15A NCAC 02T .I I I I were complied with (applicable to 40 CFR Part 503 regulated facilities). 9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10. No contravention of Ground Water Quality Standards occurred at monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit , 12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13.. All buffer requirements as specified on the permit were maintained during each application of residuals. Part C — Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Jim Walters. Director ofEUS Dept. W • 4,5 ' ao17 Permittee Name and Title (type or print) i ' fP r e ate _ i 2017 Signature of Preparer' Date Sigrikure of Land Aprier • Date (if different from Permittee) (if different from Perrnittee and Preparer) •Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) 2016 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION LUMBERTON, NC LUMBERTON, NC WWTP AEROB. DIGESTED LIQUID DRY METRIC MONTHNEAR AMOUNT UNIT DRY TONS UNIT TONS March 2016 2,070,800.00 G 274.60 D 249.06 April 2016 1,252,400.00 G 166.08 D 150.63 May 2016 173,600.00 G 23.02 D 20.88 September 2016 1,066,400.00 G 43.57 D 39.53 October 2016 595,200.00 G 24.32 D 22.06 November 2016 2,058,400.00 G 84.13 D 76.31 YEARLY TOTAL 7,216,800.00 G 615.72 D 558.47 LUMBERTON, NC WWTP LIME STABILIZED LIQUID DRY METRIC MONTHNEAR AMOUNT UNIT DRY TONS UNIT TONS July 2016 1,891,000.00 G 227.90 D 206.69 YEARLY TOTAL 1,891,000.00 G 227.90 D 206.69 1/31/2017 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0000672 Facility Name: LUMBERTON, NC NPDES# : NCO024571 or WQ# (residual only) WWTP Name: LUMBERTON WWTP Residuals Analysis Data Product Type - AEDLIQ Date Sampled (grab) or 01/21/16 Date Composited Percent Solids 3.18 PARAMETERS (mg/kg dry weight) Arsenic Cadmium Mercury Chromium Copper Lead Molybdenum Nickel Selenium Zinc Total Phosphorus TKN Ammonia -Nitrogen Nitrate and Nitrite 5 3 0.4 270 361 16 8 40 <5 448 19800 58800 4090 264 Laboratory WAYPOINT ANALYTICAL Waypoint Analytical Virginia Inc. AEDLIQ LSLIQ AEDLIQ 05/25/16 07/22/16 08/09/16 2.55 2.89 0.98 5 4 6 <2 <2 <2 <0.4 <0.4 <0.4 196 129 184 352 248 363 18 13 20 5 <5 5 33 21 31 <5 <5 <5 531 356 448 19300 14300 21000 54100 4840 46900 5880 1730 <10 <2 4360 7640 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." M Date a' ly' -Za DENR FORM RSSF (6/2003) Printed: Tuesday- January 31. 2017 at 10:43:33 for: 2101 01 .rr ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. PermitiNumber: WQ0000672 Laboratory Facility Name: LUMBERTON, NC WAYPOINT ANALYTICAL NPDES# : NCO024571 Waypoint Analytical Virginia Inc. or WQ# (residual only) WWTP Name: LUMBERTON WWTP Residuals Analysis Data Product Type AEDLIQ AEDLIQ LSLIQ AEDLIQ Date Sampled (grab) or 01/21/16 05/25/16 07/22/16 08/09/16 Date Composited Percent Solids 3.18 2.55 2.89 0.98 PARAMETERS (mg/kg dry weight) Aluminum 31700 31300 37800 39900 Calcium 11500 11500 132000 13400 Magnesium 2650 2600 3400 1860 pH 6.74 7.15 11.45 6.11 Potassium 3950 4660 3420 2770. Sodium 8240 7550 6810 6780 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Date _ a • ./ S , al 7 NR - Data Not Reported or Data Not Required DENR FORM RSSF-B (712002) Printed: Tuesday -January 31, 2017 at 10:44:05 for: 2101 01 Page: 1 of 2 Report Number: 16-025-0200 Account Number: 46525 Send To: SYNAGRO CENTRAL LLC/LUMBERTON Mary Brewer 284 BOGER RD MOCKSVILLE, NC 27028 Lab Number: 66411 Sample Id: LUMBERTON WWTP BASIN WaypointM 0 ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743.9401 ° Fax 804-271-6446 www.waypointanalytical.com Project: LUMBERTON W WTP BASIN NC CERT# 257 REPORT OFANALYSIS Date Sampled: 1/21/2016 17:45:00 Date Received: 01/25/2016 00:00 Date Reported: 01/28/2016 Total Solids 3.18 31800 100.0 JM 01/25/2016 13:30 SM-2540G Moisture. 96.82 100.0 JM 01125/201613:30 SM-2540G Total Kjeldahl Nitrogen 5.88 58800 10.0 JM 01/26/2616 08:50 SM-4500-NH3C-TKN Total Phosphorus 1.98 19800 100 KM 01/26/2016 12:09 SW 6010C Total Potassium 0.40 3950 100 KM 01/26/2016 12:09 SW 6010C Total Sulfur 1.01 10100 100 KM 01/26/2016 12:09 SW 6010C Total Calcium 1.15 11500 100 KM 01/26/2016 12:09 SW 6010C Total Magnesium 0.27 2650 100 KM 01/26/2016 12:09 SW 6010C Total Sodium 0.82 8240 100 KM 01/26/2016 12:09 SW 6010C Total Iron 18800 100 KM 01/26/2016 12:09 SW 6010C Total Aluminum 31700 100 KM 01/26/261612:09 SW 6010C Total Manganese 127 5 KM 01/26/2016 12:09 SW 6010C Total Copper 361 5 KM 01/26/2016 12:09 SW 6010C Total Zinc 448 5 KM 01/26/2016 12:09 SW 6010C Ammonia Nitrogen 0.41 4090 10.0 JM_ 01/26/2016 08:50 SM-4500-NH3C Organic N 5.47 54710 10.0 01/26/2016 08:50 CALCULATION Nitrate+Nitrite-N 264 2.00 JM 01/26/2016 08:50 SM-450ONO3F Total Cadmium 3.0 2.0 KM 01/26/2016 12:09 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced In whole or part, normay any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining ourpriorwritten authorization. Debbie Holt Page: 2 of 2 Report Number: 16-025-0200 Account Number: 46525 Send To: SYNAGRO CENTRAL LLC/LUMBERTON Mary Brewer 284 BOGER RD MOCKSVILLE, NC 27028 Lab Number: 66411 Sample Id: LUMBERTON WWTP BASIN WaypointryG' ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical.com Project: LUMBERTON WWTP BASIN NC CERT# 257 REPORT OF ANALYSIS Total Chromium 270 5 KM Total Nickel 40 5 KM Total Lead 16 5 KM Total Arsenic 5.0 3.0 KM Total Mercury 0.4 0.4 KM Total Selenium <5.0 5.0 KM pH (Standard Units)" 6.74 2.00 JM Total Volatile Solids 73.03 730300 100.0 JM Total Molybdenum 8 5 KM Comments: QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "CO AND "Na". ALL OTHER QC DATA IS ACCEPTABLE. ,Date Sampled: 1/21/2016 17:45:00 Date Received: 01/25/2016 00:00 Date Reported: 01128/2016 01/26/2016 12:09 SW 6010C 01/26/2016 12:09 SW 6010C 01/261201612:09 SW 6010C 01/26/2016 12:09 SW 6010C 01/27/201609:00 SW-7471B 01/26/2016 12:09 SW 6010C 01/26/2016 08:50 SW-9045D 01/25/201613:30 SM-2540G 01/26/2016 12:09 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Ourreports and letters are rorthe exclusive and confitlentlal use otourclients, and may not be reproduced in whole orpalt, normay any reference be made to the work, the results, or the company In eny advertising, news release, or other public announcements without obtaining ourprior written authodzefion. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name. Sample Date ReportRange Ratio 2101-01-AEDLIQ-NC LUMBERTON, NC WWTP AEROB. DIGESTED 1/21/2016 11112016-5/3112016 3.2027 LIQUID Na mgll = (Na mg/kg x % Solids) + 100 = (8240 x 3.1800) + 100 = 262.032 Ca mg/l = (Ca mg/kg x % Solids) + 100 = (11500 x 3.1800) + 100 = 365.7 Mg mgA = (mg mg/kg x % Solids) + 100 = (2660 x 3.1800) + 100 = 84.27 Na meq = Na mgA + Molec.Wgt.Na = 262.032 + 23 = 11.3927 Ca meq = Ca mgA + Molec.Wgt.Ca = 365.7 + 20 = 18.285 Mg meq = Mg mgA + Molec.Wgt.Mg = 84.27 + 12 = 7.0225 SAR = Na meq +SgrRoot[0.5 x (Ca meq + Mg meq)] = 11.3927+ Sgdtoot[0.5(18.285+7.0225)] = 3.2027 Printed: 2/3/2017 Page 1 10:11 Page: 1 of 2 Report Number: 16-153-0205 Account Number: 46525 Waypoint.. 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Send To: Synagro Central LLC/ Lumberton Project: Lumberton W WTP Mary Brewer NC Cert#257 284 Boger Road Mocksville , NC 27028 REPORT OFANALYSIS Date Sampled: 5/25/2016 10:30:00 Lab Number: 57531 _ Date Received: 06/01/2016 00:00 Sample Id : Lumberton WWTP _ Date Reported: 06/08/2016 Total Solids * 2.55 25500 100.0 RD 06/01/2016 14:24 SM-2540G Moisture * 97.45 100.0 RD 06/01/2016 14:24 SM-2540G Total Kjeldahl Nitrogen 5.41 54100 10.0 DH 06/02/2016 07:30 SM-4500-NH3C-TKN Total Phosphorus 1.93 19300 100 KM 06/02/2016 12:19 SW 6010C Total Potassium 0.47 4660 100 KM 06/02/2016 12:19 SW 6010C Total Sulfur 0.89 8940 100 KM 06/02/2016 12:19 SW 6010C Total Calcium 1.15 11500 100 KM 06/02/2016 12:19 SW 6010C Total Magnesium 0.26 2600 100 KM 06/02/2016 12:19 SW 6010C Total Sodium 0.76 7550 100 KM 06/02/2016 12:19 SW 6010C Total Iron 13400 100 KM 06102/201612:19 SW 6010C Total Aluminum 31300 100 KM 061021201612:19 SW 6010C Total Manganese 90 5 KM 06/02/2016 12:19 SW 6010C Total Copper 352 5 KM 06/02/2016 12:19 SW 6010C Total Zinc 531 5 KM 06/02/2016 12:19 SW 6010C Ammonia Nitrogen 0.59 5880 10.0 DH 06/02/2016 07:30 SM-4500-NH3C Organic N 4.82 48220 10.0 06/02/2016 07:30 CALCULATION Nitrate+Nitrite-N _ <2.00 2.00 DCH 06/02/2016 07:30 SM-450ONO3F Total Cadmium <2.0 2.0 KM 06/02/2016 12:19 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. &Uftez- to Ourreports andletters are lorthe exclusive and confidential use of ourclients; andmaynot be reproducedin whole orpart, normayanyreference be made the work; the results, orthe company in any advertIsing, news release, orotherpubtic announcements without obtaining ourprlormitten authorization. Debbie Holt Page: 2 of 2 Report Number: 16-153-0205 Account Number: 46525 Send To: Synagro Central LLC/ Lumberton Mary Brewer 284 Boger Road Mocksville , NC 27028 Lab Number: 57531 Sample Id : Lumberton W WTP Waypoint.. ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446- www.wayp ointanalytical.com Project: Lumberton W WTP NC Cert#257 1:7�7�7:ir7 Idh_IFQW69 Date Sampled: 5/25/2016 10:30:00 Date Received: 06/01/2016 00:00 Date Reported: 06/08/2016 Total Chromium 196 5 KM 06/02/2016 12:19 SW 6010C Total Nickel 33 5 KM 06/02/2016 12:19 SW 6010C Total Lead 18 5 KM 06/02/2016 12:19 SW 6010C Total Arsenic 5.0 3.0 KM 06/02/2016 12:19 SW 6010C Total Mercury <0.4 0.4 KM 06/02/2016 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 06/02/2016 12:19 SW 6010C pH (Standard Units) • 7.15 2.00 RD 06/02/2016 07:30 SW-9045D Total Volatile Solids 69.49 694900 100.0 RD 06/01/2016 14:24 SM-2540G Total Molybdenum 5 5 KM 06/02/2016 12:19 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE LCS WAS OUT OF LIMITS FOR "Ni". THE LRB WAS OUT OF LIMITS FOR "Mn", "Mo", AND "Ni". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Ourmpods and letters are for the exclusive and conhdenfial use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company In any advertising, news release, orotherpub/Ic announcements without obtaining ourprior written authothrodon. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date ReportRange Ratio 2101-01-AEDLIQ-NC LUMBERTON, NC WWTP AEROB. DIGESTED 5/2512016 6/112016-813112016 2.6347 LIQUID Na mg/I = (Na mg/kg x % Solids) + 100 =. (7550 x 2.5500) + 100 = 192.525 Ca mg/l = (Ca mg/kg x % Solids) + 100= (l l500 x 2.5500) + 100.= 293.25 Mg mg/I = (mg mg/kg x % Solids) + 100 = (2600 x 2.5600) +.100 = 66.3 Na meq = Na mg/I + Molec.Wgt.Na = 192.525 + 23 = 8.37065 Ca meq = Ca mg/I + Molec. Wgt.Ca = 293.25 + 20 = 14.6625 Mg meq = Mg mg/I + Molec. Wgt.Mg = 66.3 + 12 = 5.525 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 8.37065 + SgrRoot[0.5(14.6625+5.525)] = 2.63471 Printed: 2/3/2017 Page 1 10:12 Page: 1 of 2 Report Number: 16-204-0209 Account Number: 46525 Submitted By: Marshall Puryear Send To: Synagro Central LLC/ Lumberton Mary Brewer 284 Boger Road Mocksville, NC 27028 Waypointry ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical.com Project: Lumberton W WTP NC Cert#257 REPORT OFANALYSIS Date Sampled: 7/22/2016 10:00:00 Lab Number: 58518 Date Received: 07/22/2016 00:00 Sample Id: Lumberton W WTP Lime Date Reported: 08/02/2016 Total Solids ` 2.89 28900 100.0 JM 07/22/2016 16:00 Moisture * 97.11 100.0 JM 07/22/2016 16:00 Total Kjeldahl Nitrogen 0.48 4840 10.0 JNt 07/27/2016 13:59 Total Phosphorus 1.43 14300 100 KM 07/25/2016 10:49 Total Potassium 0.34 3420 100 KM 07/25/2016 10:49 Total Sulfur 1.00 10000 100 KM 07/25/2016 10:49 Total Calcium 13.20 132000 100 KM 07/25/2016 10:49 Total Magnesium 0.34 3400 100 KM 07/25/2016 10:49 Total Sodium 0.68 6810 100 KM 07/25/2016 10:49 Total Iron 12800 100 KM 07125/201610:49 Total Aluminum 37800 100 KM 07/25/2016 10:49 Total Manganese 136 _ 5 KM 07/25/2016 10:49 Total Copper 248 5 KM 07/25/2016 10:49 Total Zinc 356 5 KM 07/25/2016 10:49 Ammonia Nitrogen 0.17 1730 10.0 JM 07/28/2016 12:09 Organic N 0.31 3110 10.0 07/27/2016 13:59 Nitrate+Nitrite-N 4360 2.00 JM 07/25/2016 08:35 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or otherpublic announcements without obtaining our pdor written authorization. SM-2540G SM-4500-NH3C-TKN SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SM-4500-NH3C CALCULATION SM450ONO3F Debbie Holt Laboratory Supervisor Page: 2 of 2 Report Number: 16-204-0209 Account Number: 46525 Submitted By: Marshall Puryear Send To: Synagro Central LLC/ Lumberton Mary Brewer 284 Boger Road Mocksville, NC 27028 Waypoint..0 ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical.com Project: Lumberton WWTP NC Cert#257 REPORT OFANALYSIS Date Sampled: 7/22/2016 10:00:00 Lab Number: 58518 Date Received: 07/22/2016 00:00 Sample Id: Lumberton WWTP Lime Date Reported: 08/02/2016 Total Cadmium <2.0 2.0 _ KM 07/25/2016 10:49 SW 6010C Total Chromium 129 5 KM 07/25/2016 10.49 SW 6010C Total Nickel 21 5 KM 07/25/2016 10:49 SW 6010C Total Lead 13 5 KM 07/25/2016 10:49 SW 6010C Total Arsenic 4.0 3.0 KM 07125/201610:49 SW 6010C Total Mercury <0.4 0.4 JR 07128/201611:30 SW-7471B Total Selenium <5.0 5.0 KM 07/25/2016 10:49 SW 6010C pH (Standard Units)11.45 2.00 JM 07/25/2016 08:35 SW-9045D Calcium Carbonate Equivalent 32.60 326000 100 RD 07/26/2016 09:29 AOAC 955.01 Total Molybdenum <5 5 KM 07/25/2016 10:49 SW 6010C Comments: CCE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE LCS WAS OUT OF LIMITS FOR "Se". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Cr" AND "NI". THE MSD WAS OUT OF LIMITS FOR "TKN" AND "Cr". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced In whole orpmt, nor may any reference be made to the work, the results, or the company In any advertising, news release, or other public announcements without obtalning ourpiior written authorization. Debbie Holt Laboratory Supervisor Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2101.01-LSLIQ-NC LUMBERTON, NC WWTP LIME STABILIZED 7/22/2016 711/2016-713112016 0.8580 LIQUID Na mg4 = (Na mg/kg x % Solids) + 100 = (6810x 2.8900) + 100 = 196.809 Ca mg/I = (Ca mg/kg x % Solids) + 100 = (132000 x 2.8900) + 100 = 3814.8 Mg mg/1= (mg mg/kg x % Solids) + 100 = (3400x 2.8900) + 100 = 98.26 Na meq = Na mg/1 + Molec.Wgt.Na = 196.809 + 23='8.65691 Ca meq = Ca mg/1 + Molec.Wgt.Ca = 3814.8 - 20 = 190.74 Mg meq = Mg mg/I + Molec.Wgt.Mg = 98.26 + 12 = 8.18833 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 8.56691 + SgrRoot[0.5(190.74+8.18833)] = 0.857993 1� Printed: 2/3/2017 Page 1 10:14 } Admik Page: 1 of 2 Report Number: 16-224-0206 Account Number: 46525 Send To: Synagro Central LLC/ Lumberton Mary Brewer 284 Boger Road Mocksville, NO 27028 Lab Number: 58905 Sample Id :Lumberton WWTP Waypoint(21 . ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743.9401 a Fax 804-271-6446 www.waypointanalytical.com Project: Lumberton WWTP Plant NO Cert #257 REPORT OFANALYSIS Data Sampled: 8/9/2016 15:20:00 Date Received: 08/11/2016 00:00 Date Reported: 08/18/2016 Total Solids 0.98 9800 100.0 RD 08/11/2016 14:50 SM-2540G Moisture' 99.02 100.0 RD 08/111201614:50 SM-2540G Total Kjeldahl Nitrogen 4.69 46900 10.0 SB 08/12/2016 08:50 SM-4500-NH3C-TKN Total Phosphorus 2.10 21000 100 KM 08/12/2016 14:14 SW 6010C Total Potassium 0.28 2770 100 KM 08/12/2016 14:14 SW 6010C Total Sulfur 0.92 9170 100 KM 08/12/2016 14:14 SW 6010C Total Calcium 1.34 13400 100 KM 08/12/2016 14:14 SW 6010C Total Magnesium 0.19 1860 100 KM 08/12/2016 14:14 SW 6010C Total Sodium 0.68 6780 100 KM 08/12/2016 14:14 SW 6010C Total Iron 20900 100 KM 08/12/2016 14:14 SW 6010C Total Aluminum 39900 100 KM 08/12/2016 14:14 SW 6010C Total Manganese 189 5 KM 08112/2016 14:14 SW 6010C Total Copper 363 5 KM 08/12/2016 14:14 SW 6010C Total Zinc 448 5 KM 08/12/2016 14:14 SW 6010C Ammonia Nitrogen <10.0 10.0 SB 08/12/2016 08:50 SM4500-NH3C Organic N 46900 10.0 68/12/2016 08:50 CALCULATION Nitrate+Nitrite-N 7640 2.00 SB 08/12/2016 08:50 SM-450ONO3F All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. (S? Ourmicods and letters are for the exclusive and confidential use of our clients, and may not be mlimduced in whole orpad, nor may any reference be made &a to the work the results, orthe companyin any advertising, news release, orother public announcements without obtaining ourprior written aulhorization. Debbie Holt Laboratory Supervisor Page: 2 of 2 Report Number: 16-224-0206 Account Number: 46525 Send To: Synagro Central LLC/ Lumberton Mary Brewer 284 Boger Road Mocksville , NC 27028 Lab Number: 58905 Sample Id : Lumberton WWTP Waypoint. ANALYTICAL 7621 Whitepine Road, Richmond, VA23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointandlytical.com Project: Lumberton W WTP Plant NC Cert #257 REPORT OFANALYSIS Date Sampled: 8/9/2016 15:20:00 Date Received: 08/11/2016 00:00 Date Reported: 08/18/2016 Total Cadmium <2.0 2.0 KM 08/12/2016 14:14 SW 6010C Total Chromium 184 5 KM 08/12/2016 14:14 SW 6010C Total Nickel 31 5 KM 0811212016 14:14 SW 6010C Total Lead 20 5 KM 08/12/2016 14:14 SW 6010C Total Arsenic 6.0 3.0 KM 08/12/2016 14:14 SW 6010C Total Mercury <0.4 0.4 KKM 08/16/201614:55 SW-7471B Total Selenium <5.0 5.0 KM 081121201614:14 SW 6010C pH (Standard Units) ` 6.11 SJB 08/12/2016 08:50 SW-9045D Total Molybdenum 5 5 KM 08/12/2016 14:14 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al", "Fe", AND "S". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company In any advertising, news release, or other public announcements without obtaining ourpdor wdtten authodzabon. Debbie Holt Laboratory Supervisor .10 Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date ReportRange Ratio 2101.01-AEDLIQ-NC LUMBERTON, NC WWTP AEROB. DIGESTED 8/9/2016 91112016-11130/2016 1.4368 LIQUID Na mgA = (Na mg/kg x % Solids) + 100 = (6780 x 0.9800) + 100 = 66.444 Ca mg/I = (Ca mg/kg x °/u Solids) + 100 = (13400 x O.9800) + 100 = 131.32 Mg mgA = (mg mg/kg x % Solids)— 100 = (1860 x O.9800) + 100 = 18.228 Na meq = Na mgA + Molec.Wgt.Na = 66.444 + 23 = 2.88887 Ca meq = Ca mgA + Molec.Wgt.Ca = 131.32 + 20 = 6.566 Mg meq = Mg mgA + Molec.Wgt.Mg = 18.228 + 12 = 1.519 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 2.88887 + SgrRoot[0.5(6.566+1.519)] = 1.43682 Printed: 2/3/2017 Page 1 10:14 A ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: LUMBERTON, NC PREDOMINANT SOIL SERIES: RAINS OWNER OZZELL BAKER PERMIT#: W00000672 ANNUAL DRY TONS APPLIED: 45.58 SITE #: NC RO 00016 FIELD# : RO 00016 0001 OPERATOR: OZELL BAKER CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 16.90 ACRES PERMITTED: 16.90 Page: 1 Lime Applied•" Date Lbs/Ac DATE or MONTH allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Solids Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- till- zation Miner - ali- ration TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop Total Per Acre 7/26/16 192,200.00 (G) 11372.781 2.89 1.371 LULSL DRY 0-d2" STIR 0.5 0.30 4,840.0 p 1,730.00 p 4,360.00 p 6158 BERMUDAGRASS, COASTAL 728116 186,000.00 (G) 11005.917 2.99 1.326 LULSL DRY 0- 1/2" SUR 0.5 0.30 4,840.0 p 1,730.00 p 4,360.00 p 6158 BERMUDAGRASS, COASTAL Jul-16 378,200.00 (G) 22,378.698 I Total Gallons/Ac: 22,378.70 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual lbs/acre 33 0.022 0.011 0.696 1.338 0.070 NR 0.027 0.113 0.027 1.920 77.13 Cumulative ibs/ecre 0.022 0.011 0.696 1.338 0.070 NR 0.027 0.113 0.027 1.920 tt F "i r; �� PAN Limit (Ibs/acre) 1st CroP2nd Crop ff rY-r I, 'v 145Permit FD Cumulative Pollutant Loading Rate Limit (Ibs/a¢e) 36.6 34.8 1J 1339.0 267.9 15.0 '8' ', 'j# 375.0 89.0 7.500.0 LULSL = LUMBERTON, NC W WIP LIME STABILIZED LIQUID (SIGNATUIRE OF LAND APPLIER) DATE "I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for (mowing violations." N/A -Not Applicable NR=Not Reported or Not Required %-percent p-ppm or mg/kg *" Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 Application Method: SUR - Surface, INJ -Injection, SURIN- Incorporation **+ See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 Mw ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACEdTYNAME: LUMBERTON, NC PREDOMINANT SOIL SERIFS: GOLDSBORO OWNER: OZZELL BAKER PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 6.73 SPPE #: NC RO 00016 FIELD# : RO 00016 0002 OPERATOR: OZELL BAKER CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S) * See list at bottom of report ACRES UTILIZED: 3.60 ACRES PERMITTED: 3.60 Page: I Lime Applied'•' Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner- ' or Wet Tons (WTI (specify) "fie Tons Cond. Precip. cation tili- all- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 7/25116 55,800.00 (G) 15500.000 2.89 1.868 LULSL DRY 0-<1/2" SUR 0.5 0.30 4,840.Op 1,730.00 p 4,360.00p 6158 FESCUE Jul-16 55,800.00 (G) 15,500.000 1 Total Gallons/Ac: 15,500.00 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs(acre 23 0.015 0.007 0.482 0.927 0.049 NR 0.019 0.078 0.019 1.330 53.42 Cumulative lbs/acre 0.03Z 0.016 1.559 2.843 0.127 0.002 0.049 0.244 0.040 4.019 PAN Limit (Ibs/acre) 1st CroP!Lnd Crop y?emit 116a m9 V FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 � �' ` �'.i 1339.0 267.9 15.0 ,, 375.0 89.0 2500.0`- �.. LULSL=LUMBERTON, NC W WTP LIME STABILIZED LIQUID X R, IL, R -1 Lf - C201 (SIGNATURE OF LAND APPLIER) 0 DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for ]mowing violations." N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppm or mg/kg "" Volatilization Rate: Surface 0.5, Injection/Incorpomtion 1.0 • Application Method: SUR - Surface, INS - Injection, SURIN - Incorporation See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: LUMBERTON, NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: OZZELL BAKER PERMIT#: W00000672 ANNUAL DRY TONS APPLIED: 13.45 SITE #: NC RO 00016 FIELD# : RO 00016 0003 OPERATOR: OZELL BAKER CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 3.40 ACRES PERMITTED: 3.40 Page: 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner- or Wet Tons (WT) (specify) "�o Tons Cond. Precip. cation tili- all- _ Ammonia Nitrate PAN DATE or Total S Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (pprn) Crop MONTH Per Acre olids 7/25/16 111,600.00 (G) 32823.529 2.89 3.956 LULSL DRY 0-Q/2" SUR 0.5 0.30 4,840.0 p 1,730.00 p 4,360.00 p 6158 BERMUDAGRASS, COASTAL Jul-16 111,600.00 (G) 32,823.529 1 1 Total Gallons/Ac: 32,823.53 As Cd Cr Cu Pb Hg Mc Ni Se Zn P PAN TOTALS: Annual lbs/acre 49 0.032 0.016 1.021 1.962 0.103 NR 0.040 0.166 0.040 2.816 113.13 Cumulative lbs/acre 0.048 0.024 2.058 3.806 0.178 0.002 0.069 0.325 0.060 5.405 Permit PAN Limit(lbs/acre) 1st Crop2nd Crop `i °t iY*'-�t 4"t �r- ` '`' ti ;j� 203 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 F34.8 1339.0 267.9 15.0 '>� A 375.0 59.0 25000 LULSL = LUMBERTON, NC W WTP LIME STABILIZED LIQUID (SIGNATURE OF LAND APPLIER)� DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppm or mg/kg "" Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 " Application Method: SUR- Surface, INJ -Injection, SURIN -Incorporation *** See Site PH & Lime Application Records Section of Report for Fields where Lime is in be applied in 2017 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITYNAME: LUMBERTON, NC PREDOMINANT SOIL SERIES: RAINS OWNER: OZZELL BAKER PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 8.97 SITE #: NC RO 00016 FIELD# : RO 00016 0004 OPERATOR: OZELL BAKER CATION EXCHANGE CAPACrrY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 3.60 ACRES PERMITTED: 3.60 Page: 1 Lime Applied *-- Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (pp m) crop p MONTH Total Per Acre Solids 7/25/16 68,200.00 (G) 18944.444 2.89 2.283 LULSL DRY 0-<1/2" SUR 0.5 0.30 4,840.0 p 1,730.00 p 4,360.00 p 6158 BERMUDAGRASS, COASTAL 7/26/16 6,200.00 (G) 1722.222 2.89 0.208 LULSL DRY 0-Q/2" SUR 0.5 0.30 4,840.0 p 1,730.00 p 4,360.00 p 6158 BERMUDAGRASS, COASTAL Jul-16 74,400.00 (G) 20,666.666 Total Gallons/Ac: 20,666.67 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 31 0.020 0.010 0.643 1.235 0.065 NR 0.025 0.105 0.025 1.773 71.23 Cumulative lbs/acre 0.036 0.018 1,622 2.977 0.136 0.002 0.053 0.255 0.045 4.218 Permit PAN Limit (lbs/acre) 1st Crop2nd Crop I( p� �t.-..,._..-?...-.._.:. __�.i !....FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 '. 1339.0 267.9 {{�`-'� fl 375.0 89.0 25000 4..:....�.-,..,1 C L 1 �....:..�-....- LULSL = LUMBERTON, NC W WTP LIME STABILIZED LIQUID X 9� — 9,-/q-ao17 if (SIGNATURE OF LAND APPLIER) DATE J certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A=Not Applicable NR= Not Reported or Not Required %=percent p=ppm or mgAcg *"' Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 0 Application Method: SUR - Surface, INI -Injection, SURIN-Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITYNAME: LUMBERTON, NC PREDOMINANT SOIL SERIES: RAINS OWNER: OZZELLBAKER PERMIT#: W00000672 ANNUAL DRY TONS APPLIED: 23.16 SITE #: NC RO 00016 FIELD# : RO 00016 0005 OPERATOR: OZELL BAKER CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 8.70 ACRES PERMITTED: 8.70 Page : 1 Lime Applied"• Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) "�" Tons Cond. Precip. cation tili- all- Ammonia Nitrate PAN DATE or MONTH Solids Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) crop p Total Per Acre 7121/16 192,200.00, (G) 22091.954 2.89 2.662 LULSL DRY 0-<1/2" SUR 0.5 0.30 4,840.0 p 1,730.00 p 4,360.00 p 6158 BERMUDAGRASS, COASTAL Jul-16 192.200.00 (G) 22,091.954 1 Total Gallons/Ac: 22,09195 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 33 0.021 0.011 0.687 1.321 0.069 NR 0.027 0.112 0.027 1.896 76.14 Cumulative lbs/acre 0.030 0,015 1.214 2.255 0.107 <001 0.041 0.193 0.037 3.211 Permit PAN Limit (Ibs(acre) 1st Crop/2nd Crop ._ ... S p ,. �' j z , 1 134 FD Cumulative Pollutant Loading Rate Limit (lbstacre) 36.6 34.8 L-,L� 11 1339.0 267.9 15.0 .,..: -T 375.0 89.0 2500.0 t L - - LULSL = LUMBERTON, NC W WTP LIME STABILIZED LIQUID X 6 N2&4� a-14-R0l7 _ 9 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted I am aware that there are significant penalties for submitting false information, including the possibility offines and imprisonment for knowing violations." N/A —Not Applicable NR=Not Reported or Not Required %=percent p=pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ- Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 FACR.ITYNAME: LUMBERTON,NC DWNER: OZZELL BAKER SITE #: NCRO 00016 FIELD# : RO 00016 0006 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: NORFOLK PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 25.40 OPERATOR: OZELL BAKER CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 14.80 ACRES PERMITTED: 14.80 Page : 1 Lime Applied **" Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (W'I) (specify) % Dry Tons Per Residual Site Cord. Dry, Wet, Inches Precip, Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 721/16 55,800.00 (G) 3770.270 2.89 0.454 LULSL DRY 0-<I/2" SUR 0.5 0.30 4,840.Op 1,730.00 p 4,360.00p 6158 FESCUE 722/16 155,000.00 (G) 10472.973 2.89 1.262 LULSL DRY 0-<I/2" SUR 0.5 0.30 4,840.Op 1,730.00 p 4,360.00p 6158 FESCUE Jul-16 210,800.00 (G) 14,243.243 Total Gallons/Ac: 14,243.24 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 21 0.014 0.007 0.443 0.851 0.045 NR 0.017 0.072 0.017 1.222 49.09 Cumulative lbs/acre 0.042 0.021 2.182 3.944 0.171 0.003 0.066 0.339 0.052 5.564 I °ermit PAN Limit (Ibs/acre) 1st Crop2nd Crop y ( j I r + t i' '� l ,` 71 t t 85 �36.6 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 34.8 K,.._ 1339.0 267.9 I5.0 4 �•-, 375.0 89.0 25000 LULSL = LUMBERTON, NC W WTP LIME STABILIZED.LIQUID X / 1l -- as t 7 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for (mowing violations." N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH &.Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 ' ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: LUMBERTON, NC PREDOMINANT SOIL SERIES: NORFOLK OWNER: OZZELL BAKER PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 47.82 SITE #: NC RO 00016 FIELD# : RO 00016 0008 OPERATOR: OZELL BAKER CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S) * See list at bottom of report ACRES UTILIZED: 7.60 ACRES PERMITTED: 7.60 Page: 1 Lime Applied *** Daze Lbs/Ac DATE or MONTH allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Solids Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Veto- till- zation Miner - all- zation TKN Ammonia Nitrogen Nitrate and PAN m (pp ) crop p Total Per Acre 722/16 111,600.00 (G) 14684.211 2.89 1.770 LULSL DRY 0-<12" SUR 0.5 0.30 4,840.0 p 1,730.00 p 4,360.00 p 6158 BERMUDAGRASS, COASTAL 723/16 186,000.00 (G) 24473.684 2.89 2.949 LULSL DRY 0-<12" SUR 0.5 0.30 4,840.0 p 1,730.00 p 4,360.00 p 6158 BERMUDAGRASS, COASTAL 726/16 99,200.00 (G) 13052.632 2.89 1.573 LULSL DRY 0-<12" SUR 0.5 0.30 4,840.0 p 1,730.00 p 4,360.00 p 6158 BERMUDAGRASS, COASTAL Jul-16 1 396,800.00 (G) 52,210.527 Total Gallons/Ac: 52,210.53 As Cd Cr Cu Pb Hg Me Ni Se Zn P PAN TOTALS: Annual lbstacre 77 0:050 0.025 1.623 3.121 0.164 NR 0.063 0.264 0.063 4.480 179.95 Cumulative Ibs/acre 0.050 0.025 1.623 3.121 0.164 NR 0.063 0.264 0.063 4.480 1 Permit PAN Limit (Ibs/acre) 1st Crop2nd Crop C � 264 1JF N- »� FD Cumulative Pollutant Loading Rate Limit (lbs/acre 36.6 34.8-, 1339.0 267.9 S 15.0 ,� ,j 375.0 89.0 2500000 LULSL = LUMBERTON, NC W WTP LIME STABILIZED LIQUID X�—wl�� (SIGNATURE OF LAND APPLIER) V L DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A=Not Applicable NR=Not Reported or Not Required %=percent p=Plan or mglkg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ' Application Method: SUR - Surface, INI -Injection, SURIN - Incorporation *** See Site pH & Lime Application RecordsSection of Report for Fields where Lime is to be applied in 2017 l� ANNUAL LAND APPLICATION FIELD SUMMARY FORM ACILITY NAME: LUMBERTON, NC PREDOMINANT SOIL SERIES: WAGRAM WNER: J T CAMPEN PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 22.42 ITE #: NC RO 00016 FIELD# : RO 00016 0016 OPERATOR: OZELL BAKER CATION EXCHANGE CAPACITY (NON-503): ESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 4.70 ACRES PERMITTED: 4.70 Page : 1 Lima Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (VM (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method nation zation TKN Nitrogen and m (pp) crop p MONTH Total Per Acre Solids 729/16 186,000.00 (G) 39574.468 2.89 4.769 LULSL DRY 0-42" SUR 0.5 0.30 4,840.0 p 1,730.00 p 4;360.00 p 6158 BERMUDAGRASS, COASTAL Jul-16 186,000.00 (G) 39,574.463 Total Gallons/Ac: 39,574.47 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Wirral lbs(acre 59 0.038 0.019 1.230 2.366 0.124 NR 0.048 0.200 0.048 3.396 136.40 .lrmulative lbs(acm 0.246 0.143 9.932 38.308 3.781 0.034 0.712 3.097 0.208 29.470 i J -==E I errait PAN Limit Qbs/acre) 1st Crop2nd Crop ) P' e It ' �' '-� ' `% �` " ' + " J � a�f`> fee ' R �` ut es, } i 239 2D Cumulative Pollutant Loading Rate Limit Ibs/acre g ( ) 36.6 34 8 i 1339.0 267.9 gm �-:3S 375.0 15.0 `' x`, 89.0 ) 2500.0 r � J XLSL = LUMBERTON, NC W WTP LIME STABILIZED LIQUID X C&I ,, 9-14-aol-( (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A=Not Applicable NR= Not Reported or Not Required %=percent p=plan or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR- Surface, INJ -Injection, SURIN -Incorporation *"* See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 l ANNUAL LAND APPLICATION FIELD SUMMARY FORM ACILITY NAME: LUMBERTON, NC PREDOMINANT SOIL SERIES: WAGRAM ,WNER: J T CAMPEN PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 8.97 FIE #: NC RO 00016 FIELD# : RO 00016 0017 OPERATOR: OZELL BAKER CATION EXCHANGE CAPACITY (NON-503): :ESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 6.70 ACRES PERMITTED: 6.70 Page: I Lime Applied •** Date Lbs/Ac ellons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (Wl) (specify) "�* Tans Cond. Precip. cation tif- ali- Ammonia Nitrate PAN DATE or Solids Per Residual Dry, Wet, Past 24 Method zation zaton TEN Nitrogen and (ppm) Crop Total MONTH Per Acre 7/29/16 74,400.00 (G) 11104.478 2.89 1.338 LULSL DRY 0-<1/2" SUR 0.5 0.30 4,840.0 p 1,730.00 p 4,360.00 p 6158 BERMUDAGRASS, COASTAL Jul-16 74,400.00 (G) 11,104.478 rota] Gallons/Ac: 11,104AS TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN lnnual lbstacre 16 0.011 0.005 0.345 0.664 0.035 NR 0.013 0.056 0.013 0.953 38.27 :umulafive Ibs/acre 0.203 0.123 8.726 34.853 3.877 0.032 0.729 2.872 0.172 25.273 i j I I A ermit PAN Limit (Ibs(acm) 1st Crap2nd Crop - _ J ry ,� 0 s . _ � 239 ID Cumulative Pollutant Loading Rate Limit Obstacre) 36.6 34.8 L^—rn.r..v.aa - ,� 1339.0 267.9 15.0 � s 375.0 89.0 2500.0 f .ULSL = LUMBERTON, NC W WiP LIME STABILIZED LIQUID X� Q fJA 2017 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for (mowing violations." N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppm or mg/lrg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 FACILTPYNAME: LUMBERTON,NC OWNER: J T CAMPEN SITE #: NC RO 00016 FIELD# : RO 00016 0018 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: WAGRAM PERMIT#: W00000672 OPERATOR: OZELLBAKER ANNUAL DRY TONS APPLIED: 21.67 CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 12.80 ACRES PERMITTED: 12.80 Page: 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- all- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total per Acre Solids 7/30/16 179,800.00 (G) 14046.875 2.89 1.693 LULSL DRY 0- 1/2" SUR 0.5 0.30 4,840.0 p 1,730.00 p 4,360.00 p 6158 BERMUDAGRASS, COASTAL Jul-16 179,800.00 (G) 14,046.875 1 'Total Gallons/Ac: 14,046.88 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 21 0.014 0.007 0.437 0.840 0.044 NR 0.017 0.071 0.017 1.205 48.41 Cumulative lbs/acre 0.237 0.111 9.697 38.952 3.550 0.043 0.728 2.863 0.207 28.340 r 'j> Permit PAN Limit (Ibs/acre) Ist Crop/2nd Crop 245 J -. FD Cumulative Pollutant Loading Rate Limit Obs/acre) 36.6 3_4.8 1339.0 267-.9�— 15.0 I �i 375.0 89.0 ! ! 25000- LULSL=LUMBERTON,NCWWTPLIMESTABTTJ DLIQUID (SIGNATURE OF LAND APPLIER) DATE "I certify, order penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppm or mg/kg *" Volatilization Rate: Surface 0.5, Injection/Incorpomtion 1.0 * Application Method: SUR- Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACB,ITYNAME: LUMBERTON,NC PREDOMINANT SOIL SERIES: WAGRAM OWNER: J T CAMPEN PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 3.74 SITE #: NC RO 00016 FIELD# : RO 00016 0019 OPERATOR: OZELL BAKER CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 2.30 ACRES PERMITTED: 2.30 Page: 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (VM (specify) % Tons Cond. Precip. cation till- all- Ammonia Nitrate PAN DATE or Total Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Per Acre Solids 7130/16 31,000.00 (G) 13478.261 2.89 1.624 LULSL DRY 0-Q/2" SUR 0.5 0.30 4,840.0 p 1,730.00 p 4,360.00 p 6158 BERMUDAGRASS, COASTAL Jul-16 31,000.00 (G) 13,478.261 1 Total Gallons/Ac: 13,478.26 As Cd Cr Cu Pb Hg Me Ni Se Zn P PAN TOTALS: Annual lbs/acre 20 0.013 0.007 0.419 0.806 0.042 NR 0.016 0.068 0.016 1.157 46.46 Cumulative lbs/acre 0.114 0.106 5.875 34.186 2.309 0.018 0.349 2:123 0.124 19.694 Permit PAN Limit (Ibs/acre) 1st Crop2nd Crop j f < < ( - , t -r 7 I ` 246 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 25000 • ,t LULSL=LUMBERTON, NC W WTP LIME STABILIZED LIQUID (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR- Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITYNAME: LUMBERTON, NC PREDOMINANT SOIL SERIES: LUMBEE OWNER: CITY OF LUMBERTON (AIRPOR PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 52.62 SITE #: NC RO 00017 FIELD# : RO 00017 0002 OPERATOR: DELOIS ALLEN CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):" See list at bottom of report ACRES UTILIZED: 25.40 ACRES PERMITTED: 25.40 Page: 1 Lime Applied *•' Date Lbs/Ac allons (0) or Cubic Yards (CY) Dry Site Inches Appli. Vola- Miner - or Wet Tons (W1) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Total Solids Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Per Acre 4/29/16 223,200.00 (G) 8787.402 3.18 1.165 LUAEDL DRY 0-<I/2" SURIN 1.0 0.30 58,800.p 4,090.00 p 264.00 p 20767 SOYBEANS Apr-16 223,200.00 (G) 8,787.402 519116 173,600.00 (G) 6834.646 3.18 0.906 LUAEDL MOIST 0-<1/2" SURIN 1.0 0.30 58,800.p 4,090.00 p 264.00 p 20767 SOYBEANS May-16 1 173,600.00 (G) 6,834.646 Total Gallons/Ac: 15,622.05 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual lbs/acre 86 0.021 0.012 1.119 1.496 0.066 0.002 0.033 0.166 0.021 1.856 82.03 Cumulative lbs/acre r III t ' 0.097 0.046 5.385 14.619 1.408 0.027 0.318 1.521 0.092 11.808 •. Permit PAN Limit Obs/acre) Ist CroP/2nd Crop q 1� s M 174 FD Cumulative Pollutant Loading Rate Limit (lbs(acre) 36.6 34.8 "" • -1 1339.0 267.9 15.0�"` 375.0 89.0 2500.0 ? LUAEDL = LUMBERTON, NC W WTP AEROB. DIGESTED LIQUID X Cm 0-� '----1 H- O'bl7 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure drat qualified personnel properly gathered and evaluated the information submitted.I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowingviolations." N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppm or mg/kg '" Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 " Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITYNAME: LUMBERTON, NC PREDOMINANT SOIL SERIES: LUMBEE OWNER: CITY OF LUMBERTON (ArRPOR PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 65.77 SITE #: NC RO 00017 FIELD# : RO 00017 0003 OPERATOR: DELOIS ALLEN CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S).' See list at bottom of report ACRES UTILIZED: 28.00 ACRES PERMITTED: 28.00 Page: 1 Lime Applied... Date I Lbs/Ac DATE or MONTH allons (G) or Cubic Yards (CY) or Wet Tons (W'0 (specify) °� Solids Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip, Past 24 Appli- cation Method Vola- till- zation Miner - all- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop Total Per Acre 4/27/16 241,800.00 (G) 8635.714 3.18 1.145 LUAEDL MOIST 0-<I2" SURIN 1.0 0.30 58,800.p 4,090.00 p 264.00 p 20767 SOYBEANS 4/28/16 80,600.00 (G) 2878.571 3.18 0.382 LUAEDL DRY 0-<I/2" SURIN 1.0 0.30 58,800.p 4,090.00 p 264.00 p 20767 SOYBEANS 4/30/16 173,600.00 (G) 6200.000 3.18 0.822 LUAEDL DRY 0-<12" SURIN 1.0 0.30 58,800.p 4,090.00 p 264.00 p 20767 SOYBEANS Apr-16 496,000.00 (G) 17,714.285 Total Gallons/Ac: 17,714.29 As Cd Cr Cu Pb Hg Mir Ni Se Zn P PAN TOTALS: Annual lbs/acre 98 0.023 0.014 1.268 1.696 0.075 0.002 0.038 0.188 0.023 2.105 93.02 Cumulative lbs/acre 0.032 0.018 1.883 2.330 0.112 0.003 0.049 0.260 0.034 3.280 Permit PAN Limit (lbslacre) 1st Crop2nd Crop �� .�: �.r,'t �� '' -' �; a ,, gy ' 174 FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34 8 tw.' ; 1339.0 267.9 15.0 375.0 89.0 2500.0 LUAEDL = LUMBERTON, NC W WTP AEROB. DIGESTED LIQUID X_ (SIGNATURE OF LAND APPLIER) ` DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I an aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppmormg1kg "' Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 " Application Method: SUR- Surface, INJ -Injection, SURIN -Incorporation •*• See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACIITYNAME: LUMBERTON,NC PREDOMINANT SOIL SERIES: WAKULLA OWNER: R G HAMMONDS PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 31.16 SITE #: NC RO 00020 FIELD# : RO 00020 0004 OPERATOR: R G HAMMONDS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S) * See list at bottom of report ACRES UTILIZED: 33.40 ACRES PERMITTED: 33.40 Page: 1 Lime Applied "' Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appcation Vol-- ner- or Wet Tons (WT) (specify) ', Tons Cond. Pmcip. cation till- all. all. Ammonia Nitrate pp,Ll DATE or MONTH Total per Acre Solids Per Residual Dry, Wet, Past 24 Method zaion zation TKN Nitrogen and m (pp ) Crop p 10/3/16 37,200.00 (G) 1113.772 0.98 0.046 LUAEDL DRY 0-<1/2" SUR 0.5 0.30 46,900.p 10.00 p 7,640.00 p 21715 BERMUDAGRASS, COASTAL 10/4/16 130,200.00 (G) 3898.204 0.98 0.159 LUAEDL DRY 0-<1/2" SUR 0.5 0.30 46,900. p 10.00 p 7,640.00 p 21715 BERMUDAGRASS, COASTAL 1015116 186,000.00 (G) 5569.862 0.98 0.228 LUAEDL DRY 0-<1/2" SUR 0.5 0.30 46,900. p 10.00 p 7,640.00 p 21715 BERMUDAGRASS, COASTAL 10/6/16 241,800.00 (G) 7239.521 0.98 0.296 LUAEDL DRY 0-<1/2" SUR 0.5 0.30 46,900.p 10.00 p 7,640.00 p 21715 BERMUDAGRASS, COASTAL Oct-16 595,200.00 (G) 17,820.359 11/7/16 155,000.00 (G) 4640.719 0.98 0.1901 LUAEDLI DRY 0-<1/2" SUR 0.5 0.30 46,900.p 10.00 p 7,640.00 p 21715 BERMUDAGRASS, COASTAL 11/8/16 12,400.00 (G) 371.257 0.98 0.015 LUAEDL DRY 0-<1/2" SUR 0.5 0.30 46,900. p 10.00 p 7,640.00 p 21715 BERMUDAGRASS, COASTAL Nov-16 167,400.00 (G) 5,011.976 Total Gallons/Ac: 22,832.34 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual lbs/acre 41 0.011 0.004 0.343 0.677 0.037 <•001 0.009 0.058 0.009 0.836 39.19 Cumulative lbs/acre 0.248 0.080 6.513 15.047 1.099 0.037 0.315 1.726 0.180 26.331 Permit PAN Limit (lbs/acre) 1st Crop2nd Crop i• I �• j '.a i+.._ A5rY� vr" I Y I ` t..: .. 1 .. _»'ra , us:.^ Q .4s7]if.�,'ti - �.., s.i; _+fi � -.... FD Cumulative Pollutant Loading Rate Limit (Ibs/acm) 36.6 34.9 L 1339.0 267.9 15.0 ` ry'i 375.0 89.0 25000 mow. 1 i LUAEDL = LUMBERTON, NC W WTP AEROB. DIGESTED LIQUID XZ=J At a- ►G1-aof7 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for (mowing violations." N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppm or mg/kg "* Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ' Application Method: SUR-Surface, INJ-Injection, SURIN-Incorporation *** See Site pH&Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: LUMBERTON, NC PREDOMINANT SOIL SERIES: NORFOLK OWNER: HARTLEY OXENDINE PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 106.04 SITE #: NC RO 00021 FIELD# : RO 00021 0001 OPERATOR: LACY CUMMINGS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 39.70 ACRES PERMITTED: 39.70 Page: 1 Lime Applied *** Date I Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) "% Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Solids Per Residual Dry, Wet, Past 24 Method nation nation TXN Nitrogen and (ppm) Crop Total MONTH Per Acre 329/16 254,200.00 (G) 6403.023 3.18 0.849 LUAEDL DRY 0-Q/2" SURIN 1.0 0.30 58,800.p 4,090.00 p 264.00 p 20717 CORN 3130116 316,200.00 (G) 7964.736 3.18 1.056 LUAEDL DRY 0-<12" SURIN 1.0 030 58,800.p 4,090.00 p 264.00 p 20767 CORN Mir-16 570,400.00 (G) 14,367.759 11/17/16 74,400.00 (G) 1874.055 0.98 0.077 LUAEDL DRY 0-<12" SUR 0.5 0.30 46,900.p 10.00 p 7,640.00p 21715 WHEAT 11/18/16 124,000.00 (G) 3123.426 0.98 0.128 LUAEDL DRY 0-<12" SUR 0.5 0.30 46,900.p 10.00 p 7,640.00p 21715 WHEAT 11/19/16 69,200.00 (G) 1717.884 o.98 0.070 LUAEDL DRY 0-<1/2" SUR 0.5 0.30 46,900.p 10.00 p 7,640.00p 21715 WHEAT 1121116 142,600.00 (G) 3591.940 0,98 0.147 LUAEDL DRY 0-<12" SUR 0.5 0.30 46,900.p 10.00 p 7,640.00p 21715 WHEAT 1122/16 6,200.00 (G) 156.171 0.98 0.006 LUAEDL DRY 0-<12" SUR 0.5 0.30 46,900.p 10.00 p 7,640.00p 21715 WHEAT 1123/16 74,400.00 (G) 1874.055 0.98 0.077 LUAEDL DRY 0-<M" SUR 0.5 0.30 46,900.p 10.00 p 7,640.00p 21715 WHEAT 1128116 254,200.00 (G) 6403.023 0.98 0.262 LUAEDL DRY 0-<12" SUR 0.5 0.30 46,900.p 10.00 p 7,640.00p 21715 WHEAT Nov-16 744,000.00 (G) 18,740.554 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: LUMBERTON, NC PREDOMINANT SOIL SERIES: NORFOLK OWNER: HARTLEY OXENDINE PERMIT#: W00000672 ANNUAL DRY TONS APPLIED: 106.04 SITE #: NC RO 00021 FIELD# : RO 00021 0001 OPERATOR: LACY CUMMINGS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 39.70 ACRES PERMITTED: 39.70 Page: 2 Lime plied*** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (W1') (specify) "fie Tons Cond. Precip. cation till- ali- Ammonia Nitrate PAN DATE or MONTH Solids Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop Total Per Acre I otal UallonS/Aee 33,103.31 TOTALS: As Cd Cr Cu' Pb Hg Me Ni Se Zn P PAN Annual lbs/acre 79 0.028 0.015 1.311 1.932 0.092 0.002 0.038 0.200 0.027 2.393 107.61 33 Cumulative Ibs/acre 0.184 0.063 7.019 16.333 0.985 0.025 0.335 1.916 0.140 18.209 "# Permit PAN Limit (165(acre) 1st Crop2nd Crop st+ 736.6 i n[g '1 13150 J �267.9 '�'.t :„� f, t FD Cumulative Pollutant Loadin Rate Limit bs/acreC g ) F77 34.8 �� �,� j 1339.0 15.0"_ J 375.0 89.0 2500 0ti' T 1 i ,mmn� LUAEDL = LUMBERTON, NC W WTP AEROB. DIGESTED LIQUID X 01-a,4- We fl s�lr— a - / +ay 17 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A=Not Applicable NR=Not Reported or Not Required %=percent - p=ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ' Application Method: SUR-Surface, INJ-Injection, SURIN-Incorporation *** See Site pH&Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITYNAME: LUMBERTON, NC PREDOMINANT SOIL SERIES: NORFOLK OWNER: HARTLEY OXENDINE PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 121.69 SITE #: NC RO 00021 FIELD# : RO 00021 0002 A OPERATOR: LACY CUMMINGS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S).' See list at bottom of report ACRES UTILIZED: 45.90 ACRES PERMITTED: 45.90 Page : 1 Lime Applied Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (W1) (specify) % Tons Cond. Precip. as tili- ali- Ammonia Nitrate PAN DATE or MONTH Solids Per Residual Dry, Wet, Past 24 Method nation zation TKN Nitrogen and m (PP ) Cro P Teti Per Acre 3/29/16 55,800.00 (G) 1215.696 3.18 0.161 LUAEDL DRY 0-<12" SURIN 1.0 0.30 58,800.p 4,090.00 p 264.00 p 20767 CORN 3/31/16 310,000.00 (G) 6753.813 3.18 0.896 LUAEDL DRY 0-<12" SURIN 1.0 0.30 58,800.p 4,090.00 p 264.00 p 20767 CORN Mar-16 365,800.00 (G) 7,969.499 4/4/16 198,400.00 (G) 4322.440 3.18 0.573 LUAEDL DRY 0-<I/2" SURIN 1.0 0.30 582800.p 4,090.00 p 264.00 p 21767 CORN Apr-16 198,400.00 (G) 4,322.440 11/8/16 31,000.00 (G) 675.381 0,9g 0.028 LUAEDL DRY 0- 12" SUR 0.5 0.30 46,900.p 10.00 p 7,640.00p 21715 WHEAT 11/9/16 223,200.00 (G) 4862.745 0.98 0.199 LUAEDL DRY 0-<1/2" SUR 0.5 0.30 46,900.p 10.00 p 7,640.00P 21715 WHEAT 11/10/16 198,400.00 (G) 4322.440 0.98 0.177 LUAEDL DRY 0-<12" SUR 0.5 0.30 46,900.p 10.00 p 7,640.00p 21715 WHEAT 11/11/16 148,800.00 (G) 3241.830 0.98 0.132 LUAEDL DRY 0-<12" SUR 0.5 0.30 46,900.p 10.00 p 7,640.00p 21715 WHEAT 11/16/16 186,000.00 (G) 4052.288 0.98 0.166 LUAEDL DRY 0-<12" SUR 0.5 0.30 46,900.p 10.00 p 7,640.00P 21715 WHEAT 11/17/16 173,600.00 (G) 3782.135 0.98 0.155 LUAEDL DRY 0-<12" SUR 0.5 0.30 46,900. p 10.00 p 7,640.00 p 21715 WHEAT 11/18/16 124,000.00 (G) 2701.525 0.98 0.110 LUAEDL DRY 0-<12" SUR 0.5 0.30 46,900. p 10.00 p 7,640.00 p 21715 WHEAT 11/19/16 31,000.00 (G) 675.381 0.98 0.023 LUAEDL DRY 0-<12" SUR 0.5 0.30 46,900. p 10.00 p 7,640.00 p 21715 WHEAT 1121/16 31,000.00 (G) 675.381 0.98 0.028 LUAEDL DRY 0-<12" SUR 0.5 0.30 46,900. p 10.00 p 7,640.00 p 21715 WHEAT Nov-16 1,147,000.00 (G) 24,989.106 / ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITYNAME: LUMBERTON,NC PREDOMINANT SOIL SERIES: NORFOLK OWNER: HARTLEY OXENDINE PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 121.69 SITE #: NC RO 00021 FIELD# : RO 00021 0002 A OPERATOR: LACY CUMMINGS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 45.90 ACRES PERMITTED: 45.90 Page: 2 Lime Applied *** Date I Lbs/Ac ellons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (W1) (specify) % Tons Cond. Precip. cation till- all- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, past Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids Total Gallons/Ac: 37,281.05 As Cd Cr Cu Pb Ng Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 68 0.029 0.014 1.256 1.918 0.093 0.002 0.036 0.194 0.027 2.375 107.44 44 Cumulative lbs/acre 0.181 0.061 6.064 13.884 0.821 0.020 0.275 1.509 0.130 16.384 a i:., Permit PAN Limit (lbs/acre) 1st Cmp/2nd Crop i ! 4 °II ci n 1 s jj ( r "r :; -) 131 —J 50 FD Cumulative Pollutant LoadingRate Limit Ibs/acre ( ) 36.6 34.8 1339.0 267.9 15.0 A - `:;� 375.0 89.0 2500 0 ' LUAEDL = LUMBERTON, NC W vV P AEROB. DIGESTED LIQUID (SIGNATURE OF LAND APPLBER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for ]mowing violations." N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppm or mg/kg ** Volatilization Rate: Surface 0.5, InjectionfIncorporation 1.0 " Application Method: SUR- Surface, INJ -Injection, SURIN -Incorporation +*+ See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITYNAME: LUMBERTON,NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: HARTLEY OXENDINE PERMIT#: W00000672 ANNUAL DRY TONS APPLIED: 44AO SITE #: NC RO 00021 FIELD# : RO 00021 0005 OPERATOR: LACY CUMMINGS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 52.10 ACRES PERMITTED: 52.10 Page: 1 Lime Applied *** Date Lbs/Ac DATEar or MONTH allons (G) or Cubic Yards (CY) Wet Tons (WT) (specify) % Solids Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- till- zation Miner- all- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) ' Crop Total Per Acre 4/4/16 31,000.00 (G) 595.010 3.18 0.079 LUAEDL DRY 0-<U2" SURIN 1.0 0.30 58,800.p 4,090.00 p 264.00 p 20767 CORN 4/5116 303,800.00 (G) 5831.094 3.18 0.773 LUAEDL DRY 0-<1/2" SURIN 1.0 0.30 58,800.p 4,090.00 p 264.00 p 20767 CORN Apr-16 334,800.00 (G) 6,426.104 Total Gallons/Ac: 6,426.10 As Cd Cr Cu Pb Hg Me Ni Se Zn P PAN TOTALS: _ Annual lbs/acre 35 0.009 0.005 0.460 0.615 0.027 <.001 0.014 0.068 0.009 0.764 33.74 Cumulative lbs/acre 0.131 0.036 5.430 12.684 1.817 0.015 0.573 1.614 0.109 12.887 I. ] Permit PAN Limit (lbs/acre) 1st Crop2nd Crop ] �t_ I i ; t �� {t 1 _ FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 1339.0 267.9� 15.0 ', '� '; 375.0 89.0 .2500 0 a _ LUAEDL = LUMBERTON, NC W WTP AEROB. DIGESTED LIQUID (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *"* See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILrrY NAME: LUMBERTON, NC PREDOMINANT SOIL SERIES: RAINS OWNER: ROBERT BASKERVL,LE, SR PERMIT#: W00000672 ANNUAL DRY TONS APPLIED: 194.03 SITE #: NC RO 00028 FIELD# : RO 00028 0002 OPERATOR: CARNELL LOCKLEAR CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 56.90 ACRES PERMITTED: 56.90 Page: 1 Lime Applied **' Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (VM (specify) "fie Tons Cond. Precip. cation tili- all- Ammonia Nitrate PAN DATE or Total Solids Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Per Acre 3/16/16 186,000.00 (G) 3269.893 3.18 0.433 LUAEDL DRY 0-<1/2" SURIN 1.0 0.30 58,800. p 4,090.00 p 264.00 p 20767 CORN 3/17/16 303,800.00 (G) 5339.192 3.18 0.708 LUAEDL DRY 0-<1/2" SURIN 1.0 0.30 58,800.p 4,090.00 p 264.00 p 20767 CORN 3118/16 322,400.00 (G) 5666.081 3.18 0.751 LUAEDL DRY 0-<12" SURIN 1.0 0.30 58,800.p 4,090.00 p- 264.00 p 20767 CORN 3/19116 229,400.00 (G) 4031.634 3.18 0.535 LUAEDL DRY 0-<12" SURIN 1.0 0.30 58,800.p 4,090.00 p 264.00 p 20767 CORN 321/16 93,000.00 (G) 1634.446 3.18 0.217 LUAEDL DRY 0-<12" SURIN 1.0 0.30 58,800.p 4,090.00 p 264.00 p 20767 CORN Mar-16 1,134,600.00 (G) 19,940.246 9/12/16 24,800.00 (G) 435.852 0.98 0.018 LUAEDL DRY 0-<12" SUR 0.5 0.30 46,900. p 10.00 p 7,640.00 p 21715 WHEAT 9114/16 148,800.00 (G) 2615.114 0.98 0.107 LUAEDL DRY 0-<1/2" SUR 0.5 0.30 46,900.p 10.00 p 7,640.00p 21715 WHEAT 9/15/16 217,000.00 (G) 3813.708 0.98 0.156 LUAEDL DRY 0-<12" SUR 0.5 0.30 46,900.p 10.00 p 7,640.00p 21715 WHEAT 9/16/16 142,600.00 (G) 2506.151 0.98 0.102 LUAEDL DRY 0-<12" SUR 0.5 0.30 46,900.p 10.00 p 7,640.00p 21715 WHEAT 926/16 136,400.00 (G) 2397.188 0.98 0.098 LUAEDL DRY 0-<12" SUR 0.5 0.30 46,900.p 10.00 p 7,640.00p 21715 WHEAT 927/16 173,600.00 (G) 3050.967 0.98 0.125 LUAEDL DRY 0-cl2" SUR 0.5 0.30 46,900.p 10.00 p 7,640.00p 21715 WHEAT 928/16 223,200.00 (G) 3922.671 0.98 0.160 LUAEDL DRY 0-<12" SUR 0.5 0.30 46,900.p 10.00 p 7,640.00p 21715 WHEAT Sep-16 1,066,400.00 (G) 18,741.651 � 1 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITYNAME: LUMBERTON,NC PREDOMINANT SOIL SERIES: RAINS OWNER: ROBERT BASKERVILLE, JR PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 194.03 SITE #: NC RO 00028 FIELD# : RO 00028 0002 OPERATOR: CARNELL LOCKLEAR CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 56.90 ACRES PERMITTED: 56.90 Page: 2 Lime Applied *** DateLba/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (VM (specify) "�" Tons Card. Precip. cation tili- all. Ammonia Nitrate PAN DATE or MONTH Solids Per Residual Dry, Wet, Past 24 McOrod nation nation TKN Nitrogen and (pp-) Crop Total Per Acre land Uailons/Ac: 38,681.90 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual lbs/acre 110 0.036 0.019 1.710 2.465 0.115 0.003 0.050 0.259 0.034 3.055 136.88 33 Cumulative lbs/acre 0.070 0.030 3.582 4.569 0.262 0.005 0.084 0.587 0.062 5.233 1 9 Permit PAN Limit abs(acre) 1st Crop2nd Crop ) r �.__ �. 1- 1 1 �) ;_� ; 1 F j I 135 _ , __ i �_. _ �.� �_ ,_ r---.� - _ �T �, Tv' ~15.0 ._.— A �' _ ,. I 50 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8y ��i'. 1339.0 267.9 yri y� 375.0 89.0 25000 i �' 4T. LUAEDL- LUMBERTON, NC W WTP AEROB. DIGESTED LIQUID X��I&IL)d_a -1 q- av>.n (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppm or mg/kg *" Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 Application Method: SUR-Surface, INJ-Injection, SURIN-Incorporation *** See Site pH&Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 Summit Enviromnental Technologies, Inc. 3310Win St. RIVIRONMENTAL5 3.1,10LOGJ-S, IMC Cuyahoga Falls, Ohio 44223 Analytical Laboratories TEL: (330) 253-6211 FAX. (330) 253-4489 Websile: htto:/Anvw.seaekcom February 13, 2016 Nate Roth Synagro 284 Boger Rd. Mocksville, NC 27028 TEL: (336)998-7150 FAX: (336) 998-8450 RE: Lumberton WWTP Dear Nate Roth: Order No.: 16020218 Summit Environmental Technologies, Inc. received 1 sample(s) on 2/3/2016 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, Bachar Najm Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 A2LA 0724.01, Alabama 4160D, Arizona A20788, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia E87688 and 943. Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-OH-13, Kansas E-I0347, Kemueky (Undargmunsd Storage Teak) 3, Kentucky 90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Mmaeh..= M-OPH923, Minnesota 409711, Montana CERT0099, New Hampshire 2996, New Jersey 011006, New York 11777, North Carolina 39705 and 631, Ohio Drivldng Water4170, Ohio VAP CL0052, Oklahoma 9940, Omgon OH2O0001, Rhode Island LA000317, South Carolina 92016001, Taanessee TN04018, Texas T104704466-11-5, Region 8 8TMS-1, USDA(APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, Wasbagton C891, West Vhga6a 248 and 9957C and E87688, Wisconsin 399013010 Page 1 of 8 'l SUMMIT 3310 Win St. Summi(Environmenta7Technol0W,Inc. Case Narrative RIVIROMMEt:TALTECHNOLOME5, Mc. Cuyahoga Falls, Ohio 44223 WO#: 16020218 Ar lytical LaboraParie$ TEL: (330) 253-8211 FAX.: (330) 253-4489 Website: huo.,lAmov.seaekeom Date: 2/13/2016 CLIENT: Synagro Project: Lumberton WWTP This report in its entirety consists of the documents listed below. All documents contain the Summit Environmental Technologies, Inc., Work Order Number assigned to this report. Paginated Report including Cover Letter, Case Narrative, Analytical Results, Applicable Quality Control Summary Reports, and copies of the Chain of Custody Documents are supplied with this sample set. Concentrations reported with a J-Flag in the Qualifier Field are values below the Limit of Quantitation (LOQ) but greater than the established Method Detection Limit (MDL). Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods. Estimated uncertainty values are available upon request. Analysis performed by DBM, VRM, or SFG were performed at Summit Labs 2704 Eatonton Highway Haddock, GA 31033 All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as "dry weight" using the "-dry" designation on the reporting units. Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of the cover letter that may or may not pertain to this report. The information contained in this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results contained in this report are only representative of the samples received. Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible for use or interpretation of the data included herein. This report is believed to meet all of the requirements of NELAC or the accrediting / certifying agency. Any comments or problems with the analytical events associated with this report are noted below. Original Page 2 of 8 msymmur Summit Environmental Technologies, In Qualifiers and Acronyms 3310 Win b F.NYIRONMENTPLIEC$NOLOGres,IMc. Cuyahoga Falls, Ohio 4421 WO#: 16020218 Analytical Laboratories TEL: (330) 253-8211 FAX., (330) 253-446 Website: htfir1Avim.seuekco. Date: 2/13/2016 These commonly used Qualifiers and Acronyms may or may not be present in this report. Qualifiers U The compound was analyzed for but was not detected. J The reported value is greater than the Method Detection Limit but less than the Reporting Limit H The hold time for sample preparation and/or analysis was exceeded. D The result is reported from a dilution. E The result exceeded the linear range of the calibration or is estimated due to interference. MC The result is below the Minimum Compound Limit. * The result exceeds the Regulatory Limit or Maximum Contamination Limit. in Manual integration was used to determine the area response. N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response. P The second column confirmation exceeded 25%difference. C The result has been confirmed by GUMS. X The result was not confirmed when GUMS Analysis was performed. DUMB+ The analyte was detected in the associated blank G The ICB or CCB contained reportable amounts of analyte. QC-/+ The CCV recovery failed low (-) or high (+). R/QDR The RPD was outside of accepted recovery limits. QL/+ The LCS or LCSD recovery failed low (-) or high (+). QLR The LCS/LCSD RPD was outside of accepted recovery limits. QM-/+ The MS or MSD recovery failed low (-) or high (+). QMR The MS/MSD RPD was outside of accepted recovery limits. QV-/+ The ICV recovery failed low (-) or high (+). S The spike result was outside of accepted recovery limits. Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for additional information Acronyms ND Not Detected RL Reporting Limit QC Quality Control MDL Method Detection Limit MB Method Blank LOD Level of Detection LCS Laboratory Control Sample LOQ Level of Quantitation LCSD Laboratory Control Sample Duplicate PQL Practical Quantitation Limit QCS Quality Control Sample CRQL Contract Required Quantitation Limit DUP Duplicate PL Permit Limit MS Matrix Spike RegLvl Regulatory Limit MSD Matrix Spike Duplicate MCL Maximum Contamination Limit RPD Relative Percent Different M1uCL Minimum Compound Limit ICV Initial Calibration Verification RA Reanalysis ICB Initial Calibration Blank RE Reextraction CCV Continuing Calibration Verification TIC Tentatively Identified Compound CCB Continuing Calibration Blank RT Retention Time RLC Reporting Limit Check CF Calibration Factor DF Dilution Factor RF Response Factor This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting. Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this list or for additional information regarding the use of these Qualifiers on reported data. A Original Page 3 of 8 sammitE Technologies, a.. Workorder 3310310 Win n St. S Sample Summary EipVIRONMEN'rALTECBt4OLCGI-cS, INC. Cuyahoga Falls, Ohio 44223 Analytical Laboratories TEL: (330) 253-8211 FAX: (330) 253-4489 WO#: 16020218 Websile: hao:/h�v.settekcom 13-Feb-16 CLIENT: Synagro Project: Lumberton WWI? Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix 16020218-001 Lwibenon W WTP 1252016 9:40:00 AM 2/32016 12:00:00 PM Solid Page 4 of 8 i� Summit Environmental Technologies, 3310 Analytical Report I0 Win SStt. ENVIRONMENTAL IECHNOLu3125, TNC. Cuyahoga Falls, Ohio 44223 . (base report) Analytical Lahoraforie5 TEL. (330) 253-8211 FAX.- (330) 253-4489 W04: 16020218 Website: hap.,lAtvim.settekoom Date Reported: 2/13/2016 CLIENT: Synagro Tag Number: Matrix: SOLID Collection Date: 1/25/2016 9:40:00 AM Lab ID: 16020218-OOIA Project: Lumberton WWTP Client Sample ID Lumberton W WTP Analyses Result RL Qual Units DF Date Analyzed RCI SW9045D Analyst: DHC PH (SW9045D) pH 6.49 s.u.@19.3C 1 219/20162:20:00 PM - QuaOfiers: Valve an.de Mud. Cootavcv�IL 1 E Valveebovequmtenuovemige R Raldmg times for preparation or analysis emended M Manual Unegafion taM to detet®e erear wo ' MC Value u below Minimum Compowd Lick N Tentativelpdeoti5edmv�owds h1D Not Detected& the Rq,ortmg Limit O RSD i¢grratertbav RSDI®rt P secoodaalmrmcun6m'udoa...& M Pomk limit Original R RPD outside accephdrewvery limits RL Reponmg Deecdonl.imit U samewih U.Vd< MDL I Analy,< detested below quaotita5an limn Page 5 of 7 (,f�i Sunil Environmental Technologies, Inc. WO#: 16020218 3310 Win St. E"r7� FRVIRONLIENTAL 12CHkOLOGI-cS, mo Cuyahoga Falls, Ohio 44223 Date Reported: 2/1312016 Analytical Laboratories TEL. (330) 253-8211 FAY: (330) 2534489 Company: Synagro Website: hno.,1AP nv.seuekcam Address: 284 Boger Rd. MocksvilleNC 27028 Received: 2/3/2016 Project#: LumbertonWW TCLP Metals Analysis (6010) Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Lumberton WWTP 001 1/25/2016 TCLP Arsenlc(As) 0.500 ND mg/L Solid EPA 6010C 1 5.00 2/5/2016 WK Lumberton WWTP 001 1/25/2016 TCLP Barium(Ba) 5.00 ND mg/L Solid EPA6010C 1 100 2/5/2016 WK Lumberton WWTP 001 1/25/2016 TCLP Cadmium(Cd) 0.100 ND mg/L Solid EPA 6010 C 1 1.00 215/2016 WK Lumberton W WTP 001 1/25/2016 TCLP Chromium(Cr) 0.200 ND mg/L Solid EPA 6010 C 1 5.00 215/2016 WK Lumberton W WTP 001 1/2512016 TCLP Lead(Pb) 0.500 ND mglL Solid EPA 6010 C 1 5.00 - 215/2016 WK Lumberton WWTP 001 1/25/2016 TCLP Selenium(Se) 0.500 ND mg/L Solid EPA 6010 C 1 1.00 2/512016 WK Lumberton W WTP 001 1/25/2016 TCLP Silver(Ag) 0.500 ND mg/L Solid EPA 6010 C 1 5.00 21512016 WK TCLP Mercury Analysis (1311/7470) Client ID# Lab ID# Collected Analyte Rep Limit Result Units Matrix Method DF RegLvl Run Analyst Lumberton WWTP 001 1/25/2016 TCLP Mercury 0.00200 ND mg/L Solid EPA7470A 1 0.200 2111/2016 MFW SVOC SW-846: 8081-TCLP Pesticides Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Lumberton WWTP 001 1/25/2016 Chlordane, total 0.0250 ND mglL Solid EPA 8081 B 1 0.0300 2/8/2016 JBN Lumberton WWTP 001 1/25/2016 Toxaphene 0.0500 ND mg/L Solid EPA 8081 B 1 0.500 2/8/2016 JBN Lumberton WWTP 001 1/25/2016 Enddn 0.00250 ND mg/L Solid EPA 8081B 1 0.0200 2/8/2016 JBN Lumberton WWTP 001 1/25/2016 gamma-BHC 0.00250 ND mg/L Solid EPA 8081 B 1 0.400 2l8/2016 JBN Lumberton WWTP 001 1/25/2016 Heptachlor 0.00260 ND mg/L Solid EPA 8081 B 1 0.00800 2/8/2016 JBN Lumberton WWTP 001 1/25/2016 Heptachlor epopde 0.00250 ND mg/L Solid EPA 8081E 1 0.00800 2/8/2016 JBN Lumberton WWTP 001 1/25/2016 Methoxychlor 0.00250 ND mg/L Solid EPA 8081B 1 10.0 2/8/2016 JBN VOC by GC/MS (8260)-TCLP Client ID# Lab ID# Collected Analyte Rep Lint Result Units Matrix Method DF RegLvl Run Analyst Lumberton WWTP 001 1/25/2016 1,1-Dichloroethene 0.100 ND mg/L Solid EPA 8260E 1 0.700 2/5/2016 MES Lumberton WWTP 001 1125/20161,2-Dichlorcethane 0.100 ND mglL Solid EPA 8260E 1 0.500 2/5/2016 MES Lumberton WWTP 001 1/25/2016 MEK 2.00 ND mg/L Solid EPA 8260B 1 200 2/512016 MES Lumberton WWTP 001 1/25/2016 Benzene 0.100 ND mg/L Solid EPA 8260E 1 0.500 2/5/2016 MES Lumberton W WTP 001 1/25/2016 Carbon tetrachloride 0.100 ND mg/L Solid EPA 8260 B 1 0.500 2/512016 MES Lumberton WWTP 001 1/25/2016 Chlorobenzene 0.100 ND mg/L Solid EPA 8260B 1 100 215/2016 MES Lumberton WWTP 001 1/2512016 Chloroform 0.100 ND mg/L Solid EPA 8260 B 1 6.00 215/2016 MES Lumberton WWTP 001 1/25/2016 Tetrachloroelherie 0.100 ND mglL Solid EPA 8260B 1 0.700 215/2016 MES Lumberton WWTP 001 1/25/2016 Trichloroethene 0.100 ND mg/L Solid EPA 8260B 1 0.600 2/5/2016 MES Lumberton WWTP 001 1/25/2016 Vinyl chloride 0.200 ND mg/L Solid EPA 8260 B 1 0.200 2/512016 MES ✓ t 1 1 Page 6 of 8 Summit Environmental Technologies, Inc. WOk: 16020218 I'T 3310 Win St. UJFN1nRDNhIENTALTECttt20LOCIES, We Cuyahoga Falls, Ohio 44223 Date Reported: 2/13/2016 Art Iytical Laboratories TEL: (330) 253-8211 FAX... (330) 2534489 Company: Synagro iyebsile: htmdPonv v.senekcom Address: 284 Boger Rd. MocksvilleNC 27028 Received: 2/3/2016 Project#: LumbertonWW SVOC 8270 TCLP BNA List Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Lumberton WWTP 001 1/25/2016 1,4-Dichlorobenzene 0.200 ND mg/L Solid EPA 8270 C 2 7.50 2/9/2016 MO Lumberton WWTP 001 1/25/2016 2,4,5-Trichlorophenol 0.500 ND mglL Solid EPA 8270 C 2 400 219/2016 MO Lumberton WWTP 001 1/25/20162,4,6-Trichlorophenol 0.500 ND mg/L Solid ..EPA 8270C 2 2.00 2/9/2016 MO Lumberton WWFP 001 1/25120162,4-Dinitrololuene 0.200 ND mg/L Solid EPA 8270C 2 0.130 219/2016 MO Lumberton W VVTP 001 1/25/2016 Cresols, Total 10.0 ND mg/L Solid EPA 8270 C 2 200 2/9/2016 MO Lumberton WWTP 001 1/25/2016 Hexachloro-1,3- 0.200 ND mglL Solid EPA 8270C 2 0.500 219/2016 MO butadiene Lumberton WWTP 001 1/25/2016 Hexachlorobenzene 0.200 ND mg/L Solid EPA 8270 C 2 0.130 2/9/2016 MO Lumberton W WTP 001 1/25/2016 Hexachlomethane 0.200 ND mg1L Solid EPA 8270 C 2 3.00 2/9/2016 MO Lumberton WWFP 001 1/25/2016 Nitrobenzene 0.200- 0.398 mg/L Solid EPA 8270C 2 2.00 219/2016 MO Lumberton WWTP 001 1/25/2016 Pentachlorophenol 0.500 ND mg1L Solid EPA 8270C 2 100 2/9I2016 MO Lumberton WWTP 001 1/25/2016 Pyridine 0.500 ND mg/L Solid EPA 8270C 2 5.00 219/2016 MO SVOC SW-846: 8321 Herbicides-TCLP Client EN Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Lumberton WWTP 001 1/25/2016 2,4-D 5.00 ND mg/L Solid EPA 8321 A 1. 10.0 2/912016 BJH Lumberton WWTP 001 1/25/2016 2,4,5-TP 0.500 ND mg/L Solid EPA 8321 A 1 1.00 2/9/2016 BJH Page 7 of 8 Sramnit Environmental Technologies, Inc. WO#: 16020218 3310 Win SL F.81q$ON1AENTAL TECHUCLOGIES, INC Cuyahoga Falls, Ohio 44223 Date Reported: 211N016 Analytical Laboratories TEL. (330) 253-8211 FAX.- (330) 2S3-4489 Company: Synagro Website: h1tP.*11 ww.seuekcom Address: 284 Boger Rd. MocksvilleNC 27028 Received: 2/3/2016 Project#: LumbertonWW Client ID# Lab ED# Collected Analyte Result Units Matrix Method DF RL Run Analyst Lumberton WWfP 001 1/25/2016 Flashpoint (140°F) >140 °F Solid EPA 1010 1 2/11/2016 TAH Lumberton W WTP 001 1/25/2016 Cyanide, Reactive ND mg/Kg Solid EPA 9014 1 0.500 2/9/2016 MS Lumberton W WfP 001 1/25/2016 Sulfide, Reactive ND mg/Kg Solid EPA 9034 1 25.0 219/2016 MS Page 8 of 8 Summit Environmental Technologies, Inc 3310Win Street Analysis Request/Chain of Custody 3310 Win 0l,...,6— a.,u.. nn:.. AA90a T t• aan nc2 of t t F._ aan iCi AACn For Summit.Environmental Technologies, Inc, use only Page —of— ISFTNa Company Name (Please Print) S Project Name v C'J E C� e z Analyt'ted Parameters and Methods Comp�; AdWeN�m 1 ll G-Gt Vdle_ Nc, Yrojccl Addressmn� Y � �5 o, n ao 'y4� e „ J ;a rn a ^ I L1t Client Phone No f � � Repor Client Pax N0. Please xPlease� PO#1 Vd Client Ban ' ILK : dtc-Quote No. Contact n N7A Sampled Check if Ohio VAP samples # s=Ple Identification Dale Collected Time Collected fl=al LAnnl ) x i qp.' ReGn eU note I Thne Received by: Delea Tmte NolvslCommcnts: t Received In lah by: al "ban Rush Requested By: Most be approved 2 141ev Date by lab monger 7 Whirr and yellow pages should accompany samples to the laboratory. The client retains the pink page - 8 1 n 9 ooa AN N reHYr6 Summit Environmental Technologies, Inc. Cooler Recslpt Form Cusnt� `' 6yzIndfe4 of person lnspeWnpcoo(erand 71�+ samples.�� Order Number Date Received: 21 Tare Received;��Jj ,�r� Date —1U0 coolers) Opened and samples Number of CoolerslBoxes:�� inepseted WA ShipperUPS AlrAlrboms US Postal W Ik4n Pickup Other 'C Packaging: Peanuts 4'6yV P Paper Foam Nona othw Tape on eooler/bp+c � N WA \) Custody Seals Intact Y N C-O-0 In plastic remv N Cf "V Ioe _ Blue Ice WA • P+eeent�mettW WA Sample 7emPeratura IR Gun 316p21>aw � C7 �.C. + . `O FtadiologfcalTesting Ins;n+mcntsedal di51z7 Y (see ", Man roaeeS) N WA 1 N� so � try per sample for Radiological Testing. If emn;ib is NOT, the Radletogloaf Safety offlw mast 6e notlned ' CO-C Geed out property r:1 C) N Samples In separate bags N/A . N Sample containers Intact' WA N -if no, Get broken sample{s)• WA Sample abal(s) complete QD, done. eta) N Labal(s) agree with C-O-0 0 N NIA _ Correct Contalners used WA N Sufficient sample mcahmd N/A N WA Samples received Within holding ffine J�y N Bubbles absent from 40 mL vials" Y N Samples wdh bubbles e6mm are acceptable. Indicate bubble size If >Smm. Was client Contacted about samples Y N M client send new samples Y N Logged Paget of ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Lumberton WQ Permit Number: W00000672 ' WWTPName: City of Lumberton WWTP NPDESNumber: NCO024571 Monitoring Period: From 01/01/16 To 05/31/16 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) -Please indicate level achieved and alternative performed: Class A: Alt. l/A (timeltemp) _ Alt 2113 (Alk Treatment) _ Alt 3/C (Prior Testing) Alt 4/1) (No Prior Test) _ Alt 5/Process to Further Reduce Pathogens _ Alt 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost _ HeatDrying _ Heat Treatment _ Thermophilic Beta Ray _ Gamma Ray _ Pasteuriza on Class B: Alt (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization T Air Drying _ Composting _ Aerobic Digestion Anaerobic Digestion _. If annlieahle to alternative nerformed frlace A — r9acc ul e.....ele.e .:.., un.....:.... ....._:._ Parameter Allowable Level in Sludge, Pathogen Density �No. of Frequency Sample Analytical Excee- of Type Technique Minimum Gen. Mean Maximum Units dences Analysis Fecal 2xlOtothe MPN 1vlPN/g Coliform power per gram of total solids CFU <29300 <30500 <31500 CFU/g 0 quarterly grab 9222D 1000 MPN per gram of MpN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed: 0ption/Alt 1 (VSreduction) _ Option/Alt 2 (40-day bench) _ Option/Alt 3 Option/Alt. 4 (30-daybench) X (Spec.02uptake) Option/Alt 5 (14-Day Aerobic) _ Option/Alt 6 (A1kStabilization) _ Option/Alt 7 Option/Alt 8 (Drying —Stable) (Drying —Unstable) Option/Alt.9 Option/Alt.10 (Injection) _ (Incorporation) _ No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15ANCAC 02T.1106 and the vector attraction reduction requirement in CFR 503.33/15A NCAC 02T.1107 have been met" "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met" (Please note if you check this statement attach an X explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment" Jim Walters. Director of EUS Dent Preparer Name and Title (type or print) Land Applier Name and Title (if applicable) (type or print) 6 nature of Preparer* Date Signature of Land Applier (if applicable) Date •Preparer is defined in 40 CFR Part 503.9(r) and 15ANCAC 2T.1102 (26) Cameron Testing Services, Inc. Laboratory Report Synagro C PS Psojs 160090 Lumberton WWTP Yes f.r-.s-_,ram—._--_..i..:",•.;-�? Sample.19formation I C. Brown ; as 0.1/20/16 Recetvea' J.ICameron Analyses and Results I OVVVV UI a Nudae Gr Feoz Coliform-S <30800 MID 01/21/16 b <31500 CFu/g 130800 31500 C <29300 CFUra 29300 d <30100 Mfg 30100 e <30400 Mig 30400 f <30300 Mlo 30300 9 <31800 CFuro 81500 Geomean <30500 160090 01 a sbdye cr Ts (^/o) 3.20% % 0.01 01/27/16 b 3.09% % a,ot 0 3.13% % om d 3.20% % o.o1 e 3.15% % oo1 f 3.19%u % am 9 3.12% % o,oi Report Review_ Lab Dire or Date 1 NC DENR11654 NC PHHS 037799 US EPA *NC01918 4aEe 01/20/16 9222D - MF 2540 G -TS 219 S. Steele Str. Sanford NC 27330 1919-208-4240 cmSemidrontestin-.com r^� r 219 S. Steele Str. Sanford, NO 27330 Phone: 919-208-4240 Cameron 'testing Services, Inc. NO W W/GW cart. 4654 NO PHHS cart # 37799 US EPA NC01918 Chain of Custody Page _ of x Compeny^t St y4li Emau , //� ��JJ CTS lab use 9rlly, r ` • -. ' 1 Contact �, — 4l 7 Sam.1C4 lTam P; Prol , /spd f0 —U /2�k1�cJYl Addrers {Crty,; _....,._—��Pho,ne: Fax '� �!a +AriIve.; _ Notes: -- �d 5 Si�i 1 Project Regulatory. I r..,, J ����%� s �' i/iM k7'1,1/'I v V1 W ✓„ ' r (Y/N)... 5 Collected -!Name:UdiJ /�cYMY WV\ Signature. w, p� - Sample'.fnformation - Number,ofi'6ott , es = Y ", Rec�uestediAnalys�s+ 1 " ». . GI i m > 1 I Preservatives W Unprehserved-,b=HC1 I, CiTS Labrj Sample ID F o m j, . a, N S Y H2SO4 R HNQi'Na AaThlosuffate , � *v1D C91 U chi 1 m o .- . G=NaOH +)� Other Indlrale 1 4 V I ,1�/I�a 61? t� � � � � I `— e �lu�bevlah �v�,rrP 1D79�� - R,. 6.. Received - _. .`i D:ateLTime f /i't Rush work will require prior approval. Additionalcharges will apply 30D Report Sheet Project: Lumberton WW-FP 30 Day Benchtop Test GTS Prol. 1&660 Client: Synagro (EPA 625111-921013, Appendix Regulatory Sampled Received Due Ref. Methods Sid. Math. 1 9th ad. By C. Brown By J. Cameron 2540 G - TS T, Date 01120/16 Date 01/20116 Date 02/26116 Requested 2640 G -VS Analysis V Type Grab Matrix Sludge. SampJeJD - Lab D BU. I TS (I/,. VS Analyst Datw- 1,82% 72.5% 01126116 1.62% 70.1% 02fi ill 6 1.66% 69.4% 02117116 FVSR (VK) 16.1% 'Fail >16%' 1.50% 68.4% 02124116 FVSR (m.b.) 23.05% 'Fall > 15W 1.48% 68.9% 02J25118 6z Lab t erector Date: Notes: Sample started at TS :5 2%. Page I r- � 1 219 S. Steele Str. Sanford, NC 27330 Phone: 919-208-4240 Cameron Testing Services, Inc. NC W W/GW CerC #654 NC PHHS Cert# 37799 US EPA NCO1918 Chain of Custody Page of — Emad ; Company, �, , 1„ 4 n.).� _' i CTS lab us0 Onl- 4 . ": _ -- ,Contact ', lr2t I,11 _ / ��� IPhonef F7 �. Sample ac) Temp I rProJ I dd 1 /le 9d Cy�q) •777 �O7G� Address(Crty{: Statet'Zip) Fax +1 Arnve :I rpue Prgect Rggulatary . Rush;, - �,.I • Collected 3'Name: WV\ Sfgnatum: f 1`�f'•t'�0"11 frB �- J t rJ Sample Information Numbe> of bott esr. s; 4Requested,Anafysts a t d a, n x i Z 16 I ,mom o j Preservatives W Uripreserved B=HCIri i� o �,CTS La b Sample ID u E E �°' m } N 1 c7 a = Y-H2SO4 R HNO3 Na NaThiosQlfafar, ~ U •- m of o _ G=NaOH X-Ottter mdirale. ,. I r m e ' v. v � 2aFox IJJW�'_ Z'/4I /o lSi4 �t-< �L I I cal Adhs 7" s,/:d5 47 / .LA" Qv}vh tvf. v 1 &a /'d %9a r i V rc He" - 4� _ I � I l , I � I r 7..:. = .- RecBtved. Rush work will require prior approval. Additional charges will apply ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Lumberton WQ Permit Number: W00000672 WWTPName: City of Lumberton WWTP NPDESNumber: NCO024571 Monitoring Period: From 06/01/16 To 06/30/16 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt 2B (Alk Treatment) Alt 3/C (Prior Testing) Alt 4/D (No Prior Test) _ Alt 5/Process to Further Reduce Pathogens _ AIL 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying _ Heat Treatment _ Thermophilic Beta Ray Gamma Ray _ Pasteurization Class B: Alt (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization _ Air Drying _ Composting _ Aerobic Digestion Anaerobic Digestion If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee= of ' Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10tothe MPN MPN/g Coliform power per gram of total solids CFU <25500 <31400 <38200 CFU/g 0 quarterly grab SM9222D 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal colifonn Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0ption/Alt 1 Option/Alt 2 Option/Alt 3 Option/Alt. 4 (VS reduction) _ (40-day bench) (30-day bench) (Spec. 02 uptake) X Option/Alt. 5 (14-Day Aerobic) Option/Alt 9 (Injection) OptionMlt 6 (Alk Stabilization) Option/Alt. 10 (Incorporation) STATEMENT (please check the appropriate statement) Option/Alt. 7 Option/Alt. 8 (Drying —Stable) (Drying —Unstable). No vector attraction reduction alternatives were performed "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirementin 40 CFR 503.33/15A NCAC 02T.1107 have not been met" (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment" --\ Jim Walters, Director of EUS Dept t Preparer Name and Title (type or print) Land Applier Name and Title (if applicable) (type or print) S ature of Preparer* Date Signature of Land Applier (if applicable) Date 'Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) Cameron Testing Services, Inc. Laboratory Report A . -NClii tit` Synagrp Protect Lumberton e9ry ,s Sample Information Sampled W. Vamer . oare, r 05/25/16 itf ecekved Analyses and Results NO DERR 0654 NO PHHS #37799 US EPA'JNG01918 160742 Yes S. Bullard LDaie 05/25116 160742 01 a Bludge Gr Fec: Cofform-S <25500 CFUIs 2559D 05/26/16 9222D-MF b <25900 CFU/g 25900 C <35700 CFUlg 35700 d <30400 CFU/g 30400 e <33200 CFU19 $3200 ' f <36200 CFU19 382g0 9 <33400 CFU19 3340D Geomean <31400 160742 01 a 51udge cr TS (0/0) 2.75% % 0.01 05/26/16 2540 G -TS b 3.73% % 0.01 p 2.70% % 0.01 d 3.17% A 0.01 e 2.96% % 0.01 f 2.53% % 0.01 9 2.73% % Q01 Report Review Lab ffirector Date 219S. Steele Str. Sanford NO 27330 919-208-4240 clvis@=uerontestingcom U 219 S. Steele Str. Sanford, NC 27330 Cameron Testing Services, Inc. NC 1&WJCW Cert. 9654 NC PHHS Cart # 37799 US EPA NC01918 Chain of Custody Page — of Phone: 919 208-424D 4? nagr0 71y wvamer@synagro.com .. -. r rc+y'ru 1;^ �� Will Varner 2 ° ^' 336-909-8627 @ z `rc 3 i �Q 7y Z k ^,"k .f F ffil "al (284 Boger Rd. �.' . Mooksville, NC 27028, I ri g. r Name, r '�� Si nafo2: 9 "'a r1riE- x,x' ,c Pit1 n M-x7,xn W am ( nforrnon`�4 -`s `'6`N'C>:i,\. tr • 3 }, �y'e _ r pia k ahamrz•.� p w u ,n- oe �iuL?3C,-r.rcoT.., iAx. _ I V N N Z {O a [ Nf1 s ry7y1 j 1 � {[t � 1 krl{� N I M1+l" P'�}. I aw( ), Pr ' 1 rQSarvatlVP.$J_tIn f.�H(C)I Sample ID p '( N �°1 .� a E eserved ry o lH2(soa ?+(N)o3 .11(a7hiosulfae� &0H, r iIa' ❑ 1— o U' 1 m it m i (,) Outer (X) In�cate i,. tr . e. �.u•+rr U 1.Yti:a1��'�ai S_i!'M 11vh�' Set ? 30D Sv-V 7 'sue 171 i S� Feci/ j,-,,t j c sr L/ dc�6. � I iI I i ilil 1 I � 1 i.• POEMS Reib iSished1s.rl�.,, >t'nft,ili'` Rush work will require prior approval. Additional charges will apply City of Lumberton Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet p -1+—[ 'Soulfe-- Date & Analyst: Digdstet. #-I . .712.71.16 c6 lFat 11,.1 3ann ' kcl Total Solids Sample volume used for total solids test: ight-of dish: --- Weight of dish + dried solids: Weight of dried solids: Total Solids: SOUR F .121;50 0.25 9.956 Time (Minutes) Temperature Dissolved Oxygen (mg/L) 0C 0 27�M 2 3 4 5 6 —27.,00 7 8 9 & 10 11 27: 13 '2.8 1 14 P4: 0J) V. ME0,1. 15 1. 26-.001 2:0 Oxygen Consumption Rate SOUR SOUR Temperature Correction mL 9--- 9 9 g/L 0.22 mg/Uminute 1.33 (mg/g)lhr Average Sewage Sludge Temperature During Test 0C 26.8125 If sewage sludge is > 20°C, SOUR W(mglg)/hr If sewage sludge is < 20°C, SOUR (mg/g)/hr SOUR passes if result is:5 1.5 (mgfg)hr Version 11/1111 City of Lumberton Specific Oxygen Uptake Rate (SOUR) Date / Time Collected: —7• 2-7• 1 CO W IF I 1 '. ] ,-y f Analyst Initial: 1<0 Sample Location: U19. -fF Calculations: Time D.O. Temp (Min) (mgll) (°c) 1 I 0.2�1 JLI Initial DOskdlo 2 o_ 2.1SS /A_ _ --�It �SOZ/mglL/min Initial DO---15-minDO----15or-#-0f-Oareadings—Oxygen GonsumpganRate---_.—__.—____ 2 27 Digested Sludge Samples 3 5.1 2.7 X 60 r 4H.90 Or mglUmin Hr 0.2Ir-( 5 1 1 f _r_ n-7 6 y .y2 2 For Mixed Liquor Samples 7 y .2 X 60 / 8 ,'1Q -)--1 Or mg/Umin Hr 10 11 12 13 14 15 * u$CC files T TIOTALI- -t Son�li-bS IRIS 01 S a (oic� (a,-jj-VAS . s *sue- = 1.2 SOUR mg/g/hr Total Solids.(mg/L) Temp ComFenso-4-1'1) = SOUR mg/g/hr MLVSS (mg/L) Interpretation of SOUR Test Results for ML Samples High This may indicate that there are not enough solids (MLSS) for the COD > 20 mg Oi / g-MLVSS I Hr Loading 12- 20 mg Oz / g-MLVSS / Hr Normal This range will usually produce good solids sealing an dCOD removal. This may indicate that there are too many solids (MLSS) or there has < 12 mg Oy / g-MLVSS / Hr Low been a toxic ocdurence. SOURProcedurefor Mixed Liquor Samples: Collect at least Stennis of the sample to be tested. Run Total Suspended and Volatile Solids an sample: Use Smis of sample and follow the steps in the TSSNSS SOP. Other than the solids test the Procedure is the same for reading the oxygen. JR Procedure for Digested Sludge for Disposal: act at least 500mis of the sample to be tested. Total Solids on sample: Use at least 25mis of sample and follow the steps in the TS SOP. r the remaining sample Into a 1 liter beakerwith a stir bar, place the beaker on a stir plate on a moderate mbdng speed then an aeration stone to the beaker and aerate for 5 minutes. le the sample is being aerated Calibrate the DO Meter. r 5 minutes Pour the aerated sample Into a 300m1 Boo bottle with a stir bar and place the bottle onto a stir plate. While ng, place the BOD probe Into the bottle and start to measure the DO. t until meter reading has stabilized (no more than 3o sec) and start recording the DO and Temp every (1) minute for 15 Ass or unfit there is no more DO remaining. When all the readings have been recorded, clean bottles, probes and equipment ,erly. Proceed with the calculations above to complete test. Vector Attraction Reduction Requirements: (listed are the typical Alteratives we use for Sludge Disposal) Alternative 1: The mass of volatile solids in the sewage sludge shall be reduces by a minimum of 38%. Alternative 3: If Altemative 1 cannot be met for anumbicaliy digested sludge, demonstration can be made by digesting a portion of the previously digested sludge anumbically in the laboratory in a bench -scale unit for 30 additional days at 20°C. Volatile Solids must be reduced by less than IS to demonstrate compliance. Alterative 4: The specific oxygen rate (SOUR) for sewage sludge treated in an aerobic process shall be equal to or less than 1.5 mg of oxygen per hour per gram of total solids (dry weight basis) at a temperture of 20°C. Alterative 6: The pH of sewage sludge shall be ruled to 12 or higher by alkali addition and, without the addition of more alkali shag remain at 12 or higher for two hours and then at 11.5 or higher for an additional 22 hours. 7113/16 T.Smith Sample # 1 City of Lumberton U # I Total Solids Analysis Worksheet ' SM 2540 B. 1997 -- FOR PROCESS CONTROL ONLY Checked by: 1 l J Sample Day & Date: W2d 1 -?:I A G W Time IN oven7•2.I7 P I I -2Rarn Date & Time Started: _ D -- 1C0 @ I=1y a.m Time OUT of oven: -7• 22 @ 6 • al m Date & Time Completed: _7 -28 - Vo S Q � - Zq am g = Grams, Wt = Weight Analyst: Dish # Volume (MIS) Tare Wt. (g) Tare + (g) SamWt. Wet Wt. (g) Dried Wt. (g) Difference (g) Total Solids I Average TS Use if DupDupare run s ' -25 1212J 1 44 5 121 _ . 24 q 1�1 .[do?S 11344 _7 _ 2599 .34 10.15 % Solids Calculation: ;- Dried Wt. (g) X 100 = %Total solids f� Wet Wt. (g) I `r Section below is to show your work. 0 .24Sq ►3 x 100 23.015q- O 25CR I� 2L-1185� xloo X 100 = X 100 = .Q ao 1.050. 0 1. Initially use 50mis for Known and Unknowns samples and 25mis for regular samples. 2. The sample volume must yeild at least 2.5 mg of residue. 3. To get the Wet Weight; subtract the Tare Weight from the Tare+ Sample Weight ) Known Certified Known Value Obtained: Total Solids Calculation: Dried Wt. (g) x 1000 = Total Solids moll Volume (MIS) . T-18q = q qCo 2S - 259°I 25 - � 9— Limit Range: Revised 3114/16 T. Smith «�^t�K��K �00Kne��n .~"�� "~- ,°"~.~ Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet Date &Analyst: Sample # 2 Total Solids Sample volume used for total solids test: mL Weight ufdish +drindsolids: g Weight ofdried solids: 0.28 g Total Solids: 11.092 g/L SOUR Time (Minutes) Temperature Dissolved Oxygen (mg/L) DC 56 12 13 15 Oxygen Consumption Rate 0.17 nlo/L/nlinuba SOUR 0.94 (ng/q)/hr SOUR Temperature Correction Average Sewage Sludge Temperature During Test 26.375 |fsewage sludge io>2V"C.SOUR = (nog/g)/hr |fsewage sludge in<2U,C.SOUR = (nlg/g)/hr SOUR passes ifresult is:51.5(rnQ/g)br Version 11/1/11 City of Lumberton SamplC Z Specific Oxygen Uptake Rate (SOUR) Date/Time Collected: IhUYS 1 - 9 -IG Analyst Initial: Sample Location: D.O. (mgll) Temp (06 _ 12 —)7 2 1 t 3. 21 -7 43-22 27 5 6 O 7 2gr�11 S Z- t L �r /CO 9 �l CO Cact 10 2.31 11 1 12 qy 13 14 I co 2 15 1 . LV KO / KGB Cal'cuulations: pp / - t Initial DO 15 min DO 15 or# of Or readings Oxygen Consumption Rate For Digested Sludge Samples X 60 i 02 mgfUmin Hr For Mixed Liquor Samples Total Solids (mglL) X 60 Oa mg/Umin Hr MLVSS (mglL) IDS . mglUmin SOUR mgfglhr SOUR mgfgfhr Interpretation of SOUR Test Results for ML Samples High Thls may Indicate that there are not enough solids (MLSS) for the COD > 20 mg Oi / gMLVSS I Hr Loading This range will usually produce good solids settling an dCOD removal. 12-20 mg 02/g-MLVSS I Hr Normal This may Indicate That Otere are too many solids (MLSS) or there has < 12 mg Oz I g-MLVSS f Hr Low been a toxic occurrence. SOUR Procedure for Mixed Liquor Samples: Collect at least 50ands of the sample to be tested. Run Total Suspended and Volatile Solids on sample: Use 5mis of sample and follow the steps in the TSSNSS SOP. nther than the solids test. the Drocedure is the same for reading the oxvaen. JR Procedure for Digested Sludge for Disposal: sct at least 500mts of the sample to be tested. Total Solids on sample: Use at least 25mts of sample and follow the steps in the TS SOP. r the remaining sample into a 1 liter beaker with a stir bar, place the beaker on a stir plate on a moderate mixing speed then an aeration stone to the beaker and aerate for 5 minutes. Is the sample Is being aerated Calibrate the DO Meter. r 5 minutes Pour the aerated sample Into a 300ml Boo bottle with a sgr bar and place the bottle onto a stir plate. While ng, place the BOO probe Into the bolds and start to measure the DO. t until meter reading has stabilized (no more than 30 sec) and start recording the DO and Temp every (1) minute for 15 utes or unit there is no more DO remaining. When all the readings have been recorded, dean bottles, probes and equipment terly. Proceed with the calculallons above to complete test Vector Attraction Reduction Requirements: (listed are the typical Alternatives we use for Sludge Disposal) Alternative 1: The mass of volatile solids in the sewage sludge shall be reduces by a minimum of 38%. Alternative 3: If Alternative 1 cannot be met for anaembically digested sludge, demonstration can be made by digesting a pardon of the previously digested sludge anaembicaliy in the laboratory in a bench -scale unit for 30 additional days at 20°C. Volatile Solids must be reduced by less than 15 % to demonstrate compliance. Alternative 4: The specific oxygen rate (SOUR) for sewage sludge treated in an aerobic process shall be equal to or less than 1.5 mg of oxygen per hour per gram of total solids (dry weight basis) at a tempedure of 20°C. �I Alternative 8: The pH of sewage sludge shall be rested to 12 or higher by alkali addition and, without the addition of more alkali shall remain at 12 or higher for two hours and then at 11.5 or higher for an additional 22 hours. 7113/16 T.Smith Sample # 2 City of Lumberton r Total Solids Analysis Worksheet 1 j SM 2540 B. 1997 FOR PROCESS CONTROL ONLY Checked by: 5 Sample Day & Date: Thf ufs -7' � ' 1 V Time IN oven: R 1 • 22 - V-0 1 I �0 c�.m Date & Time.Started: I tarted: R -2R - I CO (9� I I (--)3 Qfm Time OUT of oven: F -7 -?q • I (.D & I G O.YY) Date & Time Completed: T -7 • 5 t - I (.0 @ .I G am _g = Grams, Wt= Weight Analyst: Y-0-- Dish # Volume (mis) Tare Wt. (0) Tare + Sam(g) Wt. Wet Wt. (g) Dried Wt. (g) 'DRY 6 T. Difference (g) Total Solids) (mgll)mgllup's FAverage TS are run ICo 2 �. I Iq 2� 2 .21�3 l I -cxl + % Solids Calculation: 'D;g.Dried Wt. (g) X 100 Sa.plc Wet Wt. (g) Section below is to show your work I� . 2-7-73 x 100 24 .ag38 _ %Total Solids X 100 = X 100 = X 100 = 1. Initially use 50mis for Known and Unknowns samples and 25mis for regular samples. 2. The sample volume must yeild at least 2.5 mg of residue. 3. To get the Wet Weight; subtract the Tare Weight from the Tare +Sample Weight Known Certified Known Value Obtained: Total Solids Calculation: 'D: T. Dried Wt. (g) x 1000 Volume (mis) Total Solids moll i� 2773 x I,OM = 11 . 25 Cfl Limit Range: Revised 3114N6 T. Smith City of Lumberton Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet Date & Analyst: Digester# 1 7/29/96 cglhat_8:28am' kd: Sample # 3 Total Solids Sample volume used for total solids test: --Weight-of-dish:-- ---- — Weight of dish + dried solids: Weight of dried solids: Total Solids: SOUR 25 36c92 127.19. 0.27 10.892 Time (Minutes) Temperature Dissolved Oxygen (mg/L) oC 0 26100E s .` 556 1 2600` 2 26;00s 518 '` 3 : 2600 "; 4 96 ; 4 2600 4.83 -' 5 6 2600 4:48'_ 7 _ 26A0 , 8 9 2&' 0 398, 11 25i00 -3:65 12 ". 2500 3:52;1. 13 2500 3'34, . ",. 14 25.00 3s16% 15 25MO 300,, mL 9 9 g/L Oxygen Consumption Rate 0.17 mg/L/minute SOUR 0.92 (mg/g)/hr SOUR Temperature Correction Average Sewage Sludge Temperature During Test oC 25.6875 If sewage sludge is > 20"C, SOUR = h�� o 7oN4W (mg/g)/hr If sewage sludge is < 20°C, SOUR = %, E.osa±c,r, (mg/g)/hr SOUR passes if result is 5 1.5 (mg/g)hr Version 1111111 Date / Time Collected: Analyst Initial: Sample Location: Time D.O. (Min) (mg/l) Initial DO 5.5 1 2 3 4 L 5 1 1 r! 6 7 8 9 10 11 12 13 14 15 City of Lumberton Specific Oxygen Uptake Rate (SOUR) F Calculations: 3.00 Temp (°C) ao XO Initial DO 15 min DO For Digested Sludge Samples X 60 / Oz mglumin Hr ) For Mixed Liquor Samples X 60 / Oa mg/L/min Hr /A � Wca or Total Solids (mglL) MLVSS (mg/L) Sampkc -A 3 = D• 17 Oi mg/Llmin SOUR mg/g/hr = SOUR mg/glhr Interpretation of SOUR Test Results for ML Samples High This may Indicate that there are not enough solids (MLSS) for the COD > 20 mg Os / g-MLVSS 1 Hr Loading 12-20 mg Oz 1g-MLVSS IHr Normal This range Will usually produce good solids settfng an clCOD removal. This may indicate that there are too many sollds (MLSS) or there has a 12 mg 0, / g-MLVSS 1 Hr Low been atoxic occurrence. (SOUR Procedure for Mixed Liquor Samples: Collect at least 500mis of the sample to be tested. Run Total Suspended and Volatile Solids on sample: Use 5mis of sample and follow the steps In the TSSfVSS SOP. Other than the solids test the procedure Is the same for reading the axvaen. 1R Procedure for Digested Sludge for Disposal: act at least Soomis of the sample to be tested. Total Solids on sample: Use at least 25mis of sample and follow the steps in the TS SOP. the remaining sample Into a 1 liter beaker with a stirbar, place the beaker on a stir plate on a moderate mixing speed then an aeration stone to the beaker and aerate for 5 minutes. e the sample is being aerated Calibrate the DO Meter. r 5 minutes Pour the aerated sample Into a 300m1 Boo bottle with a stir bar and place the battle onto a stir plate. While ng, place the BOD probe into the bottle and start to measure the DO. t until meter reading has stabilized (no mare than 30 sec) and start recording the DO and Temp every (1) minute for 15 Ace or unlit there is no more 00 remaining. When all the readings have been recorded, clean bottles, probes and equipment ,edy. Proceed with the celrxdallons above to complete test Vector Attraction Reduction Requirements: (listed are the typical Alternatives we use for Sludge Disposal) Alternative 1: The mass of volatile solids in the sewage sludge shall be reduces by a minimum of 38%. Alternative 3: If Alternative 1 cannot be met for anaerobically digested sludge, demonstration can be made by digesting a portion of the previously digested sludge anaerobically in the laboratory in a bench -scale unit for 30 additional days at 20°C. Volatile Solids must be reduced by less than 15/ to demonstrate compliance. Alternative 4: The specific oxygen rate (SOUR) for sewage sludge treated in an aerobic process shall be equal to or less than 1.5 mg of oxygen per hour per gram of total solids (dry weight basis) ale lempertum of 20°C. Alternative 6: The pH of sewage sludge shall be mated to 12 or higher by alkali addition and, without the addition or more alkali shall remain at 12 or higher for two hours and thereat 11.5 or higher for an additional 22 hours. 7/13/16 T.Smilh Sample # 3 City of Lumberton Total Solids Analysis Worksheet SM 2540 B. 1997 FOR PROCESS CONTROL ONLY Checked by: �V.S n // Sample Day & Date: Fr-1 29. Vo Time IN oven: -7 • 2G' Il0 F E) -I •1 R o rr1 Date & Time Started: yyY 1 '2G1 I —IU e 9 - VD aM Time OUT of oven: rl 12 C) /16 (� LI: I4 . , 7C5 Date & Time Completed: Minn R 1 1(0 IS •• 13 rl) g = Grams, Wt_= Weight Analyst: Kt ll Volume Tare Wt. Tare + Wet Wt. Dried Wt. Difference Total Solids Average TS Dish # SamWt. (mis) (g) (g) (g) (g) (mg �I) (g) Use if DupDup's are run % Solids Calculation: Total Solids Calculation: *D49Dried Wt. (g) I)NT Dried Wt. (g) x 1000 Ai X 100 = %Total Solids = Total Solids mgll SampIcWet Wt. (g) Volume (MIS) — below isshow Yourwork. —-- -------------------------------------------------- Se 12 ' 2, X 100 _ 12 2�23 "00 _ 25.35I3 l .01 25 1 0,C1- x 100 = _ x 100 = _ x 100 _ 1. Initially use 50mis for Known and Unknowns samples and 25mis for regular samples. 2. The sample volume must yeild at least 2.5 mg of residue. 3. To get the Wet Weight; subtract the Tare Weight from the Tare + Sample Weight Known Certified Known Value Obtained: Limit Range: RPvisad'411411 AT Smith City mfLumberton Environmental Laboratory Dato& Digester#4, ���/coll. qt�8: Total Solids Sample volume used for total solids test: 25 — — —_ —'-----'-- Weight of dried solids: 0.26 g 10.524 Total Solids: !!Ig/L IE Time (Minutes) Temperature Dissolved Oxygen (mg/L) 0C 12 MI Oxygen Consumption Rate SOUR SOUR Temperature Correction 0.14 m uhe Average Sewage Sludge Temperature During T est 25.375 |fsev«agoa|udoeiu>2O"S'8(�UR= Vhr If sewage sludge is < 20'C, SOUR = Vomion110U1 SOUR passes if result is :5 1.5 (mg/g)hr ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Lumberton WQPermitNumber: W00000672 W WTP Name: City of Lumberton W WTP NPDES Number: NCO024571 -- Monitoring Period: From 07/01/16 To 08/31/16 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. I/A (time/temp) AIL 2/B (Alk Treatment) _ Alt 3/C (Prior Testing) Alt 4/D (No Prior Test) _ Alt 5/Process to Further Reduce Pathogens _ Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost _ Heat Drying _ Heat Treatment Thermophilic Beta Ray _ Gamma Ray _ Pasteurization Class B: Alt (1) Fecal Density Alt (2) Process to Significantly Reduce Pathogens X If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization X Air Drying Composting _ ' Aerobic Digestion Anaerobic Digestion Tf annfr"hle 4n alternatve nrrfnrmrd !r'lace A n� rtnce TV, rmmnW" *hn fnllnwino mnn if. A.. dn4n• Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical " Excee- of Type Technique Minimum Gen. Mean Maximum Units dences Analysis Fecal 2x10 to the 6 MPN MPN/g Coliform power per gram of total solids CFU CFU/g 0 quarterly grab 9222D 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0pption/Alt 1 Option/AlL 2 Option/Alt 3 Option/Alt. 4 (VSreduction) (40-day bench) _ (30-daybench) (Spec. 02 uptake) Option/Alt 5 Option/Alt. 6 Option/Alt 7 Option/Alt. 8 (14-Day Aerobic) (AlkStabilization) X (Drying —Stable) (Drying —Unstable) Option/Alt 9 Option/Alt 10 (Injection) (Incorporation) _ No vector attraction reduction alternatives were performed STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15ANCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met" (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction. reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment " Jim Walters, Director ofEUS Dept Pre arer Name and Title (type or print) Si tureofPreparer* Date Land Applier Name and Title (if applicable) (type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) CLA LOG SHEET Using a pH Meferwith,Two-Point Stanardizatioon anPH Auttomatic Temperature Compensation (ATc) probe Analysis Method: SW-846 Method 9040B, off Electrometric Measurement Process A MdTHM�• racfuzxriocATtata: ,,i o dtmbe��ic,r, WW�P Control satnFLtnlG f_ccaruaw: Sample Sampler Stan Date Time bnaps Time t--quivalentpH value at25EC; Con "T if the reading is not done 24 hours Comments. I Start pH/ Temp EC i Factor the star Adjusted Start pH' PH Testing 2-Hr.: pH! Adl Temp EC 2-F usted r PH' 24-Hr pH-1 Temp EC &dusted 24-Hr pH" Start 2 Mrs 24. Ctrs i i f i = 0.03 pH un'ds x (EC Temperature measurement 25EC), Equivalent pH = Measured pl-t +J_ the CF. e, note the time (and date if not perforated the day following the initial sample date) the reading Was taken_ Di3 3 );9.2 0 Using a pH Meter with Tutu -Point Standardization and Automatic Temperature Compensation (ATC) probe Analysis Method: SW-846 Method 90$013, pH Electrometric Measurement MONTHf: FACILITYfLOCATION: _ 1� OT t lrn h % SAMPLING LOCAT'goN. I 0 Zo[U ,?ate Sample Yime Sampier hitials 17 I C i �2 4" pH Testing Analyst Initials Start Time Mart KI Temp EC Start pHa Temp LOCI 2dHu pHa 'r' mp EC I 24-H pH* Start firs Hrs A i �olrt, 1:1sn� Il.s / 2to.r AckR 2"d o.-1 � solo -1(2dli. l 10 SL # - I (. - ,Pr:or -}o ime add'i�on l � sL- lieo YL o iz:o I I 12..0 /z-7 U 12.c) 12.0 2 �` i2.03 zaw�m {.7 L y 11.�3 z 7Z03 ` I i i I � 1 li _. Oc4 • c_.,c._i__. Equivalent pH value al:25EC; Correction Factor(c.F) = 0.03 pH units,-(B Temnemtur2 mRAsnmmanf _ _.. - • - . • w. ��„_ =w „eu,s dnlr ule arart r tme, note the tune (and date if not performed the day fallowing the initial sample date) the reading yeas taken_ comment;: r �t•pn.K % 2cl—J6CLASS BIPSRP pH LOG SHEET ,.._ Using a pH M ter with Two -Point Sty dard"tion and Automatic Temperature Compensation (AFC) probe Analysis Method: SW-646 Method 9040B, pH Electrometric Measurement MORTHNEAR- PACILMNLOCAT{ON: , C I i L 1, fib(� f SAMPLING LOCATdON: f wyv_=p Icy t 5 ' pH Tesvng Analyst Initials Sample Sampler Start Start PHI Adjusted 2-Mr.: pHf Adjusted 24-Hr pH"�f Adjusted 2 14, Date Time fUtitiaLs Time Temp EC Stan pH Tem BC i P 2-Hr pH Temp EC 24-[=Ir pH" Start Mrs s ors %-1 S'rL / c: i.3' -�uG lo•z33� f Z •o� �� y /a1/� t 5v i Ey Nn value ar25tsC Correction Factor (CF) 0 03 pH s (a+. J empandure measurement ?5EC), Equivalent pH =Measured pH +/_ the CF. If theread[ne is not done 24 hours afie{ the Start Time, note the lima (and date if not performed the day following the initial sample date) the reading was taken_ Comments - - ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) FacilityName: City of Lumberton WQPermit Number: W00000672 ' WWTPName: City of Lumberton WWTP NPDESNumber: NCO024571 Monitoring Period: From 09/01/16 To 12/31/16 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt 2/13 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) _ Alt 5/Process to Further Reduce Pathogens _ Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further. Reduce Pathogens": Compost _ Heat Drying _ Heat Treatment _ Thermophilic Beta Ray Gamma Ray _ Pasteurization Class B: Alt (1) Fecal Density X Alt (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization _ Air Drying Composting _ Aerobic Digestion Anaerobic Digestion Tf annlirahle to alternative nerfnrmed Wlocc A nr Clacc Rl rmmnlefe the fnllmvino mn.ifnri.o data - Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10tothe MPN MPN/g Coliform power per gram of total solids CFU <91600 <102000 <108000 CFU/g 0 quarterly grab 9222D 1000 MPN per gam of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0ption/Alt 1 Option/Alt 2 Option/Alt 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) (Spec. 02 uptake) X Option/Alt 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (AlkStabilization) (Drying —Stable) (Drying —Unstable) Option/Alt 9 Option/Alt. 10 (Injection) _ (Incorporation) _ No vector attraction reduction alternatives were performed STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met" (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met I am aware that there are significant penalties for false certification including fine and imprisonment" Jim Walters, Director of EUS Dept, Preparer Name and Title (type or print) Land Applier Name and Title (if applicable) (type or print) S' re of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) Cameron Testing Services, Inc. Laboratory Report ,. Caient Synagro PF pr Pebidd Lumberton egula4 Sample Information W. Varner �x Dafe 08109116Recetved' Analyses and Results Lab ID,-, 5amp{e90 z U_� _ ,�AnalyfeResWt 161200 -1 SNdgr Gr Fen. CollfarmS <102000 -2 <91600 -3 <104000 -4 <103000 -6 <108000 -6 <105000 -7 <103000 Geomean <102000 161200 -1 =Wdge Cr TS {%) 0.953% -2 1.05% -3 0.896% -4 0.948% -5 0.927% -6 0.917% -7 0.974% Report J) d --- ---- -- Review Lab Director NO DENR#554 NO PHHS #37799 US EPA#NC01918 161200 Yes Cameron Rate._ 08/09116 laz000 08/10/16 elsao 104D00 10.3Da0 108000 10s000 103000 0.01 08115116 0.01 0.01 0.01 0.01 0.01 0.01 og_ /6/4 Date Std:Methods� i s Re(e-flr ence 9222D - MF 2540 G -TS 219 S. Steele Str. Sanford NC 27330 919.20&4240 chris@camemnicsting.com 219 S. Steele Str. Sanford, NO 27330 Cameron Testing Services, Inc. NC W W/GW Cert #654 NC PHHS Cert# 37799 US EPA NCO1918 -Chain of Custody Page I Of 919 208-424U S yt Ernall; mpuryear@synegro.com x+ G�5labt�uSefonly , sir t; .,s ort'iPan ? E°�Ir S na r0 Y 9 +� 3 F 336-909-8627 l r, ( ZOO ' �o �tljtact Marsha{I Puryear `�, Phone: Sam le Temp s r p' .r c� r3 Z. S1P(o +I , � 1 .,t,; , ,+ ArxVea` _ not°essFtii 284 Boger Rd. F —- 4,F�s�ate4s MOCksVllle, NC 27028tes, rr'r k i a" oil I PrAle7c�k, .-.. •,: s 1(Y/N):. i� u(Y/N)'.gl Colledcter]� i� Name �^ Signature u rZ .nm it t, c "- r11 1 t i k > ♦�F,. { 2 Y '. .s amp eilnformation , Number of bottles._ ,zr v ( Requestedypnaly�f ;,,1( �-{ gj,, , O I Sample ID d o o ° m + y ,� 0 I A 0 45 c7 g W E m Preservatives (U)0pt8served H(C)I ,r r t.�,4.TraullN'i l cs s �— r ? a 1 wID,6 H2(S)04 H(N)W (N�)Thhwsulfate Na(0)li & f� '1 o ° ;u F-- a V I m I a3,' ther(X) Ilnldicate Np) V I I mQ•"fYi�l�—`—a CA I R -.�-. hed;"� ,h� � ,,.� � , �,•' .,:..' _ ...�`��:,., `Received. "> � a�}c� �, r 1uDate(fiineft�.Idv3i�:�f!�a c+ AD rr' Iyz� Rush work will require prior approval. Additional charges will apply City of Lumberton Specific Oxygen Uptake Rate (SOUR) M Date / Time Collected: �j I - V-0 @ 095-0 Am Analyst Sample Location: ® '• m MR • mm� Mmm ®m® Calculations: KO / H H / KC.L M - 3.04 / I'7 - DO 15 or # of Oz readings For Digested Sludge Samples x 60 / 02 mg/L/min Hr Total Solids (mg/L) For Mixed Liquor Samples X 60 / 02 mg/Umin Hr MLVSS (mgfQ -44 02 mg/Llmin Oxygen Consumption Rate SOUR mgfglhr SOUR mgfglhr Interpretation of SOUR Test Results for ML Samples High This may indicate that mere are not enough solids(MLSS) for the COD - > 20 mg Oi f gfALVSS / Hr Loading 12 - 20 mg 021g-MLVSS / Hr Normal This range will usually produce good solids setting an cICOD removal. This may indicate that mere are too many solids (MLSS) or mere has < 12 mg Oi / g-MLVSS I Hr Low been a toxic ocanence. IR Procedure for Mixed Liquor Samples: ct at least 500mis of the sample to be lasted. Total Suspended and Volatile Solids on sample: Use Smis of sample and follow the steps in the TSSNSS SOP. JR Procedure for Digested Sludge for Disposal: sct at least 500mis of the sample to be tested. Total Solids on sample: Use at least 25mis of sample and follow the steps in the TS SOP. r the remaining sample Into a 1 liter beaker with a stir bar, place the beaker on a stir plate on a moderate mixing speed then an aeration stone to the beaker and aerate for 5 minutes. Is the sample Is being sanded Calibrate the DO Meter. r 5 minutes Pour the aerated sample Into a 300m1 Boo bottle with a stir bar and place the botte onto a stir plate. While ng, place the SOD probe into the bottle and start to measure the DO. t until meter reading has stabilized (no more than 30 sec) and start recording the DO and Temp every (1) minute for 15 .Ites or unlit mere is no more DO remaining. When all the readings have been recorded, clean bottles, probes and equipment redy. Proceed with the calculators above to complete test Vector Attraction Reduction Requirements: (listed are the typical Alternatives we use for Sludge Disposal) Alternative 1: The mass of volatile solids in the sewage sludge shall be reduces by a minimum of 38%. Alternative 3: If Alternative 1 cannot be met for anaerobicatly digested sludge, demonstration can be made by digesting a potion of the previously digested sludge anaerobically In the laboratory In a bench -scale unit for 30 additional days at 20PC. Volatile Solids must be reduced by less than 15%to demonstrate compliance. Alternative 4: The specific oxygen rate (SOUR) for sewage sludge treated in an aerobic process shall be equal to or less than 1.5 mg of oxygen per hour per gram of total solids (dry weight basis) at a tempedure of 20°C. Alternative 6: The pH of sewage sludge shall be fasted to 12 or higher by alkali addition and, without the addition of more alkali shall remain at 12 or higher for two hours and then at 11.5 or higher for an additional 22 hours. 7113116 T.Smith City of Lumberton Total Solids Analysis Worksheet SM 2540 B. 1997 FOR PROCESS CONTROL ONLY Sample # 4 f u n {<nowf Qcro n Checked by: o�S Sample Day & Date: �Mnn • 1 • V0 Time IN oven: M (1 p1 {(ri L"^q'•33 Clm Ds� 4 ate & Time Started: �c� 1 tCo 9 •22 n m Time OUT of oven: M C� I �C 0 l y�nm Date & Time Completed Z1.2 1(D q C)2� n rn g=Grams,Wt=lVelght --- -- --- Rnaly — ---K .- -- ------ Dish # Volume (MIS) Tare Wt. (g) Tare + Sample Wt. (g) Sample Wet Wt. (g) Dried Wt. g () Dried Wt. Difference (g) Total Solids (mg/1) Avg1eage TS (mg/1) Use if Dup's are run 10 10.5 ScxxY,ple 10.5 {q % Solids Calculation: Total Solids Calculation: WP 2E-B ' Dried Wt. Diff (g) X 100 = %Total Solids Dried Wt. Diff (g) X 1000 = Total Solids moll Sample Wet Wt. (g) Volume (MIS) ---" `—I-----_—_-----------------I-----`-------------- Sectionbelow is to show your work 10 . 2Co31 —X100 = LOCO to 2�3 l x 1, CEO _ 2q.7727(o 25 - -�rJ.5 X 100 = _ X 100 = _ X 100 = _ 8 .O 123 x I , CX7 coc) 2y9.8 1. Initially use 50mis for Known and Unknowns samples and 25mis for regular samples. 2. The sample volume must yeild at least 2.5 mg of residue. 3. To get the Wet Weight; subtract the Tare Weight from the Tare + Sample Weight Known Certified Value: Known Value Obtained: Limit Range: U n known ', 2�{9 •g City of Lumberton Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet Date & Analyst: Digester # I - -9:48.9m Ikcl Sample # 5 Total Solids Sample volume used for total solids test: I : ,- I ... . 26 mL Weight of dish + dried solids: Weight of dried solids: Total Solids: SOUR Time (Minutes) Temperature Dissolved Oxygen (mg/L) 0C 0 7 2 --25 3 4 2E 0 .3 5 6 6m197 - 7 25900 60,0--F 8 7 .590. .2 QO 7,+,6.7,67.. I-M 10 .26i00.2—�7:"'. d 51671. 11 2 25.100 12 "` 25.0 5.45 —% 13 2510.0% 14 523 15 % ..25.0 0 Oxygen Consumption Rate 0.12 mg/Uminute SOUR 0.67 (mglg)/hr SOUR Temperature Correction Average Sewage Sludge Temperature During Test 0C 25 r. If sewage sludge is > 20°C, SOUR 6.10t�t(mg/g)/hr If sewage sludge is < 20°C, SOUR SOUR passes if result is:5 1.5 (mglg)hr Version 1111111 City of Lumberton Specific Oxygen Uptake Rate (SOUR) Date / Time Collected: 1 JR - �' 1 c @ 9 • q �i rim Analyst Initial: 1� / H H / W-C-L Sample Location: ® r. M . •• ffm� Mr=.® © • • ©rlw� Mvlm� PIM • is� MW 6 6 Mmm MM. � mvw�_ mi Calculations: socmplc #5 ! = 02 mg/Lfmin Initial DO 15 min DO 15 or# of %readings Oxygen Consumption Rate For Digested Sludge Samples X 60 / Oa mg/llmin Hr Total Solids (mg)L) For Mixed Liquor Samples X 60 / Oz mg/Ilmin Hr MLVSS (mg/L) SOUR mglglhr SOUR mglglhr Interpretation of SOUR Test Results for ML Samples High This may Indicate that there are not enough solids (MLSS) for the COD > 20 mg 01! gMLVSS/ Hr Loading This range will usually produce good solids settling an dCOD removal. 12- 20 mg Or /g-MLVSS / Hr Normal This may indicate that there are too many solids (MLSS) or there has < 12 mg Or 1 g-MLVSS / Hr Low been a toxic occurrence. SOUR Procedure for Mixed Liquor Samples: Collect at least 500mis of the sample to be tested. Run Total Suspended and Volatile Solids on sample: Use 5mis of sample and follow the steps In the TSSNSS SOP. Other than the solids test. the procedure is the same for reading the oxygen. SOUR Procedure for Digested Sludge for Disposal: Collect at least 500MIs of the sample to be tested. 'Run Total Solids on sample: Use at least 25mis of sample and follow the steps in the TS SOP. Pour the remaining sample Into a 1 liter beaker with a stir bar, place the beaker on a stir plate on a moderate mixing speed then add an aeration stone to the beaker and aerate for 5 minutes. While the sample is being aerated Calibrate the DO Meter. After 5 minutes Pour the aerated sample Into a 300m1 SOD bottle with a stir bar and place the bottle onto a stir plate. While mixing, place the Boo probe into the bottle and start to measure the DO. Wait until meter reading has stabilized (no more than 30 sec) and start recording the DO and Temp every (1) minute for 15 minutes or until there is no more DO remaining. When all the readings have been recorded, clean bottles, probes and equipment property. Proceed with file calculations above to complete lest Vector Attraction Reduction Requirements: (listed are the typical Alternatives we use for Sludge Disposal) Alternative 1: The mass of volatile solids in the sewage sludge shall be reduces by a minimum of 38%. Alternative 3: If Alternative 1 cannot be met for anaerobically digested sludge, demonstration can be made by digesting a portion of the previously digested sludge anaerobically in the laboratory in a bench -scale unit for 30 additional days at 20°C. Volatile Solids must be reduced by less than 15%to demonstrate compliance. Alternative 4: The specific oxygen rate (SOUR) for sewage sludge treated in an aerobic process shall be equal to or less than 1.5 mg of oxygen per hour per gram of total solids (dry weight basis) at a lempenure of 20°C. Alternative S: The pH of sewage sludge shall be rusted to 12 or higher by alkali addition and, without the addition of more alkali shall remain at 12 or higher for two hours and then at 11.5 or higher for an additional 22 hours. 7113/16 T.Smith Sample # 5 City of Lumberton Total Solids Analysis Worksheet IP SM 2540 B. 1997 FOR PROCESS CONTROL ONLY Checked by: Sample Day & Date: —Tt d es 18(�Z• I (D Time IN oven: l T R ' j 0 e IOi .03 Date & Time Started: •Z Q \i IOC 1DOM Time OUT of oven: 2 ' (9 @ + • l +� Date & Time Completed:W R • ?) 0 q LI 0.m its _g = Grams, Wt.= 1<C L Dish # Volu me (MIS) Tare Wt. (g) Tare + Sample Wt. (g) Sample Wet Wt. (g) Dried Wt. (g) Dried Wt. Difference (g) Total Solids (Mg/1) Average TS (Mg/1) Use if Dup's are run 1co 2S qLA.Tas Im 25,3U4C6-1qqO .2(v55 10.Co It %Solids Calculation: Dried Wt. Diff (g) X 100 Sample Wet Wt. (g) Section below is to show your work. . 2(D55 —X100 25.3I-14 = %Total Solids X 100 = X 100 = X 100 = 1. Initially use 50mis for Known and Unknowns samples and 25mis for regular samples. 2. The sample volume must yeild at least 2.5 mg of residue. 3. To get the Wet Weight; subtract the Tare Weight from the Tare+ Sample Weight Total Solids Calculation: Dried Wt. Diff(g) x 1000 = Total solids moll Volume (MIS) Ito . 2Co55 x I ,0:0 = 10.G 25 Known Certified Value: Known Value Obtained: Limit Range: Revised 3/14/1ST. Smith 11 City of Lumberton Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet Date & Analyst: Digester # 1' ' $/3/16 coil st 8:49; am. ;kdI Sample # 6 Total Solids Sample volume used for total solids test: Weight of dish + dried solids: Weight of dried solids: Total Solids: mL 9-------- 9 9 g/L SOUR 25 123'�'L1 12136 0.25 10.096 Time (Minutes) Temperature Dissolved Oxygen (mg/L) aC 0 ;' 25:00"' ` . ,_ 8.02.. ,. 1 2500 2 2500 3 25.00 7t73' 4 25 00 ?.`62 , _ 6 25;00 745 a. 7 2500 733, 8 25600 . ' M13 25+.00 10 25L0.0 77r26" 10_ '' 12 :. 25.00 ;. ' 6 87' 25:00 14 25MO °'6i75. 15 "•24:OQ 6i70'" Oxygen Consumption Rate 0.09 mg/L/minute SOUR 0.53 (mg/g)/hr SOUR Temperature Correction Average Sewage Sludge Temperature During Test °C' 24.9375 If sewage sludge is > 20°C, SOUR =U-11 > 0.1 t, :, (mg/g)/hr cccu. If sewage sludge is < 20°C, SOUR = 21 wo;as'' :,r (mg/g)/hr SOUR passes if result is <_ 1.5 (mg/g)hr Versian 11/1/11 1 Date / Time Collected: Analyst Initial: Sample Location: ® r• - .. . 0 MMI ©sw® mu© m®mi t wne�. Me e M City of Lumberton Specific Oxygen Uptake Rate (SOUR) W -rr / u 1-+ / v-CL Calculations: / = Oz mg/lJmin Initial DO 15 min DO 15 or#of Oy readings Oxygen Consumption Rate For Digested Sludge Samples X 60 / OZ mg/L/min Hr Total Solids (mg/L) For Mixed Liquor Samples X 60 / Oz mg/l.lmin Hr MLVSS (mg/L) SOUR mg/g/hr SOUR mg/g/hr Interpretation of SOUR Test Results lcr ML Samples High This may indicate that there are not enough solids (MLSS) for the COD > 20 mg Or / g-MLVSS / Hr Loading , This range will usually produce good solids setting an dCOD removal. 12- 20 mg Or /g-MLVSS / Hr Normal This may indicate that there are too many solids (MLSS) or there has < 12 mg Or / g-MLVSS / Hr Low been a toxic occurrence. (SOUR Procedure for Mixed Liquor Samples: Collect at least 500mis of the sample to be tested. Run Total Suspended and Volatile Solids on sample: Use 5mis of sample and follow the steps in the TSSNSS SOP. Other than the solids test. the Dracedure Is the same for readinq the oxygen. JR Procedure for Digested Sludge for Disposal: act at least 500nds of the sample to be tested. Total Solids on sample: Use at least 25mis of sample and follow the steps In the TS SOP. the remaining sample into a 1 liter beaker with a stir bar, place the beaker on a stir plate on a moderate mixing speed then an aeration stone to the beaker and aerate for 5 minutes. e the sample is being aerated Calibrate the DO Meter. 5 minutes Pour the oersted sample Into a 300ml SOD bottle with a stir bar and place the bottle onto a stir plate. While ng, place the BOD probe Into the bottle and start to measure the 00. 1 unfit meter reading has stabilized (no more than 30 sec) and start recording the 00 and Temp every (1) minute for 15 Ass of until there is no mom DO remaining. When all the readings have been recorded, clean bodies, probes and equipment ierly. Proceed with the calculations above to complete lest. Vector Attraction Reduction Requirements: (listed are the typical Alternatives we use for Sludge Disposal) Alternative 1: The mass of volatile solids In the sewage sludge shall be reduces by a minimum of 38%. Alternative 3: If Alternative 1 cannot be met for anaerobically digested sludge, demonstration can be made by digesting a portion of the previously digested sludge anaerobically in the laboratory in a bench -scale unit for 30 addilcnal days at 20°C. Volatile Solids must be reduced by less than 15 % to demonstrate compliance. Alternative 4: The specilicoxygen rate (SOUR) forsewage sludge treated in an aerobic process shall be equal to or less than 1.5 mg of oxygen per hour per gram of total solids (dry weight basis) at a lemperture of 200C. Alternative 6: The pH ofsewage sludge shall be rasied to 12 of higher by alkali addition and, without the addition of more alkali shall remain at 12 or higher for two hours and then at 11.5 or higher for an additional 22 hoom- 7113116 T.Smith City of Lumberton ' Total Solids Analysis Worksheet SM 2540 B. 1997 FOR PROCESS CONTROL ONLY Sample # (— D19 . # 1 Checked by: —111-5 Sample Day & Date: wed ed 18.3 • 1(0 Time IN oven W R �p 11]�9 fC� q -?—'AQM Date & Time Started: VV FS-�3,•11�0 E `t LI dm Time OUT of oven: W Cl' `3• ICD IS I `D : �iCir� Date & Time Completed: 1C ZS • `i •1(o R Zs g = Grams, Wt = Weight_ -- ---Analyst _Analyst: KC L Dish # Volume (MIS) Tare Wt. (g) Tare+ Sample Wt. (g) Sample Wet Wt. (g) Dried Wt. (g) Dried Wt.' Difference (g) Total Solids (mg/1) Average TS (Mg/1) Use if Dup's are run CCQ 25 12330- 11 Aq.49t7 123.315 0.a7��� a. % Solids Calculation: Total Solids Calculation: Dried Wt. Diff (g) X 100 = %Total solids Dried Wt. Diff (g) x 1000 = Total Solids mgll Sample Wet Wt. (g) Volume (MIS) Section belowisto showyourwork I I I I I �. I O 0,1,� —X 100 = � oCn 0.252q x [VcDD 17 1 a X 100 = _ X 100 = _ X 100 = _ 1. Initially use 50m13 for Known and Unknowns samples and 25mis for regular samples. 2. The sample volume must yeild at least 2.5 mg of residue. 3. To get the Wet Weight; subtract the Tare Weight from the Tare +Sample Weight Known Certified Known Value Obtained: Limit Range: Revised 3I14116 T Smith �"����Lumberton � ��U,��u Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet Date & Analyst: Total Solids Sample volume used for total solids test: 26 noL - --_-'J8&»iUbLufdish: --_�---__�'__-_.'N10.556g/L g_----'---_---_-- VVoghtofdish +dhedsolids: g YVeight ofdhedsolids: 9 Total Solids: SOUR Time (Minutes) Temperature Dissolved Oxygen (mg/L) 0C 11 12 13 14 15 Oxygen Consumption Rate 8.07 mg/L/nlinute SOUR 0.38 (nog/g)/hr SOUR Temperature Correction Average Sewage Sludge Temperature During Test 23.5625 |fsewage sludge is >20,C.SOUR |fsewage sludge is<20,C'SOUR � ( ` SOUR passes ifresult ia:5 1.5(nQ/g)b, -' Version 1{8/11 City of Lumberton Specific Oxygen Uptake Rate (SOUR) ' Date / Time Collected: O • q -' (Q R °e 10'. z5 O A vl� Analyst Initial: Sample Location: Time (Min) D.O. (Mgt[) Temp (°c) InItIaIDO _24 1 /ld-_ 75 . 09 2 2 �.05 2 3 7. fp2 2 4 i.95 2 s 2 6 T-I I 24 7 7. ro z 8 7./Qo Z 9S2 2 3 16 50 2 3 11 7. 4 23 12 7.38 23 13 7.Z$ 23 14 7.2Z- Z 15 -7.17'_ 23 S M. Calculations: / _ __ _ __ _ _ __ OZ mLI _g/_m_in_ Initial DO 15 min DO _ 15 or# of Os readings Oxygen Consumpgan Rate For Digested Sludge Samples X 60 / Oa mg/Ilmin Hr For Mixed Liquor Samples Total Solids (mg/L) X 60 / _ Oz mg/L/min Hr MLVSS (mg/L) SOUR mgfgfhr SOUR mgfgfhr Interpretation of SOUR Test Results For ML Samples High This may indicate that there are not enough solids(MLSS) forthe COD > 20 mg O�! g-MLVSS / Hr Loading 12- 20 mg Or /g-MLVSS / Hr Normal This range will usually produce good solids settling an dCOD removal. This may indicate that there are too many solids (MLSS) or there has < 12 mg oz / g-MLVSS / Hr Low been a toxic occurrence. (SOUR Procedure for Mixed Liquor Samples: Collect at least 500m1s of the sample to be tested. Run Total Suspended and Volatile Solids on sample: Use 5mis of sample and follow the steps In the TSSNSS SOP. Other than the solids test. the procedure Is the same for reading the oxygen. JR Procedure for Digested Sludge for Disposal: act at least 500mis of the sample to be tested. Total Solids on sample: Use at least 25mis or sample and follow the steps in the TS SOP. the remaining sample Into a 1 liter beaker with a stir bar, place the beaker on a stir plate on a moderate mbdng speed then an aeration stone to the beaker and aerate for 5 minutes. e the sample is being aerated Calibrate the DO Meter. r 5 minutes Pour the aerated sample Into a 300m] Boo bottle with a stir bar and place the bottle onto a stir plate. While ng, place the Boo probe into the battle and start to measure the DO. until meter reading has stabilized (no more than 30 sec) and start recording the DO and Temp every (1) minute for 15 des or until there is no more 00 remaining. When all the readings have been recorded, clean bellies. probes and equipment �edy. Proceed with the calculations above to complete test Vector Attraction Reduction Requirements: (listed are the typical Alternatives we use for Sludge Disposal) Alternative 1: The mass of volatile solids in the sewage sludge shall be reduces by minimum of 38%. Alternative 3: If Alternative 1 cannot be met for anaerobically digested sludge, demonstration can be made by digesting a portion of the previously digested sludge anaerobically In the laboratory In a bench -scale unit for 30 additional days at 200C. Volatile Solids must be reduced by less than 15% to demonstrate compliance. Alternative 4: The specific oxygen rate (SOUR) for sewage sludge treated in an aerobic process shall be equal toror less than 1.5 mg of oxygen per hour per gram of total solids (dry weight basis) at a temperture of 200C. Alternative 6: The pH or sewage sludge shall be rasied to 12 or higher by alkali addition and, without the addition of more alkali shot] remain at 12 or higher for two hours and then at 11.5 or higher for an additional 22 hours. 7/13/16 T.Smith City of Lumberton r" Total Solids Analysis Worksheet SM 2540 B. 1997 FOR PROCESS CONTROL ONLY Sample # 17;5-a ( Checked by: Sample Day & Date: l it u r S 2 A 1 ( Time IN oven: 100 API 1 Date & Time Started: 9 A 1)(0 e I 05Za A w Time OUT of oven: n9"7;_A rv1 '/ZS Date & Time Completed: 915-i/6 !-0 /02. 0arj, ..g=Grams, Wt=_W_eight ------ --- -----90atyst: — -- ----5 - - - _._.. Dish # Volume (MIS) Tare Wt. (g) Tare + Sample Wt. (g) Sample Wet Wt. (g) Dried Wt. (g) Dried Wt. Difference (g) Total So) lids (Mg Average TS (mgll) Use if Du pis are run 1 CQ 25 C14. q3LM i)0.'-M5y 53S t 6igg 0.2039 /0. to % Solids Calculation: (' Dried Wt. Diff (g) X 100 t Sample Wet Wt. (g) Section below is to show your work 0.26xss7 ."9 X100 as. X 100 X 100 X 100 Total Solids Calculation: %Total Solids Dried Wt. Dlff (g) X 1000 = Total Solids mn/I Volume (MIS) 1. Initially use 50mis for Known and Unknowns samples and 25mis for regular samples. 2. The sample volume must yeild at least 2.5 mg of residue. 3. To gel the Wet Weight; subtract the Tare Weight from the Tare+ Sample Weight Known Certified Value: Known Value Obtained: Limit Range: P A%,iCPrf'i/1d/1r3T Rmifh City of Lumberton VJV WTP 2016 Lime Log �MWMIMEMIMf * Lime to spread at a later date. * Lime to spread at a later date. Page 1 of 5 L ` Report Number: 17-020-0622 Account Number:46525 Send To: Synagro Central LLC/ Lumberton Mary Brewer 284 Boger Road Mocksville NC 27028 1 5 r Waypoint ANALYTICAL "Every acre... Everyyear. "n, Date Received: 01/20/2017 Date Of Analysis: 01/23/2017 Farm ID: R016 SOIL ANALYSIS REPORT Date Of Report: 01/23/2017 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical.com Grower: Oaeu Buker/ Lumberton Analytical Methoci SMP Buffer pH Mehlich 3 Loss On Ignition Water pH OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Field ID Lab Number % Rate 'Soil Class Ibs/A M3 peat Rate ppm Rate ppm Rate K plant Rate M 9 ppm Rate Ca ppm Rate Na ppm Rate Soil PH Buffer Index H meg11009 meg1100g R016-1 12924 1.7 L 78 162 VH NC=135 67 M NC=34 70 M 553 M 5.9 6.86 0.7 4.2 MIN R016-2 12925 3.4 M 111 98 H NC=82 86 M NC=44 94 H 567 M 5.7 6.83 1.0 4.8 MIN R016-3 12926 2.2 L 87 166 VH NC=138 69 L NC=35 78 M 675 M 5.8 6.83 1.0 5.2 MIN R016-4 12928 3.3 M 106 68 H INC =57 69 L NC=35 147 H 841 M 5.9 6.81 1.2 6.8 MIN R016-5 12929 1.9 L 82 213 VH NC=177 93 H NC=48 80 H 577 M 6.4 0.4 4.2 MIN Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron_ Soluble salts Sample Fed ID ID K Mg o� Ca o� Na o� H o NO3 N Ppm Rate S ppm Rate Zia ppm Rate _ Min pp m Rate Fe ppm Rate Cu ppm Rate B ppm Rate SS mslcm Rate R016-1 4.1 13.9 65.8 16.7 R016-2 4.6 16.3 59.1 20.8 R016-3 3.4 12.5 64.9 19.2 R016-4 2.6 18.0 61.8 17.6 R016-5 5.7 15.9 68.7 9.5 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. samples are retained soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (mill -mhos per centimeter), megl100g maximum of thirty days aftertesting. by PdW/o IV G� H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble .analysis prepared by: WaypolntAnalNleal Virginia, Inc. C.E.C. -Cation Exchange Capacity. Salts ms/cm x 640 = ppm. - Pauric McGroary Page 2 of 5 Report Number: 17-020-0622 Account Number: 46525' Wa of nt„� 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 Send To: Synagro Central LLC/Lumberton ANALYTICAL www.waypointanalytical.com Mary Brewer "Every acre... Every year."n Grower: Ozzeu Buker/ Lumberton 284 Boger Road Mocksville NC 27028 Farm ID: R016 Date Received:01/20/2017 Date Of Report: 01/23/2017 SOIL FERTILITY RECOMMENDATIONS Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yeld Goal Lime N PpOs K20 Mg S Zn Mn Fe Cu B Field ID TonslA IbJA Ib/A Ib/A Ib/A Ib/A Ib/A MIA Ib/A Ib/A Ib/A R016-1 Adjust pH to 6.0 0 0.8 10 R016-1 Bermuda, Coastal 5 0.8 75 0 368 10 R016-2 Bermuda, Coastal 5 0.8 75 30 329 0 R016-2 Adjust pH to 6.0 0 0.8 0 R016-3 Bermuda, Coastal 5 0.8 75 0 375 2 R016-3 Adjust pH l0 6.0 0 0.6 2 R016-4 Adjust pH to 6.0 0 0.6 0 R016-4 Bermuda, Coastal 5 0.8 75 30 394 0 R016-5 Bermuda, Coastal 5 0.0 75 0 305 0 R016-5 Adjust pH to 6.0 0 0.0 0 Comments: "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." me �� Our reports and letters are for the exclusive and confidential use of our clients„ l and may not be reproduced In whole or part, nor may any reference be made to the awry work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary Page 3 of 5 Report Number: 17-020-0622 Account Number:46525 Send To: Synagro Central LLC/ Lumberton Mary Brewer 284 Boger Road Mocksville NC 27028 r Waypoint. ANALYTICAL "Every acre... Everyyear. ",u 7621 Whitepine Road, Richmond, VA 23237 Main 804.743-9401 a Fax 804-271-6446 www.waypointanalytical.com Farm ID: R016 Sample(s) : R016-3 Crop: Adjust pH to 6.0 Apply dolomitic lime to raise pH and improve the magnesium level. If dolomitic lime is not used, apply required magnesium with magnesium oxide. Epsom Salts, K-Mag or Sul-PO-Mag. Sample(s) : RO16.2,RO16-3,RO16-4,R016-5 Crop: Bermuda, Coastal Grower: Oaeu Buker/ Lumberton Apply additional 65 pounds of nitrogen after every cutting and harvest of hay. The recommended potash is the total pounds/acre needed to achieve the specified yield goal. Apply 112 or 1/3 (100-150 pounds) of the total at the first application in spring or fall. Application of the remaining should be determined by the yield achieved after the first cutting and the moisture condition. If in drought condition and yield is low the following applications should be reduced or eliminated. 'The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or Implied, concerning crop performance is made."p Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the Pow" 10 A� work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Paudc McGroary Page 4 of 5 Report Number: 17-020-0622 Account Number:46525 Send To: Synagro Central LLC/ Lumberton Mary Brewer 284 Boger Road Mocksvllle NC 27028 1 WaY- ointn� ANALYTICAL "Every acre... Everyyear."> Date Received: 01/20/2017 Date Of Analysis: 01/23/2017 Farm ID: R016 SOIL ANALYSIS REPORT Date Of Report: 01/23/2017 40 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical.com Grower: Ozzeu Buker/ Lumberton Analytical Mothod(s): SMP Buffer pH Mehlich 3 Loss On Ignition Water pH OM WN E_NR .Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Field ID Lab Number s� Rate Soil Class IbslA M3 ppm Rate ppm Rate ppm Rate K ppm Rate M 9 ppm Rate Ca ppm Rate Na ppm Rate Soil pH Buffer Index H meg1100g meq/100g R016-6 12930 1.5 L 74 329 VH NC=274 134 VH NC=69 87 H 546 M 6.0 0.7 4.5 MIN R016-8 12931 2.2 L 83 257 VH NC=214 56 L NC=29 84 L 1321 VH 7.2 0.0 7.4 MIN Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron soluble Salts Sample Fed ID ID K % Mg % Ca % No % H % NO3 N ppm Rate S ppm Rate Zn ppm Rate Mn ppm Rate Fe ppm Rate Cu ppm Rate B ppm Rate SS ms/cm Rate R016-6 7.6 16.1 60.7 15.6 R016-8 779.3 89.3 0.0 Values an this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm(parts per million), Ibs/A This repart applies to sample(s) tested. Samples are retained soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. H (High), VH (Very High). ENR- Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2= Ibs/A, Soluble Analysts prepared by WeypolntAnalyucai Virginia, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. by Paw« IV G*wr Patric McGroary Page 5 of 5 Report Number: 17-020-0622 Account Number:46525 Send To: Synagro Central LLC/ Lumberton Mary Brewer 284 Boger Road Mocksville NC 27028 Date Received:01/20/2017 Date Of Report: 01/23/2017 t , Waypoint ANALYTICAL "Every acre... Every year. "n Farm ID:R016 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Grower: Ozzeu Buker/ Lumberton SOIL FERTILITY RECOMMENDATIONS Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron ple ID FFia, Intended Crop veld Goal Lime N Pz05 K20 Mg S Zn M, Fe Cu B d ID TonslA IbIA MIA Ib/A Ib/A IbIA Ib/A Ib/A Ib/A Ib/A IbIA R016-6 Adjust pH to 6.0 0 0.0 0 R016-6 Bermuda, Coastal 5 0.0 75 0 210 0 R016-8 Adjust pH to 6.0 0 0.0 0 R016-8 Bermuda, Coastal 5 0.0 75 0 432 0 Comments: Sample(s) : R016-B Crop: Bermuda, Coastal Apply additional 65 pounds of nitrogen after every cutting and harvest of hay. The recommended potash is the total pounds/acre needed to achieve the specified yield goal. Apply 112 or 1/3 (100-150 pounds) of the total at the first application in spring or fall. Application of the remaining should be determined by the yield achieved after the first cutting and the moisture condition. If in drought condition and yield is low the following applications should be reduced or eliminated. Use ammonium sulfate as all or portion of the N requirement to reduce pH. Use K-Mag as part of the potassium source to increase magnesium level "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ 5� and may not be reproduced In whole or part, nor may any reference be made to the pow'. Pc 60w work,the results, or the company in any advertising, news release, or other public anouncements without obteining our prior written authorization. Copy right 1977. Pauric McGroary Page 1 of 3 ' - Report Number: 17-020-0621 Account Number; 46525 Send To: Synagro Central LLC/ Lumberton Mary Brewer 284 Boger Road Mocksville NC 27028 Waypoint. ANALYTICAL "Every acre... Everyyear. "ry Farm ID: R016 SOIL ANALYSIS REPORT Date Received: 01/2012017 Date Of Analysis: 01/23/2017 Date Of Report: 01/23/2017 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical.com Grower: Campen Farms/ Lumberton Analytical Molhod(s): SMP Buffer pH Mehllch 3 Loss On Ignition Water pH OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Field ID Lab Number % Rate Soil Class )ba/A M3 ppm Rate ppm Rate ppm Rate K ppm Rate M 9 ppm Rate Ca ppm Rate Na ppm Rate Soil PH Buffer Index H meg11009 meg1100g RO 16-16 12920 3.8 M 116 431 VH NC=359 65 L NC=33 67 L 946 M 5.7 6.78 1.5 7.0 MIN RO 16-17 12921 2.6 L 92 247 VH NC=206 21 VL NC=11 152 H 845 H 6.5 0.4 5.9 MIN PRO 12M 2.4 L 91 232 VH 17 VL NC=9 SS H 675 11 6.2 0.6 4.8 MINNC=193 12923 1.1 L 69 144 VH NC=120 24 VL NC=12 25 L 284 M 5.6 6.88 D.5 2.2 MIN Percent Base Saturatlon Nitrate Sulfur Zinc Manganese Iron Copper Boron soluble Salts Sample Field ID ID K % Mg % Ca % Na % H % N%N ppm Rate S ppm Rate Zn ppm Rate Mn pp m Rate Fe ppm Rate Cu ppm Rate B ppm Rate IS ms/cm Rate RO 16-16 2.4 8.0 67.6 21.4 RO 16-17 0.9 21.5 71.6 6.8 R016-18 0.9 15.3 70.3 12.5 R016-19 2.8 9.5 64.5 22.7 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per mlllion), Ibs/A This report applies to sample(s) tested. Samples are retained soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (mllll-mhos per centimeter), meq/100g maximum of thirty days after testing. b ?,W,. mr Gar H (High), VH (Very High). ENR - Estimated Nitrogen Release. (mllli-equivalent per 100 grems). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by. WaypointAnalytlral Virginia, Inc. Y C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary Page 2 of 3 Report Number: 17-020-0621 Account Number:46525 Send To: Synagro Central LLC/ Lumberton Mary Brewer 284 Boger Road Mocksville NC 27028 Date Received:01120/2017 Date Of Report: 01/2312017 Waypoint,. ANALYTICAL "Every acre... Everyyear."> Farm ID: R016 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Grower: Campen Farms/ Lumberton SOIL FERTILITY RECOMMENDATIONS Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Goa Yield l Lime N P205 K20 Mg S Zn Mn Fe Cu B Field ID TonslA Ib/A Ib/A Ib/A Ib/A Ib/A IblA Ib/A IblA Ib1A Ib/A RO 16-16 Adjust pH to 6.0 0 0.8 13 RO 16-16 Bermuda, Coastal 5 0.8 75 0 406 13 RO 16-17 Bermuda, Coastal 5 0.0 75 0 496 0 RO 16-17 Adjust pH to 6.0 0 0.0 0 RO 16-18 Bermuda, Coastal 5 0.0 75 0 495 0 RO 16-18 Adjust pH to 6.0 0 0.0 0 RO 16-19 Adjust pH to 6.0 0 0.6 55 RO 16-19 Bermuda, Coastal 5 0.8 75 0 447 55 Comments: "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced In whole or part, nor may any reference be made to the ppylia m� GIN work,the results, or the company In any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copyright 1977. Pauric McGroary Page 3 of 3 Report Number: 17-020-0621 Account Number:46525 Send To: Synagro Central LLC/ Lumberton Mary Brewer 284 Boger Road Mocksville NC 27028 Waypoint. ANALYTICAL Sample(s) : RO 16.19 Crop: Adjust pH to 6.0 Apply dolomitic lime to raise pH and improve the magnesium level. Every acre... Every year: "r Farm ID: R016 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical.com Grower: Campen Farms/ Lumberton If dolomitic lime is not used, apply required magnesium with magnesium oxide. Epsom Salts, K-Mag or Sul-PO-Mag. Sample(s) : RO 16-17,RO 16-18,RO 16-19 Crop: Bermuda, Coastal Apply additional 65 pounds of nitrogen after every cutting and harvest of hay. The recommended potash is the total pounds/acre needed to achieve the specified yield goal. Apply 112 or 1/3 (100-150 pounds) of the total at the first application in spring or fall. Application of the remaining should be determined by the yield achieved after the first cutting and the moisture condition. If in drought condition and yield Is low the following applications should be reduced or eliminated. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the Prf« IV G� wodc,the results, or the company In any advertising, news release, or other public anouncements without obtaining our pdor written authorization. Copy right 1977. 1 Paudc McGroary N 1 6111111111111 NCDA&CS i s=,.,,,4>mic Division Phone: (919) 733-2666 Website: www.nLjZjov/agronomi/ Report No. FY1 - 04158 Client: Chad Hayes Advisor: Delois/Pete Allen Predictive 273 Pete Strickland Rd 688 Deep Branch Rd. =!' Soil Report Mehlich-3 Extraction Cerro Gordo, NC28430 Lumberton, NC 28360 Sampled County: Robeson Sampled: 08/31/2016 Received: 09/07/2016 Completed: 09/16/2016 Form: Links to Helpful Information Sample ID: R0172 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., E 2.5 60-80 50 100 25 0 0 0 0 0 Note: 12 2-Bermuda hay/past., M 0.0 180-220 40 190 $ 0 0 0 0 0 Note: 12Note: Test Results [units - WN in gled; CEC and Na in meq/100 cO; NO3-N in mg/drift Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 1.80 1.26 5.9 40 3.6 4.7 42 18 31 7 46 19 28 28 86 86 31 0.1 2 Sample ID: R0173 Recommendations: Lime Nutrients (lb/acre) More Crop (tonslacre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda-hay/past., E 2.0 60-80 70 100 25 0 $ 0 0 0 Note: 12 Note: 2 -Bermuda hay/past., M 0.0 180-220 60 190 $ 0 $ 0 0 0 Note: 12 Note: Test Results [units - WN in glcO; CEC and Na in meq/100 cO; NO3-N in mg/do]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-1 Zn-AI Cu-1 Na ESP SS -I NO3-N 2.60 1.25 7.7 57 3.3 5.1 34 21 51 5 35 14 25 25 50 50 34 0.1 1 North Carolina r, 4s T0lIDCc4 7rm: FunJ fmm�is+sioia Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Trox NCDA&CS I'i_...-_)mIC Division Phone: (919) 733.2655 Website: www.;v_ -- 4! ov/agronomi/ Report No. FYI. o_2 4158 Chad Hayes Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations ' For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at one Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange rapacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-1 potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1Mn-AI2 Mn-availability index for crop 2 Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mn-I M-0 manganese index mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit wwwncacr.uov/aoronomi/obnart4.hLm- fTind information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index Wtv weight per volume The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index remaining 16 [P-1, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routine) Zn-I zinc index available)] indicate levels of plant nutrients or other fertility measurement. Visit w✓.ncacr.aov/aaronomi/uvrst.htm Page 1 of 1 Report Number: 17-003-0511 Account Number:46849 Send To: Synagro Central LLC/ PWC Mary Brewer 284 Boger Road Mocksville NC 27028 Waypoint.. ANALYTICAL "Every acre ... Every year. ",a SOIL ANALYSIS REPORT Date Received: 01/03/2017 Date Of Analysis: 01/04/2017 Date Of Report: 01/04/2017 0 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical.com Grower: Ronald Hammond Analytical Method(s): SMP Buffer pH Mehlich 3 Loss On Ignition Water pH OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E,C Sample ID Lab Field ID Number s� Soil IbsIA M3 K M 9 Ca Na Soil Buffer H Rate Class ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate PH Index meg1100g meq/100g 12 03929 2.7 93 463 VH 58 L 115 M 952 M 5.5 6.73 2.0 7.9 MIN R020 M NC=386 NC=30 -Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Sample ID Fed ID K Mg Ca Na H NO3 N S Zn Mn Fe Cu B SS % %% % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate 12 1.9 12.1 60.3 25.3 R020 Values on this report represent the plant available nutrients In the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. samples are retained sell. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days otter testing. H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli-equlvalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by: Pow' IV Goa-r C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by: Waypolnt Analytical Virginia, Ina Paudc McGroary Date Received: 01/03/2017 Date Of Report: 01/04/2017 SOIL FERTILITY RECOMMENDATIONS Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Llm0 N P205 K20 Mg S Zn Mn Fe Cu B Field ID Tons Tons1A Ib/A IbIA IbIA Ih/A MIA IbIA IbIA IbIA IbIA IbIA 12 Bermuda, Coastal 5 1.5 75 0 434 0 R020 Comments: 'The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or Implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced In whole or part, nor may any reference be made to the work,the results, or the company In any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. r NCDA&CS lY;.-.::rjmic Division Phone: (919) 733.2655 Website: www.na g:.,Uov/agronomi/ Report No. FY17- 14804 1feu i Predictive Soil Report Mehlich-3 Extraction Client: Chad Hayes 273 Pete Strickland Rd Cerro Gordo, NC 28430 Advisor: Lacy Cummins 75 Gene Rd. Pembroke, NC 28372 9. Nk'en.L1 �. Sampled County: Robeson Sampled: 11/09/2016 Received: 11/14/2016 Completed: 12107/2016 Farm: RO-21 Links to Helpful Information Sample ID: 21-2A Recommendations: Lime Nutrients (Ib/acre) More Crop (tonslacre) N P2Oe K2O Mg S Mn Zn Cu B Information Lime History: 1 -Small Grain (SG) 1.8 80-100 0 90 25 0 0 0 0 0 Note: 3 2 Test Results [units - W/V in g/cnr ; CEC and Na in meg1100 aril; NO3-N in mg/do]: Soil Class: Mineral . HM% WIV CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-1 Zn-AI Cu-I Na ESP SS-1 NO3-N 0.60 1.32 4.9 45 2.7 4.8 629 25 37 5 82 116 80 347 347 399 0.1 2 Sample ID: 21-2B Recommendations: Lime Nutrients (lb/acre) More Crop (tonslacre) N P2O6 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Small Grain (SG) 0.6 80-100 0 120 0 0 0 0 0 0 Note: 3 2- Test Results [units -WIV in g/cnr ; CEC and Na in meq/100 cO; NO3-N in mg/dO]: Soil Class: Mineral HM% WIV CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.56 1.27 6.3 72 1.8 5.7 380 12 59 12 45 114 78 769 769 684 0.1 2 Sample ID: 21-01 Recommendations: Lime Nutrients (lb/acre) More Crop (tonslacre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Small Grain (SG) 1.3 80-100 0 60 25 0 0 0 0 0 Note: 3 2- Test Results [units - WIV in glcO; CEC and Na in meq/100 cm3; NO3-N in mg/drift Soil Class: Mineral HM% WIV CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-Al Cu-I Na ESP SS-1 NO3-N 0.97 1.30 5.7 60 2.3 5.2 540 39 50 6 69 155 103 453 453 360 0.1 2 !~forth Carolina .+WI + 7ohxco Iraet Pima Crnnens.0m Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Trox NCDA&CS k._ ..omic Division Phone: (919) 733.2655 Website: www.ncW.govlagronomil Report No. FY1 F14804 Chad Hayes Page 2 of 3 Sample ID: 21-03 Recommendations: Lime Nutrients (Ib/acre) More Crop (tons/acre) N P2O6 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Small Grain (SG) 1.0 80-100 0 110 0 0 0 0 0 0 Note: 3 2- Test Results [units - WN in g/cO; CEC and Na in meg1100 cm1; NO3-N in mg/da]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-1 Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.66 1.22 8.1 62 3.0 5.7 367 14 51 11 60 127 86 921 921 763 0.1 1 Sample ID: 21-05 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Small Grain (SG) 2.0 80-100 0 70 25 0 0 0 0 0 Note: 3 2- Test Results [units - WN in g1crrr3; CEC and Na in meg1100 curl; NO3-N in mg/dop Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.60 1.30 6.3 52 3.0 4.8 565 33 43 6 81 136 92 578 578 450 0.1 1 3 NCDA&CS A_._ ,-)mic Division Phone: (919) 733.2655 Website: www.nc .goviagronomi/ Report No. FY1 '_: K,4604 Chad Hayes Page 3 of 3 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 tonlacre (50 Ib/1000 sq ft) at one Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. cu-1 copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-1 potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1 Mn-AI2 Mn-availability index for crop 2 Mn-1 manganese index Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z M-o mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.ht nYtsf nd information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P205 phosphate 8-1 sulfur index Test Results SS-1 soluble salt index Wtv weight per volume The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routine) Zn-I zinc index available)] indicate levels of plant nutrients or other fertility measurement. Visit w w ncagr.gov/aaronomi/uvrsfhtm MEMO NCDA&CS A?,-:= bomic Division Phone: (919) 733.2655 Website: www.nclr.goviagronomil Report No. FYT,�;J41 ram". Client: Chad Hayes Advisor: Carnell Locklear Predictive 273 Pete Strickland Rd 3009 Daniel McLeod Rd. Cerro Gordo, NC 28430 Red Springs, NC 28377 Soil Report It k+ Mehlich-3 Extraction F Sampled County: Robeson Sampled: 08/30/2016 Recelved: 09/07/2016 completed: 09119/2016 Farm: Links to Helpful Information Crop (tons/acre) N P2O6 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 0.3 120 -160 0 0 0 0 0 0 0 0 Note: 3 2- Test Results [units - WN in g/crrP; CEC and Na in meg1100 crrP; NOa-N in mg/dol: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-AI2 Zn-1 Zn-AI Cu-1 Na ESP SS-1 NOa-N 1.25 1.29 9.8 80 2.0 5.9 258 101 60 15 43 116 87 493 493 275 0.1 1 North Carolina Tnlnan Truu Fund Comnitsion Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Trox NCDA&CS / , Jomic Division Phone: (919) 733-2655 Website: www.ri,.-._.{t9ov/agronomil Report No. FY1..,_594155 Chad Hayes Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units I Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 tonlacre (50 Ib/1000 sq ft) at time, even if the report recommends more. You can apply the rest in similar increments every six months until the full r is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit ncagr.gov/agronomi/pubs.htm. Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find the exact fertilizer grade recommended on the report, visit wwv^.ncanr.00v/anronomi/obpart4.htmthfsf;nd information that may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizes Test Results The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The remaining 16 IN, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-1, Zn-AI, Cu-1, S-I, SS-1, Na, ESP, SS -I, NO3-N (not rou available)] indicate levels of plant nutrients or other fertility measurement. Visit wwwncacrcov/aoronomi/uvrst Report Abbreviations Ac exchangeable acidity B boron BS% % CEC occupied by basic cations ca% % CEC occupied by calcium CEC cation exchange capacity Cu-1 copper index ESP exchangeable sodium percent HM% percent humic matter K-1 potassium index K20 potash Mg% % CEC occupied by magnesium MIN mineral soil class Mn manganese Mn-All Mn-availability index for crop 1 Mn-AI2 Mn-availability index for crop 2 Mn-I manganese index M-0 mineral -organic soil class N nitrogen Na sodium NO3-N nitrate nitrogen ORG organic soil class pH current soil pH P-1 phosphorus index P206 phosphate S-1 sulfur index SS-1 soluble salt index WN weight per volume Zn-AI zinc availability index Zn-I zinc index