Loading...
HomeMy WebLinkAboutWQ0006101_2016 Annual Report_20170217RECEIVED DEQ/DWR MAR 0 S 2017 FAYETTEVILLE RREGIONAL OFFICE RECElVFp MNir 0 2 2017 Information Processing Unit " R Sec,ion CITY OF DUNN, NC RESIDUALS LAND APPLICATION PROGRAM Permit No. WQ0006101 2016 ANNUAL REPORT r. ' City of Dunn, NC Residuals Land Application Program 2016 Annual Report TABLE OF CONTENTS 1. Certification Form and Annual Operations Summary 2. Annual Residual Sampling Summary Forms, Residuals Analyses, & SAR Calculation Pages 3. Annual Land Application Field Summary Forms 4. TCLP Analyses 5. Pathogen Reduction/Vector Attraction Reduction 6. Soil pH & Lime Application Records 7. Soil Analyses 10 ANNUAL LAND APPLICATION CERTIFICATION FORM WQPermit#: W00006101 County Harnett Year2016 Facility Name (as shown on permit) Dunn W WTP & City of Dunn WTP NPDES No. NC0043176, 03-43-010 Land Application Operator Synagro Phone# (336) 998-7150 Land application of residuals as allowed by the above permit occurred during the past calendar year? X YES NO. IfNO, slip Part A, and PartB and proceed to Part C. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A —Residuals Application Summary: Total. number of application fields in the permit: 39 Total number of fields utilized for land application during the year: 8 Total amount of dry tons applied during the year for all application sites: 379.51 Total number of acres utilized for land application during the year. 161.3 Part B — Annual Compliance Statement: Facility was compliant during calendar year 2016with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water QualityX YES NO. If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were,applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading Rates in 15A NCAC 02T .I105(b) (Applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 i regulated facilities). 8. All monitoring and reporting requirements in 15ANCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit. 12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13. All buffer requirements as specified on the permit were maintained during each application of residuals. Part C — Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belied true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." If Ronald Autry, City Manager A. &—A / Permittee Name and Title (type or print) r rm '-- ate u WEB 07 ,200 Signature of Preparer* Date gnatureofLandApplier Date (if different from Permittee) (if different from Pemrittee and Preparer) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) 2016 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION ,r\DUNN, NC DUNN, NC WWTP AEROBICALLY DIGESTED LIQUID MONTH/YEAR AMOUNT UNIT April 2016 446,400.00 G September 2016 539,400.00 G November 2016 483,600.00 G YEARLY TOTAL 1,469,400.00 G DUNN, NC WTP LIQUID MONTH/YEAR AMOUNT UNIT March 2016 688,200.00 G November 2016 961,000.00 G YEARLY TOTAL 1,649,200.00 G DRY METRIC DRY TONS UNIT TONS 41.32 D 37.48 49.95 D 45.30 44.77 D 40.60 136.04 D 123.38 DRY TONS UNIT 101.60 D 141.87 D 243.47 - D DRY METRIC TONS 92.14 128.66 220.80 2/3/2017 I ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: W00006101 Facility Name: DUNN, NC NPDES# : NCO043176 or WQ# (residual -only) WWTP Name: DUNN WWTP Residuals Analysis Data Product Type AEDLIQ AEDLIQ Date Sampled (grab) or 01/12/16 02/29/16 Date Composited Percent Solids 2.22 2.22 PARAMETERS (mg/kg dry weight) Arsenic 10 8 Cadmium 2 <2 Mercury 1.1 1.4 Chromium 31 34 Copper 352 306 Lead 48 44 Molybdenum 9 8 Nickel 22 24 Selenium <5 <5 Zinc - 629 604 Total Phosphorus 23700 21200 TKN 55000 57700 Ammonia -Nitrogen 4050 9910 Nitrate and Nitrite 12400 1360 Laboratory WAYPOINT ANALYTICAL Waypoint Analytical Virginia Inc. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Dated DENR FORM RSSF (5/2003) Printed: Friday- February 3. 2017 at 09:47:03 for: 2188 01 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0006101 Facility Name: DUNN, NC NPDES# : NCO043176 or WQ# (residual only) WWTP Name: DUNN WWTP Residuals Analysis Data Product Type AEDLIQ AEDLIQ Date Sampled (grab) or 01/12/16 02/29/16 Date Composited Percent Solids 2.22 2.22 PARAMETERS (mg/kg dry weight) Aluminum 20600 22400 Calcium 10900 10900 Magnesium 3390 3200 pH 3.50 3.62 Potassium 4730 4720 Sodium 2100 17.90 Laboratory WAYPO I NT ANALYTICAL Waypoint Analytical Virginia Inc. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Date -2--4 { /2 NR - Data Not Reported or Data Not Required DENR FORM RSSF-B (7/2002) _ Printed: Friday - February 3, 2017 at 09:47:37 for: 2188 01 Page: 1 of 2 Report Number: 16-015-0209 Account Number: 46789 Submitted By: CREIGHTON BROWN Send To: SYNAGRO CENTRAL LLC/DUNN MARY BREWER 284 BOGER RD MOCKSVILLE, NC 27028 Lab Number: 66282 Sample Id: DUNN WWTP Waypoint- 0 ANALYTICAL Project: DUNN WWTP NC CERT#257 REPORT OFANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 1/12/2016 13:30:00 Date Received: 01/15/2016 00:00 Date Reported: 01/20/2016 Total Solids • 2.22 22200 100.0 JM 01/15/201615:00 SM-2540G Moisture' 97.78 100.0 JM 01/151201615:00 SM-2540G Total Kjeldahl Nitrogen 5.50 55000 10.0 JM 01/18/2016 08:30 SM-4500-NH30-TKN Total Phosphorus 2.37 23700 100 KM 01/18/2016 14:22 SW 6010C Total Potassium 0.47 4730 100 KM 01/18/2016 14:22 SW 6010C Total Sulfur 1.15 11500 100 KM 01/18/2016 14:22 SW 601OC Total Calcium 1.09 10900 100 KM 01/18/2016 14:22 SW 6010C Total Magnesium 0.34 3390 100 KM 01/18/2016 14:22 SW 6010C Total Sodium 0.21 2100 .100 KM 01/18/2016 14:22 SW 6010C Total Iron 29500 100 KM 01/18/2016 14:22 SW 6010C Total Aluminum 20600 100 KM 01/18/2016 14:22 SW 6010C Total Manganese 345 5 KM 01/18/2016 14:22 SW 6010C Total Copper 352 5 KM 01/1812016 14:22 SW 6010C Total Zinc 629 5 KM 011161201614:22 SW 6010C Ammonia Nitrogen 0.41 4050 10.0 JM 01/18/2016 08:30 SM4500-NH3C Organic N 5.09 50950 10.0 01/18/2016 08:30 CALCULATION Nitrate+Nitrite-N 11100 2.00 JM 01/18/2016 08:30 SM-450ONO3F Total Cadmium 2.0 2.0 KM 01/18/2016 14:22 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Ourmports and letters are for the exclusive and confidential use o/ourclients, and may not be reproduced In whole or part, normay anyreference be made to the work, the results, or the company In any advertising, news release, or otherpubllc announcements without obtaining ourpdor written authorimtlon. Debbie Holt Page: 2 of 2 Report Number: .16-015-0209 Account Number: 46789 Submitted By: CREIGHTON BROWN Send To: SYNAGRO CENTRAL LLC/DUNN MARY BREWER 284 BOGER RD MOCKSVILLE , NC 27028 Lab Number: 66282 Sample Id: DUNN WWTP Waypointn ANALYTICAL Project: DUNN W WTP NC CERT#257 REPORT OFANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 1/12/2016 13:30:00 Date Received: 01/15/2016 00:00 Date Reported: 01/20/2016 Total Chromium 31 5 KM 01/18/2016 14:22 SW 6010C Total Nickel 22 5 KM 01/18/2016 14:22 SW 6010C Total Lead 48 5 KM 01/18/2016 14:22 SW 6010C Total Arsenic 10.0 3.0 KM 01/18/2016 14:22 SW 6010C Total Mercury 1.1 0.4 KM 01/19/2016 09:00 SW-7471B Total Selenium <5.0 5.0 KM 01/18/2016 14:22 SW 6010C pH (Standard Units)" 3.50 2.00 JM 01/18/2016 08:30 SW-9045D Total Volatile Solids 70.00 700000 100.0 JM 01/16/2016 15:00 SM-254OG Total Molybdenum 9 5 KM 01/18/2016 14:22 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al", "Fe", "P", AND "Se". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and falters are for the exclusive and confidential use of our clients, and may not be mpmduced in whole orpart, nor may any reference be made to the work, the insults, or the company In any advertising, news release, or otherpublicannouncements without obtaining ourpriorwdilen outhodzatlon. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2188-01-AEDLIQ-NC DUNN, NC WWTP AEROBICALLY DIGESTED 1/1212016 I 1 - I 1 0.6688 LIQUID Na mg/I = (Na mg/kg x % Solids) + 100 = (2100 x 2.2200) + 100 = 46.62 Ca mgll = (Ca mg/kg x % Solids) + 100 = (10900 x 2.2200) + 100 = 241.9B Mg mgA = (mg mg/kg x % Solids) + 100 = (3390 x 2.2200) + 100 = 75.258 Na meq = Na mg/I + Molec.Wgt.Na = 46.62 + 23 = 2.02696 Ca meq = Ca mg/I + Molec.Wgt.Ca = 241.98 + 20 = 12.099 Mg meq = Mg mgA + Molec. Wgt.Mg= 75.258 + 12 = 6.2715 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 2.02696 + SgrRoot[0.5(12.099+6.2715)] = 0.668804 Printed: 2/3/2017 Page 1 11:03 Page: 1 of 2 Report Number: 16-062-0209 Account Number: 46789 Submitted By: CREIGHTON BROWN Send To: SYNAGRO CENTRAL LLC/DUNN MARY BREWER 284 BOGER RD MOCKSVILLE , NC 27028 Lab Number: 55373 Sample Id: DUNN WWTP Waypoint- 0 ANALYTICAL Project: DUNN WWTP NC CERT#257 REPORT OFANALYSIS 7621 Whitepine Road, Richmond, VA 23237 _ Main 864-743-9401 a Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 2/29/2016 16:30:00 Date Received: 03/02/2016 00:00 Date Reported: 03108/2016 Total Solids 2.22 22200 -100.0 JM 03/02/2016 15:00 SM-254OG Moisture. 97.78 100.0 JM 03/021201615:00 SM-2540G Total Kjeldahl Nitrogen 5.77 57700 10.0 JM 03/03/2016 08:44 SM-4500-NH3C-TKN Total Phosphorus 2.12 21200 100 KM 03/03/2016 11:53 SW 6010C Total Potassium 0.47 4720 100 KM 03/03/2016 11:53 SW 6010C Total Sulfur 1.06 10600 100 KM 03/03/2016 11:53 SW 6010C Total Calcium 1.09 10900 100 KM 03/03/2016 11:53 SW 6010C Total Magnesium 0.32 3200 100 KM 03/03/2016 11:53 SW 6010C Total Sodium 0.18 1790 100 KM 03/03/2016 11:53 SW 6010C Total Iron 26600 100 KM 03/03/2016 11:53 SW 6010C Total Aluminum 22400 100 KM 03/03/2016 11:53 SW 6010C Total Manganese 314 5 KM 03/03/2016 11:53 SW 6010C Total Copper 306 5 KM 03/03/2016 11:53 SW 6010C Total Zinc 604 5 KM 03/03/2016 11:53 SW 6010C Ammonia Nitrogen 0.99 9910 10.0 JM 03/03/2016 08:44 SM4500-NH3C Organic N 4.78 47790 10.0 03/03/2016 08:44 CALCULATION Nitrate+Nitrite-N 1360 2.00 JM 03/03/2016 08:45 SM-450ONO3F Total Cadmium <2.0 2.0 KM 03/03/2016 11:53 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are forthe exclusive and confidential use of ourclients, and may notbe reproduced in whole orpart normay any reference be made 4waa�dl to the work, the results, or the company in any advertising, news release, orother public announcements without obtaining ourpdorwdtten authorization. Debbie Holt Page: 2 of 2 Report Number: 16-062-0209 Account Number: 46789 Submitted By: CREIGHTON BROWN Send To: SYNAGRO CENTRAL LLC/DUNN MARY BREWER 284 BOGER RD MOCKSVILLE, NC 27028 Lab Number: 55373 Sample Id: DUNN WWTP Waypoint0 . ANALYTICAL Project: DUNN WWTP NC CERT#257 REPORT OFANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 2/29/2016 16:30:00 Date Received: 03/02/2016 00:00 Date Reported: 03108/2016 Total Chromium 34 5 KM 03/03/2016 11:53 SW 6010C Total Nickel 24 5 KM 03/03/2016 11:53 SW 6010C Total Lead 44 5 KM 03/03/2016 11:53 SW 6010C Total Arsenic 8.0 3.0 KM 03/03/2016 11:53 SW 6010C Total Mercury 1.4 0.4 KM 03/03/2016 09:00 SW-7471B Total Selenium <5.0 5.0 KM 03/03/2016 11:53 SW 6010C pH (Standard Units) • 3.62 _ 2.00 JM 03/03/201608:44 SW-9045D Total Volatile Solids 70.45 704500 100.0 JM 03/02/2016 15:00 SM-2540G Total Molybdenum 8 5 KM 03/03/2016 11:53 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MSD WAS OUT OF LIMITS FOR "Al", "Cr", "Fe", "P", AND "Se". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are forme exclusive and confidential use or our clients, and may not be reproduced In whole or part, nor may any reference be made to the work, the results, or the company In any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2188-01-AEDLIQ-NC DUNN, NC W WTP AEROBICALLY DIGESTED 2/29/2016 11112016-1213112016 0.5756 LIQUID Na mgA = (Na mg/kg x % Solids) + 100 = (1790 x 2.2200) + 100 = 39.738 Ca mgA = (Ca mg/kg x % Solids) + 100 = (10900 x 2.2200) + 100 = 241.98 Mg mgA = (mg mg/kg x % Solids) + 100 = (3200 x 2.2200) + 100 = 71.04 Na meq = Na mg/I + Molec.Wgt.Na = 39.738 + 23 = 1.72774 Ca meq = Ca mg/I + Molec.Wgt.Ca= 241.98 + 20 = 12.099 Mg meq = Mg mgA + Molec.Wgt.Mg = 71.04 + 12 = 5.92 SAR = Na meq +SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.72774+ SgrRoot[0.5(12.099+5.92)] = 0.575609 Printed: 2/3/2017 Page 1 11:04 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0006101 Facility Name: DUNN, NC NPDES#:. or WQ# (residual only). WWTP Name: DUNN WTP Residuals Analysis Data Product Type WPL Date Sampled (grab) or 01/12/16 Date Composited Percent Solids 3.54 PARAMETERS (mg/kg dry weight) Arsenic 9 Cadmium <2 Mercury <0.4 Chromium 41 Copper 38 Lead 13 Molybdenum <5 Nickel 19 Selenium <5 Zinc 78 Total Phosphorus 1740 TKN 5930 Ammonia -Nitrogen 847 Nitrate and Nitrite <2 Laboratory WAYPOINT ANALYTICAL "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Date o2 /a / i� DENR FORM RSSF (5/2003) Printed: Friday- February 3. 2017 at 09:47:13 for: 2188 02 r" J ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0006101 Facility Name: DUNN, NC NPDES#: or WQ# (residual only) WWTP Name: DUNN WTP Residuals Analysis Data Product Type wet. Date Sampled (grab) or 01/12/16 Date Composited Percent Solids 3.54 PARAMETERS (mg/kg dry weight) Aluminum 116000 Calcium 1010 Magnesium 1590 pH 5.89 Potassium 924 Sodium 631 Laboratory WAYPOINT ANALYTICAL "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Date NR - Data Not Reported or Data Not Required DENR FORM RSSF-B (7/2002) Printed: Friday- February 3, 2017 at 09:47:44 for: 2188 02 Page: 1 of 2 Report Number: 16-015-0208 Account Number: 46789 Submitted By: CREIGHTON BROWN Waypoint,. ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743.9401 a Fax 804-271-6446 www.waypointanalytical.com Send To: SYNAGRO CENTRAL LLC/DUNN Project: DUNN WTP MARY BREWER NC CERT#257 284 BOGER RD MOCKSVILLE, NC 27028 ' REPORT OFANALYSIS Date Sampled: 1/12/2016 14:15:00 Lab Number: 66281 - Date Received: 01/15/2016 00:00 Sample Id: DUNN WTP Date Reported: 01120/2016 RESULT RESULT QUANTITATION LIMIT ANALYSIS PARAMETER ANALYST �,TEITIME •D Total Solids 3.54 35400 100.0 JM 01/15/201615:00 SM-254OG Moisture' 96.46 100.0 JM 01/15/201615:00 SM-254OG Total Kjeldahl Nitrogen 0.59 5930 10.0 JM 01/18/2016 08:30 SM-4500-NH3C-TKN Total Phosphorus 0.17 1740 100 KM 01/18/2016 14:22 SW 601OC Total Potassium 0.09 924 100 KM 01/18/2016 14:22 SW 6010C Total Sulfur 1.01 10100 100 KM 01118/201614:22 SW 6010C Total Calcium 0.10 1010 100 KM 01/18/2016 14:22 SW 601OC Total Magnesium 0.16 1590 100 KM 01/18/2016 14:22 SW 6010C Total Sodium 0.06 631 100 KM 01/18/2016 14:22 SW 6010C Total Iron 33100 100 KM 01/18/2016 14:22 SW 601OC Total Aluminum 116000 100 KM 01/18/2016 14:22 SW 6010C Total Manganese 915 5 KM 01/18/2016 14:22 - SW 601OC Total Copper 38 5 KM 01/18/2016 14:22 SW 6010C Total Zinc 78 5 KM 01/18/2016 14:22 SW 6010C Ammonia Nitrogen 0.08 847 10.0 JM 01118/2016 08:30 SM-4500-NI3C Organic N 0.51 5083 10.0 01/18/2016 08:30 CALCULATION Nitrate+Nitrite-N <2.00 2.00 JM 01/18/2016 08:30 SM-450ONO3F Total Cadmium <2.0 2.0 KM 01/18/2016 14:22 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidenfial use of our clients, and may not be reproduced In whole orpart, nor may any reference be made_ to the work, the results, or the company in any advertising,news release, or therpublic announcements without obtaining ourprior written authorization. Debbie Holt t� Page: 2 of 2 Report Number: 16-015-0208 Account Number: 46789 Submitted By: CREIGHTON BROWN Send To: SYNAGRO CENTRAL LLC/DUNN MARY BREWER 284 BOGER RD MOCKSVILLE, NC 27028 Lab Number: 66281 Sample Id : DUNN WTP Waypoint. ANALYTICAL Project: DUNN WTP NC CERT#257 REPORT OFANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointa na lytica Isom Date Sampled: 1/12/2016 14:15:00 Date Received: 01/15/2016 00:00 Date Reported: 01/20/2016 Total Chromium 41 5 KM 01/18/2016 14:22 SW 6010C Total Nickel 19 5 KM 01/18/2016 14:22 SW 601OC Total Lead 13 5 KM 01/18/201614:22 SW 6010C Total Arsenic 9.0 3.0 KM 01/18/2016 14:22 SW 6010C Total Mercury <0.4 0.4 KM 01/19/2016 09:00 SW-7471B Total Selenium <5.0 5.0 KM 01/18/2016 14:22 SW 6010C pH (Standard Units)5.89 2.00 JM 01/18/2016 08:30 SW-9045D Total Volatile Solids 29.18 291800 100.0 JM 01/15/2016 15:00 SM-2540G Total Molybdenum <5 5 KM 01/18/2016 14:22 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al", "Fe", "P", AND "Se". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Ourrepods and letters are forthe exclusive and confidential use of ourclients, and may not be reproduced in whole orpatt, normay any reference be made to the work, the results, or the company In enyadvedising, news release, orother public announcements without obtelning ourpdorwdtten authodzabon. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2188-02-WPL-NC DUNN, NC WTP LIQUID 1/1212016 1N/2016-12131/2016 0.5396 Na mgA = (Na mg/kg x % Solids) + 100 = (631 x 3.5400)'+ 100 = 22.3374 Ca mgA = (Ca mg/kg x % Solids) + 100 = (1010 x 3.5400) + 100 = 35.754 Mg mgA = (mg mg/kg x % Solids) + 100 = (1590 x 3.5400) + 100 = 66.286 Na meq = Na mgA + Molec.Wgt.Na = 22.3374 + 23 = 0.971191 Ca meq = Ca mg/l + Molec. Wgt.Ca = 35.754 + 20 = 1.7877 Mg meq = Mg mgA + Molec.Wgt.Mg = 56.286 + 12 = 4.6905 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 0.971191 + SgrRoot[0.5(1.7877+4.6905)] = 0.539626 I� Printed: 2/3/2017 Page 1 11:06 ANNUAL LAND APPLICATION FIELD SUMMARY FORM ACILITYNAME: DUNN, NC PREDOMINANT SOIL SERIES: GOLDSBORO $WNER: HAROLD EDRIDGE PERMIT #: W00006101 ANNUAL DRY TONS APPLIED: 10.33 ITE #: NC CU 00034 FIELD# : CU 00034 0001 OPERATOR: HAROLD ELDRIDGE CATION EXCHANGE CAPACITY (NON-503): IESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 5.20 ACRES PERMITTED: 5.20 Page: 1 Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) aka Dry, Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- capon Method Vola- 6ti- zation Miner - all- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm ) Crop p MONTH Total per Acre Solids 9/14/16 43,400.00 (G) 8346.154 2.22 0.773 DUAEDL DRY 0-Q/2" SUR 0.5 0.30 57,700.p 9,910.00 p 1,360.00P 20652 FESCUE 9/15/16 55,800.00 - (G) 10730.769 2.22 0.993 DUAEDL DRY 0- 1/2" SUR 0.5 0.30 57,700. p 9,910.00 p 1,360.00 p 20652 FESCUE 9/16/16 12,400.00 (G) 2384.615 2.22 0.221 DUAEDL DRY 0- 1/2" SUR 0.5 0.30 57,700.p 9,910.00 p 1,360.00P 20652 FESCUE Sep-16 111,600.00 (G) 21,461.538 Total Gallons/Ac: 21,461.54 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 82 0.032 0.008 0.135 1.216 0.175 0.006 0.032 0.095 0.020 2.400 84.24 Jumulative Ibs/acre 0.189 0.059 1.430 8.164 0.983 0.050 0.294 0.701 0.155 14.242 f r .. ...- --'-• S' emit PAN Limit (lbs/acre) Ist Crop/2nd Crop ` st �^ �'^ x ( g :xvY� —=- � t `� '• ,' ` "t 'r " y�r i,r t'' w v Qr ,. 4 M���; h 'y 138 PD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 348 k hi (.�5, �,� 1339.0 267:9 15.0 � � 375.0 89.0 2500.0 � 45r" 7 P DUAEDL = DUNN, NC W WTP AEROBICALLY DIGESTED LIQUID x 1Ig , r Q-l11 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including thepossibility of fines and imprisonment for (mowing violations." N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppmormg/kg ** Volatilization Rate: Surface 0.5, Injectiondricorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 1 , ANNUAL LAND APPLICATION FIELD SUMMARY FORM ,ACR%TYNAME: DUNKNC PREDOMINANT SOIL SERIES: GOLDSBORO )WNER: HAROLD EDRIDGE PERMIT #: W00006101 ANNUAL DRY TONS APPLIED: 5.17 ME #: NC CU 00034 FIELD# : CU 00034 0002 OPERATOR: HAROLD ELDRIDGE CATION EXCHANGE CAPACITY (NON-503): 2ESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 5.70 ACRES PERMITTED: 5.70 Page: 1 Lime Applied'** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (W'1) (specify) /e Tons Cond. Precip. cation tili- all- Ammonia Nitrate PAN DATEor Per Residual Dry, Wet, Past 24 Method nation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 9/16/16 55,800.00 (G) 9789.474 2.22 0.906 DUAEDL DRY 0-Q/2" SUR 0.5 0.30 57,700.p 9,910.00 p 1,360.00 p 20652 FESCUE .Sep-16 55,800.00 (G) 9,789.474 Total Gallons/Ac: 9,789.47 As Cd Cr Cu Pb Hg Me Ni Se Zn P PAN TOTALS: Annual lbs/acre - 0.015 0.004 0.062 0.555 0.080 0.003 0.015 � 0.044 0.009 1.095 38.43 37 Cumulative Ibs/acre 0.127 0.044 0.990 6.514 0.719 0.041 0.226 0.521 0.112 11.092 �' t ?errnit PAN Limit (Ibs/acre) Ist Crop2nd Crop ` - i 1 rq yr,''' 7 ' "i' - @� 45' fivF g k�` ' ` �,,' :_' 138 V ... M�.lessK.�k<s le._c'r�k d mTjc_ FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 348 r,- r7 1339.0 267.9 15.0 O�e"'*'s 375.0 89.0 25000 ( '+ 3 DUAEDL = DUNN, NC W WTP AEROBICALLY DIGESTED LIQUID X l " A 00 , ey "2. (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properlygathered and evaluated the information submitted. I am aware that thereare significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 '1 1 } ANNUAL LAND APPLICATION FIEMI) SUMMARY FORM 'ACILITYNAME: DUNN,NC IWNER HAROLDEDRIDGE ITE #: NC CU 00034 FIELD# : CU.00034 0003 TSIDUAL SOURCE(S):* See list at bottom of report PREDOMINANT SOIL SERIES: GOLDSBORO PERMIT #: W00006101 ANNUAL DRY TONS APPLIED: 9.18 OPERATOR: HAROLD ELDRIDGE CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 4.90 ACRES PERMITTED: 4.90 Page: 1 Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Solids Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip, Past 24 Appli- cation Method Vola- till- motion Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN m (pp ) Cro p Total MONTH per Acre 9115116 74,400.00 (G) 15183.673 2,22 1.406 DUAEDL DRY 0-<1/1" SUR 0.5 0.30 57,700. p 9,910.00 p 1,360.00 p 20652 FESCUE 9/16/16 24,800.00 (G) 5061.224 2.22 0.469 DUAEDL DRY 0-<1/2" SUR 0.5 0.30 57,700.p 9,910.00 p 1,360.00p 1 20652 FESCUE Sep-16 99,200.00 (G) 20,244.897 Total Gallons/Ac: 20,24490 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 4nnual lbs/acre 77 0.030 0.007 0.127 1.147 0.165 0.005 0.030 0.090 0.019 2.264 79.46 ,umulative Ibs/aue 0.237 0.068 1.623 8.490 1.045 0.053 0.324 0.793 0.178 14.873 emit PAN Limit(bs/acre) 1st Cropand Crop �s -i1. r ' 138r M Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 F34 8 267.9 15.0 375.0 89.0 2500.0�'- .t:;5 x.3 ._...a- )UAEDL = DUNN, NC W WTP AEROBICALLY DIGESTED LIQUID (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A=Not Applicable NR-Not Reported or Not Required %=percent p=ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 ACR.ITYNAME: DUNN,NC WNER: HAROLD EDRIDGE TE #: NC CU 00034 FIELD# : CU 00034 0004 ESIDUAL SOURCE(S):• See list at bottom of report' ANNUAL LAND APPLICATION FII•:LD SUMMARY FORM PREDOMINANT SOIL SERIES: NORFOLK PERMIT #: W00006101 ANNUAL DRY TONS APPLIED: 10.91 OPERATOR: HAROLD ELDRIDGE CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 7.40 ACRES PERMITTED: 7.40 Page: 1 Lime Applied --- Date I Lbs/Ac )ATE or allons (G) or Cubic Ymds (CY) or Wet Tons (WT) (specify) % Solids Dry Tons Per Residual Site Cond. D We Dry, Inches Precip. Past 24 Appli. cation Method Vole- till- zaGon Miner - all- motion TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop Total MONTH Per Acre 9/16116 6,200.00 (G) 837.838 2.22 0:078 DUAEDL DRY 0-Q/2" SUR 0.5 0.30 57,700.p 9,910.00 p 1,360.00p 20652 FESCUE 9/17/16 ' 111,600.00 (G) 15081.081 2.22 1.396 DUAEDL DRY 0-Q/2" SUR 0.5 0.30 57,700.p 9,910.00 p 1,360.00p 20652 FESCUE Sep-16 117,800.00 (G) 15,918.919 lorai umionsi vc: 1�,YVWIL As Cd Cr Cu Pb Hg Me Ni Se Zn P PAN TOTALS: umual lbs/acre 61 0.024 0.006 0.100 0.902 0.130 0.004 0.024 0.071 0.015 1.780 62.48 :umulative lbstacre 0.216 0.063 1.395 7.848 0.976 0.048 0.286 0.719 0.161 13.766 omit PAN Limit (lbs/acre) lst Crop/2nd Crop r `r;,., 120 �... ..dk: �9 !L, k..��,. > �T�.a�,.1P� ,.a..:t,�k�,.Mi.__..�.a.sw :�� _:< 'D Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 348 i 1339.0 267.9 15.0 �i" `'a•�� 375.0 89.0 2500.0 t )UAEDL = DUNN, NC W WTP AEROBICALLY DIGESTED LIQUID X ou 11A, a- ► L�- �7 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for ]mowing violations." N/A=Not Applicable NR=Not Reported or Not Required %=percent p-ppm or mgAcg "• Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 " Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation •"* See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 'ACILITY NAME: DUNN, NC IWNER: HAROLD EDRIDGE HE #: NC CU 00034 FIELD# : CU 00034 0005 ;ESIDUAL SOURCE(S):• See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: GOLDSBORO PERMIT#: W00006101 ANNUAL DRY TONS APPLIED: 14.35 OPERATOR: HAROLD ELDRIDGE CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 7.50 ACRES PERMITTED: 7.50 Page: I Lime Applied "" Date Lbs/Ac DATEor allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) °� Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- till- nation Miner - all- za6on TIGV Ammonia Nitrogen Nitrate- and PAN (ppm) Crap MONTH Total per Acre Solids 9113116 86,800.00 (G) 11573.333 2.22 1.071 DUAEDL DRY - 0-<1/2" SUR 0.5 0.30 57,700. p 9,910.00 p 1,360.00 p 20652 FESCUE 9/14/16 68,200.00 (G) 9093.333 2.22 0.842 DUAEDL DRY 0-<1/2" SUR 0.5 0.30 57,700. p 9,910.00 p 1,360.00 p 20652 FESCUE Sep-16 155,000.00 (G) 20,666.666 "total (jallons/Ac: 2U,666.67 As Cd Cr Cu Pb Hg Mc, Ni Se Zn P PAN TOTALS: 4nnual lbs/acre - 79 0.031 0.008 0.130 1.171 0.168 0.005 0.031 0.092 0.019 2.311 81.12 lunulative lbs/acre 0.200 0.062 1.415 8.324 1.029 0.050 0.286 0.714 0.158 14.376 emit PAN Limit (Ibs/acre) 1st Crop2nd Crop `s a,� �" y=+ K ' �.._ } kiY �'. ' 138emit t.., w. rt'ir."yrl i 3 .:aF: ?D Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 1339.0 267.9 375.0 I5.0ON 89.0 )UAEDL = DUNN, NC W WTP AEROBICALLY DIGESTED LIQUID X- 2Ns-at.0 .0 ( — [ q^ C lOO 1 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 • Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *'"' See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 ACE.TI'Y NAME: DUNN, NC IWNER: HAROLD DIXON ITE #: NC HA 00008 FIELD# : HA 00008 0008 LESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: NORFOLK PERMIT #: W00019098 ANNUAL DRY TONS APPLIED: 76.46 OPERATOR: HAROLD DIXON CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 18.30 ACRES PERMITTED: 18.20 Page: 1 Lune Applied *'* Daze Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WI) (specify) "% Tons Cond. Precip. cation tili- all- Ammonia Nitrate PAN DATE or - Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 11/14/16 124,000.00 (G) 6775.956 2.22 0.627 DUAEDL MOIST 0-<12" SUR 0.5 0.30 57,700.p 9,910.00 p 1,360.00p 20652 WHEAT Nov-16 124,000.00 (G) 6,775956 11/7116 24,800.00 (G) 1355.191 3.54 0.200 DUWPL DRY 0-<12" SUR 0.5 0.40 5,930.Op 847.00 p 2.00 p 2459 WHEAT 11/8/16 198,400.00 (G) 10841.530 3.54 1.600 DUWPL DRY 0-<12" SUR 0.5 0.40 5,930.Op 847.00 p 2.00 p 2459 ,WHEAT .1119116 161,200.60 (G) 8808.743 3.54 1.300 DUWPL DRY 0-<12" SUR 0.5 0.40 5,930.Op 847.00 p 2.00 p 2459 WHEAT 11/11/16 55,800.00 (G) 3049.180 3.54 0.450 DUWPL DRY 0-<12" SUR 0.5 0.40 5,930.Op 847.00 p 2.00 p 2459 WHEAT Nov-16 1 440,200.00 (G) 24,054.644 Total Gallons/Ac: 30,930.60 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual Ibs/acre 43 0.074 0.017 0.334 0.654 0.148 0.005 0.046 0.165 0.042 1.312 38.95 Cumulative lbs/acm 0.285 0.225 2.260 17.196 1.579 0.058 0.729 1.987 0.285 45.678 'emit PAN Limit (Ibs/acre) 1st Crop2nd Crop t `�{y '�� " r " S.wr'0mmll'm.�+}�R a 1' 4 37 �"< , " 123 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 348 aN,, 1339.0 267.9 15.0 375.0 89.0 2500.0 WY DUAEDL = DUNN, NC WWI? AEROBICALLY DIGESTED LIQUID )UWPL = DUNN, NC WTP LIQUID . X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR-Surface, INJ-Injection,. SURIN-Incorporation *** See Site pH&Lime Application Records Section ofReport for Fields where Lime is to be applied in 2017 ANNUAL LAND APPLICATION FIELD SUMMARY FORM ACILITY NAME: DUNK, NC PREDOMINANT SOIL SERIES: NORFOLK OWNER: HAROLD DIXON PERMIT #: W00019098 ANNUAL DRY TONS APPLIED: 110.17 TTE #: NC HA 00008 FIELD# : HA 00008 0009 OPERATOR: HAROLD DIXON CATION EXCHANGE CAPACITY (NON-503): ESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 22.20 ACRES PERMITTED: 22.20 Pago: 1 Lime Applied *** Dale Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (W1') (specify) % Tons CorDry, Past2 cation till- Ammonia Nitrate pAN DATE or Per Residual Dry, Wet, Past 24 Method zazion zati zation TI4Q Nitrogen and pm (ppm) Crop MONTH Total Per Acre Solids I1/14/16 43,400.00 (G) 1954.955 2.22 0.181 DUAEDL MOIST 0-Q/2" SUR 0.5 0.30 57,700. p 9,910.00 p 1,360.00 p 20652 BERMUDAGRASS, COASTAL 11/15/16 192,200.00 (G) 8657.658 2.22 0.801 DUAEDL MOIST 0-Q/2" SUR '0.5 0.30 57,700.p 9,910.00 p 1,360.00p 20652 BERMUDAGRASS, COASTAL 11/16/16 124,000.00 (G) 5585.586 2.22 0.517 DUAEDL MOIST 0-Q2" SUR 0.5 0.30 57,700. p 9,910.00 p 1,360.00 p 20652 BERMUDAGRASS, COASTAL Nov-16 359,600.00 (G) 16,198.199 1119116 142,600.00 (G) 6423.423 3.54 0.948 DUWPL DRY 0-42" SUR 0.5 0.40 5,930.0p 847.00 p 2.00 p 2459 BERMUDAGRASS, COASTAL 11/10/16 297,600.00 (G) 13405.405 3.54 1.979 DUWPL DRY 0-Q2" SUR 0.5 0.40 5,930.0p 847.00 p 2.00 p 2459 BERMUDAGRASS, COASTAL 11111116 80,600.00 (G) 3630.631 3.54 0.536 DUWPL DRY 0-42" SUR 0.5 0.40 5,930.0p 847.00 p 2.00 p 2459 BERMUDAGRASS, COASTAL Nov-16 520,800.00 (G) 23,459.459 Total Gallons/Ac: 39,657.66 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 4nnual Ibs/acre 79 .0.086 0.020 0.386 1.181 0.222 0.007 0.059 0.204 0.050 2.352 75.63 :umWative Ibs/acre 0.238 0.154 1.819 1.361 0.233 33.535 ON hal„ 13.302 0.047 0.559 1.579 w emit PAN Limit (lbs/acre) 1st Crop2nd Crop (T r:: lh � s+ 'YivI f* rx�wr, f� , ,-WWWO 4 ar _ _ ,. _... .3.., .- Y. .... 9 m' 219 rD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 "",ltyd'es`n� 1339.0 267.9 15.0 375.0 89.0 l 2500.0 5u ,i' )UAEDL = DUNN, NC W WTP AEROBICALLY DIGESTED LIQUID )UWPL=DUNK, NC WTP LIQUID X CLICQ JA 1 4,E a �1�r- �a►7 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fires and imprisonment for knowing violations." N/A=Not Applicable NR=Not Reported or Not Required %=percent p-ppm or mg/kg *' Volatilization Rate: Surface 0.5, hijection/Incorpomtion 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 ANNUAL LAND APPLICATION FIELD SUMMARY FORM ACILITYNAME: DUNN, NC PREDOMINANT SOIL SERIFS: WABEE )WNER: CARL HAMILTON, JR. PERMIT #: WO0006101 ANNUAL DRY TONS APPLIED: 142.92 ITE #: NC HA 00201 FIELD# : HA 00201 0004 OPERATOR: RONNIE HAMILTON, JR CATION EXCHANGE CAPACITY (NON-503): tESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 90.10 ACRES PERMITTED: 90.10 Page: 1 Lime Applied *** Data Lbs/Ac allons (G) or Cubic Yards (CY) DD, Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation till- all- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past Method zation zation T14J Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 3/29/16 210,800.00 (G) 2339.623 3.54 0.345 DUWPL MOIST 0-<1/2" SUR 0.5 0.40 5,930.0p 847.001 p 2.00 p 2459 CORN 3/30/16 316,200.00 (G) 3509.434 3.54 0.518 DUWPL MOIST 0-<1/2" SUR 0.5 0.40 5,930.Op 847.00 p 2.00 p 2459 CORN 3/31/16 161,200.00 (G) 1789.123 3.54 0.264 DUWPL MOIST 0-<1/2" SUR 0.5 0.40, 5,930.0p 847.00 p 2.00 p 2459 CORN Mar-16 688,200.00 (G) 7,638.180 418116 124,000.00 (G) 1376.249 2.22 1 0.127 DUAEDL DRY 0-<1/2" SUR 0.5 0.30 57,700.p 9,910.00 p 1,360.00p 20652 CORN 4/9116 142,600.00 (G) 1582.686 2.22 0.147 DUAEDL DRY 0-<1/2" SUR 0.5 0.30 57,700.p 9,910.00 p 1,360.00p 20652 CORN 4/11/16 179,800.00 (G) 1995.560 2.22 0.185 DUAEDL DRY 0-<1/2" SUR 0.5 0.30 57,700.p 9,910.00 P 1,360.00p 20652 CORN Apr-16 446,400.00 (G) 4,954.495 Total Gallons/Ac: 12,592.67 As Cd Cr Cu Pb Hg Me Ni Se Zn P PAN TOTALS: Annual lbs/acre 24 0.028 0.006 0.124 0.366 0.070 0.002 0.019 0.065 0.016 0.730 23.37 Cumulative lbs/acre 0.153 0.064 0.949 6.264 1.288 0.035 0.150 0.693 0.112 11.599 'emit PAN Limit (lbs(acre) 1st Crop2nd Crop `j > o' rr.>�'r+.° nx� yg� - '`- 117 ;N7;�. k�M fik`.eSi'��isv FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 (}R` '4 1339.0 267.9 15.0no 375.0 89.0 3k 2500.0 FIFTY 7 DUWPL = DUNN, NC WTP LIQUID JUAEDL = DUNN, NC W WTP AEROBICALLY DIGESTED LIQUID X_� � M1 eye g-1L(�ywr7 (SIGNATURE OF LAND APPLIER) - DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there me significant penalties for submitting false information, including the possibility of fries and imprisonment for knowing violations." NIA =Not Applicable NR=Not Reported or Not Required %=percent p=ppmormgAcg ** Volatilization Rate: Surface 0.5, Injection/Ineorpomtion 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied im 2017 INC� ELJF.tfl9RONldENTAL rEGa!40LbGIcS, hnaly.0ca1 LaboratOrie6 February 15, 2016 Chris Brown Synagro 284 Boger Rd. Mocksville, NC 27028 TEL: (336) 998-7150 FAX: (336) 998-8450 RE: Dunn WWTP Summit Emironmental Technologies, Inc. 3310 Win St. Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX., (330) 2534489 Website: hMzYAwww.senekcom Dear Chris Brown: Order No.: 16020216 Summit Environmental Technologies, Inc. received 1 sample(s) on 2/3/2016 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, Bachar Najm Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 A2IA 0724.01. Alabama 41600, Arizona AZ0788, Atkansas 8M735, Caffirnia 07256CA, Colorado, Connecti=PH-0105, Delaware, Florida NELAC E87688, GeotgaE87688 and 943, Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-OH-13, Knows E10347, Ke cky (Uvdetgomid Stomge Tank) 3, Kennrcky 90146, Louisiana 0406l and LA12004. Maine 2Ol2Ol5. Maryland 339. Massachusetts M-OPID23, Minnesota 4O9711, Montma CERT0099, New Hampshire 2996, New ]emeyOH006, New York 11777, North Carolina 39705 and 631, Ohio D®king Water4170, Ohio VAP CL0052, Oklahoma 9940, Oregon OH2O0001, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018. Texas T104704466-11-5, Region 8 81MS-I., USDAIAPHIS P330.11-00244, Utnh OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C and E87688, Wisconsin 399013010 Page 1 of 8 Summit Environmental Technologies, Case Narrative 3310 in St. CLJ6FNIRMIERTALTECHUOLOc12S, INC_ Cuyahoga Falls, Ohio 44223 WO#: 16020216 Aru iytical Laboratories TEL: (330) 253-8211 FAX... (330)153-4489 Website: hao:/hvtnv.settekcom Date: 2/15/2016 CLIENT: Synagro Project: Dunn WWTP This report in its entirety consists of the documents listed below. All documents contain the Summit Environmental Technologies, Inc., Work Order Number assigned to this report. Paginated Report including Cover Letter, Case Narrative, Analytical Results, Applicable Quality Control Summary Reports, and copies of the Chain of Custody Documents are supplied with this sample set. Concentrations reported with a J-Flag in the Qualifier Field are values below the Limit of Quantitation (LOQ) but greater than the established Method Detection Limit (MDL). Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods. Estimated uncertainty values are available upon request. Analysis performed by DBM, VRM, or SFG were performed at Summit Labs 2704 Eatonton Highway Haddock, GA 31033 All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as "dry weight" using the "-dry" designation on the reporting units. Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of the cover letter that may or may not pertain to this report. The information contained in this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results contained in this report are only representative of the samples received. Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible for use or interpretation of the data included herein. This report is believed to meet all of the requirements of NELAC or the accrediting✓ certifying agency. Any comments or problems with the analytical events associated with this report are noted below. Original Page 2 of 8 ll Summit Environmental Technologies, In Qualifiers and Acronyms � �or 3310 Wins LLJENVIRONMENTAL TECHNOLOGIES, INC. Cuyahoga Falls, Ohio 4422 wO#: 16020216 Analytical caboratorie5 TEL: (330) 253-8211 FAX.• (330) 253-446 Website: hay.,IA ww.settek.co Date: 2/15/2016 These commonly used Qualifiers and Acronyms may or may not be present in this report. Qualifiers U The compound was analyzed for but was not detected. J The reported value is greater than the Method Detection Limit but less than the Reporting Limit. H The hold time for sample preparation and/or analysis was exceeded. D The result is reported from a dilution. E The result exceeded the linear range of the calibration or is estimated due to interference. MC The result is below the Minimum Compound Limit * The result exceeds the Regulatory Limit or Maximum Contamination Limit in Manual integration was used to determine the area response. N The result is presumptive based on a Mass Spectral Library search assuming a 1:1 response. P The second column confirmation exceeded 25% difference. C The result has been confirmed by GUMS. X The result was not confamed when GUMS Analysis was performed. B/MB+ The analyte was detected in the associated blank G The ICB or CCB contained reportable amounts of analyte. QC-/+ The CCV recovery failed low (-) or high (+). R/QDR The RPD was outside of accepted recovery limits. QL-/+ The LCS or LCSD recovery failed low (-) or high (+). QLR The LCS/LCSD RPD was outside of accepted recovery limits. QM-/+ The MS or MSD recovery failed low (-) or high (+). QMR The MS/MSD RPD was outside of accepted recovery limits. QV-/+ The ICV recovery failed low (-) or high (+), s The spike result was outside of accepted recovery limits. - Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for additional information Acronyms ND Not Detected RL Reporting Limit QC Quality Control MDL Method Detection Limit MB Method Blank LOD Level of Detection LCS Laboratory Control Sample LOQ Level ofQuantitation LCSD .Laboratory Control Sample Duplicate PQL Practical Quantitation Limit QCS Quality Control Sample CRQL Contract Required Quantitation Limit DUP Duplicate PL Permit Limit MS Matrix Spike RegLvi Regulatory Limit MSD Matrix Spike Duplicate MCL Maximum Contamination Limit RPD Relative Percent Different MinCL Minimum Compound Limit ICV Initial Calibration Verification RA Reanalysis ICB Initial Calibration Blank RE Rcextraction CCV Continuing Calibration Verification TIC Tentatively Identified Compound CCB Continuing Calibration Blank RT Retention Time RLC Reporting Limit Check CF Calibration Factor DF Dilution Factor RF Response Factor , This list of Qualifiers and Acronyms reflects the most. commonly utilized Qualifiers and Acronyms for reporting. Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms (hat do not appear in this list or for additional information regarding the use of these Qualifiers on reported data. Original Page 3 of 8 -- � � �� Summit Environmental Technologies, Inc. WOrkorder 3310 Win St. rt741A0141,IENTALTECnttOLOGI£S, Inc. Cuyahoga Falls, Ohio 442.23 Sample Summary Anaiyticel Laho+'atorie5 TEL: (330) 253-8211 FAY.. (330) 253-4489 WO#: 16020216 Website: hhup.-#�v.senekcom 15-Feb-16 CLIENT: Synagro Project: DunnWWTP Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix 16020216-001 Dunn W WCP 2/12016 4:10:00 PM 2/32016 12:00:00 PM Solid Page 4 of 8 mA_IT SmmirEmiomnentol Technologies, Inc. 3310 Win St. Analytical Re-port MVIRONMENTAL7ECW20LOOIES, IVC. Cuyahoga Falls, Ohio 44223 (base report) tirraiytical Laboratories TEL: (330) 253-8211 FAX. (330) 2534489 WO#: 16020216 Website: htro:/huww.settekcom Date Reported: 2/15/2016 CLIENT: Synagro Tag Number: Matrix: SOLID Collection Date: 2/l/2016 4:10:00 PM Lab ID: 16020216-001A Project: Donn WWTP Client Sample ID Dunn W WTP Analyses Result RL Qual Units DF Date Analyzed RCI SW9045D Analyst: DHC PH (SW9045D) pH 3.00 s.u.@18.7C 1 219/20164:10:00 PM Qualifiers: • vdueoxceo&M.&.c.nt.v rsveL E Vdueobowqumvaavonrwge H Hold'mg toots forpttpmazion or w2lnn.Ladd M Mmuel lute➢afiov and to deter®. oou, anse MC Vduehbelow Mmi..Coovowdljr. N Tmtatr lyidmfi6dmopowds ND Not X)dWd a the Reporting lion O RSD is grnterthwRRDI®R P Stoond wlonow�ofionexwels PL Permit Liodt Original R RFD ouW. oceeptedrewvw limier RI, Reporting➢rtzfiov Limit U Somploo iffiuwd<MDL d Ato0p.detemdbd.qumrtimtionlindu Page 5of8 - Summit Environmental Technologies. Inc. WO#: 16020216 3310 Win St. rNVIROWMENTAL TECRUOLOGIEF,]Ye Cuyahoga Falls, Ohio 44223 Date Reported: 2/15/2016 Ar Iytical Laboratories TEL. (330) 253-8211 R,"..• (330) 253-4489 Company: Synagro Websue: h m,.-11�v.seaekcom Address: 284 Boger Rd. MocksvilleNC 27028 Received: 2/3/2016 Project#: Dunn WWTP TCLP Metals Analysis (6010) Client ID# Lab EN Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Dunn WWTP 001 2/1/2016 TCLP Arsenic(As) 0.500 ND mg/L Solid EPA 6010 C 1 5.00 2/5/2016 WK Dunn WWfP 001 2/1/2016 TCLP Badum(Ba) 5.00 ND mg/L Solid EPA 6010C 1. 100 2/5/2016 WK Dunn W WTP 001 2/1/2016 TCLP Cadmium(Cd) 0.100 ND mg/L Solid EPA 6010 C 1 1.00 2/5/2016 WK Dunn WWTP 001 2/1/2016 TCLP Chromium(Cr) 0.200 ND mg/L Solid EPA 6010 C 1 5.00 2/5/2016 WK Dunn WWTP 001 2/1/2016 TCLP Lead(Pb) 0.500 ND mg/L Solid EPA 6010 C 1 5.00 2/5/2016 WK Dunn W WTP - 001 2/1/2016 TCLP Selenium(Se) 0.500 ND mg/L Solid EPA 6010 C 1 1.00 2/5/2016 WK Dunn W WTP 001 2/1/2016 TCLP Silver(Ag) 0.500 ND mg/L Solid EPA 6010 C 1 5.00 2/5/2016 WK TCLP Mercury Analysis (1311n470) Client ID# Lab W# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst -- inn WWTP 001 2/1/2016 TCLP Mercury 0.00200 ND mg/L Solid EPA 7470A 1 0.200 2/11/2016 MFW F I SVOC SW-846: 8081-TCLP Pesticides Client ED# Lab ID# Collected Analyte Rep Loot Result Units Matrix Method DF RegLvl Run Analyst Dunn WWtP 001 2/1/2016 Chlordane, total 0.0250 ND mg/L Solid EPA 8081B 1 0.0300 2/8/2016 JBN Dunn WWTP 001 211/2016 Toxaphene 0.0500 ND mg/L Solid EPA 8681B 1 0.500 2/8/2016 JBN Dunn WWTP 001 2/1/2016 Enddn 0.00250 ND mg/L Solid EPA 8081E 1 0.0200 2/8/2016 JBN Dunn WWTP 001 2/1/2016 gamma-BHC 0.00250 ND mg/L Solid EPA 8081B 1 0.400 2/8/2016 JBN Dunn WWTP 001 211/2016 Heptachlor 0.00250 ND mg/L Solid EPA 8081B 1 0.00800 2/8/2016 JBN Dunn WWTP 001 2/1/2016 Heptachlor epoxide 0.00250 ND mg/L Solid EPA 8081B 1 0.00800 2/8/2016 JBN Dunn WWTP 001 2/1/2016 Methoxychlor 0.00250 ND mg/L Solid EPA 8081E 1 10.0 2/8/2016 JBN VOC by GC/MS (8260)-TCLP Client ID# Lab ID# Collected Analyte Rep Loot Result Units Matrix Method DF RegLvl Run Analyst DunnWWTP 001 2/1/2016 1,1-Dichloroethene 0.100 ND mg/L Solid EPA 8260B 1 0.700 2/5/2016 MES Dunn WWTP 001 2/1/2016 1,2-Dichloroethane 0.100 ND mg/L Solid EPA 8260B 1 0.500 2/5/2016 MES Dunn WWTP 001 2/1/2016 MEK 2.00 ND mg/L Solid EPA 8260B 1 200 2/5/2016 MES Dunn WWTP 001 2/1/2016 Benzene 0.100 ND mg/L Solid EPA 8260E 1 0.500 2/5/2016 MES Dunn WWfP 001 2/1/2016 Carbon tetrachloride 0.100 ND mg/L Solid EPA 8260B 1 0.500 2/5/2016 MES Dunn W WfP 001 2/1/2016 Chlorobenzene 0.100 ND mg1L Solid EPA 8260 B 1 100 2/5/2016 MES Dunn W WTP 001 2/1/2016 Chloroform 0.100 ND mg/L Solid EPA 8260 B 1 6.00 2/5/2016 MES Dunn W WIP 001 2/1/2016 Tetrachloroethene 0.100 ND mg/L Solid . EPA 8260 B 1 0.700 2/5/2016 MES Dunn WWTP 001 211/2016 Trichloroethene 0.100 ND mg/L Solid EPA 8260 B 1 0.500 215/2016 MES ,- -7�= WWTP 001 2/1/2016 Vinyl chloride 0.200 ND mg/L Solid EPA 8260 B 1 0.200 215/2016 MES Page 6 of 8 - Sronmit8miranmental TechnoloW. WO#• 16020216 LIJ"VIRONNIENTAL TECHU01-0cIcs, rm Win 3310 Win SStt. Cuyahoga Falls, Ohio 44223 Date Reported: 2/15/2016 Analytical Laboratories TEL: (330) 253-8211 FAX., (330) 253-4489 . Company: Synagro Website: htw.-# nv.senekcom Address: 284 Boger Rd. MocksvilleNC 27028 Received: 2/3/2016 Project#: Dunn WWTP SVOC 8270 TCLP RNA List Client ED# Lab M# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Dunn WWTP 001 2/1/2016 1,4-Dlchlorobenzene 0.200 ND mgll- Solid EPA 8270C 2 7.50 2/9/2016 MO Dunn WWTP 001 211/2016 2,4,5-Trichlorophenol 0.500 ND mg/L Solid EPA 8270C 2 400 2/9/2016 MO Dunn W WTP 001 2/1/2016 2,4,6-Trichlorophenol 0.500 ND mg/L Solid EPA 8270 C 2 2.00 21912016 MO Dunn W WTP 001 2/1/2016 2,4-Dinitrotoluene 0.200 ND mg/L Solid EPA 8270 C 2 0.130 219/2016 MO Dunn W WTP 001 211/2016 Cresols, Total 10.0 ND mg/L Solid EPA 8270 C 2 200 219/2016 MO Dunn W WTP 001 2/1/2016 Hexachloro-1,3- 0.200 ND mg/L Solid EPA 8270 C 2 0.500 2/9/2016 MO butadiene Dunn W WTP 001 2/1/2016 Hexadilorobenzene 0.200 ND mg/L Solid EPA 8270 C 2 0.130 2/912016 MO Dunn WWTP 001 211/2016 Hexachloroethane 0.200 ND mg/L Solid EPA 8270 C 2 3.00 21912016 MO Dunn W WIP 001 2/1/2016 Nitrobenzene 0.200 ND mg/L Solid EPA 8270 C 2 2.00 2/9/2016 MO Dunn WWTP 001 2/1/2016 Pentachlorophenol 0.500 ND mg/L Solid EPA 8270C 2 100 219/2016 MO DunnWWTP 001 2/1/2016 Pyridine 0.500 ND mg/L Solid EPA 8270C 2 5.00 2/9/2016 MO '1 SVOC SW-846: 8321 Herbicides-TCLP Client ID# Lab EN Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Dunn WWTP 001 2/V2016 2,4-D 5.00 ND mg/L Solid EPA 8321A 1 10.0 2/9/2016 BJH Dunn WWTP 001 2/1/2016 2,4,5-TP 0.500 ND mg/L Solid EPA 8321A 1 1.00 219/2016 BJH Page 7 of 8 Summit Environmental Technologies, Inc. WO#: 16020216 summut 3310 Win Sl. F. ARON6IENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 Date Reported: 2/152016 Analytical LT6oratorfcs TEL: (330) 253-8211 FAX., (330) 253-4489 Company: Synagr0 Websile: hap.,M w.senekeom Address: 284 Boger Rd. Mocksville NC 27028 Received: 2/3/2016 Project#: DunnWWTP Client EN Lab M# Collected Analyte Result Units Matrix Method DF RL Run Analyst Dunn WWTP 001 2/1/2016 Flashpoint (140°F) >140 °F Solid EPA 1010 1 2111/2016 TAH Dunn W WTP 001 2/1/2016 Cyanide, Reactive ND mg/Kg Solid EPA 9014 1 0.500 2/9/2016 MS Dunn W WTP 001 2/1/2016 Sulfide, Reactive ND mg/Kg Solid EPA 9034 1 25.0 219/2016 MS Page 8 of 8 ®Summit10WnEnvironmental nn►ental Technologies; Lla Analysis Request/Chain of Custody Cuyao a Street For Summit Lavironmental Technologies, Ina use only Cuyahoga Falls, Ohio 44223 1?:1: 330.253.8211 Fax: 33D.253.4489 Page —of._. SET No. Core any Name (Please Print) -ProjectName ADalytieal Parameters and Methods VUW 11 CompAdd .s Project Address 2 e� 0 IL c Client Phone No. C9 i 9 7�Y-a74 Rep to Ctlenl Fax No. please Fax Remits ✓ PG# n Client Email uom No. C Contact , n Mw' N m r$ y m a Sampled by Check if Ohio VAP samples / Q ij Sample ldenttGcatian Dnte. Time Collected I Croce". C7 U' im S Z D04 Rey. ,. Summit Environmental TachnoloijbW Inc. Cooler R4001pt Form Client _.5Inleals of Perron Inspecting 000lersnd samples: f �� 1 Ordef Nomber. IIY �;C. O�i .��. Date Received.j'S fu Tlmo ReeeNedL-11a Date coolers) opened and samples 6poded:1-24 r1� �Tj' Number of CooterslBoxes: WA Shipper: ' i.7" UPS DHL Atrboms US Postal Walk4n Pickup others_ Packaging: Peanuts ar'V p Paper Foam None Other. Tape on cooler/bor. N WA Custody Seats intact Y N . lIZ71 C-0-C In plastic lee_Vl— Blue lee 1z N N/A present / absent ! melted NIA Sample Temperature-IR Gun Atr?0j05 C&D 'Z:>>C WA ' Radiological Testing Insttumentsedaif12= Y N (see pegs 2 for acan mauas) ^usotslsaat persomple for Rsdreiegleai Tssdng. If* moo in HOT. the Rediotogica aafety OMieermustbanotib d Immee9�aly. C-0-C filled outprupedy O^N NfA . Samples In separate bags v1:^J , N WA Semple containers intact O N WA 'If M. list broken sample(s): SmnPle labels) ComPlets (ID. date. eta) N WA Labels) agree wfth C-" Y N _ Cqueet contatnors used N WA WA . Sufficientsemple mcehmd N WA Samples receNed within holding tone <�Yb N Bubbles absent Rom 40 mL vials" Y N C.1 "Samples with bubbles -,6mm aka acceptable. Indicate bubble size I1>6mm. Was client conisoled about sample, Y N Will client send now samples Y N Logged Page t of 2 a UjE!R9RONhtENTALTECH!101bei=_5, INC AnafyHcaf La6afaforles February 13, 2016 Nate Roth Synagro 284 Boger Rd. Mocksville, NC 27028 TEL: (336) 998-7150 FAX: (336) 998-8450 RE: Dunn WTP Dear Nate Roth: Sunnnit Environmental Technologies, Inc. 3310 Win St. Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX.- (330) 2534489 Website: hup.-IAv .setmkcom.-IA w.setmkcom Order No.: 16020214 Summit Environmental Technologies, Inc. received I sample(s) on 2/3/2016 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, (ZG Bachar Najm Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 A21A 0724.01, Alabama 41600, Ariaom AZO7S8, Arkmsas 88-0735, California 07256CA, Colorado, Comecticsa PH-0105, Delaware, Florida NELAC E87688, Georgia E87688 and 943, Idaho OH00923, IDmois 200061 and Reg.5, Indiana C-011-13, Kansas E-10347, Kentucky (Undeegmmd Storage Tank) 3, Kmncky 90146, Louisiana04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-0PH973, Mimesom 409711, Moorman CERT0099, New Hampshire 2996. New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio Drinking Water4170, Ohio VAP CL0052, Oklaboma 9940,0regonOM00001, Rhode Island lA000317, South Carolina 92016001, Temessee TN04018, Texas T104704466-11-5, Region 88TMS-4 USDAIAPHIS P330-11-00244, Utah OH009232011-1, Vemrmt VT-87688, Vhginia 00440 and 1581, Wasbingwn C891, Wen Virginia 248 and 9957C and E87688.Wisconbm399013010 Page 1 of 8 U Vi/ I 3310 Winin SStt. Summit Environmental Technologies. Case Narrative FNFIR0NhIENTALTEC4t40Lbcie5, IPIC. Cuyahoga Falls, Ohio 44213 WO#: 16020214 Analytical Lsbaraiorfes TEL. (330)153-8211 FAX.. (330) 253-4489 Website: humllwww.settekcom Date: 2/13/2016 CLIENT: Synagro Project: .Dunn WTP This report in its entirety consists of the documents listed below. All documents contain the Summit Environmental Technologies, Inc., Work Order Number assigned to this report. Paginated Report including Cover Letter, Case Narrative, Analytical Results, Applicable Quality Control Summary Reports, and copies of the Chain of Custody Documents are supplied with this sample set. Concentrations reported with a J-Flag in the Qualifier Field are values below the Limit of Quantitation (LOQ) but greater than the established Method Detection Limit (MDL). Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods. Estimated uncertainty values are available upon request. Analysis performed by DBM,VRM, or SFG were performed at Summit Labs 2704 Eatonton Highway Haddock, GA 31033 All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as "dry weight" using the "-dry" designation on the reporting units. Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of the cover letter that may or may not pertain to this report. The information contained in this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results contained in this report are only''representative of the samples received. Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, hie, is not responsible for use or interpretation of the data included herein. This report is believed to meet all of the requirements of NELAC or the accrediting 4 certifying agency. Any comments or problems with the analytical events associated with this report are noted below. Original Page 2 of 8 -`1 � �� SummitEmiromnenmlTechnolo0WinS n 331Win Qualifiers and Acronyms F.ttvl^nONtdENTAL TECRMOLOGIcS, INC. Cuyahoga Falls, Ohio 4422 W04: 16020214 Analytical taboratodcs TEL: (330) 253-8211 FAX.. (330) 253-446 Website: hem://wim.settekco Date: 2/13/2016 These commonly used Qualifiers and Acronymsmayor may not be present in this report. Qualifiers U The compound was analyzed for but was not detected J The reported value is greater than the Method Detection Limit but less than the Reporting Limit. H The hold time for sample preparation and/or analysis was exceeded D The result is reported from a dilution. E The result exceeded the linear range of the calibration or is estimated due to interference. MC The result is below the Minimum Compound Limit. * The result exceeds the Regulatory Limit or Maximum Contamination Limit. in Manual integration was used to determine the area response. N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response. P The second column confirmation exceeded 25% difference. C The result has been confirmed by GC/MS. X The result was not confirmed when GC/MS Analysis was performed B/MB+ The analyte was detected in the associated blank G The ICB or CCB contained reportable amounts of analyte. QC-/+ The CCV recovery failed low (-) or high (+). R/QDR The RPD was outside of accepted recovery limits. QIr/+ The LCS or LCSD recovery failed low (-) or high (+). QLR The LCS/LCSD RPD was outside of accepted recovery limits. QM-/+ The MS or MSD recovery failed low (-) or high (+). - QMR 'The MS/MSD RPD was outside of accepted recovery limits. '}. QV-/+ The ICV recovery failed low (-) or high (+). 1 s The spike result was outside of accepted recovery limits. -' Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for additional information Acronyms ND Not Detected RL Reporting Limit QC Quality Control MDL Method Detection Limit MB Method Blank LOD Level of Detection LCS Laboratory Control. Sample LOQ Level ofQuamitation LCSD Laboratory Control Sample Duplicate PQL Practical Quantitation Limit QCS Quality Control Sample CRQL Contract Required Quantitation Limit DUP Duplicate PL Permit Limit MS Matrix Spike RegLvl Regulatory Limit ' MSD Matrix Spike Duplicate MCL Maximum Contamination Limit RPD Relative Percent Different MInCL Minimum Compound Limit ICV Initial Calibration Verification RA Reanalysis ICB Initial Calibration Blank RE Rcextraction CCV Continuing Calibration Verification TIC Tentatively Identified Compound CCB Continuing Calibration Blank RT Retention Time RLC Reporting Limit Check CF Calibration Factor DF Dilution Factor BY Response Factor This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting. Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this list or for additional information regarding the use of these Qualifiers on reported data. Original Page 3 of 8 Summit Environmental Technologies, Inc. Workorder SUMMIT 3310 Win St. MVIRONl.1ENTAL TECNNOLoal=S, Inc. Cuyahoga Falls, Ohio.44223 Sample Summary Analytical Laboratories TEL: (330) 253-8211 FAX.. (330) 253-4489 WO#: 16020214 Websile: ha2:11v .settekcom 13-Feb-16 CLIENT: Synagro Project: Dunn WTP Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix 16020214-001 Dunn WTP 2112016 3:30:00 AM 2/312016 12:00:00 PM Solid Page 4 of 8 �or saa rtEaP�aaaeatalTeehaa/10WinS. 33I0 Win St. Analytical Report ENVIRONMENTAL TECHN0LOGIES, Cuyahoga Falls, Ohio 44223 (base report) Analytical Laboratories TEL: (330) 253-8211 FAX., (330) 253-4489 WO#: 16020214 Website: humlAo senekcam Date Reported: 2/1312016 CLIENT: Synagro Tag Number: Matrix: SOLID Collection Date: 2/1/2016 3:30:00 AM Lab ID: 16020214-OOIA Project: Dunn WTP Client Sample ID Dunn WTP Analyses Result RL Qual Units DF Date Analyzed RCI SW9045D Analyst: DHC PH (SW9045D) - pH 5.56 S.H.@19.1C 1 2/8120162:20:00 PM Qualifiers• ' Valoe uceMa Madmm Conta®ant /eusl. E Valueebow quavtitatovmvge E Holdog tms for preparation or analysis eazMed M Manualategmton and to detammearsreryonse MC Value a belowMm. Compowdli®t N Trotatrtretyidmrifiedmn,oun& ND Not Dots etWe Reportvg J.i®t 0 MD is greater than RSDlimit P Secondrol.confirn=ovo¢eeds M Permitl,ma Original R RPD outside accepted rxove, li®b RL Reporting Dete ionlinit U SamplswithCelcval<ML J Malytedetected below gaanGtatwnli®ts Page 5of8 Summit Environmental Technologies, Inc. WO#: 16020214 3310 Win St. FtfVIRONNIENTALIEC14NOLoclEs,mrG Cuyahoga Falls, Ohio 44223 Date Reported: 2/13/2016 Anafytical. r.ahoratones TEL: (330) 253-8211 FAX: (330) 253-4489 Company: Synagro Website: bffwN ww.seaekcom Address: 284 Boger Rd. MocksvilleNC 27028 Received: 2/3/2016 Project#: Dunn WTP TCLP Metals Analysis (6010) Client ID# Lab 1D# Collected Analyte Rep Lmt Result Units Matrix Method DF ' RegLvl Run Analyst Dunn WTP 001 21112016 TCLP Arsenic(As) 0.500 ND mg/L Solid EPA 6010 C 1 5.00 2/5/2016 WK Dunn WTP 001 2/1/2016 TCLP Badum(Ba) 5.00 ND mglL Solid EPA 6010 C 1 100 2l5/2016 WK Dunn WTP 001 2/1/2016 TCLP Cadmium(Cd) 0.100 ND mglL Solid EPA 6010 C 1 1.00 2/5/2016 WK Dunn WTP 001 2/1/2016 TCLP Chromium(Cr) 0.200 ND mglL Solid EPA 6010 C 1 5.00 215/2016 WK Dunn WTP 001 2/1/2016 TCLP Lead(Pb) 0.500 ND mg/L Solid EPA 6010 C 1 5.00 215/2016 WK Dunn WTP 001 2/1/2016 TCLP Selenium(Se) 0.500 ND mg/L Solid EPA 6010 C 1 1.00 215/2016 WK Dunn WTP 001 2/1/2016 TCLP Silver(Ag) 0.500 ND mg/L Solid EPA 6010 C 1 5.00 215/2016. WK TCLP Mercury Analysis Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst mn WTP 001 2/1/2016 TCLP Mercury 0.00200 ND mg/L Solid EPA 7470A 1 0.200 2/11/2016 MFW SVOC SW-846: 8081-TCLP Pesticides Client ID# Lab ID# Collected'Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Dunn WTP 001 2/1/2016 Chlordane, total 0.0250 ND mg/L Solid EPA 8081 B 1 0.0300 2/8/2016 JBN Dunn WTP 001 2/1/2016 Toxaphene 0.050D ND mg/L Solid EPA 8081 B 1 0.500 2/8/2016 JBN Dunn WTP 001 2/1/2016 Endrin 0.00250 ND mg1L Solid EPA 8081 B 1 0.0200 2/8/2016 JBN Dunn WTP 001 2/1/2016 gamma-BHC 0.00250 ND mg/L Solid EPA 8081 B 1 0.400 2/8/2016 JBN Dunn WTP 001 2/1/2016 Heptachlor , 0.00250 ND mg/L Solid EPA 8081 B 1 0.00800 2/8/2016 JBN Dunn WTP 001 2/1/2016 Heptachlor epoxide 0.0D250 ND mg/L Solid EPA 8081 B 1 0.00800 2/8/2016 JBN Dunn WTP 001 2/1/2016 Methoxychlor 0.00250 ND mglL Solid EPA 8081 B 1 10.0 2/8/2016 JBN VOC by GC/MS Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Dunn WTP 001 2/1/2016 1,1-Dichloroethene 0.100 ND mglL Solid EPA 8260 B 1 0.700 2/5/2016 MES Dunn WTP 001 211/2016 1,2-Dichloroethane 0.100 ND mg/L Solid EPA 8260 B 1 0.500 2/5/2016 MES Dunn WTP 001 2/1/2016 MEK 2.00 ND mg/L Solid EPA 8260B 1 200 2/5/2016 MES Dunn WTP 001 2/112016 Benzene 0.100 ND mg/L Solid EPA 8260 B 1 0.500 2/5/2016 MES Dunn WTP 001 2/112016 Carbon tetrachloride 0.100 ND mglL Solid EPA 8260 B 1 0.500 2/5/2016 MES Dunn WTP 001 2/1/2016 Chlorobenzene 0.100 ND mglL Solid EPA 8260 B 1 100 2/512016 MES Dunn WTP 001 211/2016 Chloroform 0.100 ND mglL Solid EPA 8260 B 1 6.00 2/5/2016 MES Dunn WTP 061 2/1/2016 Tetrachloroethene 0.100 ND mg/L Solid EPA 8260 B 1 0.700 2/5/2016 MES Dunn WTP 001 211/2016 Trichloroethene 0.100 ND mg/L Solid EPA 8260 B 1 0.500 2/5/2016 MES --,Inn WTP 001 2/1/2016 Vinyl chloride 0.200 ND mglL Solid EPA 8260 B 1 0.200 2/6/2016 MES Page 6'of 8 {yt�l�33I0 Envrranmenlal Techno(10 Vi Inc.WO#: 16020214 Am,,Sronmit �n St.ONMENTAL LUAnalytical IECHUOLGGIES, INq Cuyahoga Falls, Ohio 44223 Date Reported: 2/13/2016 Laboratories TEL. (330) 253-8211 FAX..- (330) 253-4489 Company: Synagro iWebsite: hffy.-# ww.settekcom Address: 284 Boger Rd. MocksvilleNC 27028 Received: 2/3/2016 Project#: Dunn WTP SVOC 8270 TCLP BNA List Client ID# Lab U)# Collected Analyse Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Dunn WTP 001 2/1/2016 1,4-Dichlorobenzene 0.200 ND mg/L Solid EPA 8270 C 2 7.50 219/2016 MO Dunn WTP 001 2/1/2016 2,4,5-Trichlorophenol 0.500 ND mg/L Solid EPA 8270 C 2 400 219/2016 MO Dunn WTP 001 2/1/2016 2,4,6-Trichlorophenol 0.500 ND mg/L Solid EPA 8270 C 2 2.00 2/9/2016 MO Dunn WTP 001 2/1/2016 2,4-Dinitrololuene 0.200 ND mg/L Solid EPA 8270 C 2 0.130 2/9/2016 MO Dunn WTP 001 2/1/2016 Cresols, Total 10.0 ND mg/L Solid EPA 8270 C 2 200 2/9/2016 MO Dunn WTP 001 2/1/2016 Hexachloro-1,3- 0.200 ND mg/L Solid EPA 8270 C 2 0.500 2/9/2016 MO butadiene Dunn WTP 001 2/1/2016 Hexachlorobenzene 0.200 ND mg/L Solid EPA 8270 C 2 0.130 2/9/2016 MO Dunn WTP 001 2/1/2016 Hexachloroethane 0.200 ND mg/L Solid EPA 8270 C 2 3.00 2/9/2016 MO Dunn WTP 001 2/1/2016 Nitrobenzene 0.200 ND mg/L Solid EPA 8270 C 2 2.00 2/9/2016 MO Dunn WTP 001 211/2016 Pentachlorcphenol 0.500 ND mg/L Solid EPA 8270 C 2 100 2/9/2016 MO Dunn WTP 001 2/1/2016 Pyridlne 0.500 ND mg/L Solid EPA 8270 C 2 5.00 2/9/2016 MO SVOC SW-846: 8321 Herbicides-TCLP Client ID# Lab M# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Dunn WTP 001 _ 211/2016 2,4-D 5.00 ND mg/L Solid EPA 8321 A 1 10.0 2/9/2016 BJH Dunn WTP 001 2/1/2016 2,4,5-TP 0.500 ND mg/L Solid EPA 8321 A 1 1.00 2/9/2016 BJH Page 7 of 8 Summit Environmental Technologies, Inc. Rr WO#: 16020214 3310 Win St uAI UJEUVIRONh1ENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 Date Reported, 2/13/2016 Analytical Laboratories TEL: (330) 253-8211 FAX: (330) 253-4489 Company: Synagro Wehsite: httnl/www.senekcom Address: 284 Boger Rd. MocksvilleNC 27028 Received: 2/3/2016 Project#: Dunn WTP Client EN Lab ID# Collected Analyte Result Units Matrix Method DF RL Run Analyst Dunn WfP 001 211/2016 Flashpoint (1407) >140 °F Solid EPA 1010 1 2111/2016 TAH Dunn WfP 001 2/1/2016 Cyanide, Reactive ND mg/Kg Solid EPA 9014 1 0.500 219/2016 MS Dunn WfP 001 2/1/2016 Sulfide, Reactive ND mg/Kg Solid EPA 9034 1 25.0 219/2016 MS Page 8 of 8 Summit Environmental Technologies, Inc. 3310 Win Street Analysis Request/Chain of Custody For Summit Environmental Technologies, Inc use only 1 1 1 Cuyahoga Falls, Ohio 44M Tel: 330,253.8Z11 rax: JJUX)sAweg Page —of— SET'No. Company Name (Please Pdnt) � ,A vv Project Name u � i l 0 ,y. U o z Analytical Parameters and Methods Company dress r1�� Wlerk6�`'lc nrC Project Ad Tess M b PO .61 eQ q .Q S ,� ra y go p J J Clienl Phone / Report to Ucm Fax Na lease s ✓ ❑ Mt Client Email Please Rmail Resells ✓ uote No. Contact Pc[so t Sampled by /t ` h Check it' Ohio VAP samples V # Sample identification Date Collected 11me Collected ve�wena,naat aaa 3'3c�15LI Ire NatcJCcauments: Ii in u' by: Date I Time Received b . Dowi I time Received in lab by: Time Mow he approved Rush Rcquutcd By: by tab manager alf c the lahnm,erv. 5:3 /@ lZ.v Thecliem relates the pink page Q� �Q% Summit Environmental Technologies, Inc. Analysis Request/Chain of Custody 3310 Win Strcet For Summit Environmental Technologies, Inc. use only _ l 1 1 Cuyahoga Falls, Ohio 44223 Tel: 330.253.8711 rax: s:1vX)s.'va9 Page —of — Company Name (Please Print) Project Name W l U ;o U a�. e Z Analytical Parameters and Methods Company Addrers 2na$o�CK �zv4�G k I AA, mu Pme g go' q C II -f 6 In42 w u a (l Client Phone N . 5- �-0741r 1'Iease Rcpon to Client Fax No. 1 ✓ Q FOft Client Email Pl ose Froall Resnlls ✓ 'Quote No. contact Pcrsv s TUY\ Sampled 6y U` Check if Ohio VAP samples J Els: Sample Identification CoDate llected Mine Collected vN.�cbo`t Mh9at oa, � 3'•3c� 5L Imo. NotoXo nments: R 9in u' by: I Date I lime Received Date time Received in tab by: Mt9Time Rush Requested BY: Must he approved a[c by lab to nager "•"'^ d II a ns slwuld accom ea winpw hi the lubomwry. 2. 3 /� iLr� Thecliva wtalns the pink page. ao yo ow p g P Yvim. A v v DC-7 $N. 14 onsna Summit EnvirannWntsl Technploples, Inc. Cooler R"Wpt Form' WII$le of penon Inspecting cooterand se,nplpx rS� Order i� Date Rece(ved: 2 3 Term Recelved:�_ Dab Coolers) opened and samples Iespe —,, J_4J) (p Number of Cooler OMS: WA �7"^ Shipper. F�O�F ( UPS DHL Aubome US Postal Wak4n Pickup Other. Packaging: Peanuts 9ZEERP Paper Foam None Dlher. Tape on wobnboz N WA Custody Seale Intact Y N COCplastic 1z N WA loa Blue lcs present I absent / melted WA Sample Tsmparatum IRGunit CFL �°C _'C ,WA . Insttumaat aerial#35127 Y N RRadiologiealTesting (see page 2 for scan keaulle) /$Matparsampbfor Radlologleal Testing. Ifsarrrpla Is HOT, the Radiological Safety Officer must be no1MW ItmrlsdWW . 0-0-C ODd out propedy OY� N N/A Samples in separate bags �1�J N WA Sample contelmers intadr OY N WA 9f no, list broken sample(s); Sample tabel(s) complete (ID. date. eta) E2> N WA Labels) agreewgh C•O•C O N • NIA Conectcontafners used N WA SuffiderdsampW asceived V N WA SamPiee receh*d within holding time (�b N Bubbles absent from 40 rriL vlais" Y N � "Sample$ with bubbles <timm am acceptable. Indicate bubble size if�fimm. ' Was rLentcontacted about samples Y N Wig client send now samples Y N CgentcontacL• Datefflme• Logged in 6y Page t of 2 n ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Dunn WQPermit Number: W00006101 WWTPName: City of Dunn WWTP NPDESNumber: NCO043176 Monitoring Period: From 01/01/2016 To 12/31/2016 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) -Please indicate level achieved and alternative performed: Class A: Alt 1/A (time/temp) Alt 2/B (Alk Treatment) Alt 3/C (Prior Testing) _ Alt. 4/1) (No Prior Test) _ Alt. 5/Process to Further Reduce Pathogens _ Alt 6 (Equivalent to PFRP) _ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying _ Heat Treatment _ Thermophilic Beta Ray _ CrammaRay _ Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": . Lime Stabilization Air Drying Composting _ Aerobic Digestion Anaerobic Digestion Tf annlirable to alternative nerfnrmed (Class A nr Class Rl rmmnlete the follnwinn mnnitnrina data - Parameter Allowable Level in Sludge - Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Gen. Mean Maximum Units dances .Analysis Fecal 2x10 to the 6 MPN MPN/g Coliform powerpergram of total solids CFU <37300 <58000 <85400 CFU/g 0 Based on grab 9222D - Land App. MF 1000 MPN per gram of MPN/g total solids (dry weight) - Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt 1 Option/Alt 2 Option/Alt 3 Option/Alt 4 (VS reduction) x (40-day bench) _ (30-day bench) _ (Spec. 02 uptake) Option/Alt 5 Option/Alt 6 Option/Alt 7 Optionwt. 8 (14-Day Aerobic) (AlkStabilization) _ (Drying —Stable) _ (Drying —Unstable) Option/Alt 9 Option/Alt 10 (Injection) _ (Incorporation) _ No vector attraction reduction alternatives were performed STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requuements in 40 CFR 503.32/15ANCAC 02T.1106,and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met" (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment" Donrie Dukes Wastewater Treatment Plant Supervisor Pre arer Name and Title (type or print) Land Applier Name and Title (if applicable) (type or print) I112-,L/ � 4,- a % _ Signature ofPreparer• Date Signature of Land Applier (if applicable) Date •Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) Cameron Testing Services, Inc. L ClQnt: - Synagto Dunn WWTP Sample I Sampled W. Verner . Raw - Analyses < as Lab.IR- Sa ple 1P- m o m (9 160056 Di a iludge G b C d e If 9 160056 01 a 3lad9r Or b c d e f 9 Report Review_ lab Director Report GT&tim.: 160066 Regulatuxy . Yes :i NO DENR#654 NC PHHS #37799 US EQA#NC01918 2116 Received: J.Cameron Date. 01/12M6 i Results f N tlyte ResulC co CL Std. Methods Itef „_ P a {ratite Alfol -S <37300 cFU/g 37300 01/13116 CSC 9i2211)-MF <80200 ccurg 80200 <49900 CFUrg 49900 <55800 CFU/9 55800 <85400 cling 85400 <670.00 CFulg 67000' <46600 CFu19 46600 [mean <58000 1(%) 5.11% v. o.01 01/19/16 CSC 2540G-TS 2,33% % 0.01 3.97% % 0.01 3.59% m am 2.19% % 0.01 2.87% % 0.01 4.05% % 001 of/2L /X Date 219 S. Steele Str. Sanford NC 27330 l 919-2084240 chris;gkerpemnlestine.com 219 S. Steele Str. Sanford, NC 27330 Cameron Testing Services, Inc. NO WW/GW Cart.#654 NO PHHS Cert#37799 US EPA NCO1916 Chain of Custody Page _ of ComPany�' (rl Synagro I I Emall Y CtS-lab.iuse only '��Ei ,,. +5 tza'� . Sample Temp iC)—� Prot �� I tA:%� p0. �� IPhone API i�h �J 336-909-6627 q tl�r rre�;C Ty 284 Boger Rd. 4,15ax 3'Isr°t wi I ' �+iY Pi ��i r it,Mocksville, NC. 27028 Notes;f� aDue "Ru$h Regulatory t '"GYM).`,. CollecteG}�)W,�Name �il( Signature '':_ n fln �'p"" ne Sample lnforma4ion ' " Number gf bottles. ^_ ; RQquested Analysts y Ra r .. :. :.:� �.. o u -o, 'HCl CTS Lab a Sample..ID. �. .. ar Sal E. I_E -:°, .;�.. > " ��.I .a.. § YeS2SO4VR NO'+npr Na'ted h"'"-'" ..Sr �D 1= ;U C7 1 m c I -� a C G'NaCH X=Cther tndidaie.- _ � I-raIA �d1 G ,5( t 7r cam! s / "T • � I T I 'T r DatelTime. R'ecetved +•• ee2--- Rush work will require prior approval. Additional charges will apply Black River Wastewater Treatment Plant City of Dunn 2016 April2016 Vector Attraction Rec.—..79 Holding Tank—..68 .79-.68 = 43.5% 79-(.79x.68) September2016 Vector Attraction Rec.—.83 Holding Tank-.74 .83 - . 74 = 41.6 % 83 - (. 83 x.74) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Dunn WQ Permit Number: W00006101 {` WWTPName: City of Dunn WTP NPDESNumber: 03-43-010 \ Monitoring Period: From 01/01/2016 To 12/31/2016 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. l/A (time/temp) Alt 2/B (Alk Treatment) _ Alt 3/C (Prior Testing) Alt 4/D (No Prior Test) Alt 5/Process to Further Reduce Pathogens _ Alt 6 (Equivalent to PFRP) _ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying _ Heat Treatment _ Thermophilic Beta Ray _ Gamma Ray _ Pasteurization Class B: Alt (1) Fecal Density X Alt (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization _ Air Drying Composting _ Aerobic Digestion Anaerobic Digestion �Tf annlirahle to alternatve rierfnrm Ad lClacc A nr Clacc Rl rmmnlete the fnllnwinv mnnitnrinn data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Gen. Mean Maximum Units dences Analysis Fecal 2x10tothe MPN MPN/g Coliform power per gram of total solids <40900 <42300 <43600 CFU/g 0 Based on grab 9222D - CFU Land App. MF 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grans total bacteria (in solids (dry weight) lieu of fecal colifomt Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0ption/Alt. 1 Option/Alt. 2 Option/Alt 3 Option/Alt. 4 (VS reduction) _ (40-day bench) (30-day bench) (Spec. 02 uptake) Option/Alt 5 Option/Alt. 6 Option/Alt 7 Option/Alt 8 (14-DayAeroblc) (AlkStabiltzation) (Drying —Stable) (Drying —Unstable) Option/Alt 9 Option/Alt 10 (Injection) _ (Incorporation) _ No vector attraction reduction alternatives were performed X CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in CFR 503.33/15A NCAC 02T.1107 have not been met" (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that gpalified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Pam Gibbons Wastewater Treatment Plant Supervisor � Fr ter a and 'tie type or print) I- JWate Signature of Pre er* Land Applier Name and Title (if applicable) (type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) Cameron Testing Services, Inc. Laboratory Report -x Oak' Synagro 160055 Froj6dt: Dunn VVTP Regulatory Yes I NDENA #664 NC p P HS #37799 VS EPIA#NG01918 Sample- Information .,Sampled:- !T" W. Varner '* ; *� - 01112116 Rqcelvdd• J. Cameron _Rate. 01/1�116 Analyses and Results x as Inalyta. methods -Lab 0 ::s6mPle-1 Result' 0 I- .'-a E- Refer I . D �ince 160055 01 Sludge Gr Fee. Coliform-S <40900 CFUJO 40900 01113116 CSC 9222E) - MF b <41 500 crulg 41500 <43000 Grufa 43000 d <43600 CFUIg 43600 e <42600 crull; 42600 f <41300 cruto 41300 9 <431 00 CFulg 43100 Geornean <42300 160065 01 a Sludge or TS(%) 2.26% % am 01119J16 CSC 25403, G -TS b 2.27% % 0.01 C 2.26% % 0-01 d 2,25% 'A Out e 2.24% % Ul f 2.26% % 001 9 2.240/b 7, 001 Report Review el () 2-6 Lab Director Date 219 S. sleele Str. 0.1919-. -4 24O SarlfbM NC 27330 clids "t,s2t�8"..CoM 219 S. Steele Str. Cameron Testing Services, Inc. Sanford, NC 27330 NCVVVVIGWCert. #654 NCPHHS Cert#37799 US EPA NCO1918 Chain of Custody Page — of — Phone: 919-208-4240 IT Email;t p 06' FSR(k !qkarly',*� ON- Synag ro Xom sarnpjpTemp?" Phone. 3 09-8627 3" TC1 Alp.r." ORg �rlAffivefi 'Xdards's�(Clt�" 284 Boger Rd. A' tate, 'Mocksville, NG.27028 -D 4= Name. Signal K,fl f R, orm V, Cts"t 1W x 00 i i a,.�l id'servathrb�:-W=Unpjd9qryed �B=ltj I an pie M a) E 'o 2 > U -"�2S6j-R=HNO3'q a=�16Y61D;su Mal to "Iff E2 F- 0 d u�:NauH X:�Other,-. I W7? 1 1711 1 R M inceived". I Rush work will require prior approval. Additional charges will apply City of Dunn Lime Log 2016 Site Soil pH I pH Target I Lime Requ Date Applii HA-201-4 6.5 6 0 HA-08-8 6.4 6.0 0 HA-08-9 6.3 6 0 CU-34-1 5.7 6 1 CU-34-2 5.9 6 0.5 CU-34-3 5.7 6 1 CU-34-4 6 6 0 CU-34-5 5.7 6 1 * Lime to applied at a later date. d NC.�:_: DABCS I fjmic Division Phone: (919) 733.2665 Website: www.ni':,Z.ovlagronomil Report No. FY1?'?.-_sfJ4151 Client: Chad Hayes . Advisor: Harold Eldridge �,,,•:,uue,, Predictive 273 Pete Strickland Rd 8373 Rhodes Pond Rd 7 Cerro Gordo, NC 28430 Dunn, NC 28334 T •.F' Soil Report Mehlich-3 Extraction Nei'\'IIRN1r'• Sampled County: Cumberland Sampled: 08/31/2016 Received: 09/07/2016 completed: 09/19/2016 Farm: CU34 Links to Helpful Information Sample ID: 1 Recommendations: Lime Nutrients (Ib/acre) More Crop (tonslacre) N P205 K20 Mg S Mn Zn -Cu B Information Lime History: 1-Fescue/OGrassrrim, E 1.6 50-70 0 10 0 0 0 0 0 0 Note: 12 2-Fescue/OGrassrrim, M 0.0 120-200 0 50 0 0 0 0 0 0 Note: 12 Test Results [units - WN in glcrrP; CEC and Na in meq/100 cO; NOa-N in mg/drrP]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-1 Zn-AI Cu-1 Na ESP SS-1 NO3-N 1.08 1.21 8.5 79 1.8 5.7 202 44 55 21. 45 66 49 57 360 360 208 0.0 Sample ID: 2 Recommendations: Lime Nutrients (lb/acre) More Crop (tonslacre) N P20e K20 Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrass/Tim, E 1.3 50-70 0 20 0 0 0 0 0 0 Note: 12 2-FescuelOGrass[Tim, M , 0.0 120-200 0 50 0 0 0 0 0 0 Note: 12 Test Results [units - WN in g/crrr?; CEC and Na in meq/100 crrrl; NOa-N in mg/dO]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NOa-N 0.56 1.21 9.5 84 1.5 5.9 215 42 55 ' 27 40 113 77 85 478 478 145 0.0 Sample ID: 3 Recommendations: Lime Nutrients (lb/acre) More Crop (tonslacre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1-FescuelOGrass/Tlm, E 1.6 50-70 0 0 0 A 0 0 0 0 Note: 12 2-Fescue/OGrass/Tm,M 0.0 12o-200 0 20 0 0 0 0 0 0 Note: 12 Test Results [units - WN in g/cO; CEC and Na in meq/100 cO; NOa-N in mgldO]: Soil class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NOa-N 1.49 1.13 9.1 80 1.8 5.7 195 66 54 22 57 48 38 46 320 320 201 0.0 ' North Carolina 41 \^ rnbacca 7rwr Fuel Cmnnnssion Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. Steve Trox NCDA&CS A :_:fcmic Division Phone: (919) 733-2665 Website: www.nLL Gov/agronomi/ Report No. FY1 i%-,__:,?4151 Chad Hayes Page 2 of 3 Sample ID: 4 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P206 K20 'Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, E 1.3 50-70 D 0 0 0 0 0 0 0 Note: 12 2 -Fescue/OGrass[Tim, M 0.0 120-200 0 40 0 0 0 0 0 D Note: 12 Test Results [units - WN in g/crrf; CEC and Na in meq/100 crrrl; N63-N in mg/drrr3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% 3-1 Mn-1 Mn-All Mn-Al2 Zn-1 Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.46 1.22 7.3 79 1.6 6.0 244 49 48 28 86 61 46 54 303 303 . 326 0.1 1 Sample ID: 5 .Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, E 1.7 50-70 0 40 0 0 0 0 0 0 Note: 12 2 -Fescue/OGrass/Tim, M 0.0 120-200 0 80 0 0 0 0 0 0 Note:12 Test Results [units - WN in g1crrt3; CEC and Na in meg1100 crrP; NO3-N in mgld0]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.71 1.27 6.8 72 1.9 5.7 192 30 49 20 50 76 55 63 396 396 196 0.1 1 NCDA&CS A.'_�.., mic Division Phone: (919) 733-2655 Website: www.nLt,_.il�.Dv/agronomi/ Report No. :FYI i Chad Hayes Page 3 of 3 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either tonlacre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at time, even if the report recommends more. You can apply the rest in similar increments every six months until the full r is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-I and P-1 values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit ncagr.gov/agronomi/pubs.htm. Report Abbreviations Ac B BS% Ca% CEC Cu-1 ESP HM% K-1 K20 Mg% MIN Mn Mn-All Mn.Al2 Mn4 M-O N Na NO3-N ORG Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find pH the exact fertilizer grade recommended on the report, visit www.ncadr.00v/aoronomi/oboarta.htrmMsfnd information that P-1 may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P206 S-1 Test Results SS-1 WN The first seven values [soil class, HM%, WIV, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn Zn•I remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AP, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routine) available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncaor.00v/aoronomi/uvrst.htm I exchangeable acidity boron • CEC occupied by basic cations • CEC occupied by, calcium cation exchange capacity copper index exchangeable sodium percent percent humic matter potassium index potash % CEC occupied by, magnesium mineral soil class manganese Mn-availability index for crop 1 Mn-availability indek for crop 2 manganese index mineral -organic soil,class nitrogen sodium nitrate nitrogen , ' organic soil class current soil pH phosphorus index phosphate sulfur index soluble salt index weight per volume zinc availability index zinc index NCDA&CS Division Phone: (919) 733-2655 Website: ;v nk�".-.�ov/agronomi/ Report No. FY`1i'�ae,,4805 Client: Chad Hayes Advisor: Harold Dixon Predictive 273 Pete Strickland Rd PO Box 849 ? , a Cerro Gordo, NC 28430 Coats, NC127521 Soil Report Mehlich-3 Extraction Sampled County: Harnett -HX'veAH+"� Sampled; 11/09/2016 Recolvod: 11/14/2016 Completed: 12/06/2016 Farm: HA-08 Links to Helpful Informatlon Sample ID: 08-08 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Small Grain (SG) 0.0 80-100 0 110 25 0 0 0 0 0 Note: 3 2- Test Results [units - WN in gled; CEC and Na in meq/100 crr?; NO3-N in mg/dr ft Soil Class: Mineral 1 HM% WN CEC BS% Ac pH P-1 K4 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-1 Zn-AI Cu4 Na ESP SS -I NO3-N 0.32 1.37 6.6 88 0.8 6.4 367 17 82 5 34 126 80 245 245 113 0.1 21 Sample ID: 08-09 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O6 K2O Mg S Mn Zn. Cu B Information Lime History: 1-Bermuda hay/past., M 0.0 180-220 0 170 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in g/cO; CEC and Na in meq/100 cmil; NO3-N in mgldnP]: Soil Class: Mineral HM% WN CEC BS%o Ac pH P-1 K-1 Ca% Mg% 8-1 Mn-1 Mn-All Mn-Al2 Zn-I Zn-AI Cu.] Na ESP SS-1 NO3-N 0.41 1.31 10.6 86 1.4 6.3 620 28 78 7 46 148 101 565 565 276 0.1 11 North Carolina Tolucce 7ru>t fund ConmOsylrn+ Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. 1 Steve Trox \ t NCDABCS A.._.._mic Division Phone: (919) 733.2655 Website: www.mt& : 4)v/agronomi/ Report No. FY17' __ nA605 Chad Hayes Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at one Ca% % CEC occupied byi calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed,. use dolomitric lime. Cu-I copper ca PP index I ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-1 potassium index Ib/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by, magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1Mn-AI2 Mn-availability index for crop 2 Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mn•I manganese indexM-0 mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft, If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit wwwncaaraov/aoronomi/obnart4.htmttfsind information that P-1 phosphorus index I may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P206 phosphate S-1 sulfur index Test Results SS-1 soluble salt index f W/V weight per volume l The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-I zinc availability index remaining 16 JP -I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP; SS -I, NO3-N (not routine) Zn•1 zinc index i available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncaor.gov/aaronomi/uvrst.htm Page 1 of 2 � Report Number: 16-090-0632 Account Number:46789 Send To: SYNAGRO CENTRAL LLC/DUNN MARY BREWER 284 BOGER RD MOCKSVILLE NC 27028 Wa Ol��n� 7621 Wh(tepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com "Every acre... Every year Grower: RONNIE HAMILTON CITY OF DUNN Submitted By: CREIGHTON BROWN Farm ID: HA-201 i SOIL ANALYSIS REPORT AnalyticalMethod(s): Mehlich3 Umelndex LossOnlgnlfion WaterpH Date Received: 03/30/2016 Date Of Analysis: 03/3112016 Date Of Report: 04/0112016 OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab Field ID Number e/s .Soil ibs/A M3 K M 9 Ca Na Soil Buffer H Rate class ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate porn Rate ppm Rate PH Index meg1100g meg1100g HA-201-4 3.5 34 M 112 M 216 VH 656 M 10.4 02623 112 14 VL 6.5 5.8 MIN 4 M NC=28 N( Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride AluminumSample ID - Feld ID K Mg Ca Na H N%N S Zn Mn Fe Cu B SS CI Al % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate mslcm Rate ppm Rate ppm HA-201-4 11 L 3.2 M 221 VH 2.0 H 5.0 31.0 56.6 1.0 6.9 177 VH 0.3 VL 0.14 VL 4 NC=23 NC=60.0 NC=1381. NO=100.0 Values on this report represent the plant available nutrients In the sell. Rating after each value: VL (Very Low), L (Low), M (Medium), H (High), VH (Very High). ENR-Estimated Nitrogen Release. C.E.C. - Callon Exchange Capacity. Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a (pounds per acre), ms/cm(mllll-mhos per centimeter), meq/100g maximim of thirty days after testing. (mllll-equivalent per 100 grams). Conversions: ppm x 2=lbs/A, Soluble gnalyele prepared by: WaypolmAnalyucal MMinia, Inc. Salts ms/cm x 840 = ppm. by Pow,,mp i10- Pauric McGroary Page 2of2 'Report Number: 16-090-0632 Account Number:46789 Send To: SYNAGRO CENTRAL LLC/DUNN MARY BREWER 284 BOGER RD MOCKSVILLE NC 27028 Date Received: 03/30/2016 Date Of Report: 04/01/2016 Waypoint_ ANALYTICAL "Every acre... Every year. "TM Submitted By: CREIGHTON BROWN Farm ID: HA-201 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical.com Grower: RONNIE HAMILTON CITY OF DUNN SOIL FERTILITY RECOMMENDATIONS IJ Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron (Copper Boron Sample ID Intended Crop Yield Goal Lime N P206 K20 Mg S Zn Mn Fe - Cu B Field ID bu Tons/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A HA-201 4 Com 125 0.0 153 55 40 0 20 0 0 0 0 1.4 4 HA-201-4 AdJusl pH to 6.0 0 0.0 0 0 0 4 Comments: 'The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or Implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company In any advertising, news release, or other public anouncements without obtaining our pdorwdtten authorintlon. Copy dghl 1977. Pauric McGroary