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HomeMy WebLinkAboutNCG070117_2024 DMR_20240327 E +. N o c c.,...w o 7' co b b ^.A ca O C., M C = O I w N • c1 }. W �.y. o ? z p G n N O 0 W. cCX N W TA E '> o fYi Z C r`�A a' x 'q' 0 ¢ a, w W ,...- L., A w o o~ f F . W u c-, ^ L ¢ v O M O U .� L.. W Q C G - U u E co a p" aL � a � OC O A y > Z CZ cu O AC U oa u ,-j 0 Z d c Li, a ,au:12„ Ctr Ox Uc4 0 0 0 0 0 W U L � U a c4 I E o f r/� r/� E L "' F U O `' vD C -o A ~ o a n � n xEwrh] a o U QF a¢ Zvi ." C.) ZO . CA x w U 0 CA C c U Ail F C _ WO aA � U o. F o , in — 'm een 3 0 o m 0 0 :. E de .0 x e � _ O a .a 0 F a 0 rn 0 in cA " = � � J w uaicri co _ w h Q <n a C CA o .� r ZZ C.. ,., 17 .E Jwcn Fx .E "- w E- g .° CC a e Z2Q y .= QQ 0 e o rY `.� ZZ 0 o0W a w v 0 E o a o U o "E. fa, C7 o Z W d. L � F w •m .t•= ° `. o a .. o o a u o w ¢ �- x v v ¢ x N N > u U 0 ° cla - mLoo M ^O° _ . L. i u Ti u C7 � 10 .00 Cl) •Oa+ E = o o ,Op '' .+u Z wWm Av U E a � AvnU E L, a Q u a. 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I� py o O a o o C ,o ►�i N CO .+ C .+ = Ob 3 1C .0 O ✓ C L O C L v, m y 4., z o oW• � o ZWE � c � R .p .0 aCi E V .. el. a> u d y 7 C y a W al 0 > w O > .ui i, L ar u • L1FW Z.. AFW _ H oa 0 Cl) ROY COOPER g y r: Grvrrner t [, /O ELIZABETH S.BISER :\ _ � ` •;y Srcr.:ory •i a6^�a, DOUGLAS R.ANSEL NORTH CAROLINA Mnrrrrm Dir.'rtar Environmental Quality Stormwater Delegation of Signature Authority Form (DOSA) This form shall be used to delegate signature authority from the permit Owner (Permittee) to another party. Only the Responsible Official defined below may submit permit applications and reports required by the permit(such as Data Monitoring Reports and Annual Reports) until this form is completed and submitted to the DEMLR Stormwater Program. Please note that delegating s nature authority does not relieve the Permit Owner from the responsibili andty compliance for permit compliance. Permit Owner:The legal entity to which/whom a permit has been issued and may be an individual or an organization such as a company or government agency. Every Owner is required to have a Responsible Official who meets the legal signature authority requirements in 40 CFR 122.22, summarized below: • Fora corporation,the Responsible Official shall bea president,secretary,treasurer,or vice president in charge of a principal business function,or another individual who performs similar functions for the corporation,or the manager of one or more manufacturing,production,or operating facilities who is authorized to make management decisions about the facility operation. • For a partnership or sole proprietorship,the Responsible Official shall be a general partner or the proprietor,respectively;or • For a municipality,State,Federal,or other public agency,the Responsible Official shall be either a principal executive officer[City/County Manager]or ranking elected official[Mayor]. Please mail the DOSA Form with original wet signatures to: NCDEMLRStormwater Program, 1612 MSC,Raleigh, NC 27699-1612 Name of Organizational Entity L L`12, rmit.g.tf.4-ne!JP'l_y i i4C • Responsible Official Name Rini N1 HO( T6i.) Responsible Official Title: PLANT- D'iP\l\lg4%2 Email Address: Phone • KEv IN)• o(ai (c•)kV0(Et A,(c,M ( 5 )2443-6(,35 Mailing Address iC 0 1:k1b0:-SiP.IAl. PA(ZV- (fib 14E10.6050N1/IIlpC.207 City State Zip code NE!�D2-t ' ViLL NC 267gi( --�1 North Carolina Department of Environmental Quality 1 Division of Energy.Mineral and Land Resources DE -;) 512 North Salisbury Strccl 11612 Mail Service Ccntcr 1 Raleigh.North Carolina 276 -1612 ...v.........el r.»7..+.o.wr 019.i 07.9200 A. Persons to Receive Signature Authority The signatures of the persons listed below indicates their acceptance of signatory authority. Attach additional pages if you need more space. Delegated Party Name 1J1�1Py1� I(Cf.UJA�� Delegated Party Title S4 ENS r N�tv'at,t5 i Permit Number(s) f�iCC jC 7GGCL Email Address: 011,17-►, , Y , Phone l<.crJr„AP c� l`voC,E('a:Cvr� ZA 573 )G i y Mailing Address LC., �!�;J.•��i1�iAi QA�k 12.b • City HENJ6 Lp.s6i.) t State AIL Zip code Z"•Z-1 Signature of Delegated Party indicating acceptance of Signatory Authority: ' �✓i<<%� Date GJ - i L(-ZH Delegated Party Name DCV (N-L_1DA2.5 Delegated Party Title a12 CI-1 . 5 GCNI 21.czqLIST- Permit Number(s) I\<1 G•7ooc0 Email Address: n �, nG .-UCi tAS• I 'IC �A LS _ yOcEaccA Phone (�26;)4-15 8.5-6 S Mailing Address ICC 11-Nibv61ia1L\L pAta �i City State Zipcode eNIJf.lSGh1Y1\-L l�� Z� r 1I Signature of Delegated Party indicating acceptance of Signatory Authority: . � L ]`� • Date 03 1L-1 -Z--I Delegated Party Name Delegated Party Title Permit Number(s) Email Address: Phone Mailing Address City State Zip code Signature of Delegated Party indicating acceptance of Signatory Authority: Date Stormwater Permit Delegation of Signatory Authority Form Page 2 B. Responsible Official Signature The Responsible Official,as identified in accordance with 40 CFR 122.22, is the appropriate individual with the authorityto sign and submit reports for the organization. As the Responsible Official,I, KEVIN) I-I-LT1 c;kk (printed name), have the authorityto enter into this Agreement for . (Owner/Organization Name). I request that the DEMLR Stormwater Program include the persons listed in Part A of this form signatory authority for the above-named permit. I acknowledge that I,and the persons listed in Part A of this form work at/for my organization and have authorityto act as a signatory for purposes of the NCDEQ's electronic document systems. By submitting this application,I, Kc V i'v 4Dli (printed name),have read, understand,and accept the terms and conditions of the stormwaterpermit(s)for which I am the Responsible Official. Responsible Official Signature Title Date Stormwater Permit Delegation of Signatory Authority Form Page 3 CD 0 m c c v � __ � o 0 3 0 a a .0 0 . E. - d d O n O- ^ rD, N, 2 o < O rJ -O L c c c 3 -i c =. a o ro r ro 3 0 - a v .. N. ro rP ^, n m 9, O a 0 -' O 3 n !p no z C' rn o N 9 < < _ C a a. o !" 0 u p H O (� an O a 3 cn v v 0' Cp 0 0 0 m O N a .. 0 g . z 3 3 3 - p _ v E o o m _ toro \ ii t I H j -. - , •O a 0 N r' J a N o o Et • T , -< D. O -c a r- F o a -- z x ro o ° O D, D p v 3 �' ac .� n Qa rD "- ni 0 m , r n 0 y < a w o 7 " n 0 6 T1 a m 3 a s m o m m a a < .0 o f 1 0 0 .. o-\ -, m z.c c — a 0 n io " .— 3 _ 0 P rD !I., a 7 ro �, a0 0 n 1• - A tp !D ra c= p m ro �3 O r^p O N G) a ` p r Gl ° 3 — o v a `—< a = o c_ D -< 3 rD 1 �, '- p C a .' O O D (17 c a n a o_ SiN p — C CU FIT 3 0 - < C o - •n p o •� C O _- rD a O m ,y. 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C w 3 n o 0 0 0 3' ro LA r 0 C. > 7 0 fn 0 rt rr rn rO a �- N r o O o O a Cp K 0 0 0 r Z rt'O CD <rt a 1-•7 r a7 3 y N m o w 31000 v `•• CD n oonar•O r ornam m _'m= : T 0 0 7 v 3 'O V1 7 rD 0 r a 0 < r ID rt 7 rt n O� rD W R R to r-a CD N G to a c 'V CD -- O 0 \ OT 3 p r r r ip n r4 M c r 0 a 3 rr rt rt 0• 3 x_ p 0 •+ n -1 2X > 1 O r a O 7 O 0 (D 0C to rD 'D 3 Z 3 0 3 m D o tr o r n o n N ID t 0 3_ Z ttt n CD 3 x, 3 N r ro r 0 7 CD n 2.�„ r fD m m is 1m 0 roc n c -< O ^ < r, 3 'p n r1D 7 nr• 'O ron \ 7 3 3 Z rp < C 2 rr to ID rr 0 't (D rD n a ro rD a d N O 0 t fD 0 D) r 0 D_ 0. 1 p f' 5 .. K Q' rD 7 K r Pi 3 T3 m rD T x d rD ro 7 rt a r• 0 co 3 D, ro 0 n o v O -0 -< U c n p rr rt 6 O M a D " o O ,p < K K K K K K K K K K K K K !• 0 Z Z Z ZZIZZZZZZZZ E z ro z z z z z z z z z z z z z Z Z a a, a. o., a 7 a,7 a a, a, a, 9 D R n n D Pace Analytical Services,LLC Pace2225 Riverside Dr. Asheville,NC 28804 (828)254-7176 March 13, 2024 Mr. Doug McDaris Kyocera Engineered Ceramics 100 Industrial Park Rd. Mountain Home, NC 28758 RE: Project: Stormwater Pace Project No.: 92717411 Dear Mr. McDaris: Enclosed are the analytical results for sample(s)received by the laboratory on March 06,2024. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services-Asheville If you have any questions concerning this report, please feel free to contact me. Sincerely, • Jonathan W Biddix jonathan.biddix@pacelabs.com 704-977-0978 Project Manager Enclosures Q ACCR f�. REPORT OF LABORATORY ANALYSIS TNI ' This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 1 of 10 8QRA Pace Analytical Services,LLC ( ! 'ace 2225 Riverside Dr. Asheville,NC 28804 (828)254-7176 CERTIFICATIONS Project: Stormwater Pace Project No.: 92717411 Pace Analytical Services Asheville 2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030 Florida/NELAP Certification#:E87648 South Carolina Certification#:99030001 North Carolina Drinking Water Certification#:37712 VirginiaNELAP Certification#:460222 North Carolina Wastewater Certification#:40 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 2 of 10 Pace Analytical Services,LLC 2225 Riverside Dr. gace• Asheville,NC 28804 (828)254-7176 SAMPLE ANALYTE COUNT Project: Stormwater Pace Project No.: 92717411 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92717411001 OUTFALL 1 SM 2540D-2015 JMH1 1 PASI-A 92717411002 OUTFALL 2 SM 2540D-2015 JMH1 1 PASI-A PASI-A=Pace Analytical Services-Asheville REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services.LLC. Page 3 of 10 Pace Analytical Services,LLC ace 2225 Riverside Dr. Asheville,NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Stormwater Pace Project No.: 92717411 Sample: OUTFALL 1 Lab ID: 92717411001 Collected: 03/06/24 08:05 Received: 03/06/24 16:00 Matrix:Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method:SM 2540D-2015 Pace Analytical Services-Asheville Total Suspended Solids 18.9 mg/L 2.5 1 03/12/24 12:49 Sample: OUTFALL 2 Lab ID: 92717411002 Collected: 03/06/24 08:11 Received: 03/06/24 16:00 Matrix:Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method:SM 2540D-2015 Pace Analytical Services-Asheville Total Suspended Solids 16.9 mg/L 2.5 1 03/12/24 12:49 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/13/2024 02:10 PM without the written consent of Pace Analytical Services,LLC. Page 4 of 10 Pace Analytical Services,LLC 2225 Riverside Dr. aV//'_�a Asheville,NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92717411 QC Batch: 838323 Analysis Method: SM 2540D-2015 QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92717411001,92717411002 METHOD BLANK: 4330269 Matrix: Water Associated Lab Samples: 92717411001,92717411002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 03/12/24 12:46 LABORATORY CONTROL SAMPLE: 4330270 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Total Suspended Solids mg/L 250 254 102 90-110 SAMPLE DUPLICATE: 4330722 92717333001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 1480 1220 19 SAMPLE DUPLICATE: 4330723 92717355001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 2680 2580 4 Results presented on this page are In the units Indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/13/2024 02:10 PM without the written consent of Pace Analytical Services,LLC. Page 5 of 10 Pace Analytical Services,LLC Pace 2225 Riverside Dr. Asheville,NC 28804 (828)254-7176 QUALIFIERS Project: Stormwater Pace Project No.: 92717411 DEFINITIONS DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot. ND-Not Detected at or above adjusted reporting limit. TNTC-Too Numerous To Count J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL-Practical Quantitation Limit. RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S-Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is a combined concentration. Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values. LCS(D)-Laboratory Control Sample(Duplicate) MS(D)-Matrix Spike(Duplicate) DUP-Sample Duplicate RPD-Relative Percent Difference NC-Not Calculable. SG-Silica Gel-Clean-Up U-Indicates the compound was analyzed for,but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as "Total"may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI-The NELAC Institute. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/13/2024 02:10 PM without the written consent of Pace Analytical Services,LLC. Page 6 of 10 Pace Analytical Services,LLC 2225 Riverside Dr. ace Asheville,NC 28804 (828)254-7176 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Stormwater Pace Project No.: 92717411 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92717411001 OUTFALL 1 SM 2540D-2015 838323 9271 7411 0 02 OUTFALL 2 SM 2540D-2015 838323 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/13/2024 02:10 PM without the written consent of Pace Analytical Services,LLC. Page 7 of 10 - - - , n^ 0 n g n n m v n�n n c v 0 0 3 s /1 c o n a o i� / 0 ro i•' n r? n cor N l! N a v ° JJ 3 a Crn v a a < < a < 3 3 � N n �F �N p c — g °!fltl H I .� 1 l0 lam o c, c � 1 3 3 �`\. ti W 2 !A Z J IS C C O I I p Y C ^N 0 . ��Z \ G a ._/ p O �r33, _ V1 O C ti i] n n — 3 rn = D j ,,,— 3 o o i o u _ � f� n ao - n m O 0 o a .>i�g) 3 v a o n -Ti 1 -1 I _i z 9 --I lf1 p n a �, CC N° x- oo 6' o o n r� n a Z C C 3 ,- �; S ro ° (� ° a o G1 O _ o n Gi 0 �� 3 -�No n o? c �o = ° J• —< ° o D 1 3 A c 00 ^ n. o oR. p , 'o 0 ... -i — Z c - n •., H C 1, N41ra ` 0 o n 2 -< n v z - 73 j- ;' n v < c o ^ o < :. : : 7,, n ° 3 5 C o m n n n o O F a �' o � n 3 3 3 n _ — F a - 3 m' ffe- s Z 0 ` a Na — rD c c c n' m 0 n = rr Z N a D u 3 3 v 3 n 3 = o p > CoU c' o_ .O /•‘) O V� C m y -I El 1 3 _ C -�b ` N xm -_ , n D \) X n p J - o o C Os � ---------.33 <• cr. Oin O a nC C v a 3 Cna N < m u N v� \ n IU i .- � 5n -0 ►+ C> ^- S ? a � p a o -o -1 D -I !I .)^ O a a E -I r • • 3 n 3 .^. rli ( I ' 3 �_ _ 3 Cr n 0 m irste v 7 ro o TT a •• J N C x 3 fi C V/ n p . . — pp aa Pal n z x C Eli o n g — c n u -< rr rmro v,n -•vc <v,mmm�nn ro' a na v Cv y n C S G r'n SC� CC°N G O r, O C C u Q 01 G 1-' 3 'f. S p y .T M R I-'C CC 7 N a 0 �V a ntoV fn r.'o 7 C- I-,h r. r0 n o O 0 C: r,n h'n a r I r'r•n C n O o0 o , o 5' 3 Cl n n Y•n r-CJ CC n^• " Ln'.rt n n`<'< 3 - -. O °. Nro n ro ro ro . Si ri n 0 ro ^ a OZ cr= n n n n -I -I Q (D Z C n'- Sv.•• n C CC•'OO.ID rrf O .+H -CD r _' 0 C 2 c n - o 0 0 o = o , r rt n r C a m n C rCC(I C ° ' 0 -< n 3 0 0 o m 3 6_ J x,< n C n C-'5 ro n <n c r A �- (C s d m o W !a N TT v 3 •• CD n 0 0 0 C r•O I-'n,o Cc T, n m a !T 0 v 3 3 ro Eno n '-, ran < r'nno rt n S. ,,. �.-. r,. co .y rt rt 'O r•0. n n G N G C 'C n i •1 0 c 0 o c ^ J n n rt C r•CC a B n n 'l r 3 ro n -i -I 0 V o r C n I-n o C n n 3 0 z3 p � '" O C C " - 3 ro c nr.no CCC ° ° 00 0 3 v vm ro , C •- m 'I-CCC n 'CC n c ro CC n roC m n ,��, C m 3 n n h a In 0 3 '" Z a ao o J4 6 _ CC am nay n ' c p p a C nCr ID 0 CC H m u Cr R. n C n C+ r n = CD -< 3 y ro 'y` 5 n n C o - io 0 C `, n rt. 0 co I 0 Z (lam (Z /AZ. Z Z e Z Z .Z Z Z Z Z Z 2 e Zro \3`0, �'Cil0b Y 7 7 7 Wb ``. A' ' c \ ) n n Page 8 of 10 DC# Title: ENV-FRM-HUN1-0083 v03_Sample Condition Upon Receipt ace Effective Date:12/01/2023 Laboratory rec wing samples: Asheville [ Edenn Greenwood n Huntersville❑ Raleigh❑ Mechanicsville❑ Atlanta❑ Kernersvillen Sample Condition Client Name: WO# ' 92717411 y Upon Receipt J.4 r i Project H. i l PM: JWB Due Date: 03/21/24 Courier: ❑Fed Ex ❑UPS ❑USPS ❑Client CLIENT: 93-Kyocera ❑ Commercial []Pace ❑Other: Custody Seal Present? likes g1 o Seals Intact? Oyes No ❑N/A Date/Initials Person Examining Contents: YE'.11 Packing Material: ❑Bubble Wrap ❑Bubble Bags :None Er-Other Biological Tissue Frozen? Thermometer: ❑Yes ❑No ON%A ❑ IR Gun ID: r7-3*ti JL Type of Ice: 1 ❑Blue UNone Correction Factor: Cooler Temp: - Add/Subtract('C) ) __ Temp should he above freezing to 6'C ['Samples out of temp criteria.Samples on ice,coaling process C.i Cooler Temp Corrected(°C): ' . '? has begun USDA Regulated Soil( N/A,water sample) Did samples originate in a quarantine zone within the United States:CA,NY,or SC Did samples originate from a foreign source(internationally, (check m aps)?Dyes ❑No including Hawaii and Puerto Rico)?['Yes ONO _ Comments/Discrepancy: Chain of Custody Present? arcs ONo ON/A _ 1. _ Samples Arrived within Hold Time? Efes ❑No ON/A 2. Short Hold Time Analysis(<72 hr.)? ❑yes .(2ffo ON/A 3. Rush Turn Around Time Requested? ❑Yes Otto ❑N/A rl. Sufficient Volume? }]Yes ONo ON/A S. Correct Containers Used? 'Dies ONo ON/A 6 Pace Containers Used? ,-t,Yes ONo ON/A Containers Intact? ,E s ONo ON/A _ 7. Dissolved analysis:Samples Field Filtered? OYes ONo N/A 8. Sample labels Match COC? fires ONo ON/A 9 -Includes Date/Time/ID/Analysis Matrix: Heaclspace in VOA Vials(>5-6mm}? Des ONo v/A 10. Trip Blank Present? Oyes ❑Nu j:IN/A" 11. Trip Blank Custody Seals Present? Oyes ❑No ❑N1st" COMMENTS/SAMPLE DISCREPANCY Field Data Required? Oyes ONo Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Date/Time: Project Manager SCURF Review: Date: _ Project Manager SRF Review: - Date: Page 9 of 10 DC#_Title: ENV-FRM-HUN1-0083 v03_Sample Condition Upon Receipt /Pgce Effective Date: 12/01/2023 *Check mark top half of box if pH and/or dechlorination is verified and Project N WO# : 92717411 within the acceptance range for preservation samples. PM: JWB Due Date: 03/21/24 Exceptions:VOA,Coliforrn,TOC,Oil and Grease,ORO/8015(water)DOC,LLI Ig CLIENT: 93—Kyocera **Bottom half of box is to list number of bottles ***Check all unpreserved Nitrates for chlorine • ^ V C, .r Q V O U d a a rn N z z z - ._ n z N a z m N rn *ail, o —. r•, �+ Z ri = o /- V lJ z _ I ai v ` S U TSl el w hi n w = v v Z Z t\ rl m ,ry vi y 40. :5m O p =O N c� a a NO iJ .. p cl a i '-' iv o > v iccn j > j 2 7 S 7 2 'Dv c 0 7 0 = = N n n0- n > 2 a z _7 0 c 7 2 Z v Ls -> u u r� Scy, V c m 7 ,^, u •a) m D n nn .- -- r E .... n n n a N a n a a ° E E. E E E E O p O O n d 0., c`, 9 Q . is a E Q a , a , •S > > > > G a ,n .n a N j E E E a E E E E v v of 6v E E E E F E E io E E E E E E Q ,O ry r! i . .� N O Q q D O p r N O O O 1 3 7 3 3 ,A Z rJ m LL 7 = 3 Vr VI O S t- ] > 3 Y F t- ce 7 7 D E . r gN .'� Y. T. Q V t ri r1 rT .Y rn as as as as as n V' T. V. m O w as xi a. a. a a a a a a t7 SD t7 SD t7 SD (7 ID SD a. \ a a a t9 N I m m m m 111 3 a a a a a o o > > o Y > v, v, m a > o 1 \ 2 \ \ \ .\\ \ \ 3 \4 \ \ 1„,\\\. — — \\ — \\ C - - I .1-- - I,\\\\\ "Iiii1lo1, — — -- - \\ i \\\\ \, —i-- — —� 4 \-1 8 \ (- \- — —\ —— 16 \ - r \.- , — — -- 0. '\\.\\\\.\\ _ L____ 12 \ I 1 ' Ilk. pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Dale preservation adjusted Time preservation Amount of Preservative Lot 1I adjusted added Note: Whenever there is a discrepancy affertinp North Carolina compliance samples,a ropy of this form will be sent to the North Carolina DEAR Certification Office(lc. Out of hold,incorrect preservative,nut of temp,incorrect containers. Page 10 of 10