WQ0000601_GW Monitoring_20091221

CSK
TRANSPORTATION
Jerry L. Cato REM
Supervisor Environtnental Control
North Carolina Department
Of Natural Resources
Attn: Information Processing Unit
Division Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Dear Sir or Madam:
l
.a '1
Jrt;y J ft .. ,Jt
500 Water Street- J275
Jacksonville, FL 32202
)359-3457
(FAX)904) 245-2927
December 21, 2009
File. 9613703
Permit No. W00000601 Richmond County
CSX Transportation Inc (CSXT) Hamlet NC
Attached in triplicate, is the third triennial 2009 Ground Water Monitoring Well
Analyses, Form GW-59A and Attachment A — WWTF discharge report, as specified by
Condition 4 of the referenced permit. Due to the drought conditions at this location, monitoring
well No. 1, No. 2, No. 3, and No. '7 did not have enough water to collect a sample. Flow and
Nitrogen, Nitrate Total (as,N) for Attachment A, will be sent under separate cover.
If you have any questions or comments, please contact me at (904). 359-3457.
Sincerely, „ Q_
Jerry L. Cato
Enclosures
RECEIVED
DEC 2 9 2009
Information Processing Unit
DWQIBOG

ATTACHMENT A — LIMITATIONS AND MONITORING REQUIREMENTS
PPI001— WWTF Effluent
EFFLUENT CHARACTERISTICS
Parameter Description — Parameter Code
Flow, in conduit or thru treatment plant— 50050
Solids, Total Dissolved- 180 Deg.C— 70300
pH — 00400
Carbon, Total Organic (TOC) — 00680
Nitrogen, Nitrate Total (as N) — 00620
Barium, Total (as Ba) — 01007
Cadmium, Total (as Cd) — 01027
Chromium, Total (as Cr)— 01034
Lead. Total (as Ph) — 01051
Arsenic, Total (as As) —01002
EFFLUENT LIMITS
Monthly Average Weekly Average
1.0 1 mgd
3 X year monitoring shall be conducted in March, July and November.
W00000601 Version 3.0
Attachment A
Permit Number:
W 0000601
Q
Version:: 3.0
-44,
MONITORING REQUIREMENTS
Daily Maximum
Monitoring Frequency
Sample Type
,
Continuous
Recorder
t
LZO
L.
3Xyear
Grab
`•i
Su
3 Xyear
Grab
q•J�
L
3Xyear
Grab
3 X year
Grab
_Ole
L:
3Xyear
Gmti
=0.
3 Xyear
Grab
0.01
6
3 X year
Grab
a-0 1'
L
3 X year
Grab
O • �.`i
L
3 X year
Grab
Page I of 1

/ GW-59A COMPLIANCE REPORT FORM Permit # OOOOG 0�
l (Snhml one each monitoring period with Gi{=59 jornnt.)
1 ...„y .a.",u vu.v uuu. t W, ew-y7 vvui tins monitoring report (GW-59 an4GW.59A)
be submitted after the established due date?
NO
v2
/�IF
Was any required Information missing on the GW'-59 report forms?
the answer to question 1 or 2 is "YES" list in the space provided below the well identification nu
explain the problems encountered in obtaining the required information.
3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES
NO
Identification plate, area overgrown, etc.)? If the answer is "Y'es• ", contact the Regional Office jorguidance.
V
/�
4 Are any monitored constituents equal to or above the established standards?
YES
If the answer to question 4 is NO" skip to section B.
If the answer to question 41s "YES"list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the space provided below.,
5 For the constituents identified In question 4 above, have standards been exceeded previously for the YES
NO
same constituents) in the same well(s) in the last two years?
if the answer to question 5 is NO" skip to section B.
if the answer to question 51s "YES", list in the space provided below, each well with constituents) exceeding
standards, concentrations) reported, and sample collection date for each occurrence (for the last two years).
6
Are the monitoring wells listed In section 5located at or beyond the review boundary? YES NO
If the answer is "YES", a groundwater quality problem maybe occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer Is 'NO", monitoring wells may be Improperly
located; contact the Regional Office.
7
Is the permittee Implementing previously approved actions required by the Division involving this YES NO
groundwater quality problem?
nswer to question 7 is "YES" describe those actions in the space provided below.
nswer to quest/on 71s "NO", contact the Regional Office within 90 days• an evaluation may be
d to determine the Impact the waste disposal system Is having at the review and compliance
aries surroundlnq this facility, Failure to do so may sublect the permittee to a Notice of Violation
Tbnda
nd/orpenaltles.
rson completing this portion (GW-59A) of the monitoring report should sign below and submit this
ith GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
acknowled a tha he above Iriformti{Ion was valadand theTnformationxsubm1tte87n this �
none rt W 59A) Is.true and complete to the best of my knowledge �'�� : t
,r
Signature of P it ee (or A horized Agent) Dale
GW-59A 12/8/2003

Facility Name CSX Transportation - Hamlet Wastewater Treatment Facility
Facilty Address 173 CSX Dnve
Hamlet, NC 28345
Contact Person: MIKE GREGORY
County Richmond
Well LocatioNSity Name: see location map_Telephone #: [phone]
No. of Wells to be Sampled:
_
8
Well Identification Number (From Permit): Myy_1
For Groundwater Treatment
Well Depth _ 53.75 ft. Well Diameter. 4.0
Screened Interval:
in. Systems
Check One:
fl. to _ ft,
Depth to Water Level ft. below measudn g point.
0 Influent (98)
0 Effluent (99)
Measuring point (M.P.) is: __ft. above land surface
Gallons of water pumped/bailed before
Relative M.P. Elevation inft.:
sampling:
Field Analysis: pH
Date Sample Collected
Specific Conductance
-
uMhos
o
Temp. C Odor _Appearance
PARAMETERS.• (Samples for metals were Collected
unfiltered YES
COD
_X_ NO
Coliform: MF Fecal
_ mg/1
Nitrite (NO2) as N
Coliform: MF Total
/ 100ml
Nitrate (NO3) as N
(Note: Use MPN method for highly turbid
100m1
Phosphorus: Total as P
Dissolved Solids Total
samples)
Orthophosphate
PH (when analyzed) --
mgn
AI -Aluminum
TOC
units
Ba - Barium
Chloride —
mg/I
_
Ca - Calcium
Arsenic --- ---
mg/I
_
Cd - Cadmium
Grease and Oils —
mg/I
_
Chromium: Total
Phenol---_mg/l
_
Cu- Copper
Sulfate - —
mg/I
Fe - Iron
Specific Conductance- -----
—mgn
Hg - Mercury
Total Ammonia ------Mhos
K- Potassium
TKN as N - --
mg/I
_
Mg - Magnesium
__-.._
_ mg/I
_
Mn - Manganese
PERMIT M EXPIRATION DATE: November 30, 2009
Non -Discharge W00000601
UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field Remediation:
Rotary Distributor Land Application 0f Sludge
X Other Monitoring Well
NOTE: Values should reflect dissolved and collaidal concentrations
Date Sample Analyzed /Vp 50.
Laboratory Name: IF
- T4.peq
Certification No. -
and field acidified
_X_ YES NO)
mg/I
Ni - Nickel
mgA
—
Pb - Lead
mg/I
Mg/1
Zn - Zinc
---mgn
mg/I
Ammonia Nitrogen
_mg/I
mg/I
Other (Specify Compounds ) and concentration unit/I
mgA
mgA
-
mg/1
-----
mgA
-- ----
mg/I
mg/I
mg/I
ORGANICS: (GC, GC/MS; HPLC)
(Specify test and method #. Attach lab report)
Report Attached? Yes—(1) No_(0)
VOID method # =
VAC mof6Ad A— ---
E

IAT
ONLY
Facility Name Hamlet Wastewater Treatment Facility
Facilty Address CSX Transportation Box 191A Highway 177N
Hamlet, NC 28345 County Richmond
Contact Person: M. L. GREGORY [phone]
Well LocauoNSity Name: Location Map Attached
Well Identification Number: MW-2 For Gnam"ater Treatment Systems
Well Depth:_-- 4�.48 _ ft Well Diameter: 4_0 In. che.cOne:
Screened Interval ft. To ft. El Influent(98)
Depth to Water Level ft. below measuring 9 Point Effluent
g point is iL above land surface
Gallons of water pumped/bailed before sampling:
Field Analysis pH __ Specific Conductance
Temp. -- C App
° Odor uMhos
earance
PERMIT #: EXPIRATION DATE JUIy 31, 2`14
Non -Discharge W00000601 UIC
NPDES —
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field Remediation __
Rotary Distributor Land Application of Sludge
X Other Monitoring Well
NOTE Values should reflect dissolved and collaidal concentrations
Date Sample Collected Date Sample Analyzed
Laboratory Name ,gory„/�
Certification No. f — N
PARAMETERS• (Samples for metals were collected unfiltered _X
_YES NO
CO
Coliform: MF Fecal
100 1
/m1
C011fonn: MF Total —/
100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids Total
PH (when analyzed)
TOC --------mg/l
units
-----
Chloride
_
Arsenic
mg/l
_ _
-
Grease and Oils
mg/I
_—
Phenol
mg/I
-- -
Sulfate —_--
mgll
_
Specific Conductance
mg/I
Total Ammonia
Mhos
_
TKN as N _----
—/I
mgll
NO_2 as N
NO-3 as N
Phosphorus: Total as P
Orthophosphate
Ai -Aluminum
Be - Barium
Ca - Calcium
Cd - Cadmium
Chromium: Total _
Cu - Copper
Fe Iron
Hg Mercury
K - Potassium
Mg - Magnesium _
Mn - Manganese
and field acidified _X_ YES NO)
m9/1 NI - Nickel m /l
-------
mg/I
Pb - Lead
a
mg/I
Zn - Zinc
_ mg/I
mg/l
Ammonia Nitrogen --
--mg/I
mg/I
Other (Specify Compounds and con
centration units)
mg/l
mg/l
-
mg/l
----
—
ORGANICS: (GC, GC/MS, HPLC)
(Specify test and method #. Attach lab report)
Report Attached?Yes_(1) No_(o)
VOC : method # = _
VOC : methnri a =
DATE

Facility Name Hamlet Wastewater Treatment Facility
Facilty Address CSX Transportation, Box 191A Highway 177N
Hamlet, NC 28345 __ County
Contact Person: M. L. GREGORY (910)5824901
Well Location/Sity Name: Location Man Attached
Well Identification Number: MW-3 For Groundwater TreaMeNSystems
Well Depth:_ 45.70 fL Well Diameter. 4.0 in Che Ona:
Screened Interval _ f . To ft. 0 Influent (98)
Le
Depth to Water vel _ fL below measuring point. El Effluent (99)
Measuring point is _ fL above land surface
Gallons of water Pumpedibailed before sampling:
Field Analysis pH - "Specific Conductance uMhos:
Temp. ° C .Odor Appearance
PARAMETERS: (Samples for metals were collected unfiltered _X_ YES
CO
mg/l
Coliform: MF Fecal
/ 100ml
_
Coliform: MF Total _
/ 100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids Total _
mg/I
PH (when analyzed)
units
TOC
Chloride _
Arsenic
mg�I
mg/I
Grease and Oils
mg/f
Phenol
mg/l
Sulfate
myll
Specific Conductance
Mhos
Total Ammonia
mg/I
TKN as N
m-,r
NO-2 as N
NO-3 as N
Phosphorus: Total as P
PERMIT#: EXPIRATION DATE November 30, 2009
Non -Discharge WQ0000601 UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field Remediation
_ Rotary Distributor Land Application of Sludge
X Other Monitoring Well
NOTE Values should reflect dissolved and collaidal concentrations
Date Sample Collected Date Sample Analyzed
Laboratory Name _(p_
Certification No.
_ NO and field acidified _X_ YES NO)
mg/I 'Ni-Nickel mg/I
mg/I Pb - Lead _ mg/l
mg/I Zn-Zinc Moll
Orthophosphate mg/I
At -Aluminum /1
Be - Barium
Ca - Calcium
Cd - Cadmium _
Chromium: Total
Cu -Copper
Fe - Iron
Hg - Mercury _
K - Potassium
Mg - Magnesium
Mn - Manganese
mg
mg/I
mg/I
mg/I
mg/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and concentration units)
'ORGANICS: (GC, GC/MS, HPLC)
(Specify test and method#. Attach lab report.)
Report Attached? Yes_(1) No_(0)
VOC : method # =
VOC : method#=

ON
PAPER ONL
Facility Name Hamlet Wastewater Treatment Facility
Facllty Address CSX Transportation, Box 191A Highway 177N
Hamlet, NC 28345 County Richmond
Contact Person:M. L. GREGORY [phone]
Well Location/Site Name: Location Map Attached
Well Identification Number: MW-4 For Greundwater Treatment systems
Well Depth: 47.45 ft. Well Diameter. 2.0 In. Cneatone:
Screened Interval ft To fit. D Influent (98)
Depth to Water Level QA fL below measuring point Effluent (99)
Measuring point is fL above land surface
Gallons of water pumped/bailed before sampling:
Field Analysis pH 6.54 Specific Conductance 8:46 uMhos
Temp. °C Odor Appearance
(Samples for metals were collected unfiltered _X_ YES
Co mg8
Colifono: MF Fecal / 100ml
Colifonn; MF Total / 100ml
(Nate: Use MPN method for highly turbid samples)
Dissolved Solids Total
pH (when analyzed)
60. mg/I
units
TOC
_ 0.78 mgfl
Chloride _ moll
Arsenic
Grease and Oils _
Phenol
Sulfate
Specific Conductance
Total Ammonia _
TKN as N
<0.02
Mhos
mgll
mg/I
PERMIT M EXPIRATION DATE_ July 31, 2014
Non -Discharge W00000601 UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field Remediation _
_ Rotary Distributor Land Application of Sludge
X Other Monitoring Well
NOTE Values should reflect dissolved and collaidal concentrations
Date Sample Collected 11/10/09 Date Sample Analyzed
Laboratory Name TestAmenca Laboratories INC
Certification No. 269
NO and field acidified _X_ YES NO)
NO-2 as N
mg/l
NO-3 as N
1.5
mg)]
Phosphorus: Total as P
mg/l
Orthophosphate
mg/l
At - Aluminum
mg/I
Be - Barium
<0.01
mgfl
Ca - Calcium
mge
Cd - Cadmium
<0.005
mg/I
Chromium: Total
<0.01
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mgfl
Mn - Manganese
mg/I
NI - Nickel
mg/l
Pb - Lead <0_01
mg/I
Zn - Zinc
mgfl
Ammonia Nitrogen
mgn
Other .(Specify Compounds and concentration units)
ORGANICS: (GC, GC/MS,.HPLC)
(Specify test and method #. Attach lab report.)
Report Attached?Yes_(1) Nc_(0)
VOC : method # = _
VOC : method # _
can A. Gerhardst , D' or Environmental Systems
' Pe a ul en0 Nam nd Title -Please print or type --
GW-59 Rev. 4/98
ig a re t dtee(orAu orizedAGenO ..._�—

SUBMIT
ONLY
Facility Name Hamlet Wastewater Treatment Facility
Facilty Address CSX Transportation, Box 191A Highway 177N
Hamlet, NC 28345 County Richmond
Contact Person: M. L. GREGORY [phone]
Well Location/Sity Name: _ Location Map Attached
Well Identification Number: MW-5 For Groumhmter Treatment systems
Well Depth: ' 52.92 fL Well Diameter: 2.0 in, check one:
Screened Interval ft. To fL - E Influent(98)
Depth to Water Level 365. ft below measuring point. Effluent(99)
Measuring point is fL above land surface
Gallons of water pumped/bailed before sampling:
Field Analysis pH 5.67 Specific Conductance 1.49. uMhos
Temp. - e C Odor Appearance
PARAMETERS: (Samples for metals were collected unfiltered _X_ YES
CO
Coliform: MF Fecal
/ 100ml
Coliform: MF Total
/ 100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids Total 100.
mg/I
PH (when analyzed)
units
TOC 1.2
mg/I
Chloride
mgfl
Arsenic <0.02
mgfl
Grease and Oils
mg/1
Phenol
mg/I
Sulfate
mg/1
Specific Conductance
Mhos
Total Ammonia
mg/1
TKN as N
mg/I
[phone]
PERMIT M EXPIRATION DATE_ July 31. 2014
Non -Discharge _WC10000601 UIC -'-'
NP,DES ---.
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field _
_ Rotary Distributor x Other Monitoring We11_
Remediation: Infiltration Gallery
Re -mediation
Land Application of Sludge
NOTE Values should reflect dissolved and collaidal concentrations_
Date Sample Collected 11/10/09 Date Sample Analyzed Laboratory Name TestAmerica Laboratories. INC_
Certification No. 269-'' ---- '
NO and field acidified X_ YES
NO_2 as N
mg8
NO_3 as N
2.6
mg/l
Phosphorus: Total as P
mg8
Orthophosphate
mgn
Al - Aluminum
mg/I
Be - Barium
0.022
mgfl
Ca - Calcium
Mgt[
Cd - Cadmium
<0.005
mg/l
Chromium: Total
<0.01
mg/I
Cu - Copper
Fe - Iron
Hg - Mercury _
K -Potassium _
Mg - Magnesium
Mn - Manganese
mg/1
mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
NO)
<0.01
mg/I
Ammonia Nitrogen _mg/l
Other, (Specify Compounds and concentration units)
ORGANICS: (GC, GC/MS, HPLC)
(Specify test and method #. Attach lab report)
Report Attached?Yes_(1) No_(0)
VOC method #
VOC method # _

FORM
ONLY
Facility Name Hamlet Wastewater Treatment Facility
Facilty Address CSX Transportation, Box 191A Highway 177N
Hamlet_ NC_28345 County Richmond
Contact. Person: M. L. GREGORY [phone]
Well Location/Sity Name: Location Mao Attarherl
Well Identification Number: _MW-7 For GreundwaterTreatment Systems
Well Depth: 37.18 fL Well Diameter: 2.0 In, check one:
Screened Interval ft. To ft. DInfluent (98)
Depth to Water Level ft below measuring point Effluent (99)
Measuring point is f . above land surface
Gallons of water pumped/bailed before sampling:
Field Analysis pH Specific Conductance uMhos'
Temp eC Odor Appearance
PARAMETERS:
(Samples for metals were collected unfiltered X_ YES
CO _
mgn
Colifonn: MFFecal
/100m1
COlifond: MF Total
/ 100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids Total _
pH.(when analyzed)
----units
TOC
Chloride
Arsenic __ —
m9�
Grease and Oils _
mg/1
Phenol
mg/l
Sulfate
mgll
Specific Conductance
Mhos
Total Ammonia
mgll
TKN as N
NO-2 as N
NO-3 as N
Phosphorus: Total as P
Orthophosphate
Al -Aluminum
Be -Barium.
PERMIT M EXPIRATION DATE November 30, 2009
Non -Discharge W000o0601 UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
— Spray Field Remediation
Rotary Distributor Land Application of Sludge
O Other Monitoring Well
NOTE Values should reflect dissolved and collaidal concentrations
Date Sample Collected _ Date Sample Analyzed
Laboratory Name Mp(
Certification No.
NO and field acidified _X_ YES . NO)
mg/I NI -Nickel
mg/l Pb -Lead
mg/I Zn -Zinc
mg/I
mg/I
Ca - Calcium
m9/I
Cd -Cadmium
mgn
Chromium: Total
mgfl
Cu -Copper
mg/l
Fe -Iron
mg/1
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mgll
Mn - Manganese
'.., n
mg/1
Ammonia Nitrogen
Other (Specify Compounds and concentration units)
ORGANICS: (GC, GC/MS, HPLC)
(Specify test and method #. Attach lab report.)
Report Attached? Yes _(1) No_(o)
VOC : method#=
VOC : method # =
VOC method # _

FORM
ONLY
Facility Name Hamlet Wastewater Treatment Facility
Facility Address USX Transportation, Box 191A Highway 177N
Hamlet, NC 28345 1 County Richmond
Contact Person: M. L. GREGORY [phone]
Well Location/Sity Name: • Location Map Attached
well Identification Number: MW-8 V ForGmunda terTreamentSystems
Well Depth: 57.18 _fL Well Diameter: 2.0 In. Check One:
Screened Interval tL To ft. influent(98)
Depth to Water Level 358. fL below measuring point. ❑ Effluent (99)
Measuring point is fL above land surface
Gallons of water pumped/bailed before sampling:
Field Analysis pH_ 5.87 Specific Conductance 2.18 uMfios
Temp. ° C Odor Appearance
PARAMETERS: (Samples for metals were collected unfiltered _X_ YES
CO
Colifono: MF Fecal / 100ml
Coliform: MF Total / 100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids Total
pH (when analyzed)
TOC
100. mg/I
units
1.3 mg/I
Chloride
mg/I
Arsenic
Grease and Oils
Phenol
mg/I
Sulfate
mg/l
Specific Conductance
Mhos
Total Ammonia
mg/I
TKN as N
r nif
PERMITM EXPIRATION DATE July 31.2014
Non -Discharge W00000601 UIC
--
NPDES -- __--
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field Remediation . Rotary Distributor Land Applicati_on of Sludge
X Other Monitoring Well
NO
NOTE Values should reflect dissolved and collaidai concentrations
Date Sample Collected 11/10/09 Date Sample Analyzed
Laboratory Name TestAmerica Laboratories, INC
Certification No. 269 --" ----
and field acidified _X_ YES NO)
NO-2 as N
mg/I
NO-3 as N
2.6
mg/I
Phosphorus: Total as P
mg8
Orthophosphate
mg/I
Al - Aluminum
mg/I
Ba - Barium
0.039
moll
Ca - Calcium
mg/1
Cd - Cadmium
<0.005
mg/I
Chromium: Total
<0.01
mg/I
Cu - Copper
Fe - Iron.
Hg-_Mercury _
K - Potassium
Mg —Magnesium
Mn - Manganese
mg/I
N1- Nickel
mg/I
Pb - Lead <0.01
mg/1
Zn -Zinc
mg/l
Ammonia Nitrogen
_mg/l
Other (Specify Compounds and concentration
units)
ORGANICS: (GC, GC/MS, HPLC)
(Specify test and method #. Attach lab report.)
Report Attached? Yes_(1) No_(0)
VOC : method # _
VOC : method # _

TestAmerica
THE LEADER IN ENVIRONMENTAL TESTINC
ANALYTICAL REPORT
Job Number: 680-52521-1
Job Description: CSX Hamlet, NC WWTP
For:
ARCADIS U.S., Inc.
801 Corporate Center Drive
Suite 300
Raleigh, NC 27607-5073
Attention: Mr. Alan Pinnix
AVO�a'e6IDrrBIBd59.
P'.! nSrttiN
Wl
11R`M4e 1026
114Yt00910J6AM
Kathryn Smith
Project Manager I
[e-mail]
11/24/2009
cc: Mr. Jerry Cato
Mr. Mike Gregory
L W ON-E N V0000038652//P roject-9522202
The test results in this report meet NELAP requirements for parameters for which accreditation is required or available.
Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report
may not be reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the
person who signed this report.
Savannah Certifications and ID #s: A2LA: 0399.01; AL: 41450; ARDEQ: 88-0692; ARDOH; CA: 03217CA; CO; CT:
PH0161; DE; FL: E87052; GA: 803; Guam; HI; IL: 200022; IN; IA: 353; KS: E-10322; KY:EPPC: 90084; KY UST;, LA
DEQ: 30690; LA DW LA080008; ME: 2008022; MD: 250; MA: M-GA006; MI: 9925; MS; NFESC: 249; NV: GA00006;
NJ: GA769; NM; NY: 10842; NC DWQ: 269; NC DHHSE 13701; PA: 68-00474; PR: GA00006; RI: LA000244; SC:
98001001; TN: TN0296; TX: T104704185; USEPA: GA00006; VT: VT-87052; VA: 00302: WA; WV DEP: 094; WV
DHHR: 9950 C; WI DNR: 999819810; WY/EPAR8: 8TMS-Q
TestAmerica Laboratories, Inc. 14 Accc
TestAmerica-Savannah 5102 LaRoche Avenue, Savannah, GA 31404 ``'ia,°-�" q�'�
ryc
Tel{912) 354-7858 Fax [phone] www.testameAcainc com u•f
ene .
Page 1 of 20

r
METHOD SUMMARY
Client: ARCADIS U.S., Inc.
Job Number. 680-52521-1
Description
Lab Location
Method Preparation Method
Matrix Water
Metals (ICP)
TAL SAV
40CFR136A 200.7 Rev 4.4
Preparation, Total Metals
TAL SAV
EPA 200.7
Nitrogen, Nitrate -Nitrite
TAL SAV
MCAWW 353.2
Solids, Total Dissolved (TDS)
TAL SAV
SM SM 2540C
Organic Carbon, Total (TOC)
TAL SAV
SM SM 5310E
Lab References:
TAL SAV = TestAmerica Savannah
Method References:
40CFR136A = "Methods for Organic Chemical Analysis of Municipal Industrial Wastewater", 40CFR, Part 136, Appendix A,
October 26, 19B4 and subsequent revisions.
EPA = US Environmental Protection Agency
MCAW W = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SM = "Standard Methods For The Examination Of Water And Wastewater",
TestAmertca Savannah
Page 2 of 20

METHOD/ANALYST SUMMARY
Client: ARCADIS U.S., Inc.
Job Number. 680-52521-1
Method Analyst Analyst ID
40CFR135A 200.7 Rev 4.4 Bland, Brian BCB
MCAWW 353.2
SM SM 2540C
SM SM 5310E
TestAmerica Savannah
Ross, Jon
JR
Jackson, Michelle S MSJ
Dalton, Gloria
GJ
Page 3 of 20

SAMPLESUMMARY
Client: ARCADIS U.S., Inc.
Job Number. 680-52521-1
Date/Time Date/Time
Lab Sample ID Client Sample ID Client Matrix Sampled Received
680-52521-1
MW-5
Water
11/10/2009
0920
11/11/2009
1010
680-52521-2
MW-4
Water
11/10/2009
1140
11/1112009
1010
680-52521-3
MW-8
Water
11/10/2009
1300
11/11/2009
1010
TestAmerica Savannah
Page 4 of 20

Client: ARCADIS U.S., Inc.
Client Sample ID: MW5
Analytical Data
Job Number. 680-52521-1
Lab Sample ID:
680-52521-1
Date Sampled: 11/10/2009 0920
Client Matrix:
Water
Date Received: 11/11/2009 1010
200.7 Rev 4.4 Metals (ICP)
Method:
200.7 Rev 4.4
Analysis Batch: 680-153542
Instrument ID: ICPD
Preparation:
200:7
Prep Batch: 680-153246
-
Lab File ID: WA
Dilution:
1.0
_
Initial WeighWolume: 50 mL
Date Analyzed:
11/13/2009 1857
Final Weight/Volume: 50 mL
'Date Prepared:
11112/2009 1211
Analyte
Result (rig/L)
Qualifier
MDL RL
Arsenic
-
20
U
4.6 20
Barium
22
B
2.3 10
Cadmium
5.0
U
2.0 5.0
Chromium
10
U
12 10
-Lead
10
U
4.0 10
TestAmerica Savannah Page 5 of 20

Client: ARCADIS U.S., Inc.
Client Sample ID: MW-4
Analytical Data
Job Number. 680-52521-1
Lab Sample ID:
680-52521-2
Date Sampled: 11/10/2009 1140
Client Matrix:
Water
Date Received: 11/11/20091010
200.7 Rev 4.4 Metals (ICP)
Method:
200.7 Rev 4.4
Analysis Batch: 680-153542
Instrument ID: ICPD
Preparation:
200.7
Prep Batch: 680-153246
Lab File ID: N/A
Dilution:
1.0
Initial Weight/Volume: 50 mL
Date Analyzed:
11/13/2009 1935
Final WeighWolume: 50 mL
Date Prepared:
11/12/2009 1211
Analyte
Result (ug/L)
Qualifier
TU
MDL RL �T
Arsenic
20
4.6 20
Barium
10
U
2.3 10
Cadmium
5.0
U
2.0 5.0
Chromium
10
U
1.2 10
Lead
10
U
4.0 10
TestAmerlca Savannah Page 6 of 20

Analytical Data
Client: ARCADIS U.S., Inc.
Job Number: 680-52521-1
Client SamplelD:
MW-8
-
Lab Sample ID:
680-52521-3
Date Sampled: 11/10/2009 1300
Client Matrix:
Water
Date Received: 11/111200g 1lit o'
200.7 Rev 4.4 Metals (ICP)
Method:
200.7 Rev 4.4
Analysis Batch: 680-153542
Instrument ID:
ICPD
Preparation:
200.7
Prep Batch: 680.153246
Lab File ID:
N/A
Dilution:
1.0
Initial WelghWolume:
50 mL
Date Analyzed:
11/13/2009 1940
Final Weight/Volume:
50 mL
Date Prepared:
11/12/2009 1211
Analyte
Result (ug/L)
Qualifier
MDL
RL
Arsenic
20
U
4.6
20
Barium
39
B
2.3
10 '
Cadmium-
5.0
U
2.0'
5.0
Chromium
10
U
12
10
Lead
10
U
4.0
10
i
TestAmerica Savannah Page 7 of 20

Client: ARCADIS U.S., Inc.
General Chemistry
Analytical Data
Job Number: 680-52521-1
Client Sample lD: MW-5
Lab Sample ID: 680-52521-1
Date Sampled:
11/10/2009 0920
Client Matrix: Water
Date Received:
11/11/2009 1010
Analyte Result
Qual Units _MDL
RL
_ Dil
Method
Nitrate as N 2.6
mglL 0.10
0.50
10
353.2
Analysis Batch: 680-154337
Date Analyzed: 11/11/2009 2341
Total organic Carbon 1.2
mg/L 0.50
1.0
1.0
SM 5310B
Analysis Batch: 680-153341
Date Analyzed: 11112/2009 2211
Analyte Result
Qual Units RL
RL
Dil
Method
Total Dissolved Solids 100
mg/L 5.0
5.0
1.0
SM 254 CC
Analysis Batch: 680-153499
Date Analyzed: 11/15/2009 1920
TestAmerica Savannah Page 8 of 20

Client: ARCADIS U.S., Inc..
General Chemistry
Analytical Data
Job Number: 680-52521-1
Client Sample ID: MW4
Lab Sample ID: 680-52521-2
Date Sampled:
I Ill0/2009 1140
Client Matrix: Water
Date Received:
11/11/2009 1010
Analyte Result
Ouai Units MDL
RL
Dil
Method
Nitrate as N 1.5
mg/L 0
_.10 0.50
10
353.2
Analysis Batch: 680-154337
Date Analyzed: 11/11/2009 2341
Total Organic Carbon 0.78
J mg/L 0.50
1.0
1.0
SM 5310B
Analysis Batch: 680-153341
Date Analyzed: 11/12/2009 2157 ,
Analyte Result
Ouai Units RL
- RL
oil
Method
Total Dissolved Solids 60
mg/L 5.0
5.0
1.0
SM 2540C
Analysts Balch: 680-153499
Date Analyzed: 11/15/20091920
TestAmerica Savannah Page 9 of 20

Client: ARCADIS U.S., Inc.
General Chemistry
Analytical Data
Job Number: 680-52521-1
Client Sample ID: MW-8
Lab Sample ID: 680-52521-3
Date Sampled:
11/10/2009 1300
Client Matrix: Water
Date Received:
11/11/2009 1010
Analyte Result
Oust Units -MDL
RL
DII
Method
Nitrate as N 9.1
mg/L 0.20
1.0
20
353.2
Analysis Batch: 680-154337
Date Analyzed: 11/11/2009 2341
Total Organic Carbon 1.3
mg/L 0.50
1.0
1.0
SM 5310B
Analysis Batch: 680-153341
Date Analyzed: 11112/2009 2140
Analyte Result
Qual Units RL
RL
Dil
Method
Total Dissolved Solids 130
mg/L 5.0
5.6
1.0
SM 2540C
Analysis Batch: 680-153499
Date Analyzed: 11/15/2009 1920
TestAmerica Savannah Page 10 0£ 20

DATA REPORTING QUALIFIERS
Client: ARCADIS U.S., Inc.
Lab Section Qualifier Description
Metals
General Chemistry
TestAmerica Savannah
Job Number. 660-52521-1
B Compound was found in the blank and sample.
U Indicates the analyte was analyzed for but not detected.
J Result is less than the RL but greater than or equal to the
MDL and the concentration is an approximate value.
U Indicates the analyte was analyzed for but not detected.
F MS or MSD exceeds the control limits
J Result is less than the RL but greater than or equal to the
MDL and the concentration is an approximate value.
F RPD of the MS and MSD exceeds the control limits
Page 11 of 20

Client: ARCADIS U.S., Inc.
Method Blank -Batch: 680.153246
Lab Sample ID:
MB 680-153246/20-A
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
11/13/2009 1825
Date Prepared:
11/12/2009 1211
Analyte
Quality Control Results
Job Number: 680-52521-1
Method: 200.7 Rev 4.4
Preparation: 200.7
Analysis Batch: 680-153542 Instrument ID: ICP/AES - D
Prep Batch: 680-153246 Lab File ID: N/A
Units: ug/L Initial WelghtNblume: 50 mL
Final Weight/Volume: 50 mL
Result Qual MDL RL
Arsenic
20
U
4.6
20
Barium
4.50
J
2.3
10
Cadmium
5.0
U
2.0
5.0
Chromium
10
U
1.2
10
Lead
10
U
4.0
10
Lab Control Sample - Batch: 680.153246
Method: 200.7 Rev 4.4
Preparation: 200.7
Lab Sample ID:
LCS 680-153246121-A
Analysis Batch: 680-153542
Instrument ID: ICP/AES -
D
Client Matrix:
Water
Prep Batch: 680-153246
Lab File ID: N/A
Dilution:
1.0
Units: ug/L
Initial WeighWolume: 50
mL
Date Analyzed:
11/13/2009 1831
Final WelghWolume: 50
mL
Date Prepared:
11/12/2009 1211
Analyte
Spike Amount Result
% Rec. Limit
Qual
Arsenic
2000
2000
100
85 - 115
Barium
2000
2040
102
85 - 115
Cadmium
50.0
50.6
101
85 - 115
Chromium
200
200
100
85 -115
Lead
500
500
100
85-115
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmerica Savannah Page 12 of 20

Client: ARCADIS U.S., Inc.
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 680.153246
MS Lab Sample ID: 680.52521-1
Client Matrix:
Water - -
Dilution:
1.0
Date Analyzed:
11/13/2009 1913
.Date Prepared:
11/12/2009 1211
MSD Lab Sample ID:
680-52521-1
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
11/13/2009 1929
Date Prepared:
11112/2009 1211
Analysis Batch: 680-153542
Prep Batch: 680-153246
Analysis Batch: 680.153542
Prep Batch: 680-153246 '
Quality Control Results
Job Number: 680-52521-1
Method: 200.7 Rev 4.4
Preparation:_ 200.7
Instrument ID: ICP/AES - D
Lab File ID: NIA
Initial Weight/Volume: 50 mL
Final WeighWolume: 50 mL
Instrument ID: ICP/AES- D
Lab File ID: NIA
Initial Weight/Volume: 50 mL
Final WelghWolume: 50 mL
% Rec.
Analyte
MS
MSD
Limit
RPD
RPD Limit MS Qual 'MSD Qual
Arsenic
103
103
75.- 125
0
20
Barium -
- 104
105
75-125
0
20
Cadmium
103
103
75-125
0
20
Chromium
103
103
75 - 125
0
20
Lead
101,
102
75 - 125
0
20
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmerica Savannah Page 13 of-20

Quality Control Results
Client: ARCADIS U.S., Inc. Job Number: 680-52521-1
Method Blank - Batch: 680-154337
Method:353.2
Preparation: NIA
Lab Sample ID:
MB 680-154337/1
Analysis Batch: 680-154337
Instrument ID: KoneLab2
Client Matrix:
Water
Prep Batch: NIA
Lab File ID: NIA
Dilution:
1.0
Units: mg/L
Initial Weight/Volume: 2
mL
Date Analyzed:
11/20/2009 1436
Final Weight/Volume: 2
mL
Date Prepared:
N/A
Analyte
Result
Qual MDL
RL
Nitrate as N
0. 550
U 0.010
0.050
Lab Control Sample - Batch: 680-154337
Method: 353.2
Preparation: NIA
Lab Sample ID:
LCS 680-154337/2
Analysis Batch: 680-154337
Instrument ID: KoneLab2
Client Matrix:
Water
Prep Batch: N/A
Lab File ID: N/A
Dilution:
1.0
Units: mg/L
Initial WeighWolume: 2
mL
Date Analyzed:
11/20/2009 1436
Final WeighWolume: 2
mL
Date Prepared:
N/A
Analyte
Spike Amount Result
% Rec. Limit
Qual
Nitrate as N
1.00 1.05
105 90 - 110
Calculations are performed before rounding to avoid round -off errors In calculated results.
TestAmerica Savannah Page 14 of 20

Client: ARCADIS U.S., Inc.
Method Blank -Batch: 680-153499
Lab Sample ID:
MB-680-153499/1
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
11/15/2009 1920
Date Prepared:
NIA
Analysis Batch: 680-153499
Prep Batch: WA
Units: mg/L
Quality Control Results
Job Number: 680-52521-1
Method: SM 2540C
Preparation: NIA
Instrument ID: No Equipment Assigned
Lab File ID: NIA
Initial WeighWolume: 100 mL
Final Weightolume: 100 mL
Analyte
Result
Qual RL RL
Total Dissolved Solids
_
5:0
U 5.0 5.0'
Lab Control Sample/
Method: SM 2540C
Lab Control Sample Duplicate Recovery Report - Batch: 680.153499
Preparation: NIA
'LCS Lab Sample ID:
LCS 680-153499/2
Analysis Batch:
680-153499
Instrument ID: No Equipment Assigned
Client Matrix:
Water
Prep Batch: NIA
Lab File ID: N/A
Dilution:
1:0
Units: mg/L
Initial WeighWolume: 100 mL
Date Analyzed:
11/15/2009 1920
Final WeighWolume: 100 mL
Date Prepared:
N/A
LCSD Lab Sample ID:
LCSD 680-153499/25
Analysis Batch:
680-153499
Instrument 10: No Equipment Assigned
Client Matrix:
Water
Prep Batch: NIA
Lab File 10: NIA
Dilution:
1.0
' Units: mg/L
Initial WeighWolume: 100 mL
Date Analyzed:
11/15/2009 1920
Final WeighWolume: 100 mL
Date Prepared:
N/A
% Rec.
Analyte
LCS LCSD
Limit
RPD RPD Limit LCS Qual LCSD Qual
Total Dissolved Solids
87 81
80 - 120
7 25
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmerica Savannah Page 15 of 20

Client: ARCADIS U.S., Inc.
Quality Control Results
Job Number. 680-52521-1
Duplicate- Batch: 680-153499 Method:SM 2540C
Preparation: NIA
Lab Sample ID: 680-52451-G-2 DU Analysis Batch: 680-153499 Instrument ID: No Equipment Assigned
Client Matrix: Water Prep Batch: N/A Lab File ID: WA
Dilution: 1.0 Units: mg/L Initial WeighWolume: 100 mL
Date Analyzed: 11/15/2009 1920 Final WeighWolume: 100 mL
Date Prepared: NIA
Analyte Sample Result/Qual Result RPD Umit Qual
Total Dissolved Solids 160 154 1 25
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmerica Savannah Page 16 of 20

Client. ARCADIS U.S., Inc.
Method Blank -Batch: 680-153341
Lab Sample ID:
MB 680-153341/2
Analysis Batch: 680-153341
Client Matrix:
Water
Prep Batch: WA
Dilution:
1.0
Units; mg/L
Date Analyzed:
11/12/2009 1801
Date Prepared:
N/A
Analyte
Result Qua]
Total Organic Carbon
__..v 1.0 _ U
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 680-153341
LCS Lab Sample ID:
LCS 680-153341/4
Analysis Batch: 680-153341
Client Matrix:
Water
Prep Batch: N/A
Dilution:
1.0
Units: mg/L
Date Analyzed:
11/12/2009 1834
Date Prepared:
N/A
LCSD Lab Sample ID:
LCSD 680-153341/5
Analysis Batch: 680-153341
Client Matrix:
Water
Prep Batch: NIA
Dilution:
1.0
Units: mg/L
Date Analyzed:
11/12/2009 1848
Date Prepared:
N/A
% Rec.
Analyte LCS LCSD Limit
Total Organic Carbon
Quality Control Results
Job Number. 680-52521-1
Method:•SM 5310B
Preparation: N/A
Instrument ID: Total Organic Carbon Analyze
Lab File ID: WA
Initial WeighWolume: 25 mL
Final WeighWolume: 25 mL
MDL RL
0.50 1.0
Method: SM 5310B
Preparation: N/A
Instrument ID: Total Organic Carbon Analyze
Lab File ID: N/A
Initial WeighWolume: 25 mL
Final WeighWolume: 25 mL
Instrument ID: Total Organic Carbon Analy.
Lab File ID: N/A
Initial WeighWolume: 25 mL
Final WeighWolume: 25 mL
RPD RPD Umit LCS Qual LCSDQual
110 109 80 - 120 1 25
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmerica Savannah Page 17 of 20

Client: ARCADIS U.S., Inc.
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 680-153341
MS Lab Sample ID:
680-52526-F-2 MS
Analysis Batch: 680-153341
Client Matrix:
Water
Prep Batch: N/A
Dilution:
1.0
Date Analyzed:
11/12/2009 2301
Date Prepared:
N/A
MSD Lab Sample ID:
680-52526-F-2 MSD
Analysis Batch: 680-153341
Client Matrix:
Water
Prep Batch: WA
Dilution:
1.0
Date Analyzed:
11/12/2009 2320
Date Prepared:
N/A
Analyte MS MSD Limit
Total Organic Carbon
Duplicate - Batch: 680-153341
Lab Sample ID:
680-52466-B-1 DU
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
11/12/2009 2004
Date Prepared:
NIA
Analyte
Total Organic Carbon
106 963 80 - 120
Analysis Batch: 680-153341
Prep Batch: NIA
Units: mg/L
Quality Control Results
Job Number: 680-52521-1
Method: SM 5310B
Preparation: N/A
Instrument ID: Total Organic Carbon
Lab File ID: N/A
Initial WelghWolume: 25 mL
Final WeighWolume: 25 mL
Instrument ID: Total Organic Carbon Analyze
Lab File ID: NIA
Initial Weight/Volume: 25 mL
Final WeighWolume: 25 mL
RPD RPD Limit MS Qual MSD Qual
146 . 25 F
Method: SM 5310B
Preparation: N/A
Instrument ID: Total Organic Carbon Analyze
Lab File 10: NIA
Initial WelghWolume: 25 mL
Final WeighWolume: 25 mL
Sample Result/Qual Result RPD Limit
3.7. 3.67 1 - 25
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmerica Savannah Page 18 0£ 20
Qual

ABORATORY INFORMATION
COC $
CHAIN OF
TestAmena Savannah-5t02 Lagoche avenue. SBYannat GA31404 P:912-3544M F:912-352-OM5
Umenca North Canton- 4101 Snuffer Drive NW North Canton. OH 44720
-
TRANSPORTATION CUSTODYTesmmenra
Jco
P;330.497-9356 F:330497-0772
TeslAmerica Tampa- 6712 Benjamin Road. Sulte 100, Tampa, fL 33634 P: 813.885-7427 F:813.885-7049
SHIPMENT INFORMATION
Pensacola- 3355 McLomore Drive. Pensacola. FL32514 P850.474.1001 F:850-478-2671Shipment
�j
MethodTesWnerimBUIIBIO-IGHaaeev4odD,ive.SWtel06.AmheM4NY14228
P:716-691.2600 F:716-961-7991SNpmBni
TesWmericaCOtp9o-2417 Bond Street, Unimrsity Park. IL60466 P:708-534.5200 F.708-534-5211
Tretlnng No:
'B7o9
CSXT PROJECT INFORMATION
CSXT Protect Numb":
P101. State (State of Origin) N/v CONSULTANT INFORMATION
- y
Protect p: p v
Nc IOA031a OUD
/��t^ n
{50WOlOP.
�r�O /�
Proj.City: IL: I,e Company: AIWPSV IS
PM:
Alan Pihillix
y•'
CSXT Project Name: am a W
Atltlresa� + ) ��aa���
�1 Cor rare Wtivi" Dr.
Email: a t'im�L�Ah�CIa��S-Vs.COM1
CSXT Contact:
Ma# AX in
Q/ 1 T
LWON:6NV3&59� MLA- CAy,Slate,Lp:-PA[l NC •976D
PMne:91 `-551}-:aW-Fee
1
Turnaround Time: ❑ Standard 6-13 Days
❑
Preservadver Codes: 3 - Sulfuric Acid Note s•K I I. 1 0
COMMENTS LAB USE
1 Day Rush ,�a Specify 0 Days -
❑ 2 Day Rush
0 = No Preservatives 4 < Sodium Thiosullale Pres. METHODS FOR ANALYSIS
62f Standard 14 Days
❑ 3 Day Rush ❑ Other
1 = Hydrochloric Acid 5 = Sodium Hydroxide Code
2 = Nitric Acid 6 - Other 4
,Dbeeliverables: ❑ Other Deliv:
Ip1 CSXT Standard lq
Matrix Codes: SO Soil L10=Liquid No41 r\
(Level
13 Lave] III ❑ EDD Required, Format:
GW=Groundwater SL=Sludge o�o m
-
❑ Level IV
WW=Waste Water 01=Oil O
V
1
SIN =Surface Water SOL=Other Solid tvS
SAMPLE INFORMATION
4() V
• Containers
U
Sam Is Collection Filtere"Grapb
Sample Identification Number&
Type
Date Time Sampler YorN Q =
P
Mw-'
2
11 1 a o DT N f�T caW
M -
1140 DT N 14rw
W-g
1300 N
EMP
Relinquished By a
11 %0 O
1700
Rammed By,
Dale?me:
omarmer
nits a,SPeeClalAnalytical Requirements:
W 'S Bv.F CJ1 Crf Fb only.
Retnqulsnedey:
DatalTime:
-
c
Received B Y
Date/Tlme:
1' y`T r ` .
1
Relinquished By:
OaWlTimo:
Received BY•
Oare7Nme:
R alvetl ey Laborala
1 I
Date7Time:
e
Lab Remarks:
LAB USE: Custody Infect
Custody Seal Y LAB L r� u b
ORIGINAL -RETURN 1vLABOfTqyOPtyWIZpSAMpLES
-
❑Yes El No
d it._.a
�1
MUST BE SUBMITTED TO CSXT WITH ORIGINAL COO TAL-60d8(0509)

Login Sample Receipt Check List
Client: ARCADIS U.S., Inc.
Login Number: 52521
Creator: Daughtry, Beth
List Number: 1
Question T / F/ NA Comment
Radioactivity either was not measured or, if measured, is at or below
N/A
background
The cooler's custody seal, if present, is intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COG is present.
True
COG is filled out In ink and legible.
True
COG is filled out with all pertinent Information.
True
There are no discrepancies between the sample Me on the containers and
True
the COG.
Samples are received within Holding Time.
True
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
VOA sample vials do not have headspace or bubble is <6mm(1/4") in
NIA
diameter.
If necessary, staff have been informed of any short hold time or quick TAT
True
needs
Multiphasic samples are not present.
N/A
Samples do not require splitting or compositing.
NIA
Is the Field Sampler's name present on COC7
False
Sample Preservation Verified
True
Job Number: 680-52521-1
List Source: TestAmerica Savannah
TestAmerica Savannah
Page 20 of 20

GW-59A COMPLtANC.E REPORT FORM Permit # C 'D a Toga E[
(Suhneit one each monitoring period with GIP-59jorntr.J I A'u 3 1 2-99
1
Enter date monitoring results were due. - - Will this monitoring report (GIN-59 and GW-59A)^,YEI
r)YES-
,NO
be submitted after the established due
2
Was any required information missing on the GW-59 report forms?
YES
N
IF the answer to question t or 2 is 'YES", list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
identification plate, area overgrown, etc.)?ljthe answer is "Yes", contact the Regional Ofcejor guidance.
X
4
Are any monitored constituents equal to or above the established standards?
YES
NO
If the answer to question 4 is 'NO" skip to section 8.
If the answer to question 4 is "YES" list the affected wells individuaW with constituent(s) and eoncentretlon(s)
exceeding. in the space provided below: m&)-,V
�standards
X,1,- fe, as /J' 13m9A . Permef m,`f �D m1fA
21°Sa k,.A le/V;'/tale a N: // M7/1-
5
For the c nstituents Identified in question 4 above, have standards been exceeded previously for the
YES
NO
same constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is "NO" skip to section B.
If the answer to question 5Is "YES" list in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years).
ll—a5-08r Nri le. as A/: /0. It my/L
3-a9-o2i N:rral� as,v- 10.5 "'7/1-
/1-11-67 A4,1,;h as Al: ld-i &JIL
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
ND
x
If the answer is "YES", a groundwater quality problem maybe occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answeris "NO", monitoring wells maybe improperly
located; contact the Regional Office.
7
Is the permittee Implementing previously approved actions required by the Division involving this
YES
NO
groundwater quality problem?
X
If the answer to question 7 is 'YES, describe those actions in the space provided below.
If the answer to question 7Is `NO" contact the Regional Office within 90 days; an evaluation may be
required to determine the impzct the waste disposal system Is having at the retie' - and comollanee
'
boundaries surrounding this facility, Failure to do so maymblectthe vermittee to a Notice of Violation
fines. andforpenalties.
RECFjVtLj
2 0 2009
AUG
Processing Unit
lntormaliorr ProBq%pjnfBOG
g
The person completing this portion (GW-59A of the monitoring report should sign below and submit this
form with G W-59 forms for required wells to the address provided at the top of the current GW59 form.
f hereby aekriow_ledge that the above nformedon was evaluated and the i'nformatlon,submitted to this ]
report (¢o p' ce e�) _ GW 69A) Istrue and complete tothe hest of.my knowledge
igna re o P (or Authorized Agent) Date
OMCE
GW-59A 12/St2003

GROUNDWATER QUALITY MONITORING:
SUBMIT FORM ON YELLOW PAPER ONLY
Facifily Name: CSX Transportation - HamletP1ease Pr/nt Cready or Typa
Permit Name (it dillerent):
Facility Address; 173 CSX Drive
Ham 1
>SW.1 2n iaS County- R?�hTM+nd
Contact I
Person; Mike Greaory lr4r ---�_
WeilLocauum Site Telephone Y:_(9101 205- 6379
Name: -see locar; on man No. of Wells to be Sampled:
Well IdenGlication Number (from POrmll): Nip) -
Well Depth:'_R Well Diameter �.=WmwSy =
For Screened Interval: IL to It. luent (98)
Depth to Water Level: belawmeasurinuent (99)
Measuring Point (M.P. is: 9 point
It. above land surface. Relative M.P. Elevation in tL:'
Gallons of water pwRpadlballed.before sampting: Date s Field analysis: PHA . Specific Conductance ample collected:
Temp. "C, Odor. uMhos
Appearance
a11MENT OF ENVIRONMENT a NATURAL RESOURCES
FA QUALITY OIVMMK GROMOWATER SECTION
MAIL SERVICE CENTER
PERDisch
Non -Discharge F7Q0000601 EXPIRATION DATE: Dec. 31, 04 NPOES UIC
TVPE OF P9aMM= OPERATION BEING— Lamm MONITORED
--Remediation: hatralbn Gauery
Sway Field �Remadvtiolt
X Rotary UBubelor __I ahgywu«r or sludge
OUwr. monitoring well
NOTE: Values should reflect dissolved and .
colloidal concentrations.
Date sample analyzed:.Mon;h'T1 L r_It NO
Laboratory Nam: era n6A Saw+r�I�
Certification No. 29.9
PARA_ MET€RY(Se I
COD mp es for metals were collected unffltered X YES _NO
and told soidilied
Colilorm: MF Fecal..
IT1911
Nitrite
N
m�
Colilorm: MF Total
Total
(Note: Use MPH hmewd fur highly
/1 OOMI
Nitrate((NO3)aas
Phosphorus: Total as P
mo
turbld mnpWs)
Dissolved Solids: Total
_
Orthophosphate
�_ m94
PH ( hen analyzed)
— m9A
AI - Aluminum
mgA
mgll
TOCunits
Chloride
m9A
Be - Barium
Ca - Calcium
m 9A
_ 1
Arsenic f
gA
Cd - Cadmium
9A
m
Grease and Oils
mg/1
Chromium: Total
mgA
Phenol �--
mgll
Cu - Copper
gA
mgA
Sulfate n ormation Pr
Specific Conductance DWweoc
mgll°,
mgA
Fe -Iron
Hg - Mercury
Total Ammonia——uMhos
K - Potassium
m�
m gA
TKN'as N
mg/l
Mg - Magnesium
mgA
mgli
Mn - Manganese
mgA
G W-59
Rev. 0312000
X YES NO)
Ni - Nickel
Pb - Least
/I
mgA
Zn - Zinc
mgA
Ammonia Nitrogen
_fTI
Other (Specify Compounds and Concentration
units)
ORGANICS: (GC.GCIMS.HPLC)
(Sp"Illf tact ind method If. Attach lab report.)
Report Attached? Yes__() No—(0)
VOC menwd
method O .
method 0 .

FORM ON
PAPER ONLY
Facility Name Hamlet Wastewater Treatment
Facilty Address CSX Transportation, Box 191A
Contact Person: M. L. G
Well Location/SityName.
County Richmond,
Well Identification Number. MW-2 For Gmun`w 'Tree m tsystems
Well Depth: 41.48 ft. Well Diameter. 4.0 In. Check one:
Screened Interval - ft.To ft. Influent
(98)
Depth to Water Level 36.8 ft below measuring point Effluent (99)
Measuring point is fL above land surface
Gallons of water pumped/bailed before sampling:
Field Analysis pH 5.21 Specific Conductance uMhos
Temp. e C Odor Appearance
PARAMETERS, (Samples for metals were collected unfiltered X_ YES
CO
mg/I
Coliform: MF Fecal
/ 100ml
Colifonn: MF Total
/ 100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids Total 73.
mg/I
pH (when analyzed)
units
TOC 1.7
mgfl
Chloride
mgll "
Arsenic <0.02
mg/I
Grease and Oils
moll
Phenol
mg/I
Sulfate
mg/1
Specific Conductance
Mhos
Total Ammonia
mg/I
TKN as N
MR11
NO-2 as h
NO-3 as N
Phosphorus: Total as P
Orthophosphate
Al -Aluminum
PERMIT #: EXPIRATION DATE July 31, 2014
Non -Discharge W00000601 UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
_ Lagoon _
Spray Field _
_ Rotary Distributor _
X Other Monitorino Well
Remediation: Infiltration Gallery
Remediation
Land Application of Sludge
NOTE Values, should reflect dissolved and collaidal concentrations
Date Sample Collected 07/08/06 Date Sample Analyzed
Laboratory Name TestAmerica Laboratories, INC
Certification No. 269
NO and field acidified _X_ YES NO)
mg/1
NI'- Nickel
mg/I
S mg/I
Pb-Lead <0.01
mgll
—mg/I
Zn - Zinc
mg/I
mg/I
Ammonia Nitrogen
mgll
mg/I
Other (Specify Compounds and concentrati
Ba -Barium
on units)
0.0089 mg/I
Ca - Calcium
m9fl
Cd-Cadmium
<0.006 mg/I
Chromium: Total
0.0072 mg/I
Cu - Copper
moll
Fe - Iron
mg/1
Hg - Mercury
mg/I
K - Potassium
njgil
Mg - Magnesium
mg/I
Mn -Manganese
mall
Cad A.
ORGANICS: (GC, GC/MS, HPLC)
(Specify.test and'method #. Attach lab report)
Report Attached? Yes_(1) No_(0)
VOC method # =
VOC method # =
vnrr
and Title - Please print or type
GW59 Rev. 4/98

SUBMIT FORM ON YE11DW PAPER ONLY
GROUNDWATER QUALITY MONITORING; COMPLIAfurG nl=m . ._ •
Facility Name: -
Permit Name (if
- Hamlet
L:Ontact Person: Mike Gre County R' hme-na
Well Location/Site Name; a loca on Te1ephbnefl; (910)—'
r - No. of Wells to be Sam -Well Identification Number (from Permit): MW-
Well Depth: ~
�--1(. WallDiamet � aTnahsauSya nq. screened Interval: �� IL to _ Cbeell one ❑Influent (98)
Depth to Water Level: it.
Measuring Point (M'.P. is:�ft- below measuring point. ❑ Effluent (99)
Gallons of wafer um 1 Iet. above land surface.' Relative M.P. elevation in fL: -
P PaNbaileil before sampling: Date sample odleded:
Feld analysis;
pH �_� .Specific Contluctance
Temp. .0 Odor �uMhos
Anrwa�......
ARTYE� TUTY CF R"MENT • NATURAL RESOURCES
1(W MALL SERVICE CENTERROUNDWATER SECTION
a., ......... _.
PERMIT /: � `j.9Z2j
Non-oischenga W00000601 EXPIRATION DATE: Dec. • 31,
NPDES UIC
TYPE OF P a .�++r..
I OPERATION BEING MONITORED
Spray Feld —_Remedratian: Infiltration Gaaary
--_Rema6atlorc
X Other-- mRoary �onrittnr Land Application d Sludge
NOM Values should reflect dissolved and .
colloidal concentration
Data sample (1
analyzed;oh: w fell dlcy 14e.'e-
Laboratory Name: T
PARAMET RS(samples - - ,Certification No. �,69
COD for Metals were collected unfiltered X
--Y) —NO and Bold ar:IdNled A YES
Colitorm: MF Fecal mgA Nitrite (NOZ) as N _ No)
Coliform: MF Total 1tOOml Nitrate (NOgj as N mgA Ni -Nickel
(Hole: Uw MPH meuwd ror M9hry Wrbrd "melee) �1 Phosphorus: Total as P msA Ph - Lead— mgA
Dissolved Solids: Total Orthophosphate — mgA Zn -Zinc
m9A
pH (when analyzed) ­­�mgA Ai - Aluminum mgA Ammonia Nitrogen m�
TOC m its Ba - Barium Other (specify COmpounds eConcentration U� )
Chloride gA Ca - Calcium
Arsenic mgA Cd - Cadmium mgA
Grease and Oils mg/l Chromium: Total mgA
Phenol rngn Cu - Copper m94
Sulfate mg/1 Fe - Iron m9A
Specific Conductance mgA Hg - Mercury m94 ORGANICS. (GC.GC/M----S.HP- )
Total Ammonia--�uMhos K - Potassium mgA (saaolfy tac:nd methods. Attach let, report )
TKN as N mgA Mg - Magneswm mg vvOC Attached? Ye�_(t No_ (0)
9!l Mn - Manganese m �_: method 0
���_: meUwd 0
"mDrOd

ON YELLOW PAPER ONLY
Facility Name Hamlet Wastewater Treatment Facility
Facilty Address CSX Transportation, Box 191A Highway 177N
Hamlet, NC 28345 County Richmond
Contact Person: M. L. GREGORY [phone]
Well Location/Site Name: Location Map Attached
Well Identification Number: MW-4
Well Depth: 47.45 ft Well Diameter. 2.0 in.
Screened Interval f . To ft.
Depth to Water Level ft below measuring point
Measuring point is ft above land surface
Gallons of water pumpedibailed before sampling:
Field Analysis pH 5.32 Specific Conductance
Temp. e.0 Odor Appearance
CO
For GruundaaterTreatment Systems
Chock One
® Influent(98)
❑n Effluent(99)
uMhos
(Samples for metals were collected unfiltered X YES
mg/I
Coliform: MF Fecal
/100m1
Coliform: MF Total
/ 100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids Total 110.
mg/1
PH (when analyzed)
units
TOC 1.
mg/I
Chloride
mg0
Arsenic <0.02
mg/I
Grease and Oils
mgll
Phenol
mg/(
Sulfate
, mg/I .
Specific Conductance
Mhos
Total Ammonia
mg/I
TKN as N
mg/I
NO2asN
NO-3 as N
.Phosphorus: Total as P
Orthophosphate
Al -Aluminum
Ba - Barium
PERMIT #: EXPIRATION DATE July 31, 2014
Non -Discharge W00000601 UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field Remediation
_ Rotary Distributor Land Application of Sludge
X Other Monitoring Well
NOTE Values should reflect dissolved and collaidal concentrations
Date Sample Collected 07/07/09 Date Sample Analyzed
Laboratory Name TestAmerica Laboratories, INC
Certification No. 269
NO and field acidified _X_ YES NO)
Mgt[
1.2 —mg/I Pb -Lead <0.01 mg/I
mg/i Zn-Zinc mg/I
mg/l Ammonia Nitrogen mg/I
mg/I Other (Specify Compounds and concentration units)
<0.01 —mg/I
NI- Nickel
Ca - Calcium
mg/I
Cd-Cadmium <0.005
mg/I
Chromium: Total <0.005
mg/l
Cu - Copper
mg/I
Fe - Iron
Mgt]
ORGANICS: (GC, GC/MS, HPLC)
Hg - Mercury
mg/I
(Specify test and method #. Attach lab report)
K - Potassium
mgll
Report Attached? Yes_(1) No_(0)
Mg - Magnesium
mg/1
VOC : method # =
Mn -Manganese
mg11
VOC : method # =
VOC : method # _
Cad A. Gerhardstein, Director Environmental
Please print or type
GW-59 Rev. 4/98 Signatur of rhea (or Authorized gent) DATE

SUBMIT FORM ON
Facility Name Hamlet Wastewater Treatment_ Facility
Faciity Address CSX Transportation, BOX 191A HI hway 177N
Hamlet, NC 28345 County Richmond
Contact Person: M. L. GREGORY [phone]
Well Location/Sity Name: location Map Attached
Well Identification Number: MW-5 Fw Greuntlratm Treatment Systems
Well Depth: 52.92 ft. Well Diameter. 2.0 in. Chock One:
Screened Interval ft To ft. — © Influent(98)
Depth to Water Level 36.8 f . below measuring point ❑c Effluent (99)
Measuring point is fL above land surface
Gallons of water pumped/bailed before sampling:
Field Analysis pH 4.51 Specific Conductance uMhos
Temp, eC Odor Appearance
PARAMETERS:
CO
(Samples for metals were collected unfiltered _X_ YES
Colifonn: MF Fecal
/ 100ml
Celiferm: MF Total
/ 100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids Total 110.
mg/l
PH (when analyzed)
units
TOC 0.51
mg/I
Chloride
Arsenic <0.02
mg/I
mg/l
Grease and Oils
mg/I
Phenol
Sulfate
mg/I
Specific Conductance
mg/I
Mhos
Total Ammonia
mg/I
TKN as N
NO-2 as N
NO_3 as N
Phosphorus: Total as P
Orthophosphate
AI - Aluminum
PERMIT #: EXPIRATION DATE July 31. 2014
Non -Discharge WQ0000601 UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field Remediation
_ Rotary Distributor Land Application of Sludge
X Other Monitoring Well
NOTE Values should reflect dissolved and collaidal concentrations
Date Sample Collected 07/08/09 Date Sample Analyzed
Laboratory Name TestAmerica Laboratories, INC
Certification No. Inc
NO and field acidified _X_ YES NO)
1 Pb - Lead mg/I
m
9/ <0.01 mg/I
ing/I Zn-Zinc mg/1
mgll Ammonia Nitrogen mgfl
ea - Bariumm0.022 mg/I g/l Other (Specify Compounds and concentration units)
C —
a - Calcium
mg/1
Cd - Cadmium <0.005
mg/I
Chromium: Total <0,01
mg/l
Cu - Copper
mg/1
Fe - Iron
mg/I
Hg - Mercury
mg/I
K -.Potassium
mg/I
Mg - Magnesium
mg/I
Mn,- Manganese
mftn
NI - Nickel
ORGANICS: (GC, GC/MS, HPLC)
(Specify test and method #. Attach lab report)
Report Attached? Yes —(I) No_(0)'
VOC : method # =
VOC : method 9 _

SUBMIT FORM ON YELLOW PAPER
Facility Name Hamlet Wastewater Treatment Facility
FaciltyAddress CSX Transportation, Box 191A Highway 177N
Hamlet NC 28345 County Richmond
Contact Person: M. L. GREGORY [phone]
Well Location/Sity Name: Location Map Attached
Well Identification Number. MW-6 FWGreunaraterTm1mnrsrstem
Well Depth: 48.35 ft.Well Diameter. 2.0 in. area OM:
Screened Interval ft To ft a Influent(98)
Depth to Water Level 40.3 ft below measuring point ® Effluent (99)
Measuring point is ft above land surface
Gallons of water pumpediballed before sampling:
Field Analysis pH 4.8 Specific Conductance uMhos
Temp, e C Odor Appearance
PERMIT M
EXPIRATION DATE July 31, 2014
Non -Discharge WQ0000601 UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Remediation: Infiltration Gallery
Spray Field
Remediation
Rotary Distributor
Land Application of Sludge
X Other Monitoring
Well
NOTE Values should reflect dissolved and collaidal concentrations
Date Sample Collected 07/08/09 Date Sample Analyzed
Laboratory Name TestAmerica Laboratories, INC
Certification No. 269
PARAMETERS: (Samples for metals were collected unfiltered _X_ YES NO and geld acidified _X_ YES NO)
CO mg/I
Coliform: MF Feral / 100ml
Coliform: MF Total / 100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids Total
pH (when analyzed)
TOC
93. mg/l
mg/I
Chloride
mg/l
Arsenic <0.02
mg0
Grease and Oils
ing/l
Phenol
mg/l
Sulfate
mgl(
Specific Conductance
Mhos
Total Ammonia
mg/I
TKN as N
mall
NO-2 as N
NO-3 as N
mg/I
Phosphorus: Total as P
mg/I
Orthophosphate
mgli
At -Aluminum
mg/I
Ba - Barium 0.012
_mg/I
Ca - Calcium
mg/I
Cd - Cadmium <0.005
mg/I
Chromium: Total 0.015
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/1
K - Potassium
moll
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Ni - Nickel mg/I
Pb - Lead 0.01 mg/I
Zn - Zinc mg/I
Ammonia Nitrogen mg/l
Other (Specify Compounds and concentration units)
ORGANICS: (GC, GC/MS, HPLC)
(Specify test and method #. Attach lab report)
Report Attached? Yes_(1) No_(0)
VOC : method#=
VOC : method # =
VOC : method # =
CadA. Gerhardstein, Director Environmental
Name and Title - Please print or type
GW-59 Rev. 4198

SUBMIT FORM ON Y OW PAPER ONLY
GROUNDWATER QUALI�MON�ITORING.-
Facility
tur-
Name:. c:sX Transportation Hesse Print Clearly or Ty
Hamlet Pe
-
Permit -Name (if dwerenty
Facility Address-. 173 CSX Drive
Hamer et I r _
Contact Person: �nidS County
Rirhmna�— Mike Gre or hr"'•r frbh ty
well Locatio . t' Noma: e 1 a« T--phones: (910I 2ns_si;,o
. Pion - ---`�
Well Identilication Number (from Permit): MW- No. of Wails to be Sampled:
Well Deplh:ft. Well Diameter.__�• For Growittwatx�aUaeelsyyew
Screened Interval:_ D. to ChcekOne: ❑ Influent (98)
Depth to Water Level It.
Measuring Poin4(M.P. is:__% I»low measudn9 peinL Effluent (99)
Gallons of water tun) IL.above land surface• Relative M.P. Elevation in IL;
P Pedballed before sampling -
Field analysis: PH Date sam
pl collected:
P
Tem *SC,OdoPectitcConducfance Umhos
r ADOearanrA
DEPAa QU OF- MMONMW A NATURAL RESOURCES _ NEATER ILAU" OrnsioN, GROUNDWATER SECTION
ti7{ PAIL S TWICE CENTER
PERMIT s:
Non -Discharge W00000601 EXPIRATION DATE: Dec • 31,
NPDES UIC
TYPEO�PrIa' OPERATION -BEING MONITORED
Spay Field— Remedatioix INfluatinn Gallery
tTolary Distributor X --__Lviid Application d Sludge
Otlrr. monitoi i; ....._,
NQM- Values should rolled dissolved and —
001101dal concentrations, n 'r Date sample L t co t 1' a - N e _51_w ;c
analyzed: tM � o r. 1
LaboreloryName: _Terl
oc -
(Samples for metals
DEPAa QU OF- MMONMW A NATURAL RESOURCES _ NEATER ILAU" OrnsioN, GROUNDWATER SECTION
ti7{ PAIL S TWICE CENTER
PERMIT s:
Non -Discharge W00000601 EXPIRATION DATE: Dec • 31,
NPDES UIC
TYPEO�PrIa' OPERATION -BEING MONITORED
Spay Field— Remedatioix INfluatinn Gallery
tTolary Distributor X --__Lviid Application d Sludge
Otlrr. monitoi i; ....._,
NQM- Values should rolled dissolved and —
001101dal concentrations, n 'r Date sample L t co t 1' a - N e _51_w ;c
analyzed: tM � o r. 1
LaboreloryName: _Terl
oc -
(Samples for metals
CerWicakon.No,
Z69
CODPARAMET
were
cotleeted unaltered
X YES
ColHO= MF Fecal mgA
—_NO
Nitrite (NOR) as N
and field aoldlilsd
YES — NO)
Coliforrn: MF Total
1100m1
Nitrate (NO3) as N
mgn
Ni - Nickel
(Nov: UN YPM mmwYwd br MphlT turbid YmpMs)
Dissolved Solids: Total
/100m1
Phosphorus: Total as P
Orthophosphate —�
mgfl
R
Pb - Lea cL mgA
Zn - Zinc -mgA
pH ( hen analyzed) �--
mgA
a- Aluminum
mgn
Ammonia Nitrogen mgA
�units
Ba - Barium
m9A
m
Other (specify Compounds and—
Chloride
m gl
Ca - Calcium
Units)
Arsenic
mgA
Cd - Cadmium
mgA
Grease and Oils
mgll
Chromium: Total
mgn
Phenol
mgA
Cu -'Copper
mgA
Sulfate
mg/I
Fe - Iron
mg1l
Specific Conductance
m�
Hg - Mercury
ORGANICS: (GC,GGMS,HPLC)
Total Amrrwnia——uMhos
TKN as N
K - Potassium
Mg - Magnesium
gA
mgA
(Spscl/yttst rind method i. Attach lab mport
rt Attached?
m9A
gn
Mn -Manganese
mg/1
mgA
eP Ye�(1) No _ (o)
: metthod It a
• ..
'
---�_= methods .�_
�
GWsg
Rev. 0312000

ON YELLOW PAPER ONLY
Facility Name Hamlet Wastewater Treatment Facility
Facilty Address CSX Transportation Box 191A Highway 177N
Hamlet, NC 28345 County Richmond
Contact Person: M. L. GREGORY [phone]
Well Location/Sity Name: Location Map Attached
Well Identification Number: MW-8
Well Depth: 57.18 ft. Well Diameter. 2.0 in.
Screened Interval ft To ft
Depth to Water Level 44.3 ft. below measuring point.
Measuring point is ft above land surface
Gallons of water Pumpedibailed before sampling:
Field Anal
For GrauM WTreatment Syp ms
Cnea One:
Q Influent (98)
Effiuent(99)
ysts pH 4.78 Specific Conductance uMhos
Temp. C Odor Appearance
PARAMETERS: (Samples for metals were collected unfiltered _)_ YES
CO mg/I
Coliform: MF Fecal / 100ml
Coliform: MF Total / 100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids Total 93. m911
PH (when analyzed) units
TOC <1. m9/1
Chloride mgll
Arsenic <0.02
mg/I
Grease and Oils
mg/l
Phenol
mg/l
Sulfate
mg/I
Specific Conductance
Mhos
Total Ammonia
mg/I
TKN as N
..,..a
NO-2 as N
NO-3 as N
Phosphorus: Total as P
Orthophosphate
AI - Aluminum
PERMIT M EXPIRATION DATE July 31, 2014
Non -Discharge WQ0000601 UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
— Lagoon Remediation: Infiltration Gallery
Spray Field Remediation
_ Rotary Distributor Land Appllcation of Sludge
X Other Monitorina Well
NOTE Values should reflect dissolved and collaidal concentrations
Date Sample Collected 07/07/09 Date Sample Analyzed
Laboratory Name TestAmerica Laboratories, INC
Certification No. 269
NO and field acidified _X_ YES NO)
73. mgfi
mg/I
mg/I
Ba - Barium
0.039 mg/1
Ca - Calcium
mg/I
Cd - Cadmium
<0.005 mg/I
Chromium: Total
0.0048 mgll
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn -Manganese
mg/I
NI - Nickel
mg/l
Pb - Lead <0.01
mgli
Zn - Zinc
mg/l
Ammonia Nitrogen
mg/l
Other (Specify Compounds and concentration units)
ORGANICS: (GC, GC/MS, HPLC)
(Specify test and method #. Attach lab report)
Report Attached? Yes_(1) No_(0)
VOC : method # _
VOC : method # _
Vein
Cad A. Gerhardstein, Director Environmental
and Title - Please print
GW-59 Rev. 4/98

---ROUTE
RAILROAD TRACKS
1000,
2Z
4�
PE-Rltflr ulac0006ol
iF- � �
00
C� V
COMPLIANCE 0011AIDARY
.A
REVIEW B0LklvP44'ey
PROPERTY GPU,VbjnR Y
ff
N
p FIGURE 1. SITE MA MONITOR tdFi.1_5
A NOTIT.' All 3 51 TE 5 AJ?E INCORAWA TEO
/,,V T"I.E t; -4y, -,r"

TestAmedca
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL ,REPORT
Job Number: 680-48827-1
Job Description: CSX Hamlet, NC WWTP
For:
ARCADIS U.S., Inc.
801 Corporate Center Drive
Suite 300
Raleigh, NC 27607-5073
Attention: Mr. Alan Pinnix
Kathryn Smith
Project Manager I
[e-mail]
07/23/2009
cc: Mr. Jerry Cato
Mr. Mike Gregory
ACWVre1 fm�—.
xaNryO 8T
ra0 w10:15 AM
The test results in this report meet NELAP requirements for parameters for which accreditation is required oi� available.
Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report
may not be reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the
person who signed this report.
Savannah Certifications and ID #s: A21LA: 0399.01; AL: 41450; ARDEQ: 88-0692; ARDOH; CA: 03217CA; CO; CT:
PH0161; DE; FL: E87052; GA: 803; Guam; HI; IL: 200022; IN; IA: 353; KS: E-10322; KY EPPC: 90084; KY UST; LA
DEQ: 30690; LA DHH: LA080008; ME: 2008022; MD: 250; MA: M-GA006; MI: 9925; MS; NFESC: 249; NV: GA00006;
NJ: GA769; NM; NY: 10842; NC DWQ: 269; NC DHHS: 13701; PA: 68-00474; PR: GA00006; RI: LA000244; SC:
98001001; TN: TN0296; TX: T104704185; USEPA: GA00006; VT: VT-87052; VA: 00302; WA; WV DEP: 094; WV
DHHR: 9950 C; WI DNR: 999819810; WY/EPAR8: 8TMS-Q
TestAmerica Laboratories, Inc.
TestAmerica Savannah 5102 LaRoche Avenue, Savannah, GA 31404
Tel [phone] Fax [phone] w testamericainc.com
,N ACCp
�A4fX � g444'
Page 1 of 25

METHOD SUMMARY
Client: ARCADIS U.S., Inc.
Job Number: 680-48827-1
Description Lab Location Method Preparation Method
Matrix Water
Metals (ICP)
TAL SAV
40CFR136A 200.7 Rev 4.4
Preparation, Total Metals
TAL SAV
EPA 200.7
Nitrogen, Nitrate -Nitrite
TALSAV
MCAWW353.2
Solids, Total Dissolved (TDS)
TAL SAV
SM SM 2540C
Organic Carbon, Total (TOC)
TAL SAV
SM SM 5310E
Lab References:
TAL SAV = TestAmerica Savannah
Method References:
40CFR136A = "Methods for Organic Chemical Analysis of Municipal Industrial Wastewater", 40CFR, Part 136, Appendix A,
October 26, 1984 and subsequent revisions.
EPA = US Environmental Protection Agency
MCAW W = "Methods For Chemical Analysis Of Water And Wastes", EPA-60014-79-020, March 1983 And Subsequent Revisions.
SM = "Standard Methods For The Examination Of Water And Wastewater",
TestAmerica Savannah
Page 2 of 25

METHOD/ANALYST SUMMARY
Client: ARCADIS U.S., Inc.
Jab Number. 680-48827-1
Method Analvst Analvst ID
40CFR136A 200.7 Rev 4.4 Bland, Brian BCB
40CFR136A 200.7 Rev 4.4 Robertson, Bryn BR
MCAWW 353.2 Ross, Jon
-SM SM 2540C Johnson, Brad
SM SM 5310B Blackshear, Kim
TestAmerica Savannah
JR
BJ
KB
Page 3of 25

SAMPLE SUMMARY
Client: ARCADIS U.S., Inc.
Job Number: 680-48827-1
Date/Time
Date/Time
Lab Sample ID
Client Sample ID
Client Matrix
Sampled
Received
680-48827-1
MW-2
Water
07/08/2009 1500
07109/2009 0903
68048827-2
MW-5
Water
07/08/2009 1600
07109/2009 0903
680488274
MW-6
Water
07108/2009 1655
07/09/2009 0903
68048827-5
MW-4
Water
07/07/2009 1925
07/09/2009 0903
TestAmerica Savannah
Page 4 of 25

Analytical Data
Client: ARCADIS U.S., Inc. Job Number: 680-48827-1
Client Sample ID: MW-2
Lab Sample ID: 68048827-1 Date Sampled: 07/08/2009 1500
Client Matrix: Water Date Received: 07/09/2009 0903
200.7 Rev 4.4 Metals (ICP)
Method:
200.7 Rev 4.4
Analysis Batch: 680-142833
Instrument ID:
ICPD
Preparation:
200.7
Prep Batch: 680-142625
Lab File ID:
N/A
Dilution:
1;0
Initial WeighWolume:
50 mL
Date Analyzed:
07/15/20091934 -
-
Final WeighWolume:
50 mL
Date Prepared:
07/13/2009 1647
Analyte
Result (ug/L)
Qualifier MDL
R_L
Arsenic
_ 20
U 4.6
20
Barium
8.9
J 2.3
10
Cadmium
5.0
U 2.0
5.0
Lead
10
U 4.0
10
Method:
200.7 Rev 4.4 -
Analysis Batch: 680-'143291'
Instrument ID:
ICPD
Preparation:
200.7
Prep Balch: 680-142625
Lab File ID:
N/A
Dilution:
1.0
Initial Weight/Volume:
50 mL
Dale Analyzed:
07/15/2009 1934
Final Weight/Volume:
50 mL
Date Prepared:
07/1312009 1647
Analyte
Result (ug/L)
Qualifier MDL
RL
Chromium
7.2
J 1.2
10 -
TestAmerica Savannah Page 5 of 25

Client: ARCADIS U.S., Inc.
Analytical Data
Job Number: 680-48827-1
Client Sample ID: MW-5
Lab Sample ID: 680-48827-2 Date Sampled: 07/08/2009 1600
Client Matrix: Water Date Received: 07/09/2009 0903
200.7 Rev 4.4 Metals (ICP)
Method:
200.7 Rev 44
Analysis Batch: 680-142833
Instrument ID:
ICPD
Preparation:
200.7
Prep�Batch: 680.142625
Lab File ID:
N/A
Dilution:
1.0
Initial WeighWolume:
50 mL
Date Analyzed:
07115/20091950
Final WeighWolume:
50 mL
Date Prepared:
07/13/2009 1647
Analyte
Result (ug/L) w
_ Qualifier MDL
RL
Arsenic
R
20
U 4.6
20
Barium
22
2.3
10
Cadmium
5.0
U 2.0
5.0
Lead
10
U 4.0
10
Method:
200.7 Rev 4.4
Analysis Batch: 680-143291
Instrument ID:
ICPD
Preparation:
200.7
Prep Batch: 680-142625
Lab File ID:
N/A
Dilution:
1.0
Initial WeighWolume:
50 mL
Date Analyzed:
07115120091950
Final Weight/Volume:
50 mL
Date Prepared:
0711312009 1647
Analyte
Result (ug/L)
Qualifier MDL
RL
Chromium
10
U 1.2
10
TestAmerica Savannah Page 6 of 25

Client: ARCADIS U.S., Inc.
Client Sample ID: MW-6
Analytical Data
Job Number. 680-48827-1
Lab Sample ID:
680.488274
Date Sampled: 07/08/2009 1655
Client Matrix:
Water
Date Received: 07109/2009 0903
200.7 Rev 4.4 Metals (ICP) '
Method:
200.7 Rev 4.4
Analysis Batch: 680-142833
Instrument ID:
ICPD
Preparation:
200.7
Prep Balch: 680-142625
Lab File ID:
N/A
Dilution:
1.0
Initial WeighWolume:
50 mL
Date Analyzed:
07/15120092005
Final Welght/Volume:
50 mL
Date Prepared:
07/13/2009 1647
Analyte
Result (ug/L)
Qualifier MDL
RL
Arsenic
20
U _4.6
20
Barium
12
2.3
10
Cadmium
5.0
U 2.0
5.0
Lead
10
U 4.0
10
Method:
200.7 Rev 4.4
Analysis Batch: 680-143291
Instrument ID:
ICPD
Preparation:
200.7
Prep Batch: 680-142625
Lab File ID:
N/A
Dilution:
1.0
Initial Weight/Volume:
50 mL
Date Analyzed:
07115/20092005
Final WeighWolume:
50 mL
Date Prepared:
07/13/2009 1647
Analyte
Result (ug/L)
Qualifier MDL
RL
Chromium
15
1.2
10
TestAmerica Savannah Page 7 of 25

Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID: MW-4
Job Number: 680-48827-1
Lab Sample ID:
68048827-5
Date Sampled: 07/07/2009 1925
Client Matrix:
Water
Date Received: 07/09/2009 0903
200.7 Rev 4.4 Metals (ICP)
Method:
200.7 Rev 4.4
Analysis Batch: 680-142833
Instrument ID:
ICPD
Preparation:
200.7
Prep Batch: 680.142625
Lab File ID:
NIA
Dilution:
1.0
Initial WelghWolume:
50 mL
Date Analyzed:
07/15/2009 2010
Final WeighWolume:
50 mL
Date Prepared:
07/13/2009 1647
Analyte
Result (ug/L)
_ Qualifier MDL
J
RL _
Arsenic
v�
20
U
4.6
20
Barium
10
U
2.3
10
Cadmium
5.0
U
2.0
5.0
Lead
10
U
4.0
10
Method:
200.7 Rev 4.4
Analysis Batch: 680-143291
Instrument ID:
ICPD
Preparation:
200.7
Prep Batch: 680-142625
Lab File ID:
N/A
Dilution:
1.0
Initial WelghWolume:
50 mL
Date Analyzed:
07/15120092010
Final Weight/Volume:
50 mL
Date Prepared:
07/13/2009 1647
Analyte
Result (ug/L)
Qualifier MDL
RL
Chromium
5.7
J
1.2
10
TestAmerica Savannah Page 8 of 25

Client: `ARCADIS U.S., Inc.
General Chemistry
Analytical Data
Job Number: 680-48827-1
Client Sample ID:
MW-2
Lab Semple ID:
6BOA8827-1
Date Sampled:
07/08/2009 1500
Client Matrix:
Water
Date Received:
07/09/2009 0903
Analyte
Result
Qual Units MDL
RL
Dil
Method
Total Organic Carbon 1.7
mg/L ` 0.50
1.0
1.0
SM.53108
Analysis Batch: 680-142887
Date Analyzed: 07/15/2009 1621
Nitrate as N
1.5
mg/L 0.020
0.10
2.0
353.2
Analysis Batch: 680-142965
Date Analyzed: 07/09/2009 1441
Analyte
Result
Qual Units RL
'RL
Dil
Method
Total Dissolved Solids
73
mg/L 5.0
5.0
1.0
SM 2540C
Analysis Batch: 68D-142677
Date Analyzed: 07/14/2009 1354
TestAmerica Savannah Page 9 of 25

Analytical Data
Client: ARCADIS U.S., Inc.
General Chemistry
Job Number: 680-48827-1
Client Sample ID:
MW-5
Lab Sample ID:
68048827-2
Date Sampled:
07/08/2009 1600
Client Matrix:
Water
Date Received:
07/09/2009 0903
Analyte
Result
Qual Units MDL
�mg/L _
RL
Dil
Method
Total Organ(c Carbon _ 0.51
J 0.50
1.0
1.0
SM 53108
Analysis Batch: 680-142887
Date Analyzed: 07/15/2009 1649
Nitrate as N
1.8
mg/L 0.020
0.10
2.0
353.2
Analysis Batch: 680-142965
Date Analyzed: 07109/2009 1441
Analyte
Result
Qual Units RL
RL
Dil
Method
Total Dissolved Solids 110
mg/L 5.0
5.0
1.0
SM 2540C
Analysis Batch: 680-142677
Date Analyzed: 07/14/2009 1400
TestAmerica Savannah Page 10 of 25

Client: ARCADIS U.S., Inc.
General Chemistry
Client Sample ID: MWd
Analytical Data
Job Number: 68048827-1
Lab Sample ID: 68048827-5
Date Sampled:
07107/2009 1925
'Client Matrix: Water
Date Received:
07/09/2009 0903
Analyte Result
Qual Units MDL
RL
Oil
Method
_
Total Organlc Carbon —, 1.0
.� U mg/L 0.50
1.0
1.0
SM 5310B
Analysis Batch: 680-142887
Date Analyzed: 07/15/2009 1703
Nitrate as N 1.2
mg/L 0.010
0.050
1.0
353.2
Analysis Batch: 680-142965
Date Analyzed: 07/09/2009 1441
Analyte Result
Qual Units RL
RL
Dil
Method
Total Dissolved Solids 110
mg/L 5.0
5.0
1.0
SM 2540C
Analysis Batch: 680-142677
Date Analyzed: 07/14/2009 1450
TestAmerica Savannah Page '11 of 25

DATA REPORTING QUALIFIERS
Client: ARCADIS U.S., Inc.
Lab Section Qualifier Description
Metals
General Chemistry
TestAmerica Savannah
Job Number: 680.48827-1
U Indicates the analyte was analyzed for but not detected.
J Result is less than the RL but greater than or equal to the
MDL and the concentration is an approximate value.
U Indicates the analyte was analyzed for but not detected.
J Result is less than the RL but greater than or equal to the
MDL and the concentration is an approximate value.
Page 12 of 25

Quality Control Results
Client: ARCADIS U.S., Inc. Job Number: 680-48827-1
Method Blank - Batch: 680.142625
Method: 200.7 Rev 4.4
Preparation: 200.7
Lab -Sample ID:
MB 680-142625/16-A
Analysis Batch: 680-142633
Instrument ID: ICP/AES - D
Client Matrix:
Water
Prep Batch: 680-142625
Lab File ID: N/A
- Dilution:
1.0
Units: ug/L
InitialWeighWolume: 50 mL
Date Analyzed:
07/15/2009 1924.
Final Weight/Volume: 50 mL
.Date Prepared:
07/13/2069 1647
Analyte Result qual ' MDL RL
Arsenic
- 20
U
4.6
20
Barium
10
U
2.3
10
Cadmium
5.0
U
2.0
5.0
Chromium
10
U
12
10
Lead
10
U
4.0
10
Lab Control Sample - Batch: 680-142625
Method: 200.7 Rev 4.4
Preparation: 200.7
Lab Sample ID:
LCS 680-142625/17-A
Analysis Batch:
680-142833
Instrument ID: ICP/AES - D
Client Matrix:
Water
Prep Batch: 680-142625
,Lab
File ID: NIA
Dilution:
1.0
Units: ug/L
Initial WeightlVolume: 50
mL
Date Analyzed`.
07/15/2009 1929
Final WeighWolume: 50
mL
Date. Prepared:
07/13/2009 1647
_
'
Analyte
Spike Amount
Result
% Rec.
Limit
qual
Arsenic
2000
2020
101
85-115
Barium
2000
2100
105
85 - 115
Cadmium
50.0
60.9
102
85 - 115
Chromium
200
206
103
85 - 115
Lead
500,
505
101
85-115
Calculations are performed before rounding to avoid round -off errors In calculated results.
TestAmerica Savannah Page 13 of 25

Client: ARCADIS U.S., Inc.
Matrix Spike - Batch: 680-142625
Lab Sample ID: 68048827-1
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 07/15/2009 1939
Date Prepared: 07/13/2009 1647
Analysis Balch: 680-142833
Prep Balch: 680-142625
Units: ug/L
Analyte Sample ResultlQual
Arsenic
20
U
Barium
8.88
1
Cadmium
5.0
U
Lead
10
U
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 680-142625
MS Lab Sample ID: 68048827-1
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
07/15/2009 1939
Date Prepared:
07113/2009 1647
MSD Lab Sample ID:
680-48827-1
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
07/15/2009 1944
Date Prepared:
07/13/2009 1647
Analyte
Chromium
Quality Control Results
Job Number: 680.48827-1
Method: 200.7 Rev 4.4
Preparation: 200.7
Instrument ID: ICP/AES - D
Lab File ID: N/A
Initial WeighWolume: 50 mL
Final Weight/Volume: 50 mL
Spike Amount Result % Rec. Limit
2000
2090 104
75 - 125
2000
2170 108
75 - 125
50.0
52.6 105
75 - 125
500
521 104
75 - 125
Method: 200.7 Rev 4.4
Preparation: 200.7
Analysis Batch: 680-143291
Prep Batch: 680-142625
Analysis Balch: 680-143291
Prep Batch: 680-142625
° Rec.
MS MSD Limit
102 _----- 98 75 - 125
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmerica Savannah Page 14 of 25
Instrument ID: ICP/AES - D
Lab File ID: N/A
Initial WelghWolume: 50 mL
Final WeighWolume: 50 mL
Instrument ID: ICPIAES - D
Lab File ID: N/A
Initial WeighWolume: 50 mL
Final Weight/Volume: 50 mL
Dual
RPD RPD Limit MS Dual MSD Qual
4 20

Quality Control Results
Client ARCADIS U.S., Inc. Job Number: 68048827-1
Method Blank - Batch: 680.142965
Method: 353.2
Preparation: NIA
Lab Sample ID:
MB 680-14296511
Analysis Batch: 680-142965
Instrument ID: KcneLab2
Client Matrix:
Water
Prep Batch: N/A
Lab File ID: N/A
Dilution:
to
Units: mg/L
Initial Weight/Volume: 2
mL
Date Analyzed:
07/1612009 1527
Final WelghWolume: 2
mL
Date Prepared:
N/A
'
Analyte
Result Qual
MDL
RL
Nitrate as N
0.050 U
0.010
0.050
Lab Contra[ Sample - Batch: 680.142965
Method: 353.2
Preparation: N/A
Lab Sample ID:
LCS 680-142965/2
Analysis Batch: 680-142965
Instrument ID: KoneLab2
Client Matrix:
Water
Prep Batch: N/A
Lab File ID: WA
Dilution:
1.0
Units: mg/L
Initial WeightfVolume: 2
mL
Date Analyzed:
07/1612009 1527
Final Weight/Volume: 2
mL
Date Prepared: N/A
Analyte Spike Amount Result
Nitrate as N 1.00 1.08
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 680.142965
MS Lab Sample ID:
680-48792-A-1 MS
Analysis Batch: 680-142965
Client Matrix:
Water
Prep Batch: NIA
Dilution:
1.0
Date Analyzed:
07/08/2009 1335
Date Prepared:
N/A
MSD Lab Sample ID:
680-48792-A-1 MSD
Analysis Batch: 680-142965
Client Matrix:
Water
Prep Batch: N/A
Dilution:
1.0
Date Analyzed:
07/08/2009 1335
Date Prepared:
NIA
% Rec.
Analyte MS MSD Limit
%Rec.' Limit Qual
108 90-110
Method: 353.2
Preparation: NIA
Instrument ID: KoneLab2
Lab File ID: N/A
Initial WeighWolume: 10 mL
Final WeighWolume: 10 mL
Instrument ID: KcneLab2
Lab File ID: N/A
.Initial WelghWolume: 10 mL
Final WeighWolume: 10 mL
RPD RPD Limit MS Qua] MSD Qua[
Nitrate as N 103 108 90 - 110 4 10
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmerica Savannah Page 15 of 25

Client: ARCADIS U.S., Inc.
Duplicate - Batch: 680-142965
Lab Sample ID:
680-48792-A-8 DU
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
07/08/2009 1339
Date Prepared:
N/A
Analyte
Nitrate as N
Analysis Balch: 680-142965
Prep Batch: N/A
Units: mg/L
Sample RBsuIVCual Result
0.73 0.731
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmerica Savannah Page 16 of 25
Quality Control Results
Job Number: 68048827-1
Method: 353.2
Preparation: N/A
Instrument ID: KoneLab2
Lab File ID: N/A
Initial WeighWolume: 2 mL
Final WeighWolume: 2 mL
RPD Limit Qual
0 10

Client: ARCADIS U.S., Inc.
Method Blank -Batch: 660-142677
Lab Sample ID:
MB 680-142677/1
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
07/1412009 1302
Date Prepared:
WA
Analysis Batch: 680.142677
Prep Batch: N/A
Units: mg/L
Quality Control Results
Job Number: 680-48827-1
Method: SM 2540C
Preparation: N/A
Instrument ID: No Equipment Assigned
Lab File ID: N/A
Initial Weight/Volume: 100 mL
Final WeighWolume: 100 mL
Analyte Result Qual RL RL
Total Dissolved Solids 5.0 U 5.0 5.0
Lab Control Sample/ Method: SM 2540C
Lab Control Sample Duplicate Recovery Report - Batch: 680-142677 Preparation: N/A
LCS Lab Sample ID: LCS 680-142677/2 Analysis Batch: 680-142677 Instrument ID: No Equipment Assigned
Client Matrix: Water Prep Batch: WA Lab File ID: N/A
Dilution: 1.0 Units: mg/L Initial WeightA/olume: 100. mL
Date Analyzed: 07/14120091302 Final WeighWolume: 100 mL
DatePrepared: N/A
LCSD Lab Sample ID:
LCSD 680-142677/3
Analysis Batch: 680-142677
Client Matrix:
Water
Prep Batch: N/A
Dilution:
1.0
Units: mg/L
Date Analyzed:
07/14/2009 1315
Date Prepared:
N/A -
° Rec
Analyte
LCS LCSD Limit
Total Dissolved Solids
89 91 80- 120
Calculations are performed before. rounding to avoid round -off errors in calculated results.
Instrument ID: No Equipment Assigned
Lab File ID: N/A
Initial WelghWolume: 100 mL
Final WeighWolume: 100 mL
RPD RPD Limit LCS Quai LCSD Qual
1 _ 25
TestAmerica Savannah Page 17 of 25

Client: ARCADIS U.S., Inc.
Duplicate - Batch: 680-142677
Lab Sample ID:
680-48827-1
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
07/14/2009 1357
Date Prepared:
N/A
Analyte
Total Dissolved Solids
Analysis Batch: 680-142677
Prep Batch: N/A
Units: mg/L
Sample Result/Qual Result
73 67.0
Calculations are performed before rounding to avoid round -off errors In calculated results.
Quality Control Results
Job Number: 68048827-1
Method: SM 2540C
Preparation: N/A
Instrument ID: No Equipment Assigned
Lab File ID: N/A
Initial Welght/Volume: 100 mL
Final Weight/Volume: 100 mL
RPD Limit Qual
9 25
TestAmerica Savannah Page 18 of 25

Client: ARCADIS U.S., Inc.
Method Blank -Batch: 680.142887
Lab Sample ID:
MB 680-14288712
Analysis Batch: 680-142887
Client Matrix:
Water
.Prep Batch: N/A
Dilution:
1.0
Units: mg/L
Date Analyzed:
'07115/20091208
Date Prepared:
N/A
Analyte
Result
Total Organic Carbon
1.0
Lab Control Sample/
Lab Control Sample Duplicate RecoveryReport - Batch: 680-142887
LCS Lab Sample ID:
, LCS680-142887/4
Analysis Batch: 680-142887
Client Matrix:
Water
Prep Batch: N/A
Dilution:
1.0
Units: mg/L
Date Analyzed:
07/15/2009 1239
Date Prepared:
N/A ,
LCSD Lab Sample ID:
LCSD 680-142887/5
Analysis Batch: 680-142887
Client Matrix:
Water
Prep Batch: N/A
Dilution:
1.0'
Units: mg/L
Date. Analyzed:
07/15/2009 '1252
Date Prepared:
N/A
Analyte
Total Organic Carbon
° Rec.
LCS LCSD Limit
96 95
Quality Control Results
Job Number: 68048827=1
Method: SM 5310B
Preparation: NIA
Instrument ID: Total Organic Carbon Analyze
Lab File ID: N/A
Initial Weight/Volume: 25 mL
Final WeighWolume: 25 mL
Qual MDL RL
U 0.50 1.0
Method: SM 5310B
Preparation: N/A
Instrument ID: Total Organic Carbon Analyze
Lab File ID: N/A
Initial WeighWolume: 25 mL.
Final Weight/Volume: 25 mL
Instrument ID: Total Organic Carbon Analy.
Lab File ID: N/A
Initial WeighWolume: 25 mL
Final Welght/Volume: 25 mL
RPD RPD Limit LCS Qual LCSD Dual
80 - 120 1 25
Calculations are performed before rounding to avoid round -off enors In calculated results.
TestAmerica Savannah Page 19 of 25

Client: ARCADIS U.S., Inc.
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 680.142887
MS Lab Sample ID: 680-48851-A-1 MS
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
07/16/2009 1909
Date Prepared:
N/A
MSD Lab Sample ID:
680-48851-A-1 MSD
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
07115/2009 1922
Date Prepared:
N/A
Analyte
Total Organic Carbon
Duplicate- Batch: 680.142887
Lab Sample ID:
680-48827-1
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
07/15/2009 1631
Date Prepared:
N/A
Analyte
Total Organic Carbon
Analysis Batch: 680-142887
Prep Batch: N/A
Analysis Batch: 680-142887
Prep Batch: N/A
% Rec.
MS MSD Limit
Quality Control Results
Job Number: 680-48827-1
Method: SM 5310B
Preparation: N/A
Instrument ID: Total Organic Carbon
Lab File ID: NIA
Initial WeighWolume: 25 mL
Final Weight/Volume: 25 mL
Instrument ID: Total Organic Carbon Analyze
Lab File ID: N/A
Initial Weight/Volume: 25 mL
Final WeighWolume: 25 mL
RPD RPD Limit MS Qual MSD Qual
91 89 80 - 120 1 25
Analysis Batch: 680-142887
Prep Balch: N/A
Units: mg/L
Sample Result/Qual
1.7
Method: SM 5310B
Preparation: NIA
Instrument ID: Total Organic Carbon Analyze
Lab File ID: N/A
Initial WeighWolume: 25 mL
Final WeighWolume: 25 mL
Result RPD Limit
1.73 1 25
Calculations are performed before rounding to avoid round -off errors In calculated results.
TestAmerica Savannah Page 20 of 25
Qual

'LABORATORY
CHAIN OF
: TRANSPORTATION, CUSTODY
TAL-00060907 -
INFORMATION - - -I 1
COC #
eslAmeda Savannah-5102L2Rmbe Avenue,Savannah,GA31404 It972454.7859 F:912-352-0165
TesUkmeria North Canton• 4101 Shpifel Drive NW, North Canton, 0444720 P.336497-9396 F.330-497-0772
07"tnmeria Tampa- 6712 Benjamin Road, Suke 100, Tampa, FL 33634 P:813-885-7427 F:813.886-7049 .
CTestAmerim Pen ia-3355McLemom Drive,Peosacob,FL32514 P.850474-10m F.850d78.2671
❑TestAmeria Buffalo-lOHa4lwood Drive, Suite 106. AmheM, NY 1422E P.716-691-2600 P716.961-7991
❑TestAmerta Chicago -2417 Bond Street, University Park, IL 60466 P.,70MM-5200 R708-534-5211
SHIPMENT INFORMATION
Shipment Method: .
Shipment Tracking No'
CSXT PROJECT INFORMATION �`' Proj•State (State of Origin)
CSXT Prolee[Number: .'C"v1 LlJ 1� �('Tj Pro]. C1M dab- Lj `"
CSXT Project Nam: 11.A� e} klw ll Y'1 (�/�
CSXTContact: t''il aT i n5 - LvvON:FINV O`GrJq -
7k0S'
CONSULTANT INFORMATION .. Project R:
I(hVj;, yjldnl �'Llcl•
Company. D//�'� �� _ PM: Alm
Atldress: alj\4l.Dr YQ a Gri�lf�7i/4�, r EmaiC.�[JO(� �I�6I�WQ�'CO4M1'�iS
City, smue. Dp- Ie C oC l6ll
TumaeounclTime: Standard 6-13 Days
❑ 1 Day Rush ,�I Specify A Days -
❑ 2Day Rush V ;J 'ncard14bays
13 3 Day Rush ❑. Other
Preservative Codes: 3'=Sulfuric Acid- - _ -' Noteft
0 = No Preservatives 4 = Sodium Thiosuifate - Pres. -
1 = Hydrochloric Acid 5= Sodium .Hydroxide Code
2 = Nitric Acid 6 = Other
COMMENTS
LA13USE
METHODS
FOR
ANALYSIS
,
�^
(WIvembles: -❑ Other Deliv.,
CS)cT Standard (Level 11)
❑ Laurel..11l EDD So [red, Format:
❑ Level IV � }'1d OCT ,
Matrix Codes: SO -= SoilLIO = Liquid
GW=Groundwater `SL=Sludge
- W W = Waste Water OI = OiI '
; SW = Sudace Water SOL = Other Solid '
�
SAMPLE INFORMATION
Sample Ident cation
Containers
Sam Ie
Collection ..
Filtered
. T e
IMatrix
Number& -
Date -
,Time
Sampler
YorN
Com
Code
W�aor
g oq
Isau
I DT
N
G
G•W,
I PT
N
CAlaw
I63o
I nIT,
N .
C�
aW
bT
N
N
Relinquished By.
Daterrma` ; rj
0
Received By;
Dat
i 04 `��^luilyr�r�
Comments & Special Analytical Requirements:
(�1Rf6weiM+�
twomy 4.px4d, AyyiAoc
-
Relinquished ey.
DafeRime: '
Reserved By:
Dat Time:
Relinquished By:
Da[ertime: -
Received By
DatenIrm:
ReceivedBy laboratory:
nRirwer _ooru=um.
Dete7Tirlte. - -
Lati Remarks:
_
LAB USE: Custody intact
❑Yes❑No
Custody Seat a
A
LAB Log Number -
>7
m
N
u
0
N
m
b
a
"""" ""^""—l— A— SAMPLES INVOICE MUST BE SUBMITTED TO CSXT WITH ORIGINAL CDC

CHAIN OF
TRANSPORTATION CUSTODY
TAL•60060907
LABORATORY INFORMATION I
COC #
I-0165
OTestAmeda Savannah -5102LaRoche 4 P:9t2-J5330-4 F:R6 F-.230-4
ur Avenue. Savannah. Carter.
❑Tes Ameda NOM Carron-4t01 Snute DriveNW, North Camon.OH 44720 P: 3304979396 F:330d97.0T72
❑TeslAmetia TamDa•fi712 Benjamin Road, Suite 100, Tampa, FL 33634 P: 813-BBS-742T F: 873.685.7049
❑TestAmedm Pennmla-3355McLemore0dve,Penacola.FL32514 P:850-474-110(11 F:85D473-2671
❑TestAmeda Bvlfalo-10HMIWood Ddve,SuilelW,AmhemLWI4226 P.716-691-2600 F.716-961.7991
0TestAmetke Chicago-2417 Bond Street, University Park, IL60466 P:708-534-5200 F:700 ;534-5211
SHIPMENT INFORMATION
Shipment Method:
SNpmentTmcking No:
CSXT PROJECT INFORMATION Prof. State (State of Odgin) J1/G
CONSULTANT INFORMATION Project #:A I OLm-�. WOOL 00001
CSXT Project Number: ASZ�-%CZ Pro).Cily: MLE
PM:AL4N P11-A{.nX
(IT Company: C6015
CSXT Project Name: U p M� * n
F
Address: C� )I CGI,VO ♦ C . /" l� 1 ail:p7 Ate, �i NNIX�j 4Y-t��6ilS-L • i01ti
/�
,4
LWON.�73$6M/14 LA
CSXT Cowsma� AJDKIno
City, Stale, zip. SIGN A-C Z p- Phone:N let-[-IP2"m"(l,tR)9 N—
Turnaround Time: ❑ Standard 6.13 Days
❑ 1 Day Rush Specify # Days
❑ 2 Day Rush 91 Standard 14 Days
❑ 3 Day Rush ❑ Other .
Preservative Codes: 3= Sulfuric Acid Note.
0 = No Preservatives 4 - Sodium Thiosulfate Pres.
1 = Hydrochloric Acid 5 = Sodium Hydroxide Code
2 = Nitric Acid 8 = Other
Z
COMMENTS
LAB USE
METHODS
FOR
ANALYSIS
C�
••UU v�
—
11J
1�
M
�/a
J
O
C>
Deliverables: ❑ Other Deliv:
CSXT Standard (Level 10
Level III IN EDD Required, Format:
❑ Level IV
SAMPLE INFORMATION
Matrix Codes: SO Sol] L10=Liquid
GW =Groundwater SL= Sludge
W W = Waste Water 01= Oil
SW=Surface Water SOL=Other Solid
Sample Identification
Containers
Sam le
Collection
Flitered
Type
Matrix
Number &
Type
Date
Time
Sampler
YorN
Comp
or Grab
Code
M�--`t 971%
7/Vol
HIS-
F0
'A
— y
U mi. F03
Q
[°lZS
nv
G
Liq
R uis a By'
DIM m e:
od[ to 3a
Re ed ey:
kG.
Dat
m :
4
at�s
Comments & Special Analytical Requirements:
• 'J
Relinquished By.
Dete"rime:
Received By:
Daterrme:
Relinquished By.
Date7Time:
Received By:
Dalerrame:
Received By Laboratory:
Dale7Rme:
Lab Remarks:
LAB USE: Custody I"ct
❑Yes ONO
Custody Seat 0
#
LAB Log Number
#
ORIGINAL- RETURN TO LABORATORY WITH SAMPLES INVOICE MUST BE SUBMITTED TO CSXT WI
m
tA
m
a

'
CHAIN OF
TRANSPORTATION CUSTODY
TAL-GODS 0907
LABORATORY INFORMATION, . I
ICOC #
+la`RSWne:ta5ardnm.A-61021naoUe Are:ue,.SararnaA, GA31404 P.912.3947858 F:912352-016-i
OTesrAmerica NmhCmlm-41015huHel Ddv FM1Y,NaMCamo1gN44720 P:336-597•SA96 F:330-W-OW
OTISlAmxpm Terapa• 67128en14mla Road, Sul! 100jarnF, FL33634 P.913-811 .7427 R61S88":7049 ,
OTestwerim Pe14E01a-33SSM0Lem0re Orin. Pensason,F132314 P.850274-1001 1.850478.2M
O.TesjlwedCa DUI .0.10N4RImood Ddve,Su11e1CS,AMhen%NY14728 P:716-691.2600 F.716e51.7991
OT45tAmedmChkapo-2417Bond street, UAken1y,PeTILIL69466. P, 708•SM•520o .F Y0837S•521r
SHQ3MENT INFORMATION
ShipmentMethOd:
SSpmem40WngNC:
pSXT PROJECT INFPml. Slate(5W0 of Odgln)NG
CONSULTANT INFORMATION
Pmlectm.� IOrZa 03�, OOOdi, pOpbl
iRMATION
Prolabl /O
CSXT Number:_ISLZZDZ
PrW�Y N1LGT.Company./1�gD15
PM:
/�
CSXT-Projem Name. �Vm 77 wt
!.T
Q�
'AddR55'.'9V�.• .a.�f�'(iY•! malt rk; rlPA, tt�.�i)-C:rCIGj-L .lC,� t
CSXT CeOfeCL' - ' LWON:7- -
MRi7 lif)!C-1At _N/3$6ftML-4,
:Cily.'S{2te;:....�,r Phdne:lIcl ,QS`4' (Z jZFaz:f flR .i"'
1E16Ft A-( 17 c r l
TurrferounN Time: ❑. Standard 0-13 Days
❑ -1 Day Rush Specity N Days
2 Day Rush ®Standard 14 Days
,❑ 3Day-Rush ❑Other
-
PreselveGveCodes: 9=Su111ideAcid Nbte+}.74
0 y No Preser7aiives 4 = SodumThiosplta[e Pies.
1 =Hydrochlodc.Acld 5= Sedlumtlydmxide Cdde
2>slJicW' =:O tnc A6thers
_.. . .
1"L1
., _
COMMENTS
LAB USE
METHODS
FOR
ANALYSIS13
.
` U
T -
2 �
�
�5 U
}
�
;'r-ib
� lH
�
1`I.
p
.i;
C
tn,
"
�.
A
1
.:
, rv:
�I
I
I
Dellvembles: ❑ Other Detiv:-
Ci GSXTSfandaN (Level tl)
El Level III ®EOD Required, Format
❑ Level IV
Matrix Codes: SO=Soil UQ Liquid
GW = Gmuhd vafet SL=Sludge
yY
�W Waste Water AI=01 �
SIN SudaoaWater ., SOLD CIherSoW.
SAMPLE INFORMATION
Sample Identification
., ....
Comamers
Sample
OOIlection
FBlemd-
WCV..
Matrix
Number&
Type. ..
e D
at7me
l
Sampler
Y or N
. C" P
or Grab
Cad e
.'
'MRS
LI
..
...
..
. ... j
.
Fi /- Y�BJy�.
oul me: -
1013()
RebekeA By:
DaleTmm 'Comments
& Special Anslytiraf Requirements:
ReNnwShed elk -
Datemme:
Received Sr.
Daternme:
Re3nquisb^d By:
DateRlme:
Received By:
Cate7Tlma:
Received 87 Laboratory.
DateTme:
Lab Remarks:
LAD USE: Custody Intact
❑Yes ON.
Custody Seals
LAB Log Number
A
UNIGINAL— RETURN TO LABORATORY WITH SAMPLES INVOICE MUST 86 SUBMITTED TO CSXT WITH ORIGINAL COC

TestAli' e(ica
MANANNEMMIll
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT
Job Number: 680-48773-1
Job Description: CSX Hamlet, NC WWTP
For:
ARCADIS U.S., Inc.
801 Corporate Center Drive
Suite 300
Raleigh, NC 27607-5073
Attention: Mr. Alan Pinnix
&V,
Kathryn Smith
Project Manager I
[e-mail]
08/10/2009
Revision: 1
WWW ...
Ke ,S n
Pl*d Man 1
W1NtMU9PM
The test results in this report meet NELAP requirements for parameters for which accreditation is required or available.
Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report
may not be reproduced, except in full, without the written approval of the laboratory. Questions should be directed.to the
person who signed this Depart.
Savannah Certifications and ID #s: A21-A: 0399.01; AL: 41450; ARDEQ: 88-0692; ARDOH; CA: 03217CA; CO; CT:
PH0161; DE; FL: E87052; GA: 803; Guam; HI; IL: 200022; IN; IA: 353; KS: E-10322; KY EPPC: 90084; KY UST; LA
DEQ: 30690; LA DHH: LA080008; ME: 2008022; MD: 250; MA: M-GA006; MI: 9925; MS; NFESC: 249; NV: GA00006;
NJ: GA769; NM; NY: 10842; NC DWQ: 269; NC DHHS: 13701; PA: 68-00474; PR: GA00006; RI: LA000244; SC:
98001001; TN: TN0296; TX: T104704185; USEPA: GA00006; VT: VT-87052; VA: 00302; WA; WV DEP: 094; WV
DHHR: 9950 C; WI DNR: 999819810; WY/EPAR8: 8TMS-Q
TestAmerica Laboratories, Inc.
TestAmerica Savannah 5102 LaRoche Avenue, Savannah, GA 31404
Tel [phone] Fax [phone] wm81esttaa _er gpin
,N ACCCq
0
�nef� F
Page 1 of 20

Job Narrative
680J48773-1
Comments
Per client request, MW7 was canceled for all analysis and metals were canceled for MW6.
Receipt
All samples were received in good condition within temperature requirements.
Metals
No analytical or quality issues were noted.
General Chemistry
No analytical or quality issues were noted.
Page 2 of 20

METHOD SUMMARY
Client: ARCADIS U.S., Inc.
Job Number: 680-48773-1
Description Lab Location Method Preparation Method
Matrix: Water
Metals (ICP)
TAL SAV
40CFR136A 200.7.Rev 4.4
Preparation, Total Metals
TAL SAV
EPA 200.7
Nitrogen, Nitrate -Nitrite
TAL SAV
MCAW W 353.2
Solids, Total Dissolved (TDS)
TAL SAV
SM SM 2540C
Organic Carbon, Total (TOC)
TAL SAV
SM SM 5310B
Lab References:
TAL SAV = TestAmerica Savannah
Method References:
40CFR136A = "Methods for Organic Chemical Analysis of Municipal Industrial Wastewater", 40CFR, Part 136, Appendix A,
October 26, 1984 and subsequent revisions.
EPA = US Environmental Protection Agency
MCAWW = "Methods For Chemical Analysis Of Water. And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SM = "Standard Methods For The Examination Of Water And Wastewater",
TestAmerica Savannah
Page 3 of 20

METHOD/ANALYST SUMMARY
Client: ARCADIS U.S., Inc.
Job Number: 680-48773-1
Method Analyst Analyst ID
40CFR136A 200.7 Rev 4.4 Bland, Brian BCB
MCAWW 353.2 Ross,Jon JR
SM SM 2540C Johnson, Brad BJ
SM SM 5310E Blackshear, Kim KB
TestAmerica Savannah
Page 4 of 20

SAMPLE SUMMARY
Client: ARCADIS U.S., Inc.
Job ,Number: 6 80-48773-1
Date/Time Date/Time
Lab Sample ID Client Sample ID Client Matrix Sampled Received
68048773-1 MW-6 Water 07/07/2009 1450 07/08/2009`0825
680-48773-3 MW-8 Water 07/07/2009 1320 07/08/2009 0825
TestAmerica Savannah
Page 5 of 20

Analytical Data
Client: ARCADIS U.S., Inc.
Client Sample ID: MW-8
Job Number: 68048773-1
Lab Sample ID:
680-48773-3
Date Sampled: 07/07/2009 1320
Client Matrix:
Water
Date Received: 07/08/2009 0825
200.7 Rev 4.4 Metals (ICP)
Method:
200.7 Rev 4.4
Analysis Batch: 680-142504
Instrument ID:
ICPD
Preparation:
200.7
Prep Batch: 680-142350
Lab File ID:
N/A
Dilution:
1.0
Initial WeightNolume:
50 mL
Date Analyzed:
07/10/2009 0325
Final Weight/Volume:
50 mL
Date Prepared:
07/09/2009 1044
Analyte
Result (ug/L)
Qualifier MDL
RL
Arsenic
20
U
4.6
20
Barium
39
2.3
10
Cadmium
5.0
U
2.0
5.0
Chromium
4.8
J
1.2
10
Lead
10
U
4.0
10
TestAmerica Savannah Page 6 of 20

Analytical Data
CI'ient: ARCADIS U.S., Inc. Job Number: 680-48773-1
General Chemistry
Client Sample ID: MW-6
Lab Sample ID: 680-48773-1
Client Matrix: Water
Analyte Result
Oual Units MDL
_
Total OrganidCarbpn ��1.0`
�"— U mg/L -�0.50
Analysis Batch: 680-142652
Data Analyzed: 07/13/2009 1419
Nitrate as N' - _ 1.3 -
mg/L 0.020
Analysis Batch: 680-142965
Date Analyzed: 07/08/20091542
Malyte Result
Qual Units RL
Total Dissolved Solids 93
mg/L 17
Analysis Batch: 680-142677
Date Analyzed: 07/14120091326'
_ RL
1.0.
0.10
RL
Date Sampled: 07/07/2009 1450
Date Received: 07/08/2009 0825
DII Method
2.0 353.2
Dil Method
TestAmerica Savannah Page 7 of20

Analytical Data
Client: ARCADIS U.S., Inc.
General Chemistry
Client Sample ID:
MW-8
Lab Sample ID:
680.48773-3
Client Matrix:
Water
Job Number: 680-48773-1
Date Sampled: 07/07/2009 1320
Date Received: 07/08/2009 0825
Analyte Result Qual Units MDL RL Dil Method
— --- ---- ... - --—---- - ------
TotalOrganicCarbon 0.61 J mg/L ---0.50 1.0 1.0 SM53108
Analysis Batch: 680-142652 Date Analyzed: 07/13/20091448
Nitrate as N 13 mg/L 0.10 0.50 10 353.2
Analysis Batch: 680-142965 Date Analyzed: 07/08/2009 1542
Analyte Result Qual Units RL RL oil Method
..__.._.
TotalDissolved Solids _.--- .---..m—g/L ....__ __....._._ -------
150 '-5.0 5.0 1.0 SM 2540C
Analysis Batch: 680-142677 Date Analyzed: 07/14/2009 1329
TestAmerica Savannah Page 8 of 20

DATA REPORTING QUALIFIERS
Client: ARCADIS U.S., Inc.
Lab Section Qualifier Description
Metals
General Chemistry
TestAmerica Savannah
Job Number: 68048773-1
U Indicates the analyte was analyzed for but not detected.
J Result is Jess than the RL but greater than or equal to the MDL
and the concentration is an approximate value.,
U Indicates the analyte was analyzed for but not detected.
J Result is less than the RL but greater than or equal to the MDL
and the concentration is an approximate value.
Page 9 of 20

Client: ARCADIS U.S., Inc.
Method Blank -Batch: 680-142350
Lab Sample ID: MB 680-142350/20-A
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 07/10/2009 0219
Date Prepared: 07/09/2009 1044
Analysis Batch: 680-142504
Prep Batch: 680-142350
Units: ug/L
Quality Control Results
Job Number: 680-48773-1
Method: 200.7 Rev 4.4
Preparation: 200.7
Instrument ID: ICP/AES - D
Lab File ID: N/A
Initial WeighWolume: 50 mL
Final Weight/Volume: 50 mL
Analyte
Result
Qual
MDL
RL
Arsenic
20
U
4.6
20
Barium
10
U
2.3
10
Cadmium
5.0
U
2.0
5.0
Chromium
10
U
1.2
10
Lead
10
U
4.0
10
Lab Control Sample - Batch:
680-142350
Method: 200.7 Rev
4.4
Preparation: 200.7
Lab Sample ID:
LCS 680-142350/21-A Analysis Batch:
680-142504
Instrument ID: ICP/AES - D
Client Matrix:
Water
Prep Batch: 680-142350
Lab File ID: N/A
Dilution:
1.0
Units: ug/L
Initial Weight/Volume:
50 mL
Date Analyzed:
07/10/2009 0224
Final WeighWolume:
50 mL
Date Prepared:
07/09/2009 1044
Analyte
Spike Amount
Result
% Rec. Limit
Arsenic
2000
2010 w.
100
85 - 115
Barium
2000
2060
103
85 - 115
Cadmium
50.0
49.1
98
85 - 115
Chromium
200
205
103
85 -115
Lead
500
505
101
85-115
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmerica Savannah Page 10 of 20
Qual

Client: ARCADIS U.S., Inc.
Matrix Spike - Batch: 680-142350
Lab Sample ID: 68048773-3
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 07/10/2009 0330
Date Prepared: 07/09/2009 1044
Analyte
Arsenic
Barium
Cadmium
Chromium
Lead
Analysis Batch: 680-142504
Prep Batch: 680-142350
Units: ug/L
Quality Control Results
Job Number: 68048773-1
Method: 200.7 Rev 4.4
Preparation: 200.7
Instrument ID: ICP/AES - D
Lab File ID: N/A
Initial WeighWolume:.50 mL
Final WeighWolume: 50 mL
Sample Result/Qual Spike Amount Result
20
U
2000
2070
39
2000
2130
5.0
U
50.0
50.6
4.8
J
200
214
10
U
500
520
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmerica Savannah Page 11 of 20
% Rec. Limit
103
75 -125
104
75 - 125
101
75 -125
105
75 -125
104
75 - 125
Qual

Client: ARCADIS U.S., Inc.
Method Blank -Batch: 680-142965
Lab Sample ID:
MB 680-142965/1
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
07/16/2009 1527
Date Prepared:
NIA
Analyte
Nitrate as
Analysis Batch: 680-142965
Prep Batch: N/A
Units: mg/L
Lab Control Sample - Batch: 680-142965
Lab Sample ID:
LCS 680-14296512
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
07/16/2009 1527
Date Prepared:
N/A
Result
0.050
Analysis Batch: 680-142965
Prep Batch: N/A
Units: mg/L
Quality Control Results
Job Number: 680-48773-1
Method: 353.2
Preparation: N/A
Instrument ID: KoneLab2
Lab File ID: N/A
Initial WeighWolume: 2 mL
Final Weight/Volume: 2 mL
Qual MDL RL
U �0.010 0.050
Method: 353.2
Preparation: N/A
Instrument ID: KoneLab2
Lab File ID: N/A
Initial WeighWolume: 2 mL
Final WeighWolume: 2 mL
Analyte
Spike Amount
Result
% Rec. Limit Qua]
Nitrate as N
�^
1.00_
1.084
108 90 -110
Matrix Spike/
Method: 353.2
Matrix Spike Duplicate
Recovery Report - Batch: 680-142965
Preparation: N/A
MS Lab Sample ID:
680.48792-A-1 MS
Analysis Batch:
680-142965
Instrument ID: KoneLab2
Client Matrix:
Water
Prep Batch: N/A
Lab File ID: N/A
Dilution:
1.0
Initial WeighWolume: 10 mL
Date Analyzed:
07/08/2009 1335
Final Weighl/Volume: 10 mL
Date Prepared:
N/A
MSD Lab Sample ID:
680-48792-A-1 MSD
Analysis Batch:
680-142965
Instrument ID: KoneLab2
Client Matrix:
Water
Prep Batch: NIA
Lab File ID: N/A
Dilution:
1.0
Initial Weight/Volume: 10 mL
Date Analyzed:
07/08/2009 1335
Final WeighWolume: 10 mL
Date Prepared:
N/A
% Rec.
Analyte
MS MSD
Limit
RPD RPD Limit MS Qual MSD Qua]
Nitrate as N--
103 - 108
90.
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmerica Savannah Page 12 of 20

Client: ARCADIS U.S., Inc.
Duplicate - Batch: 680-142965
Lab Sample ID:
680-48792-A-8 DU
Client Matrix:
Water '
Dilution:
1.0
Date Analyzed'
07/08/2009 1339
Date Prepared:
N/A
Analyte
Nitrate as N
Analysis Batch: 680-142965
Prep Batch: N/A
Units: mg/L
Sample ResultlQual
0.73
Result
0.731
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmericaSavannah Page 13 of 2d
Quality Control Results
Job Number: 680-48773-1
Method: 353.2
Preparation: N/A
Instrument ID: KcneLab2
Lab File ID: N/A
Initial WeighWolume: 2 mL
Final WeighWolume: 2 mL
RPD Limit
0 10
Qual

Quality Control Results
Client: ARCADIS U.S., Inc. Job Number: 680-48773-1
Method Blank - Batch: 680-142677 Method: SM 2540C
Preparation: N/A
Lab Sample ID: MB 680-14267711 Analysis Batch: 680-142677 Instrument ID: No Equipment Assigned
Client Matrix: Water Prep Batch: N/A Lab File ID: N/A
Dilution: 1.0 Units: mg/L Initial Weight/Volume: 100 mL
Date Analyzed: 07/14/2009 1302 Final WeighWolume: 100 mL
Date Prepared: N/A
Analyte Result Qual RL RL
Total Dissolved Solids
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 680-142677
LCS Lab Sample ID: LCS 680-142677/2
Analysis Batch: 680-142677
Client Matrix:
Water
Prep Batch: N/A
Dilution:
1.0
Units: mg/L
Date Analyzed:
07/14/2009 1302
Date Prepared:
N/A
LCSD Lab Sample ID:LCSD 680-142677/3
Analysis Batch: 680-142677
Client Matrix:
Water
Prep Batch: N/A
Dilution:
1.0
Units: mg/L
Date Analyzed:
07/14/2009 1315
Date Prepared:
N/A
% Rec.
Analyte LCS LCSD
Total Dissolved Solids 89 91
Method: SM 2540C
Preparation: N/A
Instrument ID: No Equipment Assigned
Lab File ID: N/A
Initial WeighWolume: 100 mL
Final WeighWolume: 100. mL
Instrument ID: No Equipment Assigned
Lab File ID: N/A
Initial WeighWolume: 100 mL
Final WeighWolume: 100 mL
Limit RPD RPD Limit LCS Qual LCSD Qual
60 - 120 1 25
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmerica Savannah Page 14 of 20

Client: ARCADIS U.S., Inc.
Duplicate - Batch: 680-142677
Lab Sample ID:
680.48827-A-1 DU
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
07/14/2009 1357
Date Prepared:
N/A
Analyte
Analysis Batch: ''680-142677
Prep Batch: N/A
Units: mg/L
Sample Result/Qual Result
Quality Control Results
Job Number: 680-48773-1
Method: SM 2540C
Preparation: N/A
Instrument ID: No Equipment Assigned
Lab File ID: N/A
Initial WeighWolume: 100mL .
Final WeighWolume: 100 mL
RPD Limit Qual
Total Dissolved Solids 73 67.0 g 25
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmerica Savannah. Page 15 of -20

Quality Control Results
Client: ARCADIS U.S., Inc. Job Number: 680-48773-1
Method Blank - Batch: 680-142652 Method: SM 5310B
Preparation: N/A
Lab Sample ID: MB 680-142652/2 Analysis Batch: 680-142652 Instrument ID: Total Organic Carbon Anal
Client Matrix: Water Prep Batch: N/A Lab File ID: N/A
Dilution: 1.0 Units: mg/L Initial WeighWolume: 25 mL
Date Analyzed: 07/13/2009 0949 Final Weight/Volume: 25 mL
Date Prepared: N/A
Analyte Result Qual MDL RL
Total Organic Carbon �v 1.0 U 0.50 1.0
Lab Control Sample - Batch: 680-142652
Lab Sample ID:
LCS 680-142652/4
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
07/13/2009 1023
Date Prepared:
N/A
Analyte
Total Organic Carbon
Method: SM 5310B
Preparation: NIA
Analysis Batch: 680-142652 Instrument ID: Total Organic Carbon Anah
Prep Batch: N/A Lab File ID: N/A
Units: mg/L Initial WeighWolume: 25 mL
Final Weight/Volume: 25 mL
Spike Amount Result % Rec.
20.0 18.8 94
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 680-142652
MS Lab Sample ID: 680-48749-M-2 MS Analysis Batch: 680-142652
Client Matrix: Water Prep Batch: N/A
Dilution: 1.0
Date Analyzed: 07/13/2009 1118
Date Prepared: N/A
MSD Lab Sample ID: 680-48749-M-2 MSD Analysis Batch: 680-142652
Client Matrix: Water Prep Batch: N/A
Dilution: 1.0
Date Analyzed: 07/13/2009 1131
Date Prepared: N/A
Limit Qual
80-120 --
Method: SM 5310B
Preparation: N/A
Instrument ID: Total Organic Carbon
Lab File ID: N/A
Initial WeighWolume: 25 mL
Final WeighWolume: 25 mL
Instrument ID: Total Organic Carbon Anal'.
Lab File ID: N/A
Initial Weight/Volume: 25 mL
Final Weight/Volume: 25 mL
% Rec.
Analyte MS MSD Limit RPD RPD Limit
Total Organic Carbon— --- 91� T 92 80 - 120 1
Calculations are performed before rounding to avoid round -off errors in calculated results.
MS Qual MSD Qual
TestAmerica Savannah Page 16 of 20

Client: ARCADIS U.S., Inc.
Duplicate - Batch: 680=142652
Lab Sample ID:
68048764-A-2 DU
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
07/13/2009 1405
Date Prepared:
N/A
Analyte
Total Organic Carbon
Analysis Batch: 680-142652
P.rep.Batch: N/A.
Units: mg/L
Quality Control Results
Job Number. 68048773-1
Method: SM 5310B
Preparation: N/A
Instrument ID: Total"Organic. Carbon Anah
Lab File ID: N/A
Initial Weight/Volume: 25 mL
Final Weight(Volume: 25 mL
Sample Result/Qual
Result
RPD
Limit
1.6
1.53
3
25
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmerica Savannah Page 17 of 20
Qual

CHAIN OF
TRANSPORTATION CUSTODY
TAL-60060907
LABORATORY INFORMATION I
COC #
EUesuirmaca Savannah - 6102 LaRoche Avenue. Savannah. GA 314N P: 912-354-7858 F: 912-352-0165
OTestAmetico North Canton -4101 Shuttel Olive NW. Nunn Canton. Oil 44720 P:330.497.9396 F:330-497-0772
(] TestAmenw Tampa - 6712 Bentanno Road. Suite 100. Tampa. FL 33634 P: 813 805.7427 F: 813.885.7049
❑TestAmerica Pensacola- 3355 McLemere Olive. Pensacola. FL 32514 P: 650-474-1001 F: 850.478.2671
❑TesWnedca Buffalo- ICHatelelood Olive, Suite 106.A01110M. NY 14228 Pt7164191-260o F:716-961-7991
❑TeslAmedca Chicago -.2417 Bond Street. UNversdy Park. IL 66466 P:708534-5200 F:708.534-5211
SHIPMENT INFORMATION
Shipment Method: 'Ce y
I /-
Shipment Tracking No:
CSXT PROJECT INFORMATION Prof. Slope (State of Origin) `
CONSULTANT INFORMATION project v. NC I O O?, 00ag
CSXT Project Numoer: ,SZ7 Proj. City: A� 'IoT'aY
J It
Company. y{nl6yc� PM: AI_„ p'kq,x
CSXT Project Name: � W �
>, e
C//dll!rri9� � Pr. Emit: 2P k®grcadls-vz cam
Address: i Q i NN. t
CSXT Contact LWON: 6 5
< ,n
Gry, Stale. alp: q ei I 7 *' / � ��Q_7 Phone: q/p ,co3uj _' l F ;
r'1 rV li t e" 1 �'r�`
Turnaround Time: ❑ Standard 6-13 Days
❑ 1 Day Rush Specify # Days
❑ 2 Day Rush ®Standard 14 Days
❑ 3 Day Rush ❑ Other
Preservative Codes: 3=Sulfuric Acid Note tr
D - No Preservatives 4 = Sodium Thiosuliate Pres.
t = Hydrochloric Acid 5 = Sodium Hydroxide Code
2 = Nitric Acid 6 = Other
COMMENTS
LAB USE
METHODS
FOR
ANALYSIS
M
T
M
M
_�
0
N
E
8
N
f
:
N
d
p
^
^,
nn•
O
N
t
7
rJ
M
v1
J
1J
D liverables: ❑ Other Deliv:
CSXT Standard (Level II)
❑ Level III SEDD Required, Format:
❑ Level IV CSYT
Matrix Codes: SO = Soil LID = Liquid
GW = GrounWrater SL = Sludge
W W = Waste Water OI = Oil
SW te Surface Water SOL=Other Solid
SAMPLE INFORMATION
Sample Identification
Containers
Sample Collection
Filtered I
T er lMatrix
Number 8
yP
Date
Time
Sampler
Y or N
or Grab
Code
oq
145o
90
N
6r
^w
XIX
iC
X
X
w-
t6ss
R�
6r
�
?C
X
�u-g
ado
Ro
N
eu-A'
Relnquished ey' _
DaIe7Nne� I l 11
3
Receiv
ey: ` _ .
Date
e:
Comments & Special Analytical Requirements:
Relinquished By:
Dale7Thne:
Received By:
Oate/Time:
Relinquished By:
Doldrums:
Received By:
Dalerruna:
Received By Laboratory:
Daterrime:
Lab Remarks:
LAB USE: Custody Intact
❑Yes ❑No
,.,.,.,,.•�..,,�.==eo.nrrenm
Custody Seal Y
#
caul vertu nmr_iu ai
LAB Log Number
#
rnr
ORIGINAL - RETURN TO LABORATORY WITH SAMPLES

' •'
CHAIN OF
TRANSPORTATION CUSTODY
TAL-60060907
LABORATORY INFORMATION
-F:912.352.0165
COC
7estarnerica Savannah-5102LaRw4eAvenue,Savannah,GA31404 P.912354-7858
OTeslAmerira Nonh Canton -4101 Shallot Drive NW, Noah Carron, OH44720 P:330.497.9396 F-330-497-0772
❑TeaiAmendd Tampa-6712 Oeniamin Road, suite Ital TamOa. R 33634 P:813-885-7427 F:813-885d049
OTestAmPensacola Drive, Pensacola, FL 32514 P:850.474.1001 F.850.478.2671
O TesWnhIC2 Renato -10 Haeeve0ed Drive- Suite lO6,Amhersl. NY 14228 P:716-691-2600 F:716-961.7991
OTesWnerira CWUQO-241780nd SVeel.University PadY IL60466 P:706.534-5200 F.708.534.5211
SHIPMENTTNFORMATION
shipment Method:enca
1 f^
re G C
ShiP-.MT1aekin9 No:
CSXT PROJECT INFORMATION Prof. State (State of Origin)
N �,
CSXT Project Number: q [� Prof. city.,FyI a�11.I p
1 I Wn O-
CSXT Project Name: LJ_ I_ 1p
11�4 iC/ 1/U 1 /��'•�
CSXT Contact: /1 I w LWON:ENV 3Slp-�p-
/•t d•1❑3
CONSULTANT INFORMATION Projectill: WC I° p , °�
J
'emPany' RCA 1S . PM. `Clh PI ik5i1. .
Address: Fol CO LOr p� A t�1M
0" Ci 1.G1.1� ►^ pi". Email, P X®0.YYl( �fJS •CO ILv
C'[y.Stale. Lp:. 141(e1 1
Vbl l/ 8 r { 7
Turnaround Time: Standard 6-13 Days
❑ 1 Day Rush Specify If Days
❑ 2 Day Rush ®Standard 14 Days
❑ 3 Day Rush ❑ Other
Preservative Codes: 3= Sulfuric Acid Note
0 = No Preservatives 4 = Sodium.Thiosullate Pres.
I = Hydrochloric Acid 5 = Sodium Hydroxide Code
2 =. Nitric Acid 6 = Other
COMMENTS
LAB USE
METHODS
FOR
ANALYSIS
'verabies: ❑ Other Deliv:
CSXT Standard (Level II)
❑ Level III ® EDD Required, Format:
❑ Level IV 1;* isn
Matrix Code,: SO = Soil LIO = Liquid
GW = Groundwater SL =Sludge
W W = Waste Water, 01= Oil
SW=Surface Water SOL=Other Solid
n
H
SAMPLE INFORMATION
Sample Identification
Containers
Small Collection
Filtered
Tvoe
livatrix
yp
ch
Number &
Type
Date
Time
Sampler
Y or N
Comp
or Grab
Code
I
MW-
7 °
1�5-
W95
Is"
20
RO
PO
y
C?
ET
G
Tl��L'U�
Kw
rvw
X
r,uq>y
iuwJ I J
iuu,J
�oM1Y
44T
Relinquished _
Da tern e:
Ftecei aBY: 1i, r
Dae
me:
Comments&Special Analytical Requirements:
Vie -
{.8o-L(�7j'1J
Relinquished BY:.
Dat me:
Received By:
Dale rune: _
Relinquished By:
Date/Time:
Received By:
Date7Time:
Received By LaDoaatory;
ORIGINAL - RETURN TO I AR0RATORV WtTN CAIA01
Dale/Time:
Re
Lae Remarks:.
LAB USE: Custody intact
Ely..
' ON,
Custody Seal a
p
LAB Log Number
a
INVOICE MUST BE SUBMITTED'TO CSXT WITH ORIGINAL COO

Login Sample Receipt Check List
Client: ARCADIS U.S., Inc.
Login Number: 48773
Creator: Conner, Keaton
List Number: 1
Question
T / F/ NA Comment
_
Radioactivity either was not measured or, if measured, is at or below
N/A
background
The cooler's custody seal, if present, is intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent Information.
True
There are no discrepancies between the sample IDs on the containers and
True
the COC.
Samples are received within Holding Time.
True
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
VOA sample vials do not have headspace or bubble is <6mm (1/4") In
N/A
diameter.
If necessary, staff have been informed of any short hold time or quick TAT
True
needs
Multiphasic samples are not present.
N/A
Samples do not require splitting or compositing.
N/A
Is the Field Samplers name present on COC?
False
Sample Preservation Verified
True
Job Number: 680-48773-1
List Source: TestAmerica Savannah
TestAmerica Savannah Page 20 of 20

TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT
Job Number: 680-49451-1
Job Description: CSX Hamlet, NC
For:
ARCADIS U.S., Inc.
801 Corporate Center Drive
Suite 300
Raleigh, NC 27607-5073
Attention: Mr. Alan Pinnix
Ap 1m,W sa.
N Mw Srt th
Prg.Meneprl
9llR 11:15 AM
Kathryn Smith
Project Manager I
[e-mail]
08/07/2009
The test results in this report meet NELAP requirements for parameters for which accreditation is required or available.
Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report
may not be reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the
person who signed this report.
Savannah Certifications and ID #s: A2LA: 0399.01; AL: 41450; ARDEQ: 88-0692; ARDOH; CA: 03217CA; CO; CT:
PH0161; DE; FL: E87052; GA: 803; Guam; HI; IL: 200022; IN; IA: 353; KS: E-10322; KY EPPC: 90084; KY UST; LA
DEQ: 30690; LA DHH: LA080008; ME: 2008022; MD: 250; MA: M-GA006; MI: 9925; MS; NFESC: 249; NV: GA00006;
NJ: GA769; NM; NY: 10842; NC DWQ: 269; NC DHHS: 13701; PA: 68-00474; PR: GA00006; RI: LA000244; SC:
98001001; TN: TN0296; TX: T104704185; USEPA: GA00006; VT: VT-87052; VA: 00302; WA; WV DEP: 094; WV
DHHR: 9950 C; WI DNR: 999819810; WY/EPAR8: 8TMS-Q
TestAmerica Laboratories, Inc.
TestAmerica Savannah 5102 LaRoche Avenue, Savannah, GA 31404
Tel [phone] Fax [phone] m .testamericafn�p
,µ ACCCq
Page 1 of 8

METHOD SUMMARY
Client: ARCADIS U.S., Inc.
Job Number: 680-49451-1
Description Lab Location Method Preparation Method
Matrix: Water
Nitrogen, Nitrate -Nitrite
Lab References:
TAL SAV = TestAmerica Savannah
Method References:
TAL SAV MCAWW 353.2
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600l4-79-020, March 1983 And Subsequent Revisions.
TestAmerica Savannah
Page 2 of 8

METHOD/ANALYST SUMMARY
Client: ARCADIS U.S., Inc.
Job Number: 680-49451-1
Method Analyst Analyst ID
MCAWW 353.2 Ross, Jon JR
TestAmerica Savannah
WA
Page 3 of 8

SAMPLE SUMMARY
Client: ARCADIS U.S., Inc.
Job Number: 680-49451-1
Date/Time Date/Time
Lab Sample ID Client Sample ID Client Matrix Sampled Received
680-49451-1 MW-8 Water
TestAmerica Savannah
07/30/2009 1030 07/31/2009 0935
Page 4 of 8

Client: ARCADIS U.S., Inc.
General Chemistry
Analytical Data
Job Number: 680-49451-1
Client Sample ID: MW-8
Lab Sample ID: 680-49451-1 Date Sampled: 07/30/2009 1030
Client Matrix: Water Date Received: 07/31/2009 0935
Analyte Result Qual Units MDL RL Dil Method'
Nitrate as N _ -y'_-'.rv�__.-�� 11 mg/L--'i�0:10 - -��0.50--��—�100 353.2
Analysis Batch: 680-144556 Date Analyzed: 07/31/2009 1656
I
TestAmerica Savannah I Page 5 of 8

DATA REPORTING QUALIFIERS
Client: ARCADIS U.S., Inc.
Lab Section Qualifier Description
General Chemistry
TestAmerica Savannah
Job Number: 680-49451-1
U Indicates the analyte was analyzed for but not detected.
MS or MSD exceeds the control limits
Page 6 of 8

Client: ARCADIS U.S., Inc.
Method Blank -Batch: 680-144556
Quality Control Results
Job Number: 680-49451-1
Method: 353.2
Preparation: N/A
Lab Sample ID:
MB 680-14455611
Analysis Batch: 680-144556
Instrument ID: KoneLab2
Client Matrix:
Water
Prep Batch: N/A
Lab File ID: N/A
Dilution:
1.0
Units: mg/L
Initial WeighUolume: 2 mL '
Date Analyzed:
08/04/2009 1715
Final WeighWolume: 2 mL
Date Prepared:
N/A
Analyte
Result Qual
MDL RL
Nitrate as N
^
0.050 U
0.010 0.050
Lab Control Sample - Batch: 680-144556
Lab Sample ID:
LCS 680-144556/2
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
08/04/2009 1715
Date Prepared:
N/A
Analysis Batch: 680-144556
Prep Batch: N/A
Units: mg/L -
Analyte Spike Amount Result
Nitrate as N 1.00 1.02
Matrix Spike/
Matrix Spike Duplicate Recovery Report -'Batch: 680-144556
MS Lab Sample ID:
680-49514-F-1 MS Analysis Batch: 680-144556
Client Matrix:
Water Prep Batch: N/A
Dilution:
1.0
Date Analyzed:
08/04/2009 1728
Date Prepared:
N/A
MSD Lab Sample ID: 680-49514-F-1 MSD Analysis Batch: 680-144556
Client Matrix:
Water Prep Batch: N/A
Dilution:
1.0
Date Analyzed:
08/04/2009 1728
Date Prepared:
N/A
Analyte
Nitrate as N
% Rec.
MS MSD Limit
88 95 90-
Method: 353.2
Preparation: N/A
Instrument ID: KoneLab2
Lab File ID: N/A
Initial WeighWolume: 2 mL
Final WeighWolume: 2 mL
% Rec. Limit Qual
102 90-110
Method: 353.2
Preparation: N/A
Instrument ID: KoneLab2
Lab File ID: N/A
Initial WeighWolume: 10 mL
Final Weight/Volume: 10 mL
Instrument ID: KoneLab2
Lab File ID: N/A
Initial Weight/Volume: 10 mL
Final WeighWolume: 10 mL
RPD RPD Limit MS Qual MSD Qual
Calculations are performed before rounding to avoid round -off errors in calculated results.
10 F
TestAmerica Savannah Page 7 of 8

b
w
w
m
CHAIN OF
TRANSPORTATION CUSTODY
TAL.60060907
LABORATORY INFORMATION
' -
COC #
strumeric4 Savannah - 5102 LaRoche Avenue. Savannah. GA 31404 P. 912-354-7858 F: 912-352-0165
TesWnenra Noah Canton-4101 Shutter Drive NW, North Canton. OH 44720 P.330-497.9396 F:33G-49E-0T72
pTeciAmenra Tampa.6712 Benjamin Road, Suite 100. Tampa. FL 33634 P:813-885d427 P:813.685-7049
p restolmerica Pensacola -3355 McLemwe Onve. Pensacola, FL 32514 P.850-474-1001 P 1150.478.2671
pTestAmetica Buffalo -10 Huelxood Drive.Sure 106.Arimcal, NY 14228 P:716.691.2600 F: 716.961-7991
07eatAmerlea Chicago -2417 Bond Street. University Path, It 60466 P.708-534.5200 F:708.534-5211
SHIPMENT INFORMATION
ShipmentMallod: ['� _I�
I C. Ex rr-s$
Shipment Tracking No: q�/t r1 /-��
0d
CJ — �D76 6
CSXT PROJECT INFORMATION Prof. State (Slate of Origin)
CONSULTANT INFORMATION Project 0: 11 c 1 o a0 31.000 $
CSXT Project Number: p�� 2oa- Prof.Cliy: Artale
11
Company:
RCAM1 , PM: Aph
pinnl'
CS%7 Project Name: 1-1 v 1
fw-o
Address:�f /�.•..- ......fin tome, TV Email: ApinMX(BYfr�. ll--ll$.C-Ni
V".
��11
CSXT Contact: q.l. AX-lis LWON: ENV SWL9, MA
City, State. Zip:Dale1 NC a76o-� Phone: ql °�-&5`f -Id(p2 Fax:
1lNote
Turnaround Time: ❑ Standard 6-13 Days
❑ 1 Day Rush Specify # Days
❑ 2 Day Rush Standard 14 Days
❑ 3 Day Rush ❑ Other
Preservative Codes: 3 - Sulfuric Acid
0 = No Preservadves 4 = Sodium Thiosulfate Pres,
1 = Hydrochloric Acid 5 = Sodium Hydroxide Code
2 = Nitric Acid '6 = Other
l)
COMMENTS
LAB USE
METHODS
FOR
ANALYSIS
Lr)
+
Ilverablos: ❑ Other Deliv:
CSXT Standard (Level ll)
❑ Level III EDD Required, Format:
❑ Level IV
Matrix Codes: SO = Soil LID = Liquid
GW = Groundwater SL=Sludge
WW = Waste Water 01= Oil
SW = Surface Water SOL = Other Solid
SAMPLE INFORMATION
Sample Identification
containers
Sam le Collection
Filtered I
Type
Matrix
Number &
Type
Date
Time
Sampler
Y or N
Comp
or Grab
Code
1P��'�
30 0
Io30
DT
N
CIMIs
GM
Rerinquished By.
Date/Tlma_,/W 'ZOO
Received By;
Date/Time:
Comments & Special AnalytiGel Requirements:
Relinquished By.
Date7Time:
Received By:
Dale rune:
Relinquished By:
DaleTlne:
Received By.
Dalernme:
ived By Laoorafory:
..__. ..._.
D-altelTime:
Oq�i
_�
Lab Remarks:
'
.INVnIrP
LAB USE: Custody Intact
❑Yes ❑No
MII£TRF g11RMITTPn
Custody Seal 9
#
TO CgXT WITH ORIGINAL
LAB
0
COC
ORIGINAL - RETURN 10 LAt30HAIOHT W i I n wMPLES

TRANSPORTATION
Jerry L. Cato REM
Supervisor Environmental Control
North Carolina Department
Of Natural Resources
Attn: Information Processing Unit
Division Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Dear Sir or Madam:
May 22,
File. 96:
Permit No. W00000601, Richmond County
CSX Transportation, Inc. (CSXT), Hamlet. NC
500 Water Street— J275
Jacksonville, FL 32202
(FAX) (904) 5-2827
WFIVEE
JUN 01 20
OENR-FAVETfE1ALL E REGIONAL OR3CE
Attached in triplicate, is the first triennial 2009 Ground Water Monitoring Well
Analyses, as specified by Condition 4 of the referenced permit. Due to the drought conditions at
this location, monitoring well No. 6 did not have enough water to collect a sample.
If you have any questions or comments, please contact me at [phone].
Enclosures
Sincerely, /
C,,,Ierry L. Cato
RECEIVE®
MAY 2 S 2009
WATtn
l . JC, i iON
Information Processing Lint'

GW-59A COMPLIANCE REPORT FORM Permit #14Laoo
(Submit one each monitoring period with GIR59 forms.)
I
Enter date monitoring results were due. - -d Will this monitoring report (GW-59 and GW-59A)
YES
NO
be submitted after the established due date? ` n
'See-rc.yry
It:'Htr'
Z
Was any required Information missing on the GW-59 report forms?
YES
N
IF the answer to question I or 2 is "YES'; list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
Identification plate, area overgrown, etc.)? /'the answer is —yes", contact the Regional Ofce'arguldance.
"
4
Are any monitored constituents equal to or above the established standards?
YES
NO
If, the answer to question 4 is NO", skip to section B.
If the answer to question 41s "YES" list the affected wells Individually with constituent(s) and concentration(s)
exceeding standards in the space provided below.
,p I
mt,) .5 Clnrovn!'UM. 0.o5Y `'1/� `.�ruM,i ym �tmtt: (9.05ul'G
Mw'► i Ckrowt:c�n. ; C).d18 uy/� t.
M W �$ i 0-1%row\:ugn , V .G'1R; u1 L t� t
r c
5
F6r the consti uents Identified In question 4 Spoth, have standards been exceeded previously fdrhhe
YES
NO
same constituent(s) in the same well(s) in th°e last two years?
✓
If the answer to question 5 is NO'; skip to section 8.
if the answer to question 5Is "YES" list in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample'collection date for each occurrence (for the last two years).
h,Li 41, G.ors, v"I/L, L'1-9-ovi. C:vum:uw�: (5.4tBu(/1 t (3-24-08)
mW Ftg, d•a"le u1/Ll (3-24-09)_
6
Are the monitoring wells listed in section 5located at or beyond the review boundary?
YES
Nn
If the answer Is "YES", a groundwater quality problem maybe occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer Is "NO", monitoring wells maybe Improperly
located; contact the Regional Office.
7
Is the permittee implementing previously approved actions required by the Division Involving this
YES
NO
groundwater quality problem?
X
If the answer to question 7 is "YES , describe those actions in the space provided below.
If the answer to question 71s "NO'; contact the Regional Office within 90 days., an evaluation maybe
required to determine the impact the waste disposal system Is having at the review and compliance
boundaries surrounding this facility. Failure to do so may sublect the permittee to a Notice of Violation
tines. and/or penalties.
8
The person completing this portion (G W-59A) of the monitoring report should sign below and submit this
form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
I
hereby acknowledge that the o , information was evaluated and the Information submltteil n this"
(Co7Repo eA
wreport
pi'
.meWesfmnwledge
.,.
S
5 Uri —of —Pen4ff Authorized Agent) Date
\ C11'-59A 12/8/2003

rNew
TRANSPORTATION
Cal A. Gerhardslein, P.E.
Director Environmental Systems
Mr. Joel Shields
North Carolina Department of
Environment and Natural Resources
Division of Water Quality
225 Green Street - Suite 714
Fayetteville, NC 28301
Dear Mr. Shields:
s_charge Permit No.
Transportation. I
April 22, 2009
0000601 - Hamlet
500 Water Street-1275
Jacksonville, FL 32202
[phone]
(FAX) [phone]
The above referenced permitted facility has a tri-annual
monitoring requirement. The first monitoring for 2009 could not be
completed by the reporting time limit of April 28, 2009. Our contract
laboratory, Environment 1, Inc. attempted to collect monitoring well
samples at the Hamlet facility on March 17, 2009 and again on March
24, 2009. Due to problems with the pump controller unit, Environment
1 was unable to collect samples on either of the two dates. The pump
controller has been repaired and samples will be collected on April
27th.
If you have any questions or comments, please do not hesitate to
contact me at [phone].
Sincerely
Ka�'A
North Carolina DENR
Division of Water Quality
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
"Environmentally on Track"

Facility Name CSX Transportation - Hamlet Wastewater Treatment Facility
Facilty, Address 173 CSX Drive
Hamlet, NC 28345 County Richmond
Contact Person: MIKE GREGORY Telephone #: [phone]
Well Location/Sity Name: see location map No, of Wells to be Sampled: 8
Well Identification Number (From Permit): MW_1 Iror urounowater Treatment
Systems
Well Depth: 53.75 ft. Well Diameter. 4.0 in. Check One:
Screened Interval: ft. to R ®In0uent (98)
Depth to Water Level: 50.15 ft. below measuring point 7M Effluent (99)
Measuring point (M.P.) is: ft. above land surface Relative M.P. Elevation in fL: _
Gallons of water pumped/bailed before sampling: 3.9 Date Sample Collected 04/30/Of
Field Analysis: pH 5. Specific Conductance uMhos
Temp. _ ° C Odor Appearance
.�[phone]
PERMIT #: EXPIRATION DATE: November 30, 2009
Non -Discharge WO0000601 UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field Remediafion:
Rotary Distributor Land Application of Sludge
X Other Monitoring Well
NOTE, Values should reflect dissolved and collaidal concentrations
Date Sample Analyzed
Laboratory Name: ENVIRONMENT 1, INC
Cerfification No. 10
PARAMETERS: (Samples for metals were collected unfiltered _X_ YES NO and field acidified _X_ YES NO)
COD
mg/l
Colifonn: MF 'Fecal/
100ml
Coliform: MF Total
/ 100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids Total 41.
mg/l
pH (when analyzed)
units
TOC <1.
mg/I
Chloride
mg/l
Arsenic <0.005
mg/l
Grease and Oils _
Phenol
Sulfate
Specific Conductance
Total Ammonia _
TKN as N
Nitrite (NO2) as N
Nitrate (NO3) as N
Phosphorus: Total as P
Orthophosphate
AI -Aluminum
Ba - Barium
Ca - Calcium
Cd - Cadmium
Chromium: Total
Cu - Capper _
Fe - Iran
Hg - Mercury
K - Potassium
Mg - Magnesium
Mn - Manganese
SECTION Unity
1.46 mg/l
mg/l
mg/l
mg1l
0.01 mo/I
<0.001 mg/I
0.021 mg/l
ma/I
—mg/l
mg/I
mg/I
Ni - Nickel
mg/l
Pb - Lead 0.008 mg/l
Zn - Zinc mg/l
Ammonia Nitrogen mg/l
Other (Specify Compounds and concentration units)
ORGANICS: (GC, GC/MS, HPLC)
(Specify test and method #. Attach lab report.)
Report Attached?Yes_(1) No_(0)
VOC : method#=
VOC : method#=
VOC : method#=

FORM ON YELLOW PAPER ONLY
Facility Name Hamlet Wastewater Treatment Facili
Facilty Address CSX Transportation, Box 191A Highway 177N
Hamlet, NC 28345 County Richmond
Contact Person: M. L. GREGORY [phone]
Well Location/Sity Name: Location Map Attached
Well Identification Number: MW-2 For Gmundmiw Treanenl eyalema
Well Depth: 41.48 ft. Well Diameter: 4.0 in. Cher1( One:
Screened Interval: ft. To ft. ® Influent (98)
Depth to Water Level 35.7 ft. below measuring point. ❑o Effluent (99)
Measuring point is ft. above land surface
Gallons of water pumped/bailed, before sampling: 10.9
Field Analysis pH 4.5 Specific Conductance uMhos
Temp. e C Odor Appearance
PARAMETERS: (Samples for metals were collected unfiltered X YES
CO
mg/l
Coliform: MF Fecal
/100m1
Coliform: MF Total
/ 100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids Total 74.
mg/I
PH (when analyzed)
units
TOC 2.74
mg/I
Chloride
- mg/I
Arsenic <0.005
mg/i
Grease and Oils
mg/I
Phenol
mg/1
Sulfate
mg/1
Specific Conductance
Mhos
Total Ammonia
mg/I
TKN as N
mail
ss,
.._.-.' •.Phone.
PERMIT M EXPIRATION DATE November 30, 2009
Non -Discharge W00000601 UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field _
_ Rotary Distributor _
X Other Monitoring Well
Remediation: Infiltration Gallery
Remediation
Land "Application of Sludge
NOTE Values should reflect dissolved and collaldai concentrations
Date Sample Collected 04/30/09 Date Sample Analyzed
Laboratory Name ENVIRONMENT 1, INC
Certification No. 10
NO and field acidified _X_ YES NO)
NO 2 as N
mgll
NO-3 as N
2.14
mg/1
Phosphorus: Total as P
mg/I
Orthophosphate
mg/I
At - Aluminum
mg/1
Be - Barium
0.016
mg/1
Ca - Calcium
mg/I'
Cd- Cadmium
<0.001
mg/I
Chromium: Total
<0.005
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/i
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
NI - Nickel mg/1
Ph- Lead <0.005 mg/I
Zn - Zinc mg/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and concentration units)
ORGANICS: (GC, GC/MS, HPLC)
(Specify test and method #. Attach lab report.)
Report Attached? Yes —(I) No_(0)
VOC : method#=
VOC : method #=
VOC : method#=

PAPER ONLY
Facility Name Hamlet Wastewater Treatment Facility
Facilty Address CSX Transportation, Box 191A Highway 177N
Hamlet, NC 28345 County Richmond
Contact Person: M. L. GREGORY [phone]
Well Location/Sity Name: Location Map Attached
Well Identification Number: MW-3 IC Ger 00XMTMe nlsy
cn� x oo:
Well Depth: 45.70 ft. Well Diameter: 4.0 in.
Screened Interval: ft. To ft. ® Influent (98)
Depth to Water Level 39.8 ft. below measuring point. ® Effluent (99)
Measuring point is f . above land surface
Gallons of water pumpedibailed before sampling: 6.
Field Analysis pH 5.1 Specific Conductance uMhos
Temp. ° C Odor Appearance
PERMIT M EXPIRATION I
Non -Discharge WQ0000601 UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field
Rotary Distributor
X Other Monitorinc
Remediation: Infiltration Gallery
Remediation
Land Applicr
of Sludge
NOTE Values should reflect dissolved and collalcial concentrations
Date Sample Collected 04/30/09 Date Sample Analyzed
Laboratory Name ENVIRONMENT 1; INC
Certification. No. 10
(Samples for metals were collected unfiltered _X_ YES NO and field acidified _X_ YES NO)
CO mg/I
Coliform: MF Fecal / 100m[
Coliform: MF Total / loom[
(Note: Use MPN method for highly turbid samples)
Dissolved Solids Total
pH (when analyzed)
TOC
Chloride
Arsenic
<0.005
49. mg/I
mg/I
Grease and Oils
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
Mho'.
Total Ammonia
mg/I
TKN as N
migil
GW59 Rev. 4198
NO_2 as N
mg/I
NO 3 as N
1.46
mg/l
Phosphorus: Total as P
moll
Orthophosphate
mg/I
At -Aluminum
moll
Be - Barium
0.01
mg/I
Ca - Calcium
mg/I
Cd- Cadmium
<0.001
mg/I
Chromium: Total
0.012
mg/I
Cu - Copper
moll
Fe - Iron
mg/1
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
NI - Nickel mg/l
Pb - Lead <0.005 moll
Zn - Zinc moll
Ammonia Nitrogen mg/I
Other (Specify Compounds and concentration units)
ORGANICS: (GC, GC/MS, HPLC)
(Specify test and method#. Attach lab report.)
Report Attached? Yes. (1) No_(0)
VOC : method#=
VOC : method#=
VOC : method#=

ON YELLOW PAPER ONLY
Facility Name Hamlet Wastewater Treatment Facility
FaciltyAddress CSX Transportation, Box 191A Highway 177N
Hamlet, NC 28345 County Richmond
Contact Person: M. L. GREGORY [phone]
Well Location/Site Name: Location Map Attached
Well Identification Number: MW-4 ForGrourdwaWTreab ntSysmms
ceorxone:
Well Depth: 47.45 ft. Well Diameter: 2_0 in.
Screened Interval: ft. To _ft. ❑0 Influent (98)
Depth to Water Level 35.4 ft. below measuring point. 0 Effluent (99)
Measuring point is ft. above land surface
Gallons of water pumpedibailed before sampling: 5.4
Field Analysis pH 5.6 Specific Conductance uMhos
Temp. °C Odor Appearance
PARAMETERS: (Samples for metals were collected unfiltered _X_ YES
CO
mg/l
Coliform: MF Fecal
/ 100m1
Coliform: MF Total
/ 100m1
(Note: Use MPN method for highly turbid samples)
Dissolved' Solids Total 60.
mg/I .
pH (when analyzed)
units
TOC 1.24
mg/I
Chloride
mg/1
Arsenic <0.005
mg/I
Grease and Oils
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
Mhos
Total Ammonia
mg/I
TKN as N
mall
(919)7333221, .I
PERMIT #: EXPIRATION DATE November 30, 2009
Non -Discharge W00000601 UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Remediation: Infiltration Gallery
Spray Field
Remediation
Rotary Distributor
Land Application of Sludge
X Other Monitoring
Well
NOTE Values should reflect dissolved and collaldal concentrations
Date Sample Collected 04/30/09 Date Sample Analyzed
Laboratory Name ENVIRONMENT 1, INC
Certification No. 10
NO and field acidified _X_ YES NO)
NO 2 as N
mg/I
NO-3 as N
2.15
mg/I
Phosphorus: Total as P
mg/l
Orthophosphate
mg/I
Al -Aluminum
mg/I
Ba.- Barium
<0.01
mg/l
Ca - Calcium
mg/I
Cd - Cadmium
<0.001
mgll
Chromium: Total
0.02
mg/I
Cu - Copper
mgll
Fe - Iron '
mgll
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg -Magnesium
mg/I
Mn-- Manganese
mg/l
NI - Nickel mg/I
Pb - Lead <0.005 mg/I
Zn - Zinc mg/1
Ammonia Nitrogen mg/I
Other (Specify Compounds and concentration units)
ORGANICS: (GC, GC/MS, HPLC)
(Specify test and method #. Attach lab report.)
Report Attached? Yes_(1) No_(0)
VOC : method#=
VOC : method#=
VOC : method #=
Environmental
- Please print or
GW59 Rev. 4198 signature rpeionIltee, (bf Autho?MM Agent)

SUBMIT F
PAPER ONLY
DANCE REPORT FORM
r
Facility Name Hamlet Wastewater Treatment Facility
Facilty Address CSX Transportation Box 191A Highway 177N
Hamlet, NC 28345 County Richmond
Contact Person: M. L. GREGORY [phone]
Well Location/Sity Name: Location Map Attached
Well Identification Number: MW-5 Fc� x owc :NaWT.tmerlsyGWM
Well Depth: 52.92 ft. Well Diameter: 2_0 In.
Screened Interval: ft. To ft. ❑3 Influent (98)
Depth to Water Level 42.1 ft. below measuring point. ® Effluent (99)
Measuring point is fL above land surface
Gallons of water pumpedibailed before sampling: 4.8
Field Analysis pH 5:2 Specific Conductance uMhos
Temp. _' C Odor Appearance
PARAMETERS: (Samples for metals were collected unfiltered _X_YES
CO
mg/I
Coliform: MF Fecal
/ 100ml
Coliform: MF Total
/ 100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids Total 71.
mg/l
pH (when analyzed)
units
TOC 1.33
mgll
Chloride
mg/I
Arsenic <0.005
mgll
Grease and Oils
mg/1
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
Mhos
Total Ammonia
mg/I
TKN as N
mg/l
GW-59 Rev. 4198
PERMIT #:
Non -Discharge
NPDES
EXPIRATION DATE November 30, 2009
W00000601 UIC
TYPE OF PERMITTED OPERATION BEING MONITORED
_ Lagoon
_ Spray Field
Rotary Distributor _
X Other Monitoring Well
Remediation: Infiltration Gallery
Remediation
Land Application of Sludge
NOTE Values should reflect dissolved and collaldal concentrations
Date Sample Collected 04/30/09 Date Sample Analyzed
Laboratory Name _ ENVIRONMENT 1, INC
-Certification No. - 10
NO and field acidified _X_ YES NO)
NO_2 as N
mgn
NO_3 as N 0.9
mgfl
Phosphorus: Total as P
mg/I
Orthophosphate
mgn
Al -Aluminum
mg/I
Be -Barium 0.026
mg/1
Ca - Calcium _
Cd- Cadmium _
Chromium: Total
Cu -Copper _
Fe - Iron
Hg - Mercury _
K-Potassium _
Mg - Magnesium
Mn - Manganese
<0.001 mg/I
0.054 mg/I
NI - Nickel mg/I
Pb - Lead <0.005 mg/I
Zn -Zinc mg/I
Ammonia Nitrogen mg1l
Other (Specify Compounds and concentration units)
ORGANICS: .(GC, GC/MS, HPLC)
(Specify test and method #. Attach lab report.)
Report Attached?Yes_(1) No_(0)
VOC : method#=
VOC : method#=
VOC : method # =

rOROU
NDWALIANCE P
Facility Name
Facilty Address
Contact Person'.
Well,Location/Sity
. SUBMIT FORM ON YELLC
MONITOk21NG$,
x Fd
s
•r Treatment Facility "
in Box 191A Highway 177N
i County ° "'' Richmond
[phone] ,.
-
a8on Map Attached
PAPER ONLY
nVISION OF WATER QUALITY
oROUNDWATER SECTION. PE
Oz Box 27667 `
talelgh, NC 27611 7667
IAITS AND COMPIjA J UNIT
Phone [phone] "
PERMIT #: 'EXPIRATION DATE November 30, 2009
Non -Discharge W00000601 UIC
NPDES ,
TYPE OF PERMITTED OPERATION BEING MONITORED,
` Lagoon' -`Reimediation:InfiltrationGallery
R diation
Well Identification Number:'
MW-6om;
rorc,ov mrrreee,�1.sj�.,,
,.--. Spray Field eme
Rotary Distributor Land Application of Sludge
Well Depth: 48.35
-ft. Well Diameter: 2.0 'In.
❑O Influent (96)'
X Other Monitoring Well'
—
Screened Interval:
Depth to Water Level
A. _To.' ft.
ft.:below-measuring point,
O Effluent (99}
'
NOTE : Values should reflect dissolved and collaidal concentr@tlons
-Measuring-pointis ft. abovelandsurface
Gallons of water pumpedfbailed before sampling:
'Date Sample' Collected Date Sample Analyzed ..
'Field Analysis._ pH'-
'spe'clfic Conductance
`•.: �' ` - uMhos
.• Laboratory Name'ENVIRONMENT 1 INC .. -
Temp. _'C
Odor'''
Appearance
certification No., '10' _
PARAMETERS: -(Samples for metals were collected unfiltered _X- YES . ;'
NO and field acidified _X=YES NO)
- mgll
NO_2' as N
' ^ mgll 'NI,- Nickel , ' mgll
.CO
Coliform:MFFecal.
,110om
31 NO_.as,N
mg1t."Pb -Lead • moll
mgll
Coliform:-MF Total
4,100ml
'
Phosphorus: Total as P
mgll. Zn -ZInc
mgli Ammonia Nitrogen' - mgll
(Note: Use MPN method for highly
turbid samples)
Orthophosphate
-Aluminum
mgll--Other'(Specify'Compounds and concentration units),
Dissolved'Solids Total :
. mg/1 .
AI
pH (when analyzed)
units,
Be. Barium'
moll
TOC
mg/l .
Ca -Calcium
moll '
Chloride'
mg11.'',.Cd-Cadmium
m9N .
Arsenic -
` mgli ..
Chromium; Total ' '
mgfi
Grease and Oils
mg11
Cu -Copper'
mgll
'- 'mg/l ORGANICS: (GC,GC/MS,.HPLC)
Phenol
Sulfate
.<•mgll,-,.Fe-Iron,
mg/l
' Hg - Mercury
moll „,(Specify test and method #. Attach lab•re ort.)
P
,
,,Specific Conductance-'
Mhos',
f(-Pota slum
m ► Re ort'Attached? Ye
gl p s_(1) ,No_(o)
'
'Total Ammonia'
moll
Mg - Magnesium
mg/l• VOC method #=
7KN as N
mgll
Mn -Man ganese .
mgll, VOC : method #_ '
VOC method#=
GW-59 Rev. 4198
,t
Systemsl- -
itle -. Please'pnnt or type

SUBMIT FORM ON
ONLY
L7KW.UPIUYY9'I, r-F%%IVAr-ra r,,nw• • .r! .vim ...._..
cbMPLIANCE REPORT°FORM
Facility Name Hamlet Wastewater Treatment Facility
Facllty Address CSX Transportation BOX 191A Highway 177N
Hamlet, NC 28345 County Richmond
Contact Person: M. L. GREGORY [phone]
Well Location/Sity Name: Location Map Attached
For Grou:-W,Tmat .tSyateaa
Well Identification Number: MW-7 Chaaoaa:
Well Depth: 37.18 ft. Well Diameter: 2_0 In. ® Influent (98)
Screened Interval: ft. To ft. m Effluent (99)
Depth to Water Level 30.8 ft. below measuring point.
Measuring point is fL'above land surface
Gallons of water pumped bailed before sampling: 3•
Field Analysis pH 4.6 Specific Conductance uMhos
Temp. C Odor Appearance
PARAMETERS: (Samples for metals were collected unfiltered _X_YES
CO
r.rlp,
Coliform: MF Fecal
1100ml
Coliform: MF Total
1100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids Total 66.
mg/I
PH (when analyzed)
units
TOC 3.09
mgll
Chloride
mg/I
Arsenic <0.005
m91I
Grease and Oils
mg/i
Phenol
mg/I
Sulfate
mg11
Specific Conductance
Mhos
Total Ammonia
mg/I
TKN as N
mg/I
GW-59 Rev. 4198
PERMIT M EXPIRATION DATE November 30, 2009
Non -Discharge W00000601 UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
_ Lagoon _ Remediation: Infiltration Gallery
_ Spray Field _ Remediation
Rotary Distributor _ Land Application of Sludge
X Other Monitoring Well
NOTE Values should reflect dissolved and collaidal concentrations
Date Sample Collected 04/30/09 Date Sample Analyzed
Laboratory Name ENVIRONMENT 1, INC
Certification No. 10
NO and field acidified X_ YES NO)
NO_2 as N
mgn
NO-3 as N
2.36
mg/I
Phosphorus: Total as P
mg/I
Orthophosphate
mg/I
All -Aluminum
ing/l
Ba - Barium
0.024
mg/I
Ca - Calcium
mg/I
Cd- Cadmium
<0.001
mgll
Chromium: Total
0.078
mg/I
Cu -Copper
Fe -Iron
Hg -Mercury _
K - Potassium _
Mg - Magnesium
Mn - Manganese
Ni - Nickel mgn
Pb - Lead <0.005 mg/I
Zn - Zinc mg/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and concentration units)
ORGANICS: (GC, GCIMS, HPLC)
(Specify test and method #. Attach lab report.)
Report Attached? Yes_(1) No_(0)
VOC : method#=
VOC : method#=
VOC : method#=

ON
PAPER ONLY
Facility Name Hamlet Wastewater Treatment Facility
Facilty Address CSX Transportation Box 191A Highway 177N _
Hamlet, NC 28345 County Richmond
Contact Person: M. L. GREGORY (910)58&4901
Well Location/Sity Name: Location Map Attached
Far Gmmu--W,Tmam MSystems
Well Identification Number: MW-8 cnea�oae:
Well Depth: 57.18 ft. Well Diameter: 2_0 in. ® influent(98)
Screened Interval: ft. To _fL ® Effluent (99)
Depth to Water Level 43.2 ft. below measuring paint.
Measuring point is ft. above land surface
Gallons of water pumped/balled before sampling: 6.3 .
Field Analysis pH 4.9 Specific Conductance ' uMhos
Temp. C Odor Appearance
PARAMETERS: (Samples for metals were collected
CO
Coliform: MF Fecal
...1.
/ 100ml
Col'dorm: MF Total '
/ 100m1
(Note: Use MPN method for highlyturbid samples)
Dissolved Solids Total 167.
mg/I
PH (when analyzed)
_units
TOC - 1.86
mgli
Chloride
mg/l
Arsenic <0.005
mg/I
Grease and Oils
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
Mhos
Total Ammonia
mg/I
TKN as
mg/I
GW-59 Rev. 4198
PERMIT M EXPIRATION DATE November 30, 2009
Non -Discharge W00000601 UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
X YES NO
_ Lagoon _ Remediation: Infiltration Gallery
_ Spray Field _ Remediation
Rotary Distributor _ Land Application of Sludge
X Other Monitorin I Well
NOTE Values should reflect dissolved and collaidal concentrations
Date Sample Collected 04/30/09 Date Sample Analyzed
Laboratory Name ENVIRONMENT 1, INC -
Certification No. 10
and field acidified X_ YES NO)
NO_2 ,as N
mg/I
NO_3 as N
12.93
mg/I
Phosphorus: Total as P
_mg/I
Orthophosphate
mg/I
At -Aluminum
mg/I
Ba - Barium
0.056
mg/I
Ca - Calcium
rrtg/I
Cd- Cadmium
40.001
mg/I
Chromium: Total
0.078
mg/I
Cu - Copper-
mg/
Fe - Iron
mgl
Hg -Mercury
mgl
K- Potassium
mgl
Mg - Magnesium
mgi
Mn -Manganese
mgi
NI - Nickel mgll
Pb - Lead <0.005 -mg/I
Zn -Zinc mg/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and concentration units)
ORGANICS: (GC, GC/MS, HPLC)
(Specify test and method #. Attach lab report.)
Report Attached?Yes_(1) No_(0)
VOC method#=
VOC method#= ..
VOC method#=

EAmMUMMIM9 T, k60uOPeW
CSX TRANSPORTATION (HAMLET)
MIRE GREGORY
173 CSX DRIVE
HAMLET ,NC 28345
DATE COLLECTED: 04/30/09
DATE REPORTED : 05/08/09
REVIEWED BY:
MW-1 MW 2 MW-3 MW4 MW-5 Analysis Method
PARAMETERS Date Analyst Coda
PH (Field measurement), Units 5.0 4.5 5.1 5.6 5.2 04/30/09 RJH SM450OBB
Nitrate Nitrogen as N, mg/l 1.46 2.14 1.46 2.15 0.90 05101109 TWA EPA353.2
TotalOrganic Carbon, mg/1 <1.00 2.74 1.01 1.24 1.33 05104/09 SEJ SM5310C
Total Dissolved Residue, mg4 41 74 49 60 71' 05/06/09 TER SM2540C
Arsenic, ug/l <0.005 <0.005 <0.005 <0.005 <0.005 OS/01/09 CMF SM3113B
Barium, ug/l 0.010 0.016 0.010 <0.010 0.026 05/01/09 LFJ EPA200.7
Cadmium, ug4 <0.001 <0.001 <0.001 <0.001 <0.001 05/05/09 CMF SM3113D
Total Chromium, ug/l 0.021 <0.005 0.012 0.020 0.054 05/01/09 LFJ EPA200.7
Lead, ug4 0.008 <0.005 <0.005 <0.005 <0.005 05104109 CMF SM3113B
Static Water Level, feet 50.15 35.73 39.81 35.47 42.12 04/30/09 RJH
Water Bailed, Gals. 3.9 10.9 6.0 5.4 4.8 ' 04/30/09 RJH

Environment 1, Incor1=
CSX TRANSPORTATION (HAMLET).
MIXB GREGORY
173 CSX DRIVE
HAMLET ,NC 28345
ID#: 4
DATE COLLECTED: 04/30/09
DATE REPORTED : 05/08/09
REV13WED BY:
MW-6
MW-7
MW-8
Analysis
Method
PARAMETERS
Date Analyst
Code
PH (field measurement), Units
Missing
4.6
4.9
04/30/09
RJH
SM450OBB
Nitrate Nitrogen as N, mg/1
Missing
2.36
12.93
05/01/09
TWA
EPA353.2
Total Organic Carbon, mg/1
Missing
3.09
1.86
05/04/09
SEi
SM5310C
Total Dissolved Residue, mg/l
Missing
66
167
05/06/09
TRB
SM2540C
Arsenic, ug/l
Missing
<0.005
<0.005
OS/01/09
CMF
SM3113B
Barium, .ug/l
Missing
0.024
0.056
05/01/69
LFJ
EPA200.7
Cadmium, u9/1
Missing-
<0.001
<0.001
05/05/09
CMF
SM311313
Total Chromium, ug/1
Missing
0.078
0.07s
05/01/09
LFJ
EPA200.7
Lead, ug/1
Missing
<0.005
<0.005
05/04/09
CMF
SM3113B
Static Water Level, feet
Missing
30.89
43.26
04/30/09
RJB
{hater Bailed, Gals./
Missing
3.0
6.3
04/30/09
RJH

CSX QA/QC DATA SUMMARY
FACILITY: hamlet SAMPLE DATE: 04/30/09
SAMPLE LOCATION: Monitoring Wells
PARAMETER: Nitrate Nitrogen
Duplicates RPD =1.1 % (acceptable value is < 14.751/6)
Quality Control Standard Recovery =101.0 % (acceptable value is 85-115%)
Blank Value = 0.00 mg/1
PARAMETER: Total Organic Carbon
Duplicates RPD = 0.2 % (acceptable value is <10.84%)
Quality Control Standard Recovery =106.2 (acceptable value is 85-115%)
Blank Value = 0.06 mg/1
PARAMETER: Total Dissolved Residue
Duplicates RPD = 0.3% (acceptable value is <6.151/6)
*Quality Control Standard Recovery =102.2% (acceptable value is 90-100%)
Blank Value = 0.0 mg/1
* Value reported for required quarterly QC standard. "
RPD (Relative Percent Difference)
Quality control data for individual metals analyses is attached on the following
pages.

ICP
Ongoing Quality Control

TEST:_
GRAPHITE FURNACE - INITIAL & ONGOING QUALITY CONTROL
Date of Analysis: __5� / / / 09
Analyst Initials: e. l
Value, ugll
Result, ug/l
Sequence #
RL
Acceptance
Pass —Fail
Blank Check
( 0.0 )
0, )SG
r
<_ RL
( )
Value, ug/l
Result, ug/l
Sequence # -
% Recovery
Acceptance
Pass --Fail
Initial Calibration Verification
Zs-, o
$
96"
_+10%
(
Value, ug/l
Result, ug/l
Sequence #
°/o Recovery
Acceptance
Pas? —Fail
Detection Limit Standard
S: o
y, yy2
7
°l8
+10%
Value, ug/I
Value, ug/l
Value, ug/l
Value, ug/l
Value, ug/l
Initial Calibration Levels
0.0
, o
/o,
( z r o
SO.D
Value, ug/l
Result, ug/l
Sequence #
RL
Acceptance
Pass —Fail
Digested Method Blank W,*$ y-/
0 0'
0.039)
/o
_.r_
< RL
)
Rio r /
Value, upJl
Result, ug/l
Sequence #
% Recovery
Acceptance
Pass —Fail
LCS Second Sourcemid-point)
f.o
2T.SC
tI
9Y
+15%
_-)
Digested
Spike Amount, ug/l
Spike Result, ug/1
Sequence #
% Recovery
Acceptance
Pass --Fail
Matrix Spike
r S: o
a y, G 9,
( /3 )
( 99 )
±20%
L:: �)
Sample Name:
#1
GS)C SOY
Client ID# y
Sampla Result, up I
Sequence #
Location Code: wo It
09, o8z
( 12 )
Date: y-30
Digested MS
Spike Amount, ug/l
Spike Result, ug/1
Sequence #
% Recovery
Acceptance
Pass -Fail
±20%
I Dimlicate #1
25 d
y, e?
RPD
Acceptance
Pa�%s—Fail
Spike Duplicate Results
(
RPD <20%
Value, ug/l
Result, ug/1
Sequence #
RL
Acceptance
Pass --Fail
Digested Method Blank
( 0.0 1
<RL
(
LCS Second Source mid- oint
Value, ug/l
Result, ug/1
Sequence #
%Recovery
Acceptance
+15%
Pass --Fail
Digested
i Matrix Spike
Spike Amount, ug/l
[_�
Sample Name:
Spike Result, ug/l
(_�
Sequence # .
��
% Recovery
(_�
Acceptance
±20%
Pass ---Fail
#2
Client ID#
Sample Result, uga
Sequence #
Location Code:
Date:
Digested MS
Spike Amount, ug/1
Spike Result, ug/I
Sequence #
°/a Recovery
Acceptance
Pass ---Fail
Duplicate #I
+20%
RPD
Acceptance
Pass --Fail
Spike Duplicate Results
RPD
Value, ug/l
Result, ug/l
Sequence #
RL
Acceptance
Pass --Fail
Digested Method Blank
0.0
(
< RL
(
Value, ug/1
Result, ug/1
Sequence #
% Recovery
Acceptance
Pass —Fail
LCS (Second Sourcc mid -point)
+15%
Digested
Spike Amount, ug/l
Spike Result, ug/l
Sequence #
% Recovery
Acceptance
Pass --Fail
Matrix Spike
±20%
Sample Name:
#3
Client"
Sample Result, ug/I
Sequence #
Location Code:
Date:
Digested MS
Spike Amount ug/l
Spike Result, ug/l
Sequence #
% Recovery
Acceptance
Pass --Fail
+20%
Duplicate #1
(
RPD
Acceptance
Pass --Fail
Spike Duplicate Results
RPD <20%
)

TEST: G'o�
GRAPHITE FURNACE - INITIAL & ONGOING QUALITY CONTROL
Date of Analysis: __r_/ L/_O
Analyst Initials: cM�
Value, ug/1
Result, ug/l
Sequence #
RL
Acceptance
Pass --Fail
Blank Check
0.
-a.
S
I
<RL
Value, ug/l
Result, ug/1
Sequence #
% Recovery
Acceptance
Pass --Fail
Initial Calibration Verification
-2, fd
z, t8 z
I o
.103,
+10%
Value, ug/1
Result, ugll
Sequence #
%Recovery
Acceptance
Pass —Fail
Detection Limit Standard
( !.. o
) , oYS
l �S
+10%
Value, ug/1
Value, ugfl
Value, ug/1
Value, ug/l
Value,' ug/l
Initial Calibration Levels
( O.O
1; o
( 12.r
o
Value, ug/1
Result, ug/I
Sequence #
RL
Acceptance
Pass ---Fail
Digested Method Blank WtV -1
0.0
- A' of
T I
I
< RL
__- )
Wa-•f /
Value, ug/l ,
Result, ugll
Sequence #
% Recovery
Acceptance
Pass --Fail
LCS (Second Source mid -point)
Z.s 0
Z•f?/
Z 2 ,
I 1
±15%
( -f
Digested
Spike Amount, ug/l.
Spike Result, ug(I
Sequence #
% Recovery
Acceptance
Pass —Fail
Matrix Spike
( Z.JV )
(3, IGS)
c zv )
( l61 )
±20%
t_�(-j
Sample Name:
Client ID# it
Sample Result, ug/l
Sequence #
Location Code: Woy
0,571
( 73 )
Date: Y-30
Uigested MS
Spike Amount, ug/l
Spike Result, ug/1
Sequence #
% Recovery
Acceptance
Pass --Fail
Duplicate #1
z .rd)
10 /
+20%
RPD
Acceptance
Pass- Fail
Spike Duplicate Results
RPD Q0%
( (
Value, ug/l
Result, ug/l
Sequence #
RL
Acceptance
Pass--Fail
L Digested Method Blank
0.0
p
l
Value, ug/l
Result, ugA
Sequence #
%Recovery
Acceptance
Pass --Fail
! LCS (Second Sauce raid -point)
+15%
Digested
Matrix Spike
Spike Amount, ug/l
(_�
Spike Result ug/1
( 1
Sequence #
(_�
% Recovery
(
Acceptance
±20%
Pass —Fail
I-) �)
Sample Name:
#2
Client ID#
Sample Result, ug/1
Sequence #
'
Location Code:
Date:
Digested MS
Spike Amount, ug/1
Spike Result, ug/1
Sequence #
% Recovery
Acceptance
Pass --Fail
Dt licate#1
(
(
+20%
RPD
Acceptance
Pass —Fail
Spike D licate Results
RPD QO%
Value, ug/1
Result, ug/I
Sequence #
RL
Acceptance
Pass --Fail
DigestedMethodBlank
0.0
( )
<RL
LCS (Second Source mid -point)
Value, ug/I
Result, ug/1
Sequence #
% Recovery
Acceptance
+15%
Pass —Fail
Digested
Matrix Spike
Spike Amount, ug/l
��
Spike Result, ug/l
(_�
Sequence #
��
% Recovery -
(_�
Acceptance
±20%
Pass —Fail
Sample Name:
#3 .
Client ID#
Sample Result, ug/l
Sequence #
Location Code-
Date:
Digested MS
Duplicate #I
Spike Amount, ug/l
Spike Result, ug/1
Sequence #
% Recovery
Acceptance
+20%
Pass --Fail
RPD
Acceptance
Pass —Fail
Spike Duplicate Results
(
RPD <20%
( )

TEST: P
GRAPHITE FURNACE - INITIAL & ONGOING QUALITY CONTROL
Date of Analysis: _3- /_/ 0 9
Analyst Initials: e--*/
Value, ug/l
Result, ug/l
Sequence #
RL
Acceptance
Pass —Fail
Blank Check
0.0 .
O,
e
5
<_ RL
)
Value, ug/l
Result, ugll
Sequence #
% Recovery
Acceptance
Pass —Fail
Initial Calibration Verification
z S.a
7.f o
S
loo
+10%
Value, ugA
Result, ug/1
Sequence #
/o Recovery
Acceptance
Pa�Fail
Detection. Limit Standard
5 , O
Y f7.f
l &'d
±100/0
Value, ugA
Value, ug/l
Value, ug/I
Value, ug/1
Value, ug/l
Initial Calibration Levels
4, D
, O
d,o
z ,D
0, e)
Value, ugA
Result, ug/I
Sequence #
RL
Acceptance
Pass —Fail
DigestedMethodBlankWjVs-/
0.0
D,zBI
1i
<RL
W6W rj
Value, ugA
Result, ugll
Sequence #
% Recovery
Acceptance
Pass ---Fail
LCS Second Source mid -point)
(z f.v
(211,72)
ZZ
9
±15%
( Il
Digested
Spike Amount, ug/l
Spike Result, ug/l
Sequence #
% Recovery
Acceptance
Pass --Fail
.Matrix Spike
z f.0
z� 29
( 2 t/ )
/( O 1 )
+20%
(� U
#t
Sample Name:
G'sx y�y
Client ID# V
Sample Result, ugA
Sequence #
Location Code: woV
O f,9I
( Z3 )
Date: -Td
Digested MS
Spike Amount, ug/l
Spike Result, ug/1
Sequence
%Recovery
Acceptance
Pass, —Fail
I Duplicate 01
s D
( 2S,/
let
+20%
( ) )
RPD
Acceptance.
Paste -Fail
So. ike Du licate Results
d
RPD QO%'
Value, ugA
Result ug/I
Sequence #
RL
Acceptance
Pass —Fail
Digested Method Blank I
L_0_-0__1<RL
Value, ug/l
Result, ug/l
Sequence #
% Recovery
Acceptance
Pass --Fail
LCS (Second Source mid- oint)
+15%
Digested
Matrix Spike
Spike Amount, ug/l '
( 1
Spike Result, ug/l
��
Sequence #
( )
% Recovery
�_)
Acceptance
±20%
Pass —Fail
U U
Sample Name:
#2
Client ID#
Sample Result, ug/l
Sequence #
Location Code:
Date:
Digested MS
Spike Amount, ugA
Spike Result, ug/l -
-Sequence #
% Recovery
Acceptance
Pass --Fail
+20%
Duplicate 01
(
( )
RPD
Acceptance
Pass --Fail
Spike Duplicate Results
RPD «0%
Value, ug/l
I
Result, ug/l
Sequence #
RL
Acceptance
Pass —Fail
Digested Method Blank
C_±1_)<RL
(
Value, ug/l
Result, ug/l
Sequence #
%Recovery
Acceptance
Pass —Fail
LCS (Second Source mid -point)
(
+15%
( )
Digested
Spike Amount, ug/l
Spike Result, ug/l
Sequence #
% Recovery
Acceptance
Pass —Fail
Matrix Spike
(�
��
��
(_)
±20%
U (j
Sample Name:
H3
Client ID#T—
Sample Result, ug/l
Sequence #
Location Code:
Date:
Digested MS
Du licate #I
Spike Amount ug/1
(
Spike Result, ug/l
Sequence #
% Recovery
Acpt ceance
Pass --Fail
+20%
RPD
Acceptance
Pass --Fail
Spike Duplicate Results
RPD <20%
( )

Environmi...i 1, Inc
P.O. Box 7085,114 Oakmont Dr.
Greenville, NC 27858
CHAIN OF CUSTODY RECORD
Page 1 of
:. •
• ,
(910)205-079
eeeee■■■■■■■■■■■
••
eases■■■■■■■■■■■
CHEMICALPRESER
ONE •.
•
■. ,
IJDPMINGWATER
• ••
dim©■■■■■■■■■■
-�
£�■■■■■■■■■■
� .r . rs•M■■©
,IN
.
Mi■e
�
■■■■■■■■■■
.:
-
peg --
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C' forcomposite sample or a "G" for N 0— 177931
FORM a5 Gmb sample in the blocks above for each parameter requested.

J