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HomeMy WebLinkAboutNC0036269_Application_20180510lkM,., 11660. Water -Resources ENVIRONMENTAL QUALITY May 10, 2018 Mark Fowler, Facilities Director Water and Sewer Authority of Cabarrus County PO Box 707 Concord, NC 28025 Subject: Permit Renewal Application No. NC0036269 Rocky River WWTP Cabarrus County Dear Applicant: ROY COOPER Gavvrmr R1ICHAEL S. REGAN Secrermy LUgDA CULPEPPER Mertm Dhwtor The Water Quality Permitting Section acknowledges the May 2, 2018 receipt of your permit renewal application and supporting documentation. Your application will be assigned to a permit writer within the Section's NPDES WW permitting branch. Per G.S. 1SOB-3 your current permit does not expire until permit decision on the application is made. Continuation of the current permit is contingent on timely and sufficient application for renewal of the current permit. The permit writer will contact you if additional information is required to complete your permit renewal. Please respond in a timely manner to requests for additional information necessary to allow a complete review of the application and renewal of the permit. Information regarding the status of your renewal application can be found online using the Department of Environmental Quality's Environmental Application Tracker at: https•//deg nc gov/permits-regulations/permit guidance/environmental application tracker If you have any additional questions about the permit, please contact the primary reviewer of the application using the links available within the Application Tracker. SiincceQruell &y '�Qkd Wren Thedford Administrative Assistant ec: WQPS Lasertiche File w/application (MRO) Water Quality Permitting Section State of North Carolina I Environmental Quality I Water Resources 1617 Mail Service Center I Raleigh, North Carolina 27699-1617 919-807-6300 WSACC 150140011015 • NC Star Public Sector ♦ OHSAS 181101:2007 April 30, 2018 CERTIFIED MAIL RETURN RECEIPT REQUESTED NC DENR / DWQ Attn: NPDES Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 WATER & SEWER AUTHORITY OF CABARRUS COUNTY Administrative Offices 232 Davidson Hwy, Concord, NC 28027 704.786.1783 ♦ 704.795.1564 Fax Rocky River Regional WWTP 6400 Breezy Lane, Concord, NC 28025 704.788.4164 ♦ 704.786.1967 Fax www.wsacc.org Subject: NPDES #NC0036269 Renewal Application Rocky River Regional Wastewater Treatment Plant (RRRWWTP) Enclosed is the subject permit renewal application, topographic map showing the point of discharge, plant process schematic and supporting documentation for required toxicity results. Since the previous permit cycle, RRRWWTP has triggered the 26.5 MGD permit tier and is currently abiding by those limits. WSACC requests that NCDENR evaluate this trigger during the renewal process based on the average daily 3- year flow rate of 16.69 MGD being so much lower than the 21.6 MGD trigger and that the exceedance was only 21.9 MGD occurring during a record -breaking rainfall event. Thank you for your consideration of this matter. If you have any questions or comments, please feel free to contact either myself at 704.788.4164, ext. 111 or John Ritchie, Wastewater Operations Manager/ORC at 704.788.4164, ext. 114 or jritchie iftsacc.oro. Sincerely, (' \ T. Mark Fowler Facilities Director TMF/JR/blc Enclosures: Application, Topographic Map, Plant Process Schematic and Toxicity Result Data cc: NCDENR (2) John Ritchie File FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Rocky River Regional Wastewater Treatment Plant Renewal Yadkin Pee Dee , NCO036269 FORM 2A &DES FORM 2A APPLICATION OVERVI NPDES APPLICATION OVERVIEW Form 2A has been developed in a modular format and consists of a "Basic Application Information" packet and a "Supplemental Application Information" packet. The Basic Application Information packet is divided into two parts. All applicants must complete Parts A and C. Applicants with a design flow greater than or equal to 0.1 mgd must also complete Part B. Some applicants must also complete the Supplemental Application Information packet. The following items explain which parts of Form 2A you must complete. BASIC APPLICATION INFORMATION: A. Basic Application Information for all Applicants. All applicants must complete questions A.1 through A.8. A treatment works that discharges effluent to surface waters of the United States must also answer questions A.9 through A.12. B. Additional Application Information for Applicants with a Design Flow z 0.1 mgd. All treatment works that have design flows greater than or equal to 0.1 million gallons per day must complete questions BA through B.6. C. Certification. All applicants must complete Part C (Certification). SUPPLEMENTAL APPLICATION INFORMATION: D. Expanded Effluent Testing Data. A treatment works that discharges effluent to surface waters of the United States and meets one or more of the following criteria must complete Part D (Expanded Effluent Testing Data): Has a design flow rate greater than or equal to 1 mgd, Is required to have a pretreatment program (or has one in place), or Is otherwise required by the permitting authority to provide the information. E. Toxicity Testing Data. A treatment works that meets one or more of the following criteria must complete Part E (Toxicity Testing Data): 1. Has a design flow rate greater than or equal to 1 mgd, 2. Is required to have a pretreatment program (or has one in place), or 3. Is otherwise required by the permitting authority to submit results of toxicity testing. F. Industrial User Discharges and RCRA/CERCLA Wastes. A treatment works that accepts process wastewater from any significant industrial users (SIUs) or receives RCRA or CERCLA wastes must complete Part F (Industrial User Discharges and RCRA/CERCLA Wastes). SIUs are defined as: 1. All industrial users subject to Categorical Pretreatment Standards under 40 Code of Federal Regulations (CFR) 403.6 and 40 CFR Chapter I, Subchapter N (see instructions); and 2. Any other industrial user that: a. Discharges an average of 25,000 gallons per day or more of process wastewater to the treatment works (with certain exclusions); or b. Contributes a process wastestream that makes up 5 percent or more of the average dry weather hydraulic or organic capacity of the treatment plant; or C. Is designated as an SIU by the control authority. G. Combined Sewer Systems. A treatment works that has a combined sewer system must complete Part G (Combined Sewer Systems). ALL APPLICANTS MUST COMPLETE PART C (CERTIFICATION) EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Pagel of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Rocky River Regional Wastewater Treatment Renewal Yadkin Pee Dee Plant, NCO036269 BASIC APPLICATION INFORMATION PART A. BASIC APPLICATION INFORMATION FOR ALL APPLICANTS: All treatment works must complete questions A.1 through A.8 of this Basic Application Information Packet A.I. Facility Information. Facility Name Rocky River Regional Wastewater Treatment Plant Mailing Address 6400 Breezy Lane Concord, North Carolina 28025 Contact Person John W. Ritchie Title Wastewater Operations Manager Telephone Number (704) 7884164 ext. 118 Facility Address 6400 Breezy Lane (not P.O. Box) Concord, North Carolina 28025 A.2. Applicant Information. If the applicant is different from the above, provide the following: Applicant Name Water and Sewer Authority of Cabarrus County Mailing Address 232 Davidson Highway Concord North Carolina 28025 Contact Person Mark Fowler Title Facilities Director Telephone Number (704) 7884164 ext. 111 Is the applicant the owner or operator (or both) of the treatment works? ® owner ❑ operator Indicate whether correspondence regarding this permit should be directed to the facility or the applicant. ❑ facility ® applicant A.3. Existing Environmental Permits. Provide the permit number of any existing environmental permits that have been issued to the treatment works (include state -issued permits). NPDES NCO036269 PSD Emergency Generator No. 08780G01 UIC Other Air Permit No. 04475R19 RCRA Other Collection System Permit No. WQCS00009 A.4. Collection System Information. Provide information on municipalities and areas served by the facility. Provide the name and population of each entity and, if known, provide information on the type of collection system (combined vs. separate) and its ownership (municipal, private, etc.). Name Population Served Type of Collection System Ownership Charlotte Water 61,000 separate municipal Towns of Harrisburg & Mt. Pleasant 19,395 & 2,121 separate separate municipal municipal Cities of Kannaoolis & Concord 43,856 & 82,596 separate. separate municipal, municipal Total population served 208,968 EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 2 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Rocky River Regional Wastewater Treatment Renewal Yadkin Pee Dee Plant, NCO036269 A.6. Indian Country. a. Is the treatment works located in Indian Country? ❑ Yes N No b. Does the treatment works discharge to a receiving water that is either in Indian Country or that is upstream from (and eventually flows through) Indian Country? ❑ Yes ® No A.6. Flow. Indicate the design flow rate of the treatment plant (i.e., the wastewater flow rate that the plant was built to handle). Also provide the average daily flow rate and maximum daily flow rate for each of the last three years. Each year's data must be based on a 12-month time period with the 12' month of "this year' occurring no more than three months prior to this application submittal. a. Design flow rate 26.5 mgd Two Years Ago Last Year This Year b. Annual average daily flow rate 16.81 16.2 17.05 C. Maximum daily flow rate A.7. Collection System. Indicate the type(s) of collection system(s) used by the treatment plant. Check all that apply. Also estimate the percent contribution (by miles) of each. ® Separate sanitary sewer 100 % ❑ Combined storm and sanitary sewer NIA % A.8. Discharges and Other Disposal Methods. a. Does the treatment works discharge effluent to waters of the U.S.? ® Yes ❑ No If yes, list how many of each of the following types of discharge points the treatment works uses: I. Discharges of treated effluent ii. Discharges of untreated or partially treated effluent III. Combined sewer overflow points iv. Constructed emergency overflows (prior to the headworks) V. Other NIA b. Does the treatment works discharge effluent to basins, ponds, or other surface impoundments that do not have outlets for discharge to waters of the U.S.? ❑ Yes If yes, provide the following for each surface impoundment: Location: Annual average daily volume discharge to surface impoundment(s) Is discharge ❑ continuous or ❑intermittent? C. Does the treatment works land -apply treated wastewater? If yes, provide the following for each land application site: Location: Number of acres: Annual average daily volume applied to site: WA Is land application ❑ continuous or ❑ intemlittent? d. Does the treatment works discharge or transport treated or untreated wastewater to another treatment works? one mgd ❑ Yes ❑x No mgd ❑ Yes N No EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 3 of 22 FACILITY NAME AND PERMIT NUMBER: Rocky River Regional Wastewater Treatment PERMIT ACTION REQUESTED: RIVER BASIN: Plant , NC0036269 Renewal Yadkin Pee Dee If yes, describe the mean(s) by which the wastewater from the treatment works is discharged or transported to the other treatment works (e.g., tank truck, pipe). N/A If transport is by a party other than the applicant, provide: Transporter Name N/A Mailing Address Contact Person Title Telephone Number I_ ) For each treatment works that receives this dischame, provide the following: Name N/A Mailing Address Contact Person Title Telephone Number ( ) If known, provide the NPDES permit number of the treatment works that receives this discharge N/A Provide the average daily flow rate from the treatment works into the receiving facility. N/A mgd e. Does the treatment works discharge or dispose of its wastewater in a manner not Included in A.8. through A.8.d above (e.g., underground percolation, well injection): ❑ Yes ® No If yes, provide the following for each disposal method: Description of method (including location and size of site(s) if applicable): N/A Annual daily volume disposed by this method: N/A Is disposal through this method ❑ continuous or ❑ intermittent? EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 4 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Rocky River Regional Wastewater Treatment Renewal Yadkin Pee Dee Plant, NCO036269 WASTEWATER DISCHARGES: If you answered Wes" to question A.8.a, complete questions A.9 through A.12 once for each outfall (including bypass points) through which effluent Is discharged. Do not include Information on combined sewer overflows in this section. If you answered "No" to question A.8.a go to Part "Additional Application Information for Applicants with a Design Flow Greater than or Equal to 0.1 mgd." A.9. Description of Outfall. a. Ouffall number b. Location (Coy or town, if applicable) (Zip Code) (County) (State) 35 deg 19 min 30.5 sec 80 deg 32 min 09.6 sec (Latitude) (Longitude) C. Distance from shore (if applicable) N/A ft. d. Depth below surface (if applicable) N/A ft. e. Average daily flow rate 16.69 mgd f. Does this outall have either an intermittent or a periodic discharge? ❑ Yes ® No (go to A.9.g.) If yes, provide the following information: Number f times per year discharge occurs: WA Average duration of each discharge: N/A Average flow per discharge: N/A mgd Months in which discharge occurs: N/A g. Is ouffall equipped with a diffuser? ❑ Yes ® No A.10. Description of Receiving Waters. a. Name of receiving water Rocky River b. Name of watershed (if known) Rocky River United States Soil Conservation Service 14-digit watershed code (if known): 03010405020020 C. Name of State Management/River Basin (if known): Yadkin -Pee Dee United States Geological Survey 8-digit hydrologic cataloging unit code (if known): 03040105 d. Critical low flow of receiving stream (if applicable) acute N/A cis chronic 25.2 summer 35.2 winter cfs e. Total hardness of receiving stream at critical low flow (if applicable): Average 88.2 mg/L (26 samples) mg/I of CaCO3 EPA Form 3510-2A (Rev. 1.99). Replaces EPA forms 7550-6 & 7550-22. Page 5 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Rocky River Regional Wastewater Treatment Renewal Yadkin Pee Dee Plant NCO036269 A.11. Description of Treatment a. What level of treatment are provided? Check all that apply. ® Primary ® Secondary ❑ Advanced ❑ Other. Describe: Pure Oxvaen Aeration Sodium Hvoochlorite Disinfection. Incineration b. Indicate the following removal rates (as applicable): Design BOD5 removal or Design CBOD5 removal 85% % Design SS removal 85% % Design P removal % Design N removal % Other % C. What type of disinfection is used for the effluent from this oulfall? If disinfection varies by season, please describe: Sodium Hvoochlorite If disinfection is by chlorination is dechlodnation used for this oulfall? ® Yes ❑ No Does the treatment plant have post aeration? ❑ Yes ® No A.12. Effluent Testing Information. All Applicants that discharge to waters of the US must provide effluent testing data for the following parameters. Provide the indicated effluent testing required by the permitting authority for each outfall through which effluent is discharged. Do not Include information on combined sewer overflows In this section. All information reported must be based on data collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QAIQC requirements of 40 CFR Part 136 and other appropriate QAIQC requirements for standard methods for analytes not addressed by 40 CFR Part 136. At a minimum, effluent testing data must be based on at least three samples and must be no more than four and one-half years apart. Outfall number: 001 MAXIMUM DAILY VALUE AVERAGE DAILY VALUE PARAMETER Value Units Value Units Number of Samples pH (Minimum) 6.00 SM. PH (Maximum) 7.00 S.U. Flow Rate 53.2 MGD 16.8 MGD 1580 Temperature (Winter) 24 °C 18 °C 410 Temperature (Summer) 27 °C 23 °C 596 ' For pH please report a minimum and a maximum daily value MAXIMUM DAILY AVERAGE DAILY DISCHARGE POLLUTANT DISCHARGE ANALYTICAL MLIMDL Conc. Units Conc. Units Number METHOD Saamplesmplesf CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS Boos 26 mg/L 7.9 mg/L 223 SM 5210B- 2.0 mg/L BIOCHEMICAL OXYGEN 2011 DEMAND (Report one) SM 5210B- CBoos 14 mg/L 4.3 mg/L 1066 2011 2.0 mg/L #/100 SM9222D- FECAL COLIFORM > 6000 #/100 mL 49 968 19971 IDEXX 1 #/100 mL mL Colilert-18 TOTAL SUSPENDED SOLIDS (TSS) 213 mg/L 11.5 mg/L 1073 SM 2540D- 2.5 mg/L 2011 EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550.6 & 7550-22. Page 6 of 22 END OF PART A. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE EPA Forte 3510-2A (Rev. 1-99). Replaces EPA fortes 7550-6 & 7550-22. Page 7 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Rocky River Regional Wastewater Treatment Renewal Yadkin Pee Dee Plant , NCO036269 BASIC APPLICATION INFORMATION PART B. ADDITIONAL APPLICATION INFORMATION FOR APPLICANTS WITH A DESIGN FLOW GREATER THAN OR EQUAL TO 0.1 MGD (100,000 gallons per day). All applicants with a design flow rate 2 0.1 mgd must answer questions B.1 through B.6. All others go to Part C (Certification). 8.1. Inflow and Infiltration. Estimate the average number of gallons per day that flow into the treatment works from inflow and/or Infiltration. 2,200,000 god Briefly explain any steps underway or planned to minimize inflow and infiltration. An I&I policy has been in effect since 2004. Flow monitoring studies are on -going with the member jurisdictions to determine sources of I&I. Improvements include. replacing deteriorated lines. lining Ope and televising ten percent of the sewer system annually. B.2. Topographic Map. Attach to this application a topographic map of the area extending at least one mile beyond facility property boundaries. This map must show the outline of the facility and the following information. (You may submit more than one map if one map does not show the entire area.) a. The area surrounding the treatment plant, including all unit processes. b. The major pipes or other structures through which wastewater enters the treatment works and the pipes or other structures through which treated wastewater Is discharged from the treatment plant. Include outfalls from bypass piping, if applicable. c. Each well where wastewater from the treatment plant is injected underground. d. Wells, springs, other surface water bodies, and drinking water wells that are: 1) within %mile of the property boundaries of the treatment works, and 2) listed in public record or otherwise known to the applicant. e. Any areas where the sewage sludge produced by the treatment works is stored, treated, or disposed. f. If the treatment works receives waste that is classified as hazardous under the Resource Conservation and Recovery Act (RCRA) by truck, rail, or special pipe, show on the map where the hazardous waste enters the treatment works and where it is treated, stored, and/or disposed. B.3. Process Flow Diagram or Schematic. Provide a diagram showing the processes of the treatment plant, including all bypass piping and all backup power sources or redunancy in the system. Also provide a water balance showing all treatment units, including disinfection (e.g., chlorination and dechlorination). The water balance must show daily average flow rates at influent and discharge points and approximate daily flow rates between treatment units. Include a brief narrative description of the diagram. B.4. Operation/Maintenance Performed by Contractor(s). Are any operational or maintenance aspects (related to wastewater treatment and effluent quality) of the treatment works the responsibility of a contractor? ❑ Yes ® No If yes, list the name, address, telephone number, and status of each contractor and describe the contractor's responsibilities (attach additional - pages if necessary). Name: N/A Mailing Address: Telephone Number: ( 1 Responsibilities of Contractor: B.5. Scheduled Improvements and Schedules of Implementation. Provide Information on any uncompleted implementation schedule or uncompleted plans for improvements that will affect the wastewater treatment, effluent quality, or design capacity of the treatment works. If the treatment works has several different implementation schedules or is planning several improvements, submit separate responses to question B.5 for each. (If none, go to question B.6.) a. List the outfall number (assigned in question A.9) for each ouffall that is covered by this implementation schedule. 001 b. Indicate whether the planned improvements or implementation schedule are required by local, State, or Federal agencies. ❑ Yes ® No EPA Form 3510-2A (Rev. 1-99). Replaces EPA fors 7550-6 & 7550-22. Page 8 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Rocky River Regional Wastewater Treatment Renewal Yadkin Pee Dee Plant , NCO036269 C. If the answer to B.5.b is "Yes," briefly describe, including new maximum daily inflow rate (if applicable). New aeration basin, clarifier and thickener Increasing Plant capacity to 34 MGD. This expansion is not expected to occur during this permit cycle. d. Provide dates imposed by any compliance schedule or any actual dates of completion for the implementation steps listed below, as applicable. For improvements planned independently of local, State, or Federal agencies, indicate planned or actual completion dates, as applicable. Indicate dates as accurately as possible. Schedule Actual Completion Implementation Stage MM/DD/YYYY MM/DD/YYYY - Begin Construction I / / / - End Construction l I l I - Begin Discharge / / / / - Attain Operational Level e. Have appropriate permits/clearances concerning other Federal/State requirements been obtained? ❑ Yes ❑ No Describe briefly: NA B.6. EFFLUENT TESTING DATA (GREATER THAN 0.1 MGD ONLY). Applicants that discharge to waters of the US must provide effluent testing data for the following parameters. Provide the indicated effluent testing required by the permitting authority for each outfall through which effluent is discharged. Do not Include Information on combine sewer overflows In this section. All information reported must be based on data collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. At a minimum effluent testing data must be based on at least three pollutant scans and must be no more than four and on -half years old. Outfall Number: 001 MAXIMUM DAILY AVERAGE DAILY DISCHARGE DISCHARGE ANALYTICAL POLLUTANT METHOD ML/MDL Conc. Units Conc. Units Number of Samples CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS AMMONIA (as N) 17.3 mg/L 1.7 mg1L 1077 SM 4500 NH3 D- 2011 0.1 mg/L CHLORINE (TOTAL 48 pg/L 15 pg/L 1072 SM 4600 Cl G- 25 pglL RESIDUAL, TRC) 2011 DISSOLVED OXYGEN 11.1 mglL 8.4 mg/L 1072 SM 4500 O G- 2011 1.0 mg/L TOTAL KJELDAHL 14.2 mg/L 4.18 mglL 51 EPA 351.2, Rev 0.2 mglL NITROGEN (rKN) 2.19 93 NITRATE PLUS NITRITE 22.36 mg/L 17.04 mglL 51 EPA 353.2, Rev 0.04 mg/L NITROGEN 2, 1993 OIL and GREASE <6.0 mg/L <5.0 mg/L 3 EPA 1664, Rev B 5.0 mg/L SM 4500 P E- 0.03 mg/U 0.06 PHOSPHORUS (Total) 3.80 mg/L 2.62 mg/L 53 19991HACH 8190 mg/L TNT TOTAL DISSOLVED SOLIDS 410 mg/L 366 m91L 3 SM 2640 C-1997 1.0 mg/L (TDS) OTHER END OF PART B. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 8 7550-22. Page 9 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Rocky River Regional Wastewater Treatment Renewal Yadkin Pee Dee Plant , NCO036269 BASIC APPLICATION INFORMATION PART C. CERTIFICATION All applicants must complete the Certification Section. Refer to instructions to determine who is an officer for the purposes of this certification. All applicants must complete all applicable sections of Form 2A, as explained in the Application Overview. Indicate below which parts of Form 2A you have completed and are submitting. By signing this certification statement applicants confirm that they have reviewed Form 2A and have completed all sections that apply to the facility for which this application is submitted. Indicate which parts of Form 2A you have completed and are submitting: ® Basic Application Information packet Supplemental Application Information packet: ® Part D (Expanded Effluent Testing Data) ® Part E (Toxicity Testing: Biomonitoring Data) ® Part F (Industrial User Discharges and RCRAICERCLA Wastes) ❑ Part G (Combined Sewer Systems) ALL APPLICANTS MUST COMPLETE THE FOLLOWING CERTIFICATION. I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. Name and official title Mark Fowler, - " s Director �, p Signature Telephone number 704 788-4164 ext. 111 Date signed '� l:8 Upon request of the permitting authority, you must submit any other information necessary to assure wastewater treatment practices at the treatment works or Identify appropriate permitting requirements. SEND COMPLETED FORMS TO: NCDENRI DWQ Attn: NPDES Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-0 & 7550-22, Page 10 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Rocky River Regional Wastewater Treatment Renewal Yadkin Pee Dee Plant, NCO036269 SUPPLEMENTAL APPLICATION INFORMATION PART D. EXPANDED EFFLUENT TESTING DATA Refer to the directions on the cover page to determine whether this section applies to the treatment works. Effluent Testing: 1.0 mgd and Pretreatment Works. If the treatment works has a design flow greater than or equal to 1.0 mgd or it has (or is required to have) a pretreatment program, or is otherwise required by the permitting authority to provide the data, then provide effluent testing data for the following pollutants. Provide the indicated effluent testing information and any other information required by the permitting authodty for each outfall through which effluent is discharged. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected through analyses conducted using 40 CFR Part 136 methods. In addition, these data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. Indicate in the blank rows provided below any data you may have on pollutants not specifically listed in this form. At a minimum, effluent testing data must be based on at least three pollutant scans and must be no more than four and one-half years old. Outfall number. 001 (Complete once for each outfall discharging effluent to waters of the United States.) MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE POLLUTANT ANALYTICAL ML/MDL Number Conc. Units Mass Units Conc. Units Mass Units of METHOD Samples METALS (TOTAL RECOVERABLE), CYANIDE, PHENOLS, AND HARDNESS. ANTIMONY <3.0 pg/L <0.66 Ibs <3.0 pg/L <0.54 Ibs 3 EPA 200.8, Rev 5.4, 1994 3.0 pg/L ARSENIC < 10 pg/L < 1.24 Ibs 2.8 pg/L 0.41 Ibs 17 EPA 200.8, 2.5 pg/L Rev 5.4, 1994 BERYLLIUM < 5.0 pg/L < 0.58 Ibs 2.1 pg/L 0.29 Ibs 18 EPA 200.8, Rev 5.4, 1994 2.5 pg/L CADMIUM < 2.5 pg/L < 0.55 Ibs 1.8 pg/L 0.25 Ibs 18 EPA 200.8, Rev 5.4, 19 2.5 pg/L CHROMIUM < 5.0 pg/L < 0.62 Ibs 2.5 pg/L 0.35 Ibs 17 EPA 200.8, 2 5 pg/L Rev 5.4, 1994 COPPER 21 pg/L 2.61 Ibs 7.6 pg/L 1.04 Ibs 18 EPA 200.8, Rev 5.4, 1994 2.5 pg/L LEAD < 5.0 pg/L < 0.62 Ibs 2.5 pg/L 0.34 Ibs 18 EPA 200.8, 2.5 pg/L Rev 6.4, 1994 MERCURY 30.0 ng/L 0.006 Ibs 7.0 ng/L 0.001 Ibs 19 EPA 1631 E 1 ng/L NICKEL < 10 pg/L < 1.24 Ibs 4.0 pg/L 0.56 Ibs 17 EPA 200.8, 2.5 pg/L Rev 5.4. 1994 SELENIUM < 10 pg/L < 1.24 Ibs 4.4 pg/L 0.61 Ibs 18 EPA 200.8, Rev 5.4, 1994 5.0 pg/L SILVER < 2.5 pg/L < 2.36 Ibs 2.5 pg/L 0.78 Ibs 5 EPA 200.8, Rev 5.4, 1994 2.5 pg/L THALLIUM <1.0 pg/L <0.22 Ibs <1.0 pg/L <0.18 Ibs 3 EPA 20 0.8, Rev 5.4, 0 8 10pg[L ZINC 72 pg/L 12.22 Ibs 53.5 pg/L 7.32 Ibs 18 EPA 200.8, Rev 5.4, 1994 5.0 pg/L CYANIDE c 0.005 mg/L < 1.09 Ibs < 0.005 m /L 9 < 0.90 Ibs 3 SM 4500 CN- E-1999 0.005 mg/L TOTALPHENOLIC <5 pg/L <1.09 Ibs <5 pg/L <0.90 Ibs 3 EPA420.1, Spl�L COMPOUNDS 1978 HARDNESS (as CaCO3) 134 mg/L 24.7 Ibs 110 mg/L 15.3 Ibs 28 SM 2340 G 1997 5.0 mg/L Use this space (or a separate sheet) to provide information on other metals requested by the permit writer EPA Form 3510-2A (Rev. 1-99). Replaces EPA fortes 7550-6 8 7550-22. Page 11 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Rocky River Regional Wastewater Treatment Renewal Yadkin Pee Dee Plant, NCO036269 Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.) MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE POLLUTANT ANALYTICAL ML/MDL Number Conc. Units Mass Units Conc. Units Mass Units of METHOD Samples VOLATILE ORGANIC COMPOUNDS ACROLEIN < 100 pg/L <21.86 Its; < 100 pg/L <18.08 Its 3 EPA 624 100 pg/L ACRYLONITRILE <50 pg/L <10.93 Ibs <50 pg/L <9.04 Ibs 3 EPA 624 50 pg/L BENZENE <5 pg/L <1.09 Ibs <5 pg/L <0.90 Ibs 3 EPA 624 5.0 pg/L BROMOFORM <5 pg/L < 1.09 Ibs <5 pg/L < 0.90 Ibs 3 EPA 624 5.0 pg/L CARBON <5 pg/L <1.09 Ibs <5 pg/L <0.90 Its 3 EPA 624 5.0 pg/L TETRACHLORIDE CHLOROBENZENE <5 pg/L < 1.09 Ibs <5 pg/L < 0.90 Ibs 3 EPA 624 5.0 pg/L CHLORODIBROMO- <5 pg/L < 1.09 Its <5 pg/L < 0.90 Ibs 3 EPA 624 5.0 pg/L METHANE CHLOROETHANE 410 pg/L < 2.19 Ibs < 10 pg/L < 1.81 Ibs 3 EPA 624 10 pg/L 2-CHLOROETHYLVINYL <5 pg/L <1.09 Ibs <5 pg/L <0.90 Ibs 3 EPA 624 5.0 pg/L ETHER CHLOROFORM <5 pg/L < 1.09 Ibs <5 pg/L < 0.90 Ibs 3 EPA 624 5.0 pg/L DICHLOROBROMO- <5 pg/L < 1.09 Ibs <5 pg/L < 0.90 Ibs 3 EPA 624 5.0 pg/L METHANE 1,1-DICHLOROETHANE <5 pg/L <1.09 Ibs <5 pg/L <0.90 Ibs 3 EPA 624 5.0 pg/L 1,2-DICHLOROETHANE <5 pg/L <1.09 Ibs <5 pg/L <0.90 Ibs 3 EPA 624 5.0 pg/L TRANS-I,2-DICHLORO- <5 pg/L <1.09 Ibs <5 pg/L <0.90 Ibs 3 EPA 624 6.0 pg/L ETHYLENE 1,1-DICHLORO- <5 pg/L <1.09 Ibs <5 pg/L <0.90 Ibs 3 EPA 624 5.0 pg/L ETHYLENE 1,2-DICHLOROPROPANE <5 pg/L <1.09 Ibs <5 pg/L <0.90 Ibs 3 EPA 624 5.0 pg/L 1,3-DICHLORO- c 5 pg/L < 1.09 Ibs < 5 pg/L < 0.90 Ibs 3 EPA 624 5.0 pgIL PROPYLENE ETHYLBENZENE < 5 pg/L < 1.09 Its <5 pg/L < 0.90 Ibs 3 EPA 624 5.0 pg/L METHYL BROMIDE < 10 pg/L < 2.19 Ibs < 10 pg/L < 1.81 Its 3 EPA 624 10 pg/L METHYL CHLORIDE < 10 pg/L < 2.19 Ibs < 10 pg/L < 1.81 Its 3 EPA 624 10 pg/L METHYLENE CHLORIDE < 10 pg/L < 2.19 Ibs < 10 pg/L < 1.81 Its 3 EPA 624 10 pg/L 1,1,2,2-TETRA- <5 pg/L < 1.09 Ibs <5 pg/L < 0.90 Ibs 3 EPA 624 5.0 pg/L CHLOROETHANE TETRACHLORO- <5 pg/L <1.09 Ibs <5 pgIL. <0.90 Ibs 3 EPA624 5.0 pg/L ETHYLENE TOLUENE c 5 pg/L < 1.09 Ibs c 5 pg/L < 0.90 Its 3 EPA 624 5.0 pg/L EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 13 of 22 FACILITY NAME AND PERMIT NUMBER: Rocky River Regional Wastewater Treatment Plant NC0036269 , PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Yadkin Pee Dee Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United Stales.) .POLLUTANT MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE ANALYTICAL METHOD ML/MDL Conc. Units Mass Unit s Conc. Units Mass Unit s Number of Samples 1,1,1 TRICHLOROETHANE <5 pg/L <1.09 Ibs <5 pg/L <0.90 Ibs 3 EPA 624 5.0 pg/L 1,1,2- OROETHANE TRIO <5 pg/L < 1.09 Ibs < 5 pg/L < 0.90 Ibs 3 EPA 624 5.0 pg/L TRICHLOROETHYLENE < 5 p9/L < 1.09 Ibs < 5 pg/L < 0.90 Ibs 3 EPA 624 5.0 pg/L VINYL CHLORIDE < 10 pg/L < 2.19 Ibs < 10 pg/L < 1.81 Ibs 3 EPA 624 10 pg/L Use this space (or a separate sheet) to provide information on other volatile organic compounds requested by the permit writer ACID -EXTRACTABLE COMPOUNDS P-CHLORO-M-CRESOL <20 pg/L <4.37 Ibs <20 pg/L <3.62 Ibs 3 EPA 625 20 pg/L 2-CHLOROPHENOL < 10 pg/L <2.19 Ibs < 10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L 2,4-DICHLOROPHENOL <10 pg/L <2.19 Ibs <10 pg/L <1.81 Ibs 3 EPA625 10 pg/L 2,4-DIMETHYLPHENOL < 10 pg/L < 2.19 Ibs < 10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L 4,6-DINITRO-0-CRESOL < 50 pg/L <10.93 Ibs < 50 pg/L <9.04 Ibs 3 EPA 625 50 pg/L 2,4-DINITROPHENOL < 50 pg/L <10.93 Ibs < 50 pg/L <9.04 Ibs 3 EPA 625 50 pg/L 2-NITROPHENOL < 10 pg/L < 2.19 Ibs < 10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L 4-NITROPHENOL <50 pg/L <10.93 Ibs <50 pg/L <9.04 Ibs 3 EPA 625 50 pg/L PENTACHLOROPHENOL <50 pg/L <10.93 Ibs <50 pg/L <9.04 Ibs 3 EPA 625 50 pg/L PHENOL < 10 pg/L < 2.19 Ibs < 10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L 2'4'6- TRICHLOROPHENOL < 10 pg/L < 2.19 Ibs < 10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L Use this space (or a separate sheet) to provide information on other acid -extractable compounds requested by the permit writer BASE -NEUTRAL COMPOUNDS ACENAPHTHENE < 10 pg1L < 2.19 Ibs < 10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L ACENAPHTHYLENE < 10 p9/L < 2.19 Ibs < 10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L ANTHRACENE < 10 pg/L < 2.19 Ibs < 10 p9/L < 1.81 Ibs 3 EPA 625 10 pg/L BENZIDINE <100 pg/L <21.86 Ibs <100 pg/L <18.08 Ibs 3 EPA 625 100 pg/L BENZO(A)ANTHRACENE < 10 pg/L < 2.19 Ibs < 10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L BENZO(A)PYRENE < 10 pg/L < 2.19 Ibs < 10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 E 7550-22. Page 14 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Rocky River Regional Wastewater Treatment Renewal Yadkin Pee Dee Plant, NCO036269 Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.) MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE POLLUTANT ANALYTICAL MLIMDL Number Cone. Units Mass Units Cone. Units Mass Units of METHOD Samples FLUORANTRANIT HENE <10 pg/L <2.19 Ibs <10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L SENZO(GHI)PERYLENE < 10 pg/L 42.19 Ibs < 10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L BENZO( FLUORANTHENE <10 pg/L < 2.19 Ibs <10 pg/L 41.81 Ibs 3 EPA 625 10 pg/L BIS (2-CHLOROETHOXY) < 10 pg/L < 2.19 Ibs <10 pg/L < 1.81 Ibs 3 EPA 625 10 pglL METHANE BIS (2-CHLOROETHYL)- <10 pg/L 42.19 Ibs <10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L ETHER BIS (2-CHL - <10 pg/L <2.19 Ibs <10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L PROPYL)ETHER ETHER BIS(2-ETHYLHEXYL) <20 pg/L <4.37 Its <20 pg/L <3.62 Ibs 3 EPA 625 20 pg/L PHTHALATE HE <10 pg/L < 2A9 Ibs <10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L PHENYLETHERR PHENYLETHER BUTYL < 10 pg/L < 2.19 Ibs <10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L PHTHALATE LATE H <10 pg/L < 2,19 Ibs <10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L NAPHTHALTHALENE NA 4-CHLORPHENYL <10 pg/L < 2.19 Ibs <10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L PHENYLETHER CHRYSENE < 10 pg/L < 2.19 Ibs <10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L DI-N-BUTYL PHTHALATE < 10 pg/L < 2.19 Ibs <10 pg/L I < 1.81 Ibs 3 EPA 625 10 pg/L DI-N-OCTYL PHTHALATE < 10 pg/L < 2.19 Ibs <10 pg/L < 1.81 Ibs 3 EPA 625 10 pi DIBENZO(A,H) <10 pg/L < 2.19 Ibs <10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L ANTHRACENE 1,20CHLOROBENZENE <5 pg/L < 1.09 Ibs <5 pg/L < 0.90 Ibs 3 EPA 624 5 pg/L 1,3-DICHLOROBENZENE <5 pg/L <1.09 Ibs <5 pg/L <0.90 Ibs 3 EPA 624 5pg/L 1,4-DICHLOROBENZENE <5 pg/L < 1.09 Ibs <5 pg/L < 0.90 Ibs 3 EPA 624 5 pg/L 3,3-DICHLORO- <10 pg/L < 2.19 Ibs <10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L BENZIDINE DIETHYL PHTHALATE <10 pg/L < 2.19 Ibs <10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L DIMETHYL PHTHALATE <10 pg/L < 2.19 Ibs <10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L 2,4-DINITROTOLUENE <10 pg/L <2.19 Ibs <10 pg/L <1.81 Ibs 3 EPA 625 10 pg/L 2,6-DINITROTOLUENE <10 pg/L < 2.19 Ibs <10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L 1,2-DIPHENYL- <10 pg/L <2.19 Ibs < 10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L HYDRAZINE EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 15 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Rocky River Regional Wastewater Treatment Renewal Yadkin Pee Dee Plant, NCO036269 Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.) MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE POLLUTANT ANALYTICAL MLIMDL Number Conc. Units Mass Units Conc. Units Mass Units of METHOD Samples FLUORANTHENE < 10 pg/L < 2.19 Ibs < 10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L FLUORENE < 10 pg/L < 2.19 Ibs < 10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L HEXACHLOROBENZENE < 10 pg/L < 2A9 Ibs < 10 pg/L < 1.81 Ibs 3 EPA 625 10 Ill HEXACHLORO- < 10 p9/L <2.19 Ibs < 10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L BUTADIENE HEXACHLOROCYCLO- < 10 pg/L < 2.19 Ibs < 10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L PENTADIENE HEXACHLOROEfHANE < 10 pg/L <2A9 Ibs < 10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L INDENO(1,2,3-CD) < 10 pg/L <2.19 Ibs < 10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L PYRENE ISOPHORONE < 10 pg/L < 2.19 Ibs < 10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L NAPHTHALENE < 10 pg/L < 2.19 Ibs < 10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L NITROBENZENE < 10 pg/L < 2.19 Ibs < 10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L N-NITROSODI-N- < 10 pg/L < 2.19 Ibs < 10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L PROPYLAMINE , OSODI- < 10 pg/L < 2.19 Ibs < 10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L METHYLAMINE METHY N-NITROSODI- < 10 pg/L < 2.19 Ibs < 10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L PHENYLAMINE PHENANTHRENE < 10 pg/L < 2.19 Ibs < 10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L PYRENE < 10 pg/L < 2.19 Ibs < 10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L 1,2.4 < 10 pg/L < 2.19 Ibs < 10 pg/L < 1.81 Ibs 3 EPA 625 10 pg/L TRICHLOROBENZENE Use this space (or a separate sheet) to provide information on other base -neutral compounds requested by the permit writer Use this space (or a separate sheet) to provide information on other pollutants (e.g.. pesticides) requested by the permit writer END OF PART D. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 8 7550-22. Page 16 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Rocky River Regional Wastewater Treatment Plant, NCO036269 Renewal Yadkin Pee Dee SUPPLEMENTAL APPLICATION INFORMATION PART E. TOXICITY TESTING DATA POTWs meeting one or more of the following criteria must provide the results of whole effluent toxicity tests for acute or chronic toxicity for each of the facility's discharge points: 1) POTWs with a design flow rate greater than or equal to 1.0 mgd; 2) POTWs with a pretreatment program (or those that are required to have one under 40 CFR Part 403); or 3) POTWs required by the permitting authority to submit data for these parameters. • At a minimum, these results must include quarterly testing for a 12-month period within the past 1 year using multiple species (minimum of two species), or the results from four tests performed at least annually in the four and one-half years prior to the application, provided the results show no appreciable toxicity, and testing for acute and/or chronic toxicity, depending on the range of receiving water dilution. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. • In addition, submit the results of any other whole effluent toxicity tests from the past four and one-half years. If a whole effluent toxicity test conducted during the past four and one-half years revealed toxicity, provide any information on the cause of the toxicity or any results of a toxicity reduction evaluation, if one was conducted. • If you have already submitted any of the Information requested in Part E, you need not submit it again. Rather, provide the information requested in question EA for previously submitted information. If EPA methods were not used, report the reasons for using alternate methods. If test summaries are available that contain all of the information requested below, they may be submitted in place of Part E. If no biomonitoring data is required, do not complete Part E. Refer to the Application Overview for directions on which other sections of the forth to complete. E.I. Required Tests. Indicate the number of whole effluent toxicity tests conducted in the past four and one-half years. 1a chronic ❑ acute E.2. Individual Test Data. Complete the following chart for each whole effluent toxicity test conducted in the last four and one-half years. Allow one column per test (where each species constitutes a test). Copy this page if more than three tests are being reported. Test number: Ref- E4 Test number: Ref- E4 Test number: Ref- E4 a. Test information. Test Species & test method number Age at initiation of test Outfall number Dates sample collected Dale test started Duration b. Give toxicity test methods followed. Manual title Edition number and year of publication Page number(s) c. Give the sample collection method(s) used. For multiple grab samples, indicate the number of grab samples used. 24-Hour composite Grab d. Indicate where the sample was taken in relation to disinfection. (Check all that apply for each. Before disinfection After disinfection After dechlorination EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550.6 & 7550-22. Page 17 of 22 FACILITY NAME AND PERMIT NUMBER: Rocky River Regional Wastewater Treatment Plant, NC0036269 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Yadkin Pee Dee Test number: Ref- E4 Test number: Ref- E4 Test number: Ref- E4 e. Describe the point In the treatment process at which the sample was collected. Sample was collected: f. For each test, include whether the test was intended to assess chronic toxicity, acute toxicity, or both Chronic toxicity Acute toxicity g. Provide the type of test performed. Static Static -renewal Flow -through h. Source of dilution water. If laboratory water, specify type; if receiving water, specify source. Laboratory water Receiving water I. Type of dilution water. If salt water, specify "natural" or type of artificial sea salts or brine used. Fresh water Salt water j. Give the percentage effluent used for all concentrations in the test series. k. Parameters measured during the test. (State whether parameter meets test method specifications) PH Salinity Temperature Ammonia Dissolved oxygen I. Test Results. Acute: Percent survival in 100% effluent LCso 95% C.I. % % % Control percent survival % % % Other (describe) EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 18 of 22 FACILITY NAME AND PERMIT NUMBER: Rocky River Regional Wastewater Treatment Plant, NCO036269 [PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Yadkin Pee Dee Chronic: NOEC % % % IC25 % % % Control percent survival % % % Other (describe) m. Quality Control/Quality Assurance. Is reference toxicant data available? Was reference toxicant test within acceptable bounds? What date was reference toxicant test run (MM/DD/YYYY)? Other (describe) E.3. Toxicity Reduction Evaluation. Is the treatment works Involved in a Toxicity Reduction Evaluation? ❑ Yes IRINo If yes, describe: E.4. Summary of Submitted Biomonitoring Test Information. If you have submitted biomonitoring test Information, or information regarding the cause of toxicity, within the past four and one-half years, provide the dates the information was submitted to the permitting authority and a summary of the results. Date submitted: See Attachment (MM/DD/YYYY) Summary of results: (see instructions) END OF PART E. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE. EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 19 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Rocky River Regional Wastewater Treatment Plant, NCO036269 Renewal Yadkin Pee Dee SUPPLEMENTAL APPLICATION INFORMATION PART F.INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES All treatment works receiving discharges from significant Industrial users or which receive RCRA,CERCLA, or other remedial wastes must complete part F. GENERAL INFORMATION: F.I. Pretreatment program. Does the treatment works have, or is subject ot, an approved pretreatment program? ® Yes ❑ No F.2. Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (CIUs). Provide the number of each of the following types of industrial users that discharge to the treatment works. a. Number of non -categorical SIUs. 11 It. Number of CIUs. 3 SIGNIFICANT INDUSTRIAL USER INFORMATION: Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and provide the Information requested for each SIU. EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22, Page 20 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Rocky River Regional Wastewater Treatment Plant, NCO036269 Renewal Yadkin Pee Dee SIGNIFICANT INDUSTRIAL USER INFORMATION: 1 Of 14 F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: Americhem, Inc. Mailing Address: 723 Commerce Drive Concord, NC 28025 F.4. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. Disperse dyes into Plastic resins: discharge clean up water F.S. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s): master batch ( a blend of pigment and additives for plastic coloration) Raw materal(s): pigments surfactants thermoplastic resin F.6. Flow Rate. a. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. 18,000 gpd ( continuous or x intermittent) b. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. gpd ( continuous or intermittent) F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: a. Local limits N Yes ❑ No b. Categorical pretreatment standards ❑ Yes N No If subject to categorical pretreatment standards, which category and subcategory? F.8. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years? ❑ Yes N No If yes, describe each episode. EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 21 or 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Rocky River Regional Wastewater Treatment Plant, NCO036269 Renewal Yadkin Pee Dee SIGNIFICANT INDUSTRIAL USER INFORMATION: 2 of 14 F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: BFI Waste Systems of North America Mailing Address: 5105 Morehead Road Concord, NC 28027 F.4. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. Pretreated leachate. F.S. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s):lined landfill: treat contaminated leachate Raw material(s): NA F.6. Flow Rate. a. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. 34,000 gpd ( continuous or X intermittent) b. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged into the collection system In gallons per day (gpd) and whether the discharge is continuous or intermittent. gpd ( continuous or intermittent) F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: a. Local limits ® Yes ❑ No b. Categorical pretreatment standards ❑ Yes ® No If subject to categorical pretreatment standards, which category and subcategory? F.B. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years? ❑ Yes ID No If yes, describe each episode. EPA Forth 3510-2A (Rev. 1-99). Replaces EPA forms 7560-6 8 7550-22. Page 22 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Rocky River Regional Wastewater Treatment Plant, NCO036269 Renewal Yadkin Pee Dee SIGNIFICANT INDUSTRIAL USER INFORMATION: 3 of 14 F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: Charlotte-Mecklenbum Utility Department Mailing Address: 4222 Westmont Drive. Charlotte, NC 28217 F.4. Industrial Processes. Describe all the industrial processes that aged or contribute to the SIU's discharge. Domestic commercial non-si nificent industrial users and two significant industrial users. F.S. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal producl(s):NA Raw material(s): NA F.6. Flow Rate. c. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. 19,500 gpd ( continuous or X intermittent) d. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. 3,719,000 gpd (X continuous or intermittent) F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: a. Local limits ® Yes ❑ No b. Categorical pretreatment standards ❑ Yes ® No If subject to categorical pretreatment standards, which category and subcategory? F.8. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years? ❑ Yes ® No If yes, Describe each episode. EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 23 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Rocky River Regional Wastewater Treatment Plant, NCO036269 Renewal Yadkin Pee Dee SIGNIFICANT INDUSTRIAL USER INFORMATION: 4 of 14 FA Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: Heig Chem -Tex, Inc. Mailing Address: 2725 Armentrout Drive Concord, NC 28027 FA Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. Chemical mixer: discharge some rinse water and cleaning of mixing vats F.5. Principal Productis) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s): textile auxiliaries Raw malerial(s): surfactants alkalies fatty acids oils waxes and inorganic salts F.6. Flow Rate. a. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. 2,000 gpd ( continuous or X intermittent) b. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. gpd ( continuous or intermittent) F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: a. Local limits ® Yes ❑ No b. Categorical pretreatment standards ❑ Yes ® No If subject to categorical pretreatment standards, which category and subcategory? F.8. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years? ❑ Yes ® No If yes, describe each episode. EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 a 7550-22. Page 24 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Rocky River Regional Wastewater Treatment Plant, NCO036269 Renewal Yadkin Pee Dee SIGNIFICANT INDUSTRIAL USER INFORMATION: 5 of 14 F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: City of Concord— Hillorove Water Treatment Plant Mailing Address: P.O. Box 308 Concord NC 28026-0308 F.4. Industrial Processes. Describe all the Industrial processes that affect or contribute to the SIU's discharge. Municipal water treatment Plant F.6. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s): public drinking water Raw material(s): aluminum sulfatepotassium nermarmanate. sodium hypochlorite, sodium hydroxide, of mer, polvohosphate and h drofluosilicic acid. F.6. Flow Rate. c. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. 126,000 gpd ( wntinuous or X intermittent) d.Non-process wastewater flow rate. Indicate the average daily volume of non -process wastewater now discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. gpd ( continuous or intermittent) F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: a. Local limits ® Yes ❑ No b. Categorical pretreatment standards ❑ Yes ® No If subject to categorical pretreatment standards, which category and subcategory? F.8. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years? ❑ Yes ® No If yes, describe each episode. EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 8 7550-22. Page 25 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Rocky River Regional Wastewater Treatment Plant, NCO036269 Renewal Yadkin Pee Dee SIGNIFICANT INDUSTRIAL USER INFORMATION: 6 Of 14 F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: Galvan Industries, Inc. Mailing Address: P.O. Box 369 Harrisburg, NC 28075 FA. Industrial Processes. Describe all the Industrial processes that affect or contribute to the SIU's discharge. Domestic sewage and boiler blowdown. F.S. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s):NA Raw material(s): NA F.6. Flow Rate. a. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. gpd ( continuous or intermittent) b. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. 1,300 gpd ( continuous or X intermittent) F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: a. Local limits ® Yes ❑ No b. Categorical pretreatment standards ❑ Yes ® No If subject to categorical pretreatment standards, which category and subcategory? Pa. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g.. upsets, interference) at the treatment works in the past three years? ❑ Yes ® No If yes, describe each episode. EPA Form 3510-2A (Rev. 1.99). Replaces EPA forms 7550-6 & 7550-22. Page 26 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Rocky River Regional Wastewater Treatment Plant, NCO036269 Renewal Yadkin Pee Dee SIGNIFICANT INDUSTRIAL USER INFORMATION: 7 of 14 F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: Carolinas Healthcare Northeast Mailing Address: 920 Church Street North Concord, NC 28025 F.4. Industrial Processes. Describe all the Industrial processes that affect or contribute to the SIU's discharge. General hospital wastewater. F.S. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s): NA Raw material(s): NA F.6. Flow Rate. a. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. 90,000 gpd (X continuous or intermittent) b. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. gpd ( continuous or intermittent) F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: a. Local limits ® Yes ❑ No b. Categorical pretreatment standards ❑ Yes ® No If subject to categorical pretreatment standards, which category and subcategory? F.6. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years? ❑ Yes ® No If yes, describe each episode. EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 8 7550-22. Page 27 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Rocky River Regional Wastewater Treatment Plant, NCO036269 Renewal Yadkin Pee Dee SIGNIFICANT INDUSTRIAL USER INFORMATION: 8 Of 14 F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: Perdue Fames Mailing Address: 862 Harris Street NW Concord NC 28025 FA. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. Wastewater generated from various clean up processes. F.S. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s): cooking and Packaging chicken products. Raw material(s): chicken parts and oils. F.6. Flow Rate. c. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. 167,000 gpd (X continuous or intermittent) d. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. gpd ( continuous or intermittent) F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: a. Local limits ® Yes ❑ No b. Categorical pretreatment standards ❑ Yes ® No If subject to categorical pretreatment standards, which category and subcategory? Re. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years? ❑ Yes ® No If yes, describe each episode. EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 28 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Rocky River Regional Wastewater Treatment Plant, NCO036269 Renewal Yadkin Pee Dee SIGNIFICANT INDUSTRIAL USER INFORMATION: 9 of 14 F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: El. Inc. Mailing Address: 2865 N. Cannon Blvd. Kannapolis, NC 28083 F.4. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. Manufacture prescription, over the counter pharmaceuticals, and cosmetic liquids. creams, and ointments, and animal health products. F.S. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s): Pharmaceuticals Raw material(s): Confidential. F.S. Flow Rate. a. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. 3,000 gpd ( continuous or X intermittent) b. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. gpd ( continuous or Intermittent) F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: a. Local limits ® Yes ❑ No b. Categorical pretreatment standards ® Yes ❑ No If subject to categorical pretreatment standards, which category and subcategory? 40 CFR 439 subcategory D F.8. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g., upsets, Interference) at the treatment works in the past three years? ❑ Yes ® No If yes, describe each episode. EPA Forth 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 8 7550-22. Page 29 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Rocky River Regional Wastewater Treatment Plant, NCO036269 Renewal Yadkin Pee Dee SIGNIFICANT INDUSTRIAL USER INFORMATION: 10 of 14 F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: Star America Inc. Mailing Address: P.O. Box 1501 Concord, NC 28026-1501 FA. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. Dveino and boarding hosiery. F.S. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s): ladies' hosiery and children's tights Raw material(s): nylon and dyes F.6. Flow Rate. c. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. 18,000 gpd ( continuous or X intermittent) d. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. gpd ( continuous or intermittent) F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: a. Local limits ® Yes ❑ No b. Categorical pretreatment standards ❑ Yes ® No If subject to categorical pretreatment standards, which category and subcategory? F.B. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years? ❑ Yes ® No If yes, describe each episode. EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7660-6 a 7550-22. Page 30 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Rocky River Regional Wastewater Treatment Plant, NCO036269 Renewal Yadkin Pee Dee SIGNIFICANT INDUSTRIAL USER INFORMATION: 11 of 14 F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: Heritage -Crystal Cleanl. LLC Mailing Address: 2115 SPeedrail Court Concord NC 28025 FA. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. Treat industrial wastewater, recycle used Petroleum Products: discharge water after oil recovered. F.S. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s): recovered oil is sold. Raw materal(s): coagulates and flocculates. F.6. Flow Rate. a. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. 41,000 gpd (X continuous or inlemmittent) b.Non-process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. gpd ( continuous or intermittent) F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: a. Local limits ® Yes ❑ No b. Categorical pretreatment standards ® Yes ❑ No If subject to categorical pretreatment standards, which category and subcategory? 40 CFR 437 subcategory B F.8. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years? ❑ Yes ® No If yes, describe each episode. EPA Forth 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 31 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Rocky River Regional Wastewater Treatment Plant, NCO036269 Renewal Yadkin Pee Dee SIGNIFICANT INDUSTRIAL USER INFORMATION: 12 of 14 F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: Slericvcle. Inc. Mailing Address: 4403 Republic Court Concord, NC 28027 F.4. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. Clean reuseable medical waste containers boiler blowdown and domestic sewage F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s):NA Raw material(s): cleaning materials F.6. Flow Rate. c. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. 20,000 gpd ( continuous or X intermittent) d. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. gpd ( continuous or intermittent) F.7. Pretreatment Standards. Indicate whether the SlU is subject to the following: a. Local limits ® Yes ❑ No b. Categorical pretreatment standards ❑ Yes ® No If subject to categorical pretreatment standards, which category and subcategory? F.8. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years? ❑ Yes ® No If yes, describe each episode. EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550.6 & 7550-22. Page 32 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Rocky River Regional Wastewater Treatment Plant, NCO036269 Renewal Yadkin Pee Dee SIGNIFICANT INDUSTRIAL USER INFORMATION: 13 of 14 F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: Organic Dyes and Pigments Mailing Address: 1015 Concord Pkwv, North Concord, NC 28027 FA. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. Blend pigments and auxiliary chemicals, as well as liguid dyes. F.S. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s): Pigments and liquid dyes. Raw material(s): Dyes and pigments F.6. Flow Rate. a. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. 1.000 gpd ( continuous or X intermittent) b. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. gpd ( continuous or intermittent) F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: a. Local limits ® Yes ❑ No b. Categorical pretreatment standards ❑ Yes ® No If subject to categorical pretreatment standards, which category and subcategory? F.8. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years? ❑ Yes ® No If yes, describe each episode. EPA Forth 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 33 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Rocky River Regional Wastewater Treatment Plant, NCO036269 Renewal Yadkin Pee Dee SIGNIFICANT INDUSTRIAL USER INFORMATION: 14 of 14 F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: Owens Coming Mailing Address: 4535 Enterprise Drive Concord, NC 28027 F.4. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. Reprocess metal from fiberglass Production and fabricate new fiberglass production parts. F.S. Principal Product(s) and Raw Materiai(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s):Confidential Raw material(s): Confidential F.6. Flow Rate. a. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. 1,000 gpd ( continuous or X intermittent) b. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. gpd ( continuous or intermittent) F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: a. Local limits ❑ Yes ® No b. Categorical pretreatment standards ® Yes ❑ No If subject to categorical pretreatment standards, which category and subcategory? 40 CFR 471 subcategoryD F.B. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years? ❑ Yes ® No If yes, describe each episode. EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 34 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVERBASIN: Rocky River Regional Wastewater Treatment Plant, NCO036269 Renewal Yadkin Pee Dee RCRA HAZARDOUS WASTE RECEIVED BY TRUCK, RAIL, OR DEDICATED PIPELINE: F.9. RCRA Waste. Does the treatment works receive or has it in the past three years received RCRA hazardous waste by truck, rail or dedicated pipe? ❑ Yes ❑ No (go to F.12) F.10. Waste transport Method by which RCRA waste is received (check all that apply): ❑ Truck ❑ Rail ❑ Dedicated Pipe F.11. Waste Description. Give EPA hazardous waste number and amount (volume or mass, specify units). EPA Hazardous Waste Number Amount Units CERCLA (SUPERFUND) WASTEWATER, RCRA REMEDIATION/CORRECTIVE ACTION WASTEWATER, AND OTHER REMEDIAL ACTIVITY WASTEWATER: F.12. Remediation Waste. Does the treatment works currently (or has It been notified that it will) receive waste from remedial activities? ❑ Yes (complete F.13 through F.15.) ® No F.13. Waste Origin. Describe the site and type of facility at which the CERCLA/RCRAlor other remedial waste originates (or is excepted to origniate in the next five years). F.14. Pollutants. List the hazardous constituents that are received (or are expected to be received). Include data on volume and concentration, if known. (Attach additional sheets if necessary.) F.15. Waste Treatment a. Is this waste treated (or will be treated) prior to entering the treatment works? ❑ Yes ❑ No If yes, describe the treatment (provide information about the removal efficiency): b. Is the discharge (or will the discharge be) continuous or intermittent? ❑ Continuous ❑ Intermittent - If intermittent, describe discharge schedule. END OF PART F. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE EPA Form 3510-2A (Rev. 1-99). Replaces EPA fortes 7550-6 & 7550-22. Page 35 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Rocky River Regional Wastewater Treatment Plant, NCO036269 Renewal Yadkin Pee Dee SUPPLEMENTAL APPLICATION INFORMATION PART G. COMBINED SEWER SYSTEMS If the treatment works has a combined sewer system, complete Part G. G.1. System Map. Provide a map indicating the following: (may be included with Basic Application Information) a. All CSO discharge points. b. Sensitive use areas potentially affected by CSOs (e.g., beaches, drinking water supplies, shellfish beds, sensitive aquatic ecosystems, and outstanding natural resource waters). C. Waters that support threatened and endangered species potentially affected by CSOs. G.2. System Diagram. Provide a diagram, either in the map provided in GA or on a separate drawing, of the combined sewer collection system that includes the following information. a. Location of major sewer trunk lines, both combined and separate sanitary. b. Locations of points where separate sanitary sewers feed into the combined sewer system. C. Locations of in -line and off-line storage structures. d. Locations of flow -regulating devices. e. Locations of pump stations. CSO OUTFALLS: Complete questions G.3 through G.6 once for each CSO discharge oolnt. G.3. Description of Ouffall. a. Ouffall number NIA b. Location (City or town, if applicable) (Zip Code) (County) (State) (Latitude) (Longitude) C. Distance from shore (if applicable) ft. d. Depth below surface (if applicable) ft. e. Which of the following were monitored during the last year for this CSO? ❑ Rainfall ❑ CSO pollutant concentrations ❑ CSO frequency ❑ CSO flow volume ❑ Receiving water quality f. How many storm events were monitored during the last year? GA. CSO Events. a. Give the number of CSO events in the last year. events (❑ actual or ❑ approx.) b. Give the average duration per CSO event. hours (❑ actual or ❑ approx.) EPA Form 3510-2A (Rev. 1.99). Replaces EPA forms 7550-6 & 7550-22. Page 36 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Rocky River Regional Wastewater Treatment Plant, NCO036269 Renewal Yadkin Pee Dee C. Give the average volume per CSO event. million gallons (❑ actual or ❑ approx.) d. Give the minimum rainfall that caused a CSO event in the last year Inches of rainfall G.S. Description of Receiving Waters. a. Name of receiving water: b. Name of watershed/river/stream system: United State Soil Conservation Service 14-digit watershed code (if known): C. Name of State Management/River Basin: United States Geological Survey 8-digit hydrologic cataloging unit code (if known): G.6. CSO Operations. Describe any known water quality impacts on the receiving water caused by this CSO (e.g., permanent or intermittent beach closings, permanent or intermittent shell fish bed closings, fish kills, fish advisories, other recreational loss, or violation of any applicable State water quality standard). END OF PART G. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE. EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 37 of 22 ROCKY RIVER REGIONAL WASTEWATER TREATMENT PLANT CHRONIC TOXICITY MONITORING DATA (Results for Ceriodaphnia dubia and P. promelas) OUTFALL # DATES METHOD RESULTS COLLECTION ANALYSIS SUBMITTAL 001 2/12/18, 2/14/18 2/14/18-2/21/18 3/1/18 EPA Method 1002.0 NOEC 100%@EFFLUENT 001 11/6/17,11/8/17 11/8/17-11/15/17 12/5/17 EPA Method 1002.0 NOEC 100%@EFFLUENT* 001 7/31/17, 8/2/17 8/2/17-8/9/17 8/31/17 EPA Method 1002.0 NOEC 100%@EFFLUENT* 001 5/1/17, 5/3/17 5/3/17- S/10/17 5/23/17 EPA Method 1002.0 NOEC 100%@EFFLUENT* 001 2/13/17, 2/15/17 2/1S/17-2/22/17 3/9/17 EPA Method 1002.0 NOEC 100%@EFFLUENT* 001 10/31/16,11/2/16 11/2/16-11/9/16 11/30/16 EPA Method 1002.0 NOEC 100%@EFFLUENT 001 8/1/16, 8/3/16 8/3/16- 8/10/16 8/29/16 EPA Method 1002.0 NOEC 100%@EFFLUENT 001 5/2/16, 5/4/16 S/4/16-5/11/16 S/26/16 EPA Method 1002.0 NOEC 100%@EFFLUENT 001 2/1/16, 2/3/16 2/3/16-2/10/16 2/26/16 EPA Method 1002.0 NOEC 100%@EFFLUENT 001 11/16/15,11/18/15 11/18/1S-11/25/1S 12/10/15 EPA Method 1002.0 NOEC 100%@EFFLUENT 001 8/3/15, 8/5/15 8/5/1S-8/12/IS 8/27/1S EPA Method 1002.0 NOEC 100%@EFFLUENT 001 5/11/15, S/13/15 5/13/iS-5/20/15 6/9/15 EPA Method 1002.0 NOEC 100%@EFFLUENT 001 2/9/1S, 2/11/15 2/11/15-2/18/15 3/5/15 EPA Method 1002.0 NOEC 100%@EFFLUENT 001 11/3/14,11/5/14 11/5/14-11/12/14 11/26/14 EPA Method 1002.0 NOEC 100%@EFFLUENT 001 8/4/14, 8/6/14 8/6/14-8/13/14 8/2S/14 EPA Method 1002.0 NOEC 100%@EFFLUENT 001 5/5/14, 5/7/14 5/7/14-5/14/14 6/2/14 EPA Method 1002.0 NOEC 100%@EFFLUENT 001 2/10/14, 2/12/14 2/12/14-2/19/14 3/6/14 EPA Method 1002.0 NOEC75%@EFFLUENT 001 11/4/13,11/6/13 11/6/13-11/13/13 112/4/13 EPA Method 1002.0 NOEC 100%@EFFLUENT *Multispecies bioassays were conducted during February, May, August, and November of 2017 and included A promelas in addition to C. dubia . The four bioassays with A promelas had NOECs equal to 100% and used method EPA600/4-91/002. X�lj) ". %'IV If "rh 'yk) 0 'w 41 n rm, NO R PLANT PROCESS SCHEMATIC ROCKY RIVER REGIONAL WWTP m LEGEND NOTE, 1 SIDESTREAM IS PLUGGED IN MH B6 TO DIVERT FLOW TO THE MPS xas xu }sRr �aw �nwra rw u' r� w) � � Ju�Jor�iu�i i¢nm Butt[ K w J nJm� xo- a \ °aux�cm� wa ux sw[exs p��Ex § rue rw. a F Biq ] r.o rYM[5 '_ xP J n � xi J F6 ♦ f�M rrS1•vvw I I I i I 2Pin 9u6 ttv _ � � (I WM Wv Wv W9 WM W9 rw >i w% �BWdC6 VBaCQ1 ttt�� `✓��' Imo_ —_a Water & Sewer Authority of Cabarrus County Rocky River Regional Wastewater Treatment Plant MERCURY MINIMIZATION PLAN May 1, 2014 SECTION I - PURPOSE The purpose of this Mercury Minimization Plan ("MMP") is to describe best management practices through which the Rocky River Regional Wastewater Treatment Plant (RRRWWTP) will seek to reduce the amount of mercury discharged into its system and, ultimately, to the environment. The MMP compiles mercury reduction -related efforts to -date and potential future action items. It is designed to be a working document to help guide the Water & Sewer Authority of Cabanus County (WSACC) in its efforts to control mercury loadings discharged into its Publicly -Owned Treatment Works (POTW) by users of the sewer system. Such a reduction in loadings to the sewer system should translate to a reduction in the amount of mercury which is discharged from the treatment plant. The management practices summarized below may also help control some of the mercury reaching our storm sewer system as well. SECTION II — FACILITY DESCRIPTION WSACC operates a publicly owned treatment works (POTW), including a collection system and wastewater treatment plant (WWTP), which serves the cities of Concord and Kannapolis, towns of Harrisburg and Mt. Pleasant, and Cabarrus County, North Carolina. RRRWWTP's treatment process consists of a permitted 24 MGD facility. The plant design has units of process to remove/reduce suspended, colloidal, and dissolved solids, and the reduction of organic materials via biological oxidation. Ammonia nitrogen is reduced and converted to nitrates by biological oxidation. No tertiary treatment at present. Wastewater enters at MPS (barscreens), then is pumped to Headworks. This flow is combined with additional flows at the front of Headworks. After passing through barscreens, the wastewater flow enters vortex grit chambers for grit removal. From the grit system, wastewater flows to Box 10, where it is split between the 4 primary clarifiers. Depending on flow rate, the typical detention time in the primary clarifiers is 7-8 hours (volume capacity is 1.2 MG each). The supernatant flows thru V notch weirs, then to the aeration basins (mechanical mixing plus 02 blanket). The settled solids of the primaries are pumped to the gravity thickeners. Primary clarifiers remove about 95%of the TSS. The wastewater entering the aeration basins mixes with high purity oxygen and existing micro-organisms allowing for the removal of organic material such as BOD and COD. From the aeration basins the wastewater flows into the secondary clarifiers for additional settling. The supernatant flows thru the V notch weirs and goes on to disinfection. A percentage of the solids removed from the bottom of the secondary's is recirculated to the head of the aeration basin to ensure the predominance of the most effective micro-organisms for BOD and COD removal (returned activated sludge). Determined by lab results for MLSS, we must remove some of those micro-organisms from the process all together (wasting). The Waste Activated Sludge (WAS) is taken out at the same point as the RAS but is not introduced back into the treatment process. Instead it is pumped to the gravity thickeners, or back to the MPS. The supernatant from the Secondary Clarifiers flows to flume 3 (for effluent flow monitoring, plus sodium hypochlorite addition for disinfection). After hypochlorite addition, the flow enters a chlorine 11Page contact basin for a minimum 30 minutes to enable proper disinfection. From the contact basin, the wastewater is treated with sodium bisulfite for residual chlorine depletion to meet permit limits for discharge. The wastewater then passes through sample box 8 to final discharge to the Rocky River. The solids removed from the primary clarifiers are pumped to the gravity thickeners where the water separates and flows over the weirs. The solids are then pumped off the bottom, into the dewatering building, then fed to centrifuges, with polymer addition, to form a "Cake" which is then pumped to the furnace for incineration. Ash .from the incinerated solids is pulled off the bottom hearth of the furnace, mixed with non -potable carry water, and pumped to the ash pond. Most municipal treatment plants are not designed to remove mercury and it is exceedingly expensive to do so to very low levels. Incidental mercury removal occurs through typical municipal treatment with trace levels of mercury (and other metals) ending up in solids removed from the raw wastewater. Mercury is not used in the treatment processes at the WWTP. Mercury may be introduced into the sewer system through a variety of sources, such as from industrial users, laboratories, and other businesses. Residual deposits of mercury are also possible in the sewer system from historic practices. Finally, trace amounts from household products and atmospheric deposition (both wet and dry) contribute to sewer system mercury loadings. While there is typically some mercury contributed to public sewer systems statewide, it is usually in minute quantities and comprises a tiny portion of the already insignificant statewide loading for all point sources just two percent of the annual mercury loadings to all State waters. WSACC has for years measured mercury levels at the treatment plant and strive for a zero discharge SECTION III — PROGRAM PLAN A. EVALUATION OF POTENTIAL NON -DOMESTIC SOURCES CONTRIBUTING MERCURY TO THE POTW Within 24 months from the NPDES required 180-day period for development of an MMP, WSACC will evaluate available information to assess the potential for non -domestic users of the sewer system to contribute mercury to the system. The information to be reviewed may include: (1) POTW influent and effluent mercury data and trends; (2) industrial user permits and associated mercury monitoring data; (3) Toxics Release Inventory (TRI); (4) state hazardous site registry and the National Priority List relating to mercury contamination; and (5) historical records of industrial sites which have contributed mercury loadings to the sewer system. WSACC will also survey and evaluate the following common sources of mercury in its service area: (1) dentist offices; (2) hospitals; (3) laboratories; (4) auto recyclers; and (5) other potential sources of mercury based on existing information. WSACC will request that industrial users review mercury concentrations in high -volume process chemicals and demonstrate that the mercury concentrations are below industry average. WSACC will request that alternative sources for chemicals be explored if the mercury levels are determined to be significantly higher than would normally be expected. 2 1 P a g e The evaluation of potential non -domestic sources of mercury to the sewer system will be updated every five years, as warranted by prior sampling results and any additional new potentially significant sources to the system. B. ADDITIONAL CONTROL MEASURES This MMP identifies reasonable and cost-effective control measures to minimize mercury being discharged into the POTW. Below is a listing of initial BMPs for this POTW. Pollution Prevention Substances used at the WWTP will be evaluated to determine if they contain mercury or mercury -based compounds. Any such chemicals will be evaluated for substitution with non -mercury -containing substances. Housekeeping, Spill Control and Collection. and Education WSACC will develop procedures to minimize the possibility of any spill or release at the WWTP involving mercury containing substances. WSACC will add mercury identification and proper disposal to ongoing and future operator training procedures. Public Outreach WSACC will make available educational information regarding sources of household mercury and appropriate use/disposal practices. This information may be posted on WSACC's website. The availability of this information will be highlighted in periodic reports and/or outreach to WSACC's customers. WSACC will work with the Cabarrus County Household Hazardous Waste Recycling Program to increase public awareness regarding community collection points for mercury -containing products from residents/customers for proper disposal. Periodic reminders of such collection programs will be provided as part of WSACC's ongoing public outreach. Laboratory Practice WSACC operates a laboratory for purposes of complying with state and federal monitoring and sampling requirements. The laboratory is a potential source of small quantities of mercury -containing compounds. Laboratory employees will be trained in the proper handling and disposal of these materials. The laboratories have also replaced mercury thermometers with non -mercury thermometers, whenever practical. Also, WSACC currently recycles all of the COD vials used in the laboratory. C. TRACKING AND MONITORING In order to assess the implementation of the control measures, WSACC proposes to undertake the following evaluations beginning after the first full year that this MMP is implemented: 1. Survey annually at least ten percent (10%) of any non -domestic users identified as possible significant sources of mercury to the POTW; 2. Track the implementation of the programs outlined above; 3. Monitor influent mercury at least annually. Require significant non -domestic sources of mercury to monitor periodically, as warranted; and 4. Measure effluent mercury as required by the NPDES permit. 3 1 P a g e These efforts will allow WSACC to establish a baseline of influent and effluent mercury levels to assist in identifying any trends in mercury contributions from domestic and non -domestic users of the sewer system. This baseline will be tracked annually. SECTION IV — RUPLEMENTATION OF CONTROL MEASURES WSACC's pretreatment program has implemented a local limit for mercury. WSACC's pretreatment program also (1) monitors the significant industrial users for mercury and works with them, if needed, in reducing their mercury load to the POTW; (2) monitors uncontrollable sources to identify potential mercury sources; (3) in the past, has met with the local dental association to discuss mercury (amalgam) removal and the importance of minimizing mercury discharges to the POTW. WSACC will implement the control measures summarized in Section III over the permit term and will update this MMP as warranted. SECTION V - REPORTING A summary of the MMP activities will be submitted as part of the NPDES permit renewal process. 4 1 P a g e Results and summary of Mercury Minimization Plan • Survey was completed of all dental facilities. • Industrial contributors are tested annually. Substitutions were requested if they exceeded the detection level. • Northeast Hospital replaced all mercury thermometers. Northeast is also permitted by WSACC and is evaluated annually. • North Carolina Research Campus is tested annually. • All chemicals at the RRRWWTP are free of mercury and mercury based compounds. • WSACC web page has public information regarding Mercury pollution prevention and control. • WSACC's lab has replaced mercury thermometers with non -mercury thermometers.. whenever practical. We properly disposed of 17 mercury thermometers in March 2016. • WSACC's lab recycles all used COD vials. They are sent to a recycling facility about every three to four months. • Industrial waste survey was conducted in 2018 with no new sources found. • Influent.. in conjunction with outfalls and septic hauler samples are tested for mercury quarterly. Effluent samples are tested quarterly as well. Ash Pond Decant Influent Lower Rocky River 311 Pump Station Hea works (County Outfall) Influent Main Pump Station 311 (Coldwater II- Irish Buffalo Interceptor) WAS Pump Station <— Septage Miscellaneous Plant Drains Primary Sludge Primary Step 1 Primary Clarifiers (5/6) J F WAS Rocky River Regional WWTP — Process Flow Diagram Step 1 Step 1 Aeration Basins --� Secondary Clarifiers SteplScrew Pumps Step 2 Screw Pumps RAS/WAS T Additional Option for * Step 1 Screw Pump Effluent 1 1 I 1 Step 1 Effluent Option 1 I 1 I Step 2 Primary V Step 2 Step 2 Clarifiers (3/4) —_ Aeration Basins Secondary I Clarifiers RAS/WAS F Disinfection Imported Dewatered Non -Potable Sludge Waterfor Imported Liquid Flushing Sludge.I. Water Plant Use W 311 Biosolids Ash to Gravity Thickeners DO Dewatering — > Furnace � Ash Ponds > Land Application ier Overflow . W Centrate Non -Potable Water Quencher Effluent Ash Pond Decant Quencher Treated Effluent to Rocky River (see arrow downstream Revised 3113117 of Headworks above) To Main Pump Station Septage Miscellaneous Plant Drains Imported Liquid Sludge Rocky River Regional WWTP — Process Flow Diagram (Solids Only) Primary Sludge WAS Flushing Water Gravity �10 Thickeners �11 Dewaterin Thickener Overflow Centrate Quencher Effluent Imported Dewatered Sludge I g �10 Furnace Non -Potable Water y Quencher Ash Ponds Biosollds Ash to Land Application Ash Pond Decant (to Headworks) Revised 3/13/17 7A�GtiSwti I lni ji Annual Monitoring and )Pollutant Scan 76miftermit No. NC00362 9. _""'" ( Month November f Outfall _001_ Year _2015 ,• Facility Name _Rocky River W WTP ORC John Ritchie Date of sampling_11/17/15 Phone _(704)788-4164 Analytical Laboratory _WSACC O177, Environment 1 #010 Parameter sample Type .- - Analytical Method Quantitation Level Sample Result . Unite of Measurement Number of samples Ammonia as Composite SM 4500 NH3 D-1997 0.1 0.84 m L 1 Dissolved oxygen Grab SM 4500 O G- 2001 1.0 8.9 m L 1 Nitrate Nitrite Composite EPA 353.2 Rev 2, 1993 0.04 16.56 m L 1 Total K'eldahl nitrogen Composite EPA 351.2, Rev 2, 1993 0.20 2.32 m L 1 Total Phosphorus Composite EPA 365.4 1974 0.04 2.64 m L 1 Total dissolved solids Composite SM 2540 C-1997 1.0 314 m L 1 Hardness Com osite SM 2340 C-1997 0 89 m L 1 Chlorine (total residual, TRC) Grab SM 4500 Cl G-2000 25 <25 µg/L I Oil and grease I Grab IEPA 1664, Rev B 5 <5 m L 1 Metals total recoverable); de and total heitols . . - Antimony Composite EPA 200.8, Rev 5.4, 1994 3.0 <3.0 µg/L 1 Arsenic Composite EPA 200.8, Rev 5.4, 1994 1.0 <2.5 µg/L 1 Beryllium Composite EPA 200.8, Rev 5.4, 1994 1.0 <2.5 µg/L I Cadmium Composite EPA 200.8, Rev 5.4, 1994 1.0 <2.5 µg/L I Chromium Composite EPA 200.8, Rev 5.4, 1994 .1.0 <2.5 µg/L 1 Copper Composite EPA 200.8, Rev 5.4, 1994 1.0 7.3 µg L 1 Lead Composite EPA 200.8, Rev 5.4, 1994 1.0 72.5 µg/L 1 Mercury Composite EPA 245.1 Rev 3, 1994 0.2 <0.2 µg/L 1 Nickel Composite EPA 200.8, Rev 5.4, 1994 1.0 3.6 µg/L 1 Selenium Composite EPA 200.8, Rev 5.4, 1994 2.0 <5.0 µg L 1 Silver Composite EPA 200.8, Rev 5.4, 1994 1.0 <2.5 µg/L 1 Thallium Composite EPA 200.8, Rev 5.4, 1994 1.0 <1.0 µg/L 1 Zinc Composite EPA 200.8, Rev 5.4, 1994 2.0 55.5 µg L 1 Cyq9W Grab SM 4500 CN' E-1999 0.005 <0.005 m L 1 Total phenolic compounds Grab EPA 420.1,1978 5 <5 µg L 1 Vofatf16 wgmdc compounds Acrolein Grab EPA Method 624 100.00 <100.00 µg/L 1 Acrylonitn'le Grab EPA Method 624 50.00 <50.00 µg/L 1 Benzene Grab EPA Method 624 5.00 <5.00 µg/L 1 Bmmoform Grab EPA Method 624 5.00 <5.00 µg L 1 Carbon tetrachloride Grab EPA Method 624 5.00 <5.00 µg/L 1 Chlorobenzene Grab EPA Method 624 5.00 <5.00 µg L 1 Chkmodibromomethane Grab EPA Method 624. 5.00 <5.00 µg L 1 Chlomethane Grab EPA Method 624 10.00 <10.00 µg/L 1 2-chloroethylvinyl ether Grab EPA Method 624 5.00 <5.00 µg/L 1 Chloroform Grab EPA Method 624 5.00 <5.00 µg L 1 Dichhorobmmomethane Grab EPA Method 624 10.00 <10.00 µg/L 1 1,1-dichlomethane Grab EPA Method 624 5.00 <5.00 µg/L 1 1,2-dichloroetbane Grab EPA Method 624 5.00 <5.00 µg/L 1 'hans-1,2-dichloroethyleae Grab EPA Method 624 5.00 <5.00 µg/L 1 Parameter Sample Type -Analytical Method Quantitation Level I sample Result unite of lNewaurament Number of samples Volatile orgaule com ounds Cont. - - - 1,1-dichloroethylene Grab EPA Method 624 5.00 <5.00 µg L 1 1,2-dichloropropane Grab EPA Method 624 5.00 <5.00 µg/L 1 1,3-dichloropmpylene Grab EPA Method 624 5.00 <5.00 µg/L 1 Ethylbenzene Grab EPA Method 624 5.00 <5.00 µg L 1 Methyl bromide Grab EPA Method 624 10.00 <10.00 µg/L 1 Methyl chloride Grab EPA Method 624 10.00 <10.00 µg/L 1 Methylene chloride Grab EPA Method 624 10.00 <10.00 µg/L 1 1,1,2,2-tetrachlomethme Grab EPA Method 624 5.00 <5.00 µg/L 1 Tetrachloroethylene Grab EPA Method 624 5.00 <5.00 1 1 Form - DMR- PPA-1 Page 1 Annual Monitoring and Pollutant Scan permit No. _NC0036269_ Month November Outfall _001_ Year N015 (Toluene Grab EPA Method 624 5.00 1 <5.00 I µg/L 1 1,1,1-trichloroethane Grab EPA Method 624 5.00 <5.00 µg/L 1 en 1,1,2-trichlorcethe Grab EPA Method 624 5.00 <5.00 µg/L 1 Trichloroethylene Grab EPA Method 624 5.00 <5.00 Vinyl chloride Grab I EPA Method 624 10.00 <10.00 µg/L 1 Ara -extractable com ounda - P-chloro-m-creso Grab EPA Method 625 20.00 <20.00 µg/L 1 2-chlorophenol Grab EPA Method 625 10.00 <10.00 µg L 1 2,4-dichlorophenol Grab EPA Method 625 10.00 <10.00 µg L 1 2,4-dimethylphenol Grab EPA Method 625 10.00 <10.00 pg/L 1 4,6-dinitro-o-crescl Grab EPA Method 625 50.00 <50.00 µg/L 1 2,4-dinitrophenol Grab EPA Method 625 50.00 <50.00 µg/L 1 2-nitrophenol Grab EPA Method 625 10.00 <10.00 µg L 1 4-nitropheaol Grab EPA Method 625 50.00 <50.00 µg/L 1 Pentachlorophenol Grab EPA Method 625 50.00 <50.00 Phenol Grab EPA Method 625 30.00 <10.00 µg/L 1 2,4,6-trichlomphenol Grab EPA Method 625 10.00 <10.00 µg/L 1 Base -neutral compounds Acenaphthene Grab EPA Method 625 10.00 <10.00 µg/L 1 Acensphthylene Grab EPA Method 625 10.00 <10.00 µg/L 1 Anthracene Grab EPA Method 625 10.00 <10.00 µg/L 1 Benzidine Grab EPA Method 625 100.00 <100.00 µg L 1 Benzo(a)anthracene Grab EPA Method 625 10.00 <10.00 µg/L 1 Benzo(a)pyrene Grab EPA Method 625 10.00 <10.00 µg/L 1 3,4 benzofluoranthene Grab EPA Method 625 10.00 <10.00 µg/L 1 Benzo(gh4perylene Grab EPA Method 625 10.00 <10.00 µg L 1 Benzo(k)lluoranthene Grab EPA Method 625 10.00 <10.00 µg/L 1 Bis (2-cbloroethoxy) methane Grab EPA Method 625 10.00 <10.00 µg/L 1 Bis (2-chlomethyl) ether Grab EPA Method 625 10.00 <10.00 µg L 1 Bis (2-chloroisopropyl) ether Grab EPA Method 625 10.00 <10.00 µg/L 1 Bis (2-ethylhexyl) phthalate Grab EPA Method 625 20.00 <20.00 µg L 1 4-bromophenyl phenyl ether Grab EPA Method 625 10.00 <10.00 µg L 1 Butyl benzyl phthalate Grab EPA Method 625 10.00 <10.00 µg/L 1 2-chloronsphthalene Grab EPA Method 625 10.00 <10.00 µg L 1 4-chioropheuyl phenyl ether Grab EPA Method 625 10.00 <10.00 pg L 1 - Parameter . 9enipie Type Analytical Method Quantltation Level Sample _ Result - Units of Measurement Number of samples Base-noatral com ounds coat. Chrysene Grab EPA Method 625 10.00 <10.00 µg/L 1 Di-n-butyl phthalate Grab EPA Method 625 10.00 <10.00 µg/L 1 Di-n-octyl phthalate Grab EPA Method 625 10.00 <10.00 µg L 1 Dibenzo(a,h)anthracene Grab EPA Method 625 10.00 <10,00 µg/L 1 1,2-dichlorobenzene Grab EPA Method 625 10.00 <10.00 µg/L 1 1,3-dichlorobenzene Grab EPA Method 625 10.00 <10.00 µg/L 1 1,4-dichlorobeczene Grab EPA Method 625 10.00 <10.00 µg/L 1 3,3-dichlorobenzidine Grab EPA Method 625 10.00 <10.00 pg/L 1 Diethyl phthalate I Grab 1EPA Method 625 10.00 <10.00 µg/L 1 Dimethylphthalate Grab EPA Method 625 10.00 <10.00 µg/L 1 2,4-dinitrotol2ene Grab EPA Method 625 10.00 <10.00 µg/L 1 2,6-dinitrotolueae Grab EPA Method 625 10.00 <10.00 µg/L 1 1,2- Uphenylhydrazine Grab EPA Method 625 10.00 <10.00 µg/L 1 Fluoranthene Grab EPA Method 625 10.00 <10.00 µg/L 1 Fluorenc Grab EPA Method 625 10.00 <10.00 µg/L 1 Hexachlorobenzene Grab EPA Method 625 10.00 <10.00 µg/L 1 Hexachlorobutadiene Grab EPA Method 625 10.00 <10.00 µg/L 1 Hexachlorocyclo-pentadiene Grab EPA Method 625 10.00 <10.00 µg/L 1 Hexachloroethane Grab EPA Method 625 10.00 <10.00 µg L 1 Indeao(1,2,3-cd)pyrene Grab EPA Method 625 10.00 <10.00 µg L 1 Isophorone Grab EPA Method 625 10.00 <10.00 µg/L 1 Form - DMR- PPA-1 Page 2 Permit No. NC0036269_ Outfall _001_ Annual MOnitoring and Pollutant Scan Month _November_ Yea- nm e Naphthalene Grab EPA Method 625 10.00 <10.00 Nitrobenzene Grab EPA Method 625 10.00 <10.00 µg/L I N-nitrosodi-n-propylamine Grab EPA Method 625 10.00 <10.00 µg/L 1 N-rritmsodimethylemine Grab EPA Method 625 10.00 <10.00 µg/L 1 N-nitrosodiphenylamine Grab EPA Method 625 10.00 <10.00 µg/L I Phenanthrene Grab EPA Method 625 10.00 <10.00 µg/L 1 pyrene Grab EPA Method 625 10.00 <10.00 1,2,4,-trichlorobenzene Grab EPA Method 625 10.00 <10.00 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordancewitha system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or Persons who managed the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Authorized Representative name Sig¢ature . t F/I / 20/8 Date Ibrm - DMR- PPA-1 Page 3 Annual Monitoring and Pollutant Scan ennit No. NC0036269 Month May `{ Outfall _.001 Year 2016 `f. Zf ' Facility Name Rocky River WWTP ORC John Ritchie Date of sampling 5/3/2016 Phone (704)788-4164 Analytical Laboratory WSACC #0177, Environment 1 #010 Pauaeter Sample Type :... .. : . , Analytical Method : Quantitatidn Levol. , Sample Result IInits of= ICeasurement l�In�nber of samples' Ammonia as Composite SM 4500 NH3 D-1997 0.1 0.31 m L 1 Dissolved oxygen Grab SM 4500 O G- 2001 1.0 8.5 raL 1 Nitrate Nitrite Composite EPA 353.2, Rev 2, 1993 0.04. 19.04 m L 1 Total K'eldahl nitrogen Composite EPA 351.2, Rev 2, 1993 0.20 2.72 m L 1 Total Phosphorus Composite SM 4500 P E-1999 0.03 2.05 m L 1 Total dissolved solids Composite SM 2540 C-1997 1.0 340 m L 1 Hardness Composite SM 2340 C-1997 0 1 120 1 m L 1 1 Chlorine (total residual, TRC) Grab SM 4500 C1 0-2000 25 35 µg/L 1 Oil and grease Grab EPA 1664, Rev B 5 <5 m L 1 m6tals total recoverable), c aaide.ead. total:: Antimony Composite EPA 200.8, Rev 5.4, 1994 3.0 <3.0 µg/L 1 Arsenic Composite EPA 200.8, Rev 5.4, 1994 1.0 <2.5 µg/L 1 Beryllium Composite EPA 200.8, Rev 5.4, 1994 1.0 <2.5 µg/L 1 Cadmium Composite EPA 200.8, Rev 5.4, 1994 1.0 <2.5 µg/L ! Chromium Composite EPA 200.8, Rev 5.4, 1994 1.0 <2.5 µg/L 1 Copper Composite EPA 200.8, Rev 5.4, 1994 1.0 8.6 µg/L 1 Lead Composite EPA 200.8, Rev 5.4, 1994 1.0 <2.5 µg/L 1 Mercury Composite SM 3112 B-2009 0.2 <0.2 µg/L 1 Nickel Composite EPA 200.8, Rev 5.4, 1994 1.0 3.0 µg/L 1 Selenium Composite EPA 200.8, Rev 5.4, 1994 2.0 <5.0 µg/L 1 Silver Composite EPA 200.8, Rev 5.4, 1994 1.0 <2.5 µg/ L 1 Thallium Composite EPA 200.8, Rev 5.4, 1994 1.0 <1.0 µg/L 1 Zinc Composite EPA 200.8, Rev 5.4, 1994 2.0 37.3 µg L 1 Cyanide Grab SM 4500 CN- E-1999 0.005 <0.005 m /L 1 Total phenolic compounds Grab EPA 420.1,1978 5 <5 µg/L 1 Volatile or a coat' oliads ' Acrolein Grab EPA Method 624 100.00 <100.00 µg/L 1 Acrylonitrile Grab EPA Method 624 50.00 <50.00 µg/L 1 Benzene Grab EPA Method 624 5.00 <5.00 µg/L 1 Bromoform Grab EPA Method 624 5.00 <5.00 µg/L 1 Carbon tetrachloride Grab EPA Method 624 5.00 <5.00 µg/L 1 Chlorobenzene Grab EPA Method 624 5.00 <5.00 µg/L 1 Chlorodibromomethane Grab EPA Method 624 5.00 <5.00 µg/L 1 Chloroethane Grab EPA Method 624 10.00 <10.00 µg/L 1 2-chloroethylvinyl ether Grab EPA Method 624 5.00 <5.00 µg/L 1 Chloroform Grab EPA Method 624 5.00 <5.00 µg/L 1 Dichlorobromomethane Grab EPA Method 624 5.00 <5.00 µg/L 1 1,1-dichloroethane Grab EPA Method 624 5.00 <5.00 µg/L 1 1,2-dichloroethane Grab EPA Method 624 5.00 <5.00 µg/L 1 Trans-1,2-dichloroethylene Grab EPA Method 624 5.00 <5.00 µg L 1 Parameter 3dmple e : Analytical Method Quantitatioa L$vol Sample.. �tasnlf' rI Units of Measniremeat Number of I samples Volatile° 6r .. c coai ounds (Coat, 1,1-dicMaroethylene Grab EPA Method 624 5.00 <5.00 µg/L 1 1,2-dichloropropane Grab EPA Method 624 5.00 <5.00 µg/L 1 1,3-dichloropropylene Grab EPA Method 624 5.00 <5.00 µg/L 1 Etbylbenzene Grab EPA Method 624 5.00 <5.00 µg/L 1 Methyl bromide Grab EPA Method 624 10.00 <10.00 µg/L 1 Methyl chloride Grab EPA Method 624 10.00 <10.00 µg/L 1 Metbylene chloride Grab EPA Method 624 10.00 <10.00 µg/L 1 1,1,2,2-tetrachloroethane Grab EPA Method 624 5.00 <5.00 µg/L 1 Tetrachloroethylene Grab EPA Method 624 5.00 <5.00 µg/L 1 Form - DMR- PPA-1 /-Page /1 4T �j Vermit No. _NC0036269 ' Outfall001 iene Annual Monitoring and Pollutant Scan Grab I EPA M Month May Year 2016 <5.00 1 ug 1, 1, 1-trichloroethane Grab EPA Method 624 5.00 <5.00 µg/ L 1 1,1,2-trich1oroethane Grab EPA Method 624 5.00 <5.00 µg/L 1 Trichloroethylene Grab EPA Method 624 5.00 <5.00• µg/L 1 Vinyl chloride Grab EPA Method 624 10.00 <10.00 µg/L 1 Acid -extractable com ounds P-chloro-m-creso Grab EPA Method 625 20.00 <20.00 µg L 1 2-chlorophenol Grab EPA Method 625 10.00 <10.00 µg L 1 2,4-dichlorophenol Grab EPA Method 625 10.00 <10.00 µg/L 1 2,4-dimethylplienol Grab EPA Method 625.' 10.00 <10.00 µg/L 1 4,6-dinitro-o-cresol Grab EPA Method 625 50.00 <50.00 µg/L 1 2,4-dinitrophenol Grab EPA Method 625 50.00 <50.00 µg/L 1 2-nitrophenol Grab EPA Method 625 10.00 <10.00 µg L 1 4-nitrophenol Grab EPA Method 625 50.00 <50.00 µg/L 1 Pentachlorophenol Grab EPA Method 625 50.00 <50.00 µg/L 1 Phenol Grab EPA Method 625 10.00 <10.00 µg L 1 2,4,6-trichlorophenol Grab EPA Method 625 10.00 <10.00 µg/L 1 Base -neutral coinpounds . Acenaphthene Grab EPA Method 625 10.00 <10.00 µg/L 1 Acenaphthylene Grab EPA Method 625 10.00 <10.00 µg/L 1 Anthracene Grab EPA Method 625 10.00 <10.00 µg/L 1 Benzidme Grab EPA Method 625 100.00 <100.00 µg/L 1 Benzo(a)anthracene Grab EPA Method 625 10.00 <10.00 µg L 1 Benzo(a)pyrene Grab EPA Method 625 10.00 <10.00 µg/L 1 3,4 benzofluoranthene Grab EPA Method 625 10.00 <10.00 µg L 1 Benzo(ghi)perylene Grab EPA Method 625 10.00 <10.00 µg L 1 Benzo(k)fluoranthene Grab EPA Method 625 10.00 <10.00 µg/L 1 Bis (2-chloroethoxy) methane Grab EPA Method 625 10.00 <10.00 µg/L 1 Bis (2-chlomethyl) ether Grab EPA Method 625 10.00 <10.00 µg L 1 Bis (2-chloroisopropyl) ether Grab EPA Method 625 10.00 <10.00 µg/L 1 Bis (2-ethylhexyl) phthalate Grab EPA Method 625 20.00 <20.00 µg/L 1 4-bromophenyl phenyl ether Grab EPA Method 625 10.00 <10.00 µg/L 1 Butyl benzyl phthalate Grab EPA Method 625 10.00 <10.00 µg L 1 2-chloronaph#halene Grab EPA Method 625 10.00 <10.00 µg/L 1 4-chlorophenyl phenyl ether Grab EPA Method 625 10.00 <10.00 µg/L 1 Parameter Sample Type Analytical Method Quaatitation Level. Sample Result Units of Measurement Number of samples Base -neutral com onnds (coat. Chrysene Grab EPA Method 625 10.00 <10.00 µg/L 1 Di-n-butyl phthalate Grab EPA Method 625 10.00 <10.00 µg/L 1 Di-n-octyl phthalate Grab EPA Method 625 10.00 <10.00 µg/L 1 Dibenzo(ah)anthracene Grab EPA Method 625 10.00 <10.00 µg/L 1 1,2-dichlorobenzene Grab EPA Method 625 10.00 <10.00 µg/L 1 1,3-dichlorobenzene Grab EPA Method 625 10.00 <10.00 µg/L 1 1,4-dichlorobenzene Grab EPA Method 625 10.00 <10.00 µg L 1 3,3-dichlorobenzidine Grab EPA Method 625 10.00 <10.00 µg L 1 Diethyl phthalate Grab EPA Method 625 10.00 <10.00 µg/L 1 Dimethyl phthalate Grab EPA Method 625 10.00 <10.00 µg/L 1 2,4-dinitrotoluene Grab EPA Method 625 10.00 <10.00 µg L 1 2,6-dinitrotoluene Grab EPA Method 625 10.00 <10.00 µg L 1 1,2-diphenlylhydrazine Grab EPA Method 625 10.00 <10.00 µg L 1 Fluoranthene Grab EPA Method 625 10.00 <10.00 µg/L 1 Fluorene Grab EPA Method 625 10.00 <10.00 µg/L 1 Hexachlorobenzene Grab EPA Method 625 10.00 <10.00 µg/L 1 Hexachlorobutadiene Grab EPA Method 625 10.00 <10.00 µg/L 1 Hexachlorocyclo-pentadiene Grab EPA Method 625 10.00 <10.00 µg/L 1 Hexachloroethane Grab EPA Method 625 10.00 <10.00 µg/L 1 Indeno(1,2,3-cd)pyrene Grab EPA Method 625 10.00 <10.00 µg L 1 Isophorone I Grab IEPA Method 625 10.00 <10.00 µg/L 1 Form - DMR- PPA-1 Page 2 tl �H Annual Monitoring and Pollutant Scan ermit No.—NC0036269 Month May Outfall 001 Year 2016 ,iRaphdWene Grab EPA Method 625 10.00 <10.00 µg/L 1 Nitrobenzene Grab EPA Method 625 10.00 <10.00 µg/L 1 N-nitrosodi-n-propylamine Grab EPA Method 625 10.00 <10.00 µg/L 1 N-nitrosodimethylamine Grab EPA Method 625 10.00 <10.00 µg/L 1 N-nitrosodiphenylamine Grab EPA Method 625 10.00 <10.00 µg/L 1 Phenanthrene Grab EPA Method 625 10.00 <10.00 µg/L 1 Pyrene Grab EPA Method 625 10.00 <10.00 µg/L 1 1,2,4,-trichlorobenzene Grab EPA Method 625 10.00 <10.00 µg/L 1 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief; true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Authorized Representative name SiE 0 Kra, Date //.T� Form - DMR- PPA--1 Page 3 1}2 r.. Annual Monitoring and Pollutant Scan ';Permit No. _NC0036269 '" Outfall ^001 Facility Name _Rocky River WWTP Date of sampling 8/ 1/2017 Analytical Laboratory WSACC #0177, Environment 1 #010 Month -August_ Year 2017 ORC John Ritchie Phone (704)788-4164 Parameter gample Type Ana1y13cal Method Quantitatiod Level Sample Result Unfts of Measurement Number of samples Ammonia (as N) Dissolved oxygen Nitrate/Nitrite Total Kjeldahl nitrogen Total Phosphorus Total dissolved solids Composite Grab Composite Composite Composite Composite SM 4500 NH3 D-1997 SM 4500 O G- 2001 EPA 353.2, Rev 2, 1993 EPA 351.2, Rev 2, 1993 HACH 8190 TNT SM 2540 C-1997 0.1 1.0 0.04 0.20 0.05 1.0 0.12 7.6 20.04 2.35 3.30 410 mg/L mg/L mg/L mg/L mg/L mg/L 1 1 1 1 1 1 Hardness Composite SM 2340 C-1997 5.0 113 mg/L 1 Chlorine (total residual, TRC) Oil and grease Grab Grab SM 4500 Cl G-2000 EPA 1664, Rev B 25 5 29 <6 µg/L mg/L 1 1 Metals (total recoverable), npanide Antimony Arsenic as aotsl Composite Composite EPA 200.8, Rev 5.4, 1994 3.0 <3.0 µg 1 EPA 200.8, Rev 5.4, 1994 1.0 <2.5 µg/L 1 Beryllium Cadmium Composite Composite EPA 200.8, Rev 5.4, 1994 EPA 200.8, Rev 5.4, 1994 1.0 1.0 <2.5 <2.5 µg/L µg/L 1 1 Chromium Composite EPA 200.8, Rev 5.4, 1994 1.0 <2.5 µg/L 1 Copper Lead Composite Composite EPA 200.8, Rev 5.4, 1994 EPA 200.8, Rev 5.4, 1994 1.0 1.0 8.4 <2.5 µg/L jig/L 1 1 Mercury Nickel Composite Composite SM 3112 B-2009 EPA 200.8, Rev 5.4, 1994 0.2 1.0 <0.2 4.7 µg/L µg/L 1 1 Selenium Composite EPA 200.8, Rev 5.4, 1994 2.0 <5.0 N•g/L 1 Silver Composite EPA 200.8, Rev 5.4, 1994 1.0 <2.5 µg/L 1 Thallium Composite EPA 200.8, Rev 5.4, 1994 1.0 <1.0 I19/L 1 Zinc Composite EPA 200.8, Rev 5.4, 1994 2.0 55.9 lg/L 1 Cyanide Total phenolic compounds Grab Grab SM 4500 CN' E-1999 EPA 420.1,1978 0.005 5 <0.005 <5 mg/L leg/L 1 1 Volatile organic compounds Acrolein Grab EPA Method 624 100.00 <100.00 µg/L 1 Acrylonitrile Benzene Grab Grab EPA Method 624 EPA Method 624 50.00 5.00 <50.00 <5.00 µb/L ttg/L 1 1 Bromoform Grab EPA Method 624 5.00 <5.00 µg/L 1 Carbon tetrachloride Grab EPA Method 624 5.00 <5.00 µg/L 1 Chlorobenzene Grab EPA Method 624 5.00 <5.00 µg/L 1 Chlorodibromomethane Grab EPA Method 624 5.00 <5.00 ltg/L 1 Chloroethane Grab EPA Method 624 10.00 <10.00 µg/L 1 2-chloroethylvinyl ether Grab EPA Method 624 5.00 <5.00 µg/L 1 Chloroform Grab EPA Method 624 5.00 <5.00 µg/L 1 Dichlorobromomethane Grab EPA Method 624 5.00 <5.00 gg/L 1 1,1-dichloroethane Grab EPA Method 624 5.00 <5.00 ug/L 1 1,2-dichloroethane Trans-1,2-dichloroethylene Grab Grab EPA Method 624 EPA Method 624 5.00 5.00 <5.00 <5.00 µg/L µg/L 1 1 Parameter Sample Type. Analytical Method Quantitation Level Sample Result Units of Measurement Number of samples Volatile organic compounds (Cont.) 1,1-dichloroethylene Grab EPA Method 624 5.00 <5.00 pg/L 1 1,2-dichloropropane Grab EPA Method 624 5.00 <5.00 µg L 1 Form - DMR- PPA-1 �� P e 1 (/(P r FPermit No. _NC0036269, � Gutfau 001 77, Annual Monitoring and Pollutant Scan Month --August_ Year 2017 1,3-dichloropropylene Grab EPA Method 624 5.00 <5.00 µg/L 1 Ethylbenzene Grab EPA Method 624 5.00 <5.00 µg/L I Methyl bromide Grab EPA Method 624 10.00 <10.00 µg L 1 Methyl chloride Grab EPA Method 624 10.00 <10.00 ttg/L 1 Methylene chloride Grab EPA Method 624 10.00 <10.00 µg/L 1 1,1,2,2-tetrachloroethane Grab EPA Method 624 5.00 <5.00 µg/L 1 Tetrachloroethylene Grab EPA Method 624 5.00 <5.00 µg/L 1 Toluene Grab EPA Method 624 5.00 <5.00 µg/L 1 1,1,1-trichloroethane Grab EPA Method 624 5.00 <5.00 µg/L 1 1,1,2-trichloroethane Grab EPA Method 624 5.00 <5.00 !lg/L 1 Trlchloroethylene Grab EPA Method 624 5.00 <5.00 µg/L 1 Vinyl chloride Grab EPA Method 624 10.00 <10.00 µg/L I Acid -extractable compounds P-chloro-m-creso Grab EPA Method 625 20.00 <20.00 µg/L 1 2-chlorophenol Grab EPA Method 625 10.00 <10.00 µg/L 1 2,4-dichlorophenol Grab EPA Method 625 10.00 <10.00 µg/L 1 2,4-dimethylphenol Grab EPA Method 625 10.00 <10.00 µg/L 1 4,6-dinitro-o-cresol Grab EPA Method 625 50.00 <50.00 µg/L 1 2,4-dinitrophenol Grab EPA Method 625 50.00 <50.00 µg/L 1 2-nitrophenol Grab EPA Method 625 10.00 <10.00 µg/L 1 4-nitrophenol Grab EPA Method 625 50.00 <50.00 µg/L 1 Pentachlorophenol Grab EPA Method 625 50.00 <50.00 µg/L 1 Phenol Grab EPA Method 625 10.00 <10.00 µg/L 1 2,4,6-tdchlorophenol Grab EPA Method 625 10.00 <10.00 µg/L 1 Base -neutral compounds Acenaphthene Grab EPA Method 625 10.00 <10.00 µg/L 1 Acenaphthylene Grab EPA Method 625 10.00 <10.00 µg/L 1 Anthracene r Grab EPA Method 625 10.00 <10.00 µg/L 1 Benzidine Grab EPA Method 625 100.00 <100.00 µg L 1 Benzo(a)anthracene Grab EPA Method 625 10.00 <10.00 µg/L 1 Benzo(a)pyrene Grab EPA Method 625 10.00 <10.00 µg/L 1 3,4 benzofluoranthene Grab EPA Method 625 10.00 <10.00 µg/L 1 Benzo(&)perylene Grab EPA Method 625 10.00 <10.00 µg/L 1 Benzo(k)fluoranthene Grab EPA Method 625 10.00 <10.00 µg/L 1 Bis (2-chloroethoxy) methane Grab EPA Method 625 10.00 <10.00 jig/L 1 Bis (2-chloroethyl) ether Grab EPA Method 625 10.00 <10.00 µg/L 1 Bis (2-chloroisopropyl) ether Grab EPA Method 625 10.00 <10.00 µ8/L 1 Bis (2-ethylhexyl) phthalate Grab EPA Method 625 20.00 <20.00 µg/L 1 4-bromophenyl phenyl ether Grab EPA Method 625 10.00 <10.00 µg/L 1 Butyl benzyi phthalate Grab EPA Method 625 10.00 <10.00 µg/L 1 2-chloronaphthalene Grab EPA Method 625 10.00 <10.00 µg/L 1 4-chlorophenyl phenyl ether Grab EPA Method 625 10.00 <10.00 µg/L 1 . Parameter Sample Type Analytical Method Quantitation ..Level Sample Result Vans of Measurement Number of samples Base -neutral compounds (coat.) Chrysene Grab EPA Method 625 10.00 <10.00 µg/L 1 Di-n-butyl phthalate Grab EPA Method 625 10.00 <10.00 µg/L 1 Di-n-octyl phthalate Grab EPA Method 625 10.00 <10.00 jLg/L 1 Dibenzo(ah)anthracene Grab EPA Method 625 10.00 <10.00 µg/L 1 1,2-dichlorobenzene Grab EPA Method 625 10.00 <10.00 µg/L 1 1,3-dichlorobenzene Grab EPA Method 625 10.00 <10.00 µg/L 1 1,4-dichlorobenzene Grab JEPA Method 625 10.00 <10.00 µg/L 1 Form - DMR- PPA-1 page 2 Annual Monitoring and Pollutant Scan ermit No.-NC0036269 Month August 'r Outfall._001 Year 2017 3,3-dichlorobenzidiae Grab EPA Method 625 10.00 <10.00 µg/L 1 Diethyl phthalate Grab EPA Method 625 10.00 <10.00 µg/L 1 Dimethyl phthalate Grab EPA Method 625 10.00 <10.00 µg/L 1 2,4-dinitrotoluene Grab EPA Method 625 10.00 <10.00 µg/L 1 2,6-dinitrotoluene Grab EPA Method 625 10.00 <10.00 µg/L 1 1,2-dfphenylhydrazine Grab EPA Method 625 10.00 <10.00 µg/L 1 Fluoranthene Grab EPA Method 625 10.00 <10.00 µg/L 1 Fluorene Grab EPA Method 625 10.00 <10.00 µg/L 1 Hexachlorobenzene Grab EPA Method 62S 10.00 <10.00 µg/L 1 Hexachlorobutadiene Grab EPA Method 625 10.00 <10.00 µg/L 1 Hexachlorocyclo-pentadiene Grab EPA Method 625 10.00 <10.00 µg/L 1 Hexachloroethane Grab EPA Method 625 10.00 <10.00 µg/L 1 Indeno(1,2,3-cd)pyrene Grab EPA Method 625 10.00 <10.00 µg/L 1 Isophorone Grab EPA Method 625 10.00 <10.00 µg/L 1 Naphthalene Grab EPA Method 625 10.00 <10.00 µg/L 1 Nitrobenzene Grab EPA Method 625 10.00 <10.00 µg/L 1 N-nitrosodi-n-propylamine Grab EPA Method 625 10.00 <10.00 µg/L 1 N-nitrosodimethylamine Grab EPA Method 625 10.00 <10.00 µg/L 1 N-nitrosodiphenylamine Grab EPA Method 625 10.00 <10.00 µg/L 1 Phenanthrene Grab EPA Method 625 10.00 <10.00 µg/L 1 Pyrene Grab EPA Method 625 10.00 <10.00 µg/L 1 1,2,4,-trichlorobenzene Grab EPA Method 625 10.00 <10.00 µg/L 1 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry ofthe'person or persons who managed the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belied true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Authorized Representative name a e Date Form - DMR- PPA-1 Page 3 --W Effluent Toxicity Report Form -Chronic Fathead Minnow Multi -Concentration Test Date:2/24/2017 Facility. WCACC Laboratory: Meritech, Inc. x Signature of Operator in Res pnslb x Signature of Laboratory Supervisor NPDES # NC00 36269 MAIL ORIGINAL TO: Water Sciences Section Aquatic Toxicology Branch Division of Water Resources 1621 Mail Service Center Raleigh, N.C. 27699-1621 Pipe #: 001 County: Cabarrus Test Initiation Date/Tlme 2/14/2017 5:10 PM Avg WtlSurv. Controll 2.746 % Eff. Repl. 1 2 3 4 Control Surviving # Original # Wt/odginal (mg) 31 Surviving # Original # Wt/original (mg) High Concentration pH (SU) Init/Fin DO (mg/L) lnit/Fin Temp (C) InitlFin Sample Collection Start Date Grab Composite (Duration) Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) Chlorine(mg/L) Temp. at Receipt VQ 10 9 10 9 10 10 10 10 0.762 7.620 0.755 0.901 10 10 10 8 10 10 10 10 0.824 0.798 0.824 0.606 10 10 10 10 10 10 10 10 0.784 0.699 0.756 0.814 10 10 10 10 10 10 10 10 10 9 10 10 10 10 10 i0 0.863 0.754 0.$34 0.752 10 10 10 10 10 10 10 10 %Survival 95.0 EO.702 EO.871 Test Organisms Cultured In -House Outside Supplier Avg Wt (mg) 2.510 Hatch Date: 2/13117 %Survival 85.0 Hatch Time: 3:00 pm CT Avg Wt (mg) 0.763 8.06 / 7.85 8.04 / 7.86 8.09 1 7.96 8.15 / 7.97 8.22 / 7.94 8.18 / 7.89 8.19 / 7.65 8.20 / 7.28 7.97 1 6.95 8.13 ! 7.51 7.98 1 7.66 8.07 17.54 8.01 / 7.20 7.84 / 6.38 24.7 / 24.8 25.1 / 24.8 24.1 1 24.0 124.8 / 24.4 24.4 / 25.6 25.1 / 25.4 24.8 / 24.7 0 1 2 3 4 5 6 7.38 / 7.97 7.40 / 7.80 7.18 / 7.94 7.57 / 8.09 7.80 / 8.12 7.78 / 7.82 7.45 J 7.69 8.45 1 7.37 8.26 / 6.60 8.54 / 7.35 7.95 / 7.60 7.97 J 7.52 7.63 1 6.95 7.92 / 6.10 25.0 / 24.8 25.5 / 25.0 25.2 1 24.5 25.9 / 25.4 25.6 / 25.1 24.6 / 24.3 25.0 1 24.2 1 2 3 2/13/2017 2/15/2017 ZM 6/2017 23.8 24.0 24.0 96 104 110 62 91 90 602 644 638 <0.1 <0.1 <0.1 1.5 1.5 1.5 Dilution H2O Batch # 1122 1123 1124 1125 Hardness (mglL) 44 46 42 44 Alkalinity (mg/l) 55 50 52 50 Conductivity (umhoslcm) 192 206 204 195 Survival Growth Norma! �"`) M Hom. Var. �( NOEC 100 100 LOEC >100 >100 ChV >100 >100 Method Steeps Dunnett's Overall Result ChV >100 Slats Survival Growth Conc. Critical Calculated Critical calculated 31 10 19 2.41 0.5229 46.5 10 22 2.41 0.5188 62 10 22 2.4i 0.841 S 81 10 20 2.41-0.0940 100 10 22 2.41 0.7026 46.5 Surviving # %Survival 100.0 Original # Wt/original (mg) Avg Wt (mg) 0.763 ® Surviving # °%Survival 100A Original # Wt/original (mg) fluent I oxlCity Report corm-%onronic raineau Minnow mums-wncentraiton i esi Facility: WSACC NPDES # NC00 36269 Pipe #. 001 County: Cabarrus Laboratory: Meritech, Inc. 1commentsi X Signature of �Operator ' >€n �eppons ,te Charge MAIL ORIGINAL TO: Water Sciences Section Aquatic Toxicology Branch Division of Water Resources 1621 Mail Service Center Raleigh, N.C. 27699-1621 Test Initiation Date/Time 5/2/2017 4:15pm Avg WUSurv. Controll 0.907 % Eff. Repi. 1 2 3 4 Control I Surviving # Original # WUoriginal (mg) 31 Surviving # Original # Wt/original (mg) 8 7 10--j 10 10 10 10 10 0.742 0.772 0.765 0.834 10 9 9 10 10 10 10 10 0.975 0.931 0.737 0.769 % Survival 87.5 Test Organisms Cultured In -House Outside Supplier Avg Wt (mg) 1 0.778 j Hatch Date: 5/1117 % Survivall 95.0 Hatch Time: 3:00 pm CT Avg Wt (mg) 0.853 46.5 Surviving # % Survival 100.0 Original # Wt/odginal (mg) Avg Wt (mg) 0.941 62 Surviving # %Survival 9 7.5 Original # Wt/original (mg) Avg Wt (mg) 0.858 81 Surviving # %Survival 92.5 Original # Wt/odginal (mg) Avg Wt (mg) 0.861 100 Surviving # % Survival 97.5 Original # Wt/original (mg)EO.853Avg Wt (mg) 0.866 Water Quality Data Day Control 0 1 2 3 4 5 6 pH (SU) Init/Fin pH (SU) In€t/Fln Sample 1 2 3 Survival Growth Collection Start Date Grab Composite (Duration) Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) Chlodne(mg/L) Temp. at Receipt (°C) i0 10 10 10 10 10 10 10 0.904 0.946 0.845 1.068 10 9 10 10 10 10 10 10 0.877 0.889 0.749 0.917 10 10 7 10 io 10 10 10 0.812 0.698 0.926 1.008 9 10 10 10 10 10 10 10 0.855 0.870 0.885 8.08 / 7.70 8.01 / 7.$3 8.22 17.82 8.18 1 8.08 8.27 / 7.89 8.20 / 7.90 8.26 / 7.66 6.97 ! 7.62 7.06 / 7.73 6.86 ! 7.59 7.11 / 7.95 7.69 / 7.59 7.06 / 7.64 7,00 / 7.43 5/1 /2017 5/3/2017 5/4/2017 24.8 24.0 24.0 96 112 112 45 55 56 549 569 603 <0.1 <0.1 <0.1 2.1 2.1 1.2 Dilution H2O Batch # 1156 1157 1158 Hardness (mg/L) 44 46 42 Alkalinity (mg/L) 54 53 57 Conductivity (umhos/cm) 208 208 209 Normal yes Hom. Var. jf"( � NOEC 100 100 LOEC >100 >100 ChV >100 >100 Method Steers Dunnett's Overall Result ChV Stets Survive! Growth Conc. Critical Calculated Critical Calculated 31 10 20 2.41-1.1778 46.5 10 22 2.41-2.5604 62 10 21 2.41-1.2566 81 10 19.5 2.41-1.3038 100 10 21 2.41-1.3787 C4;F1mvenf TAvrnifai DAMfPfrf C#%rm_Phrnniw C•ft+MwftA RA-Ut T--& nfti4-mmn17n47 1-455MV••� ■ vA§VV%Y a%%EtfWV% • 1 I VM9IV I RNGIUiiN INN If INIV YY I ILI i11,IV1 I I VOL ■ -%W.v..v.LV 61 Facility: WSACC NPDES # NC00 36269 Pipe * 001 -County: Cabarrus Laboratory: Meritech, Inc. Comments x Signature of Operator in espvnsibi Charge x %' "� c Signature of Laboratory Supervisor MAIL ORIGINAL TO: Water Sciences Section Aquatic Toxicology Branch Division of Water Resources 1621 Mail Service Center Raleigh, N.C. 27699-1621 Test Initiation DatelTime 8/1/2017 4:15 PM % Eff. Repl. 1 2 3 control I Surviving # Original # Wt/odginal (mg) A Avg Wt/Surv. Control 0.856 10 10 10 9 10 i0 10 10 0.870 0.813 0.895 0.762 31 Surviving # Original # Wt/odginal (mg) 46.5 Surviving # Original # Wt/odginal (mg) 62 Surviving # Original # Wt/original (mg) 10 10 10 10 10 10 10 10 0.781 0.812 0.800 0.936 10 9 10 9 10 10 10 10 1.017 Q.782 0.875 0.877 81 Surviving # Original # Wt/odglnal (mg) 100 Surviving # Original # Wt/odginai (mg) Water Quality Data Control 0 1 2 pH (SU) Init/Fin DO (mg/L) In€ Mn Temp (C) Init/F€n High Concentration o 1 2 pH (SU) Init/F€n DO (mg/L) InlUFin Temp (C) lnit/Fln Sample 1 2 3 Collection Start Date Grab Composite (Duration) Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) Chlorine(mg/L) Temp. at Receipt (°C) 10 10 1Q 9 10 10 10 10 0.801 0.856 0.978 0.706 Day % Survival 97.5 Avg Wt (mg)[__0.835 % Survival 97.5 Avg Wt (mg) 0.782 % Survival 100.0 Avg Wt (mg) 0.832 % Survival 95.0 Avg Wt (mg) . 0.890 % Survival[___100.0 Avg Wt (mg) 0.877 % Survival 97.5 Avg Wt (mg)0.835 3 A 5 Test Organisms Cultured In -House Outside Supplier Hatch Date: 7/31/17 Hatch Time: 3:00 pm CT 8.15 / 7.94 8.13 / 7.66 8.19 / 7.92 8.28 / 7.94 8.15 / 7.87 8.20 / 7.87 8.15 / 7.67 8.12 / 7.15 7.79 / 6.40 8.03 / 6.84 7.80 / 7.25 7.98 / 7.01 8.00 / 6.81 7.83 / 6.84 24.4 / 25.0 24.5 / 24.8 24.2 / 25.0 25.8 1 24.9 25.8 / 24.9 24.1 / 25.8 24.4 / 24,7 3 4 6 6 6.68 / 7.44 6.95 1 7.47 6.91 / 7.77 7.01 / 7.70 6.90 / 7.69 7.08 / 7.75 6.99 / 8.49 8.45 / 6.95 7.97 / 6.33 8.29 17.01 8.73 1 6.98 8.42 / 6.95 7.98 / 7.12 8.33 / 8.79 24.2 / 25.0 24.6 / 24.8 25.2 1 24,5 24.1 / 25.2 124.3 / 24.2 25.0 / 24.5 125.2 / 25.2 7/31/2017 8/2/2017 8/3/2017 24.1 24.1 24.4 98 128 128 42 64 61 619 664 663 <0.1 <0.1 <0.1 2.1 2.6 1.3 Dilution H2O Batch # 1185 1186 Hardness (mg/L) 44 42 Alkalinity (mg/L) 51 53 Conductivity (umhos/cm) 119,11205 Survival Growth Normal jiW"� �i Hom. Var. n (fr NOEC 100 100 LOEC >100 >100' ChV >100 >100 Method Steel's Dunnett's Overall Result ChV >100 Stats Survival Growth Conc. Critical Calculated Critical Calculated 31 10 18 2.41 0.9523 46.5 10 20 2.41 0.0494 62 10 16 2.41-0.9927 81 10 20 2.41-0.7502 100 10 18 2.41-0.0045 10 10 10 9 10 10 10 10 0.605 0.809 0.786 0.728 10 i0 10 10 10 10 10 10 0.977 0.892 0.825 0.813 -�-� Effluent Toxicity Report Form -Chronic Fathead Minnow Multi -Concentration Test Date:11/17/2017 Facility: WSACC Laboratory: Meritech, Inc. x Signature of Operator in Responsible Charge X Signature of Laboratory Supervisor NPDES # NC00 36269 MAIL ORIGINAL TO: Water Sciences Section Aquatic Toxicology Branch Division of Water Resources 1621 Mail Service Center Raleigh, N.C. 27699-1621 Test Initiation Date/T€me 11/7/2017 4:40 PM °% Eff. Repl. 1 2 3 Control I Surviving # Original # Wt/odginal (mg) 31 Surviving # I gtnal # Wt/original (mg) 46.5 Surviving # �__ Origina! # Wt/original (mg) 62 Surviving # Original # Wt/odginal (mg) 81 Surviving # Original # Wt/original (mg) 100 Surviving # Original # Wt/odginal (mg) Water Quality Data Control 0 1 2 pH (SU) Init/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin Pipe#: 001 County: Cabarrus Avg Wt/Surv. Control 0.882 10 10 10 10 10 10 10 10 0.881 0.840 0.909 0.899 10 10 10 10 10 10 10 10 0.869 0.877 0.824 0.900 10 10 10 10 10 0.888 10 0.882 10 0.9fi0 10 0.920 10 10 10 10 10 10 10 10 0.972 0.958 0.848 0.833 10 10 10 10 10 10 10 10 0.910 0.861 0.893 0.687 10 10 10 10 10 10 10 10 0.995 0.933 0.899 0.982 Day °% Survival 100.0 Avg Wt (mg) 0.882 % Survi vall 100.0 Avg Wt (mg)l 0.868 % Survival 100.0 Avg Wt (mg) 1 0.913 °% Survivall 100.0 Avg Wt (mg) I 0.903 °% survival 100.0 Avg Wt (mg)l 0.838 % Survival 100.0 Avg Wt (mg) 0.952 3 4 5 Test Organisms C Cultured In -House 17 Outside Supplier Hatch Date: 11 i6/17 Hatch Time: 3:00 pm CT 8.09 / 7.91 8.16 / 8.09 8.15 / 7.70 8.05 / 7.79 8.15 / 7.94 8.20 J 7.99 6 8.22 / 7.66 7.85 / 6.24 7.85 / 6.95 1 7.58 / 6.40 1 7.71 / 6.98 1 8.08 / 7.24 1 8.00 / 7.10 124.2 7.74 J 5.79 24.3 J 25.0 24.4 / 24.3 25.5 / 24.2 25.3 / 25.3 24.7 / 24.1 / 25.3 24.7 / 24.3 High Concentration 0 1 2 3 4 5 pH (SU) Init/Fin DO (mg/L) Init/Fln Temp (C) Init/Fin 6.63 / 7.50 6.82 / 7.72 6.90 / 7.48 7.17 / 7.59 6.97 / 7.51 7.01 / 7.62 8 7.01 / 7.61 8.51 J 6.00 7.94 17.18 8.36 / 6.06 7.67 / 6.88 8.38 / 6.53 8.03 / 6.89 8.14 / 6.65 1 24.7 / 25.1 25.0 / 24.8 25.3 / 24.8 24.2 / 25.1 24.1 / 24.6 24.8 / 24.7 25.3 / 25.7 Sample 1 2 3 Collection Start Date Grab Composite (Duration) Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) Chlorine(mg/L) Term. at Receipt (°C) 11 /6/2017 11 /8/2017 11 /9/2017 23.8 24.1 24.0 94 118 122 44 55 52 595 644 658 <0.1 <0.1 <0.1 1.7 2.0 0.7 Dilution H2O Batch # 1214 1216 1216 Hardness (mg/L) 42 44 48 Alkallnity (mg/L) 53 51 55 Conductivity (umhos/cm) 210 183 223 Survival Growth Overall Result Normal P-1 P1 ChV >100 Hom. Var. ri P1 NOEC 100 100 LOEC > pp >> �p ChV >~ 100 >` 10p - Method Steel's Du_ Stats Survival Growth Conc. Critical Calculated Critical Calculated 31 10 18 2.41 0.0148 46.5 10 18 2.41-0.0302 62 10 18 2.41 -0.0205 81 10 � 18 - 2.41 � 0.0445 100 10 18 2.41-0.0700